NCG100126_MONITORING INFO_20141212

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/V I o L) 1
DOC TYPE
❑HISTORICAL FILE
MONITORING REPORTS
DOC DATE
❑ �bf� �� � a
YYYYMMDD

CERTIFICATE OF COVERAGE NO. NCG100126
STORMWATER DISCHARGE OUTFALL (SDO)
y y MONITORING REPORT
®
ERE V ED
DEC 12 2014
CENTRAL FILES
DWR SECTION
FACILITY NAME Johnston Auto Salvage _
PERSON COLLECTING SAMPLE(S) Alex Ahmady
CERTIFIED LABORATORY(S) Pace Analytical Lab # 12
Lab#
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLES COLLECTED DURING CALENDAR YEAR: 2014
(This monitoring report shall be received by the Division no later than 30 days
from the date the facility receives the sampling results from the laboratory.)
COUNTY Nash
PHONE NO. [phone]
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow" or "No Discharge" within
30 days of the end of that period to comply with permit reporting requirements.
Outfali
No.
Date
Sample Collected,
mo/dd/year
Total
Rainfall,
inches
00400
00530
- - - -
77023
01051
78141
pH,
Standard
Units
Total Suspended
Solids (TSS),
mg/L
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), mg/L
Ethylene Glycol,
mg/L
Lead, Total
Recoverable,
mg/L
Total Toxic
Organics3,
mg/L
Benchmark
-
-
6.0 — 9.01
100/502
15
8,000
(Tiers 2 and 3)
0.03
1.0
Outfall001
09/24/14
D
5.8
111
<5.0
<10.0
<0.0050
NA
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General
Permit.
1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation pH levels are lower, then the lower threshold of this benchmark
range is the pH of the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented
to demonstrate background concentrations were below the benchmark pH range of 6-9.
2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters.
Form SWU-251, last revised October25, 2012
Page 1 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122.
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent
management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the
discharger shall sign the following certification statement:
Solvent Management Plan Certification Statement
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I
certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent
management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
Signature
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service
Center
Raleigh, North Carolina 27699-1617
Date
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee or Designee)
(Date)
Form SW U-251, lost revised October 25, 2012
Page 2 of 2

, y
e
aceAnalytical
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i
October 06, 2014
Darin McClure
Mid Atlantic Associates, Inc.
RE: Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92218775
Dear Darin McClure:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on September 25, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Y
Jon D Bradley
[e-mail]
Project Manager
Enclosures
cc: Joanna Crow, Mid Atlantic Associates, Inc.
Chuck Hoffman, Mid Atlantic Associates
Beverly Oglesby, Mid Atlantic Associates, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in futl,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 13

Ice Analytical
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Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92218775
Indiana Certification IDS
7726 Moller Road, Indianapolis, IN 46266
Illinois Certification #: 200074
Indiana Certification #: C-49-06
Kansas Certification #: E-10247
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification M 37712
CERTIFICATIONS
Kentucky UST Certification #: 0042
Louisiana/NELAP Certification* 04076
Ohio VAP Certification #: CL-0065
West Virginia Certification #: 330
FloridalNELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiafVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc- Page 2 of 13

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SAMPLE ANALYTE COUNT
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92218775
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytts
Reported
Laboratory
92218776001 OUTFALL NO. 1 EPA 1664B
CLV11
1
PASI-C
EPA 8015 - Aicohol-Glycol
DMT
1
PASI-1
EPA6010
SH1
1
PASI-A
SM 2540D
TEP
1
PASI-A
EPA 9040
MAB
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc- Page 3 of 13

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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92218775
Sample: OUTFALL NO. 1 I-ab ID; 92218775001 Collected: 09/24/14 00:00 Received: 09/25/14 09:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 09/26/14 08:52
8015M Glycols in water Analytical Method: EPA 8015 - Alcohol -Glycol
Ethylene glycol ND mg/L 10.0 1 10/05/14 17:18 107-21-1
6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA 3010
Lead ND ug1L 5.0 1 09/26/14 16:50 09/29/14 20:20 7439.92-1
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 111 mg1L 16.7 1 09/26/14 03:34
9040 pH Analytical Method: EPA 9040
pH 5.8 Std. Units 0.10 1 09/27114 00:48 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/06/2014 04:49 PM without the written consent of Pace Analyticat Services, Inc.. Page 4 of 13

11�;a'ce A nalyticaI
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QUALITY CONTROL DATA
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92218775
QC Batch: GCSV119020 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92218775001
METHOD BLANK: 1293979
Associated Lab Samples: 92218775001
Parameter Units
Oil and Grease mg1L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 09/26/14 08:44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1293980
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg1L
40 34.3
86
78-114
MATRIX SPIKE SAMPLE:
1293981
92218775001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mglL
NO 40
37.7
94
78-114
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/06/2014 04:49 PM without the wntten consent of Pace Analytical Services, Inc.. Page 5 of 13

Ice Analytical
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QUALITY CONTROL DATA
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92218775
QC Batch: GCSVI13244 Analysis Method: EPA 8015 - Alcohol -Glycol
QC Batch Method: EPA 8015 - Alcohol -Glycol Analysis Description: EPA 8015 Modified
Associated Lab Samples: 92218775001
METHOD BLANK: 1168208
Associated Lab Samples:
Parameter Units
Ethylene glycol mg1L
LABORATORY CONTROL SAMPLE: 1168209
Parameter Units
Ethylene glycol mg1L
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersvilre, NC 28078
[phone]
Matrix: water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10.0 10105/1416:25
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
250 233 93 79-129
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1168210 1168211
MS MSD
92218775001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Ethylene glycol mg1L ND 250 250 220 222 87 88 67-133 1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/06/2014 04:49 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 13

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QUALITY CONTROL DATA
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92218775
QC Batch: MPRP116992 Analysis Method: EPA 6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET
Associated Lab Samples: 92218775001
METHOD BLANK: 1294728
Associated Lab Samples: 92218775001
Parameter Units
Lead ug/L
LABORATORY CONTROL SAMPLE: 1294729
Parameter Units
Lead ug1L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 5.0 09/29/14 20:11
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
500 520 104 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1294730 1294731
MS MSD
92218956006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 500 499 513 100 103 75-125 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1294732 1294733
MS MSD
9221895600E Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual
Lead ug1L ND 500 500 492 508 98 102 75-125 3
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/06/2014 04:49 PM without the written consent of Pace Analytical Services, Inc..
Page 7of13

aceAnalytrcalm
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92218775
QC Batch: WETI33394 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92218775001
METHOD BLANK: 1293964
Associated Lab Samples: 92218775001
Parameter Units
Total Suspended Solids mg1L
LABORATORY CONTROL SAMPLE: 1293965
Parameter Units
Total Suspended Solids mg1L
SAMPLE DUPLICATE: 1293966
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 1293967
Parameter
Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 09126/14 03:26
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 248 99 90-110
92218938001 Dup
Units Result Result RPD Qualifiers
mg1L 760 700 8
92218733001 Dup
Units Result Result RPD Qualifiers
mg/L ND ND
Results presented on this page are In the units Indicated by the "Units" column except where an allemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/06/2014 04:49 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 13

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Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92218775
QC Batch: WET133409
QC Batch Method: EPA 9040
Associated Lab Samples: 92218775001
SAMPLE DUPLICATE: 1294272
Parameter Units
Std. Units
pH
QUALITY CONTROL DATA
Analysis Method: EPA 9040
Analysis Description: 9040 pH
92218344002 Dup
Result Result RPD
7.6 7.6
Qualifiers
0 H6
Pace Analytical Services, Inc.
9B00 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
0
Results presented on this page are in the units Indicated by the "Units" colurnn except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/06/2014 04:49 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 13

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QUALIFIERS
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92218775
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute,
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-I Pace Analytical Services - Indianapolis
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 10/06/2014 04:49 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 13

/�aceAnalyficaI
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r
i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: JOHNSTON AUTO SALVAGE
Pace Project No.: 92218775
Lab ID
Sample ID
QC Batch Method
92218776001
OUTFALL NO. 1
EPA 1664B
92218775001
OUTFALL NO. 1
EPA 8015 - Alcohol -Glycol
92218775001
OUTFALL NO. 1
EPA 3010
92218775001
OUTFALL NO. 1
SM 2540D
92218775001
OUTFALL NO. 1
EPA 9040
Date: 10/06/2014 04:49 PM
Pace Analytical Services, Inc.
9800 Kiacey Ave. Suitet00
Huntersville, NC 28078
[phone]
QC Batch Analytical Method
GCSVI19020
GCSVI13244
MPRP116992 EPA 6010
WET133394
WET133409
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
CP115326
Page 11 of 13

//9-'Iv170eArk7lytr'0l"
i
Sample a Condition Upon R�eceil
[document Number:
F-C R R-C S-003-re v.15
Page 1 of 2
issuing Authority:
Pace Huntersville Qualiq
Client Name: ssac_
Courier: Zed E ❑ UPS❑ uspS❑ Client❑ CommercialEl Pace Other
Custody Seal on CoolerlBox Present: ❑ yes l� no Seals intact: ❑ yes ❑ noVol
� ��,"�e r ` '�
Packing Material: [�bble V� ❑ Bubble Bags ❑ None ❑ Other �/
Thermometer Used: 94 IR Gun 0 Type of Ice: We Blue None I� Samples on ice, cooling process has begun
Temp Correction Factor T1401 No Correction
Corrected Cooter'rem C
p -- --
Biological Tissue is Frozen: Yes No
Date and Initials of person examining
contents:
Temp should t•e abolre freezing to 6°C
Comments:
Chain of CustodyF'resen,.:
Ekfes ©NO
❑NrA
1.
Chain of Custody Filled Out:
ClYes C14.
❑NIA
2.
P0 ck-;e- /4-Nn1-s
Chain of CuAody Relln wished:
C3Yes (p�o
❑NrA
3.
Sampler Name & Signature on COC.
Gres ❑No
❑NIA
4.
Samples Arrived within Hold Time: 9jZC--Cyes ❑No
❑NrA
5.
Short Hold Time Analysis (<72hr):
[�res ❑No
❑NIA
6.
Rush Turn Around Time Requested:
Dyes ON
❑NIA
7.
Sufficient Volume:
❑��YYe�es Clio
❑N1A
8.
'f-�o loof(l IV�
Correct Containers Used:
L as ❑No
• ❑NIA
g,
-Pace Containers Used:
B es ONO
❑NIA
Containers Intact:
Yes ❑No
❑NIA
10.
Filtered volume re,;ei red for Dissolved tests
©Yes ❑No
21NIA
11,
_
Sample Labels matcl, COC:
❑Yes too
❑NrA
12.
011A cL �' ° S o tom` l
-Includes date;timellDlAnalysis Matrix:_
3 o� S I y �u J; c, f s h
All contalners needing preservation have beer. checked.
2/
Yes ❑No
nN1A
13.
n
J)
All containers needing preservation are found to be in
Oyes ONO
❑NIA
compliance with EPA recommendation.
��/�
❑No
exceptions: VOA, coliform, TOC, 08G, W-Cf30 (%vater)
L'IYes
Samples chocked for dechlorination:
Oyes ❑No
3 A
14.
Headspace in VOA Vials ( >6mm):
❑Yes ©No
❑NIA
15,
Trip Blank Present:
❑yes ❑rio5'IA
16.
_
Trip Blank Custody Seals Present
❑Yes ONO
9' IA
Pace Trip Blank Lot # (if purchased):
Client Notification! Resolution: Fietd Data Required? Y 1 N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Re'riew.�Date: `t 'Z'> (L�r;?V+rnl
SReview �s� Date: RF
IlklJt� �.
14t,
Note: Whenever there is a discrepancy affecting North Carolina comp,iance i
Samples, a co of this form will be sent to the North Carolina DEHNR 922i8773 :
p p5'
Certification Office ( i.e out of hold, incorrect preservative, out of temp,
incorrect containers)
Page 12 of 13

ace Analytical
Section A
Required Client Information:
CHAIN -OE -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section 8 section C
Required Project Intormation: invoice Information:
a
Page: of
Company: Mid -Atlantic Associates. Inc.
Repot To: Chuck Hoffman ([e-mail])
Attention: Chuck Hoffman
Address: 409 Rogers View Court
Copy To- Joanna Craw (jcrovin maacinline.corn)
Company Name: Mid -Atlantic Associates, inc.
REGULATORY AGENCY
Raleigh, NC 27610
Address: 409 Rogers View Court, Raleigh, NC
I- NPOES r- GROUND WATER F DRiNKING WATER
r UST F- RCRA r OTHER
Email To: [e-mail] Purchase
order No: R2575.00
Pau chicle -
Relerence:
Pie 9t9-25D-9918
Fare 919-250-9950 Project
Name: Johnston Auto Salvage
Pace Prgen Kevin Herring
site Location
Manager.
_
STATE.
NC
Requested Due OaterrAT; Standard Project
Number: R2575,00
Pace Pm01e 0 -_
Requested
Analysis
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(%( N)
Section 0 Valid Matrix Codes
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Preservatives
3-N
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AJ30MONAL COMMENTS
RELINQUISHED BY ! AFFILIATION
DATE
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SAMPLER NAME AND SIGNATURE
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-lmpenamt Nc1e. ey slgnag des Um you are ectaoling Pace'& NET 30 day part a terms and agreevrg le lair Uwrges at 1.5% Per moth for any Invoices rat paid wahin 30 days. F-ALL-Q-020reV.08, 12-Oct-2007