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HomeMy WebLinkAboutNCG060354_MONITORING INFO_20190204STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V O �j D35 y DOC TYPE 0 HISTORICAL FILE iQ.MONITORING REPORTS DOC DATE ❑ J Oi'I D --) D '7 YYYYMMDD January 13, 2020 NC Department of Environment and Natural Resources Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Attention: Central Files Subject: Discharge Monitoring Reports 11 NPDES General Permit No. NCG060000 COC# NCG060354 (R11R2) Hospira, A Pfizer Company— Nash County To Whom It May Concern: A Company RECEIVED FEe 04 20 19 CENrRk FILES DWR SECrlj Per the requirements of our general stormwater permit, the following documentation is attached for your review; ✓ Storm water Discharge Monitoring Reports for Outfalls 004B, 005, 017A ✓ Certified laboratory report All required discharge characteristics (total suspended solids, pH, oil and grease, and chemical oxygen demand) were within permitted ranges. Total rainfall was measured with an on -site rain gauge for the duration of the event. We will continue to conduct future sampling events based on the conditions indicated in our permit. Please contact me at (252) 977-8292 if you have any questions or I can provide any additional information. Sincerely, Samuei Toke EHS Manager Hospira, a Pfizer company 4285 N. Wesleyan Blvd. Rocky Mount, NC 27804 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 01/13/2020 CERTIFICATE OF COVERAGE NO. NCG06 0 3 5 4 SAMPLE COLLECTION YEAR 2019 FACILITY NAME Hospira, a Pfizer company (Rocky Mount, FACILITY ACTIVITIES INCLUDE (check all that apply): NQ ❑ use/process meats ❑ use animal fats/byproducts COUNTY Nash DISCHARGING TO SALTWATERS? ❑YES ®NO PERSON COLLECTING SAMPLES Mike Lewis LABORATORY Pace Analytical Lab Cert. # PASI-C #12, PASI-A #40 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall '_.3 or ❑ No discharge this period3 Outfall No. Sample, Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliforml, Colonies per 100 ml Enterococci', Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 120 30 1000 Soo 004E 12/17/19 3.3 6.74 <25.0 <4.8 N/A N/A 005 12/17/19 11.5 7.21 <25.0 <4.9 N/A N/A 017A 12/17/19 19.2 7.57 27.8 <4.9 N/A N/A 1 Only applies to facilities that use/process meats. 2 The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 504 6.0 — 9.0 - N/A N/A N/A N/A N/A N/A 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (ides, complete Part B) RECEIVED FEB 0 4 2m CENTRAL FILES DWR SECTION SWU-249 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE'BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: N/A Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case o "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." PI'—�r¢A/--ac.-7a (Date) Additional copies of this form may be downloaded at: http://Portal.ncdenr.org/web/wQ/ws/su/nodessw#tab-4 S WU-249 Last Revised: October 18, 2012 Page 2 of 2 Stormwater DMR Sampling Sample Date Event Start Time Event Rainfall 7I/1 TI/ 150 013 Outfall No. 004B (LVP) Time pH Temperature Outfall No. 005 (FCF) Time pH 7,X) Temperature /�, j pC Outfall No. 017A (R2) Time pH Temperature Sampled by: ;W,./�/ /-)'/ 71J 7 aceAnalytical` WVft+ WAh&cam December 31, 2019 Michael A. Lewis Hospira, Inc. - Rocky Mount, NC 4285 N. Wesleyan Blvd. Rocky Mount, NC 27804 RE: Project: Stormwater Pace Project No.: 92458192 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)634-4964 Dear Michael Lewis: Enclosed are the analytical results for sample(s) received by the laboratory on December 19, 2019, The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Samuel Toke, Hospira- Rocky Mount REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 1 of 14 aceAnalytical® urm.pawabs.com Project: Stormwater Pace Project No.: 92458192 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, hiuntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 FloridalNELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNEI-AP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 aceAnalytical t+ m.paeatabs.eam SAMPLE ANALYTE COUNT Project: Stormwater Pace Project No.: 92458192 Pace Analytical Servlcea, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92458192001 0UTFALL 017 EPA 1664E HH 1 PASI-C SM 2540D-2011 MJP 1 PASI-A SM 5220D-2011 JP1 1 PASI-A 92458192002 OUTFALL 004E EPA 1664B HH 1 PASI-C SM 25401)-2011 MJP 1 PASI-A SM 5220D-2011 JP1 1 PASI-A 92458192003 OUTFALL 005 EPA 1664E HH 1 PASI-C SM 254OD-2011 MJP 1 PASI-A SM 5220D-2011 JP1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 aceAnalytical WWW.paeelabs.cmn ANALYTICAL RESULTS Pace Analytical Services, LLC 67011 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Stormwater Pace Project No.: 92458192 Sample: OUTFALL 017 Lab ID: 92458192001 Collected: 12/17119 11:48 Received: 12/19/19 08:46 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 4.9 1 12/31/19 09:11 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 19.2 mg/L 4.2 1 12/23/19 18:14 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 27.8 mg/L 25.0 1 12124/19 23:23 12/25/19 07:01 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/31 /2019 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 14 aceAnalytical rrw.pacdabsrom ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Slormwater Pace Project No.: 92458192 Sample: OUTFALL 004E Lab ID: 92458192002 Collected: 12/17/19 10:40 Received: 12/19/19 08:46 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed GAS No. Oual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 4.8 1 12/31/19 09:12 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 3.3 mg/L 2.7 1 12/23/19 18:14 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mg/L 25.0 1 12/24/19 23:23 12/25/19 07:01 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/31/2019 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 aceAnalytrcal MMMf penult iza ANALYTICAL RESULTS Pace Analytical Services, LLC 6701 Conference Strive Raleigh, NC 27607 (919)834-4984 Project: Stormwater Pace Project No.: 92458192 Sample: OUTFALL 005 Lab ID: 92458192003 Collected: 12/17119 11:22 Received: 12/19/19 08:46 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Ouai HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mglL 4.9 1 12/31/19 09:13 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 11.5 mg1L 2.5 1 12/23/19 18:15 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mg/L 25.0 1 12/24/19 23:23 12/25/19 07:02 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12131/2019 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 ace Analytical W".paaiiII&cola QUALITY CONTROL DATA Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)B34-4984 Project: Stormwater Pace Project No.: 92458192 QC Batch: 517358 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92458192001, 92458192002, 92458192003 METHOD BLANK: 2770344 Matrix: Water Associated Lab Samples: 92458192001, 92458192002, 92458192003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 12/31/19 09:04 LABORATORY CONTROL SAMPLE: 2770345 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 32.0 80 78-114 MATRIX SPIKE SAMPLE: 2770346 92457560002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 38.5 16.7 40 78-114 M1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/31/2019 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 aceAnalytica! wir*.patdltts.tom QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92458192 QC Batch: 516469 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92458192001, 92458192002, 92458192003 Pace Analytical Services, I.LC 6701 Conference Drive Raleigh, NC 27607 (919)834-4964 METHOD BLANK: 2767268 Matrix: Water Associated Lab Samples: 92458192001, 92458192002, 92458192003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 12/23/19 18:11 LABORATORY CONTROL SAMPLE: 2767270 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 251 246 98 90-110 SAMPLE DUPLICATE: 2767271 92458028003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 125 128 2 SAMPLE DUPLICATE: 2767272 92458406001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 53.8 35.1 42 06 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/31 /2019 02:35 PM without the written consent of Pace Analytical Services, LLC, Page 8 of 14 aceAnalytical ww-p=W lbs.com QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92458192 QC Batch: 516655 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92458192001, 92458192002, 92458192003 METHOD BLANK: 2767990 Matrix: Water Associated Lab Samples: 92458192001, 92458192002, 92458192003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 12/25119 06:57 Paco Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 LABORATORY CONTROL SAMPLE: 2767991 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 762 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2768004 2768005 MS MSD 92458100001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 82.5 100 100 187 194 105 112 90-110 4 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2768006 2768007 MS MSD 92458369003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RP❑ Qual Chemical Oxygen Demand mg1L ND 100 100 121 121 109 109 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/31/2019 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 lacieAnalyficale •rsr psatsbs.c m QUALIFIERS Project: Stormwater Pace Project No.: 92458192 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)634-4984 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific anatyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 13270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SV11846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-N itrosod iphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12131 /2019 02:35 PM without the written consent of Pace Analytical Services, L.I.C. Page 10 of 14 e aceAnaljftal wxr.patalatos.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater Pace Project No.: 92456192 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92458192001 OUTFALL 017 EPA 1664E 517358 92458192002 OUTFALL 004B EPA 1664B 517358 92458192003 OUTFALL 005 EPA 1664E 517358 92458192001 OUTFALL 017 SM 25400-2011 516469 92458192002 OUTFALL 004E SM 254OD-2011 516469 92458192003 OUTFALL 005 SM 25400-2011 516469 92458192001 OUTFALL 017 SM 5220D-2011 516655 SM 52200-2011 92458192002 OUTFALL 004B SM 5220D-2011 516655 SM 5220D-2011 92458192003 OUTFALL 005 SM 5220D-2011 516655 SM 5220D-2011 Date: 12131/2019 02:35 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in ful, without the written consent of Pace Analytical Services, LLC. Analytical Batch 516665 516665 516665 Page 11 of 14 Document Name: Document Revised: February 7, 2019 Sam a Condition Ll 4n Recalpt(SCURJ Pa e 1 of 2 aCVA&,VybM • Document No,: Issuing Authority: F-CAR-CS-033-RevAg Face Carolinas Quality Office Laboratory receiving samples; Asheville Eden[] Greenwood ❑ Huntersvifle❑ Ralellihg] Mechanirsvilie❑ • SEEM Protect g: Client Name: WO# : 92458A2 I� �l t L Courier: ❑Fed Ex UPS USPPS ` Client ❑ Commercial 2Pace ❑Other 92458192 Custody Sea( Present? ElYes ONo Seats intact? ❑Yes &c, DateAriftfah pefsan Eramfning Contents:__Zp-1A Packing Material: []Bubble Wrap SSubble Sags ❑None ❑ Other Biological Tissue Frozen? Thermometer. a IT Type of Ice: 0 0 � []WetQ8lue C]Nms []Yes QN4 ®N/A �lA Gun 10: � Cooler Temp ('C): • 0.2) Correction Factor: Add/Subtract ('C) Q . U Temp should be above freezing to VC Cooler Temp Corrected ('C): []Samples out oftemp crherta. Samples on Ice, cooling process hu begun USDA Regulated Soil ([f N/A, water sample) Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples erlglnate from a foreign source (Intemat(onally, nYes nNo rndudina kaunll and h,erea Atml7 f—Wes r1Na Coraments/Discrepaing, Chain at Custody Present? es QNo N/A L Samples Arrived within Hold Time? &eS QNQ ONIA L Short Hold Time Anal)L51! (Q2 hr.)? 19Yes ❑No WA 3. Rush Turn Around Time Requested? UN &. ONJA 4. SuffirientValume?AY, []No N/A 5. Correct Containers Used? -Paco Containers Used? flYes Yes ONO IN. ❑N/A N/A 6. containers containerslntact7 Yes No N/A 7. analysts: Samples Field Filtered? Yes o N A S. Sample Labels Match COC? -Indudes Oate.Mmi fiD/Ana is Matrix: oyes C ONO ON/A 9. Headspace in VOA Vials (>S�mm)7 Yes ON. �" ,�/A 10. Trip Blank Present? Trip Blank Custody Seats Present? Dag Dyes ONO Na QN/A N/A 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/TIME: field Data Raqulred? []Yes []No a Project Manager SCURF Review: Data: Project Manager SRF Review: Date: Page 12 of 14 rr�— Document Name: DacumenCRevfsed: February 7, 2018 !r� SAm !e tttnditian U on Revel t SCfJR Page 1 of 2 ! •••' BCeRll�IytiCd�� - bacumcntNa.: IsslringAuihortty: FtARrCB•033=Ray.06 Pace Carolinas QualFly Ofiflce 'Check mark top half of box If pH and/or dechlor€nat€on is project Ff-V2458192 ver€fled and within the acceptance range for preservation WO samples. . PM; t4WB Cue pats: 12/31/19 aceptlons: VOA, Collform, TOC, Oil and Grease, ORDISO115 (water) Doc, uNg CLIENT' 91-14egp i re "Bottom half of box is to list number of bottle S T3 m d14 a 2 Z z v z d= v N 1 Z' oMi v ro al�! m g 9 g y s9 u 22y 3 x 0 %t C C C G Z Q 0 C 7 N 2 O O p, p z 9 x NNN 2 < vA R 4 aaalll a Z 7 _N �f V U u1 D 17 C U !! E d 0 1 0$ w 5 q d� a .�+ a a a >> > 7 7 ^ a+ J w ,,fy+Ei NE SE _b E E E E v w x a [Ey E g 8 E of o E E e� n tn rf 1 r, ey N �, ,� 0 $ 3 ` ,n•�1 f 1�1� N O N O m a0i ;t � n � d m m m m m m m m ¢ a tad a a a O 7 } q >> Fan m Q i 1 2 I NN I Ll 11 XN-NN1 I I 1 .1 1 1 J i 3 li N,'\NN 4 1 NNNN I N 1 -1 1 � � � �- NN -N--] NNNN I- I I I I kss N I EN I N\N I I � I I I NN M7- ) N-NNN I I I I 1-1--M i N 'I � 1.1 N\� L 1----LL---\NN 1 .11 1 M 19 I I I r-\-[\ N N f I K I \ K K f 1 1.1 1 17 1z pH Adjustment Log for Preserved Samples Sample if) Type of Preservative pH upon recelpt Date preservation adjusted Time preservatlon adjusted Amount of preservative added lot p Note: wnenever there Is a dLscrepaacy affecting North Cafollns mmpliance samples, a copy or tnu Form ami oe sent m the harm tareuna UHINK Leruncanan UMM Ire. Out of hold, incorract preservative, out of temp, incorrect containers. Page 13 of 14 ;' ;�atewaat�tiTar Section A Remdeeb CHerd Worrtntioa T pe"e,-,(2 Ck° Section Requked Project Won. liom CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain-W-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Saco" C Invoice bdor natkrn: Paae • t Ot t Compwy. i Ho5Ora, Inc•Rodry Mount NC Repo: To: klichad LcwiS Aum1orr. drew; 4285 K Weveym 91rd Copy To: Company Name: Rodcv Wlorall. NC ZrW4 Address: ✓ty4� :.: `� — _ •• Bwflt midwd.alewlsOPflxer.Com Pumtn Oroer a: z pool, ouare: Phony 1 (52)97'-5433 Fa�c Pr*ct Name: Srormwmer Pace Proota Manages rnatlnaw.brana+up .cam. ,•:x. j;'P`; Muxar,� Requ"cd this Date: Project /: lam Profile e; 4733-2 NC s ,Mina oweCOLLe ow kft%Vws ow wft wT $ CTED PrernWves se -- w.p. w.rw ww y $ rlcad r SAMPLE ID S* a Sr a $_ START em 8 r� �. e - o One GlurecWr per WX. wlx wP w < o S (A-Z.O.9!.I Co - be o Sample kis aarii unn" TOM Ta O u 1r�� Pv oQ rT� Y 9 DATE TIME GATE TIME w Oaeaaot7 wT G �/ s n c 11 /C-/o �C� 1 ryti Orman oo48 W E I 4 x x x �i,/ /l Az 1/ �► y '\ I 1 L' Outten aas WT /%' /7 x x x NA .ice rIr• 40 4 �����+ ��`'r 4afasarrLF •: �.f; �! .r JA• -.. .��a •.. _-..•� . :`.�.^ .�. � _Y ERNWO r '�GIiF�St�-i i •.. Jy7.SR�n.'.33`:.` _ Y• •:sSATE i 'iw it; Ile !?slit-L l2-l$-i4 f5 1 O r o C. - �]�f✓A�]����:�. ~ �:7'T.�:.�.Y.:t„i1�:._ �'.:[.M.t9v :��ti ::}_C=:�r3� �nC-i.Y•.a; - �R:'`; +�y�Y.��.Y. ��•i:T'�s�•-� PRINT Hams OT SAYPL£R: p SIG NATURE of SAMPLER: DATE a L ,.�•� &J 777 N �