NCG080601_COMPLETE FILE - HISTORICAL_20150625

IZt�u � �h a Fhb
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-STORMWATER DIVISION CODING -SHEET
RESCISSIONS .
PERMIT NO..
N
DOC TYPE
,�t
COMPLETE FILE'- HISTORICAL
DATE OF
.RESCISSION
❑
p � � 5 b � � 5
YYYYMMDD

f
Semi-annual Stormwater 19harge Monitoring Report •
for North Carolina Division of Water Quality General Permit No. NCGO80000
Date submitted G -9-lj
CERTIFICATE OF COVERAGE NO. NCGO8 , , D �], SAMPLE COLLECTION YEAR G1
FACILITY NAME r d u C L' GL 1(ln�al 7 SAMPLE PERIOD Jan -June ❑ July -Dec
COUNTY LV U or ❑ Monthly' (month)
PERSON COLLECTING SAMPLES T M GLL-7*1cL _ DISCHARGING TO CLASS ❑ORW ❑HQW [—]Trout ❑PNA
LABORATORY 41R45pi'f Lab Cert. # 4 I / ❑Zero -flow ❑Water Supply ❑SA
I
Comments on sample collection or analysis: RECEIVED VED ❑Other
JUN 2 5 2015 PLEASE ,REEMMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more than alms afk-R% motor oil per month.7 V yes _no
(if yes, report your analytical results in the table immediately below) C� SECTION
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period'
Outfall
Na . ;
Date r
;;Sam le Collected,
,- mo%dd/yr
, w Oo53o
��M00400v
00556
_ ..TotaLSuspended ;,
Salids,'rir�g/L ...::
d s: H, a
aStandard:units
Non_Polai; Oil and Grease .TPH EPA ;
Methodrv1664'(5GT3HEM) ,'mg/L,:
New:Motor.iOil Usa a
Annual a�erage:gal/mo
Benchmark
- ,
.50,or00see;permit...
w
'Wtthiri fi 0 "'9 0 :�
,..:....', . :15
..: .
i. •--0 _1
a
�
IS-66 L
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfall
-.w
No
Date
.. :^. v -.-'.::ra f
Sample Collected,
0055fi
�._. 4"L"�'C
�OQ530
00400'
:. �: ._. ._...-d;` .'.:- r,.u� ,.-.. .�... .,u.:
Non?Polar=.Qil and Grease/TPH EPA Method ':
SGTHEM)'
2mg/L
�:' tiY:!•l a.m
Total5uspended:Solids,
g
pH,
-5tardard:units'm/Ld/Y
P,ermi Limit
�.0 '. � <
n 15,.. � .. ^� �5,> y
�. . w.
,� _.: � . _. 50no,r�IQQ ee_permit ....
r6
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Pace I of 2

STORM EVENT CHARACTERISTICS:
Date -first event sampled) _
Total Event Precipitation (inches): t7 S
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART I1 SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in
the case -of "No Dischar e" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signatyro�b'f PVAittee)
(Date)
rLL�
Adrtional copies of this form may be downloaded at: http://portal.ncdenr.org/web/­wq/­wsLsu/npdessw#tab-4
SWU-250 •
last revised* 11, 2013
Page 3 of 2

- 0
L1©L—r1 Ar ic�1 filt�,�l
y y
6/ 1812015
JIM GLEASON
GO TRIANGLE
5201 NELSON ROAD
MORRISVILLE, NC 27560
Subject:
Report of Data - Project: STORM WATER
WorkOrder: 1506033
Attn.: JIM GLEASON
Enclosed are the results of analytical work performed in accordance with the referenced
account number. This report covers sample(s) appearing on the listing,
Thank you for selecting CompuChem for your sample analysis. If you should have
questions or require additional analytical services, please contact your representative at
1-800-833-5097
Sincerely,
Compuchem
a division of Liberty Analytical Corporation
Attachment
TOTAL NUMBER
OF PAGES
0 501 Madison Avenue, Cary, NC 27513 Tel: [phone] Fax: [phone]

CompuChem, a division of Liberty Analytical
Client: GO TRIANGLE Work: 1506033
Project: STORM WATER Sdg: 1506033 1
Lab ID Client ID Matrix Date Sampled
1506033-01 S0001 Water 06/09/2015 08:10
Date Received
06/09/2015 10:59
D
0
6/18/2015

ANALYSES DATA PACKAGE COVER PAGE
Client:
GO "TRIANGLE
Project:
STORM WATER
Laboratory:
COMPUCHEM
SDG:
1506033
Client Sample Id: Analysis: Lab Sample Id:
SD001 LPA 166413 1506033-01
SD001 SM 25401) 1506033-01RIil
certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for
other than the conditions addressed in the narrative. Release of the data contained in this hardcopy data package and in the l;Icctronic Data
Delivcrahle has been authorized by the Laboratory Manager or the Manager's designee, as verified by the following signature.
Signature: Name: Susan Bass
Datc:
E
06/18/2015
Title: Chemist III
ACCp;O -.
501 Madison Avenue, Cary, NC 27513 Tel: [phone] Fax: [phone]
Page 1 of 13

A. SDG Narrative
40
0
0
Page 2 of 13

0
CompuChem
A Division of Liberty Analytical Corp
501 Madison Avenue
Cary, North Carolina 27513
SDG NARRATIVE
SDG # 4506033
Client: GO TRIANGLE
Project: STORM WATER
METHOD: EPA 1664B, SM2540D
Unless otherwise noted on enclosed Laboratory Notices or Quality Assurance Notices, all
quality control criteria were met in the analyses of this sample.
Release of the data contained in the hardcopy data package has been authorized by the
Laboratory Manager or his/her designee, as verified by the signature below.
•
Susan W. Bass
Senior Chemist
June 18, 2015
•
Page 3 of 13

CompuChem
A division of Liberty Analytical Corporation
CompuChem's Pagination Convention
As required by the EPA CLP Statement of Work (SOW) documents, data to be delivered must be
paginated (by machine or hand). In the event that the initial numbering is incorrect (a page
numbered twice or a page skipped, for example), it is CompuChem's policy to add an alphabetic
suffix to a page number when necessary (e.g., I OOA, 10013, etc.). This policy is also applicable to
non-CLP data packages.
Revision 7 (01/12/2011)
Ell
•
•
Page 4 of 13

CompuChem
• A division of Liberty Analytical Corporation
WET CHEMISTRY DATA REPORTING QUALIFIERS
On the appropriate reporting form, under the column labeled "Q" for qualifier, each result is flagged with
the specific data reporting; qualifiers listed below, as appropriate. The qualifiers used are:
U : This flab indicates the compound was analyzed for, not detected and is reported as less than the
Method Detection Limit (MDL) (or as defined by the client). The Reporting Limit (RL), or Limit
Of Quantitation (LOQ), and the MDL will be adjusted to reflect any dilution or concentration of
the sample and, for soils, the percent moisture.
This flag indicates the reported result is an estimated value. The flag is used when an analyte is
detected and the result is less than the adjusted RLILOQ but equal to or greater than the MDL.
Q : This flag denotes that one or more quality control criteria have failed (e.g., LCS recovery,
Continuing Calibration Verification, or CCV) and reanalyses can't be performed. The Q flag is
applied to all specific analyte(s) in all samples associated with the failed quality control criteria.
B : This flag is used when the analyte is found in the associated method or calibration blank as well
as in the sample. It indicates probable blank contamination and warns the data user to take
appropriate action. The combination of flags BU or UB is not an allowable policy. Blank
contaminants are flagged B only when they are detected in the sample.
0 D: This flag is applied to an analyte when the reported result is based on a dilution.
XIYII_ :Other specific flags may be required to properly define the results. If used, the (lags will be fully
described in the SDG Narrative. The laboratory -defined flags arc limited to X, Y, and Z.
The extensions: D, S, and SD are added to the end of the Client ID and represent the
following:
D —Matrix Duplicate
S — Matrix Spike
SD — Matrix Spike Duplicate
•
Revision 0 (03-15-201 1)
Page 5 of 13

Chain of Custody Records
The laboratory shall include a copy of the Chain -of -
Custody (CoQ documentation for all of the samples in the
Work Order/S.DG.
.7
E.
Page 6 of 13

tj4e, t -- 4. n i i Ch P m
CHAIN OF CUSTODY
28519
Page — of —
---
%LLDiVision or 501 Madison Ave.
- WILiberty Analytical Corp. . Cary, NC 27513
Phone: [phone] Fax [phone]
Courier
Airbill No.
Sampling Compfete? Y or N
Z, . CRignt/Repott
Requestetl'ArialysLs
(include method and
alm")
-.'--C.Matrices:
Company Name
GO 122119W
Project Name
Gw -Ground water
WW - Waste water
SW - Surface water
SO - SoiUSediment
TB - Trip Blank
R1 - Rinsate
WP - Wipe
0 - Other
pH:V $k#le Ww-:
Address
5_2 Q A,� kol
Sampling Location
City State Zip
t 1-9 q 0
Turnaround time
Project Contact
I�Q ./,, r_L!fS
Hatch QC or Project Specific? If Specific, which Sample 11)?
Phone N
T"_ I�LPF
Are aqueous samples field filtered 60T MC13IS? Y or N
Sampler's Name
TI
Are high concentrations expected? Y or N? If yes, which I D(s)?
.,CpmpuC ierrr,W:z:
SIC
Field ID
Collection
Matrix
9
bottles
Number of Preserved Bottles
Date
Time
z
F=
so 6o,
lic-,Vjg
I
7U
If`;a�n
Lab
s
Ue-,
y
7711
Sample Unpacked By: VVIAT
Cyanide samples checked for sulfide & chlorine? Y o
i n
625 & Phenol samples checked for chlorine? Y ot�p
Sample Order Entry By: Y 'A"lk A4,
1608
Samples Received in Good Con trios Y r N samples checked for pH between 5.0-9.0? Y oa
If no, explain:
Relinquished bDate/Time:
10
Received by:
(
Datetrime:
Relinquished by-
IDate/Time:
Received by:
]Cooler
Datetrime:
,Subconta t? Y oN If es, where?
Cust oz­j(s) intact'? Y or 10n Ice? Y oy'�
Temp:
Samples stor fter date report mailed at no extra charge. ej White i'Vellow copy to lab - Pink copy for cus
W IF (�tV4-j tuz� I p- 6 OIL)

WORK ORDER
1506033
COMPUCHEM
Printed: 6/15/2015 1(1:48:53AM
Client: GO TRIANGLE
Project !+tanager: Cathy Dover
Project: S"FORN4 WATER
Project Numhcr. STORM WATER
SDG: 1506033 CASE:
Status: Batched
Report To:
Invoice To:
GO TRIANGLE
GO TRIANGLE
JIM GLEASON
JIM GLEASON
5201 NELSON ROAD
5201 NELSON ROAD
MORRISVILLE. NC 27560
MORRISVILLB, NC 27560
Phone: [phone]
Phone :[phone]
Fax: -
Fax: -
Date Due: 06/22/2015 00:00 (13 day 'FAT)
Received By: Cathy Dover Date Received: 06/09/2015 10:59
Logged In By: Cathy Dover Date logged In: 06/09/2015 1 1:55
J & B Flags?: YES TICS?: NO Deliverable: Lccel I E-mail Only EDD : NO EDIT
Metals I to? MDL iSpikcLevel: FULLSpike
LCS ONLY*ORG 166413 FIEM*TSS
Analysis Due TAT Expires Received Continents
1506033-01 SD001 [Water) Sampled 06/09/2015 08:10 Eastern
OILB:GREASE HEXANE HEM 1664B 06/22/2015 16:00 l3 07/07/2015 08:10 06/09/2015 10:59
TTL SSPND SOLIDS (TSS) 2540D WATER06122/2015 16:00 13 06/16R015 0& 10 06/09/2015 10:59
•
Page 8 of 13

ANALYSIS DATA SHEET
s D001
0lient: GO TRIANGLE. SDG: 1506033 Projcct: STORM WATER
Lab lD: 1506033-01 '%Solid: MatriN: Water Sampled: 06/09/15
Received: 06/09/15
CAS NO.
Analple
Colic.
(mglL)
MDL
RL
1).F.
Q
Method
Sequence
Analyzed
OILGRGAM."
Oil R Grease (HEM)
29.4
1.16
5,00
1
EPA 1664n
51- 18004
6/16/15 11:05
Tss
Total Suspended Solids
7.00
416
50.0
1
1
SM 2540D
5F16010
05/15 17:35
E
•
�y 1'
l—Ibc rt�r„1 Ae�alytEcal
11
�41�'� A,.O.,� 0 9
d �■fit! ". �a
x
Page 9 of 13

ANALYSIS DATA SHEET
PBZF
Client: GO'1'RIANGIA: SDG: 1506033 Project: STORM WA'1'I R
Labll)• 5061306-13LK1 Matrix. Water
L�
CAS,NO.
Analyte
Conc.
(mgll,)
IMM, IRL
U.F.
Q
dlethod
Sequence
Analyzed
OILGtEASE
Oil & Grease (HTiM)
1.16
5.00
I
U
L'PA166413
5F18004
611fi115 11:05
1tA ACCpgDA
E�IdPrf-� Ar'�r�1i-JYEceI
s
:7
Page 10 of 13

ANALYSIS DATA SHEET
W11csZi,
0ient: GO TRIANGLE
Lab ID: 5061306-IISI
SDG: 1506033 Pr( jcct: STORM WATER
Matrix: Water
CASNO.
Analvtc
nc.
g/]-)
4401
NIDL
RL
1).F.
Q
Method
Sequence
Analyzed
OILGREASE
Oil&Grease(H1,M)
.7
L16
5,00
1
ETA 166413
51;18004
6/10115 11:05
•
l�Yb�rYy Ar'-�caly Ftc�al
A0"0
Page 11 of 13

ANALYSIS DATA SHEET
PBZ11
Clicnt: GOTRIANGLS SDG: 1506033 Project: STORM WATER
LabID: 5061504-BLK1 Matrix: Water
CAS NO.
Annlplc
COnC.
(mglL)
NIDL
RL
1).F.
I Q
I Method
Sequence
Analyzed
TSS
Tnt:d Suspended Solids
0.416
5.00
1
lJ
Sot 2540D
5F16010
6/15/15 17:35
A.CCOROA ;.._.
•
Page 12 of 13

ANALYSIS DATA SHEET
wLCSZII
0icnt: GO TRIANGLE
Lab I1): 5061504-IIS 1
SDG: 1506033 Project: STORM WATER
Matrix: Water
CASINO.
Analyse
Conc.
(IngIL)
MDL
RI,
D.F.
Q
Aielhod
Sequence
Analvred
Tss
Total Suspended Solids
81.0
4.16
50,0
l
SM 2540D
51-'16010
6115115 17:35
171
w
Lldwrhy Ari alyYlc�+l
ACp .
v CRQ'92
1
Page 13 of 13