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HomeMy WebLinkAboutNCG240016_MONITORING INFO_20181029MiLD STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /v DOC TYPE ❑HISTORICAL FILE MONITORING REPORTS DOC DATE ❑ c� v I � J 0 a YYYYMMDD Quarterly_Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 10/22/2018 CERTIFICATE OF COVERAGE NO. NCG240016 SAMPLE COLLECTION YEAR 2018 FACILITY NAME Mecklenburg County Compost Central SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept COUNTY Mecklenburg County or ® Monthly' October (month) PERSON COLLECTING SAMPLES Khaliem Adams - RErDIS IH�INARRGING TO CLASS ❑ORW ❑HQW [:]Trout ❑PNA LABORATORY: Pace Analytical Services Lab Cert. # 92 ❑Zero -flow ❑Water Supply ❑SA Comments on sample collection or analysis: OCTZ 201$ ❑Other CEN T i;�Atl_ FILE' DWPA SECTION Part A: Stormwater Benchmarks and Monitoring Results ❑ Oct -Dec Total event rainfall z 2.78 in or ❑ No discharge this period3 Date Sample Colle Collected' (mo/ cted Outfall No. T55 COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks 100 mg/L' 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 10/12/2018 2 4.3 69.8 6000 7.9 0.19 0.0072 0.0050 0.015 6.6 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. s For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part ti: venicie maintenance Area ivionitoring KesulTs: only Tor Tacimies averaging 7 55 gal oT new mot Date Sample Collected' (mo/dd/yr) outfall No. pH TPH using method 1664A SGT-HEM TSS Total Rainfal12 -Check - if No Flow This Period; Average New Motor Oil Usage 6-9 15 mg/L 100 mg/L4 - - - 1 - - _ - X 75 gal/month 10/12/2018 2 6.6 <5.0 <4.8 2.7 Footnotes from Part A also aonlV to this Part B Dr oil/month. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. + TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ No REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an oriainal and one coov of this DMR, includina all "No Discharae" reports, within 30 days of receiat of the lab results (or at end of monitorina period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature o/P01-11/'2011-9/30/2016 mrftee) t Y Permit Date /c, 7 Z (Date) Last Revised 12/02/11 Page 2 of 2 aceAnalytical wwwpac�labs.wm October 18, 2018 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92403258 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on October 12, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste AccaF4�T`a TNI REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L.LC, Page 1 of 20 Environmemai Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisform, please visit littps://deg.ne.eov/about/divisions/eneray-mineral-land- resources/energy-mineral-land-permitslstorniwater-permitslnpdes-industrial-sw#tab-4 pp Permit No.: NICIGI o(l l l l l d/ or Certificatc of Coverage No.: N/C/GIa/- I/,q I-LI61 Facility Name: County: Inspecto Date of "Time of' "Total Event Precipitation (inches): Lv+r St 60AAff All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site Outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-11our storm interval does not apply if the permittee is able to document that a shorter interval is representative fbr local storm events during the sampling period, and the permittee obtains approval from the local DEMLIZ Regional Office. By this signature, 1 certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: pipe lOutfall No. a Structure (pipe, ditch, etc.):t! Receiving Stream: Desfri�e the industrial activities that occur within the Outfall drainage area: Page i of 2 SWU-242, Dist modified 07/29/2017 2. Color: Describe the color of tl c disc 3arge u (light, medium, dark) as descriptors: �t + — basic colors (red, brown, blue, etc.) and tint -own 3. Odor: Describ anv distinct odors that the discharge Lnay have (i.e., smells strongly of oil, weak Chlorine odor, etc.): _ � f Q � k 'k � L 7-e-r slr� 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 20 3 4 5 5. floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge. where l is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stonmvater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 / IkS7. Is there any foam in the stormwater discharge? 05 Yes O No. 8. Is there an oil sheen in the stormwater discharge? OYes (940. NO 9. Is there evidence of erosion or deposition at the outfall? O Yes v No. a to. Other Obvious Indicators of Sttormwater Pollution: List and describe No 0 l rrstiCJ' V' r_ Q.(�Jlit � _s Note: Lois clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S WU-2d2, Las/ modified 07/28/2017 Pace Analytical Services, LLC aceAnalytical 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 _pamiabs.com (704)875-9092 CERTIFICATIONS Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92403258 Charlotte Certification IDs 9800 KinceyAve, Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 F)orida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Fietd Services Certification #: 5342 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NCO30 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 20 aceAnalylical wwwpacelabs.cam SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: COMPOST CENTRAL 1-WEST BLVD 92403258 Analytes Lab lD Sample ID Method Analysts Reported Laboratory 92403258001 OUTFALL 002 EPA 1664B JMS 1 PASI-C EPA200.7 Rev4A 1994 SH1 3 PASI-A SM 9222D-2006 KDF 1 PASI-C SM 254OD-2011 CEH 1 PASI-A EPA 9040C RLO 1 PASI-A TKN+NO3+NO2 Calculation KDF1 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2,0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 GC 1 PASI-A SM 5220D-2011 GC i PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 20 aceAnalytical -pacafabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Sulte 100 Huntersviile, NC 28078 (704)875-9092 Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92403258 Sample: OUTFALL 002 Lab ID: 92403258001 Collected: 10/12/18 09:52 Received: 10/12/18 10:33 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 16646 Total Petroleum Hydrocarbons ND mgll- 4,8 1 10/17/18 01:52 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper 0.0071 mg/L 0.0050 1 10/13/1813:45 10/14/1819:33 7440.50-8 Lead ND mg/L 0.0050 1 1011311813:45 1011411819:33 7439-92-1 Zinc 0.015 mg/L 0.010 1 10/13/1813:45 10/14/1819:33 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-20D6 Fecal Coliforms 6000 CFU1100 mL 1.0 1 10/12/18 15:53 10/13/18 17:13 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 4.3 mg/L 2.5 1 10/16/18 02:39 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.6 Std. Units 0.10 1 10/16/18 05:41 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 7.9 mg/L 0.52 1 10/18/18 14:54 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 2.1 mg/L 0.50 1 10/14/18 14:41 10/16/18 01:14 7727-37-9 353.2 Nitrogen, NO2lNO3 pres. Analytical Method: EPA 353.2 Rev 2.D 1993 Nitrogen, NO2 plus NO3 5.7 mg/L 0.04D 2 10/17/18 10:55 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.D 1993 Phosphorus 0.19 mg1L 0.050 1 10/16/18 19:00 10/17/18 01:28 7723-14-0 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 69.8 mg1L 25.0 1 10115/18 20:00 10/16/18 20:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/18/2018 02:58 PM without the written consent of Pace Analytical Services, LLC. u2 H3 Page 4 of 20 aceAnalytical _pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92403258 QC Batch: 436564 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92403258001 METHOD BLANK: 2401908 Associated Lab Samples: 92403258001 Parameter Units Total Petroleum Hydrocarbons mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 4.8 10/17/18 01:42 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2401909 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg[L 19.2 20.1 104 64-132 MATRIX SPIKE SAMPLE: 2401910 35423403002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L 4,81-1 19.2 21.4 111 64-132 Results presented on this page are in the units Indicated by the "units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1Oil 8/2018 02:58 PM without the written consent of Pace Analytical Services, LLC, Page 5 of 20 IeAnalytical www pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92403258 Pico Analytical Services, LLC 9800 Kincey Ave, Suite 1 DO Huntersville, NC 28078 (704)875-9092 QC Batch: 436114 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92403258001 METHOD BLANK: 2399809 Matrix: Water Associated Lab Samples: 92403258001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper mg/L ND 0.0050 10/1411818:46 Lead mglL ND 0.0050 1011411818:46 Zinc mg/L ND 0.010 10/1411818:46 LABORATORY CONTROL SAMPLE: 2399810 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mglL .5 0.52 103 85-115 Lead mglL .5 0.49 98 85-115 Zinc mglL .5 0.49 98 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399811 2399812 MS MSD 92403064001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc, Result Result % Rec % Rec Limits RPD Qual Copper mglL 2.6 .5 .5 3.1 3.2 82 105 70-130 4 Lead mglL 0.0050 .5 .5 0.52 0.53 102 106 70-130 3 Zinc mglL 1.7 .5 .5 2.3 2.3 104 122 70-130 4 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399813 2399814 MS MSD 92403281001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mglL 8.9 uglL .5 .5 0.53 0.54 105 106 70-130 1 Lead mg/L ND .5 .5 0.51 0.51 101 101 70-130 0 Zinc mg1L 33.9 .5 .5 0.55 0.55 104 104 70-130 0 uglL Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/18/2018 02:58 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 20 aceAnalytical� x mv.pacelabs.com Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92403258 QC Batch: 436043 QC Batch Method: SM 9222D-2006 Associated Lab Samples: 92403258001 METHOD BLANK: 2399587 Associated Lab Samples: 92403258001 Parameter Units Fecal Coliforms CFU1100 mL SAMPLE DUPLICATE: 2399586 Parameter Units Fecal Coliforms CFU1100 mL QUALITY CONTROL DATA Analysis Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF) - CHT Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 10/13/1817:13 924D3209001 Dup Result Result 6000 600 RPD Qualifiers 164 D6.u2 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/18/2018 02:58 PM without the written consent of Pace Analytical Services, LLC Page 7 of 20 aceAnalytrcal® —pocelabs.ccm QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92403258 QC Batch: 436341 Analysis Method: SM 2540D-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 25400 Total Suspended Solids Associated Lab Samples. 92403258001 METHOD BLANK: 2400752 Matrix: Water Associated Lab Samples: 92403258001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 10/16/18 02:36 LABORATORY CONTROL SAMPLE: 2400753 Parameter Units Total Suspended Solids mglL SAMPLE DUPLICATE: 2400754 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2400755 Parameter Units Total Suspended Solids mg/L Spike Conc. 251 92403318001 Result 2440 LCS LCS Result % ReC 246 98 Dup Result 2140 92402710007 Dup Result Result ND ND Pace Analytical Services, LLC 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 % Rec Limits Qualifiers 90-110 RPD Qualifiers 13 D6 RPD Qualifiers Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full. Date: 10/18/2018 02:58 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 20 aceAnalytical www.pacelabs.cvm QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92403258 QC Batch: 436345 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92403255001 SAMPLE DUPLICATE: 2400761 92403054001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 7.3 73 0 H3 SAMPLE DUPLICATE: 2400762 92403281002 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 6.3 6.3 1 H3 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 2807E (704)875-9092 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 10/18/2018 02:58 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 20 aceAnalytrcal wew.pacaiabs.com Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92403258 QC Batch: 436148 QC Batch Method: EPA 351.2 Rev 2.0 1993 Associated Lab Samples: 92403258001 METHOD BLANK: 2399875 Associated Lab Samples: 92403258001 Parameter Units Nitrogen, Kjeldahl, Total mg/L LABORATORY CONTROL SAMPLE: 2399876 Parameter Units Nitrogen, Kjeldahl, Total mg1L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 QUALITY CONTROL DATA Analysis Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 10/16/18 00:56 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 10 9.4 94 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399877 2399878 MS MSD 92402844001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg1L 11 10 10 9.7 10.9 86 98 90-110 11 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399879 2399880 MS MSD 92403137001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qua( Nitrogen, Kjeldahl, Total mg/L 4.8 10 10 15.5 15.6 107 109 90-110 1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/18/2018 02:58 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 20 I eAnalytical wwcpacefabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92403258 QC Batch: 436373 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: , 92403258001 METHOD BLANK: 2400847 Associated Lab Samples: 92403258001 Parameter Units Nitrogen, NO2 plus NO3 mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.020 1011711810;15 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2400848 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg1L 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2400849 2400850 MS MSD 92402332002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg1L 4.0 2.5 2.5 6.0 6.0 82 81 75-125 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2400851 2400852 MS MSD 92402419001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.24 2,5 2.5 1.6 1.6 55 55 75-125 1 M1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1011812018 02:58 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 20 aceAnalytical Innrpacelabs.taorrr QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92403258 QC Batch: 436494 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.01993 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92403258001 METHOD BLANK: 2401745 Matrix: Water Associated Lab Samples: 92403258001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 10/17/18 01:13 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NG 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2401746 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.6 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2401747 2401748 MS MSD 92403453001 • Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Phosphorus mg/L ND 2.5 2.5 2.6 2.5 103 102 90.110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2401749 2401750 MS MSD 92403209001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus rng/L 0.81 2.5 2.5 3.5 3.4 108 105 90-110 2 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/18/2018 02:58 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 20 I eAnalytical tnvwpacolabs.�m QUALITY CONTROL DATA Project: COMPOST CENTRAL. 1-WEST BLVD Pace Project No.: 92403258 QC Batch: 436319 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92403258001 METHOD BLANK: 2400688 Associated Lab Samples: 92403258001 Parameter Units Chemical Oxygen Demand mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 10/16/18 20:08 Pace Analytical Services, LLC 9800 Klricey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2400689 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mglL 750 751 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2400690 2400691 MS MSD 92403094001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua] Chemical Oxygen Demand mg/L 69.8 100 100 209 190 140 121 90-110 9 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2400692 2400693 MS MSD 92403287002 Spike Spike MS MSD MS MSD % Rer Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 27.2 100 100 157 148 130 121 90-110 6 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/1812018 02:58 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 20 aceAnalytical —pacelabs.com QUALIFIERS Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92403258 DEFINITIONS Pace Analytical Services, LLC 9800 Kiacey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, it reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting Emit. MDL -Adjusted Method Detection Limit. PQL- Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used 10 calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Niirosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/18/2018 02:58 PM without the written consent of Pace Analytical Services, LLC, Page 14 of 20 I eAnalytical snvwpacelabs.c= QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92403258 Lab ID Sample ID QC Batch Method QC Batch 92403258001 OUTFALL 002 EPA 1664B 436564 92403258001 OUTFALL 002 EPA 200.7 Rev 4.4 1994 436114 92403258001 OUTFALL 002 SM 9222D-2006 436043 92403258001 OUTFALL 002 SM 254OD-2011 436341 92403258001 OUTFALL 002 EPA 9040C 436345 92403258001 OUTFALL 002 TKN+NO3+NO2 437006 Calculation 92403258001 OUTFALL 002 EPA 351.2 Rev 2.0 1993 436148 92403268001 OUTFALL 002 EPA 353.2 Rev 2.0 1993 436373 92403258001 OUTFALL 002 EPA 365.1 Rev 2.0 1993 436494 92403258001 OUTFALL 002 SM 5220D-2011 436319 Date: 10/18/2018 02:58 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Analytical Method Batch EPA 200.7 Rev 4.4 1994 436138 SM 92221)-2006 436044 EPA 351.2 Rev 2,0 1993 436330 EPA 365.1 Rev 2.0 1993 436541 SM 5220D-2011 436532 Page 15 of 20 Document Name: Document Revised: February 7, 2019 Sample Condition Upon Recei t(SCUR) Page 1 of 2 _ aceAnalytical Document No.: Issuing Authority: F:CAR=CS=033-Rev.06 —__ Pace.Carollnas Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Hunterwille [ Raleigh❑ Mechanicsville❑ smClient Name: protect W® : 9240325V Courier: ❑fedE��❑nUJt Co/%1��Z I;ent��1111111111111 I�'i ❑ Commercial []Pace❑Other: 92403258 Custody Seal Present? ❑Yes No Seals Intact? []Yes No J� q Date/initials Peron ENaminingCantenu: Packing Material: ❑Bubble wrap []Bubble Bags None ❑ Other elolcglcal Tissue Fr zen? Thermometer, ❑Yes ❑No NIA IR Gun ID: 92TO45 Type of tcD: [ et []Blue ❑None Cooler Temp ('Cl: 1.3 Correction Factor: Add/Subtract (°C) _ Temp should be above freezing to fi'C Cooler Temp Corrected ('C): El Samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Soll {Q NJA, water samplel Dld samples orriiginaatt in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Intern tionally, j7Yes t�f a including Hawaii and Puerto Ricol? nYes i'fNo Comments/Discro ant : Chain of Custody Present? (rYes ❑No NIA I. Samples Arrived within Hold Time? Ca<s ❑No []N/A 2. Short hold Time Analysis (e72 hr.)? Yes a ❑N/A of. Q�� Rush Turn Around Time Requested? Yes Na ❑N/A 4. Sufficient volume? es QND ❑NJA S. Correct Containers Used? -Pace Containers Used? Glle�s 2:Ces [:]NO ❑ND ❑NIA ❑NJA 6. Containers Intact? oKs No rIJA 7. Dissolved analysis: Samples Field Filtered? ❑Ye []NO 21,14,A a. Sample Labels Match COC? •includesDatefrime/ID/Analysis Matra: Yes �-�/ []NO []N/A 9. Heads ace in VOA Vials (>S-bmm)? ❑Yes QND NJA 10. Trip Blank Present? Trip Blank Custody Seals Present? []Yes ❑Yes ❑No ❑No NIA VfNJA 11. COMMENTS/SAMPLE ,DISCREPANCY Field Data Required? ❑Yes ❑No Lot ID of split containers: CLIENT NOT IFICATIONJRESOLUTtON - - - - - - - - - — Person contacted: Date/Time: Project Manager SCURF Review: A Date: to "l, �Gf Project Manager SRF Review. Date: I Page 16 of 20 •��dcefvraF,dira! CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. SocVon A Section B Section C jI Required Client Information: Required project Information_ Invoice Information: Pa e : I Of i 1 Company: MeckJenburg County Solid Waste lReport To: Khaliem Adams Attention: Address: 2145 Sultle Ave ICapy To: Company Name: Chariotle. NC 28208 {1 Address: Regulatory A enc Email; khafiem.adamS mecklenbur count nc. iov Purchaso Ofder#: Pace Quole: Phone: (704) 634-7705 IFax Project Name: Compost Central i-West Blvd Pace Project Manager: matthew.brainard acelabs.COm .State'I I.ocatlan . - Requested Due Date: IProject #'. Pace Prol'Ia P. 3207-1 NC I Rectuested Anal sls Filtered YIN ' - +oar ix coot: ° `o COLLECTED r Preservatives � pl by w,�a. vx Wai r WT V o U Ws- eYfula P Pltrtl SAMPLE ID �° a L9 C START END 0 r 'N' O Z o _ Z as One Character per box. '^! VVP w w a = oNi- N it Z z lJ o C o # (A-2.0-91. ) Sample Ids must be unique °l," os x ,~„ J o LL 61 < NO N c A v �G Lj�"J z H n roil Z U O J DATE TIME DATE TIME 1 Outfall OC1 WT X X X X X X I 11'y f? r�/ V 3 c� q } nx 2 Ovtlall OC2 WT V 1 C (T i G t,:'1 U X X X X X X X V 3� •4 I 5 E 6 I I 7 I I 8 3 I 9` 10,12 j >� '', NAODIifONAL COMMENTSs a -• �•'• •, - 'REUNOGISHEDBY[AFF[UJ TlOt DATE -..TIME,-,y f7. AGCEP.7E AFFIUAiiDN� - DAILY. Y, TIME• SAMPLE, CONDmONS •I ,,, C4l2-A, I SAh'iPLERNAMEAND-SIGNATURE! m PRINT Name -of SAMPLER: r. 7 u z z_ E z SIGNATURE of SAMPLER ' : PATE Signed: /r) / % 7 Document Name: Oapument Revised: February 7, ndltlod UP arr ReeNpl(SCUIII _ pII$e s of ] Oacument No.' Issuing Authority, Laboratory receiving samples: Asheville ❑ Eden© Greenwood ❑ Huntersvllle Raleigh❑ Mechanlcsvllle❑ GlrntNeme: WO# : 92403258 y CO!Project Cavdar: ❑Fed E. LJUPS f TUSPS Dien[ �I�I�■ II l I1�1 I� I �I� ❑ Commercial ❑Pace ❑other._ 92403258 Custody Seal Present? ❑Yes No Seahintac[? %]Yes BNo OelaJln40[b lerwn Eramining Cantert4: Packing Material: QBubble wrap ❑eubble gags Nane 0 Othet Illolaglral Tissue Fr un7 Thermo ie m 10. 4vn 10' 92TO45 TYpl of ire: F�K.t ❑61ue a.,[]NO11 ❑None Cooler Temp {'CI: 1. 3 Correctlon Factor:Add/Subtract r'1 Temp sdaWd be above Ireenng to VC Cooler Temp Conected('Ll: Li;7 ❑s—Ples ut of Tema uiceria.5ampies on T, wolma P—... USDA Regulated Soil I N/A, water samplel has xauo Did$ —Pie' oTl�o at ina 9uarantlne no"Within the United Stater: CA NY, ar SC kheci nupsi? f--iv. r� Dtl)a HClll a+iElnatl Frenitoreen a4erCe lime+y d"My. ... ..$)f7v.. r7r�.. CammMls/DHRS Ch]In of Cuslotl Present? No C1.1. 1. 5am les Ardred wltNn Hold Tlrne? :zo N1A Shod Hold Time Ana Is 102 hr.)T re o ci.,— RuahTumAroundnreRequested? ro JA 4. sulfkient vow— -4 uas UwA S, Carrert Conlaine,S Used? -Pee! ccmalner5 Used? ryes gf, ❑No Na ❑fvA -41A 6, Cantarners lntatll H Mis, rarA 7. Dissolved anal pli:5am les Field Filtered! Ye No NIA A. Sample labels Match COC? .In CfudeT OaSe/Time IOJAnily511 Matrix: res ^+ QNn DJA 9. Head! ate n VOA Vla11()5-6—)) OYcl OND N(A 10 Trip glank Present? Trip glans, Custod 5ea15 Pt? re1M ❑7n Yer Uii) N) N(A talA 11, COMMENTSJSAMPIC DISCREPANCY Field Deis Apiairedl ❑Yes ❑Na is iO of salicionsauwr— CUFHT NO"FICATIONIRESOLUTION Person contacted: Date(Tinse: r Prolacl MmIger SCURF R.O.- Dale: Rroleet Manager SRF Review: KA Date: 'Irl IS � i Page 18 of 20 __� aCf%AIf31ylC3i� Ocaumem Name. Sam le CopdAIan UP" R"elt(SCl1R Uocumenc Rellsed: February 7, 2018 va etol2 pocument Na.: FC4RCS-033Aev.06� Issuing Authorltr Pace Carallaas 4uali—Offcc 'Check mark top half of box If pH and/or dech(orinatlon is verified and within the acceptance range for preservation samples. Eaceptlans: VOA, Caafafm, Tor, pd and Grease, 09019015 Iwattq OOC, LLHS ieBottom half of box Is to list number of battle Project WO# : 92403258 PM: MWB Out Dale: 10/19/18 CLIENT- 92—MECK CO 01 Limon 01141 NO IN NOME 0 son NEON ON mom 110ROM 0 N 'I -in 'INS ON on MONVIVINSO IMMENVIONS HOMES man mom mom ONMENROMME NONE MEMEMOMMOOME 0 SzONSI pH Adjustment Log for Preserved 5amples F.mple In rawer P.... retie pH upe--Iat 0... pr ,.IWnadluated Tlme PrefeMSlan .dle.tee Anounl of Pre —uw: edd.d lots Ne- Whenever there n a da CNP ancy Itrlctna N W I Laro.- —prance Sam pees, a co DV or the corm will oe xnt to tt�e Npnn Latour. uIMN. un•neiapn V nK! V-e. 0V1 of hpld,nc_10.......t Ne, out of temp,..—'.. conU—s, t Pape 19 of 20 11 CHAIN -OF -CUSTODY! Analytical Request Document The Chain-ol-C-tady is a LEGAL DOCUMENT. AM reievanf fields must be campfeted a=1Ml ly. s«swn a s.��n o sworn c Rwuir.tl GR.m kifarm.Lon. R.WIrM Prvlwllnbrm.Spn: Mroi[. Mrorma . I SAMPLE ID IMMEMEMESSISsm mom son mmmom �i �III I onions MEMO I " E f 6f $pM1VPLER: }' ri 1ll . l f � pN $$ 3$y d4TE V 1 o Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 4/27/2018 CERTIFICATE OF COVERAGE NO. NCG240016 SAMPLE COLLECTION YEAR 2018 FACILITY NAME Mecklenburg County Compost Central SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec COUNTY _Mecklenburg County or ® Monthly' September (month' PERSON COLLECTING SAMPLES �Khaliem Adams DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY: Pace Analytical Services Lab Cert. # 92 C ���, rC� ❑❑Zero -flow ❑Water Supply [:]SA Comments on sample collection or analysis: G V G Other Sip .21 201S CENTRAL FILES Part A: Stormwater Benchmarks and Monitoring ReVfsSECTION Total event rainfall z 0.82 in or ❑ No discharge this period' Date Sample Cal Collected (molected ) Outfall No. TSS COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks ===> 100 mg/L' 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 9/10/2018 2 16.6 120 13.0 1.6 1.7 0.014 <0.0050 0.066 6.4 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/l/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Fart 13: venicie maintenance Area monitoring Results: only Tor Tacmues averaging > 55 gal OT new mot - Date Sample 1 Collected (mo/dd/yr) - - Outfall No. - pH TPH using method 1664A SG%NEM TSS Total RainfalE z Check- if No Flow This Period' - - Average New Motor Oil Usage 6-9 15 mg/L 100 mg/L4 - - - 1 - - - - X 75 gal/month 9/10/2018 2 6.4 <5.0 16.6 0.82 Footnotes from Part A also aoolv to this Part B FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. or oil/month. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an original and one copy of -this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results tor at end of monitoring period in the case of 'No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." l re P. rmittee) (Da ) te: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 2 of 2 aceAnaV cal www.pacolabs.com September 18, 2018 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: Compost Central 1 Pace Project No.: 92398776 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hurtersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on September 10, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 113 aceAnalytrcal www.pacDlabs.com Pace Analytical Services, LLC 9800 Kimey Ave. Suile 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: Compost Central 1 Pace Project No.: 92398776 Charlotte Certification iDs 9800 Kincey Ave. Ste 100, Huntersvilie, NC 28078 South Carolina Certification #: 99006001 LouisianaiNELAP Certification # LA170028 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 UrginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VrginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 ' m aceAnalytical Kww.pace186s.rvrrr SAMPLE ANALYTE COUNT Project: Compost Central 1 Pace Project No.: 92398776 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HunlersOle, NC 2BD78 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92398776001 Outfall 2 EPA 1664B JDL 1 PASI-C EPA 2007 Rev 4A 1994 SEP 3 PASI-A SM 9222D-2006 KDF 1 PASI-C SM 254OD-2011 CRV 1 PASI-A EPA 9040C RLO 1 PASI-A TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 BRJ 1 PASI-A EPA 365.1 Rev 2.0 1993 BRJ 1 PASI-A SM 5220D-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 aceAnalytical wwwpacMiabs.cnm ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Compost Central 1 Pace Project No.: 92398776 Sample: Outfall 2 Lab ID: 92398776001 Collected: 09/10/18 11:00 Received: 0911D118 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mglL 5.0 1 09/1711B 11:45 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 2003 Rev 4A 1994 Copper 0.014 mglL 0.0050 1 09/11/18 04:29 09/13/18 02:47 7440-50-8 Lead ND mglL 0.0050 1 09/11/18 04:29 09113/18 02:47 7439-92-1 Zinc 0.066 mglL 0.010 1 09/11/18 04:29 09113/18 02:47 7440-66-6 MB10 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms 13.0 CFU1100 mL 1.0 1 09110/18 15:50 09111/18 13:57 D6,ul 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 16.6 mglL 5.0 1 09/11/18 20:20 9040 pH Analytical Method: EPA 9040C phi at 25 Degrees C 6.4 Std. Units 0.10 1 09111118 02:57 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 1.7 mglL 0.52 1 09113/18 16:34 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 1.6 mglL 0.50 1 09111/18 11:23 09/13/18 04:39 7727-37-9 353.2 Nitrogen, N021NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 0.081 mglL 0.020 1 09111/18 03:24 R1 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus 1.7 mglL 0.050 1 09/12118 01:44 09/13118 05:01 7723-14-0 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 120 mglL 25.0 1 09/13/18 20:30 09/13/18 23:41 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/1812018 01:07 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 18 aceAnalytical www.p"labs.com Project: Compost Central 1 Pace Project No.: 92398776 QC Batch: 430957 QC Batch Method: EPA 1664B Associated Lab Samples: 92398776001 METHOD BLANK: 2377174 Associated Lab Samples: 92398776001 Parameter Units Total Petroleum Hydrocarbons mg/L LABORATORY CONTROL SAMPLE: 2377175 Parameter Units Total Petroleum Hydrocarbons mg/L QUALITY CONTROL DATA Analysis Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 09117/1811:45 Spike LCS LCS Conc. Result % Rec 20 18.7 94 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 % Rec Limits Qualifiers 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, Date: 09/18/2018 01:07 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 aceAnalytical www.pacalabs.00m Project: Compost Central 1 Pace Project No.: 92398776 QC Batch: 429912 QC Batch Method: EPA 2003 Rev 4.4 1994 Associated Lab Samples: 92398776001 METHOD BLANK: 2372647 Associated Lab Samples: 92398776001 Parameter Units Copper mg/L Lead mg/L Zinc mg/L QUALITY CONTROL DATA Analysis Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed ND 0.0050 09/13/18 02:23 ND 0.0050 09/13/18 02:23 ND 0A10 09/13/18 02:23 Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2372648 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg/L .5 0.49 99 85-115 Lead mg/L .5 0.46 93 85-115 Zinc mg/L .5 0.46 92 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2372649 2372650 MS MSD 92398766001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua! Copper mg1L ND .5 .5 0.50 0.50 99 99 70-130 0 Lead mg1L ND .5 .5 0.45 0.45 90 90 70-130 0 Zinc mg1L 0.045 .5 .5 0.51 0.51 92 92 70-130 0 Results presented on this page are In the units Indicated by the" Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2018 01:07 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 aceAnalytical wwwpecelabs.mm QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 923,38776 OC Batch: 429881 Analysis Method: SM 9222D-2006 QC Batch Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF) - CHT Associated Lab Samples: 92398776001 METHOD BLANK: 2372572 Matrix: Water Associated Lab Samples: 92398776001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Conforms CFU1100 mL ND 1.0 09111/18 13:57 SAMPLE DUPLICATE: 2372573 Parameter Fecal Colforms 92398776001 Dup Units Result Result RPD Qualifiers CFU1100 mL 13.0 40.0 102 D6,u1 Pace Analytical Services, LLG 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2018 01:07 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 ace Analytical www.pacelabs.eom QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92398776 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 430132 Analysis Method: SM 254OD-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92398776001 METHOD BLANK: 2373772 Matrix: Water Associated Lab Samples: 92398776001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 09/11/18 20:13 LABORATORY CONTROL SAMPLE: 2373773 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 246 98 90-110 SAMPLE DUPLICATE: 2373774 92399045001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 2373775 92398826001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 34.6 47A 31 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, Date: 09/18/2018 01:07 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 18 aceAnalytical wwwpacelabs.com Project: Compost Central 1 Pace Project No.: 92398776 QC Batch: 429890 QC Batch Method: EPA9040C Associated Lab Samples: 92398776001 SAMPLE DUPLICATE: 2372606 Parameter Units pH at 25 Degrees C Std. Units QUALITY CONTROL DATA Analysis Method: EPA 9040C Analysis Description: 9040 pH 92398767001 Dup Result Result RPD Qualifiers 6.5 6.4 1 H6 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 2807B (704)875-9092 Results presented on this page are In the units indicated by the "Units" column oxcept where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09118/2018 01:07 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 acMnalytical wwwpacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kircey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Compost Central 1 Pace Project No.: 92398776 QC Batch: 430142 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Associated Lab Samples: 92398776001 METHOD BLANK: 2373815 Matrix: Water Associated Lab Samples: 92398776001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg1L ND 0.50 09/13/18 0429 LABORATORY CONTROL SAMPLE: 2373816 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mgh- 10 9.4 94 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2373817 2373818 MS MSD 92397935001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RFD Qual Nitrogen, Kjeldahl, Total mg/L 29.1 50 50 69.8 64.0 81 70 90-110 9 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2373819 2373820 MS MSD 92398626006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 37A 10 10 38.4 37.7 11 3 90-110 2 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/1812018 01:07 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 aceAnalytical www.pocefabsxom Project: Compost Central 1 Pace Project No.: 92398776 QC Batch: 429917 QC Batch Method: EPA 353.2 Rev 2.0 1993 Associated Lab Samples: 92398776001 METHOD BLANK: 2372667 Associated Lab Samples: 92398776001 Parameter Units Nitrogen, NO2 plus NO3 mg/L QUALITY CONTROL DATA Analysis Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.020 09/11/18 03:17 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2372668 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2372669 2372670 MS MSD 92398776001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.081 2.5 2.5 2.5 2.1 96 82 75-125 15 R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2372671 2372672 MS MSD 92398364001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RFD Qual Nitrogen, NO2 plus NO3 mg11- 4.2 2.5 2.5 7.2 8.2 121 161 75-125 13 M1,R1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2018 01:07 PM wlthout the written consent of Pace Analytical Services, LLC. Page 11 of 18 acmnalytrcal wwwpacelabs.c n Project: Compost Central 1 Pace Project No.: 92398776 QC Batch: 430135 QC Batch Method: EPA 365.1 Rev 2.0 1993 Associated Lab Samples: 92398776001 METHOD BLANK: 2373782 Associated Lab Samples: 92398776001 Parameter Units Phosphorus mglL LABORATORY CONTROL SAMPLE: 2373783 Parameter Units Phosphorus mg1L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 09/13118 04:39 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.6 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLSCATE: 2373784 2373785 MS MSD 92398266001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.25 2.5 2.5 2.8 0.25 102 0 90-110 167 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPL{CATS: 2373786 2373787 MS MSD 92398738002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mglL 0.053 2.5 2.5 2.6 2.6 103 103 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2018 01:07 PM without the written consent of Pace Analytical Services, LLC, Page 12 of 18 QD acmnalytical www.pacelabsxom Project: Compost Central 1 Pace Project No.: 92398776 QC Batch: 430657 OC Batch Method: SM 5220D-2011 Associated Lab Samples: 92398776001 METHOD BLANK: 2376035 Associated Lab Samples: 92398776001 Parameter Units Chemical Oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 2376036 Parameter Units Chemical Oxygen Demand mglL Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 QUALITY CONTROL DATA Analysis Method: SM 5220D-2011 Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 09/13/18 2140 Spike LCS LCS % Rec Conc. Resull % Rec Limits Qualifiers 750 779 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2376037 2376038 MS MSD 92398845001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 30.6 100 100 163 186 133 156 90-110 13 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2376039 2376040 MS MSD 92399249002 Spike Spike MS MSD MS MSD %6 Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 312 100 100 452 424 140 112 90-110 6 M1,R1 Results presented on this page are in the units indicated by the"Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2018 01:07 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 aceAnalytical winvpacelabs.com QUALIFIERS Project: Compost Central 1 Pace Project No.: 92398776 DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method defection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenythydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA required holding time. M1 Matrix spike recovery exceeded QC limits_ Batch accepted teased on laboratory control sample (LCS) recovery_ RI RPD value was outside control limits. u1 Results based upon colony counts outside acceptable range. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full. Date: 09/18/2018 01:07 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 aceAnalytical WWW.Pacelabs.=n QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hurtersville, NC 28078 (704)875-9092 Project: Pace Project No.: Compost Central 1 92398776 Analytical tab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92398776001 Outfall 2 EPA 1664E 430957 92398776001 Outfall 2 EPA 200.7 Rev 4.4 1994 429912 EPA 200.7 Rev 4A 1994 429933 92398776001 Outfall 2 SM 9222D-2006 429881 SM 92221)-2006 429882 92398776001 Outfall 2 SM 2540D-2011 430132 92398776001 Outfall 2 EPA 9040C 429890 92398776001 Outfall2 TKN+NO3+NO2 430663 Calculation 92398776001 Outfall 2 EPA 351.2 Rev 2.0 1993 430142 EPA 351.2 Rev 2,0 1993 430457 92398776001 Outfall 2 EPA 353.2 Rev 2.0 1993 429917 92398776001 Outfall 2 EPA 365.1 Rev 2.0 1993 430135 EPA 365.1 Rev 2.0 1993 430202 92398776001 Outfall 2 SM 5220D-2011 430657 SM 5220D-2011 430719 Date: 09118/2018 01:07 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 18 Document Name: Document Revised: February 7, 2D18 ��CMnafytical' Sample Condition Upon Recelpt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev,06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh[] Mechanicsville❑ ffmamClient Name: / ` Pra act #: W®# : 92398776 I tt� ` - Saf1 Gl [J3 j Courier: ❑Fed Ex ❑UPS ❑LISPS `ent ❑ Commercial ❑Pace ❑Other: I I I Ills © 11 111 923, 776 Custody Seal Present? ❑Yes ON, Seals Intact? ❑Yes CfND Date/Initlels Person Erramining Contents: Packing Material: ❑Bubble wrap ❑bubble Bags QNone ❑ Other Thermometer: 92TO4S ❑� Claw, rr--�a� Type of Ice: �;.IIR Gun IO: Cooler Temp ['Cl: �, �i Correction Factor: Add/Subtract;'q -0 1 Cooler Temp Corrected ('C): USDA Regulated Solt ([ N/A, water samplel Did samples originate in a quarantine zone within the United States: CA, NY, Or SC (check mapsl? nVPc F-1Nn Biological Tissue Frozen? []Yes[:]No[7N/A ❑NOne Temp should be above freezing to 6'C ❑Samples out of temp criteria. Samples en ice, tooling process has begun Old samples origin ate from a foreign source (internatlonally, inc!„dlor Hawaii and Pueno Rimi) r"lYes I-1NO Comments/Discrepancy: Chain Of Custody Present? es No rv/A 1. 5amples Arrived within Hold Time? D<r [:]No ONJA 2, Short Hold Time Analysis (c72 hr.)? eY s QN0, ❑N/A 3. Rush Turn Around Time Re uested? Yes No ❑NIA 4. Sufficient Volume? 5 Yu No QNll S. Correct Containers Used? -Pace Containers Used? - e , Yes ❑No ONO ❑N/A ❑NIA 6. Containers Intact? 0<s No NIA 7. Dissolved analysis; Samples Field Filtered? ❑Yes ❑No EIQA 8, Sample Labels Match COC? •Includes Date/Time/ID/Analysis Matrix: [jyes ❑No ❑N/A 91 Headspace in VOA Vials (>S-6mmi? ❑yes No N-/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes ❑No Elmo ❑N/A f NIA 11. COMMENTS/SAMPLE DISCREPANCY _ Lot 10 of split containers: CLIENT NOTIFICATION/RESCILLITION Field Data Required? ❑Yes []NO Person contacted: Date/Time: /r Project Manager SCURF Review: A Date: Project Manager SRF Review: r Date: Page 16 of 18 _�180 Analytrcal' i Document Name: Sample Canditlon Upon Revel t(SCUR) Document Revised; February 7, 2018 Page 1 of 2 Document No.: F-CAR-CS-033-Rev.06 Issuing Authority: Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is Project # verified and within the acceptance range for preservation samples, Exceptlonsl: VOA, Coliform, TOC, Oil and Grease, DRO/801S (water) DOC, LLHg "Bottom half of box is to list number of bottle wa#:92398776 PM: MW8 Due Date: 09/17/18 CLIENT: 92-MECK CO ma6 O J E .a m U M 7 4 J E N 7 A. m N 7 J J E J�1 0. m ? Z a FL y ri 7 a m lJ N n V Nz S E N rh a m N m Q E N 2 A. �m 0 x ar 2 1 E a as U 0. E M. to 4 v~i o � v a a , a ¢ a 4 V Y V = b a `m ¢ ? 7 W � E a n = a E `cn.m ¢ n v+ E H E ¢ Z d J N N M a a _V 4..! O �! E O Z rn O Q O J S 4 D % 7 2 O a > E O vds � 9 > Q '� j � 9 ] Z u ;; � E m ? u m e, N E m kA ()1 C5 E S m -0 3i j E J E a b o c V1 E N 7 N a�i C E Q C 3 Na z \N- 3 4 N \\N S 6 7 S 9 tD 11 12 N\-- pH Adjustment Log for Preserved Samples Sample ID Type of preservative pH upon receipt Date preservation adjusted Time preservaNan adjusted Amount of Preservative added tot it Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (I.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 17 of 18 4% CHAIN -OF -CUSTODY ! Analytical Request Document FaceArt�yfc31 The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately Section A Section B Section C Required Client Information: Required Project information: Invoice Information: Page : 1 Of i Company. Meck$enburo Counly Solid Waste Report To: Khaliem Adams ALtention: Address 2145 Suitle Ave. Copy To: Company Name: Charlolte, NC 28208 Address, f i Regulatory Agency Email: khaliem.adams meeklenburgcountync.gov Purchasa Ordor 9: Pace Ouoto' phone: f9so)3/4.3056 Fax Project Name: Compost Central I Paco Project Manager: matlhew, brai:wcigbpacelabs.com. ' t f - State / Location Requested Due Date: Project s1: Pace Profile a: 3207.1 NC - 4Ro uested Anal sis FlHered !N •:! ' `i S. p-= a - - W,Tau CODE COLLECTED z Preservatives > ' 0r 1, q W.I. DW 3 U Wale, WT V y Waste Water WW SAMPLE I❑ Od 5v1`tl _ d q v_ START END N F n t F N z o O� One Character per box. W." WP a a = y co o 4t (A-7_ 0.9 f. -) tir Ra 01 e" OT oO V a r _ m 2 n in T a 9 n 2 c- a _ Samp[e ids must he unique T.L— TS 0 m c k U Z A m m o to L L Q. ❑ m C7 l -^7 z>� 7 ~ DATE TLME DATE TIME w � � i i x z z i O � � � to- 6 Gv-0 Im 'VIA Itoo s ly 14xI I X X 1)(IX J X1 I I I 1 vo ly 2. 3•' .'Y71 t t '11• -1'2 ' ADDITIONAL COMMENTS { '+'= r T RFSINOUISHEO BY r AFFIUAT1ON" t DATA TLME -.- •• ACCEPTED 13Y I AFFILIAT!nN -- - ` = DATE"+ -ej'� ME• - - �' '5AMPLL C.ONDITIONSz,'e•�i `- .� SAMPLER NAME AND SIGNATURE O to ❑ C u I m PRINT Name at SAMPLER: %+, i r � z } @ o z y cL = z = > SIGNATURE of SAHiPLER•/ DATE Si9 ned: /1�_��` r7 i� /i _ n ❑ to Environmental Quality Stormwater .Discharge Outfall (SDO) Qualitative Monitoring Report Far guidance on filling ow this form, please visit htt1)s:Hdecl.nc.!ov/about/divisions/energy-minera[-]and- resources/energ �-mineral-land- ermits/stormwater- ermitshi des-industrial-sNN*tah-4 Pcrmit No.: NICI- Facility Name: County: mec�h Inspector: Date ohlnspection: Time of Inspection: Total Event Precipitation (inches): . o All permits require qualitative monitoring to he performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-110ur storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DLMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: n 1 Outfall No. _� Structure (pipe, ditch, etc): Receiving Stream: ribe the industrial activities that occur within the Outfall drainage area: ) Page l of 2 SWU-242, last modified 07/28/2017 2. Color: Describe the color of the di (light, medium, dark) as descriptors: using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe at y distil t odors that the iscl arge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): ' 1[_C 0 -C d 9ie 4. CIarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 2 0 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where i is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 G. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 2 3 0 5 7. is there any foam in the stormy+pater discharge? Yes O No. 8. Is there an oil sheen in the stormwater discharge'? 0Yes �No IV 0 9. Is there evidence of erosion or deposition at the outfall? O Yes VNo. 10. Other Obvious Indicators of Stormwater Pollution: List and describe / U0 Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SW11-242, Last modified 07/28/2017 MECKLENBURG COUNTY Land Use & Environmental Services Agency Solid Waste September 4, 2018 Central Files NCI]hNR / DWQ 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention: Central Files Subject: Discharge Monitoring Report Mecklenburg County Compost Central — Certificate of Coverage No. NCG240016 Dear Central Files: Please find enclosed the Discharge Monitoring Deport, August 2018, for Mecklenburg County Compost Central, a Type I fiacility located at 5631 West Blvd, Charlotte, North Carolina. If you have any questions, please contact me at 704-634-7705 or by email at khalicm.adamscmecklenbur�ycauntync.2� Please note that sampling was conducted on two separate occasions for this month (August 8 and August 28). Due to a Mix-up at the lab, fecal coliform was not included in the original Lab Report. Sincerely, Klhalicm Adams Solid Waste Environmental Specialist: I ncloscd: 2018 DMR PEOPLE_ • PRIDE PROGRESS • PARTNERSHIP 2145 Suttle Avenue Charlotte. North Carolina 28208 11'Ii'1i'. W illeoutlCaStc.Con] Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 4/27/2018 CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME Mecklenburg County Compost Central COUNTY Mecklenburg County PERSON COLLECTING SAMPLES Khaliem Adams LABORATORY: Pace Analytical Services Lab Cert. # 92 Comments on sample collection or analysis: Fecal Coliform sample was taken on 8/28/2018. All other parameters were taken on 8/8/2018 Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec or ® Monthly' August _ (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow [:]watersupply [:]SA ❑Other Total event rainfall 2 0.24 in or ❑ No discharge this period' Date Sample Colle Collected' (mo/ cted Outfail No. TSS COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks ==_> 100 mg/L" 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 8/8/2018 2 10.8 142 - 2.7 0.60 0.016 <0.0050 0.051 6.5 8/28/2018 2 - 809 - - - - - - I Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 rari t3: venicie maintenance Area Ivlonitormg Kesults: only Tor Taclnties averaging > 55 gal oT new mot Date Sample Collected' (mo/dd/yr) Outfall No. pH TPH using method 1664A SGT-HEM TSS Total Rainfallz Check_ if No Flow This Period' Average New Motor Oil Usage 6-9 15 mg/L 100 mg10 - - 1 - - - - X 75 gal/month 8/8/2018 2 6.5 <4.8 10.8 0.24 8/28/2018 0.25 Footnotes from Part A also anoly to this Part B FOR PART A AND PART B MONITORING RESULTS: + A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. or oil/month. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an oriainal and one cony of this DMR. includina all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitorina period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CER►IFIC4TION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penaltigs foL*bmitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permit Dat/ -9/30/2016 y11 S (Date . Last Revised 12/02/11 Page 2 of 2 (�IaceAnalyticaI www.pscelabs.corn August 24, 2018 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92394936 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave, suite 100 Huntersville, NO 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on August 08, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Report was revised and reissued on 08/24/18 to include 200.7 results. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste �p pCCRf��� REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consenl of Pace Analytical Services, LLC. Page 1 of 17 (�IaxAnalytical mmpacelabsmm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92394936 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # L4170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification lDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #. E87627 Kentucky UST Certification #: 84 VirginialVEtAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, t.LC. Page 2 of 17 (�Iacmnal(Xical www.PXelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: COMPOST CENTRAL 1-WEST BLVD 92394936 Analytes lab ID Sample ID Method Analysts Reported Laboratory 92394936001 OUTFALL 002 EPA 1664B JMS 1 PASI-C EPA 200.7 Rev 4.4 1994 KQ 3 PASI-A SM 254OD-2011 CRV 1 PASI-A EPA 9040C SMK 1 PASI-A TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 Rev 2.0 1993 BRJ 1 PASI-A EPA 353.2 Rev 2.0 1993 CJH1 1 PASI-A EPA 365.1 Rev 2.0 1993 BRJ 1 PASI-A SM 5220D-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 17 laneAnalytical' wmvpacefabs.=n ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvllle, NC 28078 (704)875-9D92 Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92394936 Sample: OUTFALL 002 Lab ID: 92394936001 Collected: 08/08/18 10:21 Received: 08108/18 11:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 4.8 1 08/13/18 04:30 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper 0.016 mg/L 0.0050 1 08/18/18 06:20 08/19/18 20:34 7440-5C-8 Lead ND mg/L 0.0050 1 08/18/18 06:20 08/19/18 20:34 7439-92-1 Zinc 0.051 mg/L 0,010 1 08/18/18 06:20 08/19/18 20:34 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 10.8 mg1L 3.3 1 08/09/18 20:34 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.5 Std. Units 0.10 1 08/16/18 14:09 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 2.7 mg1L 0.52 1 08/16/18 15i26 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 2.7 mg/L 0,50 1 08/10/18 04:45 08/14/18 05:16 7727-37-9 353.2 Nitrogen, N021NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 ND mg/L 0.020 1 08/15/18 20:10 365.1 Phosphorus, Total Analytica! Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus 0.60 mg/L 0.050 1 08/09/18 04:57 08/14/18 01:09 7723-14-0 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 142 mg/L 25.0 1 08/09/18 17:43 08110/18 17:59 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fuii, Date: OB/24/2018 03:56 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 17 r aceAnalytrcal w`vw.pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92394936 QC Batch: 424553 Analysis Method: ' EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92394936001 METHOD BLANK: 2348255 Associated Lab Samples: 92394936001 Parameter Units Total Petroleum Hydrocarbons mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 4.8 08/13/18 04:20 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NO 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2348256 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 19.2 19.0 99 64-132 MATRIX SPIKE SAMPLE: 2348257 92394053001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L ND 19.2 19.3 101 64-132 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/24/2018 03:56 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 17 aceAnaVical www.pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92394936 QC Batch: 425725 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92394936001 METHOD BLANK: 2353844 Associated Lab Samples: 92394936001 Parameter Units Copper mglL Lead mg/L Zinc mg/L Matrix: Water Blank Reporting Result Limit Analyzed ND 0.0050 08/19/18 20:28 ND 0.0050 08/19/18 20:28 ND 0.010 08/19/18 20:28 Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2353845 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mglL .5 0.49 99 85-115 Lead mg/L .5 0.47 95 85-115 Zinc mglL 5 0.47 95 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2353846 2353847 MS MSD 92394936001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper rng/L 0.016 .5 .5 0.52 0.53 101 103 70-130 2 Lead rng/L ND 5 .5 0,47 0.48 94 96 70-130 2 Zinc rng/L 0.051 .5 .5 0.53 0.53 95 96 70-130 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/24/2018 03:56 PM without the written consent of Pace Analytical Services, LLC, Page 6 of 17 aceAnaIXical www.pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92394936 QC Batch: 424147 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92394936001 METHOD BLANK: 2346461 Matrix: Water Associated Lab Samples: 92394936001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mgfL ND 2.5 DB109I18 20:28 LABORATORY CONTROL SAMPLE. 2346462 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2346463 Parameter Units Total Suspended Solids mg1L Spike LCS Conc. Result 252 260 92395051001 Dup Result Result 9.4 9.2 SAMPLE DUPLICATE: 2346464 92394938001 Dup Parameter Units Result Result Total Suspended Solids mgfL 5.8 8.5 Pace Analyticat Services, LLC 9800 Kincey Ave, Suite 100 HuntersviiYe, NC 28078 (704)875-9092 LCS % Rec % Rec Limits Qualifiers 103 90-110 RPD Qualifiers 2 RPD Qualifiers 38 D6 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/24/2018 03:56 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 17 laceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92394936 QC Batch: 424520 Analysis Method: EPA 9040C QC Batch Method: EPA9040C Analysis Description: 9040 pH Associated Lab Samples: 92394936001 SAMPLE DUPLICATE: 2348189 Parameter pH at 25 Degrees C 92394817001 Dup Units Result Result Std. Units 7.2 7.2 RPD Qualifiers 0 H6 Pace Analytical Services, LLC 9800 KinceyAve, Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units Indicated by the" Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fuil, Date: 08/24/2018 03:56 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 17 aceAnalytrcal wrvw.pacefabs.ccm Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92394936 QC Batch: 424172 OC Batch Method: EPA 351.2 Rev 2,0 1993 Associated Lab Samples: 92394933001 METHOD BLANK: 2346520 Associated Lab Samples: 92394936001 Parameter Units Nitrogen, Kjeldahl, Total mg/L QUALITY CONTROL DATA Analysis Method: EPA 351,2 Rev 2.0 1993 Analysis Description: 351.2 TKN Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 08/14/18 04:19 Pace Analytical Services, LLC 9B00 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 LABORATORY CONTROL SAMPLE: 2346521 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9A 94 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2346522 2346523 MS MSD 92394831001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L ND 10 10 10.7 10.6 104 103 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2346524 2346525 MS MSD 92394942002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mgJL 1.0 10 10 12.6 12.1 115 111 90-110 3 M1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/24/2018 03:56 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 17 acmnalytical wwwpacelabs oom QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92394936 QC Batch: 425017 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92394936001 METHOD BLANK: 2350412 Associated Lab Samples: 92394936001 Parameter Units Nitrogen, NO2 plus NO3 mg/L LABORATORY CONTROL SAMPLE: 2350413 Parameter Units Nitrogen, NO2 plus NO3 mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.020 08/15/1819:44 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.7 109 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2350414 2350415 MS MSD 92394882011 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.13 2.5 2.5 2.4 2.3 89 86 75-125 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2350416 2350417 MS MSD 92394912004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mglL ND 2.5 2.5 2.0 1.9 78 75 75-125 4 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/24/2018 03:56 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 17 laneAnalyficalv www.pacalabs.cnm QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-VVEST BLVD Pace Project No.: 92394936 QC Batch: 423868 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92394935001 METHOD BLANK: 2345074 Matrix: Water Associated Lab Samples: 92394935001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 08/14118 01:01 Pace Analytical Services, LLC 9B00 Kircey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2345075 Spike LCS I_CS % ReC Parameter Units Cone. Result % Rec Limits Qualifiers Phosphorus mgJL 2.5 2.6 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2345076 2345077 MS MSD 92394853013 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L ND 2.5 2.5 2.6 2.6 104 104 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2345078 2345079 MS MSD 92395050003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.16 2.5 2.5 2.7 2.8 103 104 90-110 1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/24/2018 03:56 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 17 aceAnalytrcal www.pacelabs corn QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92394936 QC Batch: 423799 Analysis Method: SM 5220D-2011 QC Balch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92394936001 METHOD BLANK: 2344761 Associated Lab Samples: 92394936001 Parameter Units Chemical Oxygen Demand mg1L LABORATORY CONTROL SAMPLE: 2344762 Parameter Units Chemical Oxygen Demand mg1L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 08/10/1817:57 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 768 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2344763 2344764 MS MSD 92394660001 Spike Spike MS MS❑ MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 388 100 t00 471 476 83 88 90-110 1 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2344765 2344766 MS MSD 92394595001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 373 100 100 133 140 95 102 90-110 5 R1 Results presented on this page are in the units Indicated by the" Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/24/2018 03:56 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 17 lacmnalyfical' w6mpacafabs.crom QUALIFIERS Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92394936 DEFINITIONS Pace Analytical Services, LLC 980C Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting $imit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA required holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control Emits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 08/24/2018 03:56 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 17 aceAnalytieal wwwpacefabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersviiie, NC 28078 (704)875-9092 Project: Pace Project No.: COMPOST CENTRAL 1-WEST BLVD 92394936 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92394936001 OUTFALL 002 EPA 1664E 424553 92394936001 OUTFALL 002 EPA 200.7 Rev 4A 1994 425725 EPA 200.7 Rev 4.4 1994 425749 92394936001 OUTFALL 002 SM 2540D-2011 424147 92394936001 OUTFALL 002 EPA 9040C 424520 92394936001 OUTFALL 002 TKN+NO3+NO2 425418 Calculation 92394936001 OUTFALL 002 EPA 351.2 Rev 2.0 1993 424172 EPA 351.2 Rev 2.D 1993 424724 92394936001 OUTFALL 002 EPA 353.2 Rev 2.0 1993 425017 92394936001 OUTFALL 002 EPA 365.1 Rev 2.0 1993 423868 EPA 365.1 Rev 2.0 1993 423889 92394936001 OUTFALL 002 SM 5220D-2011 423799 SM 5220D-2011 424163 IMF.3Ca[+II:i�.�P.i�jE:I�X7Fi^.l�y' REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 17 Document Name: Document Revised: February 7, 2018 Sample Condltlon Upon Recel t(SCUR) Page 1 of 2 Document No.: Issuing Authority: aceArral realm F-EAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Cllent Name: Courier: "Fed Ex __— _� ❑ Commertia!—___—❑Pace. _._. _ Huntersville Q Raleigh[—] Mechanicsvllte❑ Packing Material: ❑Bubble Wrap ❑Bubble Bags None ❑ Other Thermometer: Type of ice: � Blue R Gun ID: ��92T040 0 ❑ Cooler Temp ('C): L'— Correction Factor: Add/Subtract {'C} -0.3 Cooler Temp Corrected7.,N/A, : r USDA Regulated Soil ( water sample) Did samples origl5a in a quarantine zone within the United States: CA, NY, or SC (check maps)? FIVpc i`INr, IWO#:92394936 Date/Initlals.Persors Examtning Contents: i iw't"-�� Biological Tissue Fren? ❑Yes [IN,❑N1-A []None Temp OcrGld be above freezing to 6'C Samples out of temp criteria. Samples an Ice, cooling process hasbegun Dld samples originate from a foreign source flntergtivna y, Indudln¢ Hawall and Puerto Rkoi? nYes rlNo Comments/Dlscre ancy: Chain of Custody Present? . Yes CIN. ❑NIA 1. Samples Arrived within Hold Time? EfYes No ❑N/a 2. Short Hold Time Analysis (02 hr.)? []Yes No ❑N!A 3. Rush Turn Around Time Requested? QYes No N/A 4. Sufficient Volume? es No ❑N/A 5. Correct Contalners Used? -Pace Containers Used? ❑ es Yis ❑No No ❑N/A ❑N/A 6. Containers Intact?' Yes No []N/A 7. Dissolved analysis: Samples Field Filtered? Yeses Sample Labels Match COC? -includes Date/Time/10/Analysls Matrix: I+❑ Te, f [IN. ❑N/A 9. Heads ate In VOA Vials '>5-6mm)? QYeS EINQ ; N n 10. Trip [dank Present? Trip Blank Custody Seals Present? ❑Yes Yes Na ❑N/A ❑PJ� 11. COMMENTS/SAMPLE DISCREPANCY Field Data Required? []Yes ❑Na � cam. l ,���." s��> >.�... 1 i•� r.:��4} �:t�.�� Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Date. gfe) 12 u G Project Manager SRF Review: Date: Page 15 of 17 Document Name: Document Revised: February7, 2018 _ aeeAnalytrca!' Sample Condition Upon Recel t(SCUR Page 1 of 2 Document No.: Issuing Authority: P-CAWCS-033-Rev.015 Pace Carolinas 4uall Office 'Check mark top half of box If pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coiiform, TOC, 02 and Grease, DRO/8015 (water) DOC, LLHg "*Bottom half of box is to list number of bottle Project a WO# : 92394936 PM: MWB Due Date: 08/15/18 CLIENT: 92—MECK'CO z ^' N '"' ? v u Z r = .9 a a m a w v a3 ' v x a amrS q v a a v O O N M a Ln Mp y N N a . c c z = N O= 2 n j c p N R Z D 2 n a vl > N a a 2 7 G N 3 A A E �E IJ E QO a a v iu iv E - c a 0. 4 a ¢ "� ] Oy } O a in a ¢ E 3 E E41/E�� m` m J E a` e� E J Ey E 10 �S5. E E E E E N rl `N Y q I Y N N N *QE 1 1 a a a a 1r V ati V d a LL Ur 4 l7 yN� RI to �j cn L 4 U' h N ppJJ 7 7� — m ra c a m isi m m m Q a 4 cc cc a a 7 7 7 7 CL � m Q o 1 Z 3 A 5 6 7 e 9 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservattva pH upon receipt Date presenratlon adjusted Time preservation adjusted Amount of Preservative added Lot $0 Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le. out of hold, Incorrect preservative, out of temp, tncorrect containers. Page 16 of 17 CHAIN -OF -CUSTODY 1 Analytical Request Document i i ceAnalytjral The Chain -of -Custody is a LEGAL DOCUME T. All relevant fields must be completed ac rately. Section A Section B Soction C Required Client Information: Required Project Information: Invoice Information: ! Pa e : 1 Of 1 Company, Mecklenburg County Solid Waste Repon To: Khatlem Adams I Attention: I Address: 2145 Suttle Ave Copy To: Company Name: Charlotte, NC 28208 Address: ':th'J I Ru- ulato A onc- +'a' Email: khaliem.adams(Omecklenbur count nc.00v Purchase Order#: Pace Quote: I € tl II Phone: (7Q4) 634-7705 jFax Project Name: Compost Central 1-West Blvd Pace Project Manager, ma thew.brainard acelabs.cOm . )IjX- :. State! Locdtlon_,- _• '' -'" Requested Due Data: Project #: Pace Profile #: 3207-1 I i ll II NC •' Re uestod'Anal sts•Flltoradl Yf �Ii'f. '"' bl "`�;� `-i:' V' 'me. , 5; a -_ �Z �..V . y ;nix COOP. ' o COLLECTED z Preservatives } ryc <M o-W.e watm nVY e U Wx' WT SAMPLE ID Waste Wala wW PrclP P or s of S �? START ENO a N ,~! i One Character per box. W�� vra w U a (AZ. 0-9 f, •) ou«er ar Sample ids must be unique 7jn . is i- �w u O� DATE TIME DATE TSME S S z z z i O ., r U LL N b a 1- i'• i Outfali 001 WT X X X X X X i ` I 2. Oulfell D02 WT( X X X X X X X i s. 5 6 `7 T I k ` .8 j ;t 113 1 2 i f ry _ f '`AODmONAL COMMENTS' mot- 1 r - �RELJNQLISHED BYIAFRSJATION q. ,`� . DATE' -, TIME ':i?TEP,BYf AFFIGATION=.- - - Y pt ME - 'ors �', SAM,PLE CONOITION4�� ,I If F m SAMPLERNAM EANDSIGNATURE�_ m PRINT Name of SAMPLER: v V � SIGNATURE of SAMPLER: j� r f / ,. 'r-Li"` f i r y o � ii/�r• DATE Signed: �j' �j L � 11� �I I' j aceAnalytical www,pacoiabs.com August 31, 2018 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: Compost Central 1-West Blvd Pace Project No.: 92397381 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 KIncey Ave. Suite 100 Huntersville, NC 28078 Enclosed are the analytical results for sample(s) received by the laboratory on August 28, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste TN1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. (704)875-9092 Page 1 of 10 Pace Analytical Servicas, LLC ® 9800 Kincey Ave. Suite 100 (�IaceAnalytical Huntersvilie, NC 28078 www.pacelabs.com (704)875-9092 CERTIFICATIONS Project: Compost Central 1-West Blvd Pace Project No.: 92397381 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 LouisianalNELAP Certification # LA170028 Florida/NELAP Certification E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiafVELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 10 aceAnalytical www.pacolobs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 2BO78 (704)875-9092 Project: Compost Central 1-West Blvd Pace Project No.: 92397381 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92397381001 Outfall 002 SM 92221)-2006 KDF 1 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 3 of 10 laneAnalyfical" www.pacelabs.com ANALYTICAL RESULTS Project: Compost Central 1-West Blvd Pace Project No.: 92397381 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 10o Huntersville, NC 28078 (704)875-9092 Sample: Outfall 002 Lab ID: 92397381001 Collected: 08/28/18 12:42 Received: 08/28/18 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms 809 CFU1100 mL 1.0 1 08/28/18 17:15 08/29/18 15:20 Date: 08/31/2018 03:38 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. ul Page 4 of 10 aceAnalytical www.pacefabs.corn Project: Compost Central 1-West Blvd Pace Project No.: 92397381 QC Batch: 427616 QC Batch Method: SM 9222D-2006 Associated Lab Samples: 92397381001 METHOD BLANK: 2362088 Associated Lab Samples: 92397381001 Parameter Fecal Colifosms SAMPLE DUPLICATE: 2362089 Parameter Fecal Coliforms QUALITY CONTROL DATA Analysis Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF) - CHT Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers CFUI100 ml- ND 1.0 08/29/18 15:20 92397381001 Dup Units Result Result CFUI100 mL 809 710 RPD Qualifiers 13 u1 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/31/2018 03:38 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 10 acmnalXical wwwpacefabs.com QUALIFIERS Project: Compost Central 1-West Blvd Pace Project No.: 92397381 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Dupficate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acryloniiriie by EPA Method 826D. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute, LABORATORIES PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS u1 Results based upon colony counts outside acceptable range. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/31/2018 03:38 PM without the written consent of Pace Analytcal Services, LLC. Page 6 of 1 D acmnalytrcal ® wwwpacelabs.mn QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Compost Central 1-West Blvd Pace Project No.: 92397381 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92397381001 Outfall 002 SM 9222D-2006 427616 SM 9222D-2006 r Date: 08/31/2018 03:38 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 427617 Page 7 of 10 Name: 6ocument Revised: Tebrwry 7, 2018 R[C!I LSCURI ftF-CARC$-Q33 Pi e16f2 Rev.06 Ifsuing Authority: Pace Carolinas Chralit Orfne Laboratory receiving samples: Ashevlrle❑ Eden❑ GreenwoodHuntersvillel]Raleigh❑ MachanlCFYrlle❑ CClentName; WO# : 92397381 Project# �rr/hle�l:;�•,rrl,nr.y IIl f pF�eRIII 111 Courier. LJFLd Es ❑UPS LJUSP5 [-]Client 111 I1 �- _❑Commercial__ .- —❑pace- -- ❑Other II 1 11111YYYY YY4 tttt 111 ffff _ azas�aaa. Custody Seal Present? ❑Yes CND Seaillntact? []Yes ONO -• ' Dalrrm!s+als Penon Eymldrt [anrents:���' Packing M.wlsl: 09udble Wrap ❑Bubble Bags QBoae ❑ Other Blologiml 7111ue Frozen? Thnmamet ,: 92T094 ryyeprlTa: [vet ❑awe ❑Yes QNo ❑N/A ❑Wont []IRtwnO: Cooler Templ'Ch j5-5 Cerrectlon factor:Add/41btracl l'Cj -o,j Tempchau!ddeabove Treeeingto6'C Cooler Temp Caarected j'Cr: ❑Samples put OF temp CIFEne, Samples on Ice, CcallAg procru 5asbrs'. USDA Regulated Soil IEJ N/A, water sampiel Did samples odglrate In a Quarantine acre wiLftm the untied Sutrs: CA, NY, or SC rchek mapsl? DOtanp�ts anpralefrome rweigA source liMernetlrnally, n .M P„arts ei<r0 n,•., till, edmm.nalDlrtre n Chain of Cvllody Plea Mt? - Tcr Na N A 1. Sam es AsrNed within Hold Tim0 ies no N A 2. Short Hold Time Analysis <72 hr.)? r1 NIA 3. Rush Tum A.nund Time Re unted? Yes - Np N A 6. Sufficient volume? 0y.. DNo Ow. 5_ ConectCoctalnersUsed? -Pace Cartamers Used) 01- 'IN, tie ❑nIn p!A 6 Containers WACO No MA 7. Dissolved anal str: Sam !es Field Flbered? ,- NS • tr A A. Sample Labels Maleh COC? -In,IWel DAlq,/TiMt/I AnOysls Matrlx: ❑y. tea ❑No ❑n1A 9, Heads ue o VOA IRa!s >5-Emm) rlvn No NIA 11_ Trip Clark Present? Trip War* Custody Seals Nesent] ❑yet Yes ❑no ON. ❑N?A N/A 11- COMMENT513MSPLE DISCREPANCY Field Deta peavlred7 [,lye. ON. lot ID of spilt containers: CLIENT" NOTIFICAIIQN/BESQLUTION Persian contacted: Oate/Time: Project Manager SCURF Review: _ Dew Z +� Project Manaler SRF Review: Dale: G1 j Pape 8 of 10 Document Name: 0ocumeni Rinsed: February 7, 2018 dCB/im4lrCdl� Sam 4 Candtntrn I'll.. 11-.1 t SCUR page f or2 DocumentNo.: Issuing Authority: F{giL-05033-11[v05 pane Carolinas Qualll OfFlce 'Check mark top half of boa if PH and/or dechlorination is verified and within the acceptance range for preservation samples. [eceptlenr: VaA,Colirarm,TOCAi and Grease, 000/9015 {water) 00C, LLNg ^Bottom halt of box is to list number of bottle Project p UO# : 92397381 PM: HWS Cue Onto: 09/05/18 CL16NT 92—MSCK CO 01MED son on k on a 0 M 1 DOE 0 own an on Monson E Do 0 on i'LlsonaLlean in son PH Adjustment Log for Preserved Samples tamp). ID Type of Pr[r0—U.a PH upon tt Wot C[[9 atuanatinn ldjflad Time Prnerlanon atltutt[tl amoum OF PrWrvaV�[ added Lala NPre Whantyer thlrl b a 0i ,taanW affeltlndNrtrlhCaraNalomPaantl—M.,. MY LJr.—V[nnn Drn el rfrAd, Ntorll CL Cmi![�alha, at or I—P. in[prtlel [pnlalnara Page 9 of 10 i 10 CHAIN -OF -CUSTODY / Analytical Request Document j The Chan-of-Cbsiody is a LEGAL OOCL;mew_ All ieievant nelds musl be Combleted aoeumtey. S�ctlm'R 5�caon � Sectbn C Emvrronmenfai Qualify Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfflling out tlusform, please visit }tttps://deq.nc.L,,ov/about/divisioiis/enerL"v-minesi-land- resources/enemv-ntin eraI -I and -norm its/stornnaaler-permits/nodes-industrial-sw#tab-4 Permit No.! NICI -74lgl 0/ 0 / V / 0 I or Certificate of Coverage No.: NICIG19l1l 0/V 14l Facility Name: rr t�(,i oS County: W C, i/Y] J i.t i" Phone No. Inspector: C 1, Date of Inspection: � /9/ ao Time of Inspection: Il 0 V Total Event Precipitation (inches): 0 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-h0ur storm interval does not apply if the permittee is able to document that a shorter interval is representative for focal storm events during the sampling period, and the permittee obtains approval from the local DIvMLR Regionai Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfallescrintion: Outfall No. �� Structure (pipe, ditch, etc.): f f �� /C,"(V<.�-� Receiving Stream. Describe the industrial activities that occur Within the outfall drainage area: Ilea`,; do LAGu.,I+P.n U I C9, Page 1 of 2 S W U-242, last modi I i ed 07/28/2017 2. Color: Describe the color of the.discli rge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Li I hl b r W n 3. Odor: Describ any distinct odor tha chlorine odor, etc.):Df discharge may have (i.e., smells strongly of oil, weak 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 1 2 3 (34 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5/ 7. Is there any foam in the stormwater discharge? O Yes C No. N0 8. Is there an oil sheen in the stormwater discharge? 0Yes d'No. Mo 9. Is there evidence of erosion or deposition at the outfall? 0 Yes C4 No. /V o 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. 11age 2 of 2 SWU-242, Last modified 07/28/2017 EnWronrnental quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report horguidunce onfrlling out thisform, please Wsil https://ded.nc.gov/about/divisions/energy-mineral-land- resources/energy-mineral-]and-permits/stormustrial-swi#tab-4 Perfnit No.: NIC/9 IqI a 1Q1U1 D/ or Certificate of Coverage. No.: NICIGA YI DId 10161 Facility Name: County: Inspecto Date of I Time of Total Event Precipitation (inches): V ' All permits require qualitative monitoring to be performed during a "Illeasurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMI-R Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. OutfaI cscription: Outfall No. Structure (pipe, ditch, etc.): (! Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: . f 1 • 1 I • _ ! Page I of 2 SWU-242. Last modified 07/29/2017 2. Color: Describe the color of the disc a (light, medium, dark) as descriptors: !—1 n �). using basic colors (red, brown, blue, etc.) and tint 1- f 0 "'Q Y) 3. Odor: Describe-ajiv distil t odors that the discharge lmay have (i.e., smells strongly of oil, weak chlorine odor. etc.): rV� Quo rs 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 (D 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stornlwater discharge, where I is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 0 5 7. Is there any foam in the storinwater discharge? 1QS Yes O No. [ J 8. Is there an oil sheen in the stormwater discharge? OYes No. 9. is there evidence of erosion or deposition at the outfall? o Yes No. to. Other Obvious Indicators of Storm►vater Poll�utio`n�:' List and describe f [% r Qf , lnd. C9y`�'y t,s Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 5WU-242, LaSL modified 07/28/2017 Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 4/27/2018 CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME Mecklenburg County Compost Central COUNTY Mecklenburg CountV PERSON COLLECTING SAMPLES Khaliem Adams LABORATORY: Pace Analytical Services Lab Cert. # 92 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept or ® Monthly' July (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA REC O V E D ❑Zero -flow []Water Supply ❑SA JUL 2 5 2018 ❑Other CEN T FiA' FILES DWR SECTION ❑ Oct -Dec Total event rainfall 2 0.23 in or ❑ No discharge this Period3 Date Sample Collected' (mo/dd/yr} Outfall No. TSS COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks =__> 100 mg/L4 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 7/13/2018 2 4.6 76.0 3500 0.10 0.13 0.012 <0.0050 0.10 5.9 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 4The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Date Sample Collected' (mo/dd/yr) Outfall No. pH TPH using method 1664A SGT HEM TS5 Total Rainfall' Check if No Flow This Period' Average New Motor Oil Usage 6-9 15 mg/L 100 mg/L^ - - - 1 - - - - X 75 gai/month 7/13/2018 2 5.9 <4.8 4.6 0.23 Footnotes from Part A also apply to this Part B FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an oriainal and one copv of this DMR. including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitorina period in the case of "'No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Z3 L/ (Date) Per rt D/te: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 2 of 2 aceAnalytical www.pawlabs.cam July 22, 2018 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: Compost Central 1-West Blvd Pace Project No.: 92391905 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 1DD Huntersville, NC 2BO78 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on July 13, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste Q pccu T� REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 17 Pace Analytical Services, LLC aceAnalytical 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 r wwwpacelabs.cnm (704)875-9092 CERTIFICATIONS Project: Compost Central 1-West Blvd Pace Project No.: 92391905 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certificafson M 99006001 Louisiana]NELAP Certification # LA170028 Florida]NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carodria Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221 North Carchna Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 FloridalNELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytica$ Services, LLC. Page 2 of 17 aceAnalytical ! www.paculabs.corn SAMPLE ANALYTE COUNT Pace Analytical Services, t_LC 9800 Kincey Ave. Suite 100 Huritersville, NC 28078 (704)875-9092 Project: Pace Project No.: Compost Central 1-West Blvd 92391905 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92391905001 Outfall 002 EPA 1664E JMS 1 PASI-C EPA 200.7 Rev 4.4 1994 Sf41 3 PASI-A SM 9222D-2006 KDF 1 PASI-C SM 254OD-2011 CEH 1 PASI-A EPA 9040C ECH 1 PASI-A TKN+NO3+NO2 Calculation EWS 1 PASt-A EPA 351.2 Rev 2.0 1993 BRJ 1 PASI-A EPA 353.2 Rev 2.0 1993 DMN 1 PASI-A EPA 365.1 Rev 2.0 1993 BRJ 1 PASI-A SM 5220D-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 17 aceAnapical wawpacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Compost Central 1-West Blvd Pace Project No.: 92391905 Sample: Outfall 002 Lab ID: 92391905001 Collected: 07/13118 10:29 Received: 07/13118 11:09 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Quaf 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg]L 4.8 1 07120/18 03:59 200.7 MET 1CP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper 0,012 mg1L 9.0050 1 07/14/18 04:55 07/16/18 01:48 7440-50-8 Lead ND mg/L 0.0050 1 07/14/18 04:55 07/16/18 01:48 7439-92-1 Zinc 0.10 mg/L 0.010 1 07/14/18 04:55 07/16/18 01:48 7440-66-6 M810 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Fecal Coliforms 3500 CFU1100 mL 1.0 1 07/13/18 12:22 D6,u2 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 4.6 mg/L 27 1 07/14/18 01:00 9040 pH Analytical Method: EPA 9040C pH 5.9 Std. Units 0.10 1 07/16/18 15:10 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculatlon Total Nitrogen 1.3 mg/L 0.52 1 07/22/18 15:53 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 1.2 mg1L 0.50 1 07/18118 04:31 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 0.10 mg/L 0.020 1 07120/18 12:49 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Phosphorus 0.13 mg1L 0.050 1 07/18118 05:41 7723.14-0 52200 COD Analytical Method: SM 5220D-2011 Chemical Oxygen Demand 76.0 mg/L 25.0 1 07/16/18 23:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/22/2018 03:55 PM without the written consent of Pace Analyticai Services, LLG. Page 4 of 17 aceAnalytical www.pacelabs.cem Project: Compost Central .1-West Blvd Pace Project No.: 92391905 OC Batch: 420186 OC Batch Method: EPA 1664B Associated Lab Samples: 92391905001 METHOD BLANK: 2328103 Associated Lab Samples: 92391905001 Parameter knits Total Petroleum Hydrocarbons mWL LABORATORY CONTROL SAMPLE: 2328104 Parameter Units Total Petroleum Hydrocarbons mglL Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 4.8 07/20/18 03:48 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 19.2 19.5 101 64-132 MATRIX SPIKE SAMPLE: 2328105 35402843002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 4.8U 19.2 19.5 101 64-132 Results presented on this page are In the units Indicated by the" Units" column except where an altemate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/22/2018 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 17 aceAnalytical i www.padelabscom I Project: Compost Central 1-West Blvd Pace Project No.: 92391905 QC Batch: 419181 QC Batch Method: EPA 200.7 Rev 4.4 1994 Associated Lab Samples: 92391905001 METHOD BLANK: 2323798 Associated Lab Samples: 92391905001 Parameter Units Copper mglL Lead mg/L Zinc mglL QUALITY CONTROL DATA Analysis Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 2D0.7 MET Matrix: Water Blank Reporting Result Limit Analyzed ND 0.0050 07/16/18 01:07 ND 0.0050 07/16/18 01:07 ND 0.010 07/16/18 20:02 Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2323799 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg/L .5 0.51 102 85-115 Lead mg/L .5 0.48 97 85-115 Zinc mg/L .5 0.49 99 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2323800 2323B01 MS MSD 92391271003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg1L 0.076 .5 .5 0.59 0.60 102 105 70-130 2 Lead mg/L ND .5 .5 0.46 0.47 92 94 70-130 2 Zinc mg/L 0,13 .5 .5 0.61 0.63 96 98 70.130 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2323802 2323803 MS MSD 92391882001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper my/L ND .5 .5 0.52 0.51 103 102 70-130 1 Lead mg/L ND .5 .5 0.48 0.48 97 96 70-130 1 Zinc mg1L 88.2 .5 .5 0.58 0.57 98 97 70-130 1 ug1L Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/22/2018 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 17 aceAnalytrcal& www.patelab&c= QUALITY CONTROL DATA Project: Compost Central 1-West Blvd Pace Project No.: 92391905 QC Batch: 419318 Analysis Method: SM 9222D-2006 QC Batch Method: SM 9222D-2006 Analysis Description: 9222D MBIO Fecal Coliform - CHT Associated Lab Samples: 92391905001 METHOD BLANK: 2324201 Matrix: Water Associated Lab Samples: 92391905001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU1100 mL ND 1.0 07/13118 12:22 SAMPLE DUPLICATE: 2324202 Parameter Units Fecal Coliforms CFU1100 mL 92391905001 Dup Result Result RPD Qualifiers 3500 600 141 D6,u2 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 2BO78 (704)875-9092 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07122/2018 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 17 IeAnalytical wwwpatelabs.Cont QUALITY CONTROL DATA Project: Compost Central 1-West Blvd Pace Project No.: 92391905 Pace Analytical Services, LLC 9B00 Kincey Ave. Suite 100 Huntersnille, NC 2BD78 (704)875-9092 QC Batch: 419176 Analysis Method: SM 254OD-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92391905001 METHOD BLANK: 2323779 Matrix: Water Associated Lab Samples: 92391905001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L N❑ 2.5 07/14/18 00:58 LABORATORY CONTROL SAMPLE. 2323780 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Suspended Solids mglL 251 246 98 90-110 SAMPLE DUPLICATE: 2323781 92391927001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 12.2 12.6 3 SAMPLE DUPLICATE: 2323782 92391956002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 343 347 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/22/2018 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 17 aceAnalytrcal www.patelabs.com QUALITY CONTROL DATA Project: Compost Central 1-West Blvd Pace Project No.: 92391905 QC Batch: 419285 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351,2 TKN Associated Lab Samples: 92391905001 METHOD BLANK: 2324086 Associated Lab Samples: 92391905001 Parameter Units Nitrogen, Kjeldahl, Total mglL LABORATORY CONTROL SAMPLE: 2324087 Parameter Units Nitrogen, Kjeldahl, Total mg/L Pace Analytical Services, LLG 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 07/18/18 04A3 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 10 9.8 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2324088 2324089 MS MSD 92391439002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mglL 0.91 10 10 11.2 11.3 103 104 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2324090 2324091 MS MSD 92391555001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mglL 2.0 10 10 12.3 12.0 103 100 90-110 2 Results presented on this page are In the units indicated by the"Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/22/2018 03:55 PM without the written consent of Pace Analytical Services, LLC, Page 9 of 17 m aceAnalytical www.pat:alabs.com QUALITY CONTROL DATA Project: Compost Central 1-West Blvd Pace Project No.: 92391905 QC Batch: 420209 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92391905001 METHOD BLANK: 2328160 Associated Lab Samples: 92391905001 Parameter Units Nitrogen, NO2 plus NO3 mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.020 0712011812:23 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2328161 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.6 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2328162 2328163 MS MSD 92391408015 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPO Qual Nitrogen, NO2 plus NO3 mg/L ND 2.5 2.5 2.5 2.5 99 99 75-125 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2328164 2328165 MS MSD 92391408016 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mglL ND 2.5 2.5 2.5 2.5 99 99 75-125 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/22/2018 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 17 aceAnafytical® wwwpat*abs.com QUALITY CONTROL DATA Project: Compost Central 1-West Blvd Pace Project No.: 92391905 QC Batch: 419431 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92391905001 METHOD BLANK: 2324574 Associated Lab Samples: 92391905001 Parameter Units Phosphorus mg/L LABORATORY CONTROL SAMPLE: 2324575 Parameter Units Phosphorus mg1L Pace Analytical Services, LLC 9800 Klncey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 07/18118 05:23 Spike LCS LCS % Rec Conc. Result %6 Rec Limits Qualifiers 2.5 2.6 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2324576 2324577 MS MSD 92391438001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.33 2.5 2.5 2.9 2.9 103 103 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2324578 2324579 MS MSD 92391610007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mglL 0.13 2.5 2.5 2.7 2.7 104 104 90-110 0 Results presented on this page are In the units indicated by the"Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07122/2018 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 17 acmnalytical wwwpacelabs.mm QUALITY CONTROL DATA Project: Compost Central 1-West Blvd Pace Project No.: 92391905 QC Batch: 419398 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92391905001 METHOD BLANK: 2324468 Associated Lab Samples: 92391905001 Parameter Units Chemical Oxygen Demand mg/L Matrix; Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 07/16/18 23:30 Paco Analytical Services, LLC 9B00 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2324469 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 761 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE; 2324470 2324471 MS MSD 92391502002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 2770 100 100 2760 2870 -8 96 90-110 4 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2324472 2324473 MS MSD 92391420004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 100 100 126 119 125 118 90-110 5 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except tin full, Date: 07l2212018 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 17 aceAnalXical wwwpitcolabs.corn QUALIFIERS Project: Compost Central 1-West Blvd Pace Project No.: 92391905 DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroelhylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260, N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA required holding lime. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/22/2018 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 17 Pace Analytical Services, LLC aceAnalytrcal 9800 Kincey Ave. Suite 108 J+ Huntersville, NC 28078 w6mPataelabs.mm (704 )875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Compost Central 1-West Blvd 92391905 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92391905001 Outfall 002 EPA 1664E 420186 92391905001 Outfall 002 EPA 2007 Rev 4.4 1994 419181 EPA 200.7 Rev 4.4 1994 419211 92391905001 Outfall 002 SM 9222D-2006 419318 92391905001 Outfall 002 SM 254OD-2011 419176 92391905001 Outfall 002 EPA 9040C 419294 92391905001 Outfall 002 TKN+NO3+NO2 420497 Calculation 92391905001 Outfall 002 EPA 351.2 Rev 2.0 1993 419285 92391905001 Outfall 002 EPA 353.2 Rev 2.0 1993 420209 92391905001 Outfall 002 EPA 365.1 Rev 2.0 1993 419431 92391905001 Outfall 002 SM 5220D-2011 419398 Date: 07/22/2018 03:55 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 17 Document Name: Document Revised: February 7, 2018 BCBMc?I lCci<A Sample Canditlon U on Recel t(SCUR page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Creenwond ❑ Huntersville [%� Raleigh[] Mechanicsville0 Client Name: W0# : 92391905 Kamm=Courier: f %���'i?%? t )r���� []Fed E ❑UPS ❑USPS P Client g2381 0 ❑ Commercial []Pace ❑Other, 8 5 Custody Seal Present? ❑Yes 4No Patting Material: ❑Bubble Wrap Seals Intact? ❑Yes QNo 1 ❑Bubble Bags ❑None ❑ Other Thermomele : Type of ice: IJwet Blue IR 6un lD: 92TO40 r Cooler Temp ('Cl: / .5 . (�Co�rrection Factor: Add/Subtract ('C) +0,4 Cooler Temp Corrected ('CI: —1—/ USDA Regulated Sall (IdN/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)7 ❑yesNo Date/Initials Person Examining Contents: 7 jj Biological Tissue Frozen? [] Yes []NOU No N/A ❑None TempshouId be above freezing to 6'C �`I samples out of temp criteria. Samples on Ice, cooling process has begun Did samples originate From a foreign source (internationally, including Hawaii and Puerto RIcoP ❑Yes MNo Comments/Discrepancy: Chain of Custody Present? Yes NO []N/A 1. Samples Arrived within Hold Time? • Yes QNo N/A 2. Short Hold Time Analysis (<71t hr.? yes No N/A 3. Rush Turn Around Time Requested? L1 Yes No N/A 4. Sufficient Volume? Yes C3No ❑N/A S. Correct Containers Used? yes []Nol] No N/A 6• -Pace Containers Used? /n]Yes Na ❑N/A Containers Intact? 'Yes nNo QNJA 7. Dissolved analysis: Samples Field Filtered? []Yes ❑Na ©N/A a. Samplelabels Match COC7 ©res ❑No ❑NIA 9. �� -Includes Date/Time/ID/Analysis Matrix: Headspace in VOA Vials (>5•6mm)7 rip an Present? []Yes ❑No PN/A 11. Trip Blank Custody Seals Present? Yes No / N/A COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLU70N Field Data Required? ❑Yes ❑No Person contacted: Date/Time: Project Manager SCURF Review:�� ' ; Date: AAQ Project Manager SRF Review: ��`� Date: Page 15 of 17 Document Name: Document Revised; February 7, 2018 �� aCBAII�?IyilCr�rr Sample Condition Upon Recelpt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F•CAR-CS-033•Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechiorination Is Project 0 verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottle W0#:92391905. PM: MW8 Due Date: 07/20/18 CLIENT: 92-MECK CO u G _ u Z 7 a E lA n V R m Z 7 a E O N . a m 2 7 J E O CA N 6 m Q c a `m � rl w7i R co T a E N W G. m t3 Z n E D r, M 6 0 n O ra Z ¢ N a E N 7 7 C. m ^, Z a E /NV .. V d In N n U 9 E U 3 ` 2 u n c ¢ v ,y . l7 a N ❑ ¢ u � .za l7 a Z v Gi m [ O ¢ of N M U' a w ry v x ry ¢ a _ - l? Q N + n n� Y E N N m U' ¢ Z t7 Q E y U a �t l7 ¢ 2 = O E q M U' o O �iyi z ¢ Q Y . l7 > 2 n C E q . l7 > yy O m O E O Y in f7 a ? O VI Y IT IO Q O > 2 .. a w a .9 � �, 6 7 a I ¢ U `- `° w E N w 1 r°[ io I z a N �n E O n N a u, en T $ S Z u a E � rq 4 m > 2 C 7 N E ¢ I .+ 7 z c A e N E N U N a i a a a E � 2. 3 a NN s 6 7 9 10 11 NU� 12 NNN pH Adjustment Log for Preserved Samples Semple ID Type of Preservative pH upon recelpt Date preservation adjusted Time prenervatlon adjusted Amount of Preservative added lot N Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy Of this form will be sent to the North Carolina DEHNR Cerilflcation Office (Le. Out of hold, Incorrect preservative, Out of temp, Incorrect containers. Page 16 of 17 ' fdLe�JT�t� Section A Required Client Information: Due Date: SAMPLE ID Ono Character per tsoa. IA-z. 0-91. -1 *b Samplo Ids must be unique ur r 1C 0utfau001 2 'Y 00011002 5. 6 . 7z g- 9. l 0:. 4 i21•: - -` 'ADDITIONAL'COMMEH7 Section B Required Project Information: Report To: Darren Steinhilber Copy To: Purchase Order S: Project Name: Compost Central Project a: r Tracc Cane C odM.S Water eW b WaMr tvT r9 � Woile Walar VM Product P _ V, SWUM st 00 oL r7 START W" WP a n D is T-- TS o O 1C a w K 4 va CHAIN -OF -CUSTODY 1 Analytical Req est Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fi Ids must be completed accurately. ti Section C Invoice Information: Page: 1 Of t Attention: Company Name: Address: a-G -- _ �c ' Regutato Na rh" _:rt�m=, + Pace Ovote: it Blvd Pace Project Manager, matthew.brainasd acelabS.com Pace Profile 9: 3207-1 NC s >•. Reci6estedArtal Isis Flttored M =' .' *� f r ;h " 'r l r4IK I w rTFn Preservatives } ,"F' -= sx✓-. M o 0 END U w y Zz _ a A w w •L o "i v O '- z U y z 4 `� O o. u v im a = TIIUIF a 7 2 Z 2 2 Z 2 0 CW Y N 0 a TURE of Signed: �l G'G ( 7'7lME. n 5ANPLE Cof•!t]m01J5 tom, ^°' :�' r Environmental Quality Stormwater Discharge Outfall (SD4) Qualitative Monitoring Report Forguidance onftlling out thisform, please visit hops://deq.nc.gov/about/divisions/energy-mineral-]antl- resources/energ&inineral-land-permits/storinwater-pernitslnpdes-industrial-sN41ab-4 �r Pert -nit No.: N/ClL,l o1 q /C)/ d 10l 0l or Ccrti (icate of Coverage No.: N/C/G/sn/j/Q /0 / 1 l6I Facility Name: IVI, N.(' k County: Inspector: / Date of Inspection: D Time of Inspection: Total Invent Precipitation (inches): 0' L7 15 Phone No. `-704I 6 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DFMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designce) t. Outfall Description: Outfall No. � Structure (pipe. ditch, etc.): Receiving Stream: i the industrial activities that occur within the outfall drainage area:O r r rle Y11.a.b) 4-r°i t Im Cli Page 1 of 2 SWU-242, Last modified 07/2812017 2. Color: Describe the color of the ischarge si (light, medium, dark) as descriptors: �j LEY /11 3. Odor: Dcscriany ds inct odor t� chlorine odor, etc.): (') 10 ' 00 tors (red, brown, blue, etc.) and tint r rge may have (i.e., smells strongly of oil, weak 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear, and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 1 C2) 3 - 4 5 6. Suspended Solids: Choose the number which best describes the amount of'suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: l 2 3 4 5 7. Is there any foam in the stormwater discharge? O Yes V/N o. 8. Is there an oil sheen in the stormwater discharge? OYes O/No. A h 9. 1s there evidence of erosion or deposition at the outfall? O Yes CVNo. Vn 10. Other Obvious Indicators of Stormwater Pollution: List and describe Ao &(�c I' Laj� r /\ ,S Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2of2 SwU-242, fast modified 07/2912017 Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 03/16/2018 CERTIFICATE OF COVERAGE NO. NCG240016 SAMPLE COLLECTION YEAR 2018 FACILITY NAME Mecklenburg County Compost Central SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec COUNTY Mecklenburg County R EC i— I\ /P r) or ® Monthly' March_ (month) PERSON COLLECTING SAMPLES Khaliem Adams DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY: Pace Analytical Services Lab Cert. # 92 MAR 2 1 2018 ❑Zero -flow []Watersupply [:]SA Comments on sample collection or analysis: � [:]OtherCENTRALi*li.l=.•.> D► R SECTION Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall z 0.65 in or ❑ No discharge this period' Date Sample Collected' (mo/dd/yr) Outfall No. TSS COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks 100 mg/O 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 03/12/2018 1 - - - - - - - - - 03/12/2018 2 138 192 6000 7.2 1.8 0.016 0.0052 0.049 6.2 ' Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part B. Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Date Sample Collected' (mo/dd/yr) Outfall No. pH TPH using method 1664A SGT-HEM T55 Total Rainfall' Check if No Flow This Period3 Average New Motor Oil Usage 6-9 15 mg/L 100 mg/0 - - i - - - - X 75 gal/month Click here to enter text. 2 6.2 <5.0 138 0.65 Click here to enter text. Footnotes from Part A also apply to this Part B FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an original and one copy of this DMR, includina all "No Discharae" reports. within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly resp nsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete am aware tha redsignificant penalties for submitting false information, includin the possibility of fines and imprisonment for knowing violations." (Signature of Permlttee) ( (Da{e) P mit bate: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 2 of 2 Emvu-0n men 1al Qualify Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidatace onftlling out Ihirfnrnr, please visa htttisa/ded.nagovlabout/divisions/energy-in ineral-land- resources/energy-mineral-land-permits/stormwater-permitshipdes-industri al-sw#tab-4 PermitNo.: NIGC ^ Facility Name: County: Inspector: Date of Inspection: Time of Inspection: Total Event Precipitation (inches): 0, r All pen -nits require qualitative monitoring to be perfonned during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the pennittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: A ? Outfall No. Structure (pipe, ditch,.ete.): Pt /Verb _ Receiving Stream: De ribe the industr al actiyities that occur within the outfall drainage area:ti- Page 1 of 2 SWU-242, Last modified 07/28/2017 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: o U 3. O(Ior: Describe any distinct odors that the discharge chlorine odor, etc.): _ Ff?W'L� eL� � LD r— I haves (i.ei, smells strongly of oil, weak 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 j2 j 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stortwater discharge, where l is no solids and 5 is the surface covered with loating solids: 1 2 (D 4 5 G. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is ,extremely muddy: 1 2 (3 f 4 5 y �7 C 7. Is there any foam in the stormwater discharge? 6Yes O No. l' J 8. Is there an oil sheen in the stormwater discharge? OYes (t'/No. No 9. Is there evidence of erosion or deposition at the outfall? O Yes i25/No. NO 10. Other Obvious Indicators A-121� ofStormwater Pollution: NOList and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242, Last modified 07/28/2017 aceAnalytical www pacelabs.com March 16, 2018 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: COMPOST CENTRAL 1 Pace Project No.: 92376464 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 - (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on March 12, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. it you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste ��� pCCRfp�T`nG �i TNi t4Qo �� REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in felt, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 aceAnalytical www.pacelabs.com Project: COMPOST CENTRAL 1 Pace Project No.: 92376464 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078- (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: EB7648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 FloridalNELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 aceAnalytrcal" wwwpacelabs.com SAMPLE ANALYTE COUNT Pate Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: COMPOST CENTRAL 1 92376464 Anatytes Lab ID Sample ID Method Analysts Reported Laboratory 92376464DOI OUTFALL 2 EPA 1664E JMS 1 PASI-C EPA 200.7 SER 3 PASI-A SM 9222D KDF 1 PASI-C SM 2540D EJJ 1 PASI-A EPA 9040 KMM 1 PASI-A TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 BRJ 1 PASI-A EPA353.2 CJH1 1 PASI-A EPA 365.1 MDW 1 PASI-A SM 5220D NAL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 (�IaneAnalytical wwwpacelabs com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: COMPOST CENTRAL 1 Pace Project No.: 92376464 Sample: OUTFALL 2 Lab IO: 92376464001 Collected: 03/12/18 11:01 Received: 03/12/18 11:41 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg1L 5.0 1 03/14/18 05:05 2D0.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 0.016 mg/L 0.0050 1 03/13/18 0130 03/14/18 19:16 7440-50-8 Lead 0.0052 mg/L 0.0050 1 03/13/18 03:30 03/14/18 1916 7439-92-1 Zinc 0.049 mg/L 0.010 1 03/13/18 03:30 03/14/18 1916 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D Fecal Coliforms 6000 CFU1100 mL 1.0 1 03/12/18 14:07 u2 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 138 mg/L 29.4 1 03/14/18 18:30 9040 pH Analytical Method: EPA9040 pH 6.2 Std. Units 0.10 1 03/14/16 00:33 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 7.2 mg/L 0.52 1 03/14/18 14A0 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351,2 Nitrogen, Kjeldahl, Total 4.0 mg/L 0.50 1 03/14/18 03:05 7727-37-9 353.2 Nitrogen, N021NO3 pres. AnatyticaI Method: EPA 353.2 Nitrogen, NO2 plus NO3 3.2 mg/L 0.020 1 03/14/18 D3:15 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 1.8 mg/L 0.050 1 03/14/18 21:39 7723-14-0 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 192 mg/L 25.0 1 03/14/18 18:06 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/16/2018 03:24 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 18 m (�55'neAnal(Xical wwwpacelabs.t:ont Project: COMPOST CENTRAL 1 Pace Project No.: 92376464 QC Batch: 401867 QC Batch Method: EPA 1664B Associated Lab Samples: 92376464001 METHOD BLANK: 2228898 Associated Lab Samples: 92376464001 Parameter Units Total Petroleum Hydrocarbons mg1L QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 03/14/18 04:55 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huwersville, NC 28078- (704)875-9092 LABORATORY CONTROL SAMPLE: 2228899 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 19.0 95 64-132 MATRIX SPIKE SAMPLE: 2228900 35378483001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 5.0U 20 19.8 95 64-132 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/16/2018 03:24 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 (�IaneAnalyfical" twvw.pacelabs.com Project: COMPOST CENTRAL 1 Pace Project No.: 92376464 QC Batch: 401678 QC Batch Method: EPA 200.7 Associated Lab Samples: 92376464001 METHOD BLANK: 2227995 Associated Lab Samples: 92376464001 Parameter Copper Lead Zinc QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers mg/L ND 0,0050 03/14/1819:01 mg1L ND 0.0050 03114/1819:01 mg1L ND 0.010 03/14/1819:01 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078' (704)875-9092 LABORATORY CONTROL SAMPLE: 2227996 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mglL .5 0.53 105 85-115 Lead mglL .5 0.50 101 85-115 Zinc mglL 5 0,50 101 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2227997 2227998 MS MSD 92376464001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg1L 0.016 .5 .5 0.53 0.53 103 102 70-130 1 Lead mg/L 0.0052 .5 .5 0.49 0.49 97 96 70-130 1 Zinc mg1L 0.D49 5 .5 0.53 0,54 97 97 70-130 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2227999 2228000 MS MSD 92376537001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L 371 .5 .5 0.87 0.87 100 100 70-130 0 ug/L Lead mg/L 192 5 .5 0.66 0,66 93 93 70-130 0 ug/L Zinc mg1L 891 .5 .5 1.4 1.4 93 92 70-130 0 ug/L Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/16/2018 D3:24 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 (�IaceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92376464 QC Batch: 401760 Analysis Method: SM 9222D QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - CHT Associated Lab Samples: 92376464001 METHOD BLANK: 2228377 Associated Lab Samples: 92376464001 Parameter Fecal Coliforms SAMPLE DUPLICATE: 2228378 Parameter Fecal Coliforms Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers CFUI100 mL ND 1.0 03/12/18 14:07 92376468003 Dup Units Result Result RPD Qualifiers CFUI100 mL 350 380 8 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right at the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/16/2018 03:24 AM without the written consent of Pace Analytical Services, LLC, Page 7 of 18 (�IacleAnalxical" wwwpacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92376464 QC Batch: 401997 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Tota! Suspended Solids Associated Lab Samples: 92376464001 METHOD BLANK: 2229829 Matrix: Water Associated Lab Samples: 92376464001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 03/14/18 18:23 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 LABORATORY CONTROL SAMPLE; 2229830 Spike LCS LCS % ReC Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 238 95 90-110 SAMPLE DUPLICATE: 2229831 Parameter Total Suspended Solids SAMPLE DUPLICATE: 2229832 Parameter Total Suspended Solids Units 9237633B001 Result Dup Result mg/L ND ND Units 92376373004 Result Dup Result mg/L 52.0 50.7 RPD Qualifiers RPD Qualifiers 3 Results presented on this page are In the units Indicated by the "UnI15" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/16/2018 03:24 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 18 (�Ia'cie Analytical� wwwpacelabs.aom QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92376464 QC Batch: 401858 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92376464001 SAMPLE DUPLICATE: 2228870 Parameter pH 92376536001 Dup Units Result Result RPD Qualifiers Sid. Units 7.0 7.0 0 H6 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/16/2018 03:24 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 (�IaoeAnalytical wwwpacelabs.corrt QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92376464 QC Batch: 401763 Analysis Method: EPA 351.2 QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN Associated Lab Samples: 92376464001 METHOD BLANK: 2228387 Associated Lab Samples: 92376464001 Parameter Units Nitrogen, Kjeldahl, Total mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 03/14/18 03:18 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 LABORATORY CONTROL SAMPLE: 2228388 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 10.1 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2228389 2228390 MS MSD 92376143001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 2.1 10 10 12.6 11.9 105 97 90-110 6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2228391 2228392 MS MSD 92376025002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mglL <0.50 10 10 10.7 10.8 103 104 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/16/2018 03:24 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 (�IacieAnalyfica( www.pacefsibs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92376464 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 401852 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92376464001 METHOD BLANK: 2228849 Matrix: Water Associated Lab Samples: 92376464001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.020 03/14/18 02:57 LABORATORY CONTROL SAMPLE: 2228850 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.4 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2228851 2228852 MS MSD 92376143002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 1.3 2.5 2.5 4.0 3.8 107 101 75-125 4 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2228853 2228854 MS MSD 92376272002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0,48 2,5 2.5 2.9 2.9 99 99 75-125 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03116/2018 03:24 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 aceAnalytical wwwpacelabs.mm QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92376464 QC Batch: 401988 Analysis Method: EPA 365.1 QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92376464001 METHOD BLANK: 2229781 Associated Lab Samples: 92376464001 Parameter Units Phosphorus mg1L LABORATORY CONTROL SAMPLE: 2229782 Parameter Units Phosphorus mg1L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 03/14/18 21:37 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2229783 2229784 MS MSD 92376464D01 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 1.8 2.5 2.5 4.3 4.3 102 102 90-110 0 Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/16/2018 03:24 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 aoAnalytrcal® wwwpacefabs.mm Pace Analytical Services, LLC 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: COMPOST CENTRAL 1 Pace Project No.: 92376464 QC Batch: 401886 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92376464001 METHOD BLANK: 2229030 Associated Lab Samples: 92376464001 Parameter Units Chemical Oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 2229031 Parameter Units Chemical Oxygen Demand mg/L Matrix: water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 03/14/18 18:06 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 750 745 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2229032 2229033 MS MSD 92376005002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 34.0 100 100 135 140 101 106 90-110 4 R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2229034 2229035 MS MSD 92376468001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 98.0 100 100 196 203 98 105 90-110 4 R1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fuii, Date: 03/16/2018 03:24 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 (�IacieAnalytical msw.pacefabs.com QUALIFIERS Project: COMPOST CENTRAL 1 Pace Project No.: 92376464 DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NO 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H6 Analysis initiated outside of the 15 minute EPA required holding time. R1 RPD value was outside control limits. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03116/2018 03:24 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 IacleAnalytical (� www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: COMPOST CENTRAL 1 Pace Project No.: 92376464 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NO 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92376464001 OUTFALL 2 EPA1664B 401867 92376464001 OUTFALL 2 EPA 200.7 40167B EPA 200.7 92376464001 OUTFALL 2 SM 9222D 401760 92376464001 OUTFALL 2 SM 2540D 401997 92376464001 OUTFALL 2 EPA 9040 401858 92376464001 OUTFALL 2 TKN+NO3+NO2 401967 Calculation 92376464001 OUTFALL 2 EPA 351.2 401763 92376464001 OUTFALL 2 EPA 353.2 401852 92376464001 OUTFALL 2 EPA 365.1 401988 92376464001 OUTFALL 2 SM 5220D 401886 Date: 03/1612018 03:24 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analyticak Services, LLC. Analytical Batch 401690 Page 15 of 18 Document Name: Document Revised: February 7, 2018 aceAnalytieal y - Sample Condition Upon Recelpt(SCUR) Pa e.1 of 2 Document No.: Issuing Authority: f-CAR•CS-033-Rev,06 Pace Carolinas Quality Office Laboratory receiving samples: / Asheville ElEden[-]Greenwood ❑ Huntersvijl¢ u Ralelgh❑ Mechanicsville[] Client Name: W®' : 92376464 .. t r �Q ProJectq; I` l Courier: ❑Fed Ex []UPS Us PS "'OPTent ❑Commercial ❑Pace=❑Qther- 92376464 — .._....._.. __. ...--- ------- -- -_ Custody Seal Present? ❑YesM �R Seats Intact? ❑Yes No-" _S.. Date/Initials Person Examining Contents:— Z_ Packing Material: []Bubble Wrap ubble Bags. None 0 Other Biological Tissue Frozen? Thermometer: j`� I � 3 ❑tRt;un ID: 92TO36 Ype *flee: Wet []Blue Cooler Temp ('Cj: � r Z Correction factor: Add/Subtract ('C) +Q, j Cooler Temp Corrected i-Q: i, 3 45DA Regulated Solt { NIA, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? ❑Yes ❑no- ❑Yes-- o ❑N/A ❑None Temp should be above freezing to VC []Samples out of temp criteria. Samples an ice, cooling process has begun Did samples originate from a foreign source (internatlon y, including Hawaii and Puerto Rico)? ❑Yes Comments Discrepant . Chain of Custody Present? cs Na N/A 1. Samples Arrived within Hold Time? No N/A 2. Short Hold Time Analysis c72 hr.)? Yes No []N/A 3. Rush Turn Around Time Requested? ❑Yes No ❑N/A 4. Sufficient Volume? 2< NO N/A 5. Correct Containers Used? -Pace Containers Used? Ye es ONO ONO ❑N/A N/A 6. Containers Intact? es ON13 N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes ONO []N/A 8. Sample labels Match COC7 -includes Date/Time/ID/Analysis Matrix: es �f ON. ❑N/A 9. Headspace in VOA Vials >5.6mml? QYes ❑No /A 10. Trip Blank Present? Trip Blank Custody Seats Present? ❑Yes ❑Yes No ONO ❑NIA /A li. COMMENTSISAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Field Date Required? ❑Yes []No ID of split containers: Date: J L1z Date: 3� Page 16 of 18 Document Name: Document Revised: February 7, 2018 - aceA,?al )cal ' Sample Condition Upon Recelpt(SOUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-833-Rev.05 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination Is verified and within the acceptance range for preservatlon samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, L ft "Bottom half of box Is to Ust number of bottle Project N WO# : 92376464 PM: MWB Due date: 03/19/18 CLIENT: 92-MECK CO _ u Z a 3 vE, r~-1 a Co i� a 5 9 d N a Co is n � o a M w CL c °' M in I M E i x p x .Si o c N a m Q+ (6 `Qd' z E a m z z 2 U E N m d a a E �yS C a `a N L7 a r� a G x A ¢ `w rf t7 a z y y c' E 1 ofi N N x N r ¢ .y L7 a y n Y e lQ/E� N L? a z aEE Q E .r.. «di 111777 a Z a C o > E l7 o O � Q 7 pE Fi t7 n n o 7 E �7 y q?q O o > yE 1 z LA= •' 1� 0 Y ay A & .'�.R 9M 7 Y a °' v+ 1�fFV7 u� Z d 1o7E� v, ON N 2 J E m M a 5 E N E N 9 4J 7 E a E z 3 4 5 6 7 8 9 10 11 lz PH Adjustment Log for Preserved Samples Sample iD Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot 4 Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 17 of 18 CHAIN -OF -CUSTODY / Anz %. f f lytical Request Document F1ceAnaty1iG71' The Chain -of -Custody is -a LEGAL DOCUN ENT. All relevant fields must be completed accurately. Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Page ' 1 Of 1 Company: Mecklenburq County Solid Waste Report To, Khaliem Adams Attention: Address: 2145 Sutlle Ave. Copy To: Company Name: Charlotte, NC 28209 Address, I I ReguTatory Agency Email'. krohem.adams@ameddenburgcountync.gov Purchasc,Order#. Pace Owe: j Phone: (980)314856 Far J Project Name, Compost Cernraf 1 Pace Project Manager. tthew. brainard pacelabs com. f 1 State f Location Requested Due Data, Project #; - Pace Profile #: 3207-1 1 NC Raelvastod Anal sis Filtered (YIN) 0 Z "Tmz CODE a ° COLLECTED Z Preservatives > m m 0rnk119 W2Ir DW W.I. wT U O wain, ur w u ? otlu P SAMPLE ID s 05.4tl 5L III z a, oL _ r3 START END one Character per box. w,p� wp y ...- IA-2.0-91. •} a. 01h,OT O m a Sample Ids must be unique 7— T5 K O c m o U cr I�LI I- ra- a ti `a u O n y n O Z u m r Q p o n a a l l •, wT11TET.1 DATE TIME �. a s x x z LL s 1 fi 3 3 1 IXIXIY III I X111Y XIY XJXJ I c�_�_G iOgI ttoi z 3. 4' sr- 6 9 i �i 2y' LL I I ,.. - �AUDITIONAI• COMMENTS �' "� '- '- - * RELINOUISRED BYfAFFILWTIONr 'DATE''; ;TIME P:CEPTED eY. r AFFILIATION. 'DATE ,'61Ali . SAMPLECONDITIONS_ .- SAMPLE_RASJRE _.NMEANDIGNATI PRINT Name of SAMPLER: l i 1 m - a `w i m y`- m o a ' m > E o i 19 Y SIGNATURE of SAMPLER: DATE Signed: j } ' �7� _ Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 02/16/2018 CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME Mecklenburg County Compost Central COUNTY _ Mecklenburg County PERSON COLLECTING SAMPLES Khaliem Adams LABORATORY: Pace Analytical Services lab Cert. # 92 Comments on sample collection or analysis: Sampled During First -Flush Part A: Stormwater Benchmarks and Monitoring Results period3 SAMPLE COLLECTION YEAR 2018 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec or ® Monthly' February (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑water Supply [:]SA ❑Other RECEIVE© FEB 2 0 2Tostal event rainfall z 0.25 in or ❑ No discharge this CENTRAL FILE$ Date Sample Collected' (mo/dd/yr) Outfall No. TSS COD Fecal coliform LlVVM Ora- Total nitrogen . v,e Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks =__> 100 mg/L4 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 02/07/2018 1 475 117 555 0.54 0.62 0.032 0.013 0.043 6.8 02/07/2018 2 553 1140 6000 4.2 8.0 0.040 0.020 0.21 6.0 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. s For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 4The TSS benchmark value is 100 mg/L; except when discharging to ORW, FIQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 rari 13: venicie iviaintenance Area ivionixoring Kesuits: only Tor Tacmues averaging > 55 gal OT new mot Date Sample Collected' (mo/dd/yr) Outfall No. pH TPH using method 1664A SGT-HEM T55 Total Rainfall' Check if No Flow This Period3 Average New Motor Oil Usage 6-9 15 mg/L 100 mg/L4 - - 02/07/2018 1 6.8 <5.0 475 0.25 75 gal/month 02/07/2018 2 6.0 <5.0 553 0.25 Click Here to enter text. Footnotes from Part A also anoly to this Part B x oil/month. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® No ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an oriainal and one copv of this DMR. includina all "'No Discharae" reoorts. within 30 dovs of receiot of the lab results for at end of monitorina period in the case of "No Discharae" reports} to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." kw7itDate: a orrvermitiee) Pe10/1/2011-9/30/2016 /r✓, (Dat } Last Revised 12/02/11 Page 2 of 2 J :a Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfrlling out thisform, please visit https://deg.nc.vov/about/divisions/energy-mineral-land- resources/eneerg0/0/ y��- infineraI-land-permits/stormwater-permits/npdes-industHal -skv#tab-4 !! Permit No.: NICK I �/ / V/ U / tll 01 or Certificate of Coverage No.: NICIG/g/1-0ll! I �1 Facility Name: MeckleAbVAS L O D r County: Phone No. 63 - D r Inspector: Date of Inspection: O o� d o Time of Inspection: Total Event Precipitation (inches): 0• � S— All permits require qualitative monitoring to be performed during a `'measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DI ---MLR Regional Office. By this signature, 1 certify that this report is accurate and complete to the best of my knowledge: (Signature of permittee or Designee) 1. Outfall Description: OutfalI No. 1 Structure (pipe, ditch, etc.). - Receiving Stream: be the industrial activities that occur within the outfail drainage area: Page 1 of 2 SWt1-242, Ust modified 07/28/2017 2. Color: Describe the color of th discharge ufing (light, medium, dark) as descriptors: Vt' 3. Odor: Describe ny distinct odors tha 4 thG di chlorine odor, etc.):( is colors (red, brown, blue, etc.) and tint 1r-)Ian may have (i.e., smells strongly of oil, weak 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 0 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 D 5 7. Is there any foam in the stormwater discharge? O Yes C No. Nb 8. Is there an oil sheen in the stormwater discharge? 0Yes VNo. 1" D 9. Is there evidence of erosion or deposition at the outfall? O Yes 6/ No. A to. Other Obvious ndicators of Stormwater Pollution: List and describe N J 0 In�+n r S Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017 Emirmmenral Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfilling out thisform, please visit https:l/deg.jic.s ox,/about/divisioiis/eiierey-mineral-land- resourceslenergy-m in era] -I and-perniks/sto rmwater-perni its/npdes- i nd ustrial-sw#tab-4 Permit No.: NICI�I d1 V 1 0/0/0/ 0l or C%tificate of CoveKage No.: NICIG/-2/ Vl d/ Q/ 1.161 IffiffIg"Idd _Phone No./ It . Time of Inspection: Total Event Precipitation (inches): V' ;�- is All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, 1 certify that this report is accurate and complete to the best of my knowledge: L (Signature of Permittee or Designee) 1. Outfall Description: Outfall No.� Receiving Stream: Structure (pipe, ditch, etc.): Al� , Ott ( Vt/i 1 the 4ndustAial activities that occur within the outfall drainage area: Page 1 of 2 5WU-242, last modified 07/2812017 2. Color: Describe the color of tNL isctarge,ttsing basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: f r'W Yi r I Odor: Describ an distinct 9qdors that the discharge a have (i.e. smells s ongly of oil, weak chl rim odor, etc.: , (aU !1� ; Y'r 41 V Aa o, Al r n vv, on ;vt t, nr / T j,)) iA I =4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 2 3 `./ 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. is there any foam in the stormwater discharge? VYes O No y�5 8. Is there an oil sheen in the stormwater discharge? OYes Q�No, /VD 9. Is there evidence of erosion or deposition at the outfall? O Yes cV No. PJ D 10. Other Obvious Indicators of Storm�wJatenr�,P-ollution: List and describe �D tl or+l!-'�C'ex+o rs . MIA pav �lo-n Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/29/2017 aceAnalj cal www.paceiabs.com February 15, 2018 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: Compost Central 1 Pace Project No.: 92372338 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on February 07, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste fkc 3NI REPORT OF LABORATORY ANALYSIS This report shay not be reproduced, except in full, without the wntten consent of Pace Analytcal Services, LLC. Page 1 of 19 (�IaneAnalytical w,m paeelabs o" Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)875-9092 CERTIFICATIONS Project: Compost Central 1 Pace Project No.: 92372338 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #; 99006001 LouisianatNELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VrginiafVELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification lDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #; 99030001 VirginiafVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 2 of 19 (�IaneAnalytical www.paceiabs.com SAMPLE ANALYTE COUNT Project? Compost Central 1 Pace Project No.: 92372338 Pace Analytical Services, LLC 9800 KinceyAve, Suite 100 Huntersville, NC 28078 (704)B75-9092 Lab 1D Sample ID Method Analysts Analytes Roported Laboratory 92372338001 Outfall 001 EPA 1664B JMS 1 PAS(-C EPA200.7 SH1 3 PASI-A SM 9222D KDF 1 PASI-C SM 2540D MJP 1 PASI-A EPA 9040 KDF1 1 PASI-A TKN+NO3+NO2 Calculation DMN 1 PASI-A EPA 351.2 AES2 1 PASI-A EPA 353.2 CJH 1 1 PASI-A EPA 365.1 AES2 1 PASI-A SM 52200 NAL 1 PASI-A 92372338002 Outfall 002 EPA 1664B JMS 1 PASI-C EPA200.7 SH1 3 PASI-A SM 9222D KDF 1 PASI-C SM 2540D MJP 1 PASI-A EPA9040 KDF1 1 PASI-A TKN+NO3+NO2 Calculation DMN 1 PASI-A EPA 351.2 AES2 1 PASI-A EPA353.2 CJH1 1 PASI-A EPA 365.1 AES2 1 PASI-A SM 5220D NAL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 19 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Compost Central 1 Pace Project No.: 92372338 Sample: Outfall 001 Lab ID: 92372338001 Collected: 02107/18 12:13 Received: 02107l18 13:12 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons NO mg/L 5.0 1 02/08/18 04:50 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 0,032 mg/L 0,0050 1 02/08/18 05:00 02/13/18 00:14 7440-50-8 Lead 0.013 mg/L 0.0050 1 02/08/18 05:00 02/13/18 00:14 7439-92-1 Zinc 0.043 mg/L 0.010 1 02/08/18 05:00 02/13/18 0014 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D Fecal Coliforms 555 CFU1100 mL 1.0 1 02/07/18 16:08 ul 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 475 mg/L 69.4 1 02/09/18 08:56 9040 pH Analytical Method: EPA 9040 pH 6.8 Std. Units 0.10 1 02/09/18 10:38 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 2.8 mglL 0.52 1 02/13/18 10:00 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 2.3 mg/L 0.50 1 02/10/18 12:54 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Nitrogen, NO2 plus NO3 0.54 mg/L 0.020 1 02/09/18 04:48 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 0.62 mg1L 0,050 1 02/09/1813:31 7723-14-0 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 117 mg/L 25.0 1 02/13/18 11:57 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02115/2018 05:39 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 19 (�IaeAnalytical wwwpacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Compost Central 1 Pace Project No.: 92372338 Sample: Outfall 002 Lab ID: 92372338002 Collected: 02/07/18 12:13 Received: 02/07118 13:12 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT HEM, TPH Analytical Method: EPA 16648 Total Petroleum Hydrocarbons ND mg1L 5.0 1 07/08/18 04:50 2D0.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 2D0.7 Copper 0,040 mg1L 0.0050 1 02/08/18 05700 02/13/18 00:17 7440-50-8 Lead 0.020 mg1L 0.0050 1 02/08/18 05:00 02/13/18 00:17 7439-92-1 Zinc 0.21 mglL 0.010 1 02/08/18 05:00 02/13/18 00:17 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D Fecal Coliforms 6000 CFUl100 mL 1.0 1 02/07/18 16:08 u2 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 553 mg1L 83.3 1 02/09/18 08:56 9040 pH Analytical Method: EPA 9040 pH 6.0 Std. Units 0.10 1 02/09/18 10:38 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 20.6 mg1L 0.52 1 02/13/18 10:00 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 16.4 mg1L 0.50 1 02/10/18 13:20 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Nitrogen, NO2 plus NO3 4.2 mglL 0.020 1 02/09/18 06:39 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 8.0 mglL 0.25 5 02/0911815:09 7723-14-0 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 1140 mglL 50.0 2 02/13/18 11:57 M1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/15/2018 05:39 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 19 aceAnalyticalm www.pacelabs.com QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92372338 QC Batch: 397162 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92372338001, 92372338002 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 METHOD BLANK: 2202542 Matrix: Water Associated Lab Samples: 92372338001, 92372338002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg1L ND 5.0 0210B118 04:38 LABORATORY CONTROL SAMPLE: 2202543 Spike 1-CS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L 20 19.2 96 64-132 MATRIX SPIKE SAMPLE: 2202544 92371979002 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 19.8 97 64-132 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/15/2018 05:39 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 19 aceAnalytrcal wwwpac&abs.aam QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Compost Central 1 Pace Project No.: 92372338 QC Batch: 397151 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92372338001, 92372338002 METHOD BLANK: 2202497 Matrix: Water Associated Lab Samples: 92372338001. 92372338002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper mg/L NO 0.0050 02/12/18 22:56 Lead mg/L NO 0.0050 02/12118 22:56 Zinc mg/L ND 0.010 02/12118 22:56 LABORATORY CONTROL SAMPLE: 2202498 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg/1- .5 0.48 97 85-115 Lead mg/L .5 0.43 87 85-115 Zinc mg/L .5 0.45 90 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2202499 2202500 MS MSD 92372229003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg1L ND .5 .5 0.48 0.48 95 96 70-130 1 Lead mg1L ND .5 .5 0.44 0.44 87 87 70-130 0 Zinc mg1L 11.8 .5 .5 0.47 0.47 91 91 70-130 1 ug1L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2202501 2202502 MS MSD 92372269009 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg1L NO .5 .5 0.50 0.50 99 99 70-130 0 Lead mg1L NO .5 .5 0.43 0.43 86 87 70-130 1 Zinc mg1L NO .5 .5 0.45 0.46 91 91 70-130 0 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/15/2018 05:39 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 19 aceAnalytical wwwpacefabs.com QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92372338 QC Batch: 397296 Analysis Method: SM 9222D QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - CHT Associated Lab Samples: 92372338001, 92372338002 METHOD BLANK: 2203160 Matrix: Water Associated Lab Samples: 92372338001, 92372338002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU1100 mL NO 1.0 02/07/18 16:08 SAMPLE DUPLICATE: 2203187 92372338002 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU1100 mL 6000 600 164 u2 Pace Analytical Services, LLC 9800 Kircey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shay not be reproduced, except in full, Date: 02/1512018 05:39 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 19 (�IaoeAnalXical www.pacwfaftcorn QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92372338 QC Batch: 397333 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92372338001, 92372338002 METHOD BLANK: 2203548 Matrix: Water Associated Lab Samples: 92372338001, 92372338002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 02109/18 08:52 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2203549 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 242 97 90-110 SAMPLE DUPLICATE: 2203550 92372385001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 2203551 92372237003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 61.0 61.0 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/15/2018 05:39 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 19 aceAnalytical W w.pacefabs.com QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 9237233E QC Batch: 397238 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92372338001, 92372338002 SAMPLE DUPLICATE: 2202927 Parameter pH 92372040001 Dup Units Resull Result Sid. Units 5.2 5.2 RPD Qualifiers 0 H6 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)B75-9092 Results presented an this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02I1512018 05:39 PM without the written consent of Pace Analytical Services, LLC, Page 10 of 19 acmnalytical W%Vw.pacefaba wm QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92372338 QC Batch: 397152 Analysis Method: EPA 351.2 QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN Associated Lab Samples: 92372338001, 92372338002 METHOD BLANK: 2202503 Matrix: Water Associated Lab Samples: 92372338001, 92372338002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 02110/18 13:15 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9D92 LABORATORY CONTROL SAMPLE: 2202504 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 10.7 107 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2202505 2202506 MS MSD 92371990002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 2.7 10 10 13.8 13.4 111 107 90-110 3 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2202507 2202508 MS MSD 92372328004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L ND 10 10 9.2 11.4 90 112 90-110 22 M1,R1 Results presented on this page are In the units Indicated by the "Units- column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02115/2018 05:39 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 19 acmnalytrcal www.pacelabs.00m Project: Compost Central 1 Pace Project No.: 92372338 QC Batch: 397294 QC Batch Method: EPA 353.2 Associated Lab Samples: 92372338001. 92372338002 METHOD BLANK: 2203153 Associated Lab Samples: 92372338001, 92372338002 Parameter Units Nitrogen, NO2 plus NO3 mg/L QUALITY CONTROL DATA Analysis Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.020 02/09/18 04:25 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 1 OD Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2203154 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2203155 2203156 MS MSD 92372571001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg1L 0.81 2.5 2.5 3.2 3.2 96 96 75-125 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2203157 2203158 MS MSD 92372269009 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L ND 2.5 2.5 2.4 2.4 95 95 75-125 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/15/2018 05:39 PM without the written consent of Pace Analytical Services, LLC, Page 12 of 19 aceAnalytrcal www.pacalabscam QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92372338 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HuntersvjRe, NC 28078 (704)875-9092 QC Batch: 397310 Analysis Method: EPA 365.1 QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92372338001. 92372338002 METHOD BLANK: 2203298 Matrix: Water Associated Lab Samples: 92372338001, 92372338002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0,050 02/09/1813:26 LABORATORY CONTROL SAMPLE: 2203299 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2203300 2203301 MS MSD 92372269008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result %6 ReC % Rec Limits RPD Qual Phosphorus mg1L ND 2.5 2.5 2.5 2.5 100 102 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2203302 2203303 MS MSD 92372401006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg[L ND 2.5 2.5 2.6 2.6 103 104 90-110 2 Results presented on this page are in the units Indicated by the" Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/15/2018 05:39 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 19 acmnalytical ® www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 2807E (704)875-9092 Project: Compost Central 1 Pace Project No.: 92372338 QC Batch: 397619 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92372338001. 92372338002 METHOD BLANK: 2205245 Matrix: Water Associated Lab Samples: 92372338001, 92372338002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 02/13/18 11:57 LABORATORY CONTROL SAMPLE: 2205246 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 740 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2205247 2205248 MS MSD 92372038001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Chemical Oxygen Demand mg/L 44.0 100 100 129 132 85 88 90-110 2 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2205249 2205250 MS MSD 92372338002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Chemical Oxygen Demand mg/L 1140 100 100 1280 1270 136 122 90-110 1 M1 Results presented on this page are in the units Indicated by the -Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, •Date: 0211512018 05:39 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 19 aceAnalytrcalm www.pacefabs.com QUALIFIERS Project: Compost Central 1 Pace Project No.: 92372338 DEFINITIONS Pace Analytical Services, LLC 9800 KinceyAve, Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAS I -A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H6 Analysis initiated outside of the 15 minute EPA required holding time. 101 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. u1 Results based upon colony counts outside acceptable range. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0211512018 05:39 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 19 ace Analytical www.pacelabs.cw I Project: Compost Central 1 Pace Project No.: 92372338 Lab ID Sample ID 92372338001 Outfal l 001 92372338002 Outfall002 92372338001 Outfal l 001 92372338002 Outfall002 92372338001 Outfal 1001 92372338002 Outfall002 92372338001 Outfal 1001 92372338002 Outfall002 92372338001 Outfal 1001 92372338002 Outfall002 92 372338001 O utfal 1001 92372338002 Outfall002 92372338001 Outfal 1001 92372338002 Outfall002 92372338001 Outfal l 001 92372338002 Outfall002 92372338001 O utfal 1001 92372338002 Outfall002 92372338001 O utfall 001 92372338002 Outfall002 Date: 02/15/2018 05:39 PM QUALITY CONTROL DATA CROSS REFERENCE TABLE QC Batch Method EPA 16649 EPA 1664E EPA 200.7 EPA 200.7 SM 9222D SM 9222D SM 2540D SM 2540D EPA 9040 EPA 9040 TKN+NO3+NO2 Calculation TKN+NO3+NO2 Calculation EPA 351.2 EPA 351.2 EPA 353.2 EPA 353.2 EPA 365.1 EPA 365.1 SM 5220D SM 5220D QC Batch 397162 397162 397151 397151 397296 397296 397333 397333 397238 397238 397774 397774 397152 397152 397294 397294 397310 397310 397619 397619 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kinrey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Analytical Method Batch EPA 200.7 397218 EPA 200.7 39721 B Page 16 of 19 Document Name: Document Revised: January 24, 2018 �awnaljtical" Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: issuing Authority: � F-CAR-CS-033-Rev.05 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville Raleigh❑ Mechanicsville[] Client Name: WO# : 92372338 ❑ Project H. I` l�lll�l�11 Courier: Fed Ex UP5 1 EJUSPS ❑ Commercial []Pace ❑0ther; 1111912 iiii311723318 Custody Seal Present? ❑Yes 1--E1Ho Seals Intact? Des QfTo j 1 Date/Initials Person Examining Contents: Packing Material: ❑Bubble Wrap []Bubble Bags None El Other Thermometer: Type of Ice: Wet ❑slue ❑IR Gun ID: 92T036 — CoolerTemp ('C): _ Correction Factor: Add/Subtract {'C) +0.1 Cooler Temp Corrected ('C): _1 � s _, USDA Regulated Soil ( A, water sample) Did samples origin I a quarantine zone within the United States: CA, NY, or 5C (check maps)? Flypc n Biological Tis a Frozen? Elyes o s❑N/A ❑gone Tema shcul ,be above freezing to 6'C p es out of temp criteria. Samples on lCe, cooling process as begun Did samples originate from a foreign source {intemati ally, inrludin¢ Hawaii and Puerto Rico)? []YesI a Comments/Discre ancy: Chain of Custody Present? es ❑No ❑NJA 1. Sam lesArrived within Bold Time? Yes [-]No ❑NJA 2. Short Hold Time Analysis (02 hr.)? ❑Yes •. N6 []N/A 3. Rush Turn Around Time Requested? ❑Yes _ No ❑NJA 4. Sufficient Volume?. Yes ❑No ❑N/A' 5. Correct Containers Used? -P ace Conta ine rs Used ? lffYes es .[]No❑N/A ❑No ❑NIA 6. Containers Intact? R< ❑N [-]N/A 7. Dissolved analysis: Samples Field Filtered? Dyes. No []NIA 8. Sample Labels Match COC7 -Includes Date/Time/ID/Analysis Matrix: Yes Vd ❑Na ❑NIA 9. Headspace in VOA Vials (a5-6mm)? ❑Yes ❑No NIA SU. Trip Blank Present? Trip Blank Custody Seals Present? [-]Yes Dyes - No ❑No ❑NJA N/A COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/ RESOLUTION Person contacted: Date/Time: Field Data Required? ❑Yes ❑No Project Manager SCURF Review: , Date: Project Manager SRF Review: w Date: Page 17 of 19 aceAnalytrcal Document Name: Sample Condition Upon Receipt(SCUR) Document Revised: January 24, 2018 Page 2 of 2 Document No.: F-CAR-CS-033-Rev.05 Issuing Authority; Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is Project 9 verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/9015 (rater) DOC, LLHg **Bottom half of box is to list number of bottle WO#:92372338 PM: MWB Due Date: 02/14/18 CLIENT: 92—MECK CO 2 Z N C0. m Z Z N ro z 2 .a C n73 J 4 w Z di0 a_ U x m v 0 m a J v eo � a U T a 2 a J z v AGi w = m m D a E 4 y V Y E 4 U Z u a y E a J v a Q O .a E a x a O = 6 _z S Z a 4 0 N Z v 4 O > 4 Z 0 O > Z a O > = V a O �! ? y O a N Y = I a ¢ Z z z vi _ m v O a J v 2 m C 0 Z _ E M a m yNE� N 7 aa.. torn E Q n `w n i as € N VI a M E Z a w yE7 N N a m i N U a m a 3 LL O 3 m ri C07 a `m ri _ 0 a E vNl 0 a w 10 a E N H U a m a a U a E 0 q 2 0 a E p q F- ID > E O Lo > E O q 0. la o `p Y O > ° V Y � > E ry N �- a v E s,n N a y E LA N 4 a m y u E 1 2 { lr 3 4 5 5 8 9 10 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot p Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of t4{s form will be sent to the North Carolina DEHNR Certification Of Ice {Le. Out"of hold, incorrect preservative, out of temp, incorrect containers. Page 18 of 19 CHAIN -OF -CUSTODY 1 Analytical Request Document "' 'Awca! Site Chaim -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Required Client Infom+atl— Required Project Information: Invoice information: Pa 8 : t Of 1 Cornpory: Mecklenburg County solid Waite Report To; Khaliem Adam$ Attention: Address: 2145 SuWe Am Copy To: Company Name: CharloOe, NC 213208 Address: 7� '' . R ulato -A on j,0" �`:'i'� +"` • ' Email khaliem,adams mecklenburgcounl nc.gav purchase Order iF: Pace Quote: Phone: (680)314-3856 Fax Project Name: Compost Central 1 Pate Project Manager. matthew.blainard pacelabs.tom, - ' State? I-OmdOri-+- Requested Duo Data: Project #: Pace Profile 4: 3207-1 NC Re uitsted Anal Is Filtered !N MATRIX CODE A ° COLLECTED z Preservatives " o D.i,-jW la Dw v " O Wain WT wn>e wam i plo -! P SAMPLE ID so+usam o� One Character per box. wro. '^� v START END o u a m H ,m Z m a t LI J c AI, AR (R-Z, 4.9 1. -) olt� oT o n = ¢ 'd m m M o ,N �. o o. .o m tT n m a m Q Sample ids must be unique 71— Ts x W p U m v O to H U Lu s a a O O _ = vr'i N c Q G r Q -Z Q- w DATE DATE q m O a � N r=; Z U 2 z i O i N ti D c� LL� O w - = a tY -- IT{IME/ �,f�� jTIME i•lr� - + CO _I Oulfall Dot WT ! 1j `30 r Ii 1S 7( x X X X -3..2' ��l��1 7l 4i �L 7( ryC . Oudall 002 '1JT 17�f v T f+� L+ 7( X X X X X X 3 4 6 7 10• -11 . E 12 , r .71&" _LJNOUIS 06Y.l AFFIUATIpN -- a DATE= T{ME ti — �.•€� -ACCEPTED 6YlAFFRJ/1TiON• ' .DATE — "rLTiME �� F?'.,A +'$AMPLE CON6m°NS "y ;rl ,:7�; v..t.. _ - yr „l- •0 SAMPLERNAtdEANDStGNAT1IRE._ N" PRINT Name of SAMPLER:' m $ SIGNATURE of SAMPLER: ' f DATE Signed: c° r m } Y N N i O , r O WaaVR° � c � o U G ' o .� �1�f►y RTN cnRo�® MECKLENBURG COUNTY Land Use & Environmental Services Agency Solid Waste December 20, 2017 Central Files NCDI?NR / DWQ 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention: Central Files Subject: Discharge Monitoring Reports (November) Compost Central — Certificate of Coverage No. NCG240016 Dear Central Files: RF�:FIN/ FD JAN 0 9 2018 PROCESSING UNIT Please find enclosed the Discharge Monitoring Reports for November 2017 for Compost Central, a Type I facility located at 5631 West Blvd in Charlotte, North Carolina. As indicated in the report, there were no qualifying flows that could be sampled for either period. If you have any questions, please contact me at 704-634-7705 or by email at Khalierrt.adams(�,)mecklcnbur =c, ountync.gov Sincerely, Z� I adz,� Khalicm Adams Solid Waste Environmental Specialist Enclosed: 2017 DMRs PEOPLE • PRIDE PROGRESS • PARTNERSHIP 2145 Sutt[e Avenue Char[otte. North Carolina 28208 www.wipeout%vaslexom Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 12/20/17 CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME Compost Central COUNTY Mecklenburg Count PERSON COLLECTING SAMPLES Khaliem Adams LABORATORY: Pace Analytical Services Lab Cert. # 192 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec or ® Monthly' November (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply [:]SA ❑Other Total event rainfall 2 or ® No discharge this period3 Date Sample Colle Collected' (mo/ cted C+utfall No. T55 COD Fecal conform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks =__> 100 mg/L" 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.007 mg/L 0.03 mg/L 0.067 mg/L 6-9 1 2 ' Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ' For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. "The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part B: Venicie IWalntenance Area Ivlonitoring Kesuits: only Tor Tacilives averaging > 55 gal or new mot Date Sample Collected' (mo/dd/yr) Outfall No. PH TPH using method 1664ASGT-HEM T55 Total Rainfall' Check if No Flow This Period3 Average New Motor Oil Usage 6-9 15 mg/L 100 mg/L4 - 1 X 2 X Footnotes from Part A also aooly to this Part B FOR PART AAND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. or oil/month. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an oriainal and one coov of this DMR, including all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharae" reuortsl to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." / z z c /-7- (Date) te: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 2 of 2 i Environmental { �l Quality 34N 3 Stormwater Discharge Outfall (SDO) t 'Ll Qualitative MonitoringReport owR �EcTlON horguidance onfilling out thisf rnt, please visit litti)s://deq.nc.gov/about/divisions/energy-miiter<a]-land- resources/energy-m_i neral-land-nermitslstormwater-permits/npdes-industrial-swMab-4 r Permit No.: NICI�I 1_I I 1 1 I or Certificate of Coverage No.: NICIG/OAljdll �l Facility Name:_(���,� 2 County: 10 Irf Phone No. �. i) t� } b Inspector: S Date of Inspection: 0 i I dZ ao t Time of Inspection: 0 5 C ^ Total Event Precipitation (inches): d. All permits require qualitative monitoring to be performed during a `'measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: /' . A (Signature of Permittee or Designee) 1. Outfall Description: I Outfali No. 91 Structure (pipe, ditch, etc.): r' eOel Receiving Stream: be the i ydustr al activities that occur within the Outfall drainage area: Page I of 2 SWU-242, I xst modified 07/28/2017 2. Color: Describe the color of the discharge (light, medium, dark) as descriptors: l ± 3. Odor: Descri chlorine odor, etc.): _ is colors (red, brown, blue, etc.) and tint distinct odors that the discharge may have (i.e., smells strongly of oil, weak 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: ��1��1 ] 2 � 3 J 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: ni 2 3 4 5 7. Is there any foam in the stormwater discharge? O Yes c3i No. 8. Is there an oils sheen in the stormwater discharge? 0Ycs m No. 9. Is there evidence of erosion or deposition at the outfail? O Yes 0 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Lust modified 07/2812017 MECKLENBURG COUNTY. Land Use & Environmental Services Agency Solid Waste January 25, 2018 Central Files RECP1VED NCDENR / DWQ JAN 3 1 2018 1617 Mail Service Center Raleigh, North Carolina 27699-1617 CENTRAL FILE`' Dil R SECTION Attention: Central Files Subject: Discharge Monitoring Report Compost Central — Certificate of Coverage No. NCG240016 Dear Central Files: Please find enclosed the Discharge Monitoring Report, January 2018, for Compost Central, a Type I facility located at 5631 West Blvd in Charlotte, North Carolina. If you have any questions, please contact the at 704-634-7705 or by email at khaliem.adams�mecklenbur 7c�tync.gOV Sincerely, rr` Khaliem Adams Solid Waste Environmental Specialist Enclosed: 2018 DMR PEOPLE • PRIDE PROGRESS • PARTNERSHIP 2145 Settle Avenue Charlotte, North Carolina 282028 tiv titi° w. wi peout wastexo m Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 1/25/2018 CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME Compost Central COUNTY Mecklenburg Count PERSON COLLECTING SAMPLES Khaliem Adams LABORATORY: Pace Analytical Services Lab Cert. # 92 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec or ® Monthly) Janua month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply [_]SA ❑Other Total event rainfall z 0.17 in or ❑ No discharge this period' Date Sample Colle Collected' (mo/ cted Outfall No. TSS COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks 100 mg/L4 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 01/12/2018 1 - - - - - - - - - 01/12/2018 2 6.9 82.0 - 0.059 0.22 0.0064 <0.075 0.015 6.6 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. ZThe total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Fart ti: venicie Maintenance Area monitoring Kesuirs: only Tor Taciiives averaging > 55 gal oT new mot Date Sample Collected' (mo/dd/yr) Outfall No. pH TPH using method 1664A SGT-HEM TSS Total Rainfa112 Check if No Flow This Period' Average New Motor Oil Usage 6-9 15 mg/L 100 mg/L4 - - 10/23/2017 1 - - - - X 10/23/2017 2 6.6 <5.0 6.9 0.17 75 gal/month Footnotes from Part A also annlv to this Part B or oil/month. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an original and one copv of this DMR, includina all "No Discharae" reports. within 30 dovs of receipt of the lab results for at end of monitorina period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of (Dat . Permit Date: 16/1/2011-9/30/2016 Last Revised 12/02/11 Page 2 of 2 (�IaneAnalytical www.pacuiabs.com January 24, 2018 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: Compost Central 1 Pace Project No.: 92369542 Dear Darren Steinhilber: Pace Analytical $ervices, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on January 12, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khafiem Adams, Meclenburg County Solid Waste 2��e pG[R fQ��`nQ yx TNI , l9e0 A'f�� REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 17 laneAnalytical" wwwpacelabs.aam Project: Compost Central 1 Pace Project No.: 92369542 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Sie 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Flodda/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L.C. Page 2 of 17 (�IaoAnalytical" wwwpacelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HunlersOle, NC 28078 (704)875-9092 Project: Pace Project No.: Compost Central 1 92369542 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92369542001 Outfall 2 EPA 1664B JMS 1 PASI-C EPA200.7 SH1 3 PASI-A SM 2540D NAL 1 PASI-A EPA 9040 KMM 1 PASI-A TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 BRJ 1 PASI-A EPA353.2 DMN 1 PASI-A EPA365.1 CJH1 1 PASI-A SM 5220D NAL 1 PASI-A 9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 17 Pace Analytical Services, LLG 9800 Kinsey Ave. Suite 100 laceAnalyfical" Huntersville, NC 28078 MVW PaC&W&s•CDM (704)875-9092 ANALYTICAL RESULTS Project: Compost Central 1 Pace Project No.: 92369542 Sample: Outfall 2 Lab lD: 92369542001 Collected: 01/12118 09:14 Received: 01/12/18 10:44 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg1L 5.0 1 01/17/18 04:46 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 0.0064 mg11- 0.0050 1 01/14/18 09:40 01123/18 08:22 7440-50-8 Lead ND mg1L 0.0050 1 01/14/18 09:40 01123/18 08:22 7439.92-1 Zinc 0.015 mg1L 0.010 1 01/1411809:40 01/23/1808:22 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 6.9 mg1L 3A 1 01/17/18 17:46 9040 pH Analytical Method: EPA 9040 pH 6.6 Std. Units 0.10 1 01116/18 01:21 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 2.2 mglL 0.52 1 01/18/18 17:04 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 2.1 mglL 0.50 1 01/16/18 21:03 7727-37-9 353.2 Nitrogen, N021NO3 pres. Analytical Method: EPA 353.2 Nitrogen, NO2 plus NO3 0.059 mglL 0.020 1 01/18/18 14:41 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 0.22 mglL 0,050 1 01/17/18 04:40 7723-14-0 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 82.0 mg1L 25.0 1 01/18/18 21:39 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/24/2018 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 17 aceAnalytical www.paoNabs.rnm QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92369542 QC Batch: 394490 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92369542001 METHOD BLANK: 2187032 Associated Lab Samples: 92369542001 Parameter Units Total Petroleum Hydrocarbons mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 01/17/18 04:34 Pace Analytical Services, LLC 9800 Kincey Ave. SOe 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2187033 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L 20 19.5 98 64-132 MATRIX SPIKE SAMPLE: 2187034 35367646001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L 5.0U 20 19.2 96 64-132 Results presented on this page are in the units Indicated by the "Units" column except where an altemate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01124/2018 03:11 PM without the written consent of Pace Analytical Services, LLC, Page 5 of 17 (�IaclMnalytical wwwpacelabs.tbrh QUALITY CONTROL DATA Project: Compost Central i Pace Project No.: 92369542 QC Batch: 394218 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92369542001 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 2a078 (704)875-9092 METHOD BLANK: 2185564 Matrix: Water Associated Lab Samples: 92369542001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper mglL ND 0,0050 01/23/18 07A5 Lead mg1L ND 0.0050 01/23/18 07:45 Zinc mg1L NO 0.010 01/23/18 07:45 LABORATORY CONTROL SAMPLE: 2185565 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper mglL .5 0.53 107 85-115 Lead mg1L .5 0.48 96 85-115 Zinc mg1L .5 0.47 94 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2185566 2185567 MS MSD 92369086004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mglL 257 .5 .5 0.80 0.81 109 111 70-130 1 uglL Lead mglL ND .5 .5 0.50 0.50 99 99 70-130 0 Zinc mg1L 170 .5 .5 0.65 0,68 96 102 70-130 4 uglL MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 218556B 2185569 MS MSD 92369550002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Copper mglL 47.4 .5 .5 0.58 0.59 107 109 70-130 2 uglL Lead mglL ND .5 .5 0.49 0.50 97 100 70-130 3 Zinc mglL 485 .5 .5 0.94 1.0 92 105 70-130 7 uglL Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/24/2018 03:11 PM without the written consent of Pace Anatytical Services, LLC, Page 6 of 17 aceAnalyftfcal® wwwpacelabs.com QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92369542 OC Batch: 394545 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92369542001 METHOD BLANK: 2187242 Matrix: Water Associated Lab Samples: 92369542001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 01I17118 17:39 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2187243 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 244 98 90-110 SAMPLE DUPLICATE; 2187244 92369528011 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L NO ND SAMPLE DUPLICATE: 2187245 92369619DD1 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L ND ND Results presented on this page are In the units Indicated by the" Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2018 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 17 acmnalytical wativpacefabs,vom QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92369542 QC Batch: 394305 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92369542001 SAMPLE DUPLICATE: 2186014 Parameter pH 92369704001 Dup Units Result Result RPD Qualifiers Std. Units 6.5 6,5 1 H6 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/24/2018 03:11 PM without the written consent of Pace Analytical Services, I.I.C. Page 8 of 17 laneAnalyfical www.pacelabs.com QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92369542 QC Batch: 394199 Analysis Method: EPA 351.2 QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN Associated Lab Samples: 92369542001 METHOD BLANK: 2185504 Associated Lab Samples: 92369542001 Parameter Units Nitrogen, Kjeldahl, Total mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 01/16/18 20:45 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 2807B (704)875-9092 LABORATORY CONTROL- SAMPLE: 2185505 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.6 96 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2185506 2185507 MS MSD 92369602001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg1L ND 10 10 10.2 10.0 102 100 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2185508 2185509 MS MSD 92369442002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 11.0 10 10 23.1 22.6 121 116 90-11D 2 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/24/2018 03:11 PM without the written consent of Pace Analytical Services, LLC, Page 9 of 17 (�IaceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92369542 Pace Analytical Services, LLG 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 394638 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92369542001 METHOD BLANK: 2187575 Matrix: Water Associated Lab Samples: 92369542001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg1L ND 0.020 01/18/18 14:26 LABORATORY CONTROL SAMPLE: 2187576 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg1L 2.5 2.5 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2187577 2187578 MS MSD 92369528008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua! Nitrogen, NO2 plus NO3 mi ND 2.5 2.5 2.5 2.5 101 102 75-125 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT Of LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/24/2018 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 17 aceAnalytical wwwpacelabs.cam QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92369542 QC Batch: 394433 Analysis Method: EPA 365.1 QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92369542001 METHOD BLANK: 2186758 Matrix: Water Associated Lab Samples: 92369542001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg1L ND 0.050 01117/18 04:32 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704 )875-9092 LABORATORY CONTROL SAMPLE: 2186759 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Phosphorus mg/L 2,5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2186760 2186761 MS MSD 92369184005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg1L 0.11 2.5 2.5 2.7 2.7 102 102 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2186762 2186763 MS MSD 92369523001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone, Cone. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg1L 20.3 2.5 2.5 21.0 21.3 27 39 90-110 2 M1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in futi, Date: 01/2412018 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 17 (�5a'ne Analytical www.pacoiabs.com QUALITY CONTROL DATA Pate Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)B75-9092 Project: Compost Central 1 Pace Project No.: 92369542 QC Batch: 394473 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92369542001 METHOD BLANK: 2186959 Matrix: Water Associated Lab Samples: 92369542001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 01/18/18 21:39 LABORATORY CONTROL SAMPLE: 2186960 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 764 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2186961 2186962 MS MSD 92369193005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mglL 1990 100 100 2300 2350 308 362 90-110 2 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2186963 2186964 MS MSD 92369184007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 80.0 100 100 164 171 84 91 90-110 4 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/24/2018 03:11 PM without the written consent of Pace Analytcal Services, LLC. Page 12 of 17 (�IaneAnalytical" www.paoalabsxom QUALIFIERS Project: Compost Central 1 Pace Project No.: 92369542 DEFINITIONS Paco Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrytonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H6 Analysis initiated outside of the 15 minute EPA required holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2018 03:11 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 17 acmnalyfrcal wwwpoculabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Compost Central 1 Pace Project No.: 92369542 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huniersville, NC 28078 (704)875.9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92369542001 Outfall 2 EPA 1664E 394490 92369542001 Outfall 2 EPA 200.7 394218 EPA 200.7 92369542001 Outfall 2 SM 2540D 394545 92369542001 Outfall 2 EPA 9040 394305 92369542001 Outfall2 TKN+NO3+NO2 394694 Caiculation 92369542001 Outfall 2 EPA 351.2 394199 92369542001 Oulfall 2 EPA 353.2 394638 92369542001 Outfall 2 EPA 365.1 394433 92369542001 Outfall 2 SM 5220D 394473 Date: 01124/2018 03:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 394243 Page 14 of 17 Document Name: Document Revised: August 4, 2017 Sample Condition Upon Recelpt(SCUR) Page 1 of 2 r c?CBAITalyfiCtir� Document No.: Issuing Authority: F-CAR-CS-031-Rev.04 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville Ef Raleigh❑ Mechanicsville[] • • . Client Name: WO# : 92369542 • aject 9: Courier: Fed Ex 00PS ❑LISPS �ftpnt k ❑ Commercial ❑Pace ❑Other: 92369542 Custody Seal Present? ❑Yes No Seals Intact? Des z Kmo 7 Date/Initials Person Examining Contents-,-7 Packing Material-. []Bubble Wrap 081bble Bags ❑None ❑ Other Biological Tissue Frozen? Thermomet r.' ' ' �(/ J a,/ ❑Yes ❑Na �]N/A al,GunID: , , / �'�f1s'%et ❑Blue ❑None Type of co:I Correction Factor: Cooler Temp Corrected 1'Cj: �� Temp should be above freezing to G'C ❑Samptes out of temp criteria, Samples on ice, cooling process has begun USDA Regulated Soil ( N/A, water sample) Did samples orlgl4ate In a quarantine tone within the United States: CA, NY, ur SC (check maps)? Did samples originate from a foreign source (intern (y, Ayes No includine Hawaii and Puerto Rico)? MYes FlNo Cam ments/D'rscrepan cy: Chain of Custody Present? QNo N/A 1. Samples Arrived within Hold Time? Yes 0 N N/A 2. Short Hold Time Analysis 02 hr.)? QYes Na ❑N/A 3. Rush Turn Around Tlme Requested? CJYes ElNo NIA 4. Sufficient Volume? Yes ❑No ❑N/A 5. Correct Containers Used? -Pace Containers Used? y Yes ❑No CIMO ❑N/A ❑N/A 6. Containers Intact? rJfYs ON. N/A 7. Dissolved analysis: Samples Field Filtered? ❑yes No NIA B. Sample Labels Match COC? -includes Date/Time/ID/Analysis Matrlx: es ❑No ❑N/A 9. heads ace in VOA Vials (>5.6mm)? Qyes ❑N rv/A I0. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes oYes allo LINo ❑N/A N/A 11. CLIENT NOTIFICATION/RESOLUTION Field Data� Required? ]Yes I_iNo Person Contacted:tt _ �1 � , ZI t _A&r.,— Date/Time: i � � (� I b . 3 Comments/Sample Discrepancy: Lot Ip of split containers: a Project Manager SCURF Review: Date: l� Project Manager SRF Review: L Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out oftemp, incorrect containers) Page 15 of 17 rn 0 M 3 is O 1 0 a m < a c R x v 3 n Q ❑ m C w m s rr 3 n ro � 3 rt ` r ^- O 3 � n c Q � 6 ro CL c 23 �� rA N n 3 m p a 4 � n n A S m < R 0 a N O Itcmp 8111411-325 mL Plastic Unpreserved (N/A) (CI-) OP3U-250 mL Plastic Unpreserved {N/A) OP2U-S00 mL Plastic Unpreserved (N/A) 9P1U-1 liter Plastic Unpreserved (N/A) i t^ SP45-125 mL Plastic H2504 (pH < 2) (CI-) BP3N-250 mL plastic HNO3 (pH < 2) XXXBP4Z-125 mL Plastic 2N Acetate & NaOH (>9) BP4C-125 mL Plastic NaDH (pH > 12) (CI-) WGFU-Wide-mouthed Glass jar Unpreserved AGSU-1 liter Amber Unpreserved (N/A) (CI-) AG3H-1 liter Amber HO (pH < 2) AGSU-250 mL Amber Unpreserved (N/A) (Cl-) A615-1 liter Amber 142504 (pH <21 AG35-250 mL Amber H2SO4 (pH < 2) za� z AG3A(OG3A)-250 mL Amber NH4CI {N/A){CI-) OGSH-40 mL VOA HC! (N/A) VG9T-40 mL VOA Na25203 (N/A) VG9U-40 mL VOA Unp (N/A) , OG9P-40 mL VOA H3PO4 (N/A) VOAK (6 vials per kitj-5035.kit (N/A) V/GK 13 vials per kit)-VPH/Gas kit (N/A) 5PST-125 mL Sterile Plastic (N/A -lab) SPZT-250 mL Sterile Plastic (N/A - lab) BP3A-750 mL Plastic (NH2)2504 (9.3-9.7) Cubitainer VSGU-20 mL Scintillation vials (N/A) - GN f O 3 .°: C. lu 7 7 Cr - S s m X tnn — rn S O p O' n X IA 1'f C d Cr Cun 1Tt 7 ro C. Cu ' C W O Cr r4 m C o a O 7 IN a 3 o. ro 0 V ,� eafa�rvzl CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section 8 Section C Required Client Information: Required Project Information: Invoice Information: Pape: 1 Qf 1 Company; Mecklenburg COUrlty Solid Waste Report TO' Khahem Adams Attention: Address: 2146 Suule Ave_ Copy To: Company Name. Charlotte, NC 28208 Address: R ulato Agency Email khWlem,adams mecklenburgceuntync,gov Purchase Order #: Pace Quote: Phanc: j366j314-3tS56 Fax Project Name: Compost Central 1 Pace Project Manager. matthew-brainard pacelabs. mm, - State f Location Requested Due Date: Project 4: i Pace Profile #: 3207-1 NC R uested Analysis Filtered YIN - - - MATRIX CODE o COLLECTED z Preservatives m t Gimking Wattr DVf Water WS Wail'Watc' WN � S U U P'n -i P a2°Ia SAMPLE ID o a� „ u START END v m h One Character per box. W'P� WP w w a z b e a C # - ar AR (A-Z, 0-9 f,} O[n'' OT Sample Ids must be unique d 'J F 7DATETIME 1 r ¢ z Z © i' m O ro ?. i15 G rn o. o- Wa Ti:sit 75 x w a J a w H m O =D `n d t m l— w4 O C N Z U r r Q - rn fn O O O S v3 = DATE TIME m = = = z f- 0 4 rz t ,�: Ih -� 7fff j X f' y .2 d /! i t �! i �7 f J'M i :.111 ��'i T �/ 1� 15 4— 5 7' 8: 9. a"2 'ADDITIONAL COMMENTS-�� '�-.Mw -. _ ;RELINCI115}IF�BY�APF1LfA7iON `GATE '.:: ,'.TIME. -'-'ACCEATEO BYrAFEItJAFION wOA7E ,.� j;�•;.T1ME fa ';"{" sSAMPLECONOIYEONS- SAMPLER NAME AND SIGNATURE - _ _ -- �. _ _ _ -� F-.T- t' '''' +�•>.-'.. C P I�7 Name of SAMPLE— [fl v p r u _ y� U y. vi 'c 5 N Tt1RE SAMPiE DATE Signed: r1 i '� Tyr l I ! �I �1 I—L' - - V t,v i N13 RQ ' � e x m a f � yy ��li• Q� Tly C A IF o MECKLENBURG COUNTY Land Use & Environmental Services Agency Solid Waste January 2, 2018 Central Files NCDENR / DWQ 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention: Central Files Subject: Discharge Monitoring Report Compost Central — Certificate of Coverage No. NCG240016 Dear Central Files: Please find enclosed the Discharge Monitoring Report, December 2017, for Compost Central, a "Type I facility located at 5631 West Blvd in Charlotte, North Carolina. If you have any questions, please contact me al 704-634-7705 or by email at klialiem.adams a, mecklenburgcountync.y Sincerely, Klialietn Adams Solid Waste Environmental Specialist Enclosed: 2017 DMR -/qN ORy�grloiv%. N sslN 411vlT PEOPLE • PRIDE PROGRESS • PARTNERSHIP 2145 Suttle Avenue Charlotte, North Carolina 282028 www.wipeoutwaste.com Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 01/02/2018 CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME Compost Central COUNTY Mecklenburg County PERSON COLLECTING SAMPLES Khaliem Adams LABORATORY: Pace Analytical Services Lab Cert. # 192 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec or ® Monthly' December (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ❑Other Total event rainfall 10.4 in or ❑ No discharge this period' Date Sample Collected' [mo/dd/yr] Outfall No. TSS COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks 100 mg/0 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 12/20/2017 1 193 169 2000 4.2 1.2 0.015 0.0076 0.041 7.0 12/20/2017 2 970 38.0 1100 1.2 0.27 0.0082 <0.075 0.012 6.9 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. `The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 rarT ts: venlcle Ivialnienance Area IvionlToring KesuiTs: only Tor TaciiiTIes averaging gal oT new mOT Date Sample Collected' (mo/dd/yr) Outfall No. pH TPH using method 1664A SGT-HEM TS5 Total Rainfall' Check if No Flow This Period' Average New Motor Oil Usage 6-9 15 mg/L 100 mg/L' - - 12/20/2017 1 7.0 <5.0 193 0.42 12/20/2017 2 6.9 <5.0 970 0.42 75 gal/month Footnotes from Part A also aoolv to this Part B :)r oil/month. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an oriainal and one coov of this DMR. including all "No Discharae" reports. within 30 days of receipt of the lab results (or at end of monitorina period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Sign a//,? - (Date) it Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 2 of 2 EnWronmentai Quarry Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on jilting out this form, please visit httpsT//deq.ne.gov/about/divisions/eneray-mineral-land- resources/energy-m i neral-land-perm its/stormwater-perm its/npdes- industrial-sw#tab-4 Permit No.: NICI �l ql 0l o / l 16l / or Certificate of Coverage No.: NIC/G/_I_I_I_/ 1_/ Facility Name: County: Inspector: a GI' tOA Y) � n Date of Inspection: Time of Inspection: Total Event Precipitation (inches): Phone No. l Id All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DF.MLR Regional Office. .. ....... ......... ......... ..._..._. ......... ......... ......_.. .......... ............ ...... ........ ...................................... ...... .... By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: T Outfall No. I Structure (pipe, ditch, etc.): ! &Iverf Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: Page I of 2 SWU-242, Last modified 4712812Ot7 2. Color: Describe the color of t�l]e discharge using basic colors ( ed, brown, blue, etc.) and ti (light, pledium, dark) as descriptors: Ynl� i 0,�1 e.&eQ� :� � UV n 0A,, 3. Odor: Describe any distinct odors that the chlorine odor, etc.): JO Odars be e may have (i.e., smells strongly of oil, weak 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 1 2 3 V 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 7. 8. 9. 1 2 3 4 Is there any foam in the stormwater discharge? O Yes Is there an oil sheen in the stormwater discharge? OYes 0 QIN0. kQ VNo. / V O Is there evidence of erosion or deposition at the outfall? O Yes Q(No. to. Other Obvious Indicators of StormJwj ater Pollution: Dist and describe A)p n ��1/t e"'F i�VIG(I C0 b (-s Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 5WU-242, Last moditied 07/28/2017 MIN Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance onfilling out thisform, please visit littl2s:Hdeq.nc.gov/abotti/divisions/energy-mineral-land- resources/energy-mi nera I-land-permitslstormwater-permits/nodes-ind ustrial-swgtab-4 Permit No.: NICI-; Ill�l�l�l_I or Certificate of Coverage No.: NICIGI l�hl I hl Facility Name: County: _ Inspector: Date of Inspection: Time of Inspection: Total Event Precipitation (inches): b. `1 p Phone No. All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall )ascription: OutfalI No. Receiving Stream: Structure (pipe, ditch, etc.): rtoi ribel tl�e ilndustra;Iactivitie-that occur within the outfall drainage area: Page 1 of 2 sWU-242, last modified 07128f2017 2. Color: Describe the color of the discharge ustejW g basic colors (red, brown, blue, etc.) an tintt (light, medium, dark) as descriptors: V9 Cy Mq eLIJ I q h' � t: 4rOtWn 3. Odor: Describe any distin t odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): � 0 01) f '5 4. Clarity: Choose the number which best describes the clarity of the discharge, where l is clear and 5 is very cloudy: 1 2 3 4 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where l is no solids and 5 is the surface covered with floating; sol ids: 1 2 D 4 5 6. Suspended Solids. Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 lr/ 7. Is there any foam in the stormwater discharge? O Yes IVNo. Q S. Is there an oil sheen in the stormwater discharge? OYes (140. I)O 9. is there evidence of erosion or deposition at the outfall? O Yes -+ta No. �jy 10. Other Obvious Indicators of Stormwater Pollution: List and describe I Vr7 ()' '0"r Arlo ca r� Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 5 WU-242, Last modified 07/28/2017 a1ceAnaly4lcal www.pacelabs.com January 02, 2018 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: Compost Central 1 Pace Project No.: 92367654 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on December 20, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 19 lacate-rAinalytical" wwwpacelabs.cam Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: Compost Central 1 Pace Project No.: 92367654 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #7 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 19 aceAnalX cal wwwpacelabb com SAMPLE ANALYTE COUNT Paco Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Compost Central 1 92367654 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92367654001 Outfall 001 EPA 1664B JMS 1 PASI-C EPA 200.7 DS 3 PASI-A SM 9222D KDF 1 PASI-C SM 2540D BRJ 1 PASI-A EPA 9040 KMM 1 PASi-A TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 BRJ 1 PASI-A EPA353.2 CJH 1 PASI-A EPA 365.1 MDW 1 PASI-A SM 5220D NAL 1 PASI-A 92367654002 Outfall 002 EPA 1664B JMS 1 PASI-C EPA 200.7 IDS 3 PASI-A SM 9222D KDF 1 PASI-C SM 2540D BRJ 1 PASI-A EPA 9040 KMM 1 PASI-A TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA351,2 BRJ 1 PASI-A EPA 353.2 CJH 1 PASI-A EPA 365.1 MDW 1 PASI-A SM 5220D NAL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L1.0, Page 3 of 19 m acarinalytrcal ..paceiaes.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Compost Central 1 Pace Project No.: 92367654 Sample: Outfall 001 Lap ID: 92367654001 Collected: 12/20/17 10:D4 Received: 12/20/17 11:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT•HEM, TPH Analytical Method: EPA 16648 Total Petroleum Hydrocarbons ND mg/L 5.0 1 12/26/17 04:44 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 0.015 mg1L 0.0050 1 12/23/17 03:15 12/26/17 18:15 7440-50-8 Lead 0.0076 mg/L 0.0050 1 12/23/17 03:15 12/26/17 18:15 7439-92-1 Zinc 0.041 mg/L 0.010 1 12/23/17 03:15 12/26/17 18:15 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D Fecal Coliforms 2000 CFU1100 mL 1.0 1 12/20/17 14:19 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 193 mg/L 41.7 1 12/23/17 00:05 9040 pH Analytical Method: EPA 9040 PH 7.0 Sid. Units 0.10 1 12/21/17 05:22 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 4.2 mg/L 0.52 1 12/28/17 17A0 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA351.2 Nitrogen, Kjeldahl, Total 3.4 mg1L 0.50 1 12/26/17 03:21 7727-37-9 353.2 Nitrogen, N021NO3 pres. Analytical Method: EPA 353.2 Nitrogen, NO2 plus NO3 0.80 mg/L 0.020 1 12/27/17 05A8 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 1.2 mg/L 0.050 1 12/22/17 00:26 7723-14-0 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 169 mg1L 25.0 1 12/26/17 20:02 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/02/2018 10:10 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 19 Pace Analytical Services, LLC aceAnalytical 9840 Kincey Ave. Suite 100 Huntersville, NC 28078 w wwpacelabs.conr (704)875-9092 ANALYTICAL RESULTS Project: Compost Central 1 Pace Project No.: 92367654 Sample: Outfall 002 Lab ID: 92367654002 Collected: 12/20/17 10:04 Received: 12/20117 11:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mglL 5.0 1 12/26/17 04:44 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 0.0082 mg1L 0.0050 1 12/23/17 0115 12/26/17 18:18 7440-50-8 Lead ND mg/L 0.0050 1 12/23/17 03:15 12/26/17 18:18 7439-92-1 Zinc 0,012 mg1L 0.010 1 12/23/17 03:15 12/26/17 18718 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D Fecal Coliforms 1100 CFU1100 mL 1.0 1 12/20/17 14:19 ul 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 970 mg/L 250 1 12/23/17 00:05 9040 pH Analytical Method: EPA 9040 pH 6.9 Sid. Units 0.10 1 12/21/17 05:22 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 1.2 mg/L 0.52 1 12/28/17 17:40 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 1.1 mg/L 0,50 1 12/28/17 03:22 7727-37-9 353.2 Nitrogen, N021NO3 pres. Analytical Method: EPA 353.2 Nitrogen, NO2 plus NO3 0.098 mg/L 0.020 1 12/27/17 05:49 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 0.27 mg/L 0.050 1 12/22/17 00:26 7723-14-0 5220D COD Analytical Method: SM 52200 Chemical Oxygen Demand 38.0 mg/L 25.0 1 12/26/17 20:02 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/02/2018 10:10 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 19 accAnalXical wwwpacelabs.com QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92367654 QC Batch: 392245 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92367654001, 92367654002 METHOD BLANK: 2176170 Matrix: Water Associated Lab Samples: 92367654001, 92367654002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 12/26/17 04:28 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL. SAMPLE; 2176171 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 19.7 98 64-132 MATRIX SPIKE SAMPLE; 2176172 35364308001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg]L ND 20 19.7 98 64-132 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right el the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0110212018 10:10 AM without the written consent of Pace Analytical Services, LLC, Page 6 of 19 ace.Analytifcal ttavw.pacelabs.com QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92367654 QC Batch: 392191 Analysis Method: EPA 200.7 QC Batch Method: EPA 2007 Analysis Description: 2007 MET Associated Lab Samples: 92367654001, 92367654002 METHOD BLANK: 2176018 Matrix: Water Associated Lab Samples: 92367654001, 92367654002 Blank Reporting Parameter Units Result Limit Analyzed Copper mg/L ND 0.0050 12128/1714:23 Lead mg/L ND 0.0050 12126/1717:06 Zinc mg/L ND 0.010 1212611717:06 Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2176019 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg/L .5 0.46 92 85-115 Lead mg/L .5 0.43 85 85-115 Zinc mg/L .5 0.48 95 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2176020 MS 92367514001 Spike Parameter Units Result Conc. Copper mg/L 0.013 .5 Lead mg/L ND .5 Zinc mg/L 0.073 .5 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2176022 MS 92367617009 Spike Parameter Units Result Conc. Copper mg1L ND .5 Lead mg1L ND ,5 Zinc mg1L ND .5 2176021 MSD Spike MS MSD M5 MSD % Rec Conc. Result Result % Rec % Rec Limits RPD .5 0.49 0.49 96 95 70-130 1 .5 0.44 0.44 89 88 70-130 1 .5 0.51 0.51 88 88 70-130 0 2176023 MSD Spike MS MSD - MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD .5 0.47 0.49 93 97 70-130 4 .5 0.44 0.46 88 92 70-130 5 .5 0.43 0.45 87 91 70-130 5 Results presented on this page are In the units Indicated by the"Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/02/2018 10:10 AM without the written consent of Pace Analytical Services, LLC. Quaff Qual Page 7 of 19 laoAnalytical* mmpacelabs.cotn QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92367654 QC Batch: 391980 Analysis Method: SM 9222D QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - CHT Associated Lab Samples: 92367654001, 92367654002 METHOD BLANK: 2174588 Matrix: Water Associated Lab Samples: 92367654001, 92367654002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU1100 mL ND 1.0 12/20/17 14:19 SAMPLE DUPLICATE: 2174589 92367622001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU1100 mL 395 21 D 61 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huniersville, NC 28078 (704)875-9092 Results presented on this page are In the units Indicated by the" Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /0212018 10:10 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 19 laneAnalyficalo www.paCmliibs.com QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92367654 Pace Analytical Services, LLC 9800 KinceyAve, Suito 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 392184 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92367654001, 92367654002 METHOD BLANK: 2175990 Matrix: Water Associated Lab Samples: 92367654001, 92367654002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 12/22/17 23:57 LABORATORY CONTROL SAMPLE: 2175991 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 228 91 90-110 SAMPLE DUPLICATE: 2175992 92367873010 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 17.2 17.8 3 SAMPLE DUPLICATE; 2175993 92368024004 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 10.6 11.8 11 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/02/2018 10:10 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 19 (�IaceAnalytical� www.pacelabs.com QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92367654 QC Batch: 391896 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92367654001, 92367654002 SAMPLE DUPLICATE: 2174248 Parameter pH SAMPLE DUPLICATE: 2174249 Parameter pH 92367800002 Dup Units Result Result RPD Qualifiers Sid, Units 7,0 7.0 0 H6 92367673002 Dup Units Result Result RPD Qualifiers Std. Units 6.8 6.8 0 H6 Pace Analytical Services, LLC 9800 Kincey Ave. Suite too Huntersville, NC 2807E (704)875-9092 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This reperl shall not be reproduced, except in full, Date: 01/0212018 10:10 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 19 accAnalytical www.pacefabs.cw QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92367654 QC Batch: 392386 Analysis Method: EPA 351.2 QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN Associated Lab Samples: 92367654001, 92367654002 METHOD BLANK: 2176728 Matrix: Water Associated Lab Samples: 92367654001, 92367654002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 12/28/17 03:15 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2176729 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.4 94 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2176730 2176731 MS MSD 92367533001 Spike Spike MS MSD MS MSD % Rec Parameter Units , Result Conc. Conc. Result Result %n Rec % Rec Limits RPD Quat Nitrogen, Kjeldahl, Total mg1L 7.3 10 10 17.6 16.6 103 93 90-110 6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2176732 2176733 MS MSD 92367528002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg1L ND 10 10 9.3 9.0 93 90 9D-110 4 Results presented on this page are In the units indicated by the"Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 01 /02/2018 10: 10 AM without the written consent of Pace AnalyticaS Services, LLC. Page 11 of 19 acMnalytical www.pacelabs.corrr QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92367654 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 392408 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92367654001, 92367654002 METHOD BLANK: 2176802 Matrix: Water Associated Lab Samples: 92367664001, 92367654002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.020 12/27/17 05:22 LABORATORY CONTROL SAMPLE: 2176803 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.4 96 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2176804 2176805 MS MSD 92367614007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.060 2.5 2.5 2.4 2A 92 93 75-125 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2176806 2176807 MS MSD 92367617008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L ND 2.5 2.5 2.4 2.4 94 94 75-125 0 Results presented on this page are In the units Indicated by the "Units" column except where an attemate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/02/2018 10:10 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 19 ace, Analytical www.pacelabs.mm QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92367654 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 392053 Analysis Method: EPA 365.1 QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92367654001, 92367654002 METHOD BLANK: 2175319 Matrix: Water Associated Lab Samples: 92367654001, 92367654002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 12122117 00:22 LABORATORY CONTROL SAMPLE: 2175320 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Phosphorus mglL 2.5 2.6 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2175321 2175322 MS MSD 92367533001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L O.B2 2.5 2.5 3.2 3.2 96 94 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2175323 2175324 MS MSD 92367574001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 1.2 2.5 2.5 3.6 3.6 99 98 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0110212018 10:10 AM without the written consent of Pace Analytical Services, LLC, Page 13 of 19 aceAnalytrcal www.pacelabs.ciom QUALITY CONTROL DATA Project: Compost Central 1 Pace Project No.: 92367654 QC Batch: 392354 Analysis Method: SM 5220D QC Batch Method: SM 5220❑ Analysis Description: 52200 COD Associated Lab Samples: 92367654001, 92367654002 METHOD BLANK: 2176605 Matrix: Water Associated Lab Samples: 92367654001, 92367654002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 12126117 20:02 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2176606 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 762 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2176607 2176608 MS MSD 92367464001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qua[ Chemical Oxygen Demand mg/L 67.0 100 100 176 176 109 109 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2176609 2176610 MS MSD 92367533002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 21800 100 100 21600 21700 -175 -50 90-110 1 M6 Results presented on this page are in the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/02/2018 10:10 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 19 1aceAnalytrcal www.pacelabs.com QUALIFIERS Project: Compost Central 1 Pace Project No.: 92367654 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL- Reporting Limit. Pace Analytical SaMces, LLC 9800 KiriceyAve. Su lie 100 Huntersville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. 110IMrira21taWIGIS tIlIn LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA required holding time. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. u1 Results based upon colony counts outside acceptable range. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/02/2018 10:10 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 19 aCeAnalytical wxw.pacalabs.cam QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Compost Central 1 92367654 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92367654001 Outfall 001 EPA 1664E 392245 92367654002 Outfall 002 EPA 1664B 392245 92367654001 Outfall 001 EPA 200.7 392191 EPA 200.7 392214 92367654002 Outfall 002 EPA 200.7 392191 EPA 200.7 392214 92367654001 Outfall 001 SM 9222D 391980 92367654002 Outfall 002 SM 9222D 391980 92367654001 Outfall 001 SM 2540D 392184 92367654002 Outfall 002 SM 2540D 392184 92367654001 Outfall 001 EPA 9040 391896 92367654002 Outfall 002 EPA9040 391896 92367654001 Outfall 001 TKN+NO3+NO2 392730 Calculation 92367654002 Outfall 002 TKN+NO3+NO2 392730 Calculation 92367654001 Outfall 001 EPA 351.2 392386 92367654002 Outfall 002 EPA 351.2 392386 92367664001 Outfall 001 EPA 353.2 392408 92367654002 Outfall 002 EPA 353.2 392408 92367654001 Outfall 001 EPA 365.1 392053 92367654002 Outfall 002 EPA 365.1 392053 92367654001 Outfall 001 SM 5220D 392354 92367654002 Outfall 002 SM 52201) 392354 Date: 01/02/2018 10:10 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 16 of 19 Document Name: Document Revised: August 4, 2017 e7CC�ifk?lybCdt Sample Condition Upon Receipt(SCURj Page 1 of 2 Document No.: Issuing Authority: ! F-CAR-CS-033-Rev.04 Pace QuaJity Office Laboratory receiving samples: Asheville ❑ Eden[:] Greenwood ❑ Huntersville] Raleigh[] Mechanicsville❑ Client Name:W OU92367654 NOMOMM,Project It: Courier: ❑Fed Ex ❑UPS ❑USPS Client ❑ Commercial ❑Pace ❑Other: 92367654 Custody Seal Present? []Yes dNo Seals Intact? []Yes ONo Date/Initials Person Examining Contents: Packing Material: ❑Bubble Wrap ❑Bubble Bags None ❑ Other Blalogical Tissue Frozen? - Thermometer: r f7 ,J ©wec ❑aloe �ne ❑Yes [:]No[]N/An IR Gun ID: I 1 Type of Ice:_ Correction Factor: Cooler Temp Corrected ('C): S ; 3 Temp should be above freezing to VC []Samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Soil ( &N/A, water sample) Did samples on_Rr�Ipele in a quarantine zone within the United States: CA, NY, or 5C {check mapsl7 Did samples originate from a foreign source (Ini r ationally, nYes I I1No includineHawaii and Puerto Rimt? FlYes IWrNo Comments/Discrepancy: Chain of Custody Present? Yes El No N/A 1. Samples Arrived within Hold Time? es No NIA 2. Short Hold Time Analysis (02 hr.? ❑Yes []No ❑N/A 3. Rush Turn Around Time Requested? Dyes No N/A 4. Sufficient Volume? M4es ❑No QN/A S. Correct Containers Used? -Pace Containers Used? '/❑Yes fes [:]No []NO ❑N/A NIA 6. Containers Intact? ClYrs JDNO N/A 7. Dissolved analysis: Samples Field Filtered? Qyes No N/A S. Sample Labels Match COC? -Includes Date/Time/10/Analysis MatrlK: b4s []NO ❑NIA 9. Heads ace in VOA Vials (>5.6mm)? ❑Yes F1,Np NIA 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes 0Yes ffNo ❑No ❑N/A CbKJA 11. CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Lot IO of split containers: Project Manager SCURF Review. Project Manager SRF Review: Field Data Required? ❑Yes ❑No Date/Time: Date: Z. ZG 112 yy Date: Zz I Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le. Out of hold, incorrect preservative, out of temp, incorrect contalnersi Page 17 of 19 m m 3 m O b n a ro t w m s O m Z = n tZ v m LA n b � ie tb m rt c r � o m a c q � a � T � C 3 � CLb _ LA d n 1b a IM ro A 3 0 c P. 9 rs � a �e w r`s a p ♦ R ltemN m m e ? mL Plastic Unpreserved (N/A) (Cl-) D 3 .�. Q zzzzzzzzzzzz9P41.1-125 . 8P3LI-250 mL Plastic Unpreserved (N/A) — a to SPZU-SOO mL Plastic Unpreserved (N/A) r. Q o 0 g 13 \ OPtU-1 liter Plastic Unpreserved (N/AJ Cr a S S y F~ C BP4S-125 mL Plastic H2504 (PH < 2) (Cl-) �,; 0 ]a D rL BP3N-250 m1 plastic HNO3 (pH < Z) — n x n X SP4Z-125 mL Plastic ZN Acetate & NaUH (>9) D �, zzzz BP4C-125 mL Plastic NaOH (pH > 12) (CI-) p n °1 m C a WGFU-Wide-mouthed Glass jar Unpreserved D� O Cr go CL AG1U-1 liter Amber Unpreserved (N/A) jCI-) - CO — n m O S � N zzz AG1H-1 liter Amber HCl (pH < 2) N O ro � r O AG31.1-250 mL Amber Unpreserved (N/A) (CI-) 1w D Q a AG15-1 liter Amber H2Sg4 (pH < a„_� AG35-250 mL Amber HZSO4 (pH < 2) z 2 w AG3A(DG3A)-250mLAmberNH4CIIN/A)(CI-) c m is n D69H-40 ml VOA IIC1 (N/A) � N O n ZZUZIZZ -Z VG9T-40 mL VOA Na25203 (N/A) n A VG911-40 m€ VOA Unp (N/A) DG9P-40 mL VOA H3PO4IN/A) K m O o VDAK (6 vials per kit)-5035 kit (N/A) c V/GK 13 vials per kit)-VPH/Gas kit (N/A) ■■L/n a C SP5T-125 mL Sterile Plastic (N/A — lab) 3 A w w G n Na SPZT-250 mL Sterile Plastic (N/A — lab) 7C W 0 y n r o '., an CD X O t0 n 1 Ix _ G v BP3A-250 mt Plastic (NH2)2504 (9.3.9-7) r� o V Cubitainer VSGU-20 mL Scintillation vials (N/A)- 1J 00 GN ! FaceAr>alytrraj' Section A Required Client Information: Section e Required Project Information: CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section C Invoice Information: Pacre 1 (]f f Company. Mecklenburg County Solid Waste Report Td: Darren Steinhitber Attention, - Address: 2145 Sultln Ave Copy To: Company Name: Charlotte, NC282D8 Address "sr- RegulatolZ A enc • -3`r•- `'+': '1 Er141i1: darten,steinhilber meckI2-' rync qov Purchase Order #. Pace Quote: Phone: 1704j336-4447 Fa>< Projoct Name: Compost Central 1 Paw Projecl Manager. matilhewbrainard5ppecelabs,com, -- ' 1-+`" °'-State Locatlon- Requested Due Date: Project A: Pace Profile A: 3207-1 NC :R u"ted IYZI1 Flltoiad !N �' ` ..' • fy.� ,F1� m Mx Coca COLLECTED Z Preservatives- `' lk,"g wwK OW - 8 x! O ~ W.W WT w„.W.. My P.4= P SAMPLE IC ar " pL `o u START END O' .� F 2 O i = One Character per box. w wP y a .. w d i n ' a. '^ € z • S a r, c g w are lA-z 0-91, -1 orm>re oT ti i n ' S. a �• ' Sample ids must be unique T„� Ts x TAIEII.E T11A1E1.ET O a c ite G r Z U , c W I.- F ¢ a a V m a O O _ i t L a 0 m r- d n ` 2,367�Sy N h s x s z 6 r mo O tr Y-7i Oxrttatl 001 WT [ �01 I- 's. m V! F f L'r' t Q X X X X X X X z` ' i C lv f�fv� C-+-1z OutmailDGx VVT X X X X X X X 3" r� —4r s? y.9 ; `+AbDITIGNAL C01✓HIF.NTS�^---}`-.K -RELINQUt5HF1S BYtAFF[tJA710N •; i �'OATE'.3 tii1ME p AGCEPTEOS !�[uATIONT.SAMP[�CONaRIONS 1 - f� r.l AVY G 3 N i U - :.AMPLER NAk1E AND SIGNAT'LIAE • r ',•.G + ? ' - ` ' -t -_� ti o t�7 PRINT Name of SAMPLER: V•i; ,']t-r.�:� /t �`� S i ! fT /T a x W 1-H.—ILd SrGNATURE of SAMPLER:! ' '�{7 // DATE Signed: 1 "+ � rt • 1 I �LagV�� �o � x fir"' a nROV " MECKLENBURG COUNTY Land Use & Environmental Services Agency Solid Waste November 9, 2017 Central Files NCDI--NR 1 DWQ 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention: Central Files Subject: Discharge Monitoring Report Compost Central — Certificate of Coverage No. NCG240016 Dear Central Files: Please find enclosed the Discharge Monitoring Report, October 2017, for Compost Central, a Type I facility located at 5631 West Blvd in Charlotte, North Carolina. If you have any questions, please contact me at 704-634-7705 or by email at khalieni.adams a, mecklenburgcountyrtc.gov Sincerely, Khal iem Adatns Solid Waste Environmental Specialist Enclosed: 2017 DMR PEOPLE • PRIDE PROGRESS • PARTNERSHIP 2145 Snttic Avenue Charlotte, North Carolina 282028 xvww. wipeoutwaste.com Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 11/9/17 CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME Compost Central COUNTY Mecklenburg County PERSON COLLECTING SAMPLES Khaliem Adams LABORATORY: Pace Analytical Services Lab Cert. # 192 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec or ® Monthly' October (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow []Water Supply ❑SA ❑Other Total event rainfall ? 0.4 in or ❑ No discharge this period' Date Sample Colle Collected' (mo/ cted Outfall No. TSS COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks =__> 100 mg/L' 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 10/23/2017 1 - - - - - - - - - 10/23/2017 2 20.2 183 4000 4.0 1.2 0.016 <0.0050 0.035 6.2 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Date Sample Collected; (mo/dd/yr) Outfall No. pH TPH using method 1664A SGT-NEM TSS Total Rainfall' Check if No Flow This Period' Average New Motor oil Usage 6-9 15 mg/L 100 mg/L4 - - 10/23/2017 1 - - - - X 10/23/2017 2 6.2 <5.0 20.2 0.40 75 gal/month Footnotes from Part A also apply to this Part B FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an original and one copy o this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results or at end of monitoring eriod in the case of "No DischaLge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature ii (Date) Permit D e: 10/1/2011-9/30/2016 Last Revised 12/02/11 ' Page 2 of 2 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-lan(I- resources /energy-mineral-land-permits /stormwater-permits /nncies-inindustrial-sw#tab-4 Permit No.: N/C/�/ /_/�/_/�/_/ or Certificate of Coverage No.: Facility Name: Compost Central County: Mecklenburg Phone No. (704) 588-9092 Inspector: Darren Steinhilber- Date of Inspection: a3 Time of Inspection: q Total Event Precipitation (inches): " q i" � t & All permits require qualitative monitoring to he performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: p Outfall No. Structure (pipe, ditch, etc.): i �e 1 C ��ipt Receiving Stream: Describe t)e indu�Yial activities that occur within the outfall drainage area: Omfow", I Pagel of 2 SWU-242, Last modified 07/28/2017 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) liand tint (light, medium, dark) as descriptors: D I�, -Wei b r ak -e-, .fib , l fahkL li/ I�0 , 3. Odor: Describe any distinct odors that the di weak chlorine odor, etc.): NJ odor k kLk, rge may have (i.e., smells strongly of oil, 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is nosolidsand 5 is extremely muddy: 1 2 [ 31 4 5 7. Is there any foam in the stormwater discharg*.<es Q No. Lo W am 8. Is there an oil sheen in the stormwater discharp? to Yes No. 9. Is there evidence of erosion or deposition at the outfaC o Yes N o. 10. Other Obvious Indicators of Stormwater Pollution: Listanddescribe -�Wes( 0 o wfiubrS Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 5WU-242, Last modified 07/28/2017 aceAnalytical www.pa:elabs.com October 31, 2017 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92360203 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on October 23, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures pCCRp REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 acmnalylical www.pacelabs.com CERTIFICATIONS Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92360203 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater CertifiCatiOn #: 12 Asheville Certification iDs 2225 Riverside Drive, Asheville, NC 28804 F lorid a/N E LAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #; 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginialVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 Iacmnalytical" www.p"labs.com SAMPLE ANALYTE COUNT Project: COMPOST CENTRAL. 1-WEST BLVD Pace Project No.: 92360203 Pace Analytical Services, LLC 9804 Kincey Ave. Suite100 HuniersvlUe, NC 28078078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92360203001 OUTFALL 002 EPA 1664B JMS 1 PASI-C EPA200.7 SH1 3 PASI-A SM 9222D KDF 1 PASI-C SM 2540D SLB 1 PASI-A EPA 9040 KMM 1 PASI-A TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 BRJ 1 PASI-A EPA 353.2 CJH 1 1 PASI-A EPA 365.1 MDW 1 PASI-A SM 5220D NAL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 3 of 18 Pace Analytical Services, LLC IaceAnalytical ® 9600 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs oom (704)875-9092 ANALYTICAL RESULTS Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92360203 Sample: OUTFALL 002 Lab ID: 92360203001 Collected: 10123/17 12:09 Received: 10/23/17 12:09 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT HEM, TPH Analytical Method: EPA 16648 Total Petroleum Hydrocarbons ND mg/L 5.0 1 10/26/17 03:23 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 0.016 mg/L 0.0050 1 10/24/17 21:30 10/26/17 08:30 7440-50-8 Lead ND mg/L 0.0050 1 10124/17 21:30 10/26/17 08:30 7439-92-1 Zinc 0.035 mg/L 0.010 1 10124/17 21:30 10/26/17 08:30 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D Fecal Coliforms 4000 CFU1100 mL 1.0 1 10/23/17 16:20 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 20.2 mg/L 5.0 1 10/25/17 11:15 D6 9040 pH Analytical Method: EPA 9040 pH 6.2 Std. Units 0.10 1 10/23/17 23:51 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 4,0 mg/L 0.12 1 10/31/17 11:15 351.2 Total Kjeldahi Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 3.3 mg/L 0.50 1 10/30/17 23:46 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Nitrogen, NO2 plus NO3 0.66 mg1L 0.020 1 10/26/17 03:56 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 1.2 mg/L 0.050 1 10127/17 21:23 7723-14-0 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 183 mg1L 25.0 1 10/25117 19:16 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31 /2017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 18 aceAnalytical® MVw.pwe4ab=m QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 K ricey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92360203 QC Batch: 384025 Analysis Method: EPA 16646 QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92360203001 METHOD BLANK: 2128406 Matrix: Water Associated Lab Samples: 92360203001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 10/26/17 03:16 LABORATORY CONTROL SAMPLE: 2128407 Spike LCS. LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L 20 19.5 98 64-132 MATRIX SPIKE SAMPLE: 2128408 92359385001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L ND 20 19.2 96 64-132 Results presented on this page are In the units Indicated by the "Units" column except wtiere an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 10/3112017 04:31 PM withoutthe written consent of Pace Analytical Services, LLC. Page 5 of 18 aceAnalytrcal www.pawh7 bs.com Project: COMPOST CENTRAL. 1-WEST BLVD Pace Project No.: 92360203 QC Batch: 383772 QC Batch Method: EPA200.7 Associated Lab Samples: 92360203001 METHOD BLANK: 2127063 Associated Lab Samples: 92360203001 Parameter Copper Lead Zinc QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Units Result Limit Analyzed mg/L ND 0.0050 10/26/17 06:41 mg/L ND 0,0050 10/26/17 06:41 mg/L ND 0.010 10/26/17 06A1 Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2127064 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg1L .5 0.51 102 85-115 Lead mg/L .5 0.49 98 85-115 Zinc mg/L .5 0A9 98 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2127065 2127066 MS MSD 92358917007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L ND 5 .5 0.54 0.51 107 102 70-130 5 Lead mg/L 0.0057 .5 .5 0.47 0,45 93 89 70-130 5 Zinc mg/L 0.18 .5 .5 0.69 0.67 103 98 70-130 4 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2127067 2127068 MS MSD 92359784003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mglL 19.5 .5 .5 0.53 0.52 101 101 70-130 0 ug/L Lead mg/L 9.9 ug/L .5 .5 0.48 0.48 95 94 70-130 1 Zinc mglL 48.7 5 5 054 0 53 97 95 70-130 2 ug/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 10/31/2017 04:31 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 18 (�IaceAnalytical rwwwpacelabs.cam Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92360203 QC Batch: 383744 QC Batch Method: SM 9222D Associated Lab Samples: 92360203001 METHOD BLANK: 212676E Associated Lab Samples: 92360203001 Parameter Units Fecal Coliforms CFU1100 mL SAMPLE DUPLICATE: 2126769 Parameter Fecal Coliforms QUALITY CONTROL DATA Analysis Method: SM 9222D Analysis Description: 9222D MBIO Fecal Cdiform - CHT Matrix: Water Blank Result ND 92360203001 Units Result CFU1100 mL 4000 Reporting Limit Analyzed Qualifiers 1.0 10/23/17 16:20 Dup Result RPD Qualifiers 600 148 u2 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units Indicated by the" Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 aceAnalytrcal " W"..pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92360203 QC Batch: 383829 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92360203001 METHOD BLANK: 2127296 Matrix: Water Associated Lab Samples: 92360203001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 10/25/17 11:15 Paco Analytical Services, LLC 9800 Kincey Ave. Suite 100 HuntersviRe, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2127297 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 254 102 90-110 SAMPLE DUPLICATE: 2127298 92360203001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 20.2 23.6 16 D6 SAMPLE DUPLICATE: 2127299 92360223003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 90.5 74.0 20 D6 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/3112017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 18 aceAnafXical www.pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92360203 OC Batch: 383632 Analysis Method: EPA 9040 OC Batch Method: EPA9040 Analysis Description: 9040 pH Associated Lab Samples: 92360203001 SAMPLE DUPLICATE: 2126104 92360200001 Dup Parameter Units Result Result RPD Qualifiers pH Std. Units 5.8 5.8 0 H6 Pace Analytical Services, LLC 9B00 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2017 04:31 PM without the written consent of Pace Analytical Services, L.I.C. Page 9 of 18 (�IaceAnalytical www.pacelabs com QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92360203 QC Batch: 384085 Analysis Method: EPA 351.2 QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN Associated Lab Samples: 92360203001 METHOD BLANK: 2128625 Associated Lab Samples: 92360203001 Parameter Units Nitrogen, Kjeldahl, Total mg/L LABORATORY CONTROL SAMPLE: 2128626 Parameter Units Nitrogen, Kjeldahl, Total mglL Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hurtersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 10/30/17 23:40 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 10 9.5 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2128627 2128628 MS MSD 92360015001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg1L 41.0 10 10 204 223 1630 1820 90-110 9 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2428629 2128630 MS MSD 92359510003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 0.71 10 10 9.0 9.2 83 84 90-110 2 M1 Results presented on this page are In the units Indicated by the"units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 1 B aceAnalytrcal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92360203 QC Batch: 383886 QC Batch Method: EPA 353.2 Associated Lab Samples: 92360203001 METHOD BLANK: 2127546 Associated Lab Samples: 92360203001 Parameter Units Nitrogen, NO2 plus NO3 mg/L LABORATORY CONTROL SAMPLE: 2127548 Parameter Units Nitrogen, NO2 plus NO3 mg/L Analysis Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.020 10/26/17 03:43 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE; 2127549 2127550 MS MSD 92359886002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg11- 0.25 2.5 2.5 2,8 2,8 101 101 75-125 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2127551 2127552 MS MSD 92359566001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.29 2.5 2.5 2.7 2.6 95 94 75-125 0 Results presented on this page are In the units Indicated by the" Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/3112017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 aceAnalytical www.pacelabs.cont QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92360203 QC Batch: 384014 Analysis Method: EPA 365.1 QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92360203001 METHOD BLANK: 2128363 Associated Lab Samples: 92360203001 Parameter Units Phosphorus mg/L LABORATORY CONTROL SAMPLE: 2128364 Parameter Units Phosphorus mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)675-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 10/27/17 21:19 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.5 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2128365 2128366 MS MSD 92360015001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg1L 14.3 2.5 2.5 15.0 17.2 25 115 90-110 14 MB,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2128367 2128368 MS MSD 92360469001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0,37 2.5 2.5 3.0 3.0 107 106 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 aceAnalytical www.pacela6scom Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92360203 QC Batch: 383808 OC Batch Method: SM 5220D Associated Lab Samples: 92360203001 METHOD BLANK: 2127238 Associated Lab Samples: 92360203001 Parameter Units Chemical Oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 2127239 Parameter Units Chemical Oxygen Demand mg/L Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 10/25/1719:16 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 755 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2127240 2127241 MS MSD 92360015004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1 169 750 750 861 868 92 93 90.110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2127242 2127243 MS MSD 92359510005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 47.0 750 750 739 748 92 93 90-110 1 Results presented on this page are In the units indicated by the "Units' column except where an alternate unit is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 (�IaneAnalyfical mmpacelabs.c m QUALIFIERS Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92360203 DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SWB46 Chapter 4 for the analysis of Acrolein and Acryioritrile by EPA Method 8260. N-Nitrosod iphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration, Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NsELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA required holding time. M1 Matrix spike recovery exceeded OC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. R1 RPD value was outside control limits. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 (�IaneAnalytical' vnvw.paoelab&C= QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: COMPOST CENTRAL 1-WEST BLVD Pace Project No.: 92360203 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92360203001 OUTFALL 002 EPA 1664B 384025 92360203001 OUTFALL 002 EPA 200.7 383772 EPA 200.7 92360203001 OUTFALL 002 SM 9222D 383744 92360203001 OUTFALL 002 SM 2540D 383829 92360203001 OUTFALL 002 EPA 9040 383632 92360203001 OUTFALL 002 TKN+NO3+NO2 384653 Calculation 92360203001 OUTFALL 002 EPA 351.2 384085 92360203001 OUTFALL 002 EPA 353.2 383886 92360203001 OUTFALL 002 EPA 365.1 384014 92360203001 OUTFALL 002 SM 5220D 383808 Date: 10131/2017 04:31 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 383852 Page 16 of 18 r c?CBiRc?f1Cci!< Document Name: Sample Condition Upon Recei t(SCUR) Document Revised: August 4, 2017 Page 1 of 2 Document No.: F-CAR-CS-033-Rev.04 Issuing Authority: Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersvillf[l— RalelehF l MechaniccVinpF-1 MV-1111111 M.M. On Client Name: WO# : 92360203 + Project #: Courier: ❑Fed Ex ❑UF5 ❑U5p5 v Citerit I1 �1 111 HIM 11111111 ❑ Commercial q 7 s �'j t ❑Other. 92360203 Custody Seal Present? ]Yes - :;]No J Seals Intact? ❑Yes �(]No % j + Date/InItlaEs Person Examining Contents�l� Sl? • 7.7�+� Packing Material: ❑Bubble Wrap _QB6 ble Sags []None ❑ Other Biological Tissue Frozen? Thermometer: ❑Yes [—]No •{�N� �r _Wet []Blue ❑none �Q IR Gun ID: � Type ai ue: ' Correction Factor: Cooler Temp Corrected ('C): Temp should be above freezing to 6'C �QSatlrMs out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Soil {•Q NA water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples orlginate from a foreign source (internationally, F lYes FiNa— inrludine Hawaii and Puerto Rico)) nYes RN—O ' Comm ents/Discre ancy: Chain of Custody Present? Yes Na N/A t. Samples Arrived within Hold Time? Yes CJNo N/A 2. Short Hold Time Analysis (02 hr.)? . VF1 ONO ❑N/A 3. Rush Turn Around Time Requested? Yes _QHCr ONJA 4. Sufficient Volume? —2yes ❑No ❑N/A S. Correct Containers Used? -Pace Containers Used? �E]Y8 J;JYrs ❑N'o No ❑N/A N/A 6. Containers Intact? YCS No N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes — llro NIA g. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: es ❑No ❑N/A 9. Headspace in VOA Vials (>5-6mm)? ❑Yes ❑No , 9/_A �� 10, Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes Yes ❑No NO ❑N/A ❑/A it. + CLIENT NOTIFICATION/RESO77LUTION 11 Person Contacted: lac f;c•� ��r•��1< Comments/Sample Discrepancy: c,•I. v_ _ nl •, nil __ •.f Lot 10 of split containers: Project Manager SCURF Review: Field Data Required? ❑Ycs []NO Date/Time: ICjy i t:L -- Date: _ tE) Project Manager SRF Review: ��Date: /"� ! zq iq Note: whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 16 of 18 ro m CM SD 3 m d n v ry `ra z a m -a �a Q O C n r' in 3 w r Q b n -% 0 b � a eD w rD ti 3 (D a a M LA lu 1 K r a � rl N A a c n n v n c a Itemu UP4U-225 mL Plastic Unpreserved (N/A) (❑-) m N m a m �• � e x BP3U-2SO mL Plastic Unpreserved (N/A) C S o O1 m 7 7 jr BPZU-5D0 mL Plastic Unpreserved (N/A) CL + d O 6P1U-1 liter Plastic Unpreserved (N/A) Cr 'a 7 =r O - \ X � 3 BP45-125 mt Plastic H2504 (PH < 2) (CI-) �• O, SPAN-250 mL plastic HNO3 (pH < 2) .. rD Cr O n X rn n BP42-125 mL Plastic ZN Acetate & NaOH (�9) c fu BP4C-125 mL Plastic NaOH (pH > 12) [CI-) Cr WGFU-Wide-mouthed Glass jar Unpreserved Q AG1U-1 liter Amber Unpreserved (NIA) (CI-) Cr °0 a r➢ rMr 0 n zzzz C AG1H-lbterAmber HClIPH<2) CD S_ r^ 0 AG3U-250 rrLt Amber Unpreserved (N/A) ICI-) m O AG IS-1 liter Amber H2504 [pH < 2) AG35-250 ml Amber H2SO4 (pH < 21 AG3A(DG3A)-250 mL Amber NH4Cl (N/A)(CI-) DG9H-40 mL VOA HCI [N/A) 0 VG9T-40 mL VOA Na25203 (N/A) r- 3 VG9U-40 mt VOA Unp (N/AI DG9P-4O mL VOA I13PO4 (N/A) -4 g VOAK 16 vials per kit(-5035 kit (N/A) i (a 1 V/GK 13 vials per kit)-VPH/Gas kit (N/A) 3 rn w' f�VrP SP5T-125 mL Sterile Plastic (N/A - lab) t7 A C Cn 5P2T-250 mL Sterile Plastic (N/A - lab) O N � i Ozz A z z BPIA-250 mL Plastic (NH2)2504 (9-3-9.7) r•+ I �J e Cubitaincr I � VSGU-20 mE Scintillation vials (N/A) H -4 _ GN /cer�acaj. CHAIN -OF -CUSTODY 1 Analytical Request Document - — — The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fields must be completed accurately, Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Page : 1 Of 1 Company: Mecklenburg County Solid waste Report To: Darren Sleinhilber Attention, Address: 2145 Sultlo A,.e Copy To: Company Name: Charlotte. NC 282Da Address: _Re ulato A Email' darren.sleinhilber maddenbur count ync.9ov Purchase Order #: Pace Quote: Phone' 704 579-1537 Kam' Project Name: Compost Central 1 - Wert Blvd Pace Project Manager. maithew-brainardCcDpacelabs.com. - - - -' :state I Location--,rt �' Requested Due Date: Project #: Pace Profile N: 3207-1 NC Aa uocted'Anat ilaFlHcrod Y!N Fne- ' renmuc coot — o u COLLECTED Z Preservatives `••:' �` s 7 n VU. W T 3 O U W.M. Wulr VI" P+c°uC P � OJ y I2 SAMPLE ID °'° aL Ono Character per box. W'P. op `. START END a N 'r; o ' # {A-Z• d-91'_l other Di i= w = Q. Semple Ids must be unique T.Ts x F� 1^ a a N O O T = _ L t Q� n ti i3 g L7 O n < DATE TIME DATE TIME i z i V tl F n er Outlafi 001 WT x x x x x X ,2s {LI�> J —`•o j Ouafall002 vvi 11 i�7 3�%rl x x x x x x x 3 "4 -6 7' "s �8 �10t` 71. 12' -" AOOITIONAL'CO!°MENTa�� •,' RELINOUISHEO BYIAFFILIATION - GATE- •:.T1sSE 'ACGEPTEOBYIAFFILIATIOW -'4 'DATEw ?TIME�� � CONDITIONS l'k.f-.�<b a :k�y��� -t,.. l/�L�% L3AMPLe , ��l �.✓./Lr..�r.. r( ' i %.r� !(V 1-f �r��l�`/1t % 1C%�/'r,• /"ice!/V �.,.�.j r J .t , t �1 SAMP.LEA NAMEAN STGNATUftE i a . s? 1 r - i?�a�� r it M r .}. - : •{( D ." + 3r?� :y r PRINT Name of SAMPLER: ; 11r l L c u ,� r s 3 SIGNATURE of SAMPLER: l DATE Signed: l�•L L C7-v Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 10/30/17 CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME _Mecklenburg County Compost Central (new) _ COUNTY Mecklenbure Countv PERSON COLLECTING SAMPLES Darren Steinhilber LABORATORYPace Analylical Services Lab Cert. # 12 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE: QUARTER ❑ Jan -March ❑ April -June ® July -Sept ❑ Oct -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA RECEIVEL--❑Zero-flow ❑Water Supply ❑SA [)Other IJOV 0 3 2017 CENTRAL, FILES DWR SECTION Total event rainfall z 3.10 in or ❑ No discharge this period' Date Sample Collected' (mo/dd/yr) Outfall No. T5S COD Fecal coliform Total nitrogen Total phosphorus Total capper Total lead Total zinc PH Parameter benchmarks 100 mg/L4 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.007 mg/L 0.03 mg/L 0.067 mg/L 6-9 09/1/17 1 38.4 56 >6000 1.5 0.19 0.015 <0.005 0.026 7.5 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ' For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new mo _ _ e Check H r w i Nia Date Sample Outfall No 0. pH TPH using method r m Total -� Flow ,Collected' :: - 1664ASGT-HFM T55 -Rainfall' This, Average New Motor Oil Usage (mo/dd/yr) z s rPeri od3:, y 15mg/L,'e r 160.mg/L° 9/1/17 1 7.5 1 <5.0 38.4 1 0.73 1 1 75 Pal/month Footnotes from Part A also apply to this Part B for oil/month. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an original and one copy of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files �O 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. l am aware that there are significant penalties for submitting false information, including the possibility of fines and- imprisonment for knowing violations." •(SignatuXof I)Vfnitfee) (Dat ) Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 2 of 2 aceAna lyticaI wWWPacalsbacan September 11, 2017 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: Central Compost 2-Validydale Pace Project No.: 92353776 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Darren Steinhilber: Enclosed are the analytical results for sample(s) received by the laboratory on September 01, 2017, The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures - ,�p:PCCRFQ�A REPORT OF LABORATORY ANALYSIS ,r This report shall not be reproduced, except in full, E' without the written consent of Pace Analytical Services, LLC. _ qQ Page 1 of 18 leAnalXical wiwwPacelabs.CDM Project: Central Compost 2-Valleydale Pace Project No.: 92353776 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersvil le, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #; 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)875-9092 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712. CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #. E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 Pace Analytical Services, LLC aceAnalytical0 9800 Kincey Ave. Suite 100 Huntersvilfe, NC 2807878 wwwpacefabs cam (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Central Compost 2-Valleydale 92353776 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92353776001 Outfall 001 EPA 1664B JMS 1 PASI-C EPA 200.7 SER 3 PASI-A SM 9222D CLW 1 PASI-C SM 2540D SLB 1 PASI-A EPA 9040 MDW 1 PASI-A TKN+NO3+NO2 Calculation EWS 1 PASI-A r, EPA 351.2 BRJ 1 PASI-A EPA 353.2 DMN 1 PASI-A EPA 365.1 AES2 1 PASI-A SM 5220D NAL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 a aceAnalytical www.pacclabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)B75-9092 Project: Central Compost 2-Valleydale Pace Project No.: 92353776 Sample: Outfall 001 Lab ID: 92353776001 Collected: 09/01/17 10:45 Received: 09/01/17 11A0 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg/L 5.0 1 09/05/17 06:02 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 0.015 mg/L 0.0050 1 09/09/17 02:35 09/10/17 23:52 7440-50-8 Lead ND • mg/L 0.0050 1 09/09/17 02:35 09/10/17 23:52 7439-92-1 Zinc 0.026 mg/L 0.010 1 09/09/17 02:35 09/10/17 23:52 7440-66-6 MBIO 922213 Fecal Coliform CHT SM 9222D (Analytical -Method: Fecal Coliforms 6000 CFU/100 mL 1.0 1 09/01/17 16:46 u2 25400 Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 38.4 mglL 10.0 1 09/06/17 10A9 9040 pH Analytical Method: EPA 9040 pH 7.5 Sid. Units 0.10 1 09/02/17 05:03 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 1.5 mg1L 0.12 1 09/08/17 11:06 351.2 Total Kjoldahl Nitrogen Analytical Method: EPA351.2 Nitrogen, Kjeldahl, Total 1.5 mg1L 0.50 1 09/07/17 00:17 7727-37-9 353.2 Nitrogen, N021NO3 pres. Analytical Method: EPA 353.2 Nitrogen, NO2 plus NO3 0.022 mg/L 0.020 1 09/06/17 12:16 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 0.19 mg/L 0.050 1 09/06/1712:26 7723-14-0 5220D COD Analytical Method: SM 52200 Chemical Oxygen Demand $6.0 mg/L 25.0 1 09107/17 15:27 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/11/2017 06:40 PM without the written consent of Pace Analytical Services, LLC, Page 4 of 18 0 aceAna0ca! wtuwpacelabs.com QUALITY CONTROL DATA Project: Central Compost 2-Valleydale Pace Project No.: 92353776 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 376229 Analysis Method: EPA 1664B QC Batch Method: EPA 16648 Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92353776001 METHOD BLANK: 2084295 Matrix: Water Associated Lab Samples: 92353776001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5,0 09/05/17 05:46 LABORATORY CONTROL SAMPLE & LCSD: 2084296 2084297 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Total Petroleum Hydrocarbons mg/L 20 19.3 19.4 96 97 64-132 1 30 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/11/2017 06:40 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 s _ I eAnalXical tyww.pacala6a.r�tn QUALITY CONTROL DATA Project: Central Compost 2-Valleydale Pace Project No.: 92353776 QC Batch: 376801 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92353776001 METHOD BLANK: 2087566 Associated Lab Samples: 92353776001 Parameter Units mg/L mg/L mg/L Copper Lead Zinc Matrix: Water Blank Repotting Result Limit Analyzed Qualifiers ND 0.0050 09110/17 22:38 ND 0.0050 09/10/1722:35 ND 0.010 09/10/17 22:38 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2087567 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg1L .5 0.48 96 85-115 Lead mg1L .5 0.46 92 85-115 Zinc mg1L .5 0.47 93 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2087568 2087569 MS MSD 92353390002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L 5.8 ug1L .5 .5 0.49 0.48 96 95 70-130 1 Lead mg/L 8.1 ug1L .5 .5 0.46 0.46 90 91 70-130 1 Zinc mg/L 27.0 .5 .5 0.48 0.48 91 91 70-130 0 ug/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2087570 2087571 MS MSD 92353737004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg1L ND .5 .5 0.48 0.48 96 96 70-130 0 Lead mg1L ND .5 .5 0.45 0.45 89 89 70-130 0 Zinc mg1L ND .5 .5 0.46 0A6 91 92 70-130 1 Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except 0 full, Date: 09/11/2017 06A0 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 _ aceAnalytical mvw.pacelabs.com QUALITY CONTROL DATA Project: Central Compost 2-Valleydale Pace Project No.: 92353776 QC Batch: 376266 Analysis Method: SM 92220 QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - CHT Associated Lab Samples: 92353776001 METHOD BLANK: 2084421 Matrix: Water Associated Lab Samples: 92353776001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU1100 mL ND 1.0 09/01/17 16:46 SAMPLE DUPLICATE: 2084422 92353776001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU1100 mL 6000 600 164 u2 Pace Analytical Services, I-I-C 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/11/2017 06:40 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 aceAna,(Xical —paoelaas.com QUALITY CONTROL DATA Project: Central Compost 2-Valleyda)e Pace Project No.: 92353776 QC Batch: 375439 Analysis Method: SM 25400 OC Batch Method: SM 25400 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92353776001 METHOD BLANK: 2085382 Associated Lab Samples: 92353776001 Parameter Units Total Suspended Solids mg1L LABORATORY CONTROL SAMPLE: Parameter 2085383 Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 2085384 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2085385 Parameter Units Total Suspended Solids mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 2BO78 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 09/0611710:45 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 234 94 90-110 92353841001 Dup Result Result RPD Qualifiers 25.6 23.2 10 D6 92353717001 Dup Result ' Result RPD Qualifiers 12.3 11.0 11 D6 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0911112017 06:40 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 18 (�,IaceAnalytcal" www.pacelabacam Project: Central Compost 2-Valleydale Pace Project No.: 92353776 QC Batch: 376182 QC Batch Method: EPA 9040 Associated Lab Samples: 92353776001 SAMPLE DUPLICATE: 2084106 Parameter Units pH Std. Units QUALITY CONTROL DATA Analysis Method: EPA 9040 Analysis Description: 9040 pH 92353780001 Dup Result Result RPD Qualifiers 6.5 5.6 15 D6,1-16 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 2BO78 (704)875-9092 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09I11/2017 06:40 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 aceAnalytical" *Wpacelahs.tnm Project: Central Compost 2-Valleydale Pace Project No.: 92353776 QC Batch: 376402 CIC Batch Method: EPA 351.2 Associated Lab Samples: 92353776001 METHOD BLANK: 2085266 Associated Lab Samples: 92353776001 Parameter Units Nitrogen, Kjeldahl, Total mg/L LABORATORY CONTROL SAMPLE: 2085267 Parameter Units Nitrogen, Kjeldahl, Total mg1L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA351.2 Analysis Description: 351.2 TKN Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 09/07/17 00:06 ti Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 10 9.1 91 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2085268 2085269 MS MSD 92353566002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total rng/L 93.7 10 10 106 104 121 101 90-110 2 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2085270 2085271 MS MSD 92353998003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L ND 10 10 9.5 9.5 95 95 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/11/2017 06:40 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 _ IaceAnalytical wvwpacelabs cnm QUALITY CONTROL DATA Project: Central Compost 2-Valleydale Pace Project No.: 92353776 QC Batch: 376429 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92353776001 METHOD BLANK: 2085357 Associated Lab Samples: 92353776001 Parameter Units Nitrogen, NO2 plus NO3 mg/L LABORATORY CONTROL SAMPLE: 2085358 Parameter Units Nitrogen, NO2 plus NO3 mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite lo0 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.020 0910611711:50 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.5 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2085359 2085360 MS MSD 92353566002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 193 2.5 2.5 195 197 98 166 75-125 1 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2085361 2085362 MS MSD 92352972001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg]L 2.1 2.5 2.5 4.3 4.3 89 89 75-125 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/11/2017 06:40 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 (�1.eAnalXical" www.pacelabs.cam Project: Central Compost 2-Valleydale Pace Project No.: 92353776 QC Batch: 376406 QC Batch Method: EPA 365.1 Associated Lab Samples: 92353776001 METHOD BLANK: 2085286 Associated Lab Samples: 92353776D01 Parameter Phosphorus QUALITY CONTROL DATA Analysis Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers mg1L ND 0.050 09/0611712:22 Pace Analytical Services, LLC 980D Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2085287 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.6 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2085288 2085289 MS MSD 92353612002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg1L 0.28 2.5 2.5 2.8 2.8 99 101 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2085290 2085291 MS MSD 92353998001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg1L 0.42 2.5 2.5 3.0 3.0 104 103 90-110 1 Results presented on this page are In the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/11 /2017 06A0 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 aceAnalytical www.paceiabac= Project: Central Compost 2-Valleydale Pace Project No.: 9235377B QC Batch: 376574 QC Batch Method: SM 5220D Associated Lab Samples: 92353776001 METHOD BLANK: 2086326 Associated Lab Samples: 92353776001 Parameter Units Chemical Oxygen Demand mglL QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 0910711715:27 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2086327 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mglL 750 748 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2086328 2086329 MS MSD 92353479001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 37.0 750 750 836 876 107 112 90-110 5 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2086330 2086331 MS MSD 92353998002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L ND 750 750 793 751 105 99 90-110 5 R1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0911 V2017 06:40 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 Pace Analytical Services, LLC e100 ace p �f alXicaf 9800 Kincey Ave. Suite Huntersville, NC 28078078 ww pubs-mm (704)875-9092 QUALIFIERS Project: Central Compost 2-Valleydale Pace Project No.: 92353776 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit, S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenieno using Method 8270. The result for r each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA required holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. R1 RPD value was outside control limits. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09111/2017 06:40 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 laceAnalytical" wwwpacelabsrnrn QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Central Compost 2-Valleydale Pace Project No.: 92353776 Lab ID Sample ID 92353776001 Outfal 1001 92353776001 O utfa 11001 92353776001 O utfa 11001 92353776001 O u tfa 11001 923 53776001 Outfal 1001 92353776001 Outfal 1001 92353776001 Outfalt 001 92353776001 O utf a 11001 92353776001 O utfall 001 92353776001 Outfal 1001 Date: 09/1112017 06:40 PM Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersv4e, NC 28078 (704)875-9092 QC Batch Method QC Batch Analytical Method EPA1664B 376229 EPA 200.7 376801 EPA 2007 SM 9222D 376266 SM 2540D 376439 EPA 9040 376182 TKN+NO3+NO2 376894 Calculation _ EPA 351.2 376402 EPA 353.2 376429 EPA 365.1 376406 SM 5220D 376574 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 377014 Page 15 of 18 Document Name: Document Revised: August 4, 2017 r Analytical" Sam le Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: f F-CAR-CS-033-Rev.04 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden[-] Greenwood ❑ Huntersviile Raleigh❑ Mechanicsville[] Client Name: Project fi: WO# : 92353776 Sn Qc d;I�, I V( 1AA0 Courier: ? d Ex ❑UP5 SPS ErClient ❑ Commercial ❑Pace [—]Other. 92353776 Custody Seal Present? ❑Yes �31` O Seals intact? Elves do . Date/Initilis Person Examining Contents �E 1 I 1 n'7 Packing Material: ❑Bubble Wrap ❑Bubble Bags one ❑ Other ��'\ Blologlc�aI Tr ue Frozen? Thermometer: ❑Yes 1_Jryo []N/A ❑ IR Gun 10:% j�Wet []Blue Nane Type of Ice: Correction Factor: Cooler Temp Corrected ('C): 2 , Temp should he above freezing to 6'C ❑Samples out of temp criteria. Samples on ice, cooling process � has begun USDA Regulated Soi1 ( LJ NIA, water-samplc) {lid samples origi to In a quarantine zone within the United States: CA, NY, or SC (check mapsl? Did samples originate from a foreign source (internati nally, MVPs Nn ineludine Hawaii and Puerto Ricol? MYes o Comments/Dlscre ancy: Chain of Custody Present? 04 ONO U N/A 1. Samples Arrived within Hold Time? es C]NNn N/A 2. Short Hold Time Anat is(c72hr.)? Yes UN ❑N/A 3. Rush Turn Around Time Requested? Elves Na N/A 4. Sufficleot Volume? Err ❑No []N/A S. Correct Containers Used? -Pace Containers Used? Ye es [IN. No ❑N/A N/A 6. Containers In tact? es No Q N/A 7. Dissolved analysis: Samples Field Filtered? OYe5- No ❑N/A g. Sample kabets Match COO -Includes Oate/Time/1D/Anal sis Matrlx: ffYes Aql7 [)No ❑N/A 4. Headspace in VOA Vials (>5-6mm)? ❑Yes ❑N6 N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? Elves OYes EKO LINO ❑N/ N/A 11. CLIENT NOTIFICATION/RESOLUTION Person Contacted: DateAme: Comments/Sampfe Discrepancy: Lot 10 of Split Containers: Field Data Requited? ❑Yes ❑No Project Manager SCURF Review: P Date: 01 i Project Manager SRF Review: Date: Li 5 Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le. Out of hold, incorrect preservative, out of temp, incorrect containers) J Page 16 of 18 r0 tD -4 O 3 v a c 0 m H b m 0 n t] n CL o a c �+ A. v n A 3 r► m r � O 7 m c` Cn !Z a � LA tb H � m a a Ts U$ CL 3 0 1D s a c m a n v t° 'n n n t d_ S n a_ a O �n m -J m en a W N I[emt) OP4U•t2S rnL Plastic Unpreserved (N/A) (CI-) MU-250 mL Plastic Unpreserved (NIA) 11M.SOU mL Plastic Unpreserved (N/A) r> DPIU-1 liter Plastic Unpreserved (N/A) N SP45-125 mL Plastic H2504 (pH < 2) (CI-) SP3N-150 mL plastic HNO3 (pH < 2) 9P4Z-12S mL Plastic ZN Acetate & NaOH Is9) BP4C.12S mL Plastic NaOH (pH > 12) (CI-) WGFU•Wlde-mouthed Glass jar Unpreserved AGIU-1liter Amber Unpreserved (N/A) (CI-) AG1H-1 liter Amber HCI (pH < 2) AG31JO-250 ml-Amber Unpreserved (N/A) (Cf.) AGIS-1 liter Amber H2504 (pH a 2) AG3Y2SO mL Amber H2SO4 (pH < 2) AG3A(DGMA 250mLAmber NH4Cl(N/A)(CI-) DG9H-40 mL VOA HC) (N/A) V69T-40mL VOA Na2S203IN/A) VG9U-40 mL VOA Unp (N/A) DG9P-40 mL VOA H3PO4 (NIA) VOAK (6 vials per kit)-5035 kit (N/Al V/GK (3 uials per kit)-VPH/Gas kit (NIA) SPST-125 mL Sterile Plastic (NIA - lab) SPZT-250 mL Sterile Plastic {NIA - lab) Ax ZZOA zzzz-z BP3A-250 mL Plastic (NH2)2504 (9.3-9.7) Cubitalner VSGU-20 mL Scintillation vials (N/A) GN to �. M, 0- x a 3 °: n 3 C 0 x rr yr 0a r Cu 0 !! M ri -« c s MQ �T 1 3 W= CIA Cr MI : Md d O 0' Q 04 m n 0 G Y Q �- o WN 3 a +� o z c a ^ � a_ M 1 0 N n n H !W s 0.4 •• v C ro !J t a M N C�>I ♦ _ ♦ JO C w UQ [s C o o- n o m o is � - 0 a w w r co ,�aCeAnalytrcal Section A Requlr;a Client Information: Section H Required Prvioct lnformatla .- CHAIN -OF -CUSTODY ! Analytical Request Document The Chain -of -Custody is a LEGAL [DOCUMENT. All relevant fields must be completed accurately. Section C Invoice Information: Pane - 1 of 1 Company: Mecklenburg County Solid Waste Report To: Darten Siattlhilber Attention:.;_ q .7 Z CAddress: ,r ! Z 2145 Suale Ave Copy To- CompanyName: jb' 4 C ,,.,, „� l �U.�r• 7 �.•� I Charlotte. NC 202DS Address'. —Lli .r�.'"a ---e�_"-�e•.sz: Re utata A en r.: �"::, x�r+f:.._ir�:£=€ Emaic darrens[einhilber r macklenbunc gor Purchase Order 0: Pace Ouote; Phone: 704.579-1537 Fex PrcjoCl Name: Cantrat Compost 2 • Valleydale Pew Project Manager: kovin. odwin pacelabs.mm, 4- -- `�...*."-- STate! Lacallon Requested Due Dow Project ri: Pace Profile 0, V07-1 NC uestecIAna -nlsFtltered YIN I- . "3' +•g ."g`s '.,. t' „z? z s ar25,q; MAMIx cooE a U COLLECTED a Preservatives (y •••• arnrme Wales ow-O s' V r YYrlq WT U O ZL SAMPLE ID ° a 3 START END a '^ ;r Z r Ono Character par box. W." W a a ?� � � Imo. e (A-Z, 0.91, -1 oln�r. oT u i m Q o Ii. a, a 5 U Sampla Ids must be unique T. is x W TI)AMTIME "' u m C vUi n z =. m 5 D ca Z m < a. p . A z �r ad v0i m a g M OAT£/ >• D r 2, z O r- 41 LL F n a a ¢ 1 Outfall 001 V4T r't /1) Ci- Tr V' !TIME ! 0' y I I I I I I I X X X X IX IX X fzs �..3 ~ .6 1 `AT 11 '.11D ADDITIONAL'COtd MENTS�' :.s' R_e - - RELQIOtA3HED BYlAfFILlgT10FF �r f]AYE I.. � Y��'-STfIUE�+. a �`+ .� �.a - �,ACCEPTFii r_:- 6YTRFFI TI n. �.� ATE .TI►IE� �� � SA._-C6N�H8°}: §.....r�'��.rs:•t%ni�._.a..._.-........s -.:..,,� •.-���..,:'.:�m.{. caA. Sx? ...-�ezc..., i.r.;._.e..:x..:...:_:w -�;r �r..:«.s� ;�.1 :�_•. _. �.. .-„r- .s..d 9,... _ - .�'-�':�.` .tir -maw- n:.ww, .�-..�.. �--::�- SAMPLERNAfdE'ANOS3GtfATURE`��°..; .m. o PRINT Name of SAMP4 ER: -V c y m m z o z m z SIGNATURE of SAMPLER: DATE Signed: 9. m w. O C, MECKLENBURG COUNTY Land Use & Environmental ServicR�Rn y Solid Waste IVED September 29, 2017 Central Files NCDCNR 1 DWQ 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention: Central Files OCT 04 2017 CENTRAL FILES DWR SECTION Subject: Discharge Monitoring Reports (August/September) Compost Central — Certificate of Coverage No. NCG240016 Dear Central Files: Please find enclosed the Discharge Monitoring Reports for August and September 2017 for Compost Central, a Type 1 facility located at 5631 West Blvd in Charlotte, North Carolina. As indicated in the report, there were no qualifying flows that could be sampled for either period. If you have any questions, please contact me at 980- 314-3857 or by email at Darren.Stelnhllbera,MecklenbLlr Cg ountyNC.gov. Sincerely, L/ Darren J. Steinhilber, P.E. Solid Waste Project Manager Enclosed: 2017 DMRs PEOPLE • PRIDE PROGRESS • PARTNERSHIP 2 [45 Suttle Avenue Charlotte. North Carolina 282028 www.wipeoutw.lgtc.com Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 9/29/17 CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME Compost Central COUNTY Mecklenhure Countv PERSON COLLECTING SAMPLES Darren Steinhilber LABORATORYCharlotte Mecklenburg Utilities Lab Cert. # 192 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec or ® Monthly' August (Month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply []SA [_]Other Total event rainfall z or ® No discharge this period3 Date Sample Colle Collected' (mo/ cted' Outfall No. TSS SOD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks =__> 100 mg/L4 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.007 mg/L 0.03 mg/L 0.067 mg/L 6-9 1 2 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfali. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. "The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part ts: venicie nnaintenance Area ivionitoring Kesuits: only Tor tacimies averaging > 55 gal oT new mo Date Sample -Collected; (mo/dd/yr) _ OutfallNo.pH _ .. .� �. _ xTPH�usrng method =. 1664A SGT-HEM::. - TSS •..r Total 'Rainfall'_. Check if No Flow This Periods Average New Motor Oil Usage 6-9 .: 15 mg/L 100 mg/L" _ m i X 2 X Footnotes from Part A also apply to this Part B for oil/month. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER ATANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an original and one copy of this DMR, includinq all "No Discharge"reports, within 30 days of receipt of the lab results (or at end ofmonitorina period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 i YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are signifipnt pVa�s for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature j®rmitteO / Permit te:10/1/2011-9/30/2016 (D te) Last Revised 12/02/11 Page 2of2 uarterly Stormwater Discharge_ Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 9129/17 CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME Compost Central COUNTY Mecklenbure Countv PERSON COLLECTING SAMPLES Darren Steinhilber LABORATORYCharlotte Mecklenburg Utilities Lab Cert. # 192 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec or ® Monthly) September (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow [:]WaterSupply ❑SA ❑Other Total event rainfall 2 or ® No discharge this period3 Date Sample Collected) (mo/dd/yr) Outfall No. TSS COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks ===> 100 mg/L4 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.007 mg/L 0.03 mg/L 0.067 mg/L 6-9 1 2 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part 13: venicle Maintenance Area ivlonliormg KesulTs: only Tor Tacinies averaging 55 gal oT new mo date Sample Collected' (mo/dd/yr) s _ Outfall No.., r pH TPWusing,method, 1664A SGT HEM w:x. TSS :,Total Ramfall2 �Check if No� Flow � - This :Period3 P- ; Average New Motor Oil Usage •_ � - 6-9 15 mg/L loU mg/L° - 1 X 2 X Footnotes from Part A also apply to this Part B for oil/month. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. + 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO ❑ REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an oriainal and one conv of this DMR, includina all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (SignatuW o0err6Ae9) Permit) ate:10/1/2011-9/30/2016 S (Da e) Last Revised 12/02/11 Page 2 of 2 uno ,\ u c � x R�,M on.Ruv® MECKLENBURG COUNTY Land Use & Environmental Services Agency Solid Waste August 7, 2017 Central Files NCDENR / DWQ 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention. Central Files Subject: Discharge Monitoring Report Compost Central — Certificate of Coverage No. NCG240016 Dear Central Files: CE111pn Ali( - Please find enclosed the Discharge Monitoring Reports for June and July 2017 for Compost Central, a Type I facility located at 5631 West Blvd in Charlotte, North Carolina. As indicated in the report, there was no qualifying flow that could be sampled this period. If you have any questions, please contact me at 980-314- 3857 or by email at Darren.Steinhilber a,MecklenburgCountyNC•gov. Sincerely, en J. Steinhilber, P.E. Solid Waste Project Manager Enclosed: 2017 DMR PEOPLE • PRIDE PROGRESS • PARTNERSHIP 2145 Sultle Avenue Charlotte. North Carolina 282028 www.wipcoutwaste.com Quuarter_I_y Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 8/7/17 CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME Compost Central COUNTY Mecklenbure Countv PERSON COLLECTING SAMPLES Darren Steinhilber LABORATORYCharlotte Mecklenburg Utilities Lab Cert. # 192 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results I2 SAMPLE COLLECTION YEAR 2017 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec or ® Monthly' June_ (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ❑Other Total event rainfall 2 or ® No discharge this period' Date Sample Collected' (mo/dd/yr) Outfall No. TSS COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks =__> 100 mg/L4 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.007 mg/L 0.03 mg/L 0.067 mg/L 6-9 1 2 ' Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 cart b: venicie IvlamLenance Area Ivlonitoring Kesuiu: only Tor Tacllltles averaging > gal CIT new mo Date Sample Collected) , r(mo/dd/Yr)' ` Odtfali No. �pH TPH using method - 1664A SGT-HEM � TSS �. -Total ; Rainfall' Check if Na Flow . This -Period j - Average New Motor Oil Usage 5-9 . 15 mg/L ' 100 mg- 1 X 2 X Footnotes from Part A also apply to this Part-B for oil/month. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. ' • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Teresa Bradford Moil an original and one copy of this DMR, including all "No Discharge" reports. within 30 dovs of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: i "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Date] it Date: 10/1/2011-9/30/2016 Last Revised-1"02/11 Page 2 of 2 Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted _ 817117 CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME Comoost Central COUNTY Mecklenbure Countv ` PERSON COLLECTING SAMPLES Darren Steinhilber LABORATORYCharlotte Mecklenburg Utilities Lab Cert. # 192 Comments on sample collection or analysis: T Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE QUARTER ❑ Jan=March ❑ April -June ❑ July -Sept ❑ Oct -Dec or ® Monthly' July _ (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ❑Other Total event rainfall 2 or ® No discharge this period' Date Sample Collected' (mo/dd/yr) Outfall No. T55 a• COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks =__> 100 mg/O 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.007 mg/L 0.03 mg/L 0.067 mg/L 6-9 1 2 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 4The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Date Sample. Collected) (mo/dd/yr) = 'Outfall No. = pH = TPH using method 1664A SGT HEM TSS Total Rainfallz Check WNo Flow 'This M Period' AVerage New Motor Oil Usage y '6=9� 15 mg/L - ,. 100 mg/U , 1 X 2 x Footnotes from Part A also apply to this Part B FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an oriainal and one coav of this DMR. includina all "No Discharae" reports. within 30 days of receibt of the lab results for at end of monitoring aeriod in the case of "No -Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." KurePT Ferrrnttee) t Date:10/1/2011-9/30/2016 /— (Date) Last Revised /02/11 Page 2 of 2- 9. E��VRQ C r °c u L °Rr v2 y CArtyO S MECKLEN B U RG COUNTY Land Use & Environmental Services Agency Solid Waste May 31, 2017 RECEIVED Central Files NCDENR/ DWQ JUG! 0 5 top 1617 Mail Service Center CENTRAL FILES Raleigh, North Carolina 27699-1617 DWR SECTION Attention: Central Files Subject: Discharge Monitoring Report Compost Central — Certificate of Coverage No. NCG240016 Dear Central Files: Please find enclosed the Discharge Monitoring Report, April 2017, for Compost Central, n Type I facility located at 5631 West Blvd in Charlotte, North Carolina. [f you have any questions, please contact me at 980-314-3857 or by email at Darren. Stein hilber a Mecklenbur gC ountyNC.�ov. Sine ly, Darren J. Steinhilber, P.E. Solid Waste Project Manager Enclosed: 2017 DMR PEOPLE • PRIDE PROGRESS • PARTNERSHIP 2145 Soule Avenue Charlottc, North Carolina 282028 lvli w.xvipcoutwaste.coni Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 5/31/17_ CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME Compost Central COUNTY Mecklenburg County PERSON COLLECTING SAMPLES Darren Steinhilber LABORATORYCharlotte Mecklenburg Utilities_ Lab Cert. # 192 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results period3 SAMPLE COLLECTION YEAR 2017 SAMPLE QUARTER ❑ Jan -March ❑ April -June [❑ July -Sept ❑ Oct -Dec or ® Monthly' Aril month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ❑Other Total event rainfall ? 3.10 in or ❑ No discharge this Date Sample Colle Collected' (mo/ cted Outfal! No. TSS COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks =_-> 100 mg/L' 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.007 mg/L 0.03 mg/L 0.067 mg/L 6-9 04/24/17 1 46 190 26000 1.3 1.7 0.011 <0.005 0.022 7.13 04/24/17 2 34 260 >600000 5.6 3.6 0.0093 <0.005 0.026 6.87 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 cart ts: Venlcle mamienance area Ivlonitonng Kesulis: only Tor Taclntles averaging > 53 gal UT new mo- Date Sample Collectedl' (mo/dd/yr) =. Outfall No.. pH TPH using method ' 1664A SGT NEM ` TSS r x Total: � Rainfall' Check if No � Flow This Period',' Average New Motor Oil Usage 6-9 , M 15 mg/L 100 mg/L°. 12/06/16 1 7.13 NA 46 3.10 12/06/16 2 6.87 <5.0 34 3.10 75 gal/month Footnotes from Part A also apply to this Part B :or oil/month. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. + 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an original and one copv of this DMR, includina all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 M YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 2 of 2 CHARLOTTE W6TER Environmental Laboratory Services LOCATION: Compost Central 1 LOC ID: G-COMPCENTI SAMPLE DATE -TIME: 04/24/2017 12.20 SAMPLE DESCRIPTION: Grab Laboratory Analysis Report Report Date: 05/10/2017 10:38 CHAIN OF CUSTODY #: 170424018 Parameter Result Units RL Method Start Date 1 Time Analyst Sample ID: AG18450 AG18450 Fecal Coliform 26000 CFUI100 ml 100 SM9222D-11 04/24/2017 14:20 STIR AG18450 Chemical Oxygen Demand 190 mglL 50 HACH 8000 04/25/2017 13:50 ECS AG18450 Total Suspended Solids 46 mglL 8.3 SM254OD-11 04/2512017 08:06 CRB AG18450 Metals Digestion Completed EPA 200.2 04/25/2017 01:30 RDB AG18450 Copper by ICPMS 11 ug1L 2.0 EPA 200.8 04/26/2017 13:58 RDB AG18460 Lead by ICPMS < 5.0 ug1L 5.0 EPA 200.8 04/2612017 13:58 RDB AG18450 Zinc by ICPMS 22 uglL 10 EPA 200.8 04/2712017 15:53 RDB AG18450 Total Kjeldahl Nitrogen Digestion Completed EPA 351.2 05/02/2017 09:10 TCV AG18450 Total Kjeldahi Nitrogen 1,3 mg1L 0.25 -EPA35112-93 '05/0212017 "12:34 TCV AG18450 pH Lab 7.13 su 1.00 SM4500H-B-11 05/04/2017 16:00 TCV AG18460 Total Phosphorus Digestion Completed SM4500P-B(5)-11 04/26/2017 11:00 MSC AG18460 Total Phosphorus 1.7 mg1L 0.10 SM4500P-H-11 04/26/2017 13:48 MSC Comment: Samples received above temperature for both BacT and wet chem/autochem analytes: there was no collection temperature recorded by client. pH: Sampels received over method hold time. Laboratory Supervisor: 4i-/'4l' The resuits contained on this r port are to the samples listed above. Charlotte Water-Envfronmental Laboratory Services N.C. Certification No. 192 N.C.DHHS Certification No. 37417 EPA Certification No. 01215 4222 Westmont Drive, Charlotte, North Carolina 28217 Page 1 of 1 CHARLOTTE-MECKLENBURG UTILITY DEPARTMENT Environmental Laboratory Services CHAIN OF CUSTODY RECORD 4222 Westmont Drive, Charlotte, N.C. 28217 (704) 336 - 2854 or (704) 622 - 7280 011111,0"Ti Ct P AGE OF NC DENR Certification No. 19Z NC DHHS Certification No. 37417; US EPA Certification No. 01215 Mecklenburg Waste Send REPORT To: Send INVOICE To: Sampled By (Print Name): ' CLJENP. e�,;L NCG240016 CompostCentral Compost Central Darren Sleinhilber Darren Steinhilber Witnessed By (Print & Sign Name - if applicable) FACIUTY: ADDRESS: 2145 Suttle Ave, Charlotte, NC 28208 Project Name or Code: Compost Central P.C. NUPMER 3102-2-16 CONTACT: Darren SWnhilber Sample Collecctien p Sample PChemical Sample Preservative Analyses Date I Time T e Containers ray t15E 3c m m mLAS LOCATION LOCATION E IT v �c a ¢ n y m S 2 tl - LAB 5M M. E ipr _c CODE DESCRIPTION o o E 'rn a E a c w .m w ep o m o o V n — c L `O d c`� n O rt, t, n O x O eZ-' 2 = 4 m tip rn a S (:J d 0V m z ro to V� a w'•m�-i_;.:�::aET."-✓.� G-COMPCENTI CompostCentral t i� IX IX r1=a jZ:c", = LirvP x x .:� , G-COMPCENTI Compost Central 1� o �JLL� r _�~ °�° �a- x X i x x x &k y me .. ' ^° k" G COMPCENTI Compost Central 1 < G COMPCENTI Compost Central 1 < 2 x x 1 x x xr_ G-COMPCENTt Compost Centra[ 1' o <2 Z-� ix s`g x x 1 x x x _.� 1 -4— B5 �i Sampie Temp at collection ° C Relinquished B' ignature) �• r Ree ' By: (SignatVel � DaUr ZY r � MlitaryTime • 1 i "-'Labnratory-Check=in=WritellnitialstiWiftTeinp'efatEireT::,� Sam Ie:Teiri" at;recei�in'";111;1_Fdl C h fBKtSignature) By: (Signature) Dale MltaryTime Tempf'Blank in',Cooler_ at7receiving4n_L°ab; �� c Zero 4ads a`a_w_ 8�tefioe"talo} VOAs t`_ �+'ate t �Yes�No3 0 Relinquished By: (Signature) Received By; (Signature) NC Certfication No. 192 Date Military Time Sam les in Pro er:Coritainers"d ? Y' 'rNa i:.n1a3 GhloriiTatedisain les"de ctilaririated. Com O5itec _ YesNo nC�f COMMENTS: Complete all yellow shaded areas, due areas are for;LAB U3E ONLY. Gtilosiriated:sarTi Ees de�cti[orina4ecf- Grab ..�"$� - 'No'rilar�-_-`, (GN)S�u Ifideposiit�e; :� YesNo nl [nolcaie unusual [ [me [apses min coae aE signature Defined Codes:S=Secure or U-Not Secure and C=Cooler or R=Refrig or T=Transported in cooler or O=Other with description in Comments Revision OUZ; Effective pate 041U1120T2 12l5M16 CHARLOTTE WATER Environmental Laboratory Services Sample Receipt Checklist Completed by: Initials : �JJ Date/Time: - �� I �2 L(� Cam L �} L . 701 Sample Matrix: —�istewater EDrinkingWater OCrypto/Giardia (LT2) Other: [7Field Analysis/Information Only (No coolers Custody Seal(s) intact?: Yes ONO N/A Type of Ice Used: t 11Blue Shipping Container Intact: OYes ONO kA 1L1DryIcL ONone Thermal Preservation: 'Sample Temperature measured lmmediat0y after removal from cooler; Daily IR Correction factor applied. *Notify management Immediately of any sample that did not meet temperature requirements or frozen, *If multiple parameters, In additional to BacT are collected for a site, two receipt temperatures must be measured. A receipt temperature for the BacT plus another bottle must be measured and recorded on the COC. Requirements: DW: 5 6'C WW: <_ 6*C BacT: 510'C LT2 Crypto/Glardla: s 20'C LT2 E. coli: 510'C Do sample recelpt temperatures meet requirements (including requirement by downward trend)? Yes �fup, explain below. Downward trend required to meet requirment Yes Sa oLe 1 .e c e * At time of receipt into the laboratory, the allowed downward trend may be a�plled to meet temperatur requirement. Initial temperature from the sample collector becomes critical. It samples are received next day, receipt temperatures must meet requirements listed above. Chemical Preservation: Note: *If samples are not preserved correctly, notify Personnel. Do not check BacT, TOC, VOA, THM and HAA. All containers needing preservation are found to be in EPA compliance? 0 No 7N/A loses If no, explain. *If the pH of a metals not Including Hg1 is incorrect follow these steps. *If the pH of any other chemically preserved sample Is Incorrect 1. on the COC, document sample pH prior to adding additional preservative. [not including metals], follow these steps: 2. on the COC and sample bottle, document the date/time additional 1. Any samples not properly preserved must be qualified with a preservative Is added to the sample, comment on the COC and in LIMS. 3. No comment Is needed In LIMS. 2. Notify personnel immediately of samples not correctly preserved. if possible, substitute a correctly preserved bottle. Document on COC and notify personnel. Write "DO NOT USE" on the incorrectly preserved bottle. COC Properly Filled Out? Yes F--JNo if no, explain. f COC Correction sent to Project Manager? Yes Nn>E]N/A Do sample labels agree with the COC? kNs ONO If no, explain. All sample bottles accounted for? �es �No Samples Arrived within Hold Time? J Y s ❑NO (tfno, notify Project Mgr.) Correct Bottles Used? �No ��s VOA Vials have Zero Headspace (< 6 mm)?Dyes [—]NO ONA *Bubbles should be no larger than: `ITno, not] Laboratory Section Supervisor. Short Hold Analyses (<48 hrs)? es F�No Rush Turn Around Time (TAT)? Oyes If yes, notify Laboratory section(s). If yes, np ify Project Manager. Addition Informatlon/Comments: Effective Date: April 18, 2017 This printed copy Is an UNCONTROLLED copy of the online CONTROLLED document. CHARLOTTE WT E R Environmental Laboratory Services LOCATION: Compost Central 2 LOC ID: G-COMPCENT2 SAMPLE DATE -TIME: 04/24/2017 12:30 Laboratory Analysis Report Report Date: 05/10/2017 10:38 SAMPLE DESCRIPTION: Grab CHAIN OF CUSTODY #: 170424020 Parameter Result Units RL Method Start Date / Time Analyst Sample ID: AG18453 AG18453 Fecal Coliform >600000 CFU1100 ml 100 SM9222D-11 04/24/2017 14:20 STR AG18453 Chemical Oxygen Demand 260 mglL 50 HACH 8000 04/25/2017 13:50 ECS AG18453 Total Suspended Solids 34 mg1L 8.3 SM254OD-11 04/25/2017 08:06 CRB AG18453 Metals Digestion Completed EPA 200.2 04/25/2017 01:30 RDB AG18453 Copper by ICPMS 9.3 ugfL 2.0 EPA 200.8 04/26/2017 14:02 RDB AG18453 Lead by ICPMS 46.0 ugfL 5.0 EPA 200.8 04/26/2017 14:02 RDB AG18453 Zinc by ICPMS 26 uglL 10 EPA 200.8 04/27/2017 15:55 RDB AG18453 Hexane Ext Material Silica Gel (TPH) < 5,0 mg1L 5.0 EPA 16648 05/01/2017 12:52 MCK AG18463 Hexane Extractable Material (O&G) < 5.0 tng1L 5.0 EPA 1664E 05/0112017 08:31 MCK AG18453 Total Kjeldahl Nitrogen Digestion Completed EPA 351.2 05/02/2017 09:10 TCV AG18453 Total Kjeldahl Nitrogen 5.6 mg1L 0.25 EPA351.2-93 05/02/2017 12:34 TCV AG18453 pH Lab 6.67 su 1.00 SM4500H-B-11 05/04/2017 16:00 TCV AG18453 Total Phosphorus Digestion Completed SM4500P-B(5)-11 04/2612017 11:00 MSC AG18453 Total Phosphorus 3.6 mg1L 0.10 SM4500P-H-11 04/2612017 13:48 MSC Comment: Samples received above temperature for both BacT and wet chemlautochem analytes; there was no collection temperature recorded by client. pH: Sampels received over method hold tigle. ,7/J Laboratory Supervisor: The results contained on this r ort are specific to the samples listed above. Charlotte Water -Environmental Laboratory Services N.C. Certification No. 192 N.C.DHHS Certification No. 37417 EPA Certification No. 01215 4222 Westmont Drive, Charlotte, North Carolina 28217 Page 1 of 1 CHARLOTTE-MECKLENBURG UTILITY DEPARTMENT e Environmental Laboratory Services CHAIN OF CUSTODY RECORD 4222 Westmont Drive, Chadotte, N.C. 28217 (704) 336 - 2K3 or (704) 622 - 7280 CiLmil,OTM, coc# �..�a�««.���� � __1 �, PAGE OF NC pENR Certification ND.192; NC DHHS Cettiflcatian No. 37417; U5 EPA Certiflcaiivn No. 01215 �,,,,,� �..�.,,.,� � - l../ � Mecklenburg County -Solid Waste Send REPORT To: Send INVOICE To: Sampled By (Print Name): CLIENT: Compost Central Pennit NCG240016 FACUT1': Darren Steinhilber Darren Steinhilber Witnessed By (Print & Sign Name - if applicable) ADDRESS: 2145 Suttle Ave, Charictte, NC 28208 P.D. NUIVEEFt• 3102-2-16 Project NameorCode: Compost Central CONTACT: Darren stcinhilne( Sample Collection Sample Sample'<: ChenucalPreservative Analyses Date Time Type Containers }, LOCATION LOCATION E M _° N o d H N _ i. LAB USE LAB SAMP LE IQ CODE DESCRIPTION o° R d E o N ro o v� C) L �8or Zc>a?z co iv, in C�'S cTi. m z x x z v `° d m 0 rn 5 G-COMPCENT2 Compost Central 2 X X 1 N X X .1sral G-COMPCENT2 Compost Central 2 1 � c3 o , � X X r X X X c GCCMPCENT2 Compost Central 2 C > < 2 � , s n x IX N x F _> x G-COMPCENT2 Compost Central 2 o <: XX 1� x XX ;w G-COMPCENT2 Compost Central 2 ix a <2[4t^' IX i x 1 Ln x x IX I G-CDMPCENT2 Compost Central 2 i ok Ix I I I q x x 2 :2 x�� Sample Temp at collection " C Rem ,, ` ;- e e Received Ely: (Sig Lure yrl1i T-17 Date Military Time � Labarato .,Cheek=in =Write;lnitiafs'.WithzTem erature ? — Sam `lesTer►i atAreC@lVln` ;ln;Lab .; t_M s3 Z e ,., C Rerin shed 9 Si nature : y: f 9 ) F 'ved B S nature y: ( i9 ) ❑ate Military Milita Time TernpIBlank InxCooler at;"receiving'iin i ab;_ j�Mi C Ze�o°fleads acei& tef10r715e ta.for 1/�f) 5- � _ :' 'aYeS ,NO N Rerinquished By. (Signature) Received By: (Signature) NC Cenificabon No. 192 Date Military Time r Chlorinated,sam les de iilorinated Com osste ^ '' �" �' ' e�Yes � No : Ala � vW� COMMENTS: Complete all yellow shaded areas. (BI�e areas are for lAB USE ONLY_ Chlonnati d-sarn les`de?chloin- nafed, Grab �.M es xNa n/a (CN)!Sulfide:positive Indicate unusual Time lapses with code at signature: Defined Codes:S=Secure or U=Not Secure and C=Coofer or R=Retrig or T=Transported in cooler or O=Other with description in Comments Revision 002; Effective Date 0410112012 2/15/2017 CHARLOTTE WATER Environmental Laboratory Services 1 Sample [Reeceipt Checklist l� Completed by: Initials: J`� b Date/Time: -€ �[-f'r j ? { COCK:�G2(�-J Sample Matrix: Wastewater Drinking Water DCrypto/Glardio (LT2) Other: Field Analysis/Information Only (No cooler) Custody Seal(s) Intact?: Yes [--]No N/A Type of Ice Used: Wet Slue KN Shipping Container Intact: Dyes ONO /A Dry Ice None Thermal Preservation: *Sample Temperature measured immediately after removal from cooler; Daily IR Correction Factorapplied. • Notify management immediately of any sample that did not meet temperature requirements or frozen. 'If multiple parameters, in additional to BacT are collected for a site, two receipt temperatures must be measured. A receipt temperature for the BacT plus another bottle must be measured and recorded on the COC. Requirements: DW: 5 WC WW: 5 6'C BacT: 5 10'C LT2 Crypto/Giardia: 5 20'C LT2 E. tali: 5 1O'C Do sample receipt temperatures meet requirements (including requirement by downward trend)? Yeslo, explain below. r. Downward trend required to meet requirment7 ff ] Yes n1, c o ? e. G ' At time of receipt Into the laboratory, the allowed downward trend may be applied to meet temperatur requirement. Init€a! temperature from the sample collector becomes critical. If samples are received next day, receipt temperatures must meet requirements listed above. Chemical Preservation: Note: `If samples are not preserved correctly, notify Personnel. Do not check BacT, TOC, VOA, THM and HAA. All containers needing preservation are found to he in EPA compliance? Yes ONo []N/A If no, explain. if the aH of a metals [not Including Hpi Is Incorrect, follow these steps. `If the pH of any other chemically preserved sample is incorrect 1. On the COC, document sample pH prior to adding additional preservative. (not Includlne me.talsl. follow these. Ste es: 2. On she COC and sample bottle, document the date/time additional 1. Any samples not properly preserved must be qualified with a preservative Is added to the sample, comment on the COC and in LIMS. 3. No comment is needed In LIMS. 2. Notify personnel immediately of samples not correctly preserved. If passible, substitute a correctly preserved bottle. Document on COC and notify personnel. write "DO NOT USE" on the Incorrectly preserved bottle. COC Properly Filled Out? �Y s F-1No If no, explain. CDC Correction sent to Project Manager? Dyes1:1 No 5;�JN/A Do sample labels agree with the COC? �YYes ONO If no, explain. .. _ ....- . —0 : - ..L. All sample bottles accounted for? p pes No Samples Arrived within Hold Tlme?,;>f�s No (if no, notify Project Mgr.) Correct Battles Used? 'ides F-1No VOA Vials have Zero Headspace (< 6 mm)? t1Yes € No A *Bubbles should be no larger than: O I nn, not Laboratory Section Supervisor. Short Hold Analyses (< 48 hrs)7 s ❑ No Rush Turn Around Time (TAT)? Dyes FPO If yes, notify LaboratorySectianlsi, If yes, no y Protect Manager. Addition Information/Comments: Effective Date: April 18, 2017 This printed copy Is an UNCONTROLLED copy of the online CONTROLLED document. Quarterly Stormwater Discharge MonitoringReport for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted _ 6/2/17 CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME Comoost Central COUNTY Mecklenburiz Countv PERSON COLLECTING SAMPLES Darren Steinhilber LABORATORYCharlotte Mecklenburg Utilities Lab Cert. # 192 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec or ® Monthly)_ May (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow []water supply ❑SA ❑Other Total event rainfall z or ® No discharge this period3 Date Sample Colle Collected' (mn/ cted Outfall No. T55 COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks =__> 100 mg/L4 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.007 mg/L 0.03 mg/L 0.067 mg/L 6-9 1 2 7 sUN tj a r �=riTl to . FILE-3 flWR v t ivy• 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part H: Vehicle Maintenance Area Monitoring Kesults: only for tacilities averaging > 55 gal of new mo rv, _ w -.-.Check.' if Na Date Sample Outfall No.. pH TPH using method s- Total Flow d TSS Avdrage New Motot Oil Usage Collected' 1664A SGT-HEM Rainfall' This (mo/dd/yr) Period3 6-9 15 mg/L 100 mg/L° LL 1 X 2 X Footnotes from Part A also apply to this Part B for oil/month. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO ❑ REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an original and one copy of this DMRincluding all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports)to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. i am aware that there are significanalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." c- 4rmituDrk'e: g to rmit e) _ {Date) 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 2 of 2 MECKLENBURG COUNTY Land Use & Environmental Services Agency Solid Waste May 31, 2017 Central Files NCDENR / DWQ 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention: Central Files Subject: Discharge Monitoring; Report Compost Central — Certificate of Coverage No. NCG240016 Dear Central Files: N Please find enclosed the Discharge Monitoring; Report, March 2017, for Compost Central, a Type I facility located at 5631 West Blvd in Charlotte, North Carolina. As indicated in the report, there was no qualifying; flow that could be sampled this period. If you have any questions, please contact me at. 980-314-3857 or by email at Darren. Steinhilbera Mecklenbur CountyNC.gov. Sincerely, rr Darren J.'Steinhilber, P.E. Solid Waste Project Manager Enclosed: 2017 DMR PEOPLE • PRIDE PROGRESS • PARTNERSHIP 2145 Suttle Avenue Charlotte. North Carolina 282028 www,wipeoul%vastexom Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 5 31 17 CERTIFICATE OF COVERAGE NO. NCG240016 FACILITY NAME Comoost Central COUNTY Mecklenbure Countv PERSON COLLECTING SAMPLES Darren Steinhilber LABORATORYCharlotte Mecklenburg Utilities_ Lab Cert. # 192 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑Oct -Dec or ® Monthly) March _ (month) DISCHARGING TO CLASS ❑ORW ❑HQW [:]Trout❑PNA []Zero -flow ❑Water Supply ❑SA ❑Other Total event rainfall z or ® No discharge this period] Date Sample Collected) (mo/dd/yr) Outfall No. T55 COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Porameter benchmarks =_=> 100 mg/O 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.007 mg/L 0.03 mg/L 0.067 mg/L 6-9 1 2 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 'For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 4The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. rl Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part ts: venlcle maintenance Area IvlonrEoring Kesults: only Tor Tacllities averaging > 55 gal oT new mo r , Date Sample I Collected ' (mo/dd/yr) Outfall No . pH - TPH using method '1664ASGT-NEM _:. -. Tss :,. Total Rainfa[Iz. Check _ if No Flow -This Period' . Average New Motor Oil Usage � 6-9' 15 mg/L 100 mg/L4- ° - - 1 X 2 X Footnotes from Part A also apply to this Part B for oil/month. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an original and one copy of this DMR, includina all "No Discharae" reports, within 30 days of receipt of the lab results (or at end of monitorina period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." { te) Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 2 of 2 Quarterly Stormwater Discharge_ Monitoring Resort for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 3/1/17 CERTIFICATE OF COVERAGE No. NCG24®UZ6 FACILITY NAME Compost Central COUNTY Mecklenbure Countv PERSON COLLECTING SAMPLES Darren Steinhilber LABORATORYCharlotte Mecklenburg Utilities Lab Cert. # 192 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec y�ggr� onthly' February (month) DISCHAFRK(CT&a/ �ORW ❑HQW ❑Trout ❑PNA MAR 1 � ?Ol,❑Zero-flow [_]Watersupply ❑SA [—]Other CENTRAL FILES DWR SECTION Total event rainfall 2 or ® No discharge this period' Date Sample Colle Collected' (mo/ cted Outfall No. T55 COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmorks 100 mg/L° 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.007 mg/L 0.03 mg/L 0.067 mg/L 6-9 1 2 ' Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 'For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for tacilities averaging > 55 gal of new mo- -if No Date Sample outfall No. pH 1 TPH using method Total- Flaw p'T5S Average New Motor Oil Usage collected' 1664ASGT-HEM Rainfall' TThis (mo/dd/yr) N Period3- � - 6-9 , 15 mg/L l00 mg/0, 1 X 2 X Footnotes from Part A also apply to this Part B for oil/month. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® No ❑ REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an original and one coo y oL this DMR including_all "No Dischar e" reports, within 30 do Vs of receipt of the lob results or at end of monitorin g period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or, supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 0 (Signature of r1i ittegy Permit Ie:2011-9/30/2016 c ---)) � ( a ) Last Revised 12/02/11 Page 2 of 2 Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 2/28/17 CERTIFICATE OF COVERAGE NO: NCG240016 FACILITY NAME Comoost Central COUNTY Mecklenbure Countv PERSON COLLECTING SAMPLES Darren Steinhilber LABORATORYCharlotte Mecklenburg Utilities Lab Cert. # 192 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2017 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec or ® Monthly)_ January (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA RECEIVED ❑Other MAR 13 2017 OENTRAL FILES Part A: Stormwater Benchmarks and Monitoring Results DWR SECTION Total event rainfall or ® No discharge this period3 Date Sample Col Collected) (molected) Outfall Na. T55 COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc -.OH Parometer benchmarks =__> 100 mg/L' 120 mg/L 1000 col,/100 mL 30 mg/L 2 mg/L 0.007 mg/L 0.03 mg/L 0.067 mg/L 6-9 1 2 ' Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit bate: lo/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 hart ts: venlcle maintenance Area Monitoring Kesults: only Tor Tacilimes averaging ;, 53 gal or new mo Date Sample i Collected- Outfall No. :. .r �� pH :_ b w _ ram= �.- TPH using method J664A`SGT-HEM - T55 _ ; r Total, ��Rainfall. x heck if No Flow This Period { Average New Motor Oil Usage , ��. 6-9 15 mg/L ; 100 mg/L° 1 X 2 X Footnotes from Part A also apply to this Part B for oil/month. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. ■ TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an original and one copy o this DMR includln all "No Dischar e" re orts within 30 da s o receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to_: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of ,ny knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." [Date Perr Date:10/1/2011-9/30/2016 Last Revised 12/02/11 ' Page 2 of 2