NCG020354_MONITORING INFO_20190212

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
IV C& �� 0
DOC TYPE
❑HISTORICAL FILE
MONITORING REPORTS
DOC DATE
, J ofI U�
YYYYMMDD

ANNUAL SUMMARY DISCHARGE MONITORING
REPORT (DMR) — STORMWATER
SUBMIT TO CENTRAL OFFICE*
General Permit No. NCG020000
Calendar Year 2019
*Report ALL STORMWATER monitoring data on this form (include "No Flow"Mo Discharge" and Benchmark
Exceedances) from the previous calendar year to the DEQ by MARCH 1 of each year.
Certificate of Coverage No. NCG02 ®EOM
Facility Name: Brickhaven No. 2 Mine Tract "A"
County: Chatham
Phone Number: ( Total no. of SDOs monitored 6
Certified Laboratory Research and Analytical Labs Late # 34
Lab #
Stormwater Discharge Outfall (SDO) No. 1 VMA Outfall? Yes ❑ No x❑
Is this outfall currently in Tier 2 for any parameter? Yes ❑ No 0
Was this outfall ever in Tier 2 during the past year? Yes ❑ No E)
If this outfall was in Tier 2 last year, was monthly monitoring discontinued? RECE 9F O
Yes, enough consecutive samples below benchmarks to decrease frequency ❑ FEB 12 Z019
Yes, received approval from DEMLR to reduce monitoring frequency ❑
No, turbidity benchmark exceedances did not require monthly monitoring ❑ CENTRAL FILE`
Other DVVR SECTION
Outfall No.
Total
Rainfall,
inches
TSS,
mgll
SS,
mill
Turbidity,
NTU
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Non -polar
O&G, mg1l
(VMA)
New
Motor Oil
Usage
allmo.
Stormwater
Benchmarks
indicate NO
applicable
Circle
Benchmark
42160,0•1
Circle
eeBenchGmarknn
JV 511 V
NIA
Standard applies
NIA
Standard appllWaterQuality Water ea
1
>SSe" qui.
average requlrea
lar
TO&0 monSS and itoring
Date Sample
Collected,
molddl r
06/03/2019
0.91"
11.4
<0.1
12.3
NIA
NIA
NIA
NIA
10/15/2019
0.27"
16.0
<0.1
20.5
1 NIA
NIA
NIA
NIA
Permit Date 1011/2015 — 9/30/2020
Last Revised 10-2-2015

Certificate of Coverage No. NCG02 ©00®
Additional Outfall Attachment (make copies as needed for additional outfalls)
Stormwater Discharge Outfall (SDO) No. 2 VMA Outfall? Yes ❑ No
Is this outfall currently in Tier 2 for any parameter? Yes ❑ No
Was this outfall ever in Tier 2 during the past year? Yes ❑ No
If this outfall was in Tier 2 last year, was monthly monitoring discontinued?
Yes, enough consecutive samples below benchmarks to decrease frequency ❑
Yes, received approval from DEMLR to reduce monitoring frequency ❑
No, turbidity benchmark exceedances did not require monthly monitoring ❑
Other ❑
2 OutfNo.
2
Total
Rainfall,
inches
TSS;
mgll
SS,
mill
Turbidity,
NTU
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Non -polar
O&G, mgll
(VMA)
New
Motor Oil
Usage
allmo.
Stormwater
Benchmarks
fndicafe NO
FLOWi(
a FcaBle
Circle
Benchmark
It
d �0
0f�
1J.1
Circle
Benchmark
rr
J� 511
NIA
WaterCluallty
Standard applies I
NIA
WaterGuallty
Standard applies
�'�
�55galfmo.
average requires
TSS and Non -polar
O&G msnitarin
Date Sample
Collected,
molddl r
NEEMMMMM
03/08/2019
0.97"
17.6
<0.1
15.0
NIA
NIA
NIA
NIA
09/ 11 /2019
0.13"
35.5
<0.1
39.9 1
N/A
N/A
N/A
NIA
Permit Date 10/112015 — 9130/2020
Last Revised 10-2-2015

Certificate of Coverage No. NCG02 F1 3❑�®
Additional Outfall Attachment (make copies as needed for additional outfalls)
Stormwater Discharge Outfall (SDO) No. 3 VMA Outfall? Yet] No ❑
Is this outfall currently in Tier 2 for any parameter? Yes ❑ No ❑x
Was this outfall ever in Tier 2 during the past year? Yes ❑ No ❑x
If this outfall was in Tier 2 last year, was monthly monitoring discontinued?
Yes, enough consecutive samples below benchmarks to decrease frequency Cl
Yes, received approval from DEMLR to reduce monitoring frequency ❑
No, turbidity benchmark exceedances did not require monthly monitoring ❑
Other ❑
3 Outfall No.
3
Total
Rainfall,
inches
TSS,
mgll
SS,
mIII
Turbidity,
NTU
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Non -polar
O&G, mgll
(VMA)
New
Motor Oil
Usage
allmo.
5tormwater
Benchmarks
Indicate NO
F`O1N''
a licable
nchm
Benchmark
DU 0
0.1
Benchmark
Benrcle chmark
50 5110
NIA
WaterGuality
Standard appllea
NIA
WaterQuality
Standard appliea
15
allmo
>SSgreclul
average requires
TSS and Non polar
ORG monitorin
Date Sample
Collected,
molddl r
WEEMMMMM
02/05/2019
0.21"
<5.0
<0.1
7.40
NIA
NIA
NIA
NIA
09/23/2019
0.13"
11.4
<0.1
16.5
NIA
NIA
NIA
NIA
Permit Date 10/1/2015 — 9/30/2020
Last Revised 10-2-2015

Certificate of Coverage No. NCG02 0❑00®
Additional Outfall Attachment (make copies as needed for additional outfalls)
Stormwater Discharge Outfall (SDO) No. 4 VMA Outfall? Yes ❑ No g
Is this outfall currently in Tier 2 for any parameter? Yes ❑ No
Was this outfall ever in Tier 2 during the past year? Yes ❑ No x❑
If this outfall was in Tier 2 last year, was monthly monitoring discontinued?
Yes, enough consecutive samples below benchmarks to decrease frequency ❑
Yes, received approval from DEMLR to reduce monitoring frequency ❑
No, turbidity benchmark exceedances did not require monthly monitoring ❑
Other
4 Outfall No.
4
Total
Rainfall,
inches
TSS,
mg/l
SS,
mill
Turbidity,
NTU
I
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Non -polar
O&rG, mgll
(VMA)(gal/Mo.)
New
Motor Oil
Usage
Benchmarks
fndicaf¢ NO
applicable
CircleStormwater Benchmark
Benchmark
(MV50
���w���
0.1
Circle
Benchmark
�� ,5j110
N/A
Standard appWaterGualilies s
NIA
Stalndard appater lies
15
aagereq55 i
average requires
TGdG and lar
monitoring
Date Sample
Collected,
molddl r
05/28/2019
0.26"
7.0
<0.1
6.48
NIA
NIA
NIA
NIA
10/01/2019
0.13"
5.4
<0.1
5.43
NIA
NIA
NIA
NIA
Permit Date 10/1/2015 — 9/30/2020
Last Revised 10-2-2015

Certificate of Coverage No. N0002 ®3❑❑®
Additional Outfall Attachment (make copies as needed for additional outfalls)
Stormwater Discharge Outfall (SDO) No. S VMA Outfall? Yes ❑ No ❑
Is this outfall currently in Tier 2 for any parameter? Yes ❑ No ❑X
Was this outfall ever in Tier 2 during the past year? Yes ❑ No
If this outfall was in Tier 2 last year, was monthly monitoring discontinued?
Yes, enough consecutive samples below benchmarks to decrease frequency ❑
Yes, received approval from DEMLR to reduce monitoring frequency ❑
No, turbidity benchmark exceedances did not require monthly monitoring ❑
Other ❑
Outfall No.
6
Total
Rainfall,
inches
TSS,
mgll
SS,
mill
Turbidity,
NTU
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Non -polar
O&G, mgll
(VMA)
New
Motor Oil
Usage
allmo.
Stormwater
Benchmarks
fndicafe NO
FLOW it
a ffca6fe
Benchmark
ark
(ID 0
\�
0.1
Benchmark Circle
��+t
�5J110
N/A
Water Quality
Standard applies
NIA
WaterQuality1
Standard applies
s
>65gal/ mo.
average requires
TSS mallon-polarorins
06G monkorin
Date Sample
Collected,
molddl r
WEEMMMMM
02/05/2019
0.21"
8.6
<0.1
8.89
NIA
NIA
NIA
NIA
08/27/2019
0.91"
20.9
NIA
NIA
NIA
NIA
Permit Date 10/1/2015 - 9/3012020
Last Revised 10-2-2015

Certificate of Coverage No. NCG02 [flQM®
Additional Outfall Attachment (make copies as needed for additional outfalls)
Stormwater Discharge Outfall (SDO) No. 7 VMA Outfall? Yes ❑ No 0
Is this outfall currently in Tier 2 for any parameter? Yes ❑ No ❑x
Was this outfall ever in Tier 2 during the past year? Yes ❑ No
If this outfall was in Tier 2 last year, was monthly monitoring discontinued?
Yes, enough consecutive samples below benchmarks to decrease frequency ❑
Yes, received approval from DEMLR to reduce monitoring frequency ❑
No, turbidity benchmark exceedances did not require monthly monitoring ❑
Other ❑
7 Outfall No.
Total
Rainfall,
inches
TSS,
mgll
SS,
mlll
Turbidity,
NTU
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Non -polar
O&G, mg/l
(VMA)
New
Motor Oil
Usage
allmo.
Stormwater
Benchmarks
lndicato NO
aF1.OWil
be
Circle
Benchmark
/{ A�1Y�o
0.1
Circle
Benchmark
1p sj/i 0
NIA
Standard applies
NIA
Standard applies
�55 gallmo.
average requires
TSS OLG mon tadand n ar
Date Sample
Collected,
molddl r
EN=====
05/28/2019
0.26"
16.4
<0.1
20.7
NIA
NIA
NIA
NIA
08/27/2019
091"
22.2
<0.1
34.0
NIA
NIA
NIA
NIA
Permit Date 10/1/2015 — 9/30/2020
Last Revised 10-2-2015

Certificate of Coverage No. NCG02 l[j] 5❑®
CERTIFICATION
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and
evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my
knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
[Required by 40 CFR §122.22]
Signature
Date February 11, 2020
o uyh sre�ea er rao�r�u� om��.
nw c.us. l,, .,.
o: C i ,h u.V, ou- Erpm+
E-W & q..AV. ["-�n Owe..
U.1s:7929.02. 11010I 75-059Q
Mail Annual Summary Stormwater DMR to the NCDEQ Central Office:
Note the address is correct — Central Files is housed in DWR (not DEMLR)
N.C. Department of Environmental Quality (DEQ)
Division of Water Resources
Attn: DWR Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files Telephone [phone]
Questions? Contact DEMLR Stormwater Permitting Staff in the Central Office at:
[phone]
Permit Date 1011/2015 — 9/30/2020
Last Revised 10-2-2015

ANNUAL SUMMARY DISCHARGE MONITORING
REPORT (DMR) —WASTEWATER
SUBMIT TO CENTRAL OFFICE*
General Permit No. NCG020000
Calendar Year 2019
"Report ALL WASTEWATER monitoring data on this form (include "No Flow"Mo Discharge" and Limit Violations) from
l the previous calendar year to the DEQ by MARCH 1 of each year.
Certificate of Coverage No. NCG02 ©3❑ 5❑® RF- PIS -,
Facility Name: Colon Mine 9
County: Lee
Phone Number: Total no. of oytfal(s- gnttored 1
Certified Laboratory Research & Analytical Laboratories, Inc. Lab # 34
Lab #
Wastewater (WW) Discharge Outfall No. MP-01
Is this an industrial sand mine (See 40 CFR §436 Subpart D)?
Yes ❑
No
Does this outfall discharge WW to SA waters?
Yes ❑
No IN
Does this outfall discharge WW to SB or PNA waters?
Yes ❑
No
Does this outfall discharge WW to HQW or ORW waters?
Yes ❑
No ❑X
If so, what is the 7Q10 flow rate? or Tidally influenced waters,
7Q10 not available ❑
Does this outfall discharge WW to Trout jr) designated waters?
Yes ❑
No ❑X
Were there any limit violations in the calendar year?
Yes ❑
No ❑X
Outfall No.
1
Daily Flow
Rate, cfs
pH,
SU.
TSS,
mgll
SS,
mlll
ffapplicable
Discharge
Turbidity,
NTU
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Fecal
Coliform,
col/100 ml
SA
Effluent
Limitations
Mo. Ave) Daily Max,
HQW ar ORW
50% of
7Q10
lndicare NO FLOW
if applicable
Ireshwater
6.0-9.0
saltwater
6.8-8.5
Industrial Sand
25145
HOworORW
20130
HQ. or 0RW
iQA Tr or PNA
10115
HQW, pRW,
SA, s9,PNA,
orrany Trout
0.1 /0.2
No Limit
Circle Water
Quality that applieStansard
511 0
NIA
Water Quality
Standard applies
NIA
Water Quality
Standard applies
NIA
Date Sample1�::
Collected,
moldd! r
<_`°;
�{'
} _
�, 2 rrj.;
02/19/2019
0.045
7.03
9.8
<0.1
19.2
NIA
NIA
NIA
06/25/2019
0.011
6.75
11.2
<0.1
20.5
N/A
N/A
NIA
08/29/2019
0.022
6.82
12.8
<0.1
8.79
NIA
NIA
NIA
12/ 19/2019
0.045
7.40
<5.0
<0.1
11.4
NIA
NIA
NIA
Permit Date 10/1/2015 — 9/30/2020
Last Revised 10-2-2015

Certificate of Coverage No. NCG02 t)❑ 3❑ 5❑®
CERTIFICATION
" i certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and
evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my
knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
[Required by 40 CFR §122.22]
r7 [ DNU; Hl' :+9nntl W Norman orvnia
c=us, E•nm ers®amen. nm
0-
r o••cliaran. uc•.
L En.rpm�sny A
Signature
QU- W, CN-N
QyW":20 0MA I an 4 41-
aa�:�ozo.ez.,, o,.1.„_0D
Date February
11, 2020
Mail Annual Summary Wastewater DMR to the NCDEQ Central Office:
Note the address is correct - Central Files is housed in DWR (not DEMLR)
N.C. Department of Environmental Quality (DEQ)
Division of Water Resources
Attn: DWR Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files Telephone [phone]
Questions? Contact DEMLR Stormwater Permitting Staff in the Central Office at:
[phone]
Permit Date 1011/2015 — 9/30/2020
Last Revised 10-2-2015

RESEA Ch & ANA[ylricAI Report of Analysis
r: LAORUORiES� ONC. 2/28/2019
sµ►rirrrrri�
ANA
For: Charah, LLC
.�`G.�lrp"i,�'O
435 South Tryon Street
Suite 180
Charlotte, NC 28202
•o
z� (P
:CO NC t434
Attn: Kyle Hoover
y NC tt37701 =
i y
• r
�.QSCT�¢' ��
44111111311110
Client Sample ID: MP-01
Lab Sample ID:
63253-01
Site: Colon Mine
Collection Date:
2/19/2019 14:31
Parameter
Method
Result
Units
Rep Limit Analyst Analysis Date/Time
pH
SM 4500 1-1+13-2000
7.03
Std. Units
2/19/2019 1431
Settleable Matter
SM 2540 F-1997
<0.1
tnlll
0.1
AW 2/20/2019 1430
Total Suspended Solids (TSS)
SM 2540 D-1997
9.8
mg/L
5
AW 2/25/2019
Turbidity
EPA 180.1
19.2
NTU
1
AW 2/21/2019 0940
NA = n01 ❑ric:Iy;', Ci
P.p. Bax 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] wvmrandalabs.cow Page 1

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For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
7/3/2019
1��11111I Ffo'
64.
.Q D:Vnr
NC 434 Z.
NC 1137701
Client Sample ID: MP-01 Lab Sample ID: 68639-01
Site: Colon Mine Collection Date: 6/25/2019 13:24
Parameter Method Result Units Rea Limit Analyst Analysis DaterTime
pH SM 4500 H+B-2000 6.75 Std. Units 6/25/2019 1324
Settleable Matter SM 2540 F-1997 <0.1 mlll 0.1 AW 6/26/2019 1400
Total Suspended Solids (TSS) SM 2540 D-1997 11.2 mg1L 5 AW 6/27/2019
Turbidity EPA 180.1 20.5 NTU 1 AW 6/26/2019 1600
NA = not analyzed
P.O. Sox 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 1
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RESEARCk & ANALyTiCAL
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RESEARCk& A14AIy1riCA[ Report of Analysis
UbowwiIES' Ncs 9/6/2019
911111oo..
��r
For: Charah LLC
435 South Tryon Street
Suite 180
,•`�QG .•••••.,
Charlotte NC 28202
: ° o'• cn
10 NC #34
r
Attn: Kyle Hoover
V. NC437701
•
Client Sample ID: MP-01
Lab Sample ID:
71446-01
Site: Colon Mine
Collection Date:
8/29/2019 15:18
Parameter
Method
Result
Units
Rep Limit Analyst Analysis DaterTime
pH
SM 4500 H+8-2000
6.82
Std. Units
8/29/2019 1518
Settleable Matter
SM 2540 F-1997
<0.1
ml/I
0.1
AW 8/30/2019 1600
Total Suspended Solids (TSS)
SM 2540 D-1997
12.8
mg/L
5
AW 9/4/2019
Turbidity
EPA 180.1
8.79
NTU
1
AW 8/30/2019 1600
NA = not analyzed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 1
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RESEARCh & ANA1yTICA1
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XESEARch & ANAlyricAl
LAboRATORiES� INC.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
12/31/2019
C q
:co NC 434 Sn
Z.
NC 437701
°a
U APB,
Client Sample ID: MP01
Lab Sample ID:
76331-01
Site: Colon Mine
Collection Date:
12/19/2019 10:49
Parameter
Method
Result
Units
Rep Limit And Analysis DatefTime
pH
SM 4500 H+B-2000
7.40
Std. Units
12/19/2019 1049
Settleable Matter
SM 2540 F-1997
<0.1
ml/I
0.1
AW 12/2012019 0745
Total Suspended Solids (TSS)
SM 2540 D-1997
<5
mg1L
5
AW 12/2312019
Turbidity
EPA 180.1
11.4
NTU
1
AW 12/20/2019 1030
NA = not analyzed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 1

RESEARch & ANALyTiCAI
LABORATORIES INC.
Analytical / Process conoultatlons
Phone [phone]
CHAIN OF CUSTODY RECORD
ISM

ANNUAL SUMMARY DISCHARGE MONITORING
REPORT (DMR) —WASTEWATER
SUBMIT TO CENTRAL OFFICE*
General Permit No. NCG020000
Calendar Year 2019
*Report ALL WASTEWATER monitoring data on this form (include "No Flow"/"No Discharge" and Limit Violations) from
the previous calendar year to the DEQ by MARCH 1 of��h•ye�re„ a„_._
Certificate of Coverage No. NCG02 UUUU
FEB 12 2019
Facility Name: Brickhaven No. 2 Mine Tract "A"
Chatham •EN j;Njt��_ s-ILE �,
County: DtC R r; _
Tln�!
Phone Number: (� Total no. of out a f's monitored 1
Certified Laboratory _ Research & Analytical Laboratories, Inc. Lab # 34
Lab #
Wastewater (WW) Discharge Outfall No. MP-01
Is this an industrial sand mine (See 40 CFR §436 Subpart D)?
Yes ❑
No S]
Does this outfall discharge WW to SA waters?
Yes ❑
No EN
Does this outfall discharge WW to SB or PNA waters?
Yes ❑
No
Does this outfall discharge WW to HQW or ORW waters?
Yes ❑
No ❑X
If so, what is the 7Q10 flow rate? or Tidally influenced waters,
7Q10 not available ❑
Does this outfall discharge WW to Trout (Tr) designated waters?
Yes ❑
No ❑X
Were there any limit violations in the calendar year?
Yes ❑X
No ❑
Outfall No.
MP-01
Daily Flow
Rate, cfs
pH,
SU
TSS,
mg/1
SS,
mIII
irappficable
Discharge
Turbidity,
NTU .
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Fecal
Coliform,
co11100 ml
SA
Effluent
Limitations
Mo. Ave I Daily Max.
HQW or 0RW
50% of
7Q10
Indicate NO FLOW
of applicable
freshwater
6.0-9.0
saltwater
6.8-8.5
Industrial Sand
25/45
HQW or0RW
20I30
HQW or 0RW
and Tr or PNA
101 15
HQW, ORW,
SA, 50, PNA,
or any Trout
0.110.2
No Limit
Circle Water
0 uality that applies: esard
50/25/10
NIA
Water Quality
Standard applies
NIA
Water Quality
Standard applies
NIA
Date Sample
Collected,
molddl r
MEMEMMMM
03/28/2019
0.67
5.40
<5.0
<0.1
6.33
NIA
NIA
NIA
06/24/2019
0.67
6.24
<5,0
<0.1
1.33
NIA
NIA
NIA
08/27/2019
0.67
5.99
<5.0
<0.1
8.42
NIA
NIA
NIA
11/20/2019
0.56
6.57
<5.0
<0.1
3.67
NIA
NIA
NIA
Permit Date 101112015 — 9/30/2020
Last Revised 10-2-2015

Certificate of Coverage No. N0002 ®3❑ $❑®
CERTIFICATION
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and
evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my
knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
[Required by 40 CFR §122.22]
Signature
Date February 11, 2020
flCp,0„�, ghee er namsma.e�.
I. LLC', au�'E.q�rtaalnY. En�i.�...—1 A a lkl f,
an.Na��
O1':ia o1.i i oe 345io5'Otr
Mail Annual Summary Wastewater DMR to the NCDEQ Central Office:
Note the address is correct — Central Files is housed in DWR (not DEMLR)
N.C. Department of Environmental Quality (DEQ)
Division of Water Resources
Attn: DWR Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files Telephone [phone]
Questions? Contact DEMLR Stormwater Permitting Staff in the Central Office at:
[phone]
Permit Date 10/1/2015 — 9/30/2020
Last Revised 10-2-2015

3S LI
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RESEARCh ANA1YTiCA
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
6/6/2019
} Iqurrlly��i
Jk"- "P.-
M NCn34 Z�
: NC037701
40
Nk
5 .
,r��rr11111��*
Client Sample ID: SBO #1 Lab Sample ID: 67498-01
Site: Brickhaven-Stormwater Discharge Collection Date: 6/3/2019 15:14
Parameter Method Result Units Rep Limit Analyst Analysis Date/Time
Settleable Matter SM 2540 F-1997 <0.1 mIR 0.1 AW 6/5/2019 0900
Total Suspended Solids (TSS) SM 2540 D-1997 11.4 mg1L 5 LP 6/4/2019
Turbidity EPA 180.1 12.3 NTU 1 LP 6/4/2019 1415
NA = not analyzed
P.D. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 1
Ial C:)�1 t)r^, 511: YIr

RESEARch & ANAiYTiCAt
LA ORAT®RiES� INC.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
10/18/2019
'Q
�co NC A34 Z.
s NC 037701
fo
Client Sample ID: SBO #1 Lab Sample ID: 73584-01
Site: Brickhaven-Stormwater Discharge Collection Date: 10/15/2019 14:19
Parameter Method Result Units Rep Limit Analyst Analysis Date
Settleable Matter SM 2540 F-1997 <0.1 mIA 0.1 AW 10/16/2019 1310
Total Suspended Solids (TSS) SM 2540 D-1997
Turbidity
EPA 180.1
16.0 mg/L 5 AW 10/16/2019
20.5 NTU 1 AW 10/17/2019 1224
NA = not analyzed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 1
rsl coa baSiC 4Id

U'(ESEARCh & ANA yTiCAI
r, LA ORATORIES, INC.
For: Charah, LLC
435 South Tryon Street suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
3/11/2019
�f"tll=lIlift
r
�,•`'�,b CYT�'*#
to NC M 3 4 Z (((JJJ777
r
NC437701
Client Sample ID: SBO #2 Lab Sample ID: 63930-01
Site: Bric&haven-Stormwater Discharge Collection Date: 3/8/2019 10:32
Parameter Method Result Units Rea Limit Analyst Analysis Date/Time
Settleable Matter SM 2540 F-1997 <0.1 mill 0.1 AW 318/2019 1345
Total Suspended Solids (TSS) SM 2540 D-1997 17.6 mg/L 5 AW 318/2019
Turbidity EPA 180.1 15.0 NTU 1 AW 318/2019 1611
NA = not analyzed
...-------_. __----_ ..— __... -
P.O. Box 473 106---- Sha—ri Streel_ Kernersviile,- _ --
Norih. __ Ca_rolina_--27284-_.--._Tel: [phone] Fax:---_ ---
336-936-0326 vr--ww.randalabs.co- ----- -m- - Page-- 1-

RESEARck & ANAty1racA[
LAORAT®ReEs, If4c.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
9/17/2019
Qr NC 1134 z -
NC 437701
f�E� AN�`�+•`•
Client Sample ID: S80 #2 Lab Sample ID: 71873-01
Site: Brickhaven-Stormwater Discharge Collection Date: 9/11/2019 10:30
Parameter Method Result Units Rea Limit Analyst Analysis Date/Time
Settleable Matter SM 2540 F-1997 <0.1 mlll 0.1 AW 9/11/2019 1415
Total Suspended Solids (TSS) SM 2540 D-1997 35.5 mglL 5 AW 9/12/2019
Turbidity EPA 180.1 39.9 NTU 1 AW 9/12/2019 1240
NA = not onoWed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 1
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RESEARCh & ANA[y1rBCA1
LA ORAr®RiESy INC.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
2/8/2019
` ��ti�tetrty�4
• �4r �A. ern =
NC 434 i' (n
NC .37701
Client Sample ID: SBQ #3 Lab Sample ID: 62622-01
Site: Brickhaven-Stormwater Discharge Collection Hate: 2/5/2019 12:16
Parameter Method Result Units Rep Limit Analyst Analysis Date/Time
Settleable Matter SM 2540 F-1997 <0.1 M14 0.1 AW 218/2019 1430
Total Suspended Solids (i'SS) SM 2540 D-1997
Turbidity
EPA 180.1
<5 mglL 5 AW 202019
7.40 NTU 1 AW 2/0/2019 1551
NA = not analyzed
P.p, Box 473 106 Short Slreet Kernersville, Nortf� Carolina 27284 TeL [phone] Fax: [phone] www.randalabs.com Page 1
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For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
1 0J2/2019
so
oD NC 434 Z; to =
NC 07701
ASP,'
Client Sample ID: SBO #3 Lab Sample ID: 72470-01
Site: Srickhaven-Stormwater Discharge Collection Date: 9/23/2019 14:11
Parameter Method Result Units Rep Limit Analyst Analysis DatelTime
Settleable Matter SM 2540 F-1997 <0.1 mI11 0.1 AW 9/24/2019 1400
Total Suspended Solids (TSS)
Turbidity
SM 2540 D-1997
EPA 180.1
11.4
16.5
mg/L 5 AW 9/26/2019
NTU 1 AW 9/24/2019 1612
NA = not analyzed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 1
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LAORMORkSil,
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, INC 28202
Attn: Kyle Hoover
Report of Analysis
6/4/2019
Client Sample ID: SBO #4 Lab Sample 1D: 67272-01
Site: Brickhaven -Stormwater Discharge Collection Date: 5/28/2019 16:00
Parameter Method Result Units Rep Limit Analyst Alysi nas DatelTime
Settleable Matter SM 2540 F-1997 <0.1 mIll - 0.1 Y AW 5/29/2019 1430
Total Suspended Solids (1-SS) SM 2540 D-1997 7A mg/L 5 AW 5/30/2019
Turbidity EPA 180A 6.48 NTU 1 AW 5129/2019 1422
NA = not analyzed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 1
rai rare ha'at; v'r!

�ESEARCh & ANAIYTiCAI
LAORATORiES, NCO
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
10/9/2019
pt<tttttt?t���i
NC #34 Z.
S NC 437701
• i
Client Sample ID: Si30 #4 Lab Sample ID: 72880-01
Site: Brickhaven-Storrnwater Discharge Collection Date: 10/1/2019 17:22
Parameter Method Result Units Rep Limit Analyst Analysis DatelTime
Settleable Matter SM 2540 F-1997 <0.1 mIA 0.1 AW 10/212019 1500
Total Suspended Solids (TSS) SM 2540 D-1997 5.4 mg/L 5 AW 10/3/2019
Turbidity EPA 180.1 5.43 NTU 1 AW 10/212019 1625
NA = not analyzed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel; 336-996-2841 Fax: [phone] www.randalabs.com Page 1
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UIESEARCh & ANA1y1FncA[
36,,: LA®RAir®RiES, Ptico
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
2/8/2019
trrtttt�t��fl,
�,�'
NC U34 z: en
NC #37701
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Client Sample ID: SBO 46 Lab Sample ID: 62623-01
Site: Brickhaven-Stormwater Discharge Collection Date: 2/5/2019 12:39 l
fParameter Method Result Units Rep Limit An_ alyst Analysis_Da_telTime I
Settleable Matter SM 2540 F-1997 <0,1 ml/l 0.1 AW 2/6/2019 1430 `!!!
Total Suspended Solids (TSS) SM 2540 D-1997
Turbidity
EPA 180.1
8.6 mglL 5 AW 2/6/2019
8,89 NTU 1 AW 2/612019 1555
NA = not analyzed
P.O. Box 473 106 Short Street Kernwsville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randatabs.com Page 1

KESEARCh & ArWyirQcAl
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
8/29/2019
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AMtYT0I *.
4
NC434 Zi
= NCh37701
40
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Client Sample ID: Brickhaven Stormwater S606 Lab Sample ID: 71282-01
Site: Charah, Inc Collection Date: 8/27/2019 9:52
Parameter Method Result Units Rep Limit An_ alyst Analysis Daterrime
Settleable Matter SM 2540 F-1997 <0.1 ml/I 0.1 AW 8/27/2019 1430
Total Suspended Solids (TSS) SM 2540 D-1997 17.6 mg/L 5 AW 8/28/2019
Turbidity EPA 180.1 20.9 NTU 1 AW 8/28/2019 0935
NA = not analyzed
P.O. Box 473 106 Short Street Kernersville. North Carolina 27284 Tel: [phone] Fax: [phone] www,randalabs.com Page 1
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RESEARCh & ANAIYTiCAI
:. LA®raa.T®RiES, NCO
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
6/4/2019
cu
a e p A
's co NC #34 z; cn
NC $137701
w : i
5iti,
Client Sample ID: SBO V Lab Sample ID: 67271-01
Site: Brickhaven-Stormwater Discharge Collection Date: 5/28/2019 10:21
Parameter Method Result Units Rep Limit Analyst Analysis Date/Time l
Settleable Matter_ SM 2540 F-1997 W <0.1 ml/I_ 0.1 AW 5/29/2019 1430
Total Suspended Solids (TSS) SM 2540 D-1997 16A mg/L 5 AW 5/30/2019
Turbidity EPA 180.1 20.7 NTU 1 AW 5/29/2019 1415
NA = not onClyzed
P.O. Box 473 1Db Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: 336-996-D326 www.randalabs.com� _ Page 1
SI c:na I�Ff,ir, J'id

RESEARCk & ANA1YTiCA1
i . r LA ORAimiES, INC.
i
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
8/29/2019
.o
�di NCtt34 Z.
S� NC #37701
Client Sample ID: Brickhaven Stormwater SB07 Lab Sample ID: 71283-01
Site: Charah, Inc Collection Date: 8/27/2019 9:24
Parameter Method Result Units Rep Limit Analyst Analysis DatelTime
Settleable Matter SM 2540 F-1997 <0.1 ml/I 0.1 AW 8/27/2019 1530
Total Suspended Solids (TSS) SM 2540 D-1997 22.2 mg/L 5 AW 8/28/2019
Turbidity EPA 180.1 34.0 NTU 1 AW 8/28/2019 0940
NA = riot anclyzed
P-O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] fax: [phone] www.randalabs.com Page 1

Part A Continued: Wastewater Monitoring RLquiretnents 4701
outfhlt No
�,� �
:-G�13�' � ' � .4
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.
tlt�iiftyi-
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col/ml:,a
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MAIL ORIGINAL AND ONE; COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCIIAW_.' V" & 1XV11T
VIOLATIONS) BY 111ARC11 1 OF FAC1-1 YEAR TO:
Division of Water Quality
Attn: DWQ Central Piles 1617 Mail Service Center RECF1\1E
Raleigh, North Carolina 27699-1617
[phone] FEB 12 2019
V0I/ ilfUST SIGN TIIIS CERTIFICATION FOR ANY INF'ORA?ATION REPURTED: CEN 1 t:I,L FILES
I certify, under penalty of law, that this document and all attachments were prepared under my'direeHw+r�r supervisiun in accordance +with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and beliel', true, accuritle, and complrle.
I am aware flan, thrrP FwN donifmint tie tltaes for submitting false information, including the possibility of fines and imprisonment for knowing violations,"
1 I Ff
(Signs; ure of Nrmitteef (Date)
Permit Date: 1/1/2010-12/31/2014 Lab[ Revised 02-01- 1 1
P'ICC 3 of-2

P
Part A Continued: Wastewater Monitorine Requirements reI6r'-Aar'-N dotct
Outthll t1 y`
yhLir f''`'�
s �
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NIA11. ORIGINAL AND ONE C01'Y ON 'l RIS ANNUAL SUMMARY (INCLUDING ALI. "NO FLOW", "NO 1)INC:I IA3tGE" & LIMIT'
VIOLATIONS) BY AIARCII I OF EACH )TAR'1'O:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
v)I9) 807-6379
YOU MUST SIGN THIS CF.R77FICATION FOR ANY INFORMATION RFPURTCD:
"I eerlify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in aveortlaacc nith a ayslou designetl i„
assure that qualified personnel properly gather and evaluate the informatiun submitted. Based un my inquiry of the person. or persuns who inauage the yysteii,, m
chose persons directly responsible for gathering the information, the infurmatiun submitted is, to the best of my km)N ledge and brlicf, tr-ur, uccurutc, and Votli ,lt-ty
i atn aware that than a %t niftwill ue t rs for submitting false information, including the possibility
loff fines and imprisoninent for knowing riolaliuus."
-f
(Sig lure of Permittee) (Date)
Pormit Date: 11112010-121310014 l..a�,,[ Keyiscd 0)-0-' i
I wc- i nt

Part A Continued; Wastewater Monitarina Requirements MrTIA r901q
0ut[hll1�ahMN.
r `
zhkj1r
,
r X
Settleable Solids
pH
*tA2
Standard'
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NIAIL ORIGINAL ANTI ONE COPY OF THIS ANNUAL SUMMARY (INCLUDINGALL "NO FLOW", "NO Illtii_'llrtltt:I'.:" .\ LIMIT
VIOI.ATIONS) BYhf-iRCll I OF EACH YEAR TO:
Division of Water Quality
Attii: DWQ Central Files
1617 ?vlaiI Service Center
Raleigh, North Catalina 27699-1617
�91Q) 907-6379
YOU AIUST SIGN THIS CERTIFICATION FOR ANY INFORMATION RRPORI ED.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accuralstuce rri111 it S)'ACHI dr,iknral It,
assure thal qualified personnel properly gather and evaluate the infurmaliun submitted. Based on my inquiry of the person or lice -suns who uranagv the system, r#1
11rose Persons directly responsible for gathering the information, the Information submitted is, to the best of my krrowtedgr and belicf, ii-ue, accurate, anti cunrl,WIV
I am aware th§at thorn —e 0ornifioaut neu6il ks for submitting false infornialion, including the possibility of tines and imprisonment for knowing riuialions,"
_ 3l'1T1(g
lti gnature ar Permitteel (pate)
Permit Date: I/l/2010-12/31/2014 Lust Itevis(%t tie' -o-'- t i
! hvi i 1kt, )

Part A Continued: Wastewater Monitorine Reauirements A grd ;01 y
56#1eableSolids
pH
Fecal Cotiforms
s�%r, x
:;
i4p N*•is; ,.
t`*
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MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY itNCLUDtNG ALL "NO FLOW",'*NO IDISCtIARGF" & LI1VUT
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed it)
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who mttnagv the sY;teni, 01
(hose persons directly responsible for gathering the information, the information submitted is, to the best of my Liwwledge and belief, [rue, accurate, aatl romplc-u•
I am aware. that tharr rare civnittaant peuall•Jes for submitting false information, including the possibility of fines and imprisonment for knowing violatioua."
Iti✓r�nature o Perinitteet (Date)
Permit Date: 1/1/2010-12/31/2014 last ifrvisrd 02-0 -{

Part A Continued; Wastewater Monitoring Requirements M" 10 iQ
Ouito11 r o.
.�^;
+:: '�
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MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLONv-, -NO DISCI IA14C1,.7 &- LIMIT
V101,ATIONS1 BY MARCII l OF EACH YEAR TO:
Division of Water Quality
chin: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"i certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a sPorttt designed lu
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persona who tnanage the system, o
those persons directly responsible for gathering the information, the information submitted is, to the best of my knuwledge and belief', true, acvurate, and cumpicic
I am aware.. that there sere cionifioant Reai—IDes for submitting raise information, including the possibility of fines and imprisonment for knowing ►•iulativus."
5/zl�l�
i sign ure of �Prrrnjttee) (Date)
Permh Date: 1/112010-12/31/2014 Last 1tr%c--.rd
Kwr , n!

Part A Continued: Wastewater Monitorine Requirements 5u✓tc. .20{q
.
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1 .., �t1T'rt,~} „yA
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HAIL ORIGINAL AND ONE COPY OF THIS ANNUAL.S.UNIMARY (INCLUDING ALL "NO FLOW", "NO DISCI 1ARGL" & L11�1 T
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Attu: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
(919) R07-6379
YOU AIUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance "All a system designed Iv
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or pri-som w lw nrauage the System, ul
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief', true, accurate, aml comilivir
I am aware. that thPrP nrr cionifiwnt nev61@1es for -submitting false information, including the possibility of tines and imprisonment fur knowing viulmions."
05ign3fre Jr Perinitteel (Date)
Permit hate. 1/1/2010-12/310-014 1.ust Rt:VjSrd ()_' lr' i 1

F'ari A Confirmed: Wastewater Monitoring Requirements J LL(, • 'IC C9
Outfall NO;-
I r, e:
s.�',•.:~- t, � �
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PH
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NO k
11#A11, 0111GINAL AND ONE COPY OF THIS ANNUAL SUMMARY UNCLUDING ALL "NO FLOW", "NO 1)iSCHAKIL;U" 4` LIMIT
yioi,.vrIONS) BY ALIRCH 1 OF EACH YEAR TO:
i Fivklon of Water Quality
Atin: I-)WQ Central Files
I r, l 7 ;t l;t i t Service Center
1616ah, North Carolina 27699-1617
(,oI0 07-<;774
l'ob' J1l,:U SIGN THUS CERTIFICATION FOR ANY INFORMATION REPORTED.
"I rerlify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accvrdanee with it systrul drsignrd Iq.
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who Fnamlgr the systenF, M
Fh,Fec persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and be[iei-, trur, aCCUFHIe, 111ifl rLnnllb•u-
I ant aware flint thorn swe cif=nifmant nevgll es for submitting false Information, including the possibility of fines and imprisonment fur knowing viulatiuFFs,"
IS' matnre of Permitteet (Date)
11i'mm fait,,- 111/2010-12/31/2014 Last Revisr-d 0-1-0' 1 1
F-';r..r , ,0 1

Parl A Continued: Wastewater Monitoring Requirements Q„4—�- aqq
�
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MAIL URICINAL AND ONE COPY OF THIS ANNUAL SUN MA1iY ItNCLUDlNG ALL "NO FLOW", "NO D!_SCHAI GL— &- LOUT
\1101,,�TIONS) IIY AIARCH 1 OF EACH YEAR TO.:
1"ravishcn of Water Quality
Alin: DWO Central Files
rtil 7 11dail Service Celiter
I:alria4r, Norlh Carolina 27699-1617
i 0lo Cli1-r;179
I o 111 ! LIN T.VIGN 77I1,5 Cli R7'11 "I Q 710A' FOR AN F INFORAL-1 T1 UN REPORTED:
"I cerlify, ender penalty of law, that this document and all attachments were prepared under my direction or supervision in accordarncr with ar » seem designed ril
!i"ier'e that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who inauagc thr sl•s1rin, of
rhnsc her4nns directly responsible for gathering the information, the Information submitted is, to the best of my knowledge and belief, trur, accurate, anal cumiflrrx
I am awar•r it abort art cioniYeotrnt nepfilt;es for submitting false information, including the possibility of fines and imprisonment for knowing viulatium,"
rat rr reel (Date)
I>crmi! Ftarc: 1/1/2010-I2/31/2014 I_.ttsr Kevised
lhAO. i "t"'

tart A Continued: Wastewater Monitoring Requirements 51--p �_"b ._ 9-41Iy
".fir r �.• �r:�ii'.
% s �tt�[s.�• :� l7ttII
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i 1.-kIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", -NO DISCHARGE" -K LIMIT
%'101-ItTIONS) RY MARCH 1 OF EACH YEAR TO:
I'Irvi.sion of Water Quality - - -
AIIIII DWQ Central files
t o 17 %'1:1i1 ",elvice Center
I0Icigh, Milli Carolina 27699-1617
I'tl'>1 Q1�i-ri�79
VoU MI N►'S167N MIS CER'1'1FI[:. I T70A' FO►i .•IN}' IiVFORA1.91"IONREPUR7ED,
"I evrtif., under penalty of lqw, that this document and all attachments were prepared under my direction or supervision in accurclancc %N itil to ,.stern dc:i+wticJ I,'
:,.cnrt Mal 1lunlified Personnel properly gather and evaluate the infurmation submitted. Based on my inquiry of the person or persons �. ho utarl:rcc the .ystent, --I
rlrrt:., 1wr•cnms directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belicl'.. Iran, uccuruty. tort! rontlolk-tt.
I orn :In':rrr Ihnr ell rr +—e ioni nt "evilDes for submitting false infurmulion, including the possibility of rtncs and imprisunlneni fur klRM ing + iulntitrns."
-� r
(Slanature of Perml (Date)
Ponnii Data: 1/1/2010-12/31/2014 I.Lasl Kvvisvd0"-tl'-I o
PI,e , ill")

11:irl A Corrlinited: Wastewater Monitoring Requirements �(_}ta��r' )-Oi5
outfsn P40t
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NIr111. ORIGINAL AND ONE (DOPY OFTHIS HIS ANNUAL SUMMARY INC'.LUDI<NC ALL "_NO FLONN"', "NU_I)_ISCIIARC 1.4-- c\ Ll_MIT
V101.ATION5) RV AIARCII I OF EACH YEAR TO:
1)ivisinn of Water Quality
:�IIn DWO Cenlral Files
I r, I) klaiI Service Cenier
k,llrlRh. North Carolina 27699-1617
I `i I !11 RW7-0179
11)11 ilIIISTSIGN THIS CF_NTIF7CATION FOR ANY INFORA1ATION REPORTED:
"I cer•tlf}I, under penalty of law, that this document and all attachments were prepared under my direction or supervision ill accurdance with ii systrnt dirsigned i,r
:I"nry Thal qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person o1• persons who Manage tine system, ilr
ihosc persons directly responsible for gailiering the information, the Information submitted is, to the best of my knowledge aitd helief, t►•ur, ticcurite, will comph•it-
1 :1111 aware t1t5bt if nirtoant Im sifts for submitting false information, including the possibility of tines and iniprisounient fur kitowiug viulalimis."
+aar1 'e (It PC lice) (Date)
llomw 1 im,%- 1/10010-12/.31/2014 L.,is1 Revisc-d
; of, ,

Part A Continued: Wastewater Monitoring Requirements cut? bci- col
_
OutNll No:
1• �
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MALT. ORIGiNAI AND ONE COPY OF TI11S ANNUAL, SUMMARY (INCLUDING ALL "NO ),:LOW", "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons direct responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am awar the a sig ficant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
fir f Perm a (date)
Pcrmit Date: 1/1/2010.12/31/2014 Last Revised Ot-21-11
Page 2 of 2

Part A Coufinued: Wastewater Monilorina Renuiremenls r r `ao rf
• � -
�3utfail'Nu
Date Sarriple; '� �
- ' t
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MAH, ORIGINAL. AND ONE COPY OF THIS ANNUAL, SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH 1 OF EAr,,H YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aW re that them are significant pc • o submitting raise information, including tlic possibility of t7nes and imprisonment for knowing violations."
(Signature of rmil (Date)
Permit Date: 111/2010-12/31/2014 Last Revised 01-21-1 I
Page 2 of 2

L/
;4 RESEARCh & ANA[yTICAI I
� LAbORATQRIES, INC.
AnalyticallProcess Consultations
05 April 2019
Mr. Kyle Hoover, P.E., P.G., PMP
Environmental Protection Specialist III [RECF'1 F-
Charah, LLC
435 South Tryon Street FEB 12 2019
Suite 180
Charlotte, NC 28202 {�{ +'►LEA
SCripftl
Dear Mr. Hoover:
Enclosed is one (1) copy of the Brickhaven Mine Quarterly Wastewater monitoring analysis for the
sample collected at the Brickhaven Mine site identified as MI'Ol on 28 March 2019. If you should require
any additional information or have any further questions concerning the information contained in this report
please feel free to contact me at 336.996.2841 or [e-mail].
Best Regards,
Sidney L. Champion
Executive Vice President
Director of Laboratory Services
Research & Analytical Laboratories, Inc.
P.C. Box 472 • 106 Short Street • Kernersville. North Carolina 27284 • 336-996-2841 • Fax [phone]
www.randalabs.com

RESEARCH & ANA1YTiCAt Report of Analysis
LA O RATO Ri ESF INC. 4/4/2019
,i�,r- s ` ,rn,I,
For: Charah, LLC
.• ..••"••••••,/�(80
*�'�
V C�o
435 South Tryon Street Suite 180
��`�.����
;
Charlotte, NC 28202
CC z Q n i �n
�tq NC#34 Z
Attn: Kyle Hoover
• s NC#37701 2
's ;
Client Sample ID: MP01
Lab Sample ID:
64707-01
Site: Brickhaven Mine
Collection Date:
3/28/2019 9:59
Parameter Method
Result
Units Rep Limit An� alyst Analysis Date[Tlme
pH SM 4500 H+13-2000
5.40
Std. Units
3/28/2019 0959
Settleable Matter SM 2540 F-1997
<0.1
mIA 0A
AW 3/29/2019 1430
Total Suspended Solids (TSS) SM 2540 0-1997
<5
mg/L 5
AW 4/2/2019
Turbidity EPA 180.1
6.33
NTU 1
AW 3/29/2019 1424
NA = not analyzed
P.O. BOX 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] WWW.Fandalabs.com Page 1
ral coo basir, vid

REsFAR6 & AMALyTicAL
UboRATOR!ESl Ific
AnalytlCM / Process Consultations
Phone [phone]B41
CHAIN OF CUSTODY RECORD
IVater / filaste-wafer
Afisc:
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Sample'lentperaturc at reccipt - L-
•C r '

RESEARCh & ANA1yTICA[
�-� LABORATWES, INC.
�r
Analytical/Process Consultations
CASE NARRATIVE
One (1) water sample was received in good condition on 29 March 2019. The
sample was analyzed without difficulties unless noted below (RAL #64707).
J,,� // a-y,-
GPI /01 Iy 1
Sidney L. Champion
Director of Laboratory Services
Date
R 0. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336.996-2841 • Fax [phone]
www.randalabs.com

l.� RESEARC i & ANALyTICAI
UbORATWES, INC.
Analytical/Process Consultations
28 June 2019
Mr. Kyle Hoover, P.E., P.G., PMP
Environmental Protection Specialist III
Charah, LLC
435 South Tryon Street
Suite 180
Charlotte, NC 28202
Dear Mr. Hoover:
Enclosed is one (1) copy of the Brickhaven Mine Quarterly Wastewater monitoring analysis for the
sample collected at the Brickhaven Mine site identified as MPO1 on 24 June 2019. If you should require any
additional information or have any further questions concerning the information contained in this report
please feel free to contact me at 336.996.2841 or [e-mail].
Best Regards,
Sidney L. Champion
Executive Vice President
Director of Laboratory Services
Research & Analytical Laboratories, Inc.
P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax [phone]
vAvwxandalahs.com

RESEARch & ANA1YTiCA1
LAORATORiES, INC.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
6/28/2019
,���G�Pi✓ry�+�l.Y �i�I
.�•�
M NCtl34
NC 1137701
40
r
Client Sample ID: MP01 Lab Sample ID: 68571-01
Site: Brickhaven Mine Collection Date: 6/24/2019 14:31
Parameter Method Result Units Rep Limit Analyst Analysis DateEime
PH SM 4500 H+13-2000 6.24 Std. Units 6/24/2019 1431
Settleable Matter SM 2540 F-1997 <0.1 ml/I 0.1 AW 6/25/2019 1400
Total Suspended Solids (TSS) SM 2540 D-1997 <5 mg/L 5 AW 6/26/2019
Turbidity EPA 180.1 1.33 NTU 1 AW 6/26/2019 0923
NA = not analyzed
P.O. Box 473 106 Short Street Kernersville. North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 1
E iEI Cilia 1; Fi::. ' E'_i

{ RESEARCk & ANALYTICAL
UbORATORIES, INC.
Analytical / Process Consultations
Phone [phone]
CHAIN OF CUSTODY RECORD
li'crtcr/ iVrrsleiJ�rrlcr
Afixc•.
!('mllps:nN�' j _
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tinmplr'IemperuJurral rccripl •�,�} °( —

RESEARCh & ANA yTiCA1
LABORATORIES, INC.
Analytical/Process Consultations
CASE NARRATIVE
One (1) water sample was received in good condition on 25 June 2019. The
sample was analyzed without difficulties unless noted below (RAL 468571).
/,�� // g�"— 06j28)J9
Sidney L. Champion
Director of Laboratory Services
Date
P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax [phone]
ww w,rendalabs.com

RESEARCh & ANA1yTICA[
,-' LkORATWES, INC.
Analytical/Process Consultations
30 August 2019
Mr. Kyle Hoover, P.E., P.G., PMP
Environmental Protection Specialist III
Charah, LLC
435 South Tryon Street
Suite 180
Charlotte, NC 28202
Dear Mr. Hoover:
Enclosed is one (1) copy of the Brickhaven Mine Quarterly Wastewater monitoring; analysis for the
sample identified as M111-01 collected on 22 August 2019. If you should require any additional information
or have any further questions concerning the inf-ormation contained in this report please feel free to contact
me at 336.996.2841 or infoPrandalabs.com.
Best Regards,
Sidney L. Champion
Executive Vice President
Director of Laboratory Services
Research & Analytical Laboratories, Inc.
P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2641 • Fax [phone]
www.randalabs.com

WIN RESEARCh & ANA YTiCAt
+3..qM
LA ORATORIES, INC.
L�220-wj
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
8/29/2019
r�surulrr��i
J� \\& �rT/ ��ii
o
a 'a NC #34 Z.
w s NC937701
Client Sample ID: Brickhaven Mine MP01 Lab Sample ID: 71281-01
Site: Charah, Inc Collection Date: 8/27/2019 10:02
Parameter Method Result Units Rep Limit Analyst Analysis DatetTime
pH SM 4500 H+B-2000 5.99 Std. Units 8/27/2019 1002
Settleable Matter
SM 2540 F-1997
Total Suspended Solids (TSS) SM 2540 D-1997
Turbidity
EPA 180.1
<0.1
MIA
0.1
AW
8/27/2019 1430
<5
mg/L
5
AW
8/28/2019
8.42
NTU
1
AW
8/28/2019 0932
NA = not analyzed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www,randalabs.com Page 1
;:a� co,^ to is :1ci

RESEARCh & ANA[yTICA[
LAbORATORIES, INC.
Analytical / Process Consultations
Phone [phone]
CHAIN OF CUSTODY RECORD
MME

RESEARCh & ANA[yTICA[
LAbORATWES, INC.
Analytical/Process Consultations
CASE NARRATIVE
One (1) water sample was received in good condition on 27 August 2019. The
sample was analyzed without difficulties unless noted below (RAL #71281).
Sidney L. Champion
Director of Laboratory Services
o C 130
Date
P.O. Box 473 • 106 short Street • Kernersville, North Carolina 27284 • 336-996-2B41 • Fax [phone]
www.randalabs.com

RESEARC I & ANA[yTICAI
-L4t�l LAbORATWES, INC.
r�
_,. .
Analytical/Process Consultations
27 November 2019
Mr. Kyle Hoover, P.E., P.G., PMP
L-'nvironmentai Protection Specialist III
Charah, L I-C
435 South Tryon Street
Suite 180
Charlotte, NC 28202
Dear Mr. Hoover:
Enclosed is one (1) copy of the Brickhaven Mine Quarterly Wastewater monitoring; analysis for the
sample collected at the Brickhaven Mine site identified as MP01 on 20 November 2019. If you should
require any additional information or have any further questions concerning; the information contained in this
report please feel free to contact me at 336996.2841 or infoCa�randalabs. corn.
Best Regards,
Z4 // A, ---
Sidney L. Champion
Executive Vice President
Director of Laboratory Services
Research & Analytical Laboratories, Inc.
P.O. Box 473 • 106 Short SLreeL • Kernersville, North Carolina 27284 • 336-996-2841 • Fax [phone]
www.randalabs.com

KESEARch & ArWyTiW
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
11 /2612019
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NC $134 Z'
'• NC#37701
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Client Sample ID: MP01
Lab Sample ID:
75093-01
Site: Brickhaven Mine
Collection Date:
11/20/2019 12:21
Parameter
Method
Result
Units
Rep Limit Analyst Analysis DatelTime
phi
SM 4500 H+B-2000
6,57
Std. Units
11/20/2019 1221
Settleable Matter
SM 2540 F-1997
<0.1
mill
0.1
AW 110/2019 1345
Total Suspended Solids (TSS)
SM 2540 D-1997
<5
mg/L
5
AW 11122/2019
Turbidity
EPA 180.1
3.67
NTU
1
AW 11122/2019 0922
NA = not analyzed
P.O. Box 473 106 Short Street Ketnersville, North Carolina 27284 Tel: [phone] Fax; 335-996-0326 www.randalabs.com Page 1
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