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Home My WebLink AboutNCG120096_MONITORING INFO_20190203STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. �v �C, DOC TYPE ❑HISTORICAL FILE EXMONITORING REPORTS DOC DATE )011 ❑ YYYYM M DD DocuSign Envelope ID: 38A4C65D-1A67-48DE-9AB7-C18C3BOC9367 SMITH+GARONER EN61NEERS January 24, 2020 NCDEQ Division of Water Quality Attention: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 ADDRESS TEL 14 N. Boylan Avenue, Raleigh NC 27603 919.828.0577 RECEEIVED EEB 0 3 2019 RE: Discharge Monitoring Report —January 2020 Red Rock CGD landfill ccl'~TR�� r lt_�� DWR SE C--TION Certificate of Coverage #NCG120096 General Permit #NCG120000 Dear Sir/Madam: WEB wwwsmithgantnednc.com Smith + Gardner (S+GI is pleased to submit this Discharge Monitoring Report (DMR) for stormwater monitoring at the Red Rock C&D Landfill. The facility is permitted to discharge stormwater related to landfilling activities under Certificate of Coverage ICOC) No, NCG120096, General Permit No.120000. The facility is required to monitor discharge at the following Stormwater Discharge Outfall (SDO) locations: 1. COMP-1 (Basin B, Basin 6, Basin T1); 2. COMP-2 (Basin A); 3. Sediment Basin 1 (SB-11; and 4. COMP-4 (Basin 8) Sediment Basin 1 entered Tier III status for total suspended solids [TSS) in December 2018 and improvements were made to mitigate erosion from the soil stockpile area. The samples collected at SB-1 exceeded the benchmark threshold for TSS. Monthly sampling will continue at SB-1. Samples were also taken from Comp-1 and Comp-2. Comp-2 exceeded the benchmark threshold for fecal coliform. Comp-2 received Tier III sampling relief in September 2018, so semiannual sampling will continue at Comp-2 for fecal coliform. We are providing two (2) copies of the DMR report for this submittal. If you have any questions, or require further information, please contact us via phone at (9191 828-0577 or by email. Sincerely, SMITH GARDNER, INC. Docu5igned by: J� Cc Staff Engineer, ext. 170 iessefdsmith-gardnerinc.com l DocuSigned by., 1 J+ 358C21E84007440,.. W. Michael Brinchek, P.E. Senior Project Manager, ext.128 mike(asmithgardnerinc.com Attachments CC: Don Plessinger IGFLI File H.%Proieos\Red RoO.. D15p05a11NdPDES12020\1- JanuarytiDWnripdes_ Ianuary202(I Tier 111,docx DocuSign Envelope ID: 38A4C65D-lA67-48DE-9AB7-C18C3BOC9367 This page intentionally left blank. DocuSign Envelope ID: 38A4C65D-1A67-48DE-9AB7-C18C3BOC9367 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG120000 Date submitted January 22, 2020 CERTIFICATE OF COVERAGE No. NCG12 0096 FACILITY NAME Red Rock C&D Landfill COUNTY Wake PERSON COLLECTING SAMPLES Jesse Li (Smith Gardner, Inc. LABORATORY Pace Analytical Lab Cert. # 37738 Comments on sample collection or analysis: Part A. Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2020 SAMPLE PERIOD ❑■ Jan -June ❑ July -Dec or ❑■ Monthly' Januaa month DISCHARGING TO CLASS ❑ORW ❑HQW [—]Trout ❑PNA `FIVE® ❑Zero -flow ❑Water Supply ❑SA i± E8 4 3 200 #Other C. NSw .I�', i-RAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ;WR SECTION ❑ No discharge this period' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches 3 Chemical O' xygen Demand mg/L Fecal Colffarm Colonies per 100 mL Total Suspended Solids mg/L I . pH, Standard Units Benchmarks _ - 120 1000 100 or 504 6.0-9.0 Parameter Code - 46529 00340 31616 C0530 00400 S13-1 1 /13120 0.36 34.7 200 102 6.77 Comp-1 1 /13/20 0.36 <25.0 400 16.4 6.78 Comp-2 1113/20 0.36 43.9 1480 53.0 6.77 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, theV must be re orted in the format "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-5/31/2021 SWU-248, last revised 11/1/2018 Page 1 of 2 DocuSign Envelope ID: 38A4C65D-lA67-48DE-9AB7-Cl8C3BOC9367 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new ail per month. ❑ No discharge this period-' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Non -Polar oil & Grease mg/L Total Suspended Solids, mg/L New Motor or Hydraulic Oil Usage, gal/mon Benchmarks _ - 15 100 or 504 — Parameter Code - 46529 00552 C0530 NCOIL Footnotes from Part A also apply to this Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES Q NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES Q NO ❑ REGIONAL OFFICE CONTACT NAME: Thad valentine Mail an oriainal cony of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." /—pocuSigned by: VV1/L Signature of Perm 1/24/2020 Date Permit Date: 11/1/2018-5/31/2021 SWU-248, last revised 11/1/2018 Page 2 of 2 DocuSign Envelope ID: 38A4C65D-1A67-48DE-9AB7-Ci8C3BOC9367 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG120000 Date submitted January 22, 2020 CERTIFICATE OF COVERAGE NO. NCG12 0096 FACILITY NAME Red Rock C&D Landfill COUNTY Wake PERSON COLLECTING SAMPLES Jesse Li (Smith Gardner, Inc.) LABORATORY Pace Analytical Lab Cert. # 37738 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2020 SAMPLE PERIOD ■❑ Jan -June ❑ July -Dec or *Monthly' January (month] DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA []Zero -flow []Water Supply [:]SA *Other PLEASE REMEMBER TO SIGN ON THE REVERSE 4 No dischorge this period' Outfall No. Date Sample 1 Collected (mo/dd/yr) 24-hour rainfall amount, Inches' Chemical Oxygen Demand mg/L Fecal Coliform Colonies per 100 mL Total Suspended Solids mg/L pH, Standard Units Benchmarks - - 120 1000 100 or 504 6.0-9.0 Parameter Code - 46529 00340 31616 C0530 00400 S6-1 1 /13/20 0.36 34.7 200 102 6.77 Comp-1 1113/20 0.36 <25.0 400 16.4 6.78 Comp-2 1 /13/20 0.36 43.9 1480 53.0 6.77 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-5/31/2021 5WU-248, last revised 11/1/2018 Page 1 of 2 DocuSign Envelope ID: 38A4C65D-tA67-48DE-9AS7-C18C3BOC9367 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n No discharge this period1 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hourrainfall amount, Inches3 Non -Polar Oil & Grease mg/L Total Suspended Solids, mg/L New Motor or Hydraulic Oil Usage, gal/mon Benchmarks - - 15 100 or 504 — Parameter Code 46529 00552 C0530 NCOIL Footnotes from Part A also apply to this Part 8 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: + A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES Q NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES 0 NO ❑ REGIONAL OFFICE CONTACT NAME: Thad Valentine Mail an original eopv of this DMR, including all "No Discharae" reports. within 30 days of receipt of the lab results for at end of monitorina period in the case of "No Discharge" reports) to: Division of Water Quality Attm DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." —OocuSigned by: Signature of Pe Permit Date:11/1/2018-S/31/2021 1/24/2020 Date SWU-248, last revised 11/1/2018 Page 2 of 2 r 1 5 & -1 JjL -�-x. -• _ i'1 i _ !.r � � - - .#. e 1 .• ' +iti"`'' i .ri . .tf'_ A • f G {4�.,f„! �1 �` •r....,,� l `COMP=�i '��Al'! a "t�' r ,,�: - "_, F f • ; , . .�. - •: - i J ' 4j \e' L fY �' .g � .�{ r �.l .. _ ',t _ ` f.A 1. " �S •e.- 'r} �!!''.e� s i � �4�.1" •' 'seta 'k �i �l \-� ! T�'' � I - j •"'' � i f ,r '"Jj• . rJ F' •� ' ' - 'U'I. I ' , `• l i1 r.� xi - ! ~-� `.d L -- r Cj I�» , `'fir '�, r,_,Si•'r1r -,CI: L_ ! _ ' • �r'�. J;'.: „� a -- �' e � '�.. � ?;, - •\ +• s + : - - - �'. `ti mac_ C f'{ ter-' r � • � L �• � � � »1 + ¢' �`} - ; :� _ ., � S _,` ,\ r, � "H i . all $8511�1t �.Qiltf' H` �2iaC111Y�D4 ! ,G f t � � tr'-�.a?�. t ^` ;�' � �' ' � 7�1'. _ � �� :, f .d [ "_ �� - - f ��. r� :'�-"�►' �' � rr . �.. r. �t ��-' �. r -. `! --' :s�: - all • ''`� �.,u _. F,'-Y.� � , #�''" � - '°,t '�- 1. -�(_1 ` J , •' '. .� �� - . L J / n c �e ;Red Rbck•Disposal,. J� � � .... � 3� �� f+4..�5 �r _ � � � � �� '� � �< ' ' .�� A� � � .t . �7 y �y ,,,-�- k � �•-rd- r r - r �, C, - � . .. ` � 1 _ 9r1 r f. y r '-' � ." S,.'f. ♦ . ,y tf. .y `� ,- f L '.'. x:r� ,� '♦-ti f". �, _ , _ _. ___�. J<�r^�n {s � �a�3`�YF, r ,,,� �M' t;r ,y r" �" `n�jL•r' �_ Pf�,rry;,31�{ -L7�c.c Y+. , 3.�=ti - "� •�i' ',. n' - "i` ' r1'.`, � � is i.< _ , y� 'r. �, ,� � •tiL `, � 1 ` , ,.�, - � - - t C.t.' r � t 4 -. ,�°'•. t ., ' ,I Y � >fc < t� t S � + �fi r -.e• � �. ' � i i�ti/OI11PY2� � II, c <•.11 rr !. � ,, �^' t '4 4 1� •, .�.; •� ` 1 �,,f!{� }i Cam.. _ fk='A y-'1 ✓'� j -t ry=_. ' \ :Y 6C -1;r- CSRVMNp: os7 Landfill - COMP -1 �k;\ - \ "u i•4'J �,- f �f `�' elf ,`�• � � `n„; n• � r;,t � - � � �� `t _ • .ij•��>''�.� a ��r'�r � �� o � t � � (� _ t �. C.TAK Y� .•. Stir i tt�� i A` : r. • n ,!` .�+ ' ,x�• e .�•' � � r ��4#�—� � -'� 1� ' �� i �j4 -,.1 e' N r- L `i C = TT s -'14. T j _. � � "r --.'.' . .�? ' �' � - - 'j • �" c . -«s + �{. !ll��, _ iw -•�+ . _ iy X. ..i A f ? � }� I f.`'�[fr F�. % i i jll � % �i �' r ,� � � �'•W �. 1 ti y' .}4 �. t r < �� ' ti"•�4 e r: tLTw7`c,r tXi� 5'.` t� ,-+t,,. a; ICiii19000gIEr. �Goo:gle;_Ear:th r. - F { , < '~ Y `� •,. o' r � ir" . � '.i�A w3 �� n i < .. '..4 - ,.: x. � \ 'r :' a ` � J f � ' � � .� t y-syr f.} _. � �\; .:iy _r r ;- ,a r• - - L. _ a DocuSi n Envelope ID: 38A4C65D-1A67-48DE-9AB7-C18C3BOC9367 aceMalyticale rrnw.pacel�As.tam January 22, 2020 Jesse Li Smith Gardner, Inc. 14 N. Boylan Ave Raleigh, NC 27603 RE: Project: Red Rock 13-1 Pace Project No.: 92460437 Dear Jesse Li: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28075 (704E875.9092 Enclosed are the analytical results for sample(s) received by the laboratory on January 13, 2020. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 7naceAnalyficalo velope ID: 38A4C65D-1A67-48DE-9AB7-C18C3BOC9367 WWW.pacalabs.cam Project: Red Rock 13-1 Pace Project No.:, 92460437 Pace Analytical Services Raleigh 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 - North Carolina Drinking Water Certification #: 37712 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS North Carolina Bioassay Certification #: 16 North Carolina Drinking Water Certification #: 37731 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 VirginiafVELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, LLC 9B00 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L.L.C. Page 2 of 13 DocuSi n Envelope ID: 38A4C65D-1A67-48DE-9AB7-C18C3BOC9367 ceMalXical" www.pacelabs.earn SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Project: Pace Project No.: Red Rock 13-1 92460437 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92460437001 S13-1 SM 254OD-2011 AMI 1 PASI-E SM 9222D-2006 WT 1 PASI-R SM 5220D-2011 JP1 1 PASI-A 92460437002 Comp-1 SM 25400-2011 AMI 1 PASI-E SM 922213-2006 WT 1 PASI-R SM 5220D-2011 JP1 1 PASI-A 92460437003 Comp-2 SM 25400-2011 AMI 1 PASI-E SM 9222D-2006 WT 1 PASI-R SM 52200-2011 JP1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 7En5ceAnalytica velopeID:38A4C65D-1A67-48DE-9AB7-C18C3BOC9367 I ww.pacalahs.cam ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Red Rock 13-1 Pace Project No.: 92460437 Sample: SB•1 Lab ID: 92460437001 Collected; 01/13/20 12:20 Received: 01/13120 13:27 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Total Suspended Solids MBIO 9222D Fecal Coliform RAL Fecal Coliforms 5220D COD Chemical Oxygen Demand Date: 01I2212020 08;53 AM Analytical Method: SM 254OD-2011 102 mg/L 10.0 1 0111612011:18 Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 200 CFU1100 mL 1.0 1 01/13120 15:30 01114/20 14:40 Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 34.7 mg/L , 25.0 1 01/16/20 21:38 01/17/20 05:53 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services. LLC. Page 4 of 13 P 7Envelope ID: 3BA4C65D-1A67-48DE-9AB7-C18C3BOC9367 ceAnalyfical www,oacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 { 7t74 )875-9092 Project: Red Rock 13-1 Pace Project No.: 92460437 Sample: Comp-i Lab ID: 92460437002 Collected: 01/13/20 12:45 Received: 01/13/20 13:27 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 16.4 mg/L 3.2 1 01/16/20 11:18 MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method: 5M 9222D-2006 Fecal Coliforms 400 CFU1100 mL 1.0 1 01/13/20 15:30 01/14/20 14:40 5220D COD Analytical Method; SM 5220D-2011 Preparation Method: SM 5220D-2011 . Chemical Oxygen Demand ND mg1L 25.0 1 01/16120 21:38 01/17/20 05:54 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 01/2212020 08:53 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 DocuSign Envelope ID: 38A4C65D-1A67-48DE-9AB7-C18C3BOC9367 Pace Analytical Services, LLC ceAnalytical a 9800 KinceyAve. Suits 100 Huntersville, NC 28078 www.pscelebs.com (704)875-9092 ANALYTICAL RESULTS Project: Red Rock 13-1 Pace Project No.! 92460437 Sample: Comp-2 Lab ID: 92460437003 Collected: 01113120 12:35 Received: 01/13120 13:27 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 53.0 mg/L 7.9 1 01116/20 11:19 N1113I0 9222D Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms 1480 CFU/100 mL 1.0 1 01/13/20 15:30 01/14/20 14:40 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 43.9 mg/L . 25.0 1 01/16/20 21:38 01/17/20 05:54 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 Y22/2020 08:53 AM without the written consent ai Pace Analytical Services, LLC. Page 6 of 13 7DocuSi n Envelope ID: 3BA4C65D-1A67-48DE-9AB7-C18C3BOC9367 aceAnalytical" www'PlIcelabs.com QUALITY CONTROL DATA Project: Red Rock 13-1 Pace Project No.: 92460437 OC Batch: 519522 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples. 92460437001, 92460437002, 92460437003 METHOD BLANK: 2780369 Matrix: Water Associated Lab Samples: 92460437001, 92460437002, 92450437003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 01/16/20 11:26 LABORATORY CONTROL SAMPLE: 2780370 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2780371 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2780372 Parameter Units Total Suspended Solids mg/L Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 256 102 90-110 92460646001 Dup Result Result 103 128 92460647002 Dup Result Result 776 813 RPD Qualifiers 22 RPD Qualifiers 5 Results presented on this page are In the unite indicated by the "Units" column except where an alternate unit is presented to the fight of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in futl, Date: 01/22/2020 08:53 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 7Envelope ID:"38A4C65D-1A67-48DE-9AB7-Ci8C3BOC9367 ce Analytical www.pscellbs.com QUALITY CONTROL DATA Project: Red Rock 13-1 Pace Project No.: 92460437 QC Batch: 519438 Analysis Method: QC Batch Method: SM 9222D-2006 Analysis Description: Associated Lab Samples: 92460437001, 92460437002, 92460437003 METHOD BLANK: 2779905 Matrix: Water Associated Lab Samples: 92460437001, 92460437002, 92460437003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFUI100 mL ND 1.0 01/14/20 14:40 SAMPLE DUPLICATE: 2779906 Parameter Fecal Coliforms 5M 9222D-2006 9222D Fecal Coliform(MF) - RAL 92460437001 Dup Units Result Result RPD Qualifiers CFUl100 mL 200 180 11 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/22/2020 08:53 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 f DocuSi n Envelope ID: 38A4C65D-1A67.48DE-9AB7-C18C3BOC9367 ceAnalytical www.pacata6s.com QUALITY CONTROL DATA Project: Red Rock 13-1 Pace Project No.: , 92460437 QC Batch: 519818 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92460437001, 92460437002, 92460437003 METHOD BLANK: 2781989 Matrix: Water Associated Lab Samples: 92460437001, 92460437002, 92460437003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg1L ND 25.0 01/17/20 05:42 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hun;ersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2781990 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 755 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2781991 2781992 MS MSD 2627510001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 1420 100 100 1510 1530 91 114 90-110 2 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2781993 2781994 MS MSD 2627495002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone, Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 19900 100 100 19700 19300 -229 -572 90-110 2 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/22/2020 08:53 AM without the written consent or Pace Analytical Services, LLC_ Page 9 of 13 7DocuSi n Envelope ID: 38A4C65D-1A67-48DE-9AB7-C18C3BOC9367 aceAnalytical" ww.pacelabs.com QUALIFIERS Project: Red Rock 13-1 Pace Project No.: 92460437 DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Kiwersvilte, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for. but not detected. Acid preservation may not be appropriate,for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by y EPA Method 8260. N-Nitrosodiphenylamin& decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-E Pace Analytical Services - Eden PASI-R Pace Analytical Services - Raleigh ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. Date: 01/22/2020 08:53 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 13 r DocuSi n Envelope ID: 38A4C65D-1A67-48DE-9AB7-C18C3BOC9367 aceAnalytrcal. wwx.pscdalDs.cam Project: Red Rock 13-1 Pace Project No.: 92460437 Lab ID Sample ID 92460437001 SB-1 92460437002 Comp-1 92460437003 Comp-2 92460437001 SB-1 92460437002 Comp-1 92460437003 Comp-2 92460437001 SB-1 92460437002 Comp-1 92460437003 Comp-2 Date: 01/22/2020 08:53 AM QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch Method QC Batch Analytical Method Analytical Batch SM 2540D-2011 519522 SM 2540D-2011 519522 SM 25400-2011 519522 SM 9222D-2006 519438 SM 9222D-2006 519444 SM 9222D-2006 519438 SM 922213-2006 519444 SM 92220-2006 519438 SM 92220-2006 519444 SM 5220D-2011 519818 SM 5220D-2011 519884 SM 52200-2011 519818 SM 52200-2011 519684 SM 52200-2011 519818 SM 5220D-2011 519884 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except io full, without the written consent of Pace Analytical Services, LLC. Page 11 of 13 CHAIN -OF -CUSTODY Analytical Request Document = = U+B USE'ClNiLY-Milli Wo►ke �0 :92460437 72ceMaiW4l" Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields Company Billing Information .'.^ '"r;- .',' . 1 1 I rt ter ;'f 92460437 SWIS. ar�ne� 1-f1L ALL'SHADE m ; Address 1 1n container-Preservat" T a •• Q N Ave. —fir/ Lak1 Project MaM7ger: Report To:. ail ry(`a: �/l — Preservative t : OF!nitric add, ) sulfuric add. 3 - add, 4 sodium .-' `•l 1 ;� —+ Y u` `•' ` C•' �' ` , (b) methanol, (7J) soo4 um bisulfate, (8) sodium thlomlfatehj9) hexane, lA ascorbic add, Sj ammonium suffate:1e, Copy To: Site Collection Info/Address. (C) ammonium hydro ride,;{D) TSP, (U) Unpresermd, (o) Other Analyses Lab Proflle/Linei _ •' Custoi-nerProject Name/Number: State: County/City: Time Zone Collected:, z.:::: t1sb,6ample xoceipt.Chackl ot: R I-��. l3'I IvL/ �/alC�' t 1PTt IMT( }cr �QET :r; i :r::..�.. y Ctirst�dy Son1� Present /Intaet•Y $ HA. Phone: 6o3 35-33Site/FacilityID#: ' Compliance Monitoring? rs ?'r �Gtizetody. signnturus Present r Y•�gtta: Email: "mod P•O(AL X •Yes t ]No _ ' ; Coll'ectorsigridt+sre 4ir isent' ''41, a WA, �ti��` - � i�`-' ,'•:". 'r-.' 'nBot7tlfea•'Intitct � �: . �.- - : m nA Collected By (print): Purchase Order A: DW PWS ID #: ,, Y I r • r. Ci'ci 'eotiiea'?'� n tut S� ..� j 1 Quote #: DW Location Code::; S e t Vol rr 1cA t_ `-�' '. '''• ,:- Samplotr Received�ott'xae �?t NA. Celli crud B s Imme late Pac d on ce:'' �':,: tur ): Turnaround D e R wired: L rr �� f3 pd c 1 p e- `I;- +•':.'• rI IHna a/teq� �►�y �. voa � each c �+cce tabl F [)(Yes I (No Rus(Ifm Ie Disposal: h: Field Filtered kable): S ;sample° in iioiaing Tiac :®-x tu- t . Renidaei Chlorzne J?rcacnt Y d-!� KOispose as appropriate ( ]Return I ) Same Day [ . ] Next Day ( ]Yes I NO t, f VVV - CI Szrlpb - = 'r [ ] Archlve: ( 12 Day 1 13 Day 114 Day- (.1 S Day amplm. pa acre tab ! ' (Expedite Charges Apply} Analysis: )Hold; stripe Z3e! _ - 1 ' ,�} : -'iSuZflde P>•cssnt 7 tE �,. -r;t- ' Matrix Codes (insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (VAN), i r` ] E =?_' ^Lend 'Acetate strips tT5assay (B). Vapor (V), Other (OT)Prnduct IP). So/Solid (SL1, Oil (QL),Wipe (WP}, Air AR}, Tislue1. Rio }'+' '•.r.'.: -` �•T.AB;1158=Cxt.Y: Comp/ Collected (or Res # of c r,y`- :: • : 'Lnb;scmplaF:�:/ Cwazerit a `' ` ' Customer Sample ID Matrix' Grab' Composite End p ab� Composite CI Ctns .,.:,:� Date Time Date Time C.Citiyl P -Jz Jll v. -r3: ►Z' 3S ��' ' "t' ' 3 ' co NJ-11 Co ear, ;eti 2 _ �Aomer Remarks/ Spe**JJai Conditions/Possible Hazards: Type iif ice lisedr' et' B]ye ,airy`; A.None i + 5}iORT1iOLD5 PRESENT(<72'tioiirs):`; .Y' N'; f!/A Lab'SampleTerriperature,info:' 11 ,' t ; ,+, } , Tern Stank TieceIve4� Y.' N-' NA .. Par king iVlateiSal Used: : i! ;_.• ?; ; LaS'Track[ng ..�� ,is:;��: -.:• .:: :Therm 10.9: t. s -::- Ar ,n � . �Cooler.l Temp. Upon Receipt: S'• f oC.. .s., 1/{. ~ z Sam les received `: = _ �tCooler S T)ierm corr. Factor:- - oC n - I. P--L. P t - _ ty' y" ..-Radrhem'sam Ee-s�streeried(cSOD�cpin}:� =Y� .N;`-•cNA'• '-:2': - ;�" - P r( 1, FEDE](^ UPS c .Clrent oUrier�t Pace Courte'rr ; .'Cooler l'Corrected_Ternp; aC to linqulshed by/Lomparry: (Signature) \ Date/Time: Received by/ ature} Date[nme: MT! LAB USE ONLY t Co_rnmt nEs o llnquished by/Company: (signature) Date/Time: R fired by/Company: (Signature( Dale/'Time: w Prelogm s' HCi McOH TSP Other c linquished by/Company: (Signature) Date>Tme: Received by/Company: (Signature) Date/rime:•- Pf✓i:' _ 'NOnConformance(s)% Page YES: NO of. 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