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NCG060352_COMPLETE FILE - HISTORICAL_20190701
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /v Cc,5, o DOC TYPE "ISTORICALFILE ❑ MONITORING REPORTS DOC DATE p Dbl� 0, YYYYMMDD SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality a eral Permit No. NCG060000 Date submitted Z % CERTIFICATE OF COVERAGE NO. NCG06__6_��Z SAMPLE COLLECTION YEAR % d 13 FACILITY NAME 5+b COW C �'3,Xq Q_,mc_,ec� eo -[L C1--_S FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Q _S C" f--l 4D-De/process meats Kuse animal fats/byproducts PERSON COLLECTING SAMPLES e 1 5e DISCHARGING TO SALTWATERS? EYES /JVO LABORATORY,EqCg hkhk Lab Cert. # 53 Z4 JUL Q 1 2019 LEASE REMEMBER TO SIGN ON THE REVERSE 4 WEni-! kAL FILE Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall 1. 5'jl or ❑ No discharge this period Outfall No. Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coiiform , Colonies per 100 ml Enterococci , Colonies per 100 ml Benchmark 100 or 50 Within 6.0 — 9.0 120 30 1000 500 U 2� I I I 4 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ;N no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30 100 or 50 6.0 — 9.0 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at pnV outfalls, you must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if yes, complete Part B) SWU-249 Last Revised: October 18. 2012 Page l of 2 jr— *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." M,,,- ("'-' - i(/Zq1,ra (Signature of Permittee) (Dat ) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-249 Last Revised: October 19. 2012 Paee 2 of 2 aceAnalytical' wwwpacelahacam June 17, 2019 Sal DiGiovanni S&D Coffee 300 Concord Pkwy S Concord, NC 28027 RE: Project: STORMWATER SAMPLING Pace Project No.: 92432353 Pace Analytical Services, Ll-C 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Sal DiGiovanni: Enclosed are the analytical results for sample(s) received by the laboratory on June 10, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni for Sarah Graham sarah.graham@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Mark Weisel, S&Q Coffee REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 IaceAnalXical" Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunfersville, NC 2847876 www.pacelabs.com (704)875-9092 CERTIFICATIONS Project: STORMWATER SAMPLING Pace Project No.: 92432353 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 LouisianalNELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiafVELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 leAnaVical * www.pacelab&mm Project: STORMWATER SAMPLING Pace Project No.: 92432353 Lab ID Sample ID SAMPLE SUMMARY Matrix Date Collected Date Received 92432353001 MAIN SWO-1 Water 06/10/19 10:15 06110/19 13:20 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, l_LG. Page 3 of 14 aceAnalytical www.pacelabs.mn SAMPLE ANALYTE COUNT Project: STORMWATER SAMPLING Pace Project No.. 92432353 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9492 Analytes Lab ID Sample ID Method Analysts Reported 92432353001 MAIN SWO-1 EPA 1664E JMS 1 SM 254OD-2011 MJP 1 EPA 9040C ECH 1 SM 5220D-2011 GC 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 14 aceAnalyticalo wwwpacelabs.cw ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 1C0 Huwersville, NC 28078 (704)875-9092 Project: STORMWATER SAMPLING Pace Project No.: 92432353 Sample: MAIN SWO-1 Lab ID: 92432353001 Collected: 06/10/19 10:15 Received: 06110/19 13:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO mglL 4.8 1 06/12/19 06:03 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 66.4 mg/L 20.0 1 06/14/19 12:27 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.6 Sid. Units 0.10 1 06/16/19 13:52 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 246 mglL 25.0 1 06/14/19 18:00 06/17/19 15:53 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/17/2019 04:43 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 acmnalytical www.pacetabacom QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92432353 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersviile, INC 28078 (704)875-9092 QC Batch: 480559 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92432353001 METHOD BLANK: 2599794 Matrix: Water Associated Lab Samples: 92432353001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 4.8 06/12/19 05:55 LABORATORY CONTROL SAMPLE: 2599795 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oii and Grease mg1L 38.5 37A 97 78-114 MATRIX SPIKE SAMPLE: 2599796 92432130001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 38.5 38.1 96 78-114 Results presented an this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right at the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/17/2019 04:43 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 (�IacieAnalytical * www.p&Dofabs.com QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92432353 QC Batch: 481178 Analysis Method: SM 2540D-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92432353001 METHOD BLANK: 2602782 Matrix: Water Associated Lab Samples: 92432353001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 06/14/19 12:25 LABORATORY CONTROL SAMPLE: 2602783 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE; 2602784 Parameter Units Total Suspended Solids mglL SAMPLE DUPLICATE: 2602785 Parameter Units Total Suspended Solids mglL Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)B75-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 251 250 100 90-110 92432316001 Dup Max Result Result RPD RPD Qualifiers 525 572 9 5 D6 92432341001 Dup Max Result Result RPD RPD Qualifiers 14.0 15.2 8 5 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/17/2019 04:43 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 aceAnalytical www pacelabs.com QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92432353 QC Batch: 481387 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92432353D01 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE DUPLICATE: 2603787 92432907001 Dup Max Parameter Units Result Result RPD RPD Qualifiers pH at 25 Degrees C Std. Units 6.9 6.6 4 9 H3 SAMPLE DUPLICATE: 2603893 92432429004 Dup Parameter Units Result Result pH at 25 Degrees C Std. Units 1.0 1.0 Max RPD RPD Qualifiers 0 9 1g,H3 Results presented on this page are in the units indicated by the "Units" column except where an altemate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 06117/2019 04:43 PM without the written consent of Pace Analyticai Services, LLC. Page 8 of 14 aceAnalytical www.pecelabs.mm QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92432353 QC Batch: 481291 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92432353001 METHOD BLANK: 2603444 Associated Lab Samples: 92432353001 Parameter Units Chemical Oxygen Demand mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 06/17/1915:53 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2603445 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 755 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2603446 2603447 MS MSD 92432353001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand mg/L 246 100 100 351 349 105 103 90-110 1 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2603448 2603449 MS MSD 92432572003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand mg/L 26.5 100 100 129 151 103 124 90-110 15 3 M1,R1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/17/2019 04:43 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 Pace Analytical Services, LLC cEAnalytical® 9844 KinceyAve, Suite i40 HuntorsviUe, NC 28478 a www.pacelahs.mm (744)875-9092 QUALIFIERS Pro}ect: STORMWATER SAMPLING Pace Project No.: 92432353 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS 1g Sample was not suitable to be use a probe on; pH strips used D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sampie was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0611712019 04:43 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 aceAnalytical. wivw,p 001abs.mn QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Pfaject. Pace Project No.: STORMWATER SAMPLING 92432353 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92432353001 MAIN SWO-1 EPA 1664B 480559 92432353001 MAIN SWO-1 SM 254OD-2011 481178 92432353001 MAIN SWO-1 EPA 9040C 481387 92432353001 MAIN SWO-1 SM 5220D-2011 481291 SM 52200-2011 481335 Date: 06/17/2019 04:43 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 11 of 14 ��1,,�s Sam le Condltlw Upon Rael SCUR Pa e 1 al l kg'1`kde bowmen[ No.: LI--WC hstdry Authmitsr F•CARdS-033'•Rev.D_6____ Pace Grpllnas QuaQtY DNkE _. Laboratory recehrin` samples: AshoON ❑ Eden[] Greenwood ❑ Huntersolaa— Ralelsh❑ Mechanlcsrrllle© Q]erltName: WO# : 92432353 • Sa-� %o r Project e. Oradea. Fed Fa UPS Ousin LJCmml I� I fll it IQfI�III II �If ❑ Commercial 2r+a []other:_ 02432353 Custody Seal Present? ❑Yes Vo Seale hHaa7 D. �Qmr.- / pate/Inuit PMen E...oAre CenOlAtl: �`l.G Pat" INatwlal: []Bubble Wrap uttble Baas ❑Mona ❑ Other Blaio=IalTimym stue Fr en7 i vmame�te 92TD42 TtpeFta: wat ❑elm ❑Rae Caahr Ttmp M: _ Carrwdon Factor. Add/Subtratt VC) 0.0 Caular Temp Corcected ('C); 11� Tempdsetrld ibore Reea>ry to G'C �pn out as temp uft W. Samphi en ke, ceol3na Precut �J k braaa USDA Resulated Saa{kJ NfA, water sample] Did samples arp In a 4mnntkw zone wRh6 the Urdted States: CA, NT,er SC{[heck mapsl? ten safer dlickm he. a fmataa taeke Isnrnn ally. . ❑Yes Inctuma Hawadand Fuene RICO? Ova Chain of Oftdy Present? n171N. E3.VA 1. S&Mpibs lurhred eAthln Hold TFme7 •n Mu ufA 7. Short Reld Tlma Ana la 472 hr. eo A 3. Ruch Tyra Araond Tlewe anted? - n A 4. Sufkke tvdrmre7 Ha mlwA S, CorrectCWaintrs Uted? .Pam Cogaien nused? a Y. ❑Rp Ikf OKJA A G. Conta:nett mw? Vai NB A 7. ' 01s501ve4 *— A: s.m 1es Field Fi tered? w !A a. Sample Labels Match CDC? hdudes Dat me/iD/Am s MatdA: w a ❑us ❑N/A S. H42cho.e ti VDA'"' 'S-0mrn ? NIA 1R Trip ahnk Preient7 Trkp 114MCusto Seah Present? Qrer OY. ft Ire [,JH1A A 1t.. CDMMFNTZWPU DiSCRTPANCY Lot ID oI'plt runtalnerf: WENT NOTMEATION/aCSOLUMM Person crnt>+«c- oate/Tlm: Fkld DM K"1AM1? Ares D. Project Maruaer SCURF Reulew: �Ben: Project Manger SRF Review: Date: Page 12 of 14 �eSam fe Cenditlae UPC" MCI,t Sam P S of 2 AWCd Daatoteet ko.: 1u�na Atsilterttp. f-UR QG33Aer.0a ►aa CwOnas Qualty ONke *Check mark top half of box if pH and/or dechiorinatlan Is verified and within the acceptance range for presarvatlon samples. eaa0adem MA, Confarn% ft7t.Oa and Grem, oaolamS J..Wi DOC. uNy "Bottom half of box is to list number of bottle Project W®# : 92432353 PH: SKO the Oats: 06/17/19 CLCENT: 92-S&D no in ONE iu�ii�►iii �� ��a y�■� pH Adjustment Log for Preserved Samples SaePle D TVP. er P—athe am e00e reeabt am p—r,-U a edfrdnd Time PrP -Uw adSoOa Amon[ N Preser—W add" to a Note: Whanavarthera if d i dkQaPar�q ilfanNla Morth GTPn15a tpmPQyeq HRGey a ieW a rtn nsm rrrx �e sen[ID ue ww�. �sww Knn. �ssviarw. 0 of held. b—..t P—..Oa.a, era of We%hrt ed owdak a Page 13 of 14 A CHAIN -OF -CUSTODY! Analytical Request Document d Tt. Chµ' O-Cwtady is . LEGAL WCUMEwT, An ret.v.nt Wd. moat b. mmpkIed .=-M.y. *.—A C Me.u1rN Cnna.ewn.wn: h.pcx.a.rm.sbn M..+•. a+..+4- LE ID Infl ....,.....■. ............ 111111101111 monsoon monsonsionso ............ ............ ............ ............ ® _..m.--, ,......., ® _..--.-, ,..... ... I _..---- .......... _..--.. .......... _,.---- .......... ® _..---- .......... ® .. .. • ®flif/J� /���nK®fir` 10000 MEMO NONNI INS �W WWI ./1'*►w)►�lJ6l l! M F,. uW WE I.E. PC=(Aa a r/li'llli ArcM. W SOMEONE IM M.m..r a.rMriert � i y{p pi rUREWSAMMEM •I DAT931v..: X. �% rc�L 6 L