NCG030099_MONITORING INFO_20190218

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
IV C& o3t
DOC TYPE
D HISTORICAL FILE
CIAMONITORING REPORTS
DOC DATE
p ) oil, T`x
YYYYMMDD

STORMWATER DISCHARGE OUTFALL (SDO)
ANNUAL SUMMARY DATA MONITORING REPORT (DMR)1 SPPP Annual Update DATA REVIEW FORM
Calendar Year January 2020
Individual NPDES Permit No. NCS❑❑❑❑❑❑ or
Certificate of Coverage (COC) No. NCGE[j] 0❑® 0❑❑0
This monitoring report summary of the calendar year should be kepi on file on -site with the facility SPPP.
Facility Name: Galvan Industries
County: Cabarrus
Phone Number:
7( 04 ) 455-5102
Total no. of SDOs monitored 3 RF ' IVE®
Outfall No. 1, 5, TOF , �u � V LL w
Is this outfall currently in Tier 2 (monitored monthly)? Yes ® Nd_E] i , _AL FILES
UWR SECTION
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes 0 No ❑
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWQ to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No 0
Total
Rainfall,
inches
Parameter, (units)
Total
Suspended
Solids (TSS)
pH
Copper
Lead
Zinc
Non -Polar
O&GITPH
Total Toxic
Organics
Benchmark
N/A
100 mglL
6.0 - 9.0
0.007 mglL
0.03 mg/L
0.067 mglL
15 mglL
1 mglL
Date Sample
Collected,
mmiddlyy
am=======
OF-1
0.11
807
7.2
0.526
0.0258
16.4
ND
ND
OF-5
0.11
13.8
NA
0.0109
ND
8.53
NA
NA
TOH-1
0.11
521
NA
0.492
0.174
71.4
NA
NA
SWU-264 - Generic Annual DMR
Last revised 510212018
.0

Additional Outfall Attachment
Outfall No.
Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No ❑
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No ❑
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWQ to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No ❑
Parameter, (units)
Total
Rainfall,
inches
Benchmark N/A
Date Sample
Collected,
mmlddlyy
SWU-264 - Generic Annual DMR
Last revised 510212018

I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibilityQf fires j3nd imprisonment for knowing violations."
Signature
Date
0Z0
For questions, contact your local Regional Office:
DWQ Regional Office Contact Information:
ASHEVILLE REGIONAL OFFICE
FAYETTEVILLE REGIONAL.OFFICE
MOORESVILLE REGIONAL OFFICE
2090 US Highway 70
225 Green Street
610 East Center Avenue/Suite 301
Swannanoa, NC 28778
Systel Building Suite 714
Mooresville, NC 28115
[phone]
Fayetteville, NC 28301-5043
[phone]
[phone]
RALEIGH REGIONAL OFFICE
WASHINGTON_REGIONAL OFFICE
WILMINGTONREGIONAL OFFICE
3800 Barrett Drive
943 Washington Square Mail
127 Cardinal Drive Extension
Raleigh, NC 27609
Washington, NC 27889
Wilmington, NC 28405-2845
[phone]
[phone]
[phone]
WINS_TON-SALEM REGIONAL OFFICE
CENTRAL_OFFICE
1617 Mail Service Center
I
'To preserve, protect
450 Hanes Mill Rd, Suite 300
Winston-Salem, NC 27105
Raleigh; NC 27699-1617
and enhance
[phone]
[phone]
,' North Carolina's;valer..."
�f
SWU-264 - Generic Annual DMR
Last revised 510212018

I
En vironmen tat
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-l<uid-resources/
npdes-stonnwatcr-gps
Permit No.: N/C/ / / l l I l / or Certificate of Coverage No.: N/C/G/ 0/ 3/0/0/0 /0 1
Facility Name: Galvan Indimtrips. I .
County: Cabarrus Phone No. [phone]
Inspector: Robert Mull
Date of Inspection: 01 / 0 7 / 2 02 0
Time of Inspection: 1120
Total Event Precipitation (inches):
0.11
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DE -MLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. 1 Structure (pipe, ditch, etc.): rip —rap to culvert
Receiving Stream:
Back Creek
Describe the industrial activities that occur within the outfall drainage area:
Hot -dip Galvanization
Page 1 of
SwU-242, Last modified WO1/201S

0
a
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
clear to dark grav with some suspended solids
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): odorless
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
1 2 0 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where l is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 0 4 5
7. Is there any foam in the stormwater discharge? O Yes 0 No.
S. Is there an oil sheen in the stormwater discharge? 0Yes O No.
9. Is there evidence of erosion or deposition at the outfall`? O Yes O No.
to. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
5WU-242, Last modified 00)01l2018

t
. - . ry
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on f lling oul this fbrtn, p1c•ase visit https://deq.nc,goviabout/di ViSioiis/energy-mineral-land-resources/
npdcs-storrnwater-gps
Permit No.: NICI l l l l l
Facility Name: Galvan Ind
County: Cabarrus
Inspector: Robert Mull
Date of Inspection: 01 / 0 7 / 2 0
'rime ol' Inspection: 1200
Total Event Precipitation (inches):
/ / or Certificate of Coverage No.: N/C/G/ 01 3/ 0 / 0/0 /0
1
stries. I nc.
0.11
Phone No. [phone]
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour stone
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best ol' my knowledge:
xc/Jzpo(
(Signature of Per-mittee or Designee)
1. Outfall Description:
Outfall No. 3 Structure (pipe, ditch, etc.): rip —rap to culvert
Receiving Stream:
Back Creek
Describe the industrial activities that occur within the outfall drainage area:
Hot -dip Galvanization
Page I of 2
SWU-242, Last modified 06M112018

ri
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: not flowing
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): not flowinq
4. Clarity: Choose the number which best describes the clarity of the discharge, where l is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
G. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwatcr discharge, where l is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes o No.
8. Is there an oil sheen in the stormwater discharge? 0Yes o No.
9. Is there evidence of erosion or deposition at the outfall? 0 Yes
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2019

Li
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance onfilling out this form, please visit https:/Idcq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/ 0/ 3/0/0 /0 /0 1
Facility Name: Galvan Industries. Inc.
County: Cabarrus
Inspector: Robert Mull
Date of Inspection: 01 / 0 7 / 2 0
Time of 1 nspection: 1205
Total Event Precipitation (inches):
0.11
Phone No. [phone]
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local D1:MLR
Regional Office,
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. 4 Structure (pipe, ditch, ctc.): culvert
Receiving Stream:
Back Creek
Describe the industrial activities that occur within the outfall drainage area:
Hot -dip Galvanization _
Page l ol'2
SWU-242. Last modified 06l01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: not flowing
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): not flowing
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where l is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount ot'suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge`? O Yes Q No.
8. Is there an oil sheen in the stormwater discharge? 0Yes o No.
9. Is there evidence of erosion or deposition at the outfall? O Yes No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may he
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2019

I, l
Environmental
Quallty
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling oul this Jana, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-sto rm Wat or-gps
Permit No.: NICI l l 1 / I l / or Certificate of Coverage No.: NIC/GI 01 3l 0/ 0/ 0 /0 /
Facility Name: Galvan Industries, Inc.
County: Cabarrus Phone No. [phone]
inspector: Robert Mull
Date of Inspection: 01 / 0 7 / 2 0
Time of Inspection: 1040
Total Event Precipitation (inches):
0.11
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DI -MLR
Regional Off ice.
By this signature, 1 certify that this report is accurate and complete to the best of my knowledge:
(Signature o1 Permittee or Designee)
1. Outfall Description:
Outfall No. 5 Structure (pipe, ditch, etc.): rip —rap to culvert
Receiving Stream:
Back Creek
Describe the industrial activities that occur within the outfall drainage area:
Hot -dip Galvanization
Page 1 of 2
SWU-242, Lass modified 0GI01l2018

n
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: light brown with some suspended solids
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): odorless
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 0 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where l is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solids and 5 is extremely muddy:
1 0 3 4 5
7. Is there any foam in the stormwater discharge? O Yes O No.
S. Is there an oil sheen in the stormwater discharge? 0Yes O No.
9. is there evidence of erosion or deposition at the outfall? Q Yes O No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06,01/201 R

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 14, 2020
Mark Filardi
HDR
440 S. Church St
Suite 900
Charlotte, NC 28202
RE: Project: GALVAN
Pace Project No.: 92459598
Dear Mark Filardi:
Enclosed are the analytical results for sample(s) received by the laboratory on January 07, 2020.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
-K, u-- -- -D9, --s
Kevin Herring
[e-mail]
1(704)875-9092
HORIZON Database Administrator
Enclosures
cc: Coleman Marchin, HDR
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 35

UceAnalytical
www.pacelabs.cem
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Project: GALVAN
Pace Project No.: 92459598
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
LouisianalNELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E67648
Massachusetts Certification #: M-NCO30
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VrginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in tuli,
without the written consent of Pace Analytical Services, LLC. Page 2 of 35

aceAnalytical
www.pacalabs.cam
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
GALVAN
92459598
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92459598001
OF #1
EPA 1664B
WAM
1
PASI-C
EPA608.3
SEM
29
PASI-C
EPA 200.7 Rev 4.4 1994
' DS, KQ
3
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
SAS
35
PASI-C
SM 2540D-2011
CEH
1
PASI-A
EPA 9040C
ECH
1
PASI-A
92459598003
OF #5
EPA 200.7 Rev 4.4 1994
DS
3
PASI-A
SM 2540D-2011
CEH
1
PASI-A
92459598004
TOW-1
EPA 200.7 Rev 4.4 1994
DS, KQ
3
PASI-A
SM 2540D-2011
CEH
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 35

I
aceAnalytical
www.pacolabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
PROJECT NARRATIVE
Project: GALVAN
Pace Project No.: 92459598
Method: EPA 1664E
Description: 1664 SGT-HEM, TPH
Client: HDR Engineering
Date: January t4, 2020
General Information:
1 sample was analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 518742
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 70117129001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 2776866)
• Total Petroleum Hydrocarbons
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 35

aceAnalytrcal
www.pacolabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersvilie, NC 28078
[phone]
PROJECT NARRATIVE
Project: GALVAN
Pace Project No.: 92459598
Method: EPA 608.3
Description: 608 PCB Pest RVE
Client: HDR Engineering
Date: January 14, 2020
General Information:
1 sample was analyzed for EPA 608.3. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SOUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 608.3 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 518256
S3: Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
• OF #1 (Lab ID: 92459598001)
• Tetrachloro-m-xylene (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 5 of 35

aceAnalXical
www.pactiabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: GALVAN
Pace Project No.: 92459598
Method: EPA 200.7 Rev 4.4 1994
Description: 200.7 MET ICP
Client: HDR Engineering
Date: January 14, 2020
General Information:
3 samples were analyzed for EPA 200.7 Rev 4.4 1994. All samples were received in acceptable condition with any exceptions noted
below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 Rev 4.4 1994 with any exceptions noted below.
initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below,
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with.any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 518426
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92459440001,92459598003
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 2775277)
• Zinc
• MSD (Lab 10: 2775278)
• Zinc
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 6 of 35

aceAnalytical
www,pecelabs.cam
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: GALVAN
Pace Project No.: 92459598
Method: EPA 625.1
Description: 625 RVE
Client: HDR Engineering
Date: January 14, 2020
General Information:
1 sample was analyzed for EPA 625.1. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SOUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA625.1 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 518713
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92459417002
R1: RPD value was outside control limits.
• MSD (Lab ID: 2776769)
• Hexachlorocyclopentadiene
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 35

aceAnalytrcalm
www,pacolabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: GALVAN
Pace Project No.: 92459598
Method: EPA 624.1
Description: 624 Volatile Organics
Client: HDR Engineering
Date: January 14, 2020
General Information:
1 sample was analyzed for EPA 624.1. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within OC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch; 518323
Lt: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples
may be biased high.
• LCS (Lab ID: 2774586)
• trans-1,2-Dichloroethene
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 518323
A matrix spike and/or matrix spike duplicate (MSIMSD) were performed on the following sample(s): 92459630003
P5: The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.
• MS (Lab ID: 2774587)
• 2-Chloroethylvinyl ether
• MSD (Lab ID: 2774588)
• 2-Chloroethylvinyl ether
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
wkhout the written consent of Pace Analytical Services, L.L.C. Page 8 of 35

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[phone]
PROJECT NARRATIVE
Project: GALVAN
Pace Project No.: 92459598
Method: SM 254OD-2011
Description: 2540D Total Suspended Solids
Client: MDR Engineering
Date: January 14, 2020
General Information:
3 samples were analyzed for SM 2544D-2011. All samples were received in acceptable condition with any exceptions noted below or
on the chain -of custody and/or the sample condition upon receipt form (SOUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: 518756
D6: The precision between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 2776958)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 9 of 35

aceAnalyflcal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
PROJECT NARRATIVE
Project: GALVAN
Pace Project No.: 92459598
Method: EPA 9040C
Description: 9040 pH
Client: HDR Engineering
Date: January 14. 2020
General Information:
1 sample was analyzed for EPA 9040C. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below,
1­13: Sample was received or analysis requested beyond the recognized method holding time.
• OF 91 (Lab ID: 92459598001)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 10 of 35

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ANALYTICAL RESULTS
Project: GALVAN
Pace Project No.: 92459598
Sample: OF #1
Lab ID: 92459598001 Collected: 01/07/20 11:20
Received: 01/07/20 14:00 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND
mg/L
5.0
1
01/10/20 10:36
608 PCB Pest RVE
Analytical Method: EPA 608.3
Preparation Method: EPA 608.3
Aldrin
ND
ug/L
0.050
1
01/08/20 14:43
01/14/20 00:12
309-00-2
alpha-BHC
ND
ug/L
0.050
1
01/08/20 14:43
01/14/20 00:12
319-84-6
beta-BHC
ND
ug1L
0.050
1
01/08/20 14:43
01/14/20 00:12
319-85-7
delta-BHC
ND
ug/L
0.050
1
01/08/20 14:43
01/14/20 00:12
319-86-8
gamma-BHC (Lindane)
ND
1
0.050
1
01/08/20 14:43
01/14/20 00:12
58-89-9
Chlordane (Technical)
ND
ugIL
0.50
1
01/08/20 14:43
01/14/20 00:12
57-74-9
alpha -Chlordane
ND
ug1L
0.050
1
01/08/20 14:43
01/14/20 00:12
5103-71-9
gamma -Chlordane
ND
ug1L
0.050
1
01/08/20 14:43
01/14/20 00:12
5103-74-2
4,4'-DDD
ND
ugIL
0.050
1
01/08/20 14:43
01/14/20 00:12
72-54-8
4,4'-DDE
ND
ug1L
0.050
1
01/08/20 14:43
01/14/20 00:12
72-55-9
4,4'-DDT
ND
ug1L
0.050
1
01/08/20 14:43
01/14/20 00:12
50-29-3
Dieldrin
ND
ugIL
0.050
1
01/08/20 14:43
01/14/20 00:12
60-57-1
Endosulfan I
ND
ug1L
0,050
1
01/08/20 14:43
01/14/20 00:12
959-98-8
Endosulfan 11
ND
ug1L
0.050
1
01/08/20 14:43
01/14/20 00:12
33213-65-9
Endosulfan sulfate
ND
ug1L
0.050
1
01/08/20 14:43
01/14/20 00:12
1031-07-8
Endrin
ND
ug/L
0.050
1
01/08/20 14:43
01/14/20 00:12
72-20-8
Endrin aldehyde
ND
ug/t_
0.050
1
01/08/20 14:43
01/14/20 00:12
7421-93-4
Heptachlor
ND
ug1L
0.050
1
01/08/20 14:43
01/14/20 00:12
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
1
01/08/20 14:43
01/14120 00:12
1024-57-3
PCB-1016 (Aroclor 1016)
ND
ug/t_
0.50
1
01/08/20 14:43
01/14/20 00:12
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
1
01/08/20 14:43
01/14/20 00:12
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
1
01/08/20 14:43
01/14/20 00:12
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
1
01/08/20 14:43
01/14/20 00:12
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
1
01/08/20 14:43
01/14/20 00:12
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0,50
1
01/08/20 14:43
01/14/20 00:12
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
1
01/08/20 14:43
01/14/20 00:12
11096-82-5
Toxaphene
ND
ug/L
0.50
1
01/08/20 14:43
01/14/20 00:12
8001-35-2
Surrogates
Tetra ch loro-m-xyl ene (S)
192
%
10-130
1
01/08/20 14A3
01/14/20 00:12
877-09-8 S3
Decachlorobiphenyl (S)
76
%
10-130
1
01/08/20 14A3
01/14/20 00:12
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Copper
526
ug/L
5.0
1
01/09/20 01:30
01/09/20 19:31
7440-50-8
Lead
25.8
ug1L
5.0
1
01/09/20 01:30
01/09/20 19:31
7439-92-1
Zinc
16400
ug/L
50.0
5
01/09/20 01:30
01/10/20 02:37
7440-66-6
625 RVE
Analytical Method: EPA 625.1
Preparation Method: EPA 625.1
Acenaphthene
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
83-32-9
Acenaphthylene
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
208-96-8
Anthracene
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
01110/2009:50
01/13/20 19:10
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
50-32-8
Benzo(b)fluoranthen e
ND
ug/L
5.0
1
OV10120 09:50
01/13/20 19:10
205-99-2
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 01/14/2020 01:29 PM
without the written consent of Pace Analytical
Services, LLC.
Page 11 of 35

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9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: GALVAN
Pace Project No.: 92459598
Sample: OF #1 Lab ID: 92459598001 Collected: 01/07/20 11:20 Received: 01/07/20 14:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method: EPA625.1 Preparation Method: EPA625.1
Benzo(g,h,i)perylene
NO
ug/L
5.0
1
01/1000 09:50
01/13/20 19:10
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
207-08-9
4-Bromophenylphenyl ether
NO
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
85-68-7
4-Chloro-3-methylphenol
NO
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
59-50-7
bis(2-Chloroethoxy)methane
NO
ug/L
10.0
1
01/10/20 09:50
01/13/20 19:10
111-91-1
bis(2-Chloroethyl) ether
NO
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
111-44-4
2-Chloronaphftlene
ND
uglL
5.0
1
01/10/20 09:50
01/13/20 19:10
91-53-7
2-Chlorophenol
ND
uglL
5.0
1
01/10/20 09:50
01/13/20 19:10
95-57-8
4-Chlorophenylphenyl ether
NO
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
7005-72-3
Chrysene
NO
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
218-01-9
Dibenz(a,h)anthracene
NO
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
53-7D-3
3,T-Dichlorobenzidine
NO
ug1L
25.0
1
01/10/20 09:50
01/13/20 19:10
91-94-1
2,4-Dichlorophenol
NO
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
120-83-2
Diethylphthalate
NO
ug1L
5.0
1
01/10/20 09:50
01/13/20 19:10
84-66-2
2,4-Dimethyl phenol
ND
ug1L
10.0
1
01/10/20 09:50
01/13/20 19:10
105-67-9
Dim ethyl phthalate
ND
ug1L
5.0
1
01/10/20 09:50
01/13/20 19:10
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
84-74-2
4,6-Dinitro-2-methylphenol
NO
ug/L
20.0
1
01/10/20 09:50
01/13/20 19:10
534-52-1
2,4-Dinitrophenol
NO
ug/L
50.0
1
01/10/20 09:50
01/13/20 19:10
51-28.5
2,4-Dinitrotoluene
NO
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
121-14-2
2,6-Dinitrotoluene
NO
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
606-20-2
Di-n-octylphthalate
NO
ug1L
5.0
1
01/10/20 09:50
01/13/20 19:10
117-84-0
bis(2-Ethyl hexyl)phtha late
NO
ug1L
5.0
1
01/10/20 09:50
01/13/20 19:10
117-81-7
Fluoranthene
NO
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
206-44-0
Fluorene
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
87-68-3
H exachloro benzene
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
01/10/20 09:50
01/13/20 19:10
77-47-4
Hexachloroethane
NO
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
193-39-5
Isophorone
ND
ug/L
10.0
1
01/10/20 09:50
01/13/20 19:10
78-59-1
Naphthalene
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
91-20-3
Nitrobenzene
NO
ug1L
5.0
1
01/10/20 09:50
01/13/20 19:10
98-95-3
2-Nitrophenol
NO
ug/L
5.0
1
01/10/2609:50
01/13/20 19:10
88-75-5
4-Nitrophenol
NO
ug/L
50.0
1
01/10/20 09:50
01/13/20 19:10
100-02-7
N-Nitrosodimethylamine
NO
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
62-75-9
N-Nitroso-di-n-propylamine
NO
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
621-64-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
1
01/10/20 09:50
01/13/20 19:10
86-30-6
2,2'-Oxybis(1-chloropropane)
NO
ug/L
5.0
1
01/10/20 W50
01/13/20 19:10
108-60-1
Pentachlorophenol
NO
ug/L
10.0
1
01110/2009:50
01/1312019:10
87-86-5
Phenanthrene
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
85-Cl-8
Phenol
NO
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
108-95-2
Pyrene
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
129-00-0
1, 2,4-Trichloro benzene
ND
ug/L
5.0
1
01/10/20 09:50
01/13/20 19:10
120-82-1
2,4,6-Trichlorophenot
ND
ug/L
10.0
1
01/10/20 09:50
01/13/20 19:10
88-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/14/2020 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 35

aceAnalX cal
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Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
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ANALYTICAL RESULTS
Project: GALVAN
Pace Project No.: 92459598
Sample: OF #1 Lab ID: 92459598001 Collected: 01/07/20 11:20 Received: 01/07/20 14:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Surrogates
Nitrobenzene-d5 (S)
74
%
10-120
1
01/10/20 09:50
01/13/20 19:10
4165-60-0
2-Fluorobiphenyl (S)
53
%
15-120
1
01/10/20 09:50
01/13/20 19:10
321-60-8
Terphenyl-d14 (S)
82
%
11-131
1
01/10/20 09:50
01/13/20 19:10
1718-51-0
Phenol-d6 (S)
51
%
10-120
1
01/10/20 09:50
01/13/20 19:10
13127-88-3
2-Fluorophenol (S)
65
%
10-120
1
01/10/20 09:50
01/13/20 19:10
367-12-4
2,4,6-Tribromophenol (S)
108
%
10-137
1
01/10/20 09:50
01/13/20 19:10
118-79-6
624 Volatile Organics
Analytical Method:
EPA 624.1
Acrolein
NO
ug/L
5.0
1
01/09/20 01:21
107-02-8
Acrylonitrile
ND
ug1L
5.0
1
01/09/20 01:21
107-13-1
Benzene
ND
ug/L
1.0
1
01/09/20 01:21
71-43-2
Bromodichlorom ethane
ND
ug1L
2.0
1
01/09/20 01:21
75-27-4
Bromoform
NO
ug/L
2.0
1
0110912O 01:21
75-25-2
Bromomethane
ND
ug/L
2.0
1
01/09/20 01:21
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
01/09/20 01:21
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
01/09/20 01:21
108-90-7
Chloroethane
NO
ug/L
2.0
1
01/09/20 01:21
75-00-3
2-Chloroethylvinyl ether
ND
ug/L
5.0
1
01/09/20 01:21
110-75-8 c3
Chloroform
NO
ug/L
2.0
1
01/09/20 01:21
67-66-3
Chloromethane
NO
ug/L
2.0
1
01/09/20 01:21
74-87-3
Dibromochloromethane
NO
ug/L
2.0
1
01/09/20 01:21
124-48-1
1,2-Dichlorobe nzene
ND
ugtL
2.0
1
01/09/20 01:21
95-50-1
1,3-Dichlorobenzene
NO
ug1L
2.0
1
01/09/20 01:21
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
01/09/20 01:21
106-46-7
1,1-Dichloroethane
NO
ug/L
2.0
1
01/09/20 01:21
75.34-3
1,2-Dichloroethane
NO
ug/L
2.0
1
01/09t20 01:21
107-06-2
1,1-Dichloroethene
NO
ug/L
2.0
1
01/09/20 01:21
75-35-4
trans- 1,2-Dichloroethene
NO
ug/L
2.0
1
01/09/20 01:21
156-60-5 L1
1,2-Dichloropropane
NO
ug/L
2.0
1
01/09/20 01:21
78-87-5
cis- 1,3-Dichloropropene
NO
ug/L
2.0
1
01/09/20 01:21
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
2.0
1
01/09/20 01:21
10061-02-6
Ethylbenzene
NO
ug/L
1.0
1
01/09/20 01:21
100-41-4
Methylene Chloride
NO
ug/L
2.0
1
01/09/20 01:21
75-09-2
Naphthalene
NO
ug1L
5.0
1
01/09/20 01:21
91-20-3
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
01/09/20 01:21
79-34-5
Tetra chloroethene
ND
ug1L
2.0
1
01/09/20 01:21
127-18-4
Toluene
ND
ug1L
1.0
1
01/09/20 01:21
108-88-3
1,1,1-Trichloroethane
ND
ug/L
2.0
1
01/09/20 01:21
71-55.6
1,1,2-Trichloroethane
NO
ug/L
2.0
1
01/09/20 01:21
79-00-5
Trichioroethene
NO
ug/L
2.0
1
01/09/20 01:21
79-01-6
Vinyl chloride
NO
ug/L
2.0
1
01/09/20 01:21
75-01-4
Surrogates
4-Bromofluorobenzene (S)
104
%
70-130
1
01/09/20 01:21
460-00-4
Toluene-d8 (S)
85
%
70-130
1
01/09120 01:21
2037-26-5
1,2-Dichloroethane-d4 (S)
108
%
70-130
1
01/09/20 01:21
17060-07-0
Date: 01/14/2020 01:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 35

Pace Analytical Services, LLC
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville, NC 28078
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ANALYTICAL RESULTS
Project: GALVAN
Pace Project No.: 92459598
Sample: OF #1 Lab ID: 92459598001 Collected: 01/07/20 11:20 Received: 01/07/20 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D-2011
Total Suspended Solids 807 mg/L 25.0 1 01/10/20 11:27
9040 pH Analytical Method: EPA 9040C
pH at 25 Degrees C 7.2 Std, Units 0.10 1 01/12/20 15:02 H3
REPORT OF LABORATORY ANALYSIS
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Date: 01/14/2020 01:29 PM without the written consent of Pace Anaiyticat Services, LLC. Page 14 of 35

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)B75-9092
ANALYTICAL RESULTS
Project: GALVAN
Pace Project No.: 92459598
Sample: OF #5 Lab ID: 92459598003 Collected: 01/07/20 10:40 Received: 01/07/20 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Copper
10.9 ug/L
5.0 1
01/09/20 01:30 01/09/20 19:43 7440-50-8
Lead
ND uglL
5.0 1
01/09/20 01:30 01/09/20 19:43 7439-92-1
Zinc
8530 uglL
10.0 1
01/09/20 01:30 01/09/20 19:43 7440-66-6 M1
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
13.8 mg/L
2.5 1
01/10/20 11:29
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
® 9B00 KinceyAve. Suite 100
aceAnalytrcal Huntersvilie, NC 2807E
www.paculabs.com
[phone]
ANALYTICAL RESULTS
Project: GALVAN
Pace Project No.: 92459598
Sample: Tli Lab ID: 92459598004 Collected: 01/07/20 10:45 Received: 01/07/20 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed GAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Copper
492 ug/L
5.0
1
01/09/20 01:30 01/09/20 19:52 7440-50-8
Lead
174 ug/L
5.0
1
01/09/20 01:30 01/09/20 19:52 7439-92-1
Zinc
71400 ug/L
100
10
01/09/20 01:30 01/10/20 02:43 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
521 ri
25.0
1
01/10/20 1i:29
REPORT OF LABORATORY ANALYSIS
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aceAnalXical
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Pace Analytical Services, LLC
9800 KinceyAve . Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN
Pace Project No.: 92459598
QC Batch: 518742 Analysis Method: EPA 16648
QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH
Associated Lab Samples: 92459598001
METHOD BLANK: 2776864
Associated Lab Samples: 92459598001
Parameter Units
Total Petroleum Hydrocarbons mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 01/10/2010:15
LABORATORY CONTROL SAMPLE:
2776865
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 20.6
103
64-132
MATRIX SPIKE SAMPLE:
2776866
70117129001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
7.9 20
18.7
54
64-132 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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4
aceAnalytical
www.pactiabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN
Pace Project No.: 92459598
QC Batch: 518426 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92459598001, 92459598003, 92459598004
METHOD BLANK: 2775273
Matrix: Water
Associated Lab Samples:
92459598001, 92459598003, 92459598004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Copper
ug/L
ND 5.0
01109/2018747
Lead
uglL
ND 5.0
0110912018:47
Zinc
ug1L
ND 10.0
01109/2018:47
LABORATORY CONTROL SAMPLE:
2775274
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Copper
ug/L
500
488 98 85-115
Lead
ug/L
500
482 96 85-115
Zinc
ug/L
500
463 93 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2775275
2775276
MS
MSD
92459440001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper
ug/L
ND
500
500
509
500
101
100
70-130
2
Lead
ug/L
ND
500
500
487
481
97
96
70-130
1
Zinc
ug/L
ND
500
500
483
477
96
95
70-130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2775277
2775278
MS
MSD
92459598003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua[
Copper
ug/L
10.9
500
500
513
504
100
99
70-130
2
Lead
ug/L
ND
500
500
498
489
99
97
70-130
2
Zinc
ug/L
8530
500
500
8790
8740
52
43
70-130
1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/14/2020 01:29 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 35

aceAnalytical
www.patalaba,tam
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Hinlersville, NC 28078
(704)875-W92
Project: GALVAN
Pace Project No.: 92459598
QC Batch: 518323
QC Batch Method: EPA 624.1
Associated Lab Samples: 92459598001
QUALITY CONTROL DATA
Analysis Method: EPA 624.1
Analysis Description: 624 MSV
METHOD BLANK: 2774585
Associated Lab Samples: 92459598001
Parameter
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,1,1-Trichloroethane
uglL
ND
2.0
01/08/20 23:52
1,1,2,2-Tetrachloroethane
uglL
ND
2.0
01/08/20 23:52
1.1,2-Trichloroethane
uglL
ND
2.0
01/08/20 23:52
1,1-Dichloroethane
uglL
ND
2.0
01/08/20 23:52
1,1-Dichloroethene
uglL
ND
2.0
01/08/20 23:52
1,2-Dichlorobenzene
uglL
ND
2.0
01/08/20 23:52
1,2-Dichloroethane
uglL
ND
2.0
01/08/20 23:52
1,2-Dichloropropene
ug/L
ND
2.0
01/08/20 23:52
1,3-Dichlorobenzene
uglL
ND
2.0
01/08/20 23:52
1.4-Dichlorobenzene
ug/L
ND
2.0
01/08/20 23:52
2-Chloroethylvinyl ether
ug/L
ND
5.0
01/08/20 23:52
Acrolein
uglL
ND
5.0
01/08/20 23:52
Acrylonitrile
uglL
ND
5.0
01/08/20 23:52
Benzene
uglL
ND
1.0
01/08/20 23:52
Bromodichlorom ethane
uglL
ND
2.0
01/08/20 23:52
Bromoform
uglL
ND
2.0
01/08/20 23:52
Bromomethane
uglL
ND
2.0
01/08/20 23:52
Carbon tetrachloride
uglL
ND
2.0
01/08/20 23:52
Chlorobenzene
ug/L
ND
2.0
01/08/20 23:52
Chloroethane
ug/L
ND
2.0
01/08/20 23:52
Chloroform
ug/L
ND
2.0
01/08/20 23:52
Chloromethane
ug/L
ND
2.0
01/08/20 23:52
cis- 1,3-Dichloropropene
uglL
ND
2.0
01/08/20 23:52
Dibromochloromethane
ug/L
NO
2.0
01/08/20 23:52
Ethylbenzene
ug1L
ND
1.0
01/08/20 23:52
Methylene Chloride
uglL
ND
2.0
01108i20 23:52
Naphthalene
uglL
ND
5.0
01/08/20 23:52
Tetrachloroethene
ug1L
ND
2.0
01/08/20 23:52
Toluene
uglL
ND
1.0
01/08/20 23:52
trans- 1.2-Dichloroethene
uglL
ND
2.0
01/08/20 23:52
trans- 1,3-Dichloropropene
ug/L
ND
2.0
01/08/20 23:52
Trchloroethene
ug/L
ND
2.0
01/08/20 23:52
Vinyl chloride
ug1L
ND
2.0
01/08/20 23:52
1,2-Dichloroethane-d4 (S)
%
105
70-130
01/08/20 23:52
4-Bromoftuorobenzene (S)
%
104
70-130
01/08/20 23:52
Toluene-d8 (S)
%
96
70-130
01/08/20 23:52
Qualifiers
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN
Pace Project No.: 92459598
LABORATORY CONTROL. SAMPLE:
Parameter
2774586
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
50
58.6
117
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
58.1
116
60-140
1,1,2-Trichloroethane
ug/L
50
51.7
103
70-130
1,1-Dichloroethane
ug1L
50
61,1
122
70-130
1,1-Dichloroethene
ug/L
50
64.5
129
50-150
1,2-Dichlorobenzene
ug1L
50
49.9
100
65-135
1,2-Dichloroethane
ug/L
50
55.0
110
49-155
1,2-Dichloropropane
ug/L
50
54.5
109
35-165
1,3-Dichlorobenzene
ug/L
50
50.3
101
70-130
1,4-Dichlorobenzene
ug/L
50
50.6
101
65-135
2-Chloroethylvinyl ether
ug/L
100
98.1
98
1-225
Acrolein
ug/L
250
276
110
60-140
Acrylonitrile
ug/L
250
290
116
60-140
Benzene
ug/L
50
50.5
101
65-135
Bromodichloromethane
ug/L
50
52.6
105
65-135
Bromoform
ug/L
50
59.4
119
70-130
Bromomethane
ug/L
50
62.0
124
15-185
Carbon tetrachloride
ug/L
50
49.3
99
70-130
Chlorobenzene
ug/L
50
50.7
101
65-135
Chloroethane
ug/L
50
55.2
110
40-160
Chloroform
ug/L
50
55.1
110
70-135
Chloromethane
ug/L
50
52.2
104
1-205
cis-1,3-Dichloropropene
ug/L
50
51.9
104
25-175
Dibromochloromethane
ug/L
50
46.6
93
70-135
Ethylbenzene
ug/L
50
50.6
101
60-140
Methylene Chloride
ug/L
50
60.9
122
60-140
Naphthalene
ug/L
50
43.7
87
70-130
Tetrachloroethene
ug/L
50
49A
99
70-130
Toluene
ug/L
50
47.5
95
70-130
trans-1,2-Dichloroethene
ug/L
50
65.4
131
70-130 L1
trans-1,3-Dichloropropene
ug/L
50
49.8
100
50-150
Trichloroethene
ug/L
50
53.7
107
65-135
Vinyl chloride
ug1L
50
57.5
115
5-195
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-8 romofluoro benzene (S)
%
107
70-130
Toluene-0(S)
%
90
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2774587
2774588
MS
MSD
92459630003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
500
500
578
592
116
118
52-162
2
1,1,2,2-Tetrachloroethane
ug/L
ND
500
500
541
554
108
111
46-157
2
1,1,2-Trichloroethane
ug/L
ND
500
500
645
428
129
86
52-150
40
1,1-Dichloroethane
ug/L
ND
500
500
541
530
108
106
59-155
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/14/2020 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 35

aceAnalytical
www.pactiabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN
Pace Project No.: 92459598
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2774587
MS
92459630003 Spike
Parameter Units Result Conc,
MSD
Spike
Conc.
2774588
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1-Dichloroethene
ug1L
ND
500
500
614
571
123
114
1-234
7
1,2-Dichlorobenzene
ug/L
NO
500
500
502
515
100
103
18-190
3
1,2-Dichloroethane
ug/L
NO
500
500
483
551
97
110
49-155
13
1,2-Dichloropropane
uglL
NO
500
500
553
474
111
95
1-210
15
1,3-Dichlorobenzene
ug/L
ND
500
500
509
527
102
105
59-156
4
1,4-Dichlorobenzene
ug/L
ND
500
500
513
517
103
103
18-190
1
2-Chloroethylvinyl ether
ug/L
NO
1000
1000
NO
NO
0
0
1-305
P5
Acrolein
ug/L
ND
2500
2500
3200
2960
128
119
40-160
8
Acrylonitrile
ug/L
ND
2500
2500
2710
2440
108
98
40-160
10
Benzene
uglL
ND
500
500
625
594
123
117
37-151
5
Bromodichloromethane
ug/L
ND
500
500
540
448
108
90
35-155
i9
Bromoform
ug/L
NO
500
500
502
469
100
94
45-169
7
Bromomethane
ug/L
ND
500
500
232
339
46
68
1-242
37
Carbon tetrachloride
ug/L
ND
500
500
660
549
132
110
70-140
18
Chlorobenzene
ug/L
NO
500
500
521
539
104
108
37-160
3
Chloroethane
uglL
ND
500
500
633
601
127
120
14-230
5
Chloroform
4L
ND
500
500
628
570
125
113
51-138
10
Chloromethane
uglL
NO
500
500
514
512
103
102
1-273
0
cis-1,3-Dichloropropene
ug/L
ND
500
500
524
405
105
81
1-227
26
Dibromochloromethane
ug/L
ND
500
500
520
497
104
99
53-149
4
Ethylbenzene
ug/L
ND
500
500
545
550
109
110
37-162
1
Methylene Chloride
ug/L
ND
500
500
597
553
119
111
1-221
8
Naphthalene
uglL
ND
500
500
491
625
98
125
70-130
24
Tetra ch loroethen e
ug/L
ND
500
SOD
517
532
103
106
64-148
3
Toluene
ug/L
ND
500
500
623
429
122
83
47-150
37
trans-1,2-Dichloroethene
uglL
ND
500
500
642
551
128
110
54-156
15
trans- 1,3-Dichloropropene
ug/L
ND
500
500
592
378
118
76
17-183
44
Trichloroethene
ug/L
NO
500
500
572
582
114
116
70-157
2
Vinyl chloride
ug/L
ND
500
500
577
566
115
113
1-251
2
1,2-Dichloroethane-d4 (S)
%
85
93
70-130
4-Bromofluorobenzene (S)
%
103
104
70-130
Toluene-d8(S)
%
105
75
70-130
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/14/2020 01:29 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 35

aceAnalytical
www.pecetabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN
Pace Project No.: 92459598
QC Batch: 518256 Analysis Method: EPA 608.3
OC Catch Method: EPA 608.3 Analysis Description: 608 PCB Pest Red Vol
Associated Lab Samples: 92459598001
METHOD BLANK: 2774285
Associated Lab Samples: 92459598001
Parameter
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
4,4'-DDD
ug/L
NO
0.050
01/14/20 01:55
4,4'-DDE
ug/L
ND
0.050
01/14/20 01:55
4,4'-DDT
ug/L
ND
0.050
01/14/20 01:55
Aldrin
ug/L
ND
0.050
OV14120 01:55
alpha-BHC
ug1L
ND
0.050
01/14/20 01:55
alpha -Chlordane
ug1L
ND
0.050
01/14/20 01:55
beta-BHC
ug1L
ND
0.050
01/14/20 01:55
Chlordane (Technical)
ug1L
NO
0.50
01/14/20 01:55
delta-BHC
ug/L
ND
0.050
01/14/20 01:55
Dieldrin
ug1L
ND
0.050
01/14/20 01:55
Endosulfan I
ug/L
ND
0.050
01/14/20 01:55
Endosulfan II
ug/L
ND
0.050
01/14/20 01:55
Endosulfan sulfate
ug/L
ND
0.050
01/14/20 01:55
Endrin
ug/L
NO
0.050
01/14/20 01:55
Endrin aldehyde
ug/L
NO
0,050
01/14/20 01:55
gamma-BHC (Lindane)
ug/L
NO
0.050
01/14/20 01:55
gamma -Chlordane
ug/L
ND
0.050
01/14/20 01:55
Heptachlor
ug/L
NO
0.050
01/14/20 01:55
Heptachlor epoxide
ug/L
ND
0.050
01/14/20 01:55
PCB-1016 (Aroclor 1016)
ug/L
ND
0,50
01 /14120 01:55
PCB-1221 (Aroclor 1221)
ug/L
ND
0,50
01/14/20 01:55
PCB-1232 (Aroclor 1232)
ug/L
ND
0.50
01/14/20 01:55
PCB-1242 (Aroclor 1242)
ug/L
ND
0.50
01/14/20 01:55
PCB-1248 (Aroclor 1248)
ug1L
ND
0.50
01/14/20 01:55
PCB-1254 (Aroclor 1254)
ug/L
NO
0.50
01/14/20 01:55
PCB-1260 (Aroclor 1260)
ug/L
NO
0.50
01/14/20 01:55
Toxaphene
ug/L
NO
0.50
01/14/20 01:55
Decachlorobiphenyl (S)
%
95
10-130
01/14/20 01:55
Tetrachloro-m-xylene (S)
%
52
10-130
01/14/20 01:55
Qualifiers
LABORATORY CONTROL SAMPLE:
2774286
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
uglL
0.25
0.23
92
31-141
4,4'-DDE
ug/L
0.25
0.21
84
30-145
4,4'-DDT
ug/L
0.25
0.22
89
25-160
Aldrin
ug/L
0.25
0.11
45
42-140
alpha-BHC
ug/L
0.25
0.21
85
37-140
alpha -Chlordane
ug/L
0.25
0.22
88
45-140
beta-BHC
ug/L
0.25
0.29
116
17-147
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /14/2020 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 35

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN
Pace Project No.: 92459598
LABORATORY CONTROL SAMPLE:
2774286
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
delta-BHC
ug/L
0.25
0.25
99
19-140
Dieldrin
ug1L
0.25
0,23
93
36-146
Endosulfan I
ug/L
0.25
0,23
91
45-153
Endosulfan 11
ug/L
0.25
0.23
92
1-202
Endosulfan sulfate
ug/L
0.25
0.26
104
26-144
Endrin
ug/L
0.25
0.24
96
30-147
Endrin aldehyde
ug/L
0,25
0.23
90
50-148
gamma-BHC (Lindane)
ug/L
0.25
0.23
92
32-140
gamma -Chlordane
ug/L
0.25
0.16
66
45-140
Heptachlor
ug/L
0.25
0.15
59
34-140
Heptachlor epoxide
ug/L
0.25
0.22
86
37-142
Decachlorobiphenyl (S)
%
107
10-130
Tetrachloro-m-xylene (S)
%
64
10-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2774633
2774634
MS
MSD
92459598002
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc,
Result
Result
% Rec % Rec
Limits
RPD Qual
4,4'-DDD
ug/L
ND
0.25
0.25
0.23
0.23
93
94
31-141
1
4,4'-DDE
ug/L
ND
0.25
0.25
0.16
0.17
63
69
30-145
8
4,4'-DDT
ug/L
ND
0.25
0.25
0.19
0.20
76
80
25-160
5
Aldrin
ug/L
NO
0.25
0.25
0.12
0.15
48
59
42-140
20
alpha-BHC
ug/L
NO
0.25
0.25
0.19
0.23
78
91
37-140
16
alpha -Chlordane
ug/L
NO
0.25
0.25
0.18
0.20
73
78
45-140
7
beta-BHC
ug/L
NO
0.25
0.25
0.28
0.31
112
123
17-147
9
delta-BHC
ug/L
NO
0.25
0.25
0.24
0.25
96
100
19-140
4
Dieldrin
ug/L
NO
0.25
0.25
0.22
0.23
88
91
36-146
3
Endosulfan I
ug/L
NO
0.25
0.25
0,21
0.22
83
87
45-153
5
Endosulfan II
ug/L
NO
0.25
0.25
0.24
0.24
94
95
1-202
1
Endosulfan sulfate
ugIL
ND
0.25
0.25
0.25
0.26
100
103
26-144
3
Endrin
ug/L
ND
0.25
0.25
0.23
0.23
91
92
30-147
2
Endrin aldehyde
ug/L
NO
0,25
0.25
0.25
0.25
99
100
50-150
1
gamma-BHC (Lindane)
ug/L
NO
0,25
0.25
0.21
0.25
84
98
32-140
16
gamma -Chlordane
ug/L
NO
0.25
0.25
0.14
0.17
58
69
45-140
19
Heptachlor
ug/L
NO
0.25
0.25
0.15
0,18
60
73
34-140
20
Heptachlor epoxide
ug/L
NO
0,25
0,25
0.22
0,23
87
91
37-142
4
Decachlorobiphenyl (S)
%
52
52
10-130
Tetrachloro-m-xylene (S)
%
101
116
10-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/14/2020 01:29 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 35

aceAnalXical
www.pacalabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: GALVAN
Pace Project No.: 92459598
QC Batch: 518713
QC Batch Method: EPA 625.1
Associated Lab Samples: 92459598001
QUALITY CONTROL DATA
Analysis Method: EPA 625.1
Analysis Description: 625 MSS
METHOD BLANK: 2776766
Associated Lab Samples: 92459598001
Parameter
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
NO
5.0
01112/2013:43
2,2'-Oxybis(1-chloropropane)
ug1L
NO
5.0
01112/2013:43
2,4,6-Trichlorophenot
ug/L
NO
10.0
01112/2013:43
2,4-Dichlorophenol
ug/L
ND
5.0
01112/2013:43
2,4-Dimethyiphenol
ug/L
NO
10.0
01112/2013A3
2,4-Dinitrophenol
ug/L
NO
50.0
01112/2013:43
2,4-Dinitrotoluene
ug/L
ND
5.0
01/12/2013:43
2,6-Dinitrotoluene
ug/L
ND
5.0
01/12/2013:43
2-Chloronaphthalene
ug/L
ND
5.0
01/12/2013:43
2-Chlorophenol
ug/L
ND
5.0
01/12/2013:43
2-Nitrophenol
ug/L
ND
5.0
01/12/2013:43
3,X-Dichlorobenzidine
ug/L
NO
25.0
01/1212013:43
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
01/1212013:43
4-Bromophenylphenyl ether
ug/L
ND
5.0
01/12/20 13:43
4-Chloro-3-methyl phenol
uglL
ND
5.0
01/1212013:43
4-Chlorophenylphenyl ether
uglL
ND
5.0
01/12/20 13:43
4-Nitrophenol
ug/L
ND
50.0
01/12/2013:43
Acenaphthene
ug/L
ND
5.0
0111212013:43
Acenaphthylene
ug/L
ND
5.0
01/1212013:43
Anthracene
uglL
ND
5.0
01/1212013:43
Benzo(a)anthracene
ug/L
NO
5.0
0111212013:43
Benzo(a)pyrene
ug/L
ND
5.0
01112/2013:43
Benzo(b)fluoranthene
ug/L
ND
5.0
01/12/2013:43
Benzo(g,h,i)perylene
ug/L
ND
5.0
01112/2013:43
Benzo(k)Fluoranthene
ug/L
ND
5.0
01/12/2013:43
bis(2-Chloroethoxy)methane
ug1L
NO
10.0
01/12/2013:43
bis(2-Chloroethyl) ether
ug1L
ND
5.0
01/12/20 13:43
bis(2-Ethylhexyl)phthalate
ug1L
ND
5.0
0111212013:43
Butylbenzylphthalate
ug1L
ND
5.0
01112/2013:43
Chrysene
ug/L
ND
5.0
01/12/2013:43
Di-n-butylphihalate
ug/L
ND
5.0
01112/2013:43
Di-n-octylphthalate
ug/L
ND
5.0
01112/2013:43
Dibenz(a,h)anthracene
ug/L
ND
5.0
01/12/2013:43
Diethylphthalate
ug/L
NO
5.0
01/12/2013:43
Dimethylphthalate
ug/L
NO
5.0
01112/2013:43
Fluoranthene
ug/L
NO
5.0
01/12/2013:43
Fluorene
ug/L
NO
5.0
01/12/2013:43
Hexachloro-1,3-butadiene
ug/L
NO
5.0
01/12/2013:43
Hexachlorobenzene
ug/L
NO
5.0
01/12/2013:43
Hexachlorocyclopentadiene
ug/L
ND
10.0
01/12/2013:43
Hexachloroethane
ug/L
ND
5.0
01/1212013:43
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /14/2020 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 35

m
aceAnalytical
www,pacolahe.com
Pace Analytical Services, 1-LC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN
Pace Project No.: 92459598
METHOD BLANK: 2776766
Associated Lab Samples: 92459598001
Parameter
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
01/12/201143
Isophorone
ug/L
ND
10.0
01/12/20 13:43
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
01/1212013:43
N-Nitrosodimethylamine
ug/L
ND
5.0
01/12/20 13:43
N-Nitrosodiphenylamine
ug/L
ND
10.0
01112/2013:43
Naphthalene
ug/L
ND
5.0
01112/2013:43
Nitrobenzene
ug/L
NO
5.0
01112/2013:43
Pentachlorophenol
ug/L
NO
10.0
01112/2013:43
Phenanthrene
ug/L
NO
5.0
01/12/20 13:43
Phenol
ug/L
ND
5.0
01/1212013:43
Pyrene
ug/L
ND
5.0
01/12/20 13:43
2,4,6-Tribromophenol (S)
%
66
10-137
01/12/20 13:43
2-Fluorobiphenyl (S)
%
54
15-120
01/12/20 13:43
2-Fluorophenol (S)
%
54
10-120
01/12/20 13:43
Nitrobenzene-d5 (S)
%
59
10-120
01/12/20 13:43
Phenol-d6 (S)
%
43
10-120
01/12/20 13:43
Terphenyl-d14 (S)
%
80
11-131
01/12/20 13:43
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2776767
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
27.2
54
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
32.8
66
36-166
2,4,6-Trichlorophenol
ug/L
50
41.0
82
37-144
2,4-Dichlorophenol
ug/L
50
38.6
77
1-191
2,4-Dimethylphenol
ug/L
50
40.4
81
32-119
2,4-Dinitrophenol
ug/L
250
253
101
1-181
2,4-Dinitrotoluene
ug/L
50
45.5
91
39-139
2,6-Dinitrotoluene
ug/L
50
45.0
90
50-158
2-Chloronaphthalene
ug/L
50
34.0
68
60-118
2-Chlorophenol
ug/L
50
38.2
76
23-134
2-Nitrophenol
ug/L
50
37.1
74
29-182
3,3'-Dichlorobenzidine
ug/L
100
86.1
86
1-262
4,6-Dinitro-2-methyiphenol
ug/L
100
110
110
1-181
4-Bromophenylphenyl ether
ug/L
50
39.7
79
53-127
4-Chloro-3-methylphenol
ug/L
100
82.7
83
22-147
4-Chlorophenylphenyl ether
ug/L
50
38.5
77
25-158
4-Nitrophenol
ug/L
250
167
67
1-132
Acenaphthene
ug/L
50
38.0
76
47-145
Acenaphthylene
ug/L
50
41.6
83
33-145
Anthracene
uglL
50
45.0
90
1-166
Benzo(a)anthracene
ug/L
50
48.3
97
33-143
Benzo(a)pyrene
ug1L
50
50.5
101
17-163
Benzo(b)Fluoranthene
ug/L
50
51.5
103
24-159
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/14/2020 01:29 PM without the written ccnsent of Pace Analytical Services, LLC. Page 25 of 35

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)a75-9092
QUALITY CONTROL DATA
Project: GALVAN
Pace Project No.: 92459598
LABORATORY CONTROL SAMPLE:
Parameter
2776767
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Benzo(g,h,i)perylene
ug/L
50
52.7
105
1-219
Benzo(k)fluoranthene
ug/L
50
52.2
104
11-162
bis(2-Chloroethoxy)methane
ug/L
50
37.8
76
33-184
bis(2-Chloroethyl) ether
ug/L
50
37.1
74
12-158
bis(2-Ethyl hexyl)phtha late
ug/L
50
43.4
87
8-158
Butylbenzylphthalate
ug/L
50
44.4
89
1-152
Chrysene
ug/L
50
48.2
96
17-168
Di-n-butylphthalate
ug/L
50
42.1
84
1-118
Di-n-octylphthalate
ug/L
50
43.5
87
4-146
Dibenz(a,h)anthracene
ug/L
50
53.8
108
1-227
Diethyl phtha late
ug/L
50
43.2
86
1-114
Dimethylphthalate
ug/L
50
42.3
85
1-112
Fluoranthene
ug1L
50
46.2
92
26-137
Fluorene
ug/L
50
42.2
84
59-121
Hexachloro-1,3-butadiene
ug/L
50
24.0
48
24-116
Hexachlorobenzene
ug/L
50
43.4
87
1-152
Hexachlorocyclopentadiene
ug/L
50
29.5
59
25-150
Hexachloroethane
uglL
50
23.8
48
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
52.3
105
1-171
Isophorone
ug/L
50
38.6
77
21-196
N-Nitroso-di-n-propylamine
ug1L
50
39.7
79
1-230
N-Nitrosodimethylamine
ug/L
50
37.5
75
25-150
N-Nitrosodiphenylamine
ug/L
50
42.0
84
25-150
Naphthalene
ug/L
50
33.4
67
21-133
Nitrobenzene
ug/L
50
37.1
74
35-180
Pentachlorophenol
ug/L
100
98.8
99
14-176
Phenanthrene
ug/L
50
44.5
89
54-120
Phenol
ug/L
50
27.4
55
5-112
Pyrene
ug/L
50
47.0
94
52-115
2,4,6-Tribromophenol (S)
%
97
10-137
2-Fluorobiphenyl (S)
%
63
15-120
2-Fluorophenol(S)
%
65
10-120
Nitrobenzene-d5(S)
%
67
10-120
Phenol-d6 (S)
%
54
10-120
Terphenyl-d14 (S)
%
82
11-131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2776768
MS
Parameter
1,2,4-Trichlorobenzene
2,2'-Oxybis(1-chloropropane)
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
92459417002
Spike
Units
Result
Conc.
ug/L
ND
50
ug/L
NO
50
ug/L
ND
50
ug/L
ND
50
ug1L
ND
50
Qualifiers
2776769
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
50
26.0
33.2
52
66
44-142
24
50
29.0
30.9
58
62
36-166
6
50
37.6
40.5
75
81
37-144
7
50
34.1
37.2
68
74
1-191
9
50
36.5
39.9
73
80
32-119
9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/14/2020 01:29 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 35

aceAnalytical
www.picalabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN
Pace Project No.: 92459598
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2776768
MS
92459417002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2776769
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits RPD Qual
2,4-Dinitrophenol
ug/L
ND
250
250
236
224
94
89
1-181
5
2,4-Dinilrotoluene
ug1L
ND
50
50
41.2
43.4
82
87
39-139
5
2,6-Dinitrotoluene
ug/L
ND
50
50
41.8
43.2
84
86
50-158
3
2-Chloronaphthalene
ug/L
ND
50
50
30.5
36.9
61
74
60-118
19
2-Chlorophenol
ug/L
ND
50
50
33.7
35.7
67
71
23-134
6
2-Nitrophenol
ug/L
ND
50
50
34.4
38.3
69
77
29-182
11
3,3'-Dichlorobenzidine
ug/L
ND
100
100
70.4
74.5
70
75
1-262
6
4,6-Dinitro-2-methylphenol
ug/L
ND
100
100
105
109
105
109
1-181
4
4-Bromophenylphenyl ether
ug/L
ND
50
50
38.3
40.0
77
80
53-127
4
4-Chloro-3-methylphenol
ug/L
ND
100
100
72.7
78.6
73
79
22-147
8
4-Chlorophenylphenyl ether
ug/L
ND
50
50
35.2
38.3
70
77
25-158
8
4-Nitrophenol
ug/L
ND
250
250
153
154
61
61
1-132
1
Acenaphthene
ug/L
ND
50
50
34.1
39.4
68
79
47-145
15
Acenaphthylene
ug/L
ND
50
50
36.2
42.1
72
84
33-145
15
Anthracene
ug/L
ND
50
50
41.8
42.9
84
86
1-166
3
Benzo(a)anthracene
ug/L
ND
50
50
44.7
45.1
89
90
33-143
1
Benzo(a)pyrene
ug/L
ND
50
50
46.1
46.6
92
93
17-163
1
Benzo(b)fluoranthene
ug/L
ND
50
50
47.6
48.8
95
98
24-159
3
Benzo(g,h,i)perylene
ug/L
ND
50
50
47.6
47,5
95
95
1-219
0
Benzo(b)fluoranthene
ug/L
ND
50
50
48.0
48.4
96
97
11-162
1
bis(2-Chloroethoxy)methane
ug/L
ND
50
50
34.3
37.0
69
74
33-184
8
bis(2-Chloroethyi) ether
ug/L
ND
50
50
32.8
36.8
66
74
12-158
11
bis(2-Eth yl hexyl)phtha late
ug/L
ND
50
50
41.7
42.1
83
84
8-158
1
Butyibenzylphtha late
ug/L
ND
50
50
42.3
42.7
85
85
1-152
1
Chrysene
ug/L
ND
50
50
45.1
45.0
90
90
17-168
0
Di-n-butylphthalate
ug/L
ND
50
50
39.3
40.5
79
81
1-118
3
Di-n-octylphthalate
ug/L
ND
50
50
41.3
42.4
83
85
4-146
3
Dibenz(a,h)anthracene
ug/L
ND
50
50
48.0
47.4
96
95
1-227
1
Diethylphthalate
ug/L
ND
50
50
39.7
40.5
79
81
1-114
2
Dimethylphthalate
ug/L
ND
50
50
38.8
39.9
78
80
1-112
3
Fluoranthene
ug/L
ND
50
50
42.2
43.4
84
87
26-137
3
Fluorene
ug/L
ND
50
50
38.7
41.9
77
84
59-121
8
Hexachloro-1,3-butadiene
ug/L
ND
50
50
23.3
31.6
47
63
24-116
30
H exachloro benzene
ug/L
ND
50
50
41.0
42.1
82
84
1-152
3
Hexachlorocyclopentad iene
ug/L
ND
50
50
28.5
39.1
57
78
25-150
31 R1
Hexachloroethane
ug/L
ND
50
50
23.2
29.3
46
59
40-113
23
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
50
46.8
46.9
94
94
1-171
0
Isophorone
ug/L
ND
50
50
35.0
38.5
70
77
21-196
10
N-Nitroso-di-n-propylamine
ug/L
ND
50
50
34.6
38.0
69
76
1-230
9
N-Nitrosodimethylamine
ug/L
ND
50
50
33.8
35.0
68
70
25-150
3
N-Nitrosodiphenylamine
ug/L
ND
50
50
42.7
43.4
76
78
25-150
2
Naphthalene
ug/L
ND
50
50
30.7
35.5
61
71
21-133
15
Nitrobenzene
ug/L
ND
50
50
34.5
37.6
69
75
35-180
9
Pentachlorophenol
ug/L
ND
100
100
93.8
98.5
94
99
14-176
5
Phenanthrene
uglL
ND
50
50
41.5
42.4
83
85
54-120
2
Phenol
ug/L
ND
50
50
26.8
26.6
54
53
5-112
1
Results presented
on this page are in
the units indicated by the
"Units" column except where an alternate unit is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /14/2020 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 35

U
cAnal rcal
www.pscelabs.coln
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: GALVAN
Pace Project No.: 92459598
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2776768
2776769
MS
MSD
92459417002 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
Pyrene
ug1L ND 50
50 45.8
45.2 92
90
52-115 1
2,4,6-Tribromophenol (S)
%
104
101
10-137
2-Fluorobiphenyl (S)
%
67
63
15-120
2-Fluorophenol (S)
%
64
63
10-120
Nitrobenzene-d5 (S)
%
70
70
10-120
Phenol-d6 (S)
%
59
56
10-120
Terphenyl-d14(S)
%
87
79
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/14/2020 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 35

r
aceAnalytica!
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntorsville, NC 28078
(704 )875-9092
QUALITY CONTROL DATA
Project: GALVAN
Pace Project No.: 92459598
QC Batch: 518756 Analysis Method: SM 2540D-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92459598001, 92459598003, 92459598004
METHOD BLANK: 2776955 Matrix: Water
Associated Lab Samples: 92459598001, 92459598003, 92459598004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL ND 2.5 01/10/20 11:23
LABORATORY CONTROL SAMPLE: 2776956
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mglL 251 244 97 90-110
SAMPLE DUPLICATE: 2776957
92459598001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
807
775 4
SAMPLE DUPLICATE: 2776958
92459911001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg1L
112
188 51 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/14/2020 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 35

aceAnalytical
www.pacelabs.cam
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
QUALITY CONTROL DATA
Project: GALVAN
Pace Project No.: 92459598
QC Batch: 518900 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Associated Lab Samples: 92459598001
SAMPLE DUPLICATE: 2777675
Parameter
pH at 25 Degrees C
SAMPLE DUPLICATE: 2777676
Parameter
pH at 25 Degrees C
92459865001 Dup
Units Result Result RPD Qualifiers
Std. Units 7.1 7.1 0 H3
92460256003 Dup
Units Result Result RPD Qualifiers
Std, Units 8.1 8.1 0 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: OV1412020 01:29 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 35

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
aceAnalytical Huntersville, NC 28078
www.pacelil com [phone]
QUALIFIERS
Project: GALVAN
Pace Project No.: 92459598
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
,f - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit,
POL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
P5 The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.
R1 RPD value was outside control limits.
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
c3 Analysis of 2-chloroethyl vinyl ether was performed from a sample that was field preserved to pH < 2 with HCI. Acid
preservation is not allowed for this parameter by the test method of for NPDES compliance per 40CFR Part 136.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/14/2020 01:29 PM wlthout the written consent of Pace Analytical Services, LLC. Page 31 of 35

UeAnal t cal
l
www.pacelab3.com
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
GALVAN
92459598
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92459598001
OF #1
EPA 1664E
518742
92459598001
OF 91
EPA 608.3
518256
EPA 608.3
518588
92459598001
OF #1
EPA 200.7 Rev 4.4 1994
518426
EPA 200.7 Rev 4.4 1994
518438
92459598003
OF #5
EPA 200.7 Rev 4.4 1994
518426
EPA 200.7 Rev 4.4 1994
518438
92459598004
TOH-1
EPA 200.7 Rev 4.4 1994
518426
EPA 200.7 Rev 4.4 1994
518438
92459598001
OF #1
EPA 625.1
518713
EPA 625.1
518888
92459598001
OF #1
EPA 624.1
518323
92459598001
OF #1
SM 254OD-2011
518756
92459598003
OF #5
SM 2540D-2011
518756
92459598004
TOH-1
SM 254OD-2011
518756
92459598001
OF #1
EPA 9040C
518900
Date: 01114/2020 01:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 32 of 35

i
Document Name:
Document Revised: February 7, 2019
_ aceAnalyfical-
Sample Condition Upon Recet t(SCUR}
Page 1 of 2
Document No.:
Issuing Authority:
i
F-CAR-CS-033•Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑
. . , . CllentN�me: WO# : 92459598
. o• r � � Project t+.: IIIII
Courier: ❑Fed.Ex ❑UPS ❑LISPS ❑Client�I�I I� 11111111111111Commercial Mf a ❑Other:
Custody Seal Present? ❑Yes JDNO Seals Intact? [:]Yes Ot 0
Datehnitiats Person Examining Contents:
Packing Material: ❑Bubble Wrap ola"�Ibble Bags ❑alone ❑ Other Biological Tissue Frozen?
Thermometer: Type of Ise: et ❑Blue ❑None Dyes �u ❑MIA
Gun 10:4zilu_
Cooler Temp {'C): 11, 1 hCorrection Factor: Add/Subtract (°C) (� O.O°C 1 Temp should be above freezing to 6'C
Cooler Temp Corrected {'C):
. []Simples out of temp criteria. Samples on ice, cooling process
hasbegun
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Internationally,
Yes
Including Hawaii and Puerto Rico)? IJYes L]No
_Woo
'
Cornments/olscre ant :
Chain of Costod F-ese+u?
es No N/A
i.
Samples Arrived within Hold Time?
es ❑Na NIA
2.
Short Hold Time Anal Is (02 hr,)?
Yes N/A
3.
Rush Turn Around Time Requested?
❑Yes ©Ko []N/A J.
4.
i
Suffirient Volume?
2!:-:� uno ❑N;A
j 5,
6.
Correct Containers Used? Yes ❑No ❑6.1I,
_ -Pace Containers Used? es ❑No _ ❑t;A
Containers Intact?
OVes No N/A
7.
Dissolved analysis: Samples Field Filtered?
DY. Nor [ZN/A
8 �!
Sample Labels Match COC?
-Includes DatejTime/ID/Analysis Matrix:
❑res ❑No []N/A
9.
_
Headspace in VOA Vials (>5-6mm)?
f-- No- N/4
10. T 1?
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes E5No ❑N1A
Yes Na NIA
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATIONIRESOLLITION
Person Contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Pme:
Date:
Date:
Field Data Requh.,.0 [:]Yes [:]No
Page 33 of 35

Document Name:
Document Revised: February 7, 2018
"
aCeAMVka(Document
Sample Condition Upon Rece! t SCURI
Page I of 2
�
No.:
IssuingAuthority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination Is Project #
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
WO#:92459598
PM: KLH1 Due Dale: 01/I4/20
CLIENT: 92-HOR
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pH Adjustment Log for Preserved Samples
Sample ID
Type o]' Preservative
pH upon recelpt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
tat tt
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina OEHNR Certification Office {i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
r
+;13
Page 34 of 35

CHAIN -OF -CUSTODY 1 Analytical Request Document
M The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fields must be completed accurately.
4r
Section A Section 6 Section C
Required Client Information: Required Project Information: Invoice Information: Pa e : t Of 1
Company, HDR Report To: amen Y: 1r.r7�• iY- Attention:
Address: 440 South Church Street Copy To: Company Name:
Suite T000, Charlotte, NC 28202
Address:
-
Email: .r r L • f- ; ;�1.; {t3 j-A I'�ti I n +-*1
Purchase Order #:
Pace Quote:
Phone: JFax
Project Name: Galvan
Pace Project Manager, kevin.fieni pacelabs.comt.
--State•lLocation
Requested Due Date:
Project III:
Paca Profile A: 6906.5
NC
.--
'Requtsicted
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MATRIX cone
COLLECTED
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