NCG080770_MONITORING INFO_20140501

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
IVC& b�b-7 � u
DOC TYPE
❑HISTORICAL FILE
C�MONITORING REPORTS
DOC DATE
❑
YYYYMMDD

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCG080000 SAMPLES COLLECTED DURING CALENDAR YEAR:
CERTIFICATE OF COVERAGE NO. NCG08 0770 _ (This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sam ling results from the laboratory.)
FACILITY NMN'IE opt/ L.1 COUNTY /%&ge Q. 51,1a (4029 } ,
PERSON COLLECTING SAMPLES fo PHONE NO. (R%Y/) S96 ZZZ^� t
CERTIFIED LABORATORY L_ Lab # 1 QFq_god J
Lab # PLEASE SIGN ON THE RI'VERSE
Part A; Vehicle Maintenance Areas Monitoring Requirements
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? —yes
(if yes. report your analytical results in the table immediately below)
Outfall
No.
Date
Sample Collected,
mo/dd/ r
00530
00400
00556
Total Suspended Solids,
m
pH,
Standard units
Oil and Grease,
mgfL
New Motor Oil Usage,
Annual average al/mo
Benchmark
100 -
Within 6.0 — 9.0
30
!?m !
/
o "s x©
1 X"%a V
201
Note: if you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier �pr�7:Ic,r,2 V gpp�Ec
See General Pernut text. DWQJBOG
Part Ii: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals
Outrall
No.
Date
Sample Collected,
mo/dd/ r
00556
00530
00400
Oil and Grease,
m g
Total Suspended Solids,
m /L
pH,
Standard units
Permit Limit
-
30
100
6.0 — 9.0
STORM EVENT CHARACTERISTICS:
Date � %S ; (first event sampled)
Total Eve t Precipitation (inches): 2—
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attu: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
SWU-250-102 J O7
Pa-c i „7 2

"I certify, under penalty of law, that this document and all attachments were prepared under nay direction or
supervision in accordance with. a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
ao�L
(Signature of Perk, ttee) ( ate)
S W U-750-102107
Page I- (); I

/IceAnalyfical"
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April 25, 2014
Mr. Bob Newman
Horizon Coach Lines
1251 W, Craighead Rd.
Charlotte, NC 28206
RE: Project: OUTFALL
Pace Project No.: 92197611
Dear Mr. Newman:
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, 128078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on April 16, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Vu i o t r( {
Angela Baioni for
Laura J Cooper
[e-mail]
Project Manager
Enclosures
A�CRfO/
�r
TNI;
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, Inc..
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Project: OUTFALL
Pace Project No.: 92197611
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analydcal Servicos, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(7 04 )875-9092
Page 2 of 11

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SAMPLE ANALYTE COUNT
Project: OUTFALL
Pace Project No.: 92197611
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID Sample ID Method
Analysts
Reported
Laboratory
92197611001 OUTFALL #1 EPA 1664E
CLW
1
PASI-C
SM 2540D
1
WRC
1
PASI-A
EPA9040
I
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: OUTFALL
Pace Project No.: 92197611
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvilte, NC 28078
[phone]
Sample: OUTFALL #1
Parameters
Lab I0: 92197611001 Collected: 04/15/14 15:30
Results Units Report Limit DF
Received: 04/16114 10:43 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg/L
5.0 1
04/17/14 11:31
2540D Total Suspended Solids
Analytical Method: SM 2540D
I
Total Suspended Solids
25.4 mg/L
5.0 1
04F22/14 20:48
9040 pH
Analytical Method: EPA 9040
pH
6.5 Sid. Units
0,10 1
0408114 13:30 H6
Date: 04/25/2014 09:48 AM
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
without the written consent of Pace Analytical Services, Ina.
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QUALITY CONTROL DATA
Project: OUTFALL
Pace Project No.: 92197611
OC Batch: GCSV117282 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92197611001
METHOD BLANK: 1180267
Associated Lab Samples: 92197611001
Parameter Units
Oil and Grease mg/L
LABORATORY CONTROL SAMPLE: 1180268
Parameter Units
Oil and Grease mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 04/17/1411:25 1
Spike LCS
Corc. Result
40 38.5
Pace Anatytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
LCS % Rec
R e c Limits Qualifiers
96 78-114
MATRIX SPIKE SAMPLE: 1180269
92197663004 Spike MS MS %Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Gil and Grease mg/L NO 40 38.8 j 93 78-114
Date: 04/25/2014 09:48 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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QUALITY CONTROL DATA
Project: OUTFALL
Pace Project No.: 92197611
QC Batch: WET13O655 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92197611001
METHOD BLANK: 1183321
Associated Lab Samples: 92197611001
Parameter Units
Total Suspended Solids mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
N❑ 2.5 04/22/14 20'A4
Pace Anatytical Sary IC85, tnC.
9800 Kincey Ave. Suite 100
huntersville, NC 2807a
[phone]
LABORATORY CONTROL SAMPLE:
1183322
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
Total Suspended Solids
mglL
250
252 101
80-12
SAMPLE DUPLICATE: 1183323
92197561001
Dup
Parameter
Units
Result
Result RPD
Qualifiers
Total Suspended Solids
mg&
NO
ND
SAMPLE DUPLICATE: 1183324
92197643001
Dup
Parameter
Units
Result
Result RPD
Qualifiers
Total Suspended Solids
mg/L
10.0
12.6
23 D6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except m full,
Date: 04/25/2014 09:48 AM without the written consent of Pace Analytical Services, Inc,.
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QUALITY CONTROL DATA
Project: OUTFALL
Pace Project No.: 92197611
QC Batch: WET130602 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92197611001
SAMPLE DUPLICATE: 1181329
Parameter Units
Sid. Units
pH
Date: 04/25/2014 09:48 AM
92197495001 Dup
Result Result
7.2 7.1
RPD Qualifiers
1 D6,H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800KinceyAve, Suile100
Huntersville, NC 28078
(704 )875-9092
Page 7 of 11

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QUALIFIERS
Project: OUTFALL
Pace Project No.: 92197611
DEFINITIONS
DF - Dilution Factor, if feported, represents the factor applied to the reported data due to changes in sample pr
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes 10 Azubenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery an
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethyivinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6
H6
Pace Analytical Services, Inc.
9800 K+nceyAve. Suite 100
Huntersville, NC 28078
[phone]
dilution of
RPD values.
reported for
The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
Analysis initiated outside of the 15 minute EPA recommended holding time.
REPORT OF LABORATORY ANALYSIS
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Date: 04/25/2014 09:48 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11

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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: OUTFALL
Pace Project No.: 92197611
Pace Analytical Services, Inc,
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92197611001
OUTFALL #1
EPA 1664B
GCSV117282
92197611001
OUTFALL #1
SM 2540D
WET130655
92197611001
OUTFALL #1
EPA 9040
WET130602
Date: 04/25/2014 W48 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,.
Page 9 of 11