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HomeMy WebLinkAboutNCG030689_MONITORING INFO_20190204STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V Cc, DOC TYPE ❑HISTORICAL FILE C� MONITORING REPORTS DOC DATE ❑ YYYYMMDD Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. NCG03 o 6 8 9 FACILITY NAME AwNC COUNTY Durham PERSON COLLECTING SAMPLES Hakim Lundy LABORATORY PACE Analytical Lab Cert. # 12 Comments on sample collection or analysis: Outfall No. 1 Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ❑ Jan -June Q July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA �y _'''' ❑Zero -flow ❑Water Supply [:]SAfE C E I V E D ❑Other Retention Pond release to Neuse River FEB 0 4 2019 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CEhTP,AL FILES DW'R SECTION ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics5 Benchmarks _ - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141 11/15/18 10.37 28.9 mg/L 5.3 ND ND 0.0102 ND ND ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you trust still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-24S, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Storm water Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Hakim Lundy Name (Print name) Assistant Mgr. Safety Environmental Title (Print title) Signature Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 COS30 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/l/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original copy of this DMR, including oll "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attw DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee Date Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Palle 3 of 3 Pace Analytical Services, LLC 6701 Conference Drive laceAnalytical'- Raleigh, NC 27607 www.pace)abs.com (919)834-4984 1 ` Page 1 of 3 Laboratory Report Hakim Lundy Report Date: 11/30/2018 A W North Carolina Date Received: 11/16/2018 4112 Old Oxford Highwy Durham, NC 27712 Project: SW OUTFALL 1 11115 Pace Project No.: 92407733 Sample: OUTFALL 1 Method tab ID: Parameters 92407733001 Collected: 11/15/18 12:25 Matrix: Results Units Report Limit Water Analyzed Qualifiers EPA 1664B Oil and Grease NO mg1L 5.0 11130/1 B 05:53 EPA 1664B Total Petroleum Hydrocarbons NO mgIL 5.0 11/30/18 05:53 EPA 608.3 Aldrin ND ug/L 0.050 11/27/18 17:18 EPA 608.3 alpha-BHC NO ug/L 0,050 11/27/18 17:18 EPA 608.3 beta-BHC NO ug/L 0.050 11/27/18 17:18 EPA 608.3 delta-BHC ND ug/L 0.050 11/27/18 17:18 EPA 608.3 gamma-BHC (Lindane) NO ug1L 0.050 11/27/18 17:18 EPA 608.3 Chlordane (Technical) NO ugIL 0.50 11/27/18 17:18 EPA 608.3 alpha -Chlordane NO ug/L 0.050 11/271181T18 EPA608.3 gamma -Chlordane NO ugIL 0.050 11/2711817:18 EPA 608.3 4,4'-000 ND ug1L 0.050 11/2711817:18 EPA 608.3 4,4'-DDE NO ug/L 0.050 11/27/18 17:18 EPA 608.3 4,4'-DDT NO ug1L 0.050 1112711817:18 EPA 608.3 Dieldrin NO ug1L 0.050 11/2711817:18 EPA 608.3 Endosulfan I NO ug/L 0.050 11/27/18 17:18 EPA 608.3 Endosulfan II NO ugIL 0.050 11/27/18 17:18 EPA 608.3 Endosulfan sulfate NO ugIL 0.050 11/27/18 17:18 EPA608.3 Endrin NO ugIL 0.050 11/2711817:18 EPA 608.3 Endrin aldehyde NO ug1L 0.050 11/27/18 17:18 EPA 608.3 Heptachlor NO ugIL 0.050 11/27/18 17:18 EPA 608.3 Heptachlor epoxide NO ugIL 0.050 11/27/18 17:18 EPA608.3 PCB-1016 (Aroclor 1016) NO ugIL 0.50 11/27/18 17:18 EPA 608.3 PCB-1221 (Aroclor 1221) NO ug/L 0.50 11/27/18 17:18 EPA 608.3 PCB-1232 (Aroclor 1232) NO ug1L 0.50 11/27/18 17:18 EPA 608.3 PCB-1242 (Aroclor 1242) ND ug1L 0.50 11127/1 B 17:18 EPA 608.3 PCB-1248 (Aroclor 1248) NO ug/L 0,50 11/27118 17:18 EPA 608.3 PCB-1254 (Aroclor 1254) NO ug/L 0.50 11/27/18 17:18 EPA 608.3 PCB-1260 (Aroclor 1260) NO ug/L 0.50 11/27/18 17:18 EPA 608.3 Toxaphene NO ug1L 0.50 11/27/18 17:18 EPA 8082A PCB-1016 (Aroclor 1016) ND ug1L 0.50 11/20118 11:25 EPA 8082A PCBA221 (Aroclor1221) NO ug1L 0.50 11/20/18 11:25 EPA 8082A PCB-1232 (Aroclor 1232) NO ug/L 0.50 11/20/18 11:25 EPA 8082A PCB-1242 (Aroclor 1242) NO ug/L 0.50 11/20/18 11:25 EPA 8082A PCB-1248 (Aroclor 1248) NO ug1L 0.50 11/20/18 11:25 EPA 8082A PCB-1254 (Aroclor 1254) ND ug/L 0.50 11/20/18 11:25 EPA 8082A PCB-1260 (Aroclor 1260) ND ugIL 0.50 11/20/18 11:25 EPA 200.7 Rev 4.4 1994 Copper NO ug/L 5.0 11/20/18 02:37 EPA 200.7 Rev 4A 1994 Lead NO ug/L 5.0 11/20/18 02:37 EPA 200.7 Rev 4.4 1994 Zinc 10.2 ugIL, 10.0 11/20/18 02:37 EPA625.1 Acenaphthene NO ug1L 4.9 11/2111802:05 EPA625.1 Acenaphthylene NO ug1L 4.9 11/2111802:05 EPA 625.1 Anthracene NO ug1L 4.9 11/21/18 02:05 Page 1 of 6 Pace Analytical Services, LLG 14eAnalytical 6701 Conference Drive Raleigh, NC 27607 wwwpacelabs.car (919)834-4984 Page 2of3 Sample: OUTFALL 1 Lab ID: 92407733001 Collected: 11115118 12:25 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers EPA 625.1 Benzo(a)anthracene NO ug1L 4.9 11/21/18 02:05 EPA 625.1 Benzo(a)pyrene NO ug1L 4.9 11/21/18 02 05 EPA 525.1 Benzo(b)fluoranthene NO ug/L 4.9 11121/18 02:05 EPA 625.1 Benzo(g,h,i)perylene NO ug/L 4,9 11/21/1802:05 EPA 625.1 Benzo(k)flucranthene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 4-Bromophenylphenyl ether NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Butylbenzylphthalate ND ug1L 4.9 11/2111802:05 EPA 525.1 4-Chloro-3-methylphenol NO ug1L 4,9 11/21/18 02:05 EPA 625.1 bis(2-Chloroethoxy)methane NO ug1L 9.8 11/21/18 02:05 EPA625.1 bis(2-Chloroethyl) ether NO ug1L 4.9 11/21/18 02:05 EPA 625.i 2-Chloronaphthalene NO ug1L 4.9 11/2111802:05 EPA625.1 2-Chlorophenol NO ug1L 4.9 11/21/18 02:05 EPA 625.1 4-Chlorophenylphenyl ether NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Chrysene ND ug1L 4.9 11/21/18 02:05 EPA625.1 Dibenz(a,h)anthracene ND ug1L 4.9 11/2111802:05 EPA 625.1 3,3'-Dichlorobenzidine NO ug1L 24.5 11/2111802:05 EPA 625.1 2,4-Dichlorophenol NO ug1L 4.9 11/21/18 02:05 EPA 625.1 Diethylphth a late NO ug1L 4.9 11/21/18 02:05 EPA 625.1 2,4-Dimethylphenol NO ug1L 9.8 11/21/18 02:05 EPA 625.1 Dimethylp hth a late NO ug1L 4.9 1112111 B 02:05 EPA 625.1 Di-n-buyphthalate NO ug/L 4.9 11/21/18 02:05 EPA 625.1 4,6-Dinitro-2-methylphen ol NO ug/L 19.6 11/21/18 02:05 EPA 625.1 2,4-Dinitrophenol NO ug1L 49.0 11/2111802:05 EPA 625.1 2,4-Dinitrotoluene NO ug1L 4.9 11/21/18 02:05 EPA 625.1 216-Dinitrotoluene NO ug1L 4.9 11/2111802:05 EPA 625.1 Di-n-octylphthalate NO ug1L 4.9 11/21118 02:05 EPA 625.1 bis(2-Ethylhexy1)phthalate NO ug1L 4.9 11/21/18 02:05 EPA 625.1 Fluoranthene NO ug1L 4.9 11/21/18 02:05 EPA 625.1 Fluorene NO ug1L 4.9 11/21/18 02:05 EPA625A Hexachloro-1,3-butadiene NO ug1L 4.9 11/21/18 02:05 EPA 625.1 Hexachlorobenzene NO ug1L 4.9 11/21/18 02:05 EPA625.1 Hexachlorocyclopentadiene NO ug1L 9.8 11/21/18 02:05 EPA 625.1 Hexachloroethane ND ug1L 4.9 11/2111802:05 EPA 625.1 Indeno(1,2,3-cd)pyrene NO ug1L 4.9 11/21/18 02:05 EPA 625.1 Isophorone NO ug1L 9.8 11/21/18 02:05 EPA 625.1 Naphthalene NO ug1L 4.9 11/21/18 02:05 EPA 625.1 Nitrobenzene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 2-Nitrophenol NO ug1L 4.9 11/2111802:05 EPA 625.1 4-Nitrophenol NO ug/L 49.0 11/21/18 02:05 EPA 625.1 N-Nitrosodimethylamine NO ug/L 4.9 11/21/18 02:05 EPA 625.1 N-Nitroso-di-n-propylamine ND ug1L 4.9 11121/1802:05 EPA 625.1 N- N itrosod iphenyla mine NO ug/L 9.8 11/21/18 02:05 EPA 625.1 2,2'-Oxybis(1-chloropropane) NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Pentachlorophenol NO ug/L 9.8 11/21/18 02:05 EPA 625.1 Phenanthrene NO ug/L 4.9 11121/1802:05 EPA 625.1 Phenol ND ug/L 4.9 11/21/18 02:05 EPA 625.1 Pyrene NO ug1L 4.9 11/21/18 02:05 EPA 625.1 1,2,4-Trichlorobenzene NO ug1L 4.9 11/21/18 02:05 EPA 625.1 2,4,6-Trichlorophenol NO ug1L 9.8 11/21/18 02:05 EPA624.1 Benzene NO ug/L 2.0 11/2911810:56 EPA624.1 Bromodichloromethane NO ug1L 2.0 11/2911810:56 EPA 624.1 Bromoform NO uglL 2.0 11/29/1810:56 EPA624.1 Bromomethane NO ug1L 2.0 11/2911810:56 EPA624.1 Carbon tetrachloride NO ug1L 2.0 11/2911810:56 EPA624.1 Chiorobenzene NO ug1L 2.0 11/2911810:56 EPA624.1 Chloroethane NO ug/L 2.0 11/29/1810:56 EPA624.1 Chloroform NO ug/L 2.0 11/29/1810:56 EPA 624.1 Chloromethane NO ug/L 2.0 11/29/18 10:56 Page 2 of 6 _.aceAnalytical ..Pacelaf sS mn Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 3 of 3 Sample: QUTFALL 1 Method Parameters Lab ID: 92407733001 Collected: 11/15/18 12:25 Matrix: Results Units Report Limit Water Analyzed Qualifiers EPA624,1 Dibromochloromethane ND ug/L 2.0 11/29/1810:56 EPA624.1 1,2-Dichlorobenzene NO ug/L 2.0 11/29/1810:56 EPA624.1 1,3-Dichlorobenzene ND ug/L 2.0 11/29/1810:56 EPA624.1 1,4-Dichlorobenzene ND ug/L 2.0 11/2911810:56 EPA624.1 1,1-Dichloroethane ND ug/L 2.0 11/2911810:56 EPA624.1 1,2-Dichloroethane ND ug/L 2.0 11/2911810:56 EPA624.1 1, 1 -Dichloroethene NO ug/L 2.0 11129/1810:56 EPA624,1 cis- 1,2-Dichloroethene NO ug1L 2.0 11129/1810:56 EPA624.1 trans-1,2-Dichloroethene NO ug/L 2.0 11/29/1810:56 EPA624.1 1,2-Dichloropropane NO ug/L 2.0 11/29/1810:56 EPA624.1 cis-1,3-❑ichloropropene NO ug1L 2.0 11129/1810:56 EPA624.1 trans- 1,3-Dichloropropene NO ug/t_ 2.0 11/2911810:56 EPA624.1 Ethylbenzene NO ug/L 2.0 11/29/1810:56 EPA 624.1 Methylene Chloride NO u91L 2.0 11/29/18 10:56 EPA624.1 1,1,2,2-Tetrachloroethane NO ug/t_ 2.0 11/2911B 10:56 EPA 624.1 Tetra ch loroeth ene NO ug1L 2.0 11/29/18 10:56 EPA624.1 Toluene NO ug1L 2.0 11/29/1810:56 EPA 624.1 1.1,1-Trichloroethane NO ug1L 2.0 1112911810:56 EPA624.1 1,1,2-Trichloroethane NO ug1L 2.0 11/29/1610:56 EPA624.1 Trichloroethene ND ug/L 2.0 11/29/1810:56 EPA 624.1 Trichlorofluoromethane ND ug/L 2.0 11129/18 10:56 EPA624.1 Vinyl chloride ND ug1L 2.0 1V29/1810:56 SM 2540D-2011 Total Suspended Solids 28.9 mg1L 3.3 11/20/18 11:34 EPA 9040C pH at 25 Degrees C 5.3 Std. Units 0.10 11/18118 14:23 H3 EPA420.4 Rev 1.0 1993 Phenol NO mg/L 0.010 11/20118 17:22 SM 4500-CN-E-2011 Cyanide NO mg/L 0.0080 11/25/18 18:30 ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. Reviewed by: Cam--_ Chris Derouen (828)254-7176 christopher.derouen@pacelabs.com Charlotte Certification IDs 9800 KinceyAve. Ste 100, Huntersville, NC 28079 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 Page 3 of 6 I _ Docurneut Name: Document Revised: February 7, 2018 f Sample Condition Upon Etecei t(SCUR) Page 1 of 2 1" Document No.; issuing Authority.- _ - F-CAR•C5-b33:Rev.06 Pace carclingsQuaYty office �J Laboratory receiving samples; Asheville ❑ Eden❑ Greenwood FJ Huntersville ❑ Raleigh[] Mechanicsville[] . CiientName: I��O ' 914 0220 if ®733 • • � Project NJ' N)G'Wn �c1rl�l,r�C\ jj I� I 6 Cnurler: ❑Fed Ex ❑LIPS ❑LISPS ❑Client Commercial ❑Pace ❑other:_ llj 02407733 Custody Seal Present? ❑Yes Qa $oais intact? Fly's 29, patrJlaitlais Person Examining Contents: d -3h Packing Materlal: ❑Bubble Wrap rlBuhble Bags 'SVOnc ❑ othe, Biological Tissue �Frozen? []Yes ON- t`"/A Thermometer. Type of ice: iq�Ve[ ❑Blue ❑Nord ❑IRCunID:,�1?r.�1;5 Cooler Temp ('C): '-A A Correction Factor: Add/Subtract ('Ci lV ti _ Temp should be above freezing to b'C Cooler Temp Corrected (°C): `� ❑Samptesocrt of ,emnp criteria. Samplesnr, ica, roofing process lmas ielrun USDA Regulated Soil {['�-'HJA,watersample) Did samples oillg!npce in a yuorantine torte sti win the Un'ned Slates: CA, NY, or SC (check ma ps)? Old samples ar'bfnat_ frnrn a foreign source (into: r>Y,lonally, r]vd, fulG� !,A,A;-tt—Il nn,i Pi-ein Rlrnl7 i"IYes vll __ _�- _ �� GommentsfDtscrcpan_cy: µ-�- 1 hain of Custody P_rsent? - --- Yes !:)"') Samples Arrived withlo Hold T{rre? as E]No oo'A �N/A 1. - Shurt Hold Time Analysis (<72 hr.)? Ycs ❑Na — _ R�u•h_Turn _AroundTime Requasted? - - ]y- 5!���QN/A d. --- � 5. 6. Sufficient Volume? - Yes- _ ❑Nn N/A CnrectCuntainersUsed? V 'des ONO ©N/n _ -Pace Contaii iers Used? -- _— Yr_s [QNo G.N/A Containp.s lit ct ? Yes ❑hn_. NIA 7.-�_..,...... --- .,. �f)is_solvedanalysis: Samples Feld Flttrred? Nn - /,5 -._-...._-..__. S. _ 9. ��es Sample Labels Match CDC? r [��Yes ON'. L2.N/A ncludest7ate/ffine/ID/Anaycis Matrix Nead_space In VOA Vlals (>5-GmmJ? -µ R ^ oYes ❑pro C�N/A_ 10. "rip Blank present? ❑Yes [ jNo ©N/A Tl. rrl0Blank CwtadySails ?resart? r-Nn I-1Nn riNlA _ COMMENTS/SAMPLE DISCREPANCY CLIENT N0TIFICA1ION/RES0LUTtON Person Q mtactPd: Date/ Pme: Lot ID of solhconlainers: Proj"t Manager SCURF Review;- i j Project Manager SRF lleview: Fletdoata Required? I fYes ONO Page 4 of 6 ! 00tument Nanms: �� �k ��• Sample Condicfnn Upon Recei ' Document No,: F•CAR-CS-033-Remli `Check rnark top half of box if pH andlor dech€urination is verified andw(thin the acceptance range for preservation samples. Fxe.gUons VOA, Cofi}orm, TOC, oil and Grea,e, GIRO/8015 (water) DOC, Ugr 4'9attam half of box is to list numbor of battle Document Revfsed February 1, 2ma A(SCUR) Page 1 of 2 Issuing Authority: Pace Carolinas Quality Dfflce Project iYlllC,Il fV' X4I24107733 PM: COI Dtre Date: 12/04/18 CLIENT: 91-•141M, y 2 z a ti a N n i Z ry 1, 11II vv v 2 tt m v = ¢ 4 I O u o y o.15n. y° v y y r °^ 7 u ° ? 2 ., i Yi c a n. ti R a o n .a E ❑ 4 6 ¢ V. E w e1' d n n q d E d 1 Ln Q E € E E v I: w E E E gE C C C E p� G E N n P J 1 rf r. " N 1 at �i r, ti 0 7 .1 I Im Q a r a I m 4 n N m o l7 a a o a d �, i7 L" t7 0 m m m as a m s 4 d S d d d o ] 7 0 7 13 WS pH Adjustment log for Preserved Samples ample ro Iypc of ?r6s h zt3va p+t upan receipt pate prnserva t;na adjusted ilnie Preservation Amount n{ Peeservatly Lot g — adjusted �J added rlctn: Nheressr CAere IS a dlscrepzncy arfnCINg Nonh CaralL%A complla�Ce samples. a ::opY 0` tkls form WKI be tent to the Nnrth Caratjnq (16HNR Ce,t;r.Calien OMICC {Le. Page 5 of 6 to ��eAnaoical- Section A Raauaed Dicn: Irdorcatwc Section B Reauflcd ?Ini!d 1-Yormat�on: CHAIN-0F::.CUST0DY f Analyticai Request Document The Chrin-af-Cuyyody is a LEGAL :)DCUMENT. AR relevant Ii & must he cnmP7etec arc rz!c1}, Section C I— Imo+ -- Page: of zonwnrr A W North Carolina R=xr.T°:.y�sari�Y c3p�'► lm 1 �. V1i \ �nrn:or_ Accounts Payable - - 4c rests 4112 Did Oxford I lwy Cove To: C—XnyNam^ s- A W North Carolina REGULATORY AGENCY Durham, NC 27712 Addrn=: r NPDES GROUND WATER ORINKING WATER F` UST r RCRA OTH'_FZ Ema]Ta: daAdkanrtianen@awnc.com =urehwceOraerNa: -ace 0me Prior: 919.479-2243 Fax 919-47M955 Outran arse ?eelea Chris Derouen Sao L,oeation +tTnapnr, . �• STATE' Requested Due DaterTAT: rImpd M mber: Pac+ �.crfe a: Requested Anarysls:Flltered ff(N) "' Section 0 Valid L72r>Sx Coda 0a z 1 RM••4M ClwrlW - M— +�L°JL aaoe g COLLECTED 0 vx �v�'ER Vm u T'DYPQ$tr'': Gt7rrPO:7:E I' N KOWCr f'CO S ST0.9T FA WB SAMPLE lc WPE Jail JiR . >u 4 sumpfe 10,j MUST BE UNIDUE TmsIE m m Q U " J U " ( ` c9 - a �, 18. 4S N N O O }. V3 �J t� -+ V1iT �lQ r u`r CA TIRE Df TE PrAE n st 7 S Z Z rL a p a U ck ip F U cc Pa�eProject NoJ Lab I.D. i °- Z i YoiAr is=t NI I I I I I e to I k fir_ f I I A06RS64AL,COIddFENTSRELRSQ4!lSXE�_BY r_AFFRJATlON - ' -GATE " : 7WtE p �`ACCEPTEO SY l AFFRJATIQN' .- -: GATE - - 'TME'.:'. SAMPLE C.ONDn10NS 'zao Z0 SAMPL.ER.TiA_LIEA_NDS1_GFIAi[1RE -•' '., '^ - �;{�.- t - _ d �� .. - N - " � �_ t c 3 PRWT Name of SAMPLER_: t SIGMX76 E vt SAMPLER: -- Dare S:gned /fir ' C V N • ..- _ tLaw7Dma:_/1 e/i u _. .- .. ... -hn%zva Xce:6Yx7T�r+3 �hJC � yov am are;:rcy r7aee h$: 1J c:y V.Tpnerxterms ene aaree.rg'a Lse 7,m6e. d 7.SSC;,cl r-�:^sn rat arr inwara nc c+a:G nKh'a �, Cay:. .._ . � ...... .- .,, i=-ki_L-Q-026rev.92. 3 2-17=5-?.Oi:7 0 to - PROTECTED E H S Dept. i 12/21/18 Division of Water Quality Atten: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention DWQ Central Files Per our Stormwater permit (NCG030689), the following documents are enclosed: • Stormwater discharge monitoring report for outfall 1, 2, 3. + Analytical data from Pace Analytical from rain water samples outfall 1, 2, 3. Results show no over exceedance of parameters set in benchmarks. FYI- Our contact David Kannianen is no longer with the company thus resulting in the delay of the 30 day commitment to turn in monitoring report exceeded. K' a a i Lundy Safety/Fnviron mental Assistant Mgr. AWNC 4112 Old Oxford Rd. Durham N.C. 27712 919 452-3958 RECJF�j V iEF,�qN 02 2019 � cE?V ri. DwR EC -ripe 1� MONT" CAROLINA Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted / Z - Z / - IS. CERTIFICATE OF COVERAGE NO. NCG03 0 6 8 9 FACILITY NAME AWNC COUNTY Durham PERSON COLLECTING SAMPLES Hakim Lundy LABORATORY PACE Analytical Lab Cert. # 12 Comments on sample collection or analysis: Outfall No. 1 Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD Jan -June 0 July -Dec or 0 Monthly' (month j DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply [:]SA ❑Other Retention Pond release to Neuse River PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches' Total Suspended Solids pH, Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organicss Benchmarks _ - 100 mg/L or 50 mg/O 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141 11/15/18 10.37inches 28.9 mg/L 5.3 ND ND 0.0102 ND N/A ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. a See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. $ Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40.CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Hakim Lundy Name (Print name) Assistant Mgr. Safety Environmental Titl int title) iZ-I1—r, ignature Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format "<XX m L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches New Motor oil or Hydraulic oil Usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L° Parameter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original copy_ o�this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant pea2W_U for submitting false information, including the possibility of fines and imprisonment for knowing violations." re of Perm l2 Date Permit Date:11/1/2018-05/31/2021 SWU-24S, last revised 11/1/2018 Page 3 of 3 Pace Analytical Services, LLC 6701 Conference Drive laceAnalytical Raleigh, NC 27607 www.pacefabs.com (919 )834-4984 Page 1 of 3 Laboratory Report Hakim Lundy Report Date: 11/30/2018 A W North Carolina Date Received: 11/16/2018 4112 Old Oxford Highwy Durham, NC 27712 Project: SW OUTFALL 1 11115 Pace Project No.: 92407733 Sample: OUTFALL 1 Method Lab ID: 92407733001 Collected: 11/15/18 12:25 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers EPA 1664E Oil and Grease NO mgIL 5.0 11/30/18 05:53 EPA 16646 Total Petroleum Hydrocarbons NO mg/L 5.0 11/30/18 05:53 EPA 608.3 Aldrin NO ug/L 0.050 11/27/1817:18 EPA 608.3 alpha-BHC NO ug/L 0.050 11/27/18 17:18 EPA 608.3 beta-BHC NO ug/L 0.050 11/27/1817:18 EPA 608.3 delta-BHC NO ug/L 0.050 11/27/18 17:18 EPA 608.3 gamma-BHC (Lindane) ND ug1L 0.050 11/27/18 17:18 EPA 608.3 Chlordane( Technical) NO ug/L 0.50 11/2711817:18 EPA 608.3 alpha -Chlordane ND ug/L 0.050 11/2711817:18 EPA 608.3 gamma -Chlordane NO ug/L 0.050 11/27/18 17:18 EPA608.3 4,4'-DDD NO ug/L 0.050 11/2711817:18 EPA 608.3 4,4'-DDE NO ug/L 0.050 11/27/1817:18 EPA 608.3 4,4'-DDT NO ug/L 0.050 11/27/1817:18 EPA 608.3 Dieldrin NO ug/L 0.050 11/27/1817A8 EPA608.3 Endosulfan I NO ug/L 0.050 11/27/1817:18 EPA 608.3 Endosulfan II NO ug/L 0.050 11/2711817:18 EPA 608.3 Endosutfan sulfate ND ug/L 0.050 11/27/18 17:18 EPA608.3 Endrin NO ug/L 0,050 11127/1817:18 EPA 608.3 Endrin aldehyde ND ug/L 0.050 11/27/18 17:18 EPA 608.3 Heptachlor ND ug/L 0.050 11/27/18 17:18 EPA 608.3 Heptachlor epoxide NO ug/L 0.050 11 /27/18 17:18 EPA 608.3 PCB-1016 (Aroclor 1016) ND ug/L 0.50 11/27/18 17:18 EPA 608.3 PCB-1221 (Aroclor 1221) NO ug/L 0.50 11/27/1817:18 EPA 608.3 PCB-1232 (Aroclor 1232) ND ug1L 0.50 11/2711817:18 EPA 608.3 PCB-1242 (Aroclor 1242) NO ug1L 0.50 11/2711817:18 EPA 608.3 PCB-1248 (Arodor 1248) ND ugtL 0.50 11/27/18 17:18 EPA 608.3 PCB-1254 (Arodor 1254) ND ug/L 0.50 11/27/18 17:18 EPA 608.3 PCB-1260 (Aroclor 1260) NO ug/L 0,50 11/27/18 17:18 EPA 608.3 Toxaphene NO ug/L 0.50 11/2711817:18 EPA 8082A PCB-1016 (Aroclor 1016) NO ug/L 0,50 11/20/18 11:25 EPA 8082A PCB-1221 (Aroclor 1221) NO ug/L 0.50 11/20/18 11:25 EPA 8082A PCB-1232 (Aroclor 1232) NO ug/L 0.50 11/20/18 11:25 EPA 8082A PCB-1242 (Aroclor 1242) NO ug/L 0,50 11/20/18 11;25 EPA 8082A PCB-1248 (Arodor 1248) NO ug/L 0.50 11120/18 11:25 EPA 8082A PCB-1254 (Aroclor 1254) NO ug/L 0,50 11/20/18 11:25 EPA 8082A PCB-1260 (Aroclor 1260) NO ug/L 0.50 11/20/18 11:25 EPA 200.7 Rev 4.4 1994 Copper NO ug/L 5.0 11/20/18 02:37 EPA 200.7 Rev 4.4 1994 Lead NO ug/L 5.0 11/20/18 02:37 EPA 200.7 Rev 4.4 1994 Zinc 10.2 ug& 10.0 11/20/18 02:37 EPA 625.1 Acenaphthene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Acenaphthylene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Anthracene NO ug/L 4.9 11/21/18 02:05 Page 1 of 6 ® aceAnalytical www.pacetabs.com Pace Analytical Services, LLC 6701 Conference Drive RaEeigh, NC 27607 (919)834-4984 Page 2 of 3 Sample: OUTFALL 1 Lab 1i7: 92407733001 Collected: 11/15/18 12:25 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers EPA 625.1 Benzo(a)anlhracene ND ug/L 4.9 11/21/1802:05 EPA 625.1 Benzo(a)pyrene ND ug/L 4.9 11/21/1802:05 EPA 625.1 Benzo(b)fluoranthene NO ug/L 4.9 11/21/1802:05 EPA 625.1 Benzo(g,h,i)perylene NO ug/L 4.9 11/21/1802:05 EPA 625.1 Benzo(k)fiuoranthene NO ug/L 4.9 11/21/1802:05 EPA 625.1 4-Bromophenylphenyl ether NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Butylbenzylphthalate NO ug/L 4.9 11/2111802:05 EPA 625.1 4-Chloro-3-methylphenol NO ug/L 4.9 11/21/18 02:05 EPA 625.1 bis(2-Chloroethoxy)methane NO ug/L 9.8 11/21/18 02:05 EPA 625.1 bis(2-Chloroethyl) ether NO ug/L 4.9 11/21/18 02:05 EPA 625.1 2-Chloron2phthalene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 2-Chlorophenol NO ug/L 4.9 11/21/18 02:05 EPA 625.1 4-Chlorophenylphenyl ether NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Chrysene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Dibenz(a,h)anth racene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 3,3'-Dichlorobenzidine NO ug/L 24.5 11/21/18 02:05 EPA625A 2,4-Dichlorophenol NO ug/L 4.9 11/21/1802:05 EPA 625.1 Diethylphtha late NO ug/L 4,9 11/21/18 02:05 EPA 625.1 2,4-Dimethyl phenol NO ug/L 9.8 11/21/18 02:05 EPA 625.1 Dimethylphthalate NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Di-n-butylphthalate NO ug/L 4.9 11/21/1802:05 EPA 625.1 4,6-Dinitro-2-methylphenol NO ug/L 19.6 11/21/18 02:05 EPA 625.1 2,4-Dinitrophenol NO ug/L 49.0 11/21/18 02:05 EPA 625A 2,4-Dinitrotoluene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 2,6-Dinitrotoluene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Di-n-octylphthalate NO ug/L 4.9 11/21/18 02:05 EPA 625.1 bis(2-E thyl hexyl)phthalate NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Fluoranthene NO ug/L 4.9 11/21/1802:05 EPA 625.1 Fluorene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Hexachloro-1,3-butadiene NO ug/L 4.9 11/21/1802:05 EPA 625.1 Hexachlorobenzene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Hexachlorocyclopentad iene NO ug/L 9.8 11/21/18 02:05 EPA 625.1 Hexachloroethane NO ug/L 4.9 11/2111802:05 EPA625A Indeno(1,2,3-cd)pyrene NO ug/L 4.9 1112111802:05 EPA 625.1 Isophorone NO ug/L 9.8 11/21/18 02:05 EPA 625.1 Naphthalene NO ug/L 4.9 11/21/18 02:05 EPA625A Nitrobenzene NO ug/L 4.9 11/21/1802:05 EPA 625.1 2-Nitrophenol NO ug/L 4.9 11/21/18 02:05 EPA 625.1 4-Nitrophenol NO ug/L 49.0 11/21/18 02:05 EPA 625.1 N-Nitrosodimethylamine NO uglL 4.9 11/21/1802:05 EPA 625.1 N-Nitroso-di-n-propylamine NO uglL 4.9 1112111802:05 EPA 625.1 N-Nitrosodiphenylamine NO uglL 9.8 11121/1802:D5 EPA 625.1 2,2'-Oxybis(1-chloropropane) NO uglL 4.9 11/2111802:05 EPA 625.1 Pentachlorophenol NO ug/L 9.8 11/21/18 02:05 EPA 625.1 Phenanthrene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Phenol NO ug1L 4.9 11/2111802:05 EPA 625.1 Pyrene NO ug/L 4.9 11/21/1802:05 EPA 625.1 1,2,4-Trichlorobenzene NO uglL 4.9 11/21/1802:05 EPA 625.1 2,4,6-Trichlorophenol NO uglL 9.8 11/21/18 02:05 EPA 624.1 Benzene NO ug/L 2.0 11/29/1810:56 EPA 624.1 Bromodichloromethane NO uglL 2.0 11/29/18 10:56 EPA 624.1 Bromoform NO ug/L 2.0 11/29/18 10:56 EPA 624.1 Bromomethane NO ug/L 2.0 11/2911810:56 EPA 624.1 Carbon tetrachloride NO ug/L 2.0 11/29/1810:56 EPA 624.1 Chlorobenzene NO ug/L 2.0 11/2911810:56 EPA 624.1 Chloroethane NO uglL 2.0 11/29/1810:56 EPA 624.1 Chloroform NO ug/L 2.0 11/29/18 10:56 EPA 624.1 Chloromethane NO uglL 2.0 11/29/18 10:56 Page 2 of 6 aceAnalytrcal wwwpacelabs.com Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: OUTFALL 1 Lab ID: 92407733001 Collected: 11/15/18 12:25 Matrix: Water Method Parameters Results Units Report Limit EPA 624.1 Dibromochloromethane ND ug/L 2.0 EPA 624.1 1,2-Dichlorobenzene ND ug/L 2.0 EPA 624.1 1,3-Dichlorobenzene ND ug/L 2.0 EPA 624.1 1,4-Dichlorobenzene ND ug/L 2.0 EPA 624.1 1,1-Dichloroethane ND ug/L 2.0 EPA624.1 1,2-D'rchloroethane ND ug/L 2.0 EPA 624.1 1,1-Dichloroethene ND ug/L 2.0 EPA 624.1 cis-1,2-Dichloroethene ND ug/L 2.0 EPA 624.1 trans-1,2-Dichloroethene ND ug/L 2.0 EPA 624.1 1,2-Dichloropropane ND ug/L 2.0 EPA 624.1 cis-1,3-Dichloropropene ND ug/L 2.0 EPA 624.1 trans-1,3-Dichloropropene ND ug/L 2.0 EPA 624.1 Ethylbenzene ND ug/L 2.0 EPA 624.1 Methylene Chloride ND ug/L 2.0 EPA 624.1 1,1,2,2-Tetrachloroethane ND ug/L 2.0 EPA 624.1 Tetrachloroethene ND ug/L 2.0 EPA 624.1 Toluene ND ug/L 2.0 EPA 624.1 1. 1, 1 -Trichloroethane ND ug/L 2.0 EPA 624.1 1,1,2-Trichloroethane ND ug/L 2.0 EPA 624.1 Trichloroethene ND ug/L 2.0 EPA 624.1 Tri chlorofluo ro methane ND ug/L 2.0 EPA 624.1 Vinyl chloride ND ug/L 2.0 SM 254OD-2011 Total Suspended Solids 28.9 mg/L 3.3 EPA 9040C pH at 25 Degrees C 5.3 Std. Units 0.10 EPA 420.4 Rev 1.0 1993 Phenol ND mg/L 0.010 SM 4500-CN-E-2011 Cyanide ND mg/L 0,0080 ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. Reviewed by: Chris Derouen (828)254-7176 christopher.derouen@pacelabs.com Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiafVELAP Certification #: 460222 Analyzed 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11/29/18 10:56 11 /20118 11:34 11/18/18 14:23 11/20/18 17:22 11/25/18 18:30 H3 Page 3 of 3 Qualifiers Page 3 of 6 i Document Name: Document Revised: February 7, 2018 26kWyUcal' _Sample Condition Upon Recefpt(SCUR) Page 1 of 2 ._ Document No.: F•CAR-CS-033-Rev.06 ) Issuing Authority: Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicsville[] Client Name: f `,�� f �d` 4C, 7 03 • • Projact 191H�e Caurfer. []Fed Ex EJUPS ❑USPS ❑Client Cl Commercial ❑Pace QOther:� u jD (� 11 11 199 kkll 1 02407733 Custody. Seal Present? ❑Yes [moo Seals Intact? []Yes 26o. pate/initlals Person Eaaminirg Contents: d �S5 Packing Material: ❑Bubble Wrap ❑Rubble bags one ❑ other Biological Tissue Frozen? Thermometer. (]Yes []No EWA ❑ IF Gun ID: flk-f" S YYpe of Ice:t ❑Blue ❑Nary i 1 Cooler Temp ('C): �-A A Correction Factor: Add/Subtract ('C) , V • 1 — Temp snouid be aEave f[eezing to fi'C Cooler Temp Corrected ('C): (3Sarnptes out of temp crreda. Samples ar. ke, cooling process USDA Regulated Soil { N/A watersample) his 5ecur. Did samples orlg:n to In a quasantlne zone w€t5in the United States: CA, NY, or SC (check maps)? old samples or$Ifsate from a foreign source (ante: Onally r-1V.1 L, A..A:..O.....s, sea D—An obeli f TY►s lKwo Comments plscrcpancy: Cha a otCustody Prrsrnt? Yes ❑Nn QNIA 1. Samples Arrived within Hold Tme? es �Nc NIA Short Hold Time Anal sis (02 hr.)? Yes ONO ❑rVA 3. Rush Turn Around Time Requested? �� ❑Ycs o ❑NIA 4. SufFlcient Valume? Correct Containers Used? -Pace Containers Used? cs es Yra Q24 ❑NIA _ ONO .QN/A EINO NIA S. _ 6. Containers Intact? yeS ONO N/A 7. Dissolved anal Is: Samples Held Filtered? — w Yin No /A 8. Sample labels Match CDC? es Otto -includes 0ate/Tlme/ID/An2,'yS1s MatfL)L ­161� []NIA 9. Veadspace In VOA vials >5.6mm)? aes QN0 Q.NIA 10. Trip Blank Present? r__ r P Blank Custody Seals Present? ❑Yes ❑Yes_ _ []No ❑No ❑N/A NIA 11. _ COMMENTS/SAMPLE DISCREPANCY Lot ID of sort conlainefs: CLIENT NOTIFICATION/RESOLUTION Person contacted: T Date/Tine: Pro)ert,Managar SCURF Review: Project Manager SRF Review: Field oat,Rcquired? ❑Yes ❑No Date: Date *0- Page 4 of 6 Document Nome: �f Sample condit[ llpan Rea �c�Ara�ytl�� Document No.: F-CAR-CW33-Rev.0 'Check mark top half of box if pH and/or dechlorination Is verified and within the acceptance range For preservation samples, Fxcepuorw VOA, C95fa m, roc, Oa and Grease, DRO/8015 lvrnterj DOC, Ug "Elattam halt of box Is to list number of bottle Dacurnent RwAsed: >+ebmary 1, 2018 Page l of 2 Issuing Authority: Pace Carolinas Oual'tty Dfftce Project ii,,ii fl - COM'177142 PM: COI Due. Date: 12/04/18 CLIENT: 91-4114 fit,' zz L X z z ? z_ z C1 D z ryrt a = x d Q a A n � n^ is 9 d ' .� '� � 4� � � $ x✓ � y � ,?`� <. a�. l'�3 Z „ � $ � _ a c n c ix O z° = I , vn gl o a ? Y m in s1 N $ y C 7 7 7 r. u 1 u = V eJ Z yu v IU r 7 t X , R L = Y �1 /� Z z P a a 7 os. v s V Z . A ZCL fl a nEE 4 pa A ° :t 4 f a a a .ai E d u i 7 E > E E 7 E 5 e c GE 3 ^ .+ � y .:r z ru'v .r o r"j. 10 O S i � g :°• g l � '.� n � $ '�' T E a a N M a z mWi N d u 0 a ''t l� C9 la o A H 8 m d a t 4 4 Q r Q O 7 7 O } } s,t rn As d 7 t +V 31 L . I I l U T2 pH Adjustment log for Preserved Samples Sample ID Type or Preservatve pH upon recelpt Date preservation adjusted Sirra preservation A.•nount or Preservative lot Y adjusted added r I I Reter Whenever t`.ere Is a dtscrepancy arfecring Nanh Carollnv torepllance samples, a cnpY a° this (amt wM ba sort to the North Csrorine peHNR CertTrcation Oniea (Le. Page 5 of 6 tD ace Analytical - Section A Reauked rb—i ire— , "a - — - " Section S Rowl•*d Pmgft= tonne� CHAIN -OF -CUSTODY I Analyticai Request Document The Crem -Cas adyksa LEGAL DOCUMENT. AArekvardl '' nwstbeuwnpkledaocurrildy. Section C � 1�- _r -- lpage: of I con�+y', A 1,V Nona Caru0na Reper. To: Ail— A=m;n:s payatAe Andrew: 4112 Old Oxford I twy Copy To CwnMV NA- A W NoM Carolina REGULATORY AGENCY Ourham, NC 2T712 Ad**n: F NPDES r-. GROt.)ND, WATER F DRINKING WATER r7. UST 17. RCRA r- OTHER Emil To. davidkanrtianen@awnc.com fie!: Pr.r.e: 919-479-2243 F— 919-479-8955 I Proied hla—� outran I PP*d Chris De=en ubrlq— Loc . allon �, 5�� STATE. Requeslad Due 0-1enAT. ".rA*r. Pau "C"le a, • RequeSted Ana Is: Fiftered. (Y(N Section D Vafid WIrk COCICS !P' W C�", ve_euor, COLLECTED Preservarives r: J51 DRNKP4 WArFX ow 2 sm vm 70k VM cohOM-1c 0 I= 0 r 57XTr c.M1avr Q? OL Z to SAMPLE 0 tWE An Alk w m(A-Z, 0-0 1.-1 utmi, OT Uj F' z Sommp�e IDs MUST BE UNIQUE IMPAX. Ts 0 X to -0 C, CL 0 z X ]= I M-7-7 3 �k. OUA44 JE , 9 DATE TIME CAM n-AF I x z z 2 Z5 3 Cv C:, 12 rojecthlaJLab I.D. I G 106 kno MIS as izi Oo C;1 1XI I I r; :7,w. v 6N �msk Ni 11 1 A I I I I I �­RE f AFFILIATtM. UNQUISHIM I!a DATE':`" Z��6EPTED8Wi A �T[iAF'�_, S"PtE MNDffKW4 L) PRINT Nam 4d SAMPLER •'X 9 _6 E DATE S4fwkd IA- Mwmyyy): L) 0 E0 .� f�. � V�! PROTECTED Dept. 12/21/18 Division of Water Quality Atten: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention DWQ Central Files Per our Stormwater permit (NCG030689), the following documents are enclosed: e Stormwater discharge monitoring report for outfall 1, 2, 3. Analytical data from Pace Analytical from rain water samples outfall 1, 2, 3. Results show no over exceedance of parameters set in benchmarks. FYI- Our contact David Kannianen is no longer with the company thus resulting in the delay of the 30 day commitment to turn in monitoring report exceeded. K'nd-Regards Hake ,Lundy' r��•' r Safety/Environmental Assistant Mgr. AWNC 4112 Old Oxford Rd. Durham N'.C. 27712 919 452-3958 1'�L U NORT1, OAROLMA • Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted / Z - Z / -- /,S� CERTIFICATE OF COVERAGE NO. NCG03 0 6 8 9 FACILITY NAME AWNC COUNTY burham PERSON COLLECTING SAMPLES Hakim Lundy LABORATORY PACE Analytical Lab Cert. # 12 Comments on sample collection or analysis: Outfall No. 1 Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD 0 Jan -June July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply [:]SA 00then Retention Pond release to Neuse River PLEASE.REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -> ❑ No discharge this period?z outfall.No. -• - Date Sample Collected1 (mo/dd/yr) 24-hour rainfall amount, . Inches Total Suspended Solids pH, Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic OrganicsS. Benchmarks' - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter;Code 46529 C0530 00400 01119 01051 01094 00552 78141 11/15/18 10.37inches 28.9 mg/L 5.3 ND ND 0.0102 ND N/A 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General.Permit, Section 8, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the: requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31)_ Permit Date: 11/1/2018-05/31/2021 5WU-245, last revised 11/1/2018 Page 1 of 3. Facilities that incorporate a solvent management plan into the 5tormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan Shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the 5tormwater Pollution Prevention Plan." Hakim Lundy Name (Print name) Assistant Mgr. Safety Environmental Title int title} j ignature iL-IL --fk, Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall Na. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/0 Parameter Code - 45529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 5WU-245, last revised 11/1/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS. • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE.SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES 0 NO El 1F YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES 0 NO 0 REGIONAL OFFICE CONTACT NAME: Mail an original copy of this DMR includingall "No Discharge" reports, within 30 days of receipt of the lab results or at end of manitorin period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27G99-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate,: and complete. t am aware that there are significant penalties for submitting false information, including the possibility of.€fines and imprisonment for knowing violations." re of Perm Permit Date:11/1/2D18-05/31/2021 t 2 Date SWU-245, last revised 11/1/2018 Page 3 of 3 5 Nace Analytical services, LLc 6701 Conference Drive i aceAnalytical Raleigh, NC 27607 / w.tiv�acefabs cam � (9 i 0)A34-4964 Page 1 of 3 Laboratory Report Hakim Lundy Report Date: 11/30/2018 A W North Carolina Date Received: 11/16/2018 4112 Old Oxford Highwy Durham, NC 27712 Project: SW OUTFALL 1 11115 Pace Project No.: 92407733 Sample: OUTFALL 1 Method Lab ID: Parameters 92407733001 Collected: 11/15/18 12:25 Matrix: Results Units Report Limit Water Analyzed Qualifiers EPA 1664B Oil and Grease ND mg/L 5.0 11/30118 05:53 EPA 1664B ToW Petroleum Hydrocarbons ND mg/L 5.0 11130/18 05:53 EPA 608.3 Aldrin NO ug1L 0,050 11127/18 17:18 EPA608.3 alpha-BHC ND ug/l_ 0.050 11/2711817:18 EPA 608.3 beta-BHC ND ug1L 0.050 11/27/18 17:18 EPA608.3 delta-BHC NO ug1L 0.050 11127/1817:18 EPA608.3 gamma-BHC (Lindane) ND ug/L 0,050 11/27/18 17:18 EPA608.3 Chlordane (Technical) NO ug/L 0.50 11/27/18 17:18 EPA 608.3 alpha -Chlordane ND ug/L 0.050 11/27/18 17:18 EPA608.3 gamma -Chlordane NO ug/L 0.050 11/27/18 17:18 EPA608.3 4.4'-DDD ND ug/L O,050 11/2711817:18 EPA608.3 4.4'-DDE NO ug1L 0.050 11/27/18 17:18 EPA608.3 4.4'-DDT NO ug/L 0.050 11/27/1817:18 EPA608.3 Dieldrin NO ug/L 0.050 1112711817:18 EPA 608.3 Endosulfan I NO ug/L 0.050 11/27/18 17:18 EPA608.3 Endosulfan II NO uglL 0.050 11/27/18 17:18 EPA608.3 Endosulfan sulfate NO ug1L 0.050 11/27118 17:18 EPA608.3 Endrin ND uglL 0.050 11/27/18 17:18 EPA 608.3 Endrin aldehyde NO ug/L 0.050 11/27118 17:18 EPA608.3 Heptachlor ND ug1L 0.050 11/27/18 17:18 EPA608.3 Heptachlor epoxide ND ug/L 0.050 11/27/1817:18 EPA 608.3 PCB-1016 (Aroclor 1016) ND ug1L 0.50 11/27/18 17:18 EPA 608.3 PCB-1221 (Aroclor 1221) NO ug/L 0.50 11/27/18 17:18 EPA 608.3 PCB-1232 (Aroclor 1232) NO ug/L 0.50 11/27/18 17:18 EPA 608.3 PCB-1242 (Aroclor 1242) NO ug/L 0.50 11/27/18 17:18 EPA608.3 PCB-1248 (Aroclor 1248) ND ug/L 0.50 11/27/18 WAB EPA 608.3 PCB-1254 (Aroclor 1254) ND ug/L 0.50 11/27/18 17:18 EPA 608.3 PCB-1260 (Aroclor 1260) ND ug/L 0.50 1112708 17:18 EPA608.3 Toxaphene ND ug/L 0,50 11/2711817:18 EPA8082A PCB-1016 (Aroclor 1016) ND ug/L 0.50 11/20/18 11:25 EPA 8082A PCB-1221 (Aroclor 1221) NO ug/L 0.50 11/20118 11:25 EPA 8082A PCB-1232 (Aroclor 1232) NO ug/L 0,50 11/20/18 11:25 EPA8082A PCB-1242 (Aroclor 1242) NO ug/L 0.50 11/20/18 11:25 EPA8082A PCB-1248 (Aroclor 1248) NO ug1L 0.50 11/20/i811:25 EPA 8082A PCB-1254 (Aroclor 1254) NO ug1L 0.50 11/20/18 11:25 EPA8082A PCB-1260 (Aroclor 1260) ND ug/L 0.50 11120/18 11:25 EPA 200.7 Rev 4.4 1994 Copper NO ug/L 5.0 11/20/18 02:37 EPA200.7 Rev A 1994 Lead No ug,L 5.0 11/20/1802:37 EPA 200.7 Rev 4.4 1994 Zinc 10.2 ug/L 10.0 11/20/18 02:37 EPA625.1 Acenaphthene ND ug/L 4.9 11121/1802:05 EPA 625.1 Acenaphtiiylene NO ug/L 4.9 11121/18 02:05 EPA 625.1 Anthracene NO ug1L 4.9 11/21/18 02:05 Page 1 of 6 r� �� aceAnalylcal wmv.pacelobs. ccm 1 i Pace analytical Services, LLC 6701 Conference Drive Raleigh, NC 276D7 (919)834-4984 Page 2 of 3 Sample: OUTFALL 1 Method Lab ID: 92407733001 Parameters Results Collected:' 11/15118 12:25 Matrix: Units Report Limit Water Analyzed Qualifiers EPA 625.1 Benzo(a)anthracene NO ug/L 4,9 11/21/18 02:05 EPA 625.1 Benzo(a)pyrene NO ug/L 4.9 11/21118 02:05 EPA 625.1 Benzo(b)fluoranthene NO uglL 4.9 11/21118 02:05 EPA 625.1 Benzo(g,h,i)perylene NO ug/L 4.9 11121118 02:05 EPA 625.1 Benzo(k)ftuoranthene NO ug/L 4.9 11/21/18 02:05 EPA625,1 4-Bromophenylphenylether NO ug/L 4.9 11/2111802:05 EPA 625.1 Butylbenzylphthatate ND ug/L 4.9 11)21/1802:05 EPA 625.1 4-Chloro-3-methylphenot NO ug/L 4.9 11/21/18 02:05 EPA 625.1 bis(2-Chloroethoxy)methane ND ug/L 9.8 11121/18 02:05 EPA 625.1 bis(2-Chtoroethyl) ether ND ug/L 4.9 11/21/18 02:05 EPA 625.1 2-Chioronaphthalene ND ug/L 4.9 11/21/18 02:05 EPA 625.1 2-Chtorophenol ND ug/L 4.9 11/21/18 02:05 EPA 625.1 4-Chlorophenylphenylether NO uglL 4.9 11/21/18 02:05 EPA 625.1 Chrysene ND ug/L 4.9 11/21/18 02:05 EPA 625.1 Oibenz(a,h)anthracene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 33-Dichlorobenzidine NO ug1L 24.5 '11121/18 02:05 EPA 625.1 2,4-Dichlorophenol NO uglL 4.9 11/21/18 02:05 EPA 625.1 Diethylphthalate ND ug/L 4.9 11/21/1802:05 EPA 625.1 2,4-Dimethylphenol ND uglL 9.8 11121/18 02:05 EPA 625.1 Dimethylphtha late Nil ug/L 4.9 11/21/18 02:05 EPA 625.1 Di-n-butylphthalate NO ug/L 4.9 11/21/18 02:05 EPA 625.1 4,6-Dinitro-2-methylphenoi NO ug/L 19.6 11/21/18 02:05 EPA 625.1 2,4-Dinitrophenol ND ug/L 49.0 11/21/18 02:05 EPA 625.1 2,4-DWtrotoiuene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 2,6-Dinitrotoluene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Di-n-octylphthalate NO ug1L 4.9 11/21/18 02:05 EPA 625.1 bis(2-Ethylhexyl)phthalate NO ug1L 4.9 11/21/18 02:05 EPA 625.1 Fluoranthene NO ug/L 4.9 11/21/18 02:05 EPA625,1 Fluorene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Hexachloro-1,3-butadiene ND ug/L 4.9 11/21/18 02:05 EPA 625.1 Hexachlorobenzene ND ug/L 4.9 11/21118 02:05 EPA 625.1 Hexachlorocyclopentadiene NO ug/L 9.8 11/21/18 02:05 EPA 625.1 Hexachloroethane NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Indeno(1,2,3-cd)pyrene NO ug/L 4.9 11121/18 02:05 EPA625,1 Isophorone NO ug/L 9.8 11/21/18 02:05 EPA 625.1 Naphthalene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Nitrobenzene NO ug/L 4.9 11121/18 02:05 EPA 625,1 2-Nitrophenol NO ug/L 4.9 11/21/18 02:05 EPA 625.1 4-Nitrophenol ND ug/L 49.0 11/21/1802:05 EPA 625.1 N-Nitrosodimethylamine NO ug/L 4.9 11/21118 02:05 EPA 625.1 N-Nitroso-di-n-propylamine ND ug/L 4.9 11/21/18 02.05 EPA625.1 N-Nitrosod iphenyla mine NO ug/L 9.8 11/21118 02:05 EPA625.1 2,2'-Oxybis(1-chloropropane) ND ug/L 4.9 11/21118 02:05 EPA 625.1 Pentachlorophenot ND ug/L 9.8 11/21/18 02:05 EPA 625.1 Phenanthrene NO ug/L 4.9 11/21/18 02:05 EPA 625.1 Phenol NO ug/L 4.9• 11/21/18 02:05 EPA 625.1 Pyrene ND uglL 4.9 11)21/1802:05 EPA 625.1 1,2,4-T6chlorobenzene NO ug/L 4.9 11/21/18 02:05 EPA625.1 2,4,6-Trichlorophenol NO ug/L 9.8 1112111802:05 EPA624.1 Benzene NO ug/L 2.0 11/2911810.56 EPA 624.1 Bromodichloromethane NO ug/L 2.0 1112911810:56 EPA 624.1 Bromoform NO ug/L 2.0 11/29/18 10:56 EPA 624.1 Bromomethane NO uglL 2.0 11/29/1810:56 EPA 624.1 Carbon tetrachloride NO uo/L 2.0 11/29/18 10:56 EPA 624.1 Chlorobenzene NO ug/L 2.0 11/29/18 10:56 EPA 624.1 Chloroethane NO ug/L 2.0 11/29f1810:56 EPA 624.1 Chloroform NO ug/L 2.0 11129/18 10:56 EPA 624.1 Chloromethane ND uglL 2.0 11/29/13 10:56 Page 2 of 5 /�paceAnalyticaI� �' vrvw.pacelabs.ccm Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 ;919i834-4984 Sample: DUTFALL 1 Lab It]: 92407733001 Collected: 11/15118 12:25 Iviatrix: Water Method Parameters Results Units EPA 624.1 Dibromochloromethane ND uglL EPA 624.1 1,2-Dichlorobenzene NO uglL EPA624,1 1.3-Dichlorobenzene NO ug/L EPA624,1 1,4-Dichlorobenzene NO ug/L EPA 624.1 1,1-Dichloroethane NO ug/L EPA 624.1 1,2-Dichloroethane ND ug/L EPA 624.1 1,1-Dichloroethene ND ug/L EPA 624.1 cis-1,2-Dichloroethene ND ug/L EPA 624.1 trans-1.2-Dichloroethene NO ug/L EPA 624.1 1,2-Dichloropropane ND ug/L EPA 624.1 cis-1,3-DicNoropropene NO ug/L EPA 624.1 trans- 1,3-Dichloropropene NO ug/L EPA 624.1 Ethylbenzere NO ug/L EPA 624.1 Methylene Chloride NO ug/L EPA 624.1 1,1,2,2-Tetrachloroethane NO ug/L EPA624,1 Tetrachloroethene NO ug/L EPA 624.1 Toluene ND ug/L EPA 624.1 1,1,1-Trichloroethane ND ug1L EPA 624.1 1,1,2-Trichloroethane ND ug/L EPA 624.1 Trichloroethane ND ug/L EPA 624.1 Trichloroflueromethan e ND ug/L EPA 624.1 Vinyl chloride ND ug/L SM 25400-2011 Total Suspended Solids 28.9 mg1L EPA 9040C pH at 25 Degrees C 5.3 Std, Units EPA420A Rev 1.0 1993 Phenol ND mg/L SM 4500-CN-E-2011 Cyanide NO mg/L ANALYTE QUALIFIERS Page 3 of 3 Report Limit Analyzed Qualifiers 2.0 11/29/18 10:56 2.0 11/29/18 10:56 2.0 11/29/18 10:56 2.0 1 V2911 B 10:56 2.0 11/29/18 10:5G 2.0 11/29/18 10:56 2.0 11/29/18 10:56 2.0 11 /29/ 18 10:56 2.0 11/29/18 10:56 2.0 11/29/18 10:56 2.0 11/29/18 1 D:56 2.0 11/29/18 10:56 2.0 11129/18 10:56 2.0 11/29118 10:56 2.0 11/29/18 10:56 2.0 11129/18 10:56 2.0 11/29118 10:56 2.0 11/29/18 10:56 2.0 11/29/18 10:56 2.0 11/29118 10:56 2.0 11/29118 10:56 2.0 11/29/18 10:56 3.3 11/20/18 11:34 0.10 11/18/18 14:23 H3 0.010 11/20/18 17:22 0,0080 11 /25118 18:30 H3 Sample was received or analysis requested beyond the recognized method holding time. Reviewed by: Chris Derouen (828)254-7176 Christopher.derouen@pacelabs.com Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 Page 3 of 6 Dacprsient Name: Document Revised: February 7, 2019 Sample Condition Upon Ret�t(sCUR} _ Page 1 of 2 _ f dGBf�lk71��ICd� Document No.: ISSUNAuthority: F-CAR-CS-033-Fev.Cfi j Pace Caroiinae Clua€ity Ot{ice Laboratory receiving samples: Asheville ❑ Eden[] Greenwood Huntersville [] Rale(gh[] Mechanicsville(] lJ �� A •9 ilia 11 �n nm I' .P momClient IVtiI ���ia ' ��,q"t'11,0 3 e Project '' • Nat, mI '4 ��' NUY11.1 �'_clrOl;r�0. I i II Courier: ❑Fed €x rJups ❑USPS ❑Client ❑ Commercial ❑F'ace [jOthert,__ 02407733 Cuslody.Seal Present? QYes QKP Seals intact? ❑Yes erlo pate/lnitlafs Person crsmiaing Contents: tE k(a (y` d zb Packing hlaterlaI; ❑bubble Wrao [[Bubble sags '2Nanc ❑ Dt#iec Biological Tissue Frozen? Thermometer: ❑Yes []i~lo �d%A ❑IRC=unlD )tUI;S Type oflce: �SNe[ ❑Blue Dt!ore Cooler Temp ('Q: i-!r .tl Coirection Factory Add/Subtract ('C) li siiouiit be, slave freer=:ng to 6'C Cooler Temp Corretled (°C}: (ISalnples out cf ;ernp crlteria.::impies nn lee, cooling reoctss has 5tgur: USDA Regulated sail ( N/e><watersample) Did samples or€g;n� to in a quarantine zone within the United States: CA, NY, or SC (Gteck maps)? Did samples orb!natc from a roreign scur.e (intemat anally, riva, 1-1-.r — if--4 7n.4 P—dtR Qlrr.3) MPS t0ffl CommentsJD€ssCRancy� Chain of (iutody P: event? ---� OyesSamples Arrived wiWln 4old i,,rre? es ❑Nc—�tN/,� 2. f _--- Short Hold_71me Analysis (<72 hr.l? Yes ❑No Off/A 3. Rush Turn Around Throe Requested? — _ )yrs o I7NJn— 4. Sufficient Velure? — — IJNn_ N/A 5. CorrrctCu;a4iners used?Y es�[JNo ky. -Pace Containers Used? Mo 1, /n _ Containers Intoa? Yes ON -I N/A 7. — — — _ DissoNed analysis: Samples Field Filtered? Iniple — Y s Ho t r+r,t S. _ 9. S Labels Match CDC? . CIN', [JNIA -includes Gate/Time/ID/Anaivs€s Matrix: Neadspace In VOA vials r>S.T,rnm]1 �MKI'as ©:to L,v/A 10. I Tr€p Olnnk Present? !]yes QNo ❑N/A 11. Trip Blank Custody Seals ?resent) CIYes ©No ;!/A ��-- COMMENTS/SAMPLE DISCREPANCY Lot ID of spit comainurs: CLIENT NOURCATION/RESOLUTION Field oats Required? []Yes CQ Na Person zGi`.tactad: _ — Gate/i'nc: �� .• _T. Project 4lrsnager SCURF Reulew: lb Le! Project Manager Siff Review! Dim: Page of 6 i C Iz .CBArar��iC�i! Document IVnnid: :_onditjoon Upon Recei Document NO.: F-CAR•CS-033-itev.06 *Check mark top half of box if pH andf or dechiorination is verified and within -the acceptance range for preservation samples. Nceplicav VOA, Coliform, TOC, Oil and f.• me, DRO/8015 (water) DOC, ti}ig "Bottom half of box is to list number of bottle Document Re sed: February 7, 201S _hge 1 of 2 Issuing Authority; Pate Carolinas Quality Office Project dal �> � ' 41017 ""1"33 I'M: CfI Due Date: 12/04/18 CLIENT: 91-•111414C WIZz R Z Q Y 401 vz V Nad R p Q KI Q Z tl1 1 V u A ? u u rJ c i yCy Q I1 vl J J T I * < i. > O } > G J E E E 5 J E Y .J E J E 9 a` 4 t .J E (+yn i o [Y w In> = r o = M JQ� t� E E pE E 7 j rS1 N Ih m RRait 'rJ-� " Oar m ]� d } 17 N 6 0. M1 4 v a. �/1 m e p Cr 7r m 7v 4 4 Q Q S �{ O > +� +V a Sarnple fD pH Adjustment igpe of Presarvatrve OR ttpan receipt Log for Preserved Date Praserv.it!en adjusted Samples Time preservation A.iicunt of Preservative LaS It adjuited adfed dote: ' bower t'm ri a aLicreputvt atICV11e VOrih Carollm Ccnipliaare ianples, a :apy cr tl•Ia lone will bi sent ta:he Nartn Caralioa LIEHNn cCrU'Sutlatt UMM t:,e. Page 5 of 6 CD 5ICeAnaVIc,! Sect;.. A RCquirod Cticnt lr,:on-.u;pr S Ci AIM -OF• CUSTODY I AnalytiCai Request Document Tre Chzirrdr-Cua:ndy iq a LEGAL DOCUMENT. N reievam tietds must be cnmpleled acwrssr3}'. Suction B Section C RaQolmd Pmi'ct "o maibM i.w.>:ry rntrv-.+: -- Page: br zam�wy: A `.V Norm Carolina Repo. To: 4; ui r M U/A&f Atlem'or,: Account$ Payable -.. Acdmrz; 4112 Old Oxford; levy Copy To: Compeny Na. x- A W North Cartltina RSGiTLI4TQRY AGENCY Durham. NC 27712 Atl a c N?DES C- GROUND WATER' 7' DRiNKtNG WATER r- UST r. RCRA r OTHER Er"I To. caVldkannianen@awnc.com ?urrt+asC thaer No,: sacr Owtc Refrrer.Ge.: Pr%WC 919 479-2243 Fa): 919-47M955 ",n a Name-. Outrall P:cz Pectea Chris Derauen Sitc l.acation wrx, v , STAT1=: RCdueslad Ouz 0a1e11AT: Requested Anafysis' Fi tered (YIN ScctidTa D Valid 0.7atlx Cadcv - � x � :ror:,r.he c.�n uY.<rriertrea >:>nTpix nnnc COLLECTED Preser vafives >: I diaiuuu wArtr. Cv� � � - 2 vawN:Ct•Jr,'ER tJw a r-' cowpo iT[ C i?GC�IJ:T T g 'STAiT J. IJ31i1e .'.,:, CQ v of cx u O to "•r S SAMPLE ID vWm v", a m {J.-(A-7-6.9 1 ; ; csc•.kw oT o n. n- 'r" 1. m a r Sr..,P'k 10- atUT, BE UNIDIJE vsa»r O } es' a�i � Q X Ild •J Z 0 N //--�� O C ' °� to r�� V F4 0 C ^� m a o Z O aS a �ry[,,� u}, ~ �}}}"Xct va CA1E TtYE pat'E T1fAE 2 2 Z 2 O `ray Q U [�� I ca F C> at"3Ce t'OeCt No./ Lab I.D. • .1 1 'IT 1Y; 111no tilts 17.1 1 1 1 1 1 1 1 1 1 1 j 4o f. = 2115 Vofc i k I 7 '12 i ' ` - " At3p1'Flp`JAL•COr+1NENT5 ' � ;. -,; 7-- ' ", i ' ". REUN©UESH� 6Y f AFFiIJATiON "- `; ; QATE' .>Tu1E '''"ACCEPTE6 6Y l AF RIATION - .. DATE" - - 'TEME. • � SAMPLE CONDMONS rr /C l ,., iJ II t� lti• •zocr -5AMPLE:t.AlklhE ANOSIGNATURE _ s •� -= 'a i my PRWTNameofSAMPLER, r SeGNATUREofSAMPLER:.. DATES:gned _ F `—' M V q i, Lj us .w.c:Eys.,nrn:; ftr yso-alcasc:wry.-sx'sr•i•134•� Y' ti,s-rmseFYyreev�•aM.Wprars;-rot,ss'v:,r,::,4ram:r;�r,c nC�c.:c:.e,•ms�e,�:. - _. _. 1•A_L-4ezorev.�a•,2-OH-?.OG7 0 Lo 0 Cn M Q. Stormwater Discharge Monitories Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted / CERTIFICATE OF COVERAGE NO. NCG03 0 6 8 9 FACILITY NAME AWNC COUNTY Durham PERSON COLLECTING SAMPLES Hakim Lundy LABORATORY PACE Analyticat Lab Cert. # 12 Comments on sample collection or analysis: Outfall No. 2 Part A: Stormwater Benchmarks and Monitoring Results z / —/ SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ❑ Jan -June Q July -Dec or ❑ Monthly' _ (month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow [:]WaterSupply ❑SA ❑Other Retention Pond release to Neuse river PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?' Outfall No. Date Sample Collected) (mo/dd/yr) 24-hour rainfall amount, inches' Total Suspended Solids pH, Standard units .Total Copper Total Lead Total Zinc Non -Polar O&G/ Total Petroleum. Hydrocarbons Total Toxic Organics Benchmarks _ 100 mg/L or 50 mg/L° 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46S29 C0530 00400 01119 01051 01094 00552 78141 11/15/18 10.37inches 6.7mg/L 6.3 ND ND 0.036 ND N/A ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Hakim Lundy Name (Print name) Assistant Mgr. Safety Environmental Title (Print ' ws-j r � �F 4 ure � r 1Z­ 2--t—I�<- Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No dischorge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - 15 mg/L 100 mg/L or 50 mg/L" Parameter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/l/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL7 YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original copy of this_DMR, including all "No Discharge" reports, within 30 days of receipt of the tab results (or at end of monitoring period in the case of "No Discharge" reports] to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly respo a`thering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am awa`e t-hayhge--Jre significant penaltres,for submitting false information, including the possibility of fines and imprisonment for knowing violations." / .z --z 1. Signs ut re of_P_ermittee % Date Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 3of3 Pace Analytical Services, LLC 6701 Conference Drive aceAnalytiea! Raleigh, NC 27607 unn+ pacelabs.crom (919)834.4984 t Page 1 of 3 Laboratory Report Hakim Lundy Report Date: 12JO112018 A W North Carolina Date Received: 11/16/2018 4112 Old Oxford Highwy Durham, NC 27712 Project: SW OUTFALL 2 11/15 Pace Project No.: 92407734 Sample: OUTFALL 2 Method Lab ID: Parameters 92407734001 Collected: 11115118 13:00 Matrix: Results Units Report Limit water Analyzed Qualifiers EPA 1664B Oil and Grease NO mg/L 5.0 11/30/18 05:53 EPA 1664E Total Petroleum Hydrocarbons NO mg/L 5.0 11/30/18 05:53 EPA 608.3 Aldrin NO ug1L 0.050 11/27/18 17:43 EPA 608.3 alpha-BHC ND uglL 0.050 11/2711817:43 EPA608.3 beta-BHC NO ug1L 0,050 11/2711817:43 EPA 608.3 delta-BHC NO ug1L 0.050 1112711817:43 EPA 608.3 gamma-BHC (Lindane) ND ug/L 0.050 11/27/18 17:43 EPA 608.3 Chlordane (Technical) NO ug1L 0.50 11/27/18 17:43 EPA 608.3 alpha -Chlordane NO ug/L 0.050 11/27/18 17:43 EPA 608.3 gamma -Chlordane NO ug/L 0.050 11/27/18 17:43 EPA 608.3 4.4'-DDD NO ug/L 0.050 11127/18 17:43 EPA 608.3 4,4'-DDE NO ug/L 0.050 11/27/1817:43 EPA 608.3 4,4'-DDT ND ug/L 0.050 11/2711817:43 EPA 608.3 Dieldrin NO ug1L 0.050 11/27/18 17:43 EPA 608.3 Endosulfan 1 NO ug/L 0.050 11/27/18 17:43 EPA 608.3 Endosulfan 11 NO ug/L 0.050 11127/1817:43 EPA 608.3 Endosulfan sulfate NO ug/L 0.050 11/27/18 17:43 EPA 608.3 Endrin NO ug/L 0.050 11/27/18 17:43 EPA 608.3 Endrin aldehyde NO ug/L 0.050 111271lS17:43 EPA 608.3 Heplachlor NO ug/L 0.050 11/27/18 17:43 EPA 608.3 Heptachlor epoxide NO ug1L 0.050 11/27/18 17:43 EPA 608.3 PCB- 1016 (Aroclor 1016) ND ug/L 0.50 111271l8 17:43 EPA 608.3 PCB-1221 (Arodor1221) NO ugiL 0.50 11/2711817:43 EPA 608.3 PCB-1232 (Arcclor 1232) NO ug/t_ 0,50 11127/18 17:43 EPA608.3 PCB-1242 (Aroclor 1242) NO ug1L 0,50 11/27118 17:43 EPA 608.3 PCB-1248 (Aroclor 1248) NO ug1L 0.50 11/27/18 17:43 EPA 608.3 PCB-1254 (Aroclor 1254) ND ug1L 0.50 11/27/18 17:43 EPA 60B.3 PCB-1260 (Aroclor 1260) NO ug/L 0.50 11/27/18 17:43 EPA 608.3 Toxaphene NO ug1L 0.50 11/27/18 17A3 EPA 8082A PCB-1016 (Aroclor 1016) NO ug/L 0.50 11/20/18 11:37 EPA8082A PCB-1221 (Aroclor 1221) NO ug/L 0.50 11/20/18 11:37 EPA8082A PCB-1232 (Aroclor 1232) NO ug/L 0.50 11/20/18 11:37 EPA 8082A PCB-1242 (Aroclor 1242) NO ug/L 0.50 11/20/18 11:37 EPA8082A PCB-1248 (Aroclor 124B) ND ug/L 0.50 11/20/18 11:37 EPA 8082A PCB-1254 (Aroclor 1254) NO ug/L 0.50 11/20/18 11:37 EPA 8082A PCB-1260 (Aroclor 1260) NO ug1L 0.50 1112008 11:37 EPA 2003 Rev 4.4 1994 Copper NO ugiL 5.0 11120/18 02:40 EPA 200.7 Rev 4.4 1994 Lead NO ugiL 5.0 11120118 02:40 EPA200.7 Rev 4.4 1994 Zinc 36.8 ugiL 10.0 11/20/18 02:40 EPA625.1 Acenaphthene ND ugiL 4.9 11/21/18 02:33 EPA 625.1 Acenaphthylene NO ug1L 4.9 11121118 02:33 EPA 625.1 Anthracene NO ug/L 4.9 1112l/18 02:33 Page 1 of 6 PaceAnalytical Services, LLC 7,4,PalceAn�lytical ¢ 6701 Conference Drive Rafeigh, NC 27607 r whwparelabs.com (919)834.4984 i Page 2 of 3 Sample: OUTFALL 2 Lab ID: 92407734001 Collected: 11/15118 13:00 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers EPA625.1 Benzo(a)anlhracene ND Ljg/L 4.9 11/21/18 02:33 EPA625.1 Benzo(a)pyrene NO uglL 4.9 11121/1802:33 EPA 625.1 Benzo(b)(luoranthene NO uglL 4.9 1112l/18 02:33 EPA625.1 Benzo(g,h,i)perylene ND uglL 4.9 11/21/18 02:33 EPA625.1 Benzo(k)fluoranthene ND uglL 4.9 11/21118 02:33 EPA 625.1 4-Bromophenylphenyl ether NO ug1L 4.9 11/21/18 02:33 EPA625.1 8utyibenzylphlhalate ND ug1L 4.9 11/21118 02:33 EPA 625A 4-Chloro-3-methyl phenol NO ug1L 4.9 11/21/18 02:33 EPA 625A bis(2-Chloroethoxy)methane ND uglL 9.8 11/21/18 02:33 EPA625.1 bis(2-Chloroethyl) ether NO uglL 4.9 11/21/18 02:33 EPA 625.1 2-Chloronaphthalene ND uglL 4.9 11/21/18 02:33 EPA 625.1 2-Chlorophenol ND ug1L 4.9 11/21/18 02:33 EPA625.1 4-Chlorophenylphenyl ether NO uglL 4.9 11/21118 0223 EPA 625.1 Chrysene NO uglL 4.9 11121118 02:33 EPA 625.1 Dibenz(a,h)anthracene NO ug1L 4.9 11/21/18 02:33 EPA625.1 3,3'-Dichlorobenzidine ND ug/L 24.5 1112111802:33 EPA625.1 2,4-Dichlorophenol ND ug1L 4.9 1112111802:33 EPA625.1 Diethylphthalate NO uglL 4.9 11121/1802:33 EPA 625.1 2,4-Dimethylphenol NO uglL 9.8 11/21118 02:33 EPA 625A Dime thylph tha late ND uglL 4.9 11/21/18 02:33 EPA625.1 Di-n•butylphthalale ND uglL 4.9 11/21118 02:33 EPA 625.1 4,6-D ini tro-2- m ethyl phenol ND ug1L 19.6 11/21/18 02:33 EPA 625.1 2,4-Dinitrophenol ND ug1L 49.0 11/21/18 02:33 EPA625.1 2,4-Dinilrotoluene ND uglL 4.9 11121/1802!33 EPA625.1 2,6-Dinitrotoluene NO uglL 4,9 11/21/18 02:33 EPA 625.1 Di-n-octylphthalate NO uglL 4.9 11/21/18 02:33 EPA625.1 bis(2-F=thylhexyS)phthalate ND ug1L 4.9 11/21118 02:33 EPA 625.1 Fluoranthene ND uglL 4A 11/21/18 02:33 EPA 625.1 Fluorene ND ug1L 4.9 11/21/18 02:33 EPA 625A Hexachloro-1,3-butadiene NO ug/L 4.9 11/21118 02:33 EPA625.1 Hexachlorobenzene ND uglL 4.9 1112111802;33 EPA 625.1 Hexachlorocyclopentadiene NO uglL 9.8 11/21118 02:33 EPA 625.1 Hexachloroethane ND uglL 4.9 11/21/18 02:33 EPA625.1 Indeno(1,2,3-cd)pyrene ND uglL 4.9 1112111802:33 EPA625.1 Isophorone ND uglL 9.8 11/21118 02:33 EPA625.1 Naphthalene ND uglL 4.9 11/21/18 02:33 EPA 625.1 Nitrotenzene NO uglL 4.9 11/21/18 02:33 EPA 625.1 2-Nilrophenol NO uglL 4.9 11/21/18 02:33 EPA625.1 4-1\litrophenol NO uglL 49.0 11/21118 02:33 EPA625.1 N-Nitroso6rnethyiamine ND ug1L 4.9 11/21/18 02:33 EPA625.1 N -Ni troso-di-n-p ropylam ine ND ug1L 4.9 11/21/18 02:33 EPA625.1 N-Ni trosodiph enyiamine ND ug1L 9.8 11/21/1802:33 EPA625.1 2,2'-Oxybis(1-chloropropane) ND uglL 4.9 1112111802:33 EPA 625.1 Pentachlorophenol ND ug1L 9.8 11/21118 02:33 EPA 625.1 Phenanthrene ND uglL 4.9 11/21118 02:33 EPA625.1 Phenol ND uglL 4.9 11121/1802:33 EPA 625.1 Pyrene ND uglL 4.9 11/21118 02:33 EPA625.1 1,2,4-Trichlorobenzeile ND ug1L 4.9 1112111802:33 EPA 625.1 2,4,6-Trichlorophenol ND ug1L 9.8 11121118 02:33 EPA624.1 Benzene ND uglL 2.0 11129/1811:12 EPA 624.1 Bromodichloromethane ND uglL 2.0 11129/18 11:12 EPA 624.1 Bromoform ND uglL 2.0 11/29/18 11:12 EPA 624.1 BTomomethane NO uglL 2.0 11/29/1811:12 EPA 624.1 Carbon tetrachloride ND ue1L 2.0 11/29/18 11:12 EPA 624.1 Chlorobenzene NO ug1L 2.0 11129/18 11:12 EPA 624.1 Chloroethane ND ug1L 2.0 11/29/1811:12 EPA 624.1 Chloroform NO ug1L 2.0 11129/18 11:12 EPA 624.1 Chloromethane ND uglL 2.0 11129118 11:12 Page 2 of 6 P� 1__ alceAnalytical mrs.pacelabs.c= i Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (9 t 9)834-4984 Page 3 of 3 Sample: OUTFALL 2 Method Parameters Lab lD: 92407734001 Collected: 11/15118 13:00 Matrix: Results Units Report Limit Water Analyzed Qualifiers EPA624.1 Dibromochloromethane ND ug/L 2.0 11/29/1811:12 EPA624.1 1,2-Dichlorobenzene ND ugll- 2.0 11/29/1811:12 EPA 624.1 1,3-Dichlorobenzene ND ug/L 2.0 11129/18 11:12 EPA 624.1 1,4-Dichlorobenzene ND uglL 2.0 11129/1611:12 EPA 624.1 1,1-Dichloroethane ND uglL 2.0 1112911811:12 EPA 624.1 1,2-Dichloroethane ND uglL 2.0 11/2911811:12 EPA 624.1 1,1-1)ichloroelhene ND ug/L 2.0 11/29/1811:12 EPA624A cis-1,2-Dichloroethene ND ug1L 2.0 11/29/1811:12 EPA 624.1 trans- l,2-Dichloroelhere ND ug1L 2.0 11/29118 11 : 12 EPA 624.1 1,2-Dichloropropane ND ug/L 2.0 11/2911811:12 EPA 624.1 cis-1,3-Dich1eropropene ND ug/L 2.0 11/29/1811:12 EPA 624.1 trans- 1, 3-Dichloropropene ND ug/L 2.0 11/29/1811:12 EPA 624.1 Ethylbenzene ND uglL 2.0 11129/1811:12 EPA624A Methylene Chloride ND ug/L 2.0 11/29/1811:12 EPA 624.1 1,1,2,2-Tetrachloroethane ND ug1L 2.0 11129/1811:12 EPA 624.1 Tetrachloroethene ND ug1L 2.0 11/29/18 11:12 EPA 624.1 Toluene ND ug1L 2.0 11/29/18 11:12 EPA 624.1 1.1,1-Trichloroethane ND ug1L 2.0 11/2911811:12 EPA 624.1 1,1.2-T6chloroethane ND ug/L 2.1) 11/2911811:12 EPA 624.1 Trichloroethene ND ug/L 2.0 11129M811:12 EPA 624.1 Trichlorofluoromethane ND ug/L 2.0 11/29/1811:12 EPA 624.1 Vinyl chloride ND ug/L 2.0 11/2911811:12 SM 2540D-2011 Total Suspended Solids 6.7 mg/L 2.5 11/20/18 1124 EPA 9040C pH at 25 Degrees C 6.3 Std, Units 0.10 11/18/18 14:27 H3 EPA420.4 Rev 1.0 1993 Phenol ND mg/L 0.010 11/20/1817:24 SM 4500-CN-E-2011 Cyanide ND mg1L 0.0080 11/25/18 16:31 ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. Reviewed by: Chris Derouen (828)254-7176 christopher.derouen@pacelabs.com Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 LouisianalNELAP Certification # LAI70028 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 MrginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 Page 3 of 6 Document Name: Document Revised: Februasy 7, 2016 Sam)tio Condition Upon Receipt{SCUR) Paga 1 of 2 G$f��G(,�� Ducun�wnt Na.: Issuing Authority: FCAR-C.S•033-itev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville [] Eden[] Greenwood ❑ Wuntersville }� f� Raleigh[]❑ Mechanlcsvllle ,11 client Name: 64 Ualr:ii' Project p Courier: ❑ dEx +❑UPS ❑USPS� ❑Clfeni ❑ Commercial ❑?ace ❑Other; 97.401734 Custody Seal Present? []Yes [�_Ffo Seals intact? ❑Yes eqo Oate/iniria h Person Exsminfng contents: t ti 1 V_11� d 5+h Packing Material: ❑Bubble Wrap ❑Bubble Bags E one ❑ Other BlologicaI Tissue Frozen? Thermometer; ❑yes pNu LWA �JlTnl 5 Type of ice: �`lt ♦]olue []Nora❑IRGunID: —_ Cooler Temp J'CJ: ""IA •tt _ Correction Fnctnr:'Add/5ubtract ('CI Temp Should 'oe aboae freezing to b'C Cooler Temp Corrected ('C); (l5arrmpfes out of temp ciiterla. sampres on Icp, coating. pr,ress has begun USDA Regulated Sall (� N)A, miter iarrlp€e) Dld samples oriarnp to in a quarantine zone within the United States: f % NY, or SC {check :naps)? Did samples ur:pinate fron+ a foreign source (Inrernatfnnally, I -IV F, ..Il .-A [1....— 01-0 MY— TXn _ -- -- — -_- -Comments/Discrepancy: i Chain of Custody Present? _ _ _ Yts [�NO ON/A _ Samples Arrivcd within Hold Time? ©No J]N/A- 2 3. _ _r+ Short Huld Tfine Anafysls (<72 he.J? 'des No ❑rt/A A Ruch Turn Around Time Rc ue_ .tom ed7 DYes ', o rt/a 4. Sufficient Yolurne? IDYL, EIND ©WA 5. Correct Conta iRUS Used? -Puce Containers Used? Eqs i.JNa nV/A Yes )JVa CJN/a�— G. Contolners 3ntuct? as ON. N/A 7. _ _ Dissolved anal sis: Samples Field Ffiteteo? ~� [',Errs Qr4o Sample Labels Match COC? rrs C)no ©N/A 9. •IndudesDatr./Time/IbJAnalysls Mat€ :___.sn_!S,_.---- - l i'.r' -a dspace In VOA Vi26 (>5 brm} l (*]Yes FJrro ❑N/A 10, Trip Wank Present? []Yes []No ❑N/A 11. Trip Blank Custody Seals Present? FlYv 17111a MM/A CORIMEhITS/SAMPLE DLSCREPANCY Lot 10 of sp[ : containers: CLIENT N01EFIC7TION,7iESOWTION Fleid Data Required? ❑Yes ❑No i Person contacted: ,� Datertme: �_.—- i 1 � f Project Manager SCURF Revfaw: �... _- Date: li ! Project F Y c( Ic rvianag(,rSR Review. Oate: Page 14 o€ T Document `fame: Sam le Candfilon Upon Rao Document No.: f-CAR•CS-033-Rcv.06 'Check mark top half of box if pH and/or dechlorination is verified and w(thin the acceptance range for preservation samples. Exceptions: VOJti Coliform, 3 OC, OR and Grease, DRC/8OS S jwatnf) DOC, U.Kk; "Bottom half of box is to list number of bottle Document Re�75ed: February 7, 2018 Page 1 of 2 Issuing Autfitarrty: Pace Carolinas CtualitYC)MU 1 1 Project1 L f- . Cj drdlf"177_IA 11M.- GU1 Due Date: 12/04/18 I`'LIENT: Ell.- AI N ' Z V a ry L v v r1f A v Tii u a � L Z ell 4 a 13A —N i a 1 ry t• r�' v r f Q Y z ti C Y d 4% y v u jj S a r r I a u n3 u n S N L 3 a F .r r Sl Lu � exi rry '7 H C 9 o E n � z v M I o u _ [ z Pr S E. •L ��,`rr May C tx M IL � � E E E ` O O O 6 u n 2 � y -9 gg z 7 u r� � a. a. q 1 . U `f: u� D .0 V u h a it m m as to m o m r a 7 ' I 4 c E DE `p I gg� x "� ! N 1 7C r s 4 Y ►r- 'U i7 b Lh i7 i7 CR 0 0. N � a a a� a a � 7 � G q D . mj p a�i h y1 li m .( 7 O #7 II I •21 �~ pH Adjustment Log for Preserved Samples 1 Sartlpre 10 Type of is: eaerva'ive ptiupon raaeipt Date preservaticn adjusted Time preservation adjusted IAmount of Preservati•re added Cat 9 Mote- Wnerlecer tj,C,E IS d rslscrepaocy attecting NU[W �,M ollna :Ampllaree samalef, a tapy m cols rnrrn w1F ae tent trs Ins Rorin s.a ra..na �cn.�.• uu,.a..,,u•.y= y=• Page 5 of aceAnafj4ica! Section A ,xra.,:_ rr"I nIo R cor Section B Rea Ai d Pr cl IraornaWn' GHA1N-OF -CUSTODY f Analytical Request Document Tice Ch2in-of-Cusfody is a LEGAL DOC VI.U--Nl . PM rzkwdnt SCM must oc compicicd x.=wC{y. Section C Irvoier ln:v d": Cam;a:.y: A W North Cardina ReCart Ta' Q 7d+tR1dnCrY A.Wf44n: ACMLfntS PayalblC V Atlaress' a t 12 Old Oxford Wvey [opy ro: %om:a'v uz— A W North Carob REGULATORY. -AGENCY JDUrham• PVC 277,2 Adsrvs. F "PDES f- GROUNDWATER DRINKING WATER UST r' RCP,A 17 6T}iER FJ+ra:lrv: da>:idkannianengawne.com f'Ischase6rd'rN°.: 1'a a�xr- Rere,a : Phax: 919-t79-2243 Fm[ 919-A79-8955 pro.eiNanve: Qe*ejj -•t_�` P'k�"� ChrisDerOUen Site Location CT�—;� u4"Qg r. - . •. STATE: esd Due UatwTAT: Requ,e pmIk ..14 cr. PacePI.G4 u: Requested AnatyS� Fittered (Y!N) SaCtion B Ve11d mats• cases P Cfrn lnro�nmmn v T o�E =' e a COLLECTED PreservalNt s $ i' 'jFl�'I@IO WATER RV nr-_4 T � _ V C�h�CC:T>: C(AY'0. •'i£ O r r _ SAMPLE lD � 0 � � (o-z. a3 r.•) c n AR u, Sx"* toc rrus- lac UNIQUE Te.A T; o a r rTs V a X G ti U (� Q e6 LL =p 7 ^. Z'-to? ay w o ��+z ti O ti Z m=.¢ 2 O J d c,o n w m ti N m Pace Projcci NoJ lab I.D. DATE TINE PATE TIMe - : T T Z C) rip i— U .. 00 G L v s { 7 ' i5 s_ Q n .-; AVk)FnQNAL COMMEhrTS - - -REuNQan3HE0rBy IAF"UAn0N � • '..: ry`:/ DATE , -T7ME;'�., .-�?.CCEPTEP BY,l AFF111n110 'DATE � -TIA7E `� SAMPLE C017DkT16N�S/ - - it & j Za k[It6,It kgZ0 SAMPLER NAA,E.ANQ SIGNATURE': i :: .•! " - '. ., . - - ... a ? $ P"JT Name of SAh1PLEiL• SiGNATUFE of $AY.PLER: -r OATMroSi d i •1r..oa"sr.note.CYN•r��^nvi.Iwm�a,, .�.�a»rpn�; Pis's r�E.� a.er i+apne:a terw. ana aq•e ek,; one at�pr�te e!1.5': per nor:n t.��r n�*;r•. r�r w..a.+r ye aM, -'• r-AILS--a7-o:cu.08..2-0r..zao7 0 6) Cn Q Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted / ~ 7— CERTIFICATE OF COVERAGE, NO. NCG03 0 6 8 9 FACILITY NAME AWNC ___ COUNTY Durham PERSON COLLECTING SAMPLES Hakim Lundy LABORATORY PACE Analytical Lab Cert. # 12 Comments on sample collection or analysis: Outfall No..3 Part A. Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ❑ Jan -June E] July -Dec or 0 Monthly' _ (Month) DISCHARGING TO CLASS ❑ORW ❑HQW [:]Trout ❑PNA ❑Zero -flow ❑Water Supply F. ❑Other Retention Pond release to Neuse River PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/Total Total Petroleum: Hydrocarbons ................ Toxic Organics5 Benchmarks _ - 100 mg/L or 50 mg/0 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141 11/15/18 10.37inches 8.0mc3/L 6.5 ND ND 0.025mg/L ND N/A ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. n See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433,11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Hakim Lundy Name (Print name) Assistant Mgr. Safety Environmental Title (Print title) Signature'- 412 —c;,_ / le Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part Ei: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > SS gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' New Motor Oil or Hydraulic Oil usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/O Parameter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 1111/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS:. • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS_ SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART Il SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES Q NO 0 IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES E] NO [] REGIONAL OFFICE CONTACT NAME: Mail an original copy of this DMR, including al! "No Discharge" reports, within 30 days of receipt of the lab results tor at end of monitoringperiod in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance With a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the nest of my knowledge and belief, true, accurate, and complete. I am aware that there are_signifa a.Qtpenalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." re of Perm �-2~ Date Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 3 of 3 a Pace Analytical Services, LLC / aceAnaly�ircal 6701 Conference Drive Raleigh, NC 27607 � rwnvpacelaLs.conr (919}$34-49$a Page 1 of 3 Laboratory Report Hakim Lundy Report Date: 11/30/2018 A W North Carolina Date Received: 11/16/2018 4112 Old Oxford Highwy Durham, NC 27712 Project: 5VV OUTFALL 3 11115 Pace Project No.: 92407735 Sample: OUTFALL 3 Method Lab ID: 92407735001 Collected: 11115/18 11:15 Matrix: Parameters Results Units Report Limit Water Analyzed Qualifiers EPA 1664B Oil and Crease NO mg1L 5.0 11/30118 05:53 EPA 1664B Total Petroleum Hydrocarbons ND mgfL 5.0 11130118 05:53 EPA 608.3 Aldrin ND ug/L 0,050 11/27/18 18:09 EPA 608.3 alpha-BHC ND ug/L 0.050 11/27/18 18:09 EPA 608.3 beta-BHC ND ug/L 0.050 11/27/18 18:09 EPA 608.3 delta-BHC ND ug/L 0.050 11/27/18 18:09 EPA 608.3 gamma-BHC(Lindane) ND ug/L 0.050 1112711818:09 EPA 608.3 Chlordane (Technical) NO ug1L 0.50 11/27/18 18:09 EPA 608.3 alpha -Chlordane ND uglL 0,050 1112711818:09 EPA608.3 gamma -Chlordane ND uglL 0.050 11/27/18 18:09 EPA 608.3 4,4'-DDD NO uglL 0.050 11127l18 18:09 EPA 608.3 4,4'-DDE NO ug/L 0.050 11127l18 18:09 EPA 608.3 4,4'-DDT NO ug/L 0.050 11/2711818,09 EPA608.3 Dieldrin NO ug/L 0.050 11/2711818:09 EPA 608.3 EndosulfanI NO ug/L 0.050 11/2711818:09 EPA 608.3 Endosulfan Il ND ug1L 0.050 11/27/18 18:09 EPA 608.3 Endosulfan sulfate ND ug1L 0.050 11127/18 18:09 EPA 608.3 Endrin ND ug/L 0.050 11/27/18 18:09 EPA 608.3 Endrinaldehyde ND ug/L 0.050 11/2711818:09 EPA 608.3 Heptachlor NO ug/L 0,050 11/27/18 18:09 EPA 608.3 Heptachlor epoxide NO ug/L 0,050 11/27/18 18:09 EPA 608.3 PCB-1016 (Aroclor 1016) ND uglL 0,50 11/27/18 18:09 EPA608.3 PCB-1221 (Aroclor 1221) ND ug/L 0.50 11/27/18 18:09 EPA 608.3 PCB-1232 (Aroclor 1232) NO ug/L 0.50 11/27/18 18:09 EPA 608 3 PCB-1242 (Aroclor 1242) NO ug1L 0.50 11 /27118 18:09 EPA 608.3 PCB-1248 (Aroclor 1248) ND ug/L 0.50 11/27/18 18:09 EPA608.3 PCB-1254 (Aroclor 1254) ND ug/L 0.50 11/27/18 18:09 EPA 608.3 PCB-1260 (Aroclor 1260) NO ug/L 0.50 11/27/18 1&09 EPA 608.3 Toxaphene ND ug/L 0.50 11/27/18 18:09 EPA 8082A PCB-1016 (A€ocior 1016) ND ug/L 0,50 11120l18 11:50 EPA 8082A PCB-1221 (Aroclor 1221) ND ug/L 0.50 11/20/18 11:50 EPA 8082A PCB-1232 (Aroclor 1232) ND ug/L 0.50 11/20/18 11:50 EPA 8082A PCB-1242 (Aroclor 1242) NO ug1L 0.50 11120/18 11:50 EPA 8082A PCB-1248 (Aroclor 1248) NO ug/L 0,50 11/20/18 11:50 EPA 8082A PCB-1254 (Aroclor 1254) NO ug/L 0.50 11/20/18 11:50 EPA 8082A PCB-1260 {Aroclor 1260) NO ug/L 0.50 11/20/1 B 11:50 EPA 200.7 Rev 4.4 1994 Copper ND uglL 5.0 11/20118 02:43 EPA 200.7 Rev 4.4 1994 lead NO ug/L 5.0 11/20/18 02:43 EPA 200.7 Rev 4.4 1994 Zinc 25.3 uglL 10.0 11/20118 02:43 EPA 625.1 Acenaphthene NO ug/L 4.8 11/21/18 03:00 EPA 625.1 Acenaphthylene ND ug1L 4.6 11/21118 03:00 EPA 625.1 Anthracene NO ug1L 4.8 11/21/18 03:00 Page 1 of 6 I'laeAnalytical& J vnnepacefabs.com Pace Analytical Services, LLC 6731 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 2 of 3 Sample: OUTFALL 3 Lab lD: 92407735001 Collected: 11115/18 11:15 Matrix: Water Method Parameters Results Units Report Limit Analyzed Qualifiers EPA 625.1 Benzo(a)anthracene NO ug/L 4.8 1112111803:00 EPA 625.1 Benzo(a)pyrene NO ug/L 4.8 11/21/18 03:00 EPA 625.1 8enzo(b)fluoranthene ND ug/L 4.8 11/21/18 03:00 EPA 625.1 Benzo(g,h,i)perylene ND ug/L 4.8 11/21/18 03:00 EPA 625.1 Benzo(k)Ouoranthene ND ug/L 4,8 11/21/18 03:00 EPA 625.1 4-Bromophenyiphenyl ether ND ug/L 4.8 11/21/18 03:00 EPA 625.1 Butylbenzylphthalate ND ug/L 4.8 11121/18 03:00 EPA 625.1 4-Chloro-3-methylphenol ND ug/L 4.8 11/21/18 03:00 EPA 625.1 bis(2-Chloroelhoxy)methane NO ug/L 9.5 11/21/18 03:00 EPA 625.1 bis(2-Chloroethyl) ether NO ug/L 4.8 11/21118 03:00 EPA625.1 2-Chloronaphthalene NO ug1L 4.8 11/21/18 03:00 EPA625A 2-Chlorophenot NO ugIL 4.8 11/21/18 03:00 EPA825.11 4-Chlorophenylphenylether NO ugIL 4.8 11/21118 03:00 EPA 625.1 Chrysene ND ug/L 4.8 11121/18 03:00 EPA 625.1 Dibenz(a,h)anthracene NO ug1L 4.8 11/21/18 03:00 EPA625.1 3,3'-Dichlorobenzidine NO ug/L 23.8 11/21/18 03:00 EPA 625.1 2,4-Dichlorophonol ND ug1L 4.8 11/21/18 03:00 EPA 625.1 Diethyl phthalate ND ug/L 4.8 11/21/18 03:00 EPA 625.1 2,4-Dimethyl phenol ND ug/L 9.5 11/21118 03:00 EPA 625.1 Dim ethyl phthala te ND ug/L 4.8 11/21118 03:00 EPA 625.1 Di-n-butylphthalate ND ug/L 4.8 11/21/18 03:00 EPA 625.1 4,6-Dinitro-2-methylphenol NO ug/L 19.0 11/24118 03:00 EPA625A 2,4-Dinitrophenol ND ug/L 47.6 11/21118 03:00 EPA 625.1 2,4-Dinilrotoluene ND ugfL 4.8 11/21/18 03:00 EPA 625.1 2,6-Dinitro(oluene ND ugIL 4.8 11121/18 03:00 EPA 625.1 Di-n-octylphthalate ND ug/L 4.8 11121/18 03:00 EPA 625-1 bis(2-Ethylh exyl)phthal ate ND ug/L 4.8 11/21/18 03:00 EPA625.1 Fluoranthene ND ugIL 4.8 11/21/18 03:00 EPA 625.1 Fluorene ND ug1L 4.8 11/21118 03:00 EPA 625.1 Hexachloro-1,3-butadiene NO ug/L 4.8 11/21118 03:00 EPA 625.1 Hexachlorobenzene NO ug1L 4.8 11/21/18 03:00 EPA 625.1 Hexachlorocydopentadiene NO ug/L 9:5 11/21118 03:00 EPA 625.1 Hexachioroethan e ND ug/L 4.8 11/21118 03:00 EPA 625.1 Indeno(1,2,3-cd)pyrene NO ug/L 4,8 11/21/18 03:00 EPA 625.1 Isophorone NO ug/L 9.5 11/21118 03:00 EPA 625.1 Naphthalene ND ug/L 4.8 11/21/18 03:00 EPA 625.1 Nitrobenzene ND ug/L 4.8 11/21/18 03:00 EPA 625.1 2-Nitrophenol NO ug/L 4.8 11/21/18 03:00 EPA 625.1 4-Nitrophenol NO ug/L 47.6 11/21/18 03:00 EPA 625.1 N-Nitrosodimethylamine ND ug/L 4.8 11/21/18 03:00 EPA 625.1 N-Nitroso-di-n-propylamine NO ugIL 4.8 11/21118 03:00 EPA 625.1 N-Nitrosodiphenylamine NO ug/L 9.5 11/24/180100 EPA 625.1 2,2'-Oxybis(1-chloropropane) NO ug/L 4.8 11/21/18 03:00 EPA 625.1 Pentachlorophenol NO ug/L 9.5 11/21/18 03:00 EPA 625.1 Phenanthrene NO ug/L 4.8 11/21/18 03:00 EPA 625.1 Phenol ND ug/L 4.8 11121/18 03:00 EPA 625.1 Pyrene N❑ ug1L 4.8 11/21/18 03:00 EPA 625.1 1,2,4-Trichlorobenzene ND ug/L 4.8 11121/18 03:00 EPA525.1 2,4,6-Trichlorophenol NO ugIL 9.5 11121/18 03:00 EPA624,1 Benzene' NO ug/L 2.0 11/29/1811:29 EPA 624.1 Bromodichloromethane ND ug/L 2.0 11/29/18 11:29 EPA 624.1 Bromoform ND ug/L 2.0 11/2911811:29 EPA 624.1 Bromomelhane ND ugIL 2.0 11/2911811:29 EPA 624.1 Carbon tetrachloride NO ug/L 2.0 11/2911811:29 EPA 624.1 Chlorobenzene ND ug/L 2.0 11/2911811:29 EPA 624.1 Chloroethane NO ug/L 2.0 11129/18 11:29 EPA624.1 Chloroform ND ug/L 2.0 11/29/1811:29 EPA 624.1 Chloromethane NO ug/L 2.0 11 /29/18 11:29 Page 2 of 6 e aceAnalyticai'5' vmvpacofabs.com Pace Analytical Services, LLG 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Page 3 of 3 Sample: OUTFALL 3 Method Lab ID: Parameters 92407735001 Collected: 11/15/18 11:15 Matrix: Results Units Report Limit Water Analyzed Qualifiers EPA624,1 Dibromochlorom ethane ND ug/L 2.0 1112911811:29 EPA624.1 1,2-Dichlorobenzene ND ug/L 2.0 11129/1811:29 EPA624.1 1,3-Dichlorobenzene ND uglL 2.0 1112911811:29 EPA624.1 1,4-Dichlorobenzene ND ug1L 2.0 11129/1811:29 EPA624A 1,1-Dichloroethane ND ug/L 2.0 1112911811:29 EPA 624.1 1,2-Dichloroethane ND ug/L 2.0 11129/18 11:29 EPA 624.1 1,1-Dichioroethene ND ug/L 2.0 11129/18 11:29 EPA624.1 cis-1,2-Dichloroethene ND ug1L 2.0 11/29/18 11 :29 EPA624.1 trans-1,2-Dichloroethene ND uglL 2.0 11129/1811:29 EPA624.1 1,2-Dichloropropane ND uglL 2.0 11129/1811:29 EPA624,1 cis-1,3-Dichloropropene ND ug1L 2.0 1112911811:29 EPA624.1 trans-1,3-Dichloropropene ND uglL 2.0 11129/1811:29 EPA624.1 Ethylbenzene ND ug1 2.0 11/29/1811:29 EPA624A Methylene Chloride N❑ uglL 2.0 11/2911811:29 EPA624.1 1,1,2,2-Tetrachloroethane ND ug/L 2.0 11/2911811:29 EPA624.1 Tetrachloroethene ND ug/L 2.0 11/2911811:29 EPA624.1 Toluene ND ug1L 2.0 11129/1811:29 EPA 624.1 1,1,1-Trichloroethane ND ug/L 2.0 11129/1811:29 EPA624.1 1,1,2-Trichloroethane ND ug/L 2.0 11129118 11 :29 EPA624.1 Trchloroethene ND ug/L 2.0 11/29/1811:29 EPA624.1 Trichlorofluoromethane ND ug/L 2.0 11 /29/16 11 :29 EPA624.1 Vinyl chloride ND ug/L 2.0 11129/1811:29 SM 2540D-2011 Total Suspended Solids 8.0 mg/L 2.5 11120/18 11:34 EPA 9040C pH at 25 Degrees C 6.5 Std. Units 0.10 11/18/18 14:14 H3 EPA 420.4 Rev 1.0 1993 Phenol ND mg/L 0.010 11/20118 17:25 SM 4500-CN-E-2011 Cyanide Nil mg/L 0.0080 11/25/18 18:32 ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. Reviewed by: Chris Derouen (828)254-7176 christopher.derouen@pacelabs.com Charlotte Certification 1Ds 9800 Kincey Ave. Ste 100, Hunlersviile, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #:99030001 Mrginia/VELAP Certification M 460222 Page 3 of 6 Oncurnent ?tame; rpira ment Revised:February 7, 2018 5ample Conditlon Upon Aecefpt(SCUR) Page 1 of 2Document No.: issufng Authorjty: F-CAR•CS-033-Rev.06 Carolinas QaaiJ Offfce Laboratory receiving samples: AshevilleEden[] Greenwood Huntersville[] Raleigh[] Mechanicsville[] Client Name: �IV1V � �' ' � �,o� �07 7 0� 5 . - � Project k ��Fed �. � `�`," Courfer: —O❑LISPS ExUPS ❑CiienC ❑ commercial ❑Pace ❑u!her._ 07407735 Custody Seaf Present? ❑Yes Qf6 Seals Intact? ❑Yes eVo t1 itL_"l l� slate/p;iilatSPCr30n Esarttining Cnnteob: d �h PaCkinghlater faf: ❑rsubbre wrap E ]Bubble Begs 'eVane ❑ Other efo(ogical Tissue Frozen? Thermometer: []Yes ❑No NO/ —A ❑ fA fii wt iD: c(ljpt; ;9Paof.i<a: �t [J[llue ❑None Cooler Temp ('C): LA A Correction Factor; Add/Subtract (`C) t 0 • t 'C Ternp siiauld he ahnve freexirsg to 6`C Cooler Temp Corrected { J : _ ❑5arnpies pet of teary rito9a. Samples on Ire, cooling process USD,aRcgulated5eli {[�]N;A,watersantpfel has begun Old sa—m�ples 0`gfnntR in a gt:arantfne lone wlthin the United States: CA, VY, or 5C (check maps)? Old samples originate from a foreign source (internationally, r IY. lv o inciudine lfaw-M and Puerto Rico)? QYes 191f. T Chain Of Custody Present? As t-INo EIN/A CnmrnentsJDBctepancy: 1. — J— ` Samples Arrived withln Hold T)me? [ es QNo ❑IiIA 2. --_.� Short Hull Time Analysis (02 hr.)? 7as ❑tm NIA 3. Rush Turn Arcund' irna Requested? r 5uffkientValrsme7 fDYis []No. [JNIA Cnrrer ctCuntainersUsed? -Pace Containers Used? YLI r el ❑No Dtio -v/A ❑ ❑NJ.i�_ _S_ 6. _ _.J — Containers intact? Dissolved anal sls: Samples Field Fiterr_d_? .es I es QNo LNo QN/A 116 7. 3. _ _ _ sample labels Match CDC7 -includes Date/Time/1D/, mla sis Neadspace in VOA Vials 1>5•6nini)? �res ❑Yes ❑No LLIa J JNJA ❑NfA 9. 10. _ 11. W Trip Tank Presen,? ❑Yni LI,No CNIA LTrip plank Custody Seals ?resent? ores ( No ❑NlA_ COMMENTSJSAMPLE DISCREPANCY Field Data Rewired? ❑Yes []NO Lot iD of split con taioem _ CLIENT NOTIFICATIONJRPSOtUTION — Person contacted: ] project 4lanager SCURF Review: j Project Manager SRf Review: _ Date: Page 4 of 6 0acument Name: Sample Condillan Upan Reccl —pacument No.; F-CAR-CS-033-Reu06 DncumantRevised: february7, 2019 Page 10€ '- Issuing Authority: Pace Catvlfrras Quality Office_ rr ma rn 'Check mark top half of box if pH and/or dechlorination Is Project i I, `2��11_3 7 73%) verifled and within the acceptance range for preservation __� _ — sampies. PM: CD1 Out! Date: 12/04/18 Exceptlans: VOA, Coliform, roe, Oil and Grease, DRO/9015 (water) DOC, WHg ct.IE'uf : 9].—AWNC ' 'Bottom half of box is to list nuniber of bottle a ' N J j, < N I I cr t v �, e s " r, a � ;< z r z M = u ir g 1 7 y u 3 7 w 4 P x 0 �i 7 2 o 3 > 7 u E 7 7 e St" e z a ry p a e_ J el _0E E v p U p � I u` �E �J < Ci �1 > > 7., fn E > r•r n l7 Q dl ea O U 7n N Y� n j e. in m a o a m a. m CL rn a 3 o a w a Q a a C7 f ¢ n to >> 0 W a> 1 R a Y l 'I6 f pH adjustment log for Preserved samples�T Sample ID Type of Praserntive pH upon receipt Date presemticn adjusted the Prarenadoll adiustrd ^ —_ Amoil to Prnsurvativc added la:� NOM: Wh3no•fef rNef@ IS A C!f[re pdRCy' jrfe'riir�C', �VL'fU: Cr rn7na Cemp�IanCe ! amplus, a enpv Or rnlS :O�r+ wlri Ga SegF IA tT�! r+unn Ldr•-• Ou! of hold, lucnfrect preierra tiv+, oaf of ternp, ir.cor,sa comairars. Page 5 of 6 a�eAnalytical" i CHAIN -OF CUSTODY i Analytical Request aocuriien: The Chain -at -Custody is a LG-6L DOCUMCNi. AS rcievam Tides must he compfsteC 2ccurately. Section A Section B Section C Page.• d Required Dent Irrormawn: Required P viml Irdomaxion +nvore In'orma,iaz. c -P- ,Y. A W North Carolina mwTO: 11�.a.i4wroirwgp 4 1 tt5cnoor� AetnunL; P3yatilP Y't tYi �durC�a; 4112 Old Oxforc6 Hwy QQW Tn, C--Pkry t1nn t: A V) Nodh Carolina REGULATORY. AGENCY ' - Durham, MC 27712 Add-4s: 7, NPOES f— GROUKOWATER i DRiNKINGWATER r- UST f RCPA i- OTHER =ma;l TV: davidunnianenoawac com surd sse Ofcer No.: P" cxe Phorc: 919-479-2243 F.W 919-479-89S5 �' �� Outf�ll v^m�7p ' ChliSDar[OUPs1 Sae_Lacation STATE: PtequWrd Due 4ate7TAT; Proj= NURIL�: r-O pmrjo s: _- - RafaucstedArinlysls Flitered (YfN)';- 1 / Stetson C Y.I:d Maui. Requi.-d Ckm kr:orna:cn w�rFrx r.-nr a 'o COLLECTED Preservatives > grrwkmcwnr ev+ �y _-,- WATER wr .r:m:sT V � m a-,rar ES+CiCWE 2 cr C7 Z SAMPLE !D ::'°` Yr " ° C N4 AN 4 0 m 0 �� f Sa p,e tos R.JST nc UNIQUE U%5LJr -+ rJ m C N OL ,a, u`s r' 4 4 rn QATE YIME DATF TWIE Z m O L c � S Z U 2 rrs Z z a L D ..�r ^' O 'n? F- S LJ N .II lr� N cn Cu C cn O Hr >~ L� Pace Project Not Lab 1-6. VIM ! i -`•S 6.. c, ?9. 11= 12 ' _ -, `+ "-; -ACTE68YlIFFIL fAON E.0AY •AA .. TIME SAMPLE CONDTONS,AR i +SAMPLEFfJAME J:tJ05tGNATUlZE''. . ::rs' r. - _ - :i - o �• a PRWT N,11MO Ot S"K;ER: - r - E:... u1GNATURE of SA.Mp i , PATE Signetl ' f `: hr:ronari Net[: Ly Allir7 e., :rm rau are rr ,Prina ✓��:': r 7 ; :a coy La+J�p+-w kan� sn;, a:rcc�rr, w L' I: Sncr z ei Tay; per ranch foram•r.+ni;sa ncn Fsd r.Y+3; v F yy '' r • . - F.ALC•O-G2Crev.GS. 1,Z•C7 -2007 a STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF ENERGY, MINERAL AND LAND RESOURCES GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE No. NCG030689 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, AW North Carolina is hereby authorized to discharge stormwater from a facility located at AW North Carolina 4112 Old Oxford Highway Durham Durham County to receiving waters designated as Neuse River, a class WS-IV;NSW,CA water in the Neuse River Basin, in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, 11, 111, and IV of General Permit No. NCG030000 as attached. This certificate of coverage shall become effective January 25, 2018. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day January 25, 2018. ORIGINAL SIGNATURE by RICHARD L. RIDDLE, JR. for William E. (Toby) Vinson P.E., CPM Interim Director, Division of Energy, Mineral and Land Resources By the Authority of the Environmental Management Commission NCG030689 N W E S Map Scale 1. 24, 000 Z� > P %-A 0 lb 0 1 AW North Carolina Q� �, (7 AW North Carolina Latitude: 360 05'29" N Longitude: 780 50' 14" W County: Durham Receiving Stream: Neuse River (Falls Lake below NPE) Index No: 27-(1) Stream Class: WS-IV;NSWCA Sub -basin: 03-04-01 (Neuse River Basin) M Facility Location Energy, Mineral & Land Resources ENVIRONMENTAL QUALITY January 25, 2018 Mr. David Kannianen AW North Carolina 4112 Old Oxford Hwy Durham, NC 27712 ROY COOPER Governor MICHAEL S. REGAN Secretary WILLIAM E. (TOBY) VINSON, JR. Interim Director Subject: General Permit No. NCG030000 AW North Carolina Issuance of COC No. NCG030689 & Rescission ofNCGNE0275 Durham County Dear Mr. Kannianen: In accordance with your application for a discharge permit received on December 8, 2017, we are forwarding herewith the subject certificate of coverage (COC) to discharge under the subject state — NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection Agency dated October 15, 2007 (or as subsequently amended). We are also hereby rescinding No -Exposure Certification NCGNE0275 for the subject facility. Please take notice that this certificate of coverage is not transferable except upon approval of the Division of Energy, Mineral and Land Resources (DEMLR). DEMLR may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by DEMLR, the Coastal Area Management Act, or any other federal, state or local government permit that may be required. If you have any questions concerning this permit, please contact Julie Ventaloro at telephone number (919) 807-6370 or by email julie.ventaloro@ncdenr.gov. Sincerely, ORIGINAL SIGNATURE by RICK RIDDLE for William E. (Toby) Vinson, Jr., P.E., CPM cc: Raleigh Regional Office, Thad Valentine Central Files Stormwater Permitting Program Files State of North Carolina I Environmental Quality I Energy. Mineral and Land Resources 512 N. Salisbury Street 1 1612 Mail Service Center I Raleigh. North Carolina 27699-1612 919 707 9200