NCG120056_MONITORING INFO_20190213

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
w
DOC TYPE
❑ HISTORICAL FILE
❑*ONITORING REPORTS
DOC DATE
❑ f'�� �I G� t-� l
YYYYMMDD

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG120000
Date submitted February 7, 2020
CERTIFICATE OF COVERAGE NO. NCG12 0 0 5 B SAMPLE COLLECTION YEAR 2020
FACILITY NAME upper Piedmont Regional Landfill SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
COUNTY Person or *Monthly' January (month
PERSON COLLECTING SAMPLES Chris Gustin DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
LABORATORY ENCO Lab Cert. # 591 RECEIVED ❑Zero -flow ❑Water Supply [_]SA
Comments on sample collection or analysis:
FEB � � 2019 ❑i Other SWS-iv, NSW
CENTRAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Part A: Stormwater Benchmarks and Monitoring Results iJVITR ;i=CiTEQN
❑ No discharge this periodz
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Chemical Oxygen
Demand
mg/L
Fecal Caliform
Colonies per 100 ml
Total Suspended
mg/L Solids
pH,
Standard Units
Benchmarks
_
-
120
1000
100 or 504
6.0-9.0
Parameter Code
-
46529
00340
31616
C0530
00400
002
01/27/20
0.14
110
1000
300
6.8
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfali.
'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -
numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the
detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX".
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-5/31/2021 SWU-248, last revised 11/1/2018
Page 1 of 2

Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period2
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches3
Non -Polar Oil & Grease
mg/L
Total Suspended Solids,
mg/L
New Motor or Hydraulic Oil Usage,
gal/man
Benchmarks
_
-
15
100 or 504
—
Parameter Code
-
46529
00552
C0530
NCOIL
002
01 /27/20
0.14
<2.70
300
>55
Footnotes from Part A also apply to this Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCE€DANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
IR TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES © NO Q
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES © NO F1
REGIONAL OFFICE CONTACT NAME:
Mall an original copy of this DMR, including all "No Discharae" reports, within 30 days of receipt of the lob results (or at end of monitorina Deriod in the
case of "No Discharge" reports] to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons dir tly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete
am awe yFiat�e are 5ignificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
SignaturW of Permittee
Permit Date: 11/l/2018-5/31/2021
7 rr Zy
Date
SWU-248, last revised 11/1/2018
Page 2 of 2

ENICO Laboratories
TiE
Accurate. Timely. Responsive. Innovative.
102-A woodwinds Industrial Court
Cary NC, 27511
Phone: 919.467,3090 FAX: [phone]
Wednesday, February 5, 2020
Republic Services of NC (RE014)
Attn: Christopher Gustin
9650 Oxford Rd
Rougemont, NC 27572
RE: Laboratory Results for
Project Number: Semi -Annual, Project Name/Desc: Upper Piedmont Stormwater
ENCO Workorder(s): CC20359
Dear Christopher Gustin,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Monday, January 27, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable, This report shall not be reproduced except in
tull, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Meghan K Shea
Project Manager
Enclosure(s)
FINAL This wport relates only to Me sample as [Ltieivetl by the laboratory, and may only be reproduced in full. Page 1 of 9

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: Uutrall #2
Lab ID: CC20359-01
Sampled: 01/27/20 09:45
Received: 01/2700 11:29
Parameter Preparation
D iime
Prep Date/Timets]
Analysis Date/T1meW
EPA 1664A EPA 1661A
02/24/20
01/29/20 18:11
01/30/20 15:38
SM 254OD-2011 NO PREP
02/03/20
0112900 08:50
01/29/20 10:12
5M 522OD-2011 Same
02/24/20
01/30/20 10:17
D1130/20 15:20
FINAL This report relates only to the sample as received by me laboratory, and may only be reproduced in full. Page 2 Of g

C
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SAMPLE DETECTION SUMMARY
Client W- outtall #2 Lab ID: CC20359-01
Analvtg liesulks Flag mDL E24 Units Method N
cheuulcai Oxygen Demand
-lotal Suspended Solids
]l0
300
mg1L SM 522OD-2011
mg/L SM 254OD-2011
HNAI. i ['is repurt relates unly to the sample as rLterved by the Wboratory, and may only be reproduced in full. I Page 3 OF S

CSNLe9
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ANALYTICAL RESULTS
Description, Outfall #2 Lab Sample ID:CC2035MI Received: 01/27/20 11:29
Matrix: Surface Water Sampled:01/27/20 09:45 Work order: CC20359
Project: Upper Piedmont Stormwater Sampled BV:Client
Classical Chemistry Parameters
^ - ENCG Cary —fled aaalyfe [MC 5911
AnaMe rW Number] Results aas
Units
pE
LHDL
ML
Batch
L`lC had
Analyzed
01 ri4tes
Chemical Oxygen Demand, 110
mg/L
1
10
10
OA30017
SM 522OD-2011
01/30/20 15:20
.10C
Total Suspended Solids^ 300
mg/L
10
25
Z5
OA290O7
SM 254OD-2011
01129/20 10:12
ZGW
Classical Chemistry Parameters
Anal NumberNumberl Resul flaq
Units
PE
MOL
M
Datch
Method
Anahged
Oy Notes
Oil & Grease (HEM-SGT) Non -Polar Material 2.70 U
mg/l,
1
2.70
5.00
OA29017
EPA 1664A
01/30/20 15:38
SMA
FINAL This report relates only to the sample as rea eived by the laboratory, and may only be reproduced In full I page 4 0f g

011-
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OA29007 - NO PREP
Blank (OA29007-51-91)
Prepared: 01/29/2020 08:50 Analyzed: 01/29/2020 10:12
Spike Source %REC
RPD
Andivte
Result
Flag
POL
Units
Level Result %REC Limits RPO
Limit
Notes
Total Suspel loed Solids
2.5
U
2.5
mg/L
LCS (OA29007-BSl)
Prepared: 01/29/2020 08:50 Analyzed: 01/29/2020 10:12
Spike Source %REC
RPD
Ar WAC
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
'lutal Suspended Solids
95
2.5
mg/L.
100 95 80-120
Duplicate (OA29007-13UPl)
Prepared: 01/29/2020 08:50 Analyzed: 01/29/2020 10:12
Source., CC21933-01
Spike Source 0/uREC
RPO
Andlyte
Result
Flag
POL
Units
Level Result %REC Limits RPD
Limit
Notes
7alal Suspended Sulids
260
25
mg/L
170 41
20
QM-12
Duplicate (OA29007-DUP2)
Prepared: 01/29/2020 08:50 Analyzed: 01/29/2020 10:12
Source. MOS53-01
Spike Source %REC
RPD
AndI
Result
Flag
P01,
Units
Level Result %REC Limi RPD
Limit
Notes
Total Suspended Solids
2200
250
mg/L
2400 12
20
Batch OA30017 - Same
Blank (OA30017-BLI(l)
Prepared: 01130/2D20 10:17 Analyzed: 01/30/202D 15:20
Spike Source %REC
RPD
Andlvtic
Result
EII
POL
Units
Level get %REC Limits RPD
Limit
tjiltes
Chemical Oxygen Demand
10
LI
10
mg/1-
LCS (OA30017-eSIL)
Prepared: 01/30/2020 10:17 Analyzed: 01/30/2020 15:20
Spike Source %REC
RPD
Atwlyte
Result
Flag
POL
Units
Level Result %REC Limit RPD
Limi
Notes
Chemical Oxygen Demand
500
10
mg/L
500 100 90-110
Matrix. Spike (OA30017-M51)
Prepared: 01/30/2020 10:17 Analyzed: 01/30/2020 15:20
Source: CC20359-01
Spike Source %REC
RPD
A1lalvte
Result
Flag
POI.
Units
Level Result %REC Limits RPD
Limi
Notes
Cheeical Oxygen Demand
660
10
mg/L
526 110 105 90-110
Matrix Spike Dup (OA30017-MSD1)
Prepaeed: 0113012020 M 17 Analyzed: 01/30/2020 15:20
Source:CC20359-01
Spike Source °JoREC
RPD
Analvtn
Result
Flag
POL
units
Level Result %REC Umit5 RPO
Limit
Notes
Chemical Oxygen Demand
650
10
mg/L
526 110 102 90-110 3
5
Classical Chemistry Parameters - Quality Control
Batch OA29O17 - EPA 1664E
Blank (OA29017-BLk1)
Prepared: 01/29/2020 18:11 Analyzed: 01/30/2020 15:38
Spike Source %REC
RPD
A11d]vte
Result
Flag
POL
Units
Level Result %REC Limits RPO
Limil
Notes
Oil lk Gieuse (l1F.M-SGT) Non -Polar Material
2.70
U
5.00
M91L
FINAI, -I his cpurl i elates only to the sample as eeceived by the laboratory, end may only be reproduced In lull. I Page 5 o I 9

Ce i Sk I E__ 9)
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch OA20017 - EPA 16648 - Continued
LCS (OA29017-13SI) Prepared: 01/29/2020 18:11 Analyzed: 01/30/2020 15:38
Spike Source %REC RPD
.Analvte Result Flaq POL Units Level Result °/aREC Limits RPD Unitt Notes
Oil & Grease (HEM-SGT) Non -Polar Material 66.0 5.00 mg/L 80.0 82 64-132
LCS Dup (OA29017-BSDI) Prepared: 01/29/2020 18:11 Analyzed: 01/30/2020 15:38
Spike
Source
%REC
RPD
.&WIft
Result FJa_q
PQL
Unite
Level
fe5q °hREC
Lim] RPb
Limit Notes
Oil & Grease (HEM-SGT) Non -Polar Material
80.3
5.00
mg/L
82.0
98
64-132 70
34
Matrix Spike (OA29017-MSI)
Prepared: i l/29120Z0 t8:11 Analyzed: 01/30/2020 15:36
Source: CC203S9-01
Spike
Source
%REC
RPD
Analyte
Result Flan
POL
Units
Level
13wlL %REC
limits RPD
Limit Notes
Oil & Grease (HEM-SG1) Non -Polar Material
78.9
5.00
mg/L
75.5
2.70 U 104
64-132
FINAL This report relates only to the sample as received by the laboratory, and may only, be reproduced In full. I Page 6 et

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
] The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U l he analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate,
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 250% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QM-12 Precision between duplicate samples was outside acceptance limits.
HNAI I I115 I KIUII reldl U] 611]y to IhU sanll>le - I clwd l y the laWl logy, and may only b' reproduced In lull. Page 7 oE71

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ClreR'. r:am!
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Reauestad
Anetvse$
Pequeslel7 f ui narou
Republic Services of NC (RE014)
Semi Annual
TimesOD
1
SOures�.
9650 O� Rd
Io;9 :S t:rif:l��esC
� o Upper Piedmont Stomwater
#
IF
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Noi4 Rust. reaue5Ll sJtie�
amea:art�i- 0�' Irx- !acim I U
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SD 1 Bill= In;,
Rougemant, NC 27572
2018:
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Staiidard
Expedited
Due I I
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(336) 354-360
-rely rrnq ion47c:
Chrisbpher Gusfin
SamyrtrlFl New Adhiial*a (P.Iij
J 8iirny Contact
Christopher Gus6n
°
—co
•¢
LL
°
rn
~
Sasnalcrlst S:pnatu _
Sw: Lacal*n 1Time Zorn
Lab Workorder
CC20359
PM%e:vetion
{Set
CDdes)
(:�antvine
as nucussaryl
liom r
SamplF F) (rrold loe:llllicawn)
Gollect:{!r, Oale
CCBieclro^
'U.IF.
Gam,- ! Gratr
Malm
(S-e wo9S)
T=l € of
(lpn!amem
I
Sampie Comments
O=,n'- L-
5W
5
X X , X
X
<-- Total S of Cantainers
;,;�v t pmnarea $y DaIsITSmB
Ael:npui ^ BY
Oater/ilmL
Recerveo 95' as/l/e'Trr:lt'
Corsrl . tsrSPedal Reporting Raquiremertts
Ralinpu,. till y
Date Tani
RateFly D11197tsrn
RelinquLshed By
OaleTimeI
Rec ivad y j Oa:eTlms
pal¢r l', & Tema on Re.e'.pt �
�. L
r
ConStion on Aaceipl
Acceptable Unacceptable
lJi L2Tti: GV!-Graunr!»'a:8r SO-SOO 6W-Omtking LVa!er SE -Sediment SW-Surla Cs Waw IVIM-Wass ater A-44 O•pthg: (ygaP kr co:nme:ns) Presarvellon: I•Ice H+0 N-1it3O3 S.H?SOd NO-14&QH 0-0Iher Idelail in t mmenls)
Note: All ram Aes su7mitted la ENGO Lee* are in aocwaanct u'!dl the term and cendows listed m irte reverse 0 iris lursn, unless prio: %Tilton aQmaments exist

Sample Preservation Verification
ENCO Cary
r
Work Order: CC20359 Project: Upper Piedmont Stormwater
r lierii: Republic Services of NC {RE0,14) Project #: Semi -Annual
Logged In: 27-Jan-20 11.59 Logged By: John C King I j
Preservation Check Performed By: '� Date/Time:
CC20359-01
;
Cont.
Type 'F
w!i'res•(pH); '
Requirement.'
pH.Checked!
In;Eontrol
Date/Time.w,.
pMAdjusted .A`djusietl'
frfiaRent UsedlCa'rziments .;r,.'
B
250mLA+l•12SO4
<2
Y i N I NA-
Y i N! �V
C
250ml-Ai+12SO4
<2
Y I N 1 C44
Y! N I
D
250ml-P,M2504
<2
,! N 1 NA
Y I N i NA
Ras enr Name ID Rea ent Narne ID Reactent Name ID
1 3 5
4 6
I}I.1 Stfip 1D
Page 9 of 9
C.1LI.MNT1Printlwko—PreservationCheck.rpt 1

laneAnalyfical""
ww vscdlabz.cera
January 29, 2020
Meghan Shea
ENCO Labs
102 A-Woodswinds Industrial Co
Cary, NC 27511
RE: Project: CC20359
Pace Project No.: 92462364
Pace Analytical Services, LLC
9000 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Meghan Shea:
Enclosed are the analytical results for sample(s) received by the laboratory on January 27, 2020.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please f eel free to contact me.
Sincerely,
Sarah Graham
[e-mail]
[phone]
Project Manager
Enclosures
cc: Chuck Smith, ENCO Labs
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 10

Pace Analytical Servlres, LLC
aceAnalytical 9800 KinceyAve. Suite00
Huntersvllle, NC 7.8078
www.Pscdabs.corn
{704 j875-9097.
CERTIFICATIONS
Project: CC20359
Pace Project No.: 92462364
Pace Analytical Services Raleigh
6701 Conference Drive, Raleigh, NC 27607 North Carolina Bioassay Certification #: 16
North Carolina Wastewater Certificafion #: 67 North Carolina Drinking Water Certification #: 37731
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. LLC. Page 2 of 10

w
aceAnalytical
www.pacelabs.com
Project: CC20359
Pace Project No.: 92462364
Lab 10 Sample 1D
92462364001 Outtall #2
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)87 59092
SAMPLE ANALYTE COUNT
Analytes
Method Analysts Reported Laboratory
SM 9222Q-2006 WT 1 PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not tre reproduced, except in Tull,
without the written consent 01 Pace Analytical Services, LLC. Page 3 of 10

laneAnapical"
WWW.pacelahs.cota
ANALYTICAL RESULTS
Pace Analytical Services, LLG
9500 i(incey Ave. Suite 100
Fluntersvilfe, NG 28078
[phone]
Project: CC20359
Pace Project No.: 92462364
Sample: Outfall 02 Lab ID: 92462364001 Collected: 01/27/20 09:45 Received: 01/27/20 12:34 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
Fecal Coliforms 1000 CFU1100 mL 1.0 1 01/28/20 13:05 01/29/20 11:30
Date: 01/29/2020 04:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 4 of 10

laceAnalXica(
www.poestabs.com
Project CC20359
Pace Project No.: 92462364
QC Balch: 522056
QC Balch Method. SM 9222D-2006
Associated Lab Samples: 92462364001
METHOD BLANK: 2792518
Associated Lab Samples: 92462364001
Parameter Units
Fecal Colitorms CFU1100 mL
SAMPLE DUPLICATE: 2792519
Parameter
Fecal Colitorms
QUALITY CONTROL DATA
Analysis Method: SM 9222D-2006
Analysis Description. 9222D Fecal Coliform(MF) - RAL
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 01/29/2011730
92462364001 Dup
units Result Result RPD Qualifiers
CFUI100 mL 1000 1400 33
Pace Analytical Services, LLC
9800 Kincey Ave. Suite too
Huntersvitle, NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented bathe right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 01/2912020 04:03 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 10

aceAnalXical
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QUALIFIERS
Project: CC20359
Pace Project No.: 92462364
DEFINITIONS
OF - Dilution Factor. if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit,
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(71)4)8759092
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicale)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNl -The NELAC Institute.
LABORATORIES
PASI-R Pace Analytical Services - Raleigh
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date'. 01 /29/2020 04'.03 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 10

a�
ace Analytical
www,pacalahs.tam
i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: CC20359
Pace Project No.: 92462364
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92462364001 Outfall #2 SM 9222D-2006 522056 SM 92220-2006 522057
Dale: 01/29/2020 04:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 10

Document Name: •
Document Revised: February 7, 2018
�r,, h,f
Sample Condition Upon Rece( t(SCUR]
Page 1 of 2
Document No,:
€ssuingAuthority:
r C8R1)a%f1C81'
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville❑ Raleigh® Mechanicsville[]
• Olent*Name: WO# : 92462364
OMWWG w — LJ .,6, Project Al:
Courier: ❑Fed Ex ❑UPS ❑uSPS &Client
❑ Commercial []Pace ❑Other: 92462364
Custody Seal Present? []Yes KNo Seals Intact? []Yes [SNo ,r ``1
Date(In dais Parson Examining Contents: Zry`>1 f ' t -
Packing Material:. ❑Bubble wrap • ❑Bubble Bags ' KNone ❑ Other alologlcal Tissue Fromn?
Thermometer: /] ❑Yes ❑No ®N/A
❑IR Gun In:
i o0� TYPeoflce: ®We[ ❑slue. []None
Cooler Temp f%): / 0 Correction Factor: Add/Subtract ('C) Q. U
- Temp should be above freezing to 6'C
Cooler Temp Corrected ('t]: ❑Samples out of temp criteria. Samples on Ice, coaling process
has begun
USDA Regulated Sail (K N/A, water sample)
Old samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)7 old samples originate iron, a foreign source limernationaily,
❑Yes nNo Includlna Hawaii and Puerto RIrol7 nYes nwo
Comments /D is cr e p a n cy:
Chain of Custody Present?
Yes
❑Ne
QNJA
1,
Sam tes Arrived within told Time?
®Yes
No
[]NIA
2.
Short Hold Time Analysts <72 hr.)?
e5
Na
❑NIA
9.
Rush Turn Around Tlme Requested?
[]res.
No
[]N/A
A. Y
Sufficient Volume?
es
Na
NIA
S.
Correct Contalners Used?
-Pace Containers Used?
]Yes
es
❑No
Nn
[]NIA
QNIA
6.
Containers Intact?
Yrs
QNo
NIA
7.
Dissolved analysis; Samples Field Filtered?
Yes
QNo
ZJNJA
a,
Sample Labels Match CDC?
-includes Date/Time/ID/Analysts Matrix:
j&Yes
J
[]No
❑NIA
_
e.
µ
Headspace In VOA Vials (>S-6mm)7
OYes
ONO
ONIA
1D.'
Trip Blank Present? -
TTIp Blank Custody Seals Present? _ _
❑Yes
❑Yes
[]No KNIA
014o &A
11.
CUM` ME�N}TS/SAMPLE MSCREPANCY Field Data Required? []Yes ❑No
�41(i."O'1
t
{ r
Irv, l i' � I'I R Lot'IDofspiit wntafners: I r ii. C ��, � 1 -.•
Person contacted: �ri�l<' "r', '� !Y 1 Date/Time; r' ! " , Fo j:� , X( )
Project Manager SCURF Review: �t % Date:
Project Manager SRF Review: rj Date:
Page S of 10

DOCUfttent Name:
Docurnent Revised: February 7, 2018
Pace,�ialytic�fl '
Sample Condltton U on Recei t SCURj
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR•CS•033-Rev.U6
PaceCaroljnas 4ualityOffice
¢Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Ekceptluns: VUA, Collfarm, TOC, Oil and Grease, DRO/8015 (water) DOC, 1-1-Hg
"Bottom half of box is to list number of bottle
Project# WO# : 92462364
PM: SMS Due Date: 02/05/20
CLIENT: 92-ENCO
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pH Adjustment Log for Preserved Samples
Sample 10
Type of Preservative
pH upon recelpt
Date preservation adjusted
Tlmepresetvation
adjusted
Amount of Preservative
added
Lot
Note: Whenever there is a discrepancyafferting North Carolina compliance samples, a copy of this fG6r11 will be sent to the IJonh Carollna DEIINR Certlllcatlun Office (Le.
Out of hold, blurred pteservjtive, out of temp, incorrnct contalners.
Page 9 of 10

SUIICONTRACT ORDE11
ENCO Cary
CC20359
SENDING LABORNFOR'Y: It MEATINGJ..ABORAIQRY;
ENCO Cary Pace Analytical (Raleigh NC)
102-A Woodwinds Industrial Comt 4915 Waters Edge Dr 9120
Cary, NC 27511 Raleigh, NC 27606
Phone: [phone] Phone :[phone]
Fax: [phone] Fax:
Project Manager: Stephanie rrauz Project State of Origin: North Carolina
Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Commenta
Outfall #2 Surfacc Water 17-Jan-20 (19:45 I I i .I,I
Coliform, Fecal 92238 05-reb-20 15:00 27-Jar,-20 17:40
Containers Supplied:
Stchlc250mL1' i•Nal'liio (F)
=z72�
)^ L7-2-0) 12 ' 3r
Released By Date Received By Date
Page Vs edloof 10