NCG030175_MONITORING INFO_20190203

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
O 3 D I / 5
DOC TYPE
❑yHISTORICAL FILE
MONITORING REPORTS
DOC DATE
❑ ����� D� v3
YYYYMMDD

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted 1129120
CERTIFICATE OF COVERAGE NO. NCG03 0 1 7 5
FACILITYNAME Specialty Product Technologies
COUNTY Bladen
PERSON COLLECTING SAMPLES Branden Carson
LABORATORY Pace Analytical Lab Cert. # 12
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2019
SAMPLE PERIOD 0 Jan -June 0 July -Dec
or ❑ Monthly' month
a SDISCHAFRGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
FEB 0 3 2019 *Other Middle Cape Fear
CEN T'fV\L EILE5
DWR SECTIOtj PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches
Total Suspended Solids
pH,
pH,
Standard units
Total Copper
Total Lead
Total Zinc
O&G/
Total Petroleum
Hydrocarbons
Total Toxic
. Organics'
Benchmarks
-
-
100 mg/L or 50 mg/L4
6.0 — 9.0
0.010 mg/L
0.675 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
46529
C0530
00400
01119
01051
01094
00552
78141
001
12/30/19
.24
8.3
7.5
.010
<.005
.037
<5
NA
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page i of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Sally Creasy
Name (Print name)
VP, Operation-Dynapar/SPT-North America
'title (Print title)
( �&RAA C& A !IZq
2b
Signature I Da e
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part 8: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period ?2
Out{all No.
Date Sample Collected!
(mo/dd/yr)
24-hour rainfall amount,_
inches3
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
- _
-
-
15 mg/L
100 mg/L or 50 mg/L°
Parameter Code
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results Lor at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attw DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
of Permittee
Permit Date:11/1/2018-05/31/2021
//Z� ?�
Date
SWU-245, last revised 11/1/2018
Page 3 of 3

L lea
F.nvironnaenlal
Qualify
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance onfrlling out thisform, please visil https:Hdeq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: NICI I I. l I l I 1 or Certificate of Coverage No.: NICIGI 013 I 0 I 1 l7 / 5l
Facility Name: Specialty Product Technologies
County: Bladen
Inspector: Branden Carson
Date of Inspection: 12/30/19
Phone No. 910-862-4506
Time of Inspection: 11 am RECEFI\ Fn _ - _
Total Event Precipitation (inches):.24
FEB 0 3 2019
CEN HV\L FILES
UWR SECTION?
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. M
Receiving Stream:
Structure (pipe, ditch, etc.): pipe
Describe the industrial activities that occur within the outfall drainage area: Industrial manufacturing
Page I of 2
sWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
f (light, medium, dark) as descriptors: CI&-/- loy - 16'0 f/-t
3. Odor: Describe an distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): _ f,'o �;'ry �
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 0 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 W 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes Or No.
8. Is there an oil sheen in the stormwater discharge? 0Yes 911�0.
9. Is there evidence of erosion or deposition at the outfall? O Yes p'No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Rage 2 of 2
$WU-242, Last modified 06/01/2018

lac ie Analytical !
ww.pacdmb%.com
January 15, 2020
Zachary Lewis
Speciality Product Technologies
RE: Project: Stormwater Sampling
Pace Project No.: 92459129
Dear Zachary Lewis:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on January 02, 2020.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIi1NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
I-—
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Matt Lewis, Specialty Product Technologies
Louis Maitiand, Specialty Product Technologies
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page i of 22

lacmnalyficalo
ww.paWabs.c=
Project: Stormwater Sampling
Pace Project No.: 92459129
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
LouisianalNELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
FioridalNELAP Certification*. E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 2 of 22

aceAnalytical
wrrw.pacela6s.cwn
SAMPLE ANALYTE COUNT
Project: Stormwater Sampling
Pace Project No.: 92459129
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92459129001 Samples EPA 1664B
HH
1
PASI-C
EPA608.3
SEM
29
PASI-C
EPA 200.7 Rev 4.4 1994
KQ
3
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624A
CL
34
PASI-C
SM 2540D-2011
MJP
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 22

(�IaneAnalXical
WWW' "Ab3.tom
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater Sampling
Pace Project No.: 92459129
Sample: Samples
L.ab ID: 92459129001 Collected: 12/30/19 11:00
Received: 01/02/20 13:38 Matrix: Water
Parameters
Results
Units
Report Limit
OF
Prepared
Analyzed
CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO
mg/L
5.0
1
01/14/20 16:53
608 PCB Pest RVE
Analytical Method:
EPA608.3
Preparation Method: EPA608.3
Aldrin
NO
ug/L
0.050
1
01/03/20 11:23
011081201611
309-00-2
alpha-BHC
NO
ug/L
0.050
1
01/0312011:23
01/08/20 16:11
319-84-6
beta-BHC
ND
ug/L
0.050
1
01/03/20 11:23
01/0812016:11
319-85-7
delta-BHC
ND
ug/L
0,050
1
01103/2011:23
01108/2016:11
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
1
01/03/20 11:23
01/08/20 16:11
58-89-9
Chlordane (Technical)
NO
ug/L
0.50
1
01/03/20 11:23
01/08/20 16:11
57-74-9
alpha -Chlordane
ND
ug/L
0.050
1
0110312011:23
01/08/2016.11
5103-71-9
gamma -Chlordane
ND
ug1L
0.050
1
0110312011:23
01/08/20 16:11
5103-74-2
4,4'-DDD
ND
ug/L
0.050
1
0110312011:23
01108/2016:11
72-54-8
4,4'-DDE
NO
ug1L
0.050
f
01103/2011:23
01108/2016:11
72-55-9
4.4'-DDT
NO
ug1L
0.050
1
01103/2011:23
01/08/20 16:11
50-29-3
Dieldrin
ND
ug/i_
0.050
1
01103/2011:23
01108/2016:11
60-57-1
Endosulfan I
NO
ug/L
0.050
1
01/03/20 11:23
01/08/20 16:11
959-98-8
Endosulfan II
ND
ug/L
0.050
1
01/03/20 11:23
01/08/20 16:11
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
1
01/03120 11:23
01/08/20 16:11
1031-07-8
Endrin
NO
ug/L
0.050
1
01/03/20 11 :23
01/08/20 16:11
72-20-8
Endrin aldehyde
ND
ug/L
0.050
1
01/03/20 11:23
01/08120 16:11
7421-93-4
Heptachlor
NO
ug/L
0.050
1
01103/2011:23
01/0812016:11
76-44-8
Heptachlor epoxide
NO
uglL
0.050
1
01/03/20 11:23
01/08/20 16:11
1024-57-3
PCB-1016 (Aroclor 1016)
NO
ug/L
0,50
1
01/03/20 11:23
01/08/20 16:11
12674-11-2
PCB-1221 (Aroclor 1221)
NO
ug/L
0.50
1
01/03/20 11:23
01/08/20 16:11
11104-28-2
PCB-1232 (Aroclor 1232)
NO
ug/L
0.50
1
01/03/20 11:23
01/08/20 16:11
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
1
01/03/20 11:23
01/08/20 16:11
53469-21-9
PCB-1248 (Aroclor 1248)
NO
ug/L
0.50
1
01/03/20 11:23
01/08/20 16:11
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0,50
1
01/03/20 11:23
01/08/20 16:11
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
1
01/03/20 11:23
01/08/20 16:11
11096-82-5
Toxaphene
NO
ug1L
0.50
1
01/0312011:23
01/013/2016:11
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
72
%
10-130
1
01/03/20 11:23
01/08/20 16:11
877-09-8
Decachlorobiphenyl (S)
10B
%
10-130
1
01/03/20 11:23
01/08/20 16:11
2051-24-3
200.7 MET ICP
Analytical Method: EPA200.7 Rev 4.4 1994 Preparation Method: EPA200.7 Rev 4.4 1994
Copper
10.3
ug1L
5.0
1
01/03/20 00:25
01/06/20 00:21
7440-50-8
Lead
ND
ug/L
5.0
1
01103/20 00:25
01/06/20 00:21
7439-92-1
Zinc
37.1
ug/L
10.0
1
01/03/20 00:25
01/06/20 00:21
7440-66-6
625 RVE
Analytical Method: EPA 625.1
Preparation Method:
EPA 625.1
Acenaphthene
NO
ug/L
5.0
1
01/06/2012:13
01/0612015:57
83-32-9
Acenaphthylene
NO
ug/L
5.0
1
01/06/2012:13
0110612015:57
208-96-8
Anthracene
NO
ug/L
5.0
1
0110612012:13
0110612015:57
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
0110612012:13
0110612015:57
56-55-3
Benzo(a)pyrene
NO
ug/L
5.0
1
01/0612012:13
01/06/2015:57
50-32-8
Benzo(b)fluoranthene
NO
ug/L
5.0
1
01/0612012713
01/06/2015:57
205-99-2
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in
full.
Date: 01/15/2020 07:36 AM
without the written consent of Pace Analytical
Services,
LLC,
Page 4 of 22

aceAnalyifical
www.pecelobs.t:om
ANALYTICAL RESULTS
Project: Stormwater Sampling
Pace Project No.: 92459129
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Samples Lab ID: 92459129001 Collected: 12/30/19 11:00 Received: 01102/20 13:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method: EPA625.1 Preparation Method: EPA625.1
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
01106/2012:13
01106/2015:57
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
01/06/2012:13
01/06/2015:57
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
01/06/20 12:13
01/06/20 15:57
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
01/06/2012:13
01/06/2015:57
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
01/06/2012:13
0110612015:57
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
01106/2012:13
01106/2015:57
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
01/06/20 12:13
01106/20 15:57
111-44-4
2-Chtoronaphthalene
ND
uglL
5.0
1
01106/2012:13
01/06/2015:57
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
01/0612012:13
01/0612015:57
95-57-B
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
01/06/20 12:13
01/06/20 15:57
7005-72-3
Chrysene
ND
ug/L
5.0
1
01/06/2012:13
01/0612015:57
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
01/0612012:13
01/0612015:57
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
01/06/2012:13
01/0612015:57
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
01/06/2012:13
01/0612015:57
120-83-2
Diethylphtha late
ND
ug/L
5.0
1
01/06/2012:13
01/06/2015:57
84.66-2
2,4-Dimethylphenol
ND
ug1L
10,0
i
01/06/2012:13
01/0612015:57
105-67-9
Dimethylphthalate
ND
ug1L
5.0
1
0110612012:13
01/06/2015:57
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
01/06/2012:13
01/06/2015:57
84-74-2
4, 5-Dini tro-2-methyl phenol
ND
ug/L
20,0
1
01/06/2012713
01/06/2015:57
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
01106/2012:13
01106/2015:57
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
01106/2012:13
01106/2015:57
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
01106/2012;13
0110612015:57
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
01/06/2012:13
01/06/2015:57
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
01/06/2012:13
01/06/2015:57
117-81-7
Fluoranlhene
ND
ug/L
5.0
1
01106/2012:13
0110612015:57
206-44-0
Fluorene
ND
ug/L
5.0
1
0110612012:13
01106/2015:57
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
01106/2012:13
01106/2015:57
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
01/0612012:13
01106/2015:57
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
01/0612012:13
01106/2015:57
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
01/0612012:13
0110612015:57
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
01106/2012:13
01/0612015:57
193-39-5
Isophorone
ND
uglL
10.0
1
01106/2012:13
01/06/2015:57
78.59-1
Naphthalene
ND
uglL
5.0
1
01/0612012;13
01/06/2015757
91-20-3
Nitrobenzene
ND
uglL
5.0
1
01/0612012:13
01/0612015:57
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
01106/2012:13
01/06/2015:57
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
01/06/2012:13
01/0612015:57
100-02-7
N-Nitrosodimethylamine
N❑
ug/L
5.0
1
01/0612012:13
01/06/2015:57
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
01/06/2012:13
0110612015:57
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
01/06/2012:13
0110612015:57
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
01/06/2012:13
01106/2015:57
108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
01/0612012:13
01/0612015:57
87-86-5
Phenanthrene
ND
ug/L
5.0
1
01106/2012:13
01106/2015:57
85-01-8
Phenol
ND
ug/L
5.0
1
01106/2012:13
01/06/2015:57
108-95-2
Pyrene
ND
ug/L
5.0
1
01/0612012:13
01/06/2015:57
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
01/06/2012:13
0110612015:57
120.82-1
2,4,6-Trichlorophenol
N❑
ug/L
10.0
1
01/0612012:13
01/0612015:67
88-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/15/2020 07:36 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 22

r
(�15'cieAnalytical*
www.pacetgbs.com
Project:
Pace Project No.:
Sample: Samples
625 RVE
Stormwater Sampling
92459129
Parameters
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol(S)
2,4,6-Tribromophenol (S)
624 Volatile Organics
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chioroethane
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1, 1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis- 1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1, 2-Trichloroethane
Trichloroethene
TrichIorofluoromethane
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
2540D Total Suspended Solids
Total Suspended Solids
Date: 01/15/2020 07:36 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92459129001 Collected: 12/30/19 11:00 Received: 01/02/20 13:38 Matrix: Water
Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Analytical Method: EPA625.1 Preparation Method: EPA625.1
53
%
51
%
86
%
39
%
49
%
86
%
Analytical Method:
EPA624A
NO
ug/L
NO
ug/L
NO
ug]L
NO
ug/L
NO
ug/L
NO
ug1L
ND
ug/L
ND
ug1L
NO
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
ND
ug1L
19.7
ug/L
ND
ug1L
NO
ug/L
ND
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
ND
ug/L
NO
ug/L
NO
ug/L
NO
ug/L
ND
ug/L
•103 %
80 %
103 %
Analytical Method: SM 254OD-2011
8.3 mg1L
10-120
1
01106/2012:13 01106/2015:57 4165-60-0
15-120
1
01/06/2012:13 01/0612015:57
321-60-8
11-131
1
01/06/2012:13 01/06/2015:57
1718-51-0
10-120
1
01106/2012:13 01/06/2015:57
13127-88-3
10-120
1
01/06/2012A3 01/06/2015:57
367-12-4
10-137
1
01/06/2012:13 01/06/2015:57
118-79-6
1.0
1
01/0312016:05
71-43-2
2.0
1
01/03/2016:05
75-27-4
2.0
1
01 /03/20 16:05
75-25-2
2.0
1
01103/2016:05
74-83-9
2.0
1
01 /03/20 16:05
56-23-5
2,0
1
01 /03120 16:05
108-90-7
2.0
1
01/0312016:05
75-00-3
2.0
1
01/03/2016:05
67-663
2.0
1
01103/2016:05
74-87-3
2.0
1
01 /03/20 16:05
124-48-1
2.0
1
01103/2016:05
95-50-1
2.0
1
0110312016:05
541-73-1
2.0
1
01 /03120 16:05
106-46-7
2.0
1
01/0312016:05
75-34-3
2.0
1
01 /03/20 16:05
107-06-2
2.0
1
0110312016:05
75-35-4
2.0
1
01/03/20 16:05
156-59-2
2.0
1
01/03/20 16:05
156-60-5
2.0
1
01/03/2016:05
78-87-5
2.0
1
01/03/20 16:05
10061-01-5
2.0
1
01/03/20 16:05
10061-02-6
1.0
1
01 /03120 16:05
100-41-4
2.0
1
01103/2016:05
75-09-2
2.0
1
01103/2016:05
79-34-5
2,0
1
01 /03/20 16:05
127-18-4
1.0
1
01 /03120 16:05
108-88-3
2.0
1
01/03/2016:05
71-55-6
2.0
1
01/03/2016:05
79-00-5
2.0
1
01/0312016:05
79-01.6
2.0
1
01/03/2016:05
75-69-4
2.0
1
01/03/2016:05
75-01.4
70-130
1
01/03/2016:05
460-00-4
70-130
1
01/03/2016:05
2037-26-5
70-130
1
01 /03/20 16:05
17060-07-0
2.5
1
01/03120 10:29
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 22

aceAnalytical
ntwtl.wailbs.eam
QUALITY CONTROL DATA
Project: Stormwater Sampling
Pace Project No.: 92459129
OC Batch: 519329 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92459129001
METHOD BLANK: 2779561
Associated Lab Samples: 92459129001
Parameter Units
Oil and Grease mg/L
LABORATORY CONTROL. SAMPLE? 2779562
Parameter Units
Oil and Grease mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 01/14/2016:52
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
40 36.0 90 78-114
MATRIX SPIKE SAMPLE: 2779563
92459833002 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L ND 40 7.8 17 78-114 M1
Results presented on this page are In the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2020 07:36 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 22

leAnalytical
www4mcetaes.cam
QUALITY CONTROL DATA
Project: Stormwater Sampling
Pace Project No.: 92459129
QC Batch: 517676 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92459129001
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 2771558
Matrix: Water
Associated Lab Samples: 92459129001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Copper
ug1L
ND 5.0
01/05/20 23:59
Lead
ug/L
ND 5.0
01/05120 23:59
Zinc
ug1L
ND 10.0
01/05/20 23:59
LABORATORY CONTROL SAMPLE: 2771559
Spike
LCS
LCS % Rec
Parameter
Units
Cone.
Result
% Rec Limits Qualifiers
Copper
ug/L
500
483
97 85-115
Lead
ug/L
500
482
96 85-115
Zinc
ug/L
500
474
95 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2771560
2771561
MS
MSD
92459126001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits RPD Qual
Copper ug/L
<5.0
500
500
512
500
102
99
70-130 3
Lead ug1L
<5.0
500
500
500
484
100
97
70-130 3
Zinc ug1L
<10.0
500
500
505
490
100
97
70-130 3
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 01 /15/2020 07:36 AM without the written censent of Pace Analytical Services, LLC. Page 8 of 22

Iac
(
eAnalytical
tiWW PkaC1t1bS.CWn
QUALITY CONTROL DATA
Project: Stormwater Sampling
Pace Project No.: 92459129
CC Batch: 517794 Analysis Method: EPA 624A
QC Batch Method: EPA624.1 Analysis Description: 624 MSV
Associated Lab Samples: 92459129001
METHOD BLANK: 2771970 Matrix: Water
Associated Lab Samples: 92459129001
Parameter
Units
1,1,1-Trichloroethane
ug/L
1,1,2,2-Tetrachloroethane
ug/L
1,1,2-Trichloroethane
ug/L
1,1-Dichloroethane
ug/L
1,1-Dichloroethene
ug/L
1,2-Dichlorobenzene
ug/L
1,2-Dichloroethane
ug1L
1,2-Dichloropropane
ug1L
1,3-Dichlorobenzene
uglL
1,4-Dichlorobenzene
ug1L
Benzene
uglL
Bromodichloromethane
uglL
Bromoform
ug/L
Bromomethane
ug/L
Carbon tetrachloride
ug1L
Chlorobenzene
ug/L
Chloroethane
ug/L
Chloroform
ug/L
Chloromethane
ug1L
cis-1,2-Dichloroethene
ug/L
cis- 1,3-Dichloropropene
ug1L
Dibromochloromethane
ug1L
Ethylbenzene
uglL
Methylene Chloride
ug1L
Tetrachloroethene
ug1L
Toluene
uglL
trans-1,2-Dichloroethene
uglL
trans- 1,3-Dichloropropene
uglL
Trichloroethane
uglL
Trichlorofluoromethane
ug/L
Vinyl chloride
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
Blank
Result
Reporting
Limit
Analyzed
ND
2.0
D110312015:30
ND
2.0
01/03/2015:30
ND
2.0
01/03/201610
ND
2.0
01/0312015:30
ND
2.0
01/03/2015:30
ND
2.0
01/03/2015:30
ND
2.0
01/03/2015:30
ND
2.0
01103/2015:30
ND
2.0
01103/2015:30
NO
2.0
01/03/2015:30
ND
1.0
01/03/2015;30
ND
2.0
0110312015:30
ND
2.0
01/0312015:30
ND
2.0
01/0312015:30
ND
2.0
01/03/20 15:30
ND
2.0
01/03/2015:30
ND
2.0
01/03/2015:30
ND
2.0
01/03/2015:30
ND
2.0
01/0312015:30
ND
2.0
01/03/2015:30
ND
2.0
01/03/2015:30
ND
2.0
0110312015:30
ND
1.0
01/03/2015:30
ND
2.0
01103/2015:30
ND
2.0
01/03/2015:30
ND
1.0
01/03/2015:30
ND
2.0
01/03/2015;30
ND
2.0
01/03/2015:30
ND
2.0
01/0312015:30
ND
2.0
01 /03120 15:30
ND
2.0
01/03/20 15:30
102
70-130
01/0312015:30
99
70-130
01/03/2015:30
84
70-130
01/03/2015:30
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2771971
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane uglL 20 19.4 97 70-130
1,1,2,2-Tetrachloroethane ug1L 20 19.8 99 60-140
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/15/2020 07;36 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 22

la'ceAnalytical
tvww.paalacs.com
QUALITY CONTROL DATA
Project: Stormwater Sampling
Pace Project No.: 92459129
LABORATORY CONTROL SAMPLE:
Parameter
2771971
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,2-Trichloroethane
uglL
20
15.1
76
70-130
1,1-Dichloroethane
uglL
20
16.5
82
70-130
1,1-Dichloroethene
ug1L
20
18.0
90
50-150
1,2-Dichiorobenzene
uglL
20
20.2
101
65-135
1,2-Dichloroethane
uglL
20
19.5
98
49-155
1,2-Dichloropropane
ug/L
20
20.0
100
35-165
1,3-Dichlorobenzene
ug/L
20
20.0
100
70-130
1,4-Dichlorobenzene
ug/L
20
20.1
100
65-135
Benzene
ug/L
20
19.7
98
65-135
Bromod ichlo rometha ne
ug1L
20
19.6
98
65-135
Bromoform
uglL
20
21.6
108
70-130
Bromomethane
ug1L
20
25.2
126
15-185
Carbon tetrachloride
ug1L
20
18.4
92
70-130
Chlorobenzene
ug1L
20
19.8
99
65-135
Chloroethane
ug/L
20
113A
92
40-160
Chloroform
ug/L
20
19.3
96
70-135
Chloromethane
ug1L
20
17.5
88
1-205
cis-1,2-Dichloroethene
uglL
20
17.5
87
68-146
cis- 1,3-Dichloropropene
uglL
20
19.3
97
25-175
Dibromochtoromethane
uglL
20
19.1
95
70-135
Ethylbenzene
uglL
20
19.8
99
60-140
Methylene Chloride
uglL
20
17.8
89
60-140
Tetrachloroethene
uglL
20
18.5
92
70-130
Toluene
ug/L
20
17.3
86
70-130
trans-1,2-Dichloroethene
ug/L
20
18.8
94
70-130
trans-1,3-Dichloropropene
U91L
20
17.0
85
50-150
Trichloroethene
uglL
20
20.3
102
65-135
Trichlorofluoromethane
ug1L
20
18.1
91
50-150
Vinyl chloride
uglL
20
18.0
90
5-195
1,2-Dichloroethane-d4 (S)
%
103
70-130
4-Bromofluorobenzene (S)
%
105
70-130
Toluene-d8 (S)
%
89
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2771972
MS
Parameter
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
92459129001 Spike
Units
Result
Cone.
ug1L
ND
20
uglL
ND
20
ug1L
ND
20
ug1L
ND
20
ug1L
ND
20
uglL
NO
20
ug1L
ND
20
ug1L
ND
20
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
2771973
MSD
Spike
MS
MSD
MS
MSD
% Rec
Cone.
Result
Result
% Rec
% Rec
Limits
20
19.6
21.5
98
108
52-162
20
20.9
22.7
105
113
46-157
20
18.9
19.5
94
97
52-150
20
18.4
20.1
92
101
59-155
20
19.7
23.1
99
115
1-234
20
20.0
20.6
100
103
18-190
20
19.8
20.8
99
104
49-155
20
19.9
21.2
99
106
1-210
RPD
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/15/2020 07:36 AM without the written consent of Pace Analytical Services, LLC.
10
8
3
9
16
3
5
7
Qual
Page 10 of 22

aceAnalytical®
wrfw.pacelaba.com
QUALITY CONTROL DATA
Project: Stormwater Sampling
Pace Project No.: 92459129
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2771972
MS
9245912,3001 Spike
Parameter
Units
Result Conc
1,3-Dichlorobenzene
uglL
NO
1,4-Dichlorobenzene
uglL
NO
Benzene
uglL
NO
Bromodichloromethane
uglL
NO
Bromoform
uglL
NO
BTOmomethane
uglL
NO
Carbon tetrachloride
ug/L
NO
Chlorobenzene
ug/L
NO
Chloroethane
ug/L
ND
Chloroform
ug/L
ND
Chloromethane
ug/L
ND
cis-1,2-Dichloroethene
ug/L
19.7
cis- 1,3-Dichloropropene
uglL
NO
Dibromochloromethane
ug/L
ND
Ethylbenzene
uglL
ND
Methylene Chloride
ug1L
NO
Tetrachloroethene
uglL
NO
Toluene
uglL
NO
trans-1,2-Dichloroethene
uglL
NO
trans-1,3-Dichloropropene
ug/L
NO
Trichooroethene
ug/L
ND
Trichlorofluoromethane
ug/L
ND
Vinyl chloride
ug/L
ND
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
2771973
MSD
Spike MS
Conc. Result
20
20
19.9
20
20
20.1
20
20
20.5
20
20
19.1
20
20
21.4
20
20
19.0
20
20
18.8
20
20
20.3
20
20
19.7
20
20
18.0
20
20
22.2
20
20
33.1
20
20
18.6
20
20
20.3
20
20
20.1
20
20
19.0
20
20
20.4
20
20
17.4
20
20
20.1
20
20
18.2
20
20
22.3
20
20
18.8
20
20
19.7
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MSD
MS
MSD
% Rec
Result
% Rec
% Rec
Limits
RPD
20.7
99
104
59-156
4
21.0
100
105 '
18-190
5
20.9
102
105
37-151
2
20.7
96
104
35-155
8
22.5
107
113
45-169
5
19.7
95
98
1-242
3
20.3
94
101
70-140
8
21.1
101
105
37-160
4
21.3
99
107
14-230
8
20.6
90
103
51-138
14
21.8
111
109
1-273
1
39.9
67
101
45-174
19
17.4
93
87
1-227
7
20.6
101
103
53-149
1
21.0
101
105
37-162
4
20.6
95
103
1-221
8
20.2
102
101
64-148
1
18.4
87
92
47-150
6
21.7
100
109
54-156
8
18.9
91
95
17-183
4
23.4
105
111
70-157
5
20.2
94
101
17-181
7
20.3
96
99
1-251
3
95
96
70-130
99
104
70-130
86
88
70-130
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01115/2020 07:36 AM without the written consent of Pace Analytical Services, LLC.
Clual
Page 11 of 22

lacmnalyticals
www.pscettdtstem
Project: Stormwater Sampling
Pace Project No.: 924591213
QC Batch: 517722
QC Batch Method: EPA608.3
Associated Lab Samples. 92459129001
METHOD BLANK: 2771654
Associated Lab Samples: 92459129001
Parameter
Units
4,4'-DDD
ug1L
4,4'-DDE
ug/L
4,4'-DDT
ug1L
Aldrin
ug/L
alpha-BHC
ug/L
alpha -Chlordane
ug/L
beta-BHC
ug/L
Chlordane (Technical)
ug/L
delta-BHC
ug/L
Dieldrin
ug/L
Endosulfan I
ug/L
Endosulfan 11
ug/L
Endosulfan sulfate
ug/L
Endrin
ug/L
Endrin aldehyde
ug/L
gamma-BHC (Lindane)
ug/L
gamma -Chlordane
ug/L
Heptachlor
ug1L
Heptachlor epoxide
ug/L
PCB-1016 (Aroclor 1016)
ug/L
PCB-1221 (Aroclor 1221)
ug/L
PCB-1232 (Aroclor 1232)
ug/L
PCB-1242 (Aroclor 1242)
ug/L
PCB-1248 (Aroclor 1248)
ug/L
PCB-1254 (Aroclor 1254)
ug/L
PCB-1260 (Aroclor 1260)
ug/L
Toxaphene
ug/L
Decachlorobiphenyl (S)
%
Teirachloro-m-xylene (S)
%
QUALITY CONTROL DATA
Analysis Method: EPA 608.3
Analysis Description: 608 PCB Pest Red Vol
Matrix: Water
Blank
Result
Reporting
Limit
Analyzed
ND
0.050
01/08/2017:25
ND
0.050
01/08/2017:25
ND
0.050
01/0812017:25
ND
0.050
01108/2017:25
ND
0.050
01/0812017:25
ND
0,050
0110812017:25
ND
0,050
01/08/2017:25
ND
0.50
0110812017:25
ND
0.050
01 /08120 17:25
ND
0.050
01/08/2017:25
ND
0.050
01/08/20 17:25
ND
0,050
01/08/2017:25
ND
0.050
01108/2017:25
ND
0.050
01/08/2017:25
ND
0.050
01/08/2017:25
ND
0.050
01/08/2017:25
ND
0.050
01/08/2017:25
ND
0.050
01/08/2017:25
ND
0.050
0110812017:25
ND
0.50
0110812017:25
ND
0.50
01 /08/20 17:25
ND
0.50
01108/2017:25
ND
0,50
01/08/2017:25
ND
0.50
01/0812017:25
ND
0.50
01/08/2017:25
ND
0.50
01/08/2017:25
ND
0.50
01/08/2017:25
91
10-130
01108/2017:25
64
10.130
01108/2017:25
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
2771655
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
4,4'-DDD
ug/L
0.25
0.18
73
31-141
4,4'-DDE
ug/L
0.25
0.18
73
30.145
4A-DDT
ug/L
0.25
0.20
78
25-160
Aldrin
ug/L
0.25
0.17
68
42-140
alpha-BHC
ug/L
0.25
0.16
65
37-140
alpha -Chlordane
ug/L
0.25
0.18
72
45-140
beta-BHC
ug/L
0,25
0.21
85
17-147
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/15/2020 07:36 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 22

aceAnalytical"
wlrw,p e1IAbS.t:turl
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, 128078
[phone]
Project: Stormwater Sampling
Pace Project No.. 92459129
LABORATORY CONTROL SAMPLE:
2771655
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
delta-BHC
u9i
0.25
0.17
67
19-140
Dieldrin
uglL
0.25
0.17
69
36-146
Endosulfan I
ug1L
0.25
0.17
69
45-153
Endosulfan II
ugll-
0.25
0.17
68
1-202
Endosulfan sulfate
uglL
0.25
0.18
73
26-144
Endrin
ug/L
0.25
0.17
68
30-147
Endrin aldehyde
ug/L
0.25
0.19
77
50-150
gamma-BHC (Lindane)
ug/L
0.25
0.18
72
32-140
gamma -Chlordane
ug/L
0.25
0.15
60
45-140
Heptachlor
ugfL
0.25
0.16
65
34-140
Heptachlor epoxide
ug/L
0,25
0.18
72
37-142
Decachlorobiphenyl (S)
%
95
10-130
Tetrachloro-m-xylene (S)
%
66
10-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2771656
2771657
MS
MSD
92455188004
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
4,4'-DDD
ug1L
NO
0.25
0.25
0.17
0.18
69
73
31-141
5
4,4'-DDE
uglL
ND
0.25
0.25
0,16
0.18
65
70
30-145
9
4,4'-DDT
i
ND
0.25
0.25
0.18
0.19
70
75
25-160
6
A)drin
uglL
ND
0.25
0.25
0A5
0.17
61
66
42-140
8
alpha-BFiC
uglL
ND
0.25
0.26
0,16
0.16
65
65
37-140
0
alpha -Chlordane
uglL
NO
0.25
0.25
0.17
0.18
68
73
45-140
7
beta-BHC
uglL
ND
0.25
0.25
0.21
0.21
84
85
17-147
1
delta-BHC
uglL
ND
0.25
0.25
0.16
0.17
66
66
19-140
1
Dieldrin
uglL
NO
0.25
0.25
0.17
0.17
66
70
36-146
5
Endosulfan I
uglL
ND
0.25
0.25
0.17
0.17
68
70
45-153
3
Endosulfan II
uglL
NO
0.25
0.25
0.17
0.17
67
69
1-202
3
Endosulfan sulfate
uglL
NO
0.25
0.25
0.18
0.19
74
74
26-144
1
Endrin
uglL
NO
0.25
0.25
0.16
0.17
66
68
30-147
3
Endrin aldehyde
ug1L
NO
0.25
0.25
0.17
0.17
70
70
50-150
0
gamma-BHC (Lindane)
uglL
NO
0,25
0.25
0.18
0.17
72
70
32-140
4
gamma -Chlordane
ug1L
ND
0.25
0.25
0,13
0.14
51
55
45-140
7
Heptachlor
i
ND
0.25
0.25
0.15
0.16
61
64
34-140
5
Heptachlor epoxide
uglL
ND
0.25
0.25
0.17
0,17
68
70
37.142
3
Decachlorobiphenyl (S)
%
80
76
10-130
Tetrachloro-m-xylene (S)
%
67
62
10-130
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Ws report shall not be reproduced, except in full,
❑ate: 01/15/2020 07:36 AM without the written consent of Pace Analytical Services, Lit;.
Page 13 of 22

laneAnalyticalo
ttlww pacellbs,tam
QUALITY CONTROL DATA
Project: Stormwater Sampling
Pace Project No.: 92459129
QC Batch: 517914 Analysis Method: EPA 625.1
QC Batch Method: EPA625.1 Analysis Description: 625 MSS
Associated Lab Samples: 92459129001
METHOD BLANK: 2772492
Associated Lab Samples: 92459129001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug1L
ND
5.0
01106/2018:29
2,2'-Oxybis(t-chloropropane)
ug1L
NO
5.0
0110612018:29
2,4,6-Trichlorophenol
ug1L
NO
10.0
01/06/2018:29
2,4-Dichlorophenul
ug1L
NO
5.0
0110612018:29
2,4-Dimethylphenol
ug1L
ND
10,0
01106/2018:29
2,4-Dinitrophenol
ug1L
ND
50.0
01/0612018:29
2,4-Dinitrotoluene
ug/L
NO
5.0
01/0612018:29
2,6-Dinitrotoluene
ug/L
NO
5.0
01/06/2018:29
2-Chloronaphthalene
ug/L
NO
5.0
01/06/2018:29
2-Chlorophenol
ug1L
ND
5.0
01/06/2018:29
2-Nitrophenol
ug/L
NO
5.0
01/0612018:29
3,3'-Dichlorobenzidine
ug/L
NO
25.0
01106/2018:29
4,6- Di nitro-2-methyl phenol
ug/L
NO
20.0
01/06/2018:29
4-Bromophenylphenyl ether
ug/L
NO
5.0
01/06/20 18:29
4-Chloro-3-methylphenol
ug1L
NO
5.0
01/06/2018:29
4-Chlorophenylphenyl ether
ug/L
NO
5.0
01/06/20 18:29
4-Nitrophenol
ug/L
NO
50.0
01/06/2018:29
Acenaphthene
ug1L
NO
5.0
01/06/2018:29
Acenaphthylene
ug1L
NO
5.0
01/06/2018:29
Anthracene
ug1L
NO
5.0
01/0612018:29
Benzo(a)anthracene
ug1L
NO
5.0
0110612018:29
Benzo(a)pyrene
ug1L
NO
5.0
01/06/2018:29
Benzo(b)fluoranthene
ug/L
NO
5.0
01/06/2018:29
Benzo(g,h,)perylene
ug/L
ND
5.0
01/06/2018:29
Benzo(k)fluoranthene
ug/L
ND
5.0
0110612018:29
his(2-Chloroethoxy)methane
ug1L
ND
10.0
0110612018:29
bis(2-Chloroethyl) ether
ug1L
ND
5.0
01/06/20 18:29
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
01/0612018:29
Butylbenzylphthalate
ug/L
NO
5.0
01106/2018:29
Chrysene
ug/L
NO
5.0
01/06/2018:29
Di-n-butylphthalate
ug/L
NO
5.0
01/06/2018:29
Di -n-octylphth a late
ug/L
NO
5.0
01/0612018:29
Dibenz(a,h)anthracene
ug/L
NO
5.0
01/06/2018:29
Diethylphthalate
ug/L
NO
5.0
01/06/2018:29
Dimethylphthalate
ug/L
NO
5.0
01/0612018:29
Fluoranthene
ug1L
NO
5.0
01106/2018:29
Fluorene
ug1L
NO
5.0
01106/2018:29
Hexachloro-1,3-butadiene
ug1L
NO
5,0
01106/2018:29
Hexachlorobenzene
ug1L
NO
5.0
01/06/2018:29
Hexachlorocyclopentadiene
ug1L
NO
10.0
01106/2018:29
Hexachloroethane
ug1L
NO
5.0
01/06/2018.29
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 01/15/2020 07:36 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 22

ace Analytical
NNW Facelahs.com
QUALITY CONTROL DATA
Project: Stormwater Sampling
Pace Project No.: 92459129
METHOD BLANK: 2772492
Associated Lab Samples: 92459129001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Indeno(1,2,3-cd)pyre ne
uglL
ND
5.0
01106/2018:29
Isophorone
uglL
ND
10.0
01/0612018:29
N-N itroso-di -n-propyla mine
uglL
ND
5.0
01/0612018:29
N-Nitrosodimethytamine
ugll-
ND
5.0
0110612018:29
N-Nitrosodiphenylamine
uglL
ND
10.0
01/06/20 18:29
Naphthalene
uglL
ND
5.0
01106/2018:29
Nitrobenzene
ug1L
ND
5.0
01/0612018:29
Pentachlorophenol
ug1L
ND
10.0
01106/2018:29
Phenanthrene
u911-
ND
5.0
01/0612018:29
Phenol
ug1L
ND
5.0
01/0612018:29
Pyrene
ug/L
ND
5.0
01/0612018:29
2,4,6-Tribromophenol (S)
%
127
10-137
D1106120 18:29
2-Fluorobiphenyl (S)
%
96
15-120
01/06/20 18:29
2-Fluorophenol (S)
%
88
10-120
01/06/20 18:29
Nitrobenzene-d5 (S)
%
94
10-120
01/06/20 18:29
Phenol-d6 (S)
%
72
10-120
01/06/20 18:29
Terphenyl-d14 (S)
%
124
11-131
01/06/20 18:29
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2772493
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
uglL
50
44.5
89
44-142
2,2'-Oxybis(1-chloropropane)
uglL
50
41.6
83
36-166
2,4,6-Trichlorophenol
uglL
50
50.1
100
37-144
2,4-Dichlorophenol
uglL
50
47.3
95
1-191
2,4-Dimethylphenol
uglL
50
46.0
92
32-119
2,4-Dinitrophenol
uglL
250
309
124
1-181
2,4-Dinitrotoluene
uglL
50
52.4
105
39-139
2,6-Dinitrotoluene
ug1L
50
50.9
i02
50-158
2-Chloronaphthalene
ug1L
50
44.6
89
60-118
2-Chlorophenol
ug/L
5D
44.7
89
23-134
2-Nitrophenol
ug/L
50
50.6
101
29-182
3,3'-Dichlorobenzidine
ug/L
100
93.2
93
1-262
4,6-Dinitro-2-methylphenol
ug1L
100
138
138
1-181
4-Bromophenylphenyl ether
ug/L
50
47.3
95
53-127
4-Chloro-3-methylphenol
ug1L
100
95.6
96
22-147
4-Chlorophenylphenyl ether
ug1L
50
45.0
90
25-158
4-Nitrophenol
ug1L
250
177
71
1-132
Acenaphthene
ug1L
50
45.8
92
47-145
Acenaphthylene
uglt_
50
49.8
100
33-145
Anthracene
ug1L
50
50.6
101
1-166
Benzo(a)anthracene
uglL
50
51.3
103
33-143
Benzo(a)pyrene
uglL
50
54.4
109
17-163
Benzo(b)fluoranthene
uglL
50
52.6
105
24-159
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/15/2020 07:36 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 22

aceAnalytical
'
wtirr.pacal163.t4t0
QUALITY CONTROL DATA
Project: Stormwater Sampling
Pace Project No.: 92459129
LABORATORY CONTROL SAMPLE 2772493
Parameter
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Benzo(g,h,i)perylene
uglL
50
55.1
110
1-219
Benzo(k)ffuoranthene
uglL
50
53.9
108
11-162
bis(2-Chlomethoxy)methane
uglL
50
42.4
85
33-184
bis(2-Chloroethyl) ether
uglL
50
42.7
85
12-158
bis (2-Ethylhexyl)phth a late
uglL
50
52.9
106
8-158
Butylbenzylphthalate
ug/L
50
52A
104
1-152
Chrysene
uglL
50
51.9
104
17-168
Di-n-butylphthalate
uglL
50
50.8
102
1-118
Di-n-octylphthalate
uglL
50
57.4
115
4-146
Dibenz(a,h)anthracene
uglL
50
54.1
108
1-227
Diethylphthalate
uglL
50
47.7
95
1-114
Dimethylphthalate
ug/L
50
46.0
92
1-112
Fluoranthene
uglL
50
52.5
105
26-137
Fluorene
uglL
50
47.3
95
59-121
Hexachloro-1,3-butadiene
uglL
50
45.4
91
24-116
Hexachlorobenzene
uglL
50
49.8
100
1-152
Hexachlorocyclopentad iene
uglL
50
53.4
107
25-150
Hexachloroethane
uglL
50
41.9
84
40-113
Indeno(1,2,3-cd)pyrene
uglL
50
53.7
107
1-171
Isophorone
uglL
50
45.2
90
21-196
N-Nitroso-di-n-propylamine
uglL
50
43.8
88
1-230
N-N itrosod imethyl a mine
ug1L
50
37.6
75
25-150
N-Nitrosod iphenyla mine
uglL
50
48.0
96
25-150
Naphthalene
uglL
50
45.8
92
21-133
Nitrobenzene
uglL
50
44.1
88
35-180
Pentachlorophenol
uglL
100
127
127
14-176
Phenanthrene
uglL
50
49.4
99
54-120
Phenol
ug1L
50
36.0
72
5-112
Pyrene
ug1L
50
52.6
105
52-115
2,4,6-Tribromophenol (S)
%
135
10-137
2-Fluorobiphernyl (S)
%
88
15-120
2-Fluorophenot (S)
%
82
10-120
Nitrobenzene-d5 (S)
%
86
10-120
Phenol-d6 (S)
%
69
10-120
Terphenyl-d14 (S)
%
102
11-131
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fufi,
Date: 01/15/2020 07:36 AM without the written consent of Pace Analytical Services, LLC.
Page 16 of 22

laceAnalytical
>owpacelobixem
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Stormwater Sampling
Pace Project No.: 92459129
QC Batch: 517749
Analysis Method:
SM 2540D-2011
QC Batch Method: SM 254OD-2011
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92459129001
METHOD BLANK: 2771740
Matrix:
Water
Associated Lab Samples: 92459129001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 01/03/20 10:28
LABORATORY CONTROL SAMPLE: 2771741
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250
252
101 90-110
SAMPLE DUPLICATE: 2771742
92459105001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
346
400 14
SAMPLE DUPLICATE: 2771743
92459087003
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
119
111 7
Results presented on this page are In the units indicated by the" Units" column except where an alternate unit Is presented to the right of the resuit.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/15/2020 07:36 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 22

aOAnalj6cal
www.pacefsbs tom
QUALIFIERS
Project: Slormwater Sampling
Pace Project No.: 92459129
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenythydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether,
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N -Nitrosodiphenyl a mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /15/2020 07:36 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 22

lacmnalyticalo
WW.p&Cel&ha.C=
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Stormwater Sampling
Pace Project No.: 92459129
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92459129001
Samples
EPA 16648
519329
92459129001
Samples
EPA608.3
517722
EPA608.3
517876
92459129001
Samples
EPA 200.7 Rev 4.4 1994
517676
EPA 200.7 Rev 4.4 1994
517687
92459129001
Samples
EPA625.1
517914
EPA625.1
517981
92459129001
Samples
EPA 624.1
517794
92459129001
Samples
SM 254OD-2011
517749
Date: 01/15/2020 07:36 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 22

Document Name:
Document Revised: February 7, 2018
_ CeAnaly hVl
Y
Sample Condition Upon Recei t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR•CS-433-Rev.05
Pace Carolinas Quality Office
Laboratory receiving samples: �,
Asheville ❑ Eden❑ Greenwood ❑ Huntersvllle. jam' Raleigh[] Mechanicsville[]
Client Name: /�, W® 92459 1 69
5 "�4 C r'Vt� �'G� �"llaGc'�7'5 Project i.
D q I I II
Courier: ❑Fed Ex ❑USPS []Client 111:111,111
❑ Commercial []Pace ❑Other: 924SO129
Custody Seal Present? ❑Yes ANos6als Intact? ❑Yes
Datellnitiah Person Examining Contents:
Packing Material: []Bubble Wrap ubble Bags ❑None [] Other .-.Blulagical TisWe F en?
Thermomr ❑Y
etees ❑No N/A
I Gun ID: 92TO5$ rype Wee:et ❑Slue ©None
Cooler Temp I'Cl: Correction Factor: Add/Subtract VC) O.0°C
IT). J : Temp should be above freezing to 6'C
Cooler TempCorrected
❑5ampies out of temp criteria. Samples an ice, cooling process
hasbegun
USDA Regulated Sall KNIA, water sample)
Did samples oriidnate In a quarantine zone wlthin the United States: CA, NY, or SC (check maps)? Did samples oriF;lnate From a foreign source (Intemat€anally.
Yes No
Indudiag Hawaii and Puerto Ricc)? ❑Yes ❑No
r
Commentt/-Ultere anc , .
Chain of Custody Present?
Yes
Na
NIA
1.
Samples Arrived within Hold Time?
es
[]No_
N A
2,
Short Hold Time Analysis 1<72 hr. ?
Yes
a
N A
3.
Rush TurnAround Time Requested?
ElVes
K5/ ❑NIA
4.
sufficient Volta me? "
es
Na
r!/A
S.
Correct Containers Used?
-Pace Containers Used?
(-
s
ON-
ONO
ON/A
[-]N/A
_
6.
Containers Intact?
JR<
ONo
N A
7.
Dlssalved analysis: '_acz+" les Field Fittered?
Yes
a
❑N/A
B.
Sample Labels Match COC?
-includes Date/Time/l0/Anal ds Matrix:
Gm.--
es
/
❑No
❑N/A
'w/�,
C0G
'Heads ace in VOA Vials (>S-5mm)? :'
Yes
Now
N/A
t0. G. ro CS I•-G�
Trip Blank Present?
Trip Blank Custod Seals Present?
OYes,
OYes
2 o
ONo
❑N/A
A
11,
COiMMENTS/SAMPLEIDISCREPANCY I I Field{ Data Required? Des ❑No �
CO '• . /7•�_ �. � f L��l 5s:yrr n l� i � .J-:�/3C�.� �� S. � 1ii• ,� � c10 �t.�- lS fi�s�•�', �-1. 'yu2 / «V � �"1
�u� 1.!- : c� �� C �:Z .1 `,•�-tu., 11 ' c:� G - . .l.L- : ��P �, c„�,C� C.�:� � �nt.c�. -t,l % •�_�_
_ Lot ID of split_ containers:
CLIENT NOTIFICATION/RESOLUTION T T
Person contacted: Date/Time,
Project Manager SCURF Review:
Project Manager SRF Review:
Date: �{
Date:
Page 20 of 22

Document Name:
Document Revised: February 7, 2018
h�
i = .Anapical"
Sam le Condition U on Recel t sCUR
Page 1 of 2
Document No,:
Issuing Authority:
1
F-CAR-CS-033•Rev.06
Pace Carolinas Quail ty Office
'Check mark top half of box if pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
••Bottom half of box is to list number of bottle
Project, W® . 92.459129
Ph: TIH Due.Date: 01/16/20
CLIENT: 92-DANANER
v
Z
2
2
Q
2
2
Z
Y
m
u
m
3
n
^
v
Y'
.=a
a
1
p
pp;
d
s
�'
n
n
q
a
ro
=
ry
b
a
it
7
M
C
N
z
Z
c
u_
D
2
Eg'
d
r0
n
`�
3�
y
2
o
c
UUW'In3
7
V
_
`m
_
S
e3
LD
;
p
�`
`�'
`w
s
E
a
4
E
¢
A
Q
6E
d
>
s
S
'^
:
¢
E
E
a
E
E
E
>
£
a
.�
E
E.
E
J
E
E
ir.
E
E
E
vy1�
N
p
8
_
,N-1
N
..
ypE�
.'
vyE
0
m
m
m
to
In
to
N
I
y
N
Z
�
-.
l I
NN
N
A
f:
111
H
5
5
7
g
—
N
9
10
11
12
Sample ID TVpo of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative
adjusted added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Cert
Out of hold, Incorrect preservative, out of temp, incorrect containers.
Lot N
Page 21 of 22

�0 CHAIN -OF -CUSTODY 1 Analytical Request Document
�.a The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Regvlred Client tntomutiom Requ6red Project Information: Invoice Information: _ PagC : t Of t
Comparw: R--;ahv p,M. [ReportTo; Fkarie Jnwrnien M.*Mkn
Email:
Purchase Order #:
Pace Ovote:
Prlone:
Fax
Projw Nano. Slormwater Sam li
P.. Project MDrlager: g eka.baioni pacelabs,com,
Requested Due Dale:
1proled M.
Pace Profile C; 1279.5
�'_`^� nested Anaf
z
z
MA:Rtx CODE
S
u
COLLECTED
Preservatives
r;
Dr" W" DW
Wales Vn
S
(r
t
G
Wuta Wata WHr
i
0
SAMPLE
ID
Ptoma:e P
SL
u_
START
END
a'
- to _
F
6
:
One Charactei
per box.
W W
r�
_
pp
-. o.
C'
(A-i^ e_y
' �}
atw CT
}�
h
Z
C
M
}�
s
#
Sample Ids
t be unique
T— it.
V
F
a
O
e
e
N
C
CJ
W
Fen
d
EM
g
h
DATE
TIME
DATE
TIME .
a
_
S
M
z
z
j
a
$
O f
SAMPLER NAu A!
SPRINT
�
m
Name of
N
N
SIGNATURE of
O
N
N
DATE
3
State'/
■ nm
of
u `o
.5 m �m
.m �_
N