NCG020072_COMPLETE FILE - HISTORICAL_20161227

,2W
STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
IV C& lQ DI) 7
DOC TYPE
�HISTORICAIFILE
❑ MONITORING REPORTS
DOC DATE
❑ � o ► 0a a �)
YYYYMMDD

Cat " LWO
38 Spruce St". Esat LwWnae ow, MA 0102E • FAX 413152"M • la 418f1t2S&M
December 27, 2016
Scott Mard w
Carolina Suarock, LLC
200 Horan Drive, State 100
RaleiA NC 27615
Project Location, Butner Quetry
CCaart Job Number.
Project Number: [naaej
Laboratory work Order Nwnber: 16L1044
Enclosed are results of analyser for samples received by the laboratory on December 20, 2016. U you have any question
eoncerniq this repast, please feel five to contact me.
Sincerely,
Kerry K. MoGee
Project Manspr
T" Of Contents
Page 1 of 13

Table of Contents
Sample Summary
Casa Narrative
Sample Results
16L1044-01
16L1044-02
Sample Preparation Information
QC Data
Table of Contents
3
4
5
5
6
7
8
Conventional Chemistry Parameters by EPA/APHAISW-846 Mettroas (fatal) 8
81SS374 8
BlSS405 8
B166406 8
B166483 8
Flag/QualWw Summary 9
Certificatlons 10
Chain of C istody/Sample Receipt 11
Page 2of13

' raga of Contahts
k en
(%f11'
ss Spnxv Sheet • East Lonp nmdowr, MA 01 M * FAX 41 6 "7a. 41
c, wlm. sunmck u.0
200 Hwisam Drivc. Suite 100
BalelRb, NC 27615
ATM Boca Martino
REPORT DATE: IMAM
ANALYTICAL SUADIAYY
WORK ORM N1B IaAo"
Tho resale of oWyses pofa mcd an 16e fntlnwing smapto sabndtted to the CUN-TOT AndyamI Labomtmyl are fmmd in ddt upon.
PROn= T=AnON: Bum= Qmny
FEUD LVAMA ff LAB M- MATRIX SAMPLE DLi3CR7rF6N TEST SUB LAB
Outlet 6 16'L1 N"I watt Water EPA 1664E
EPA 160.1
SM21 22 2MOD
SMI22 4500 H B
Ouiet 9 16LI044.02 Wasit Wat= EPA I90.1
SM2 i 22 2.WD
SM I-22 2MOF
SM1I-22 450O H B
Page 3 of 13

en
39 Spnwo Street' East Lwarmedpw, MA 01078 • FAX 41SAMS 906' TEL 413IM&M
CABS NAMAiIYY SUf1tmL►1<Y
All fepatiad rewdiy are vrithin defined Isbaratory quaff y canter] oWeatives unless (fated below or dhmw'laa gaalified In dd s npmt
OMl-22 MID 1110
H-OS
Holding ate was exceeded pH anabrda should be performed s * at time of satrrpligg. Nominal l S m(atme holding time was
exceeded.
Ataabta & Sampk*) QMDBad
PH
IA.1044-01[Outletb], I6LtO4+MOade191
The results of azwlyles reported onlyrelate to samples submittcd to the Con -Teat Ans"cal Laboratory for teatiM.
1 car* that the emilyses listed above, rmlew speeifloelly listed m subcontracted, deny, were performed under my direction eoowdimg In dx approved methodologies listed
Im this docammt, and that based upon my inquiry of those {individuals iumtedistety tespaadble for obtaiaimy the itsformA m, the material conteitud in this report Is, to the
best of my knowledge end belief, oeetnsto and complete.
W
Use A. Wortbinglon
project Manage
Table of Cmtanb
Pape 4 of 13

wom�® ThWe of Contwft
LABORATORY
38 SMM SftM • E*M Lmw medaw. MA 010M • FAX 41&12643106 • TEL 47>lM6,4M
prefect Locadea l3nmv Quarry Smmple Daoriptiam: Weds 0 L 16LI044
Date R=dvcd: 12120d2016
Fud ftmpk Nt OMW b SmwW: 12nQ % 09:30
Ssspuk w. If1.101401
saomle Matrix wade wa1;r
Convmd=M CMemMry Farness by RPAL4FBAtSW-M Mdbo i (ru4D
Daft
A2mnb n
An*u
Rantl:
RL DL
unto
AOttlsted
Pend
AdlpM
Aoaiyr!
pn@14.3•C
7.9
PH two
1
H-W 201424OBa
UfM6
12f12F1621A0
18
Sewc,MeSdidt
ND
0.10
MUL
I
SII I-n2MU
1212im
1212MGIW0
DAM
Totid Sumpmd SaU&
ND
5.0 42
MVL
1
9M21.2225M
12f27J16
12122/1613:10
LL
T-bift
0.79
0.50
NTI1
I
EPA 180.1
12121/16
12/21116 15:20
MM
O11A G cm ()AIM)
m
IA 12
MOL
I
EPA 16640
UW16
12=16 J"
LL
Page 5 of 13

Tebbe of t'idlltBlil$
dIII 39 Spruce Sbvd a Fast Longmeadow, MA OlOn' FAX 41WS2S4XW' lEL 4
Prpjeel tAK*tkm: Homer Qnarry Sample Da:cri d". Work Order. 14L1O44
Dote Received: 12/20/2016
Flew Sample p: Onflef 9 Sampled: 12)2vnl6 09..-W
Semnk1D: JUJU4.82
Saronle Masstx: Wage 5!per —
Cap o CbemhkT Pasaata: by EPAIAPOAATW4L46 Mew (r@W
Dole
Dawnft
Analrts
Ressdls
RL
DL Ucld Dlim!!ao
H1eiQt9d 141dhod
Prapasod
AWY4
pH ®14.5'C
9.0
~pH Lhdu 1
19r5 001324l66R 0
11=16
121t7116 2l-00
1S
Scoksble Solids
ND
0.10
BJA 1
SM21.22 2%W
1N21A6
12/211161630
DAI
Total Suspended Solids
ND
5.0
4-2 mg/L 1
ShOl-22 2340D
12WI6
IZW1613:10
1L
S-bidlty
1.3
0.50
NTU 1
EPA 180.1
12/11/M
12121A6 15:20
1NA4
Page 6 of 13

� '*tEsta Table orConter4ts
'lop, AWLYMW r
39 Spn" Stet' East Longmeadow, MA 01M 0 FAX 413PJ254405 • TEL 41=5 2=
Sample E>rt acdm Data
RPA 1664E
Lab Nemfm PneM 1D] Bseds Zubw [m14 Dap
16LI044-01 [Ouiet6l B166M 1000 11/l7/16
BPA 160.1
Lab Namber (held ID] Ba! eb Wdd [m1.( PbW 1914 Dab
16L1044-01 [Oedet6l B166374 25A 25.0 12/21/16
16L10t1-02(00ttet9) B166374 25A 25.0 12/21A6
1zMI42 2540D
Leh K=ber (Fldd 11D] Batr3 Ie01s! (a¢L( Due
161.1041-0I[tAelee6J 8166W 100 1=2116
16L104442 [Ostld 9] B166406 100 12aVI6
shut-22 25411F
Lab Nomber MM m] Bateh lot" [U] Date
16LI014-0I (Oullct6] B166373 1000 12n1n6
16LI044-02 (OU114 9) B166373 1000. 1=1/16
SMI-22 450 B B
Lab N®bw ]FLM DD] Bad# Iddd W4 Bats
16L1044-01 [Qade/6] 8166M 50.4 MOWN
16LI044-02 [Omlet91 B16"93 50.0 M22116
Pa O7of13

Table of Cwtents
APMYT" LA30RATORY
39 Spy Str" I East Longmeadow, MA 01CO * FAX [phone]M * TEL 41SW5-2=
QUALITY CONTROL
CzamwOomal Cbunh&y Parmeten by EPA/APHANW4W Mcbmie (Tat mD -(ftuft Cmtrw
Re wft SAM Boa= vim FJPD
-ytc Rowt [bait unib LAM Remit VAX Lhnift RPD Lbsk New
RE-k (9166VM41LKI)
hqwW&Andyzc& 12021p6
Twbidity
OM
NTU
I
LCS (816637&Wl)
ftp"&Amh=& 12J21/16
—i�ilo
Tw"ty
4b,--
050
4bo 993
LeSDap (B1607"mi)
h"arod & Awdy=& flal/ld
Twwdhy
0.50
NIV
440 99S 90.110 0.00 1
Dopikaft(B36M40m)
Saw= I ILI04442
PtqWW & Ana"od 12121116
O.So
NM
020 5.23
nbmk (036645401U)
hqstgd& Analyzed:12=6
Oil & (NM
1.4
nq;fL
LA:S(BI464054M)
Pnpavi & Amtym WM 6
Oil a coam MEK
19
nqVL
20.0 93.0 78-114
Bahl MIMS - SAW-U LWD
rmpmW & Amstymed; 121M 6
HD
2.5
-a&
hqmnd & Ana4m*. 1=16
ToW SuWamded Solfib
194
10
MVL
200 97,0 70.1-136
Batth B166493 - 9=1-22 0110 H B
LCE (8I66491MI) Prepama & Anw"D& 11=n6
6A PH units 6,00 100 98.5-110
Page 8 of 13

j� Tattle of Contents
LABORAYMY
38 Spruce SWM • Ese1 Longmeadow, MA 01=1 "FAX41SAIMS•61G1i' TEL 413tE2&=
PL ACJQUAll1 M OUKKAUY
• QC try h o�Csids o! ermehlished Gmhs.
1 Wide mcovery Gamin rabbis hM fir ddlicolt compound
j Wido RPD Anib es4b WW fm Afficub =Wom d.
0 Dam etterdod died ncommetdW or regulatory level
ND Not Doteeted
RL Rspmtmg Limit
DL i dkW Detects m Limit
blCL [tdud== ComlamimW Level
Ppeem reaovcrws and Fdolve percent dilkrmop (RPD&) are determined by to sanwm tnhlg vahtos In elm
uleaLdm which bave act been rounded.
No rrmft have hoes blank aftsated mku VoWftd in Me moo mtrative seethm,
H-0 Holding timo was mended pH amiysn sb=W be pm*uo d ittmaodiseely as thma of asrnplimg. Nomhal 15
numsto holding time was amec"
] Detected but below the Rqwqg Limit patireu ealMndim su dmdx themStae, mm# n in esemmd
conve"Ieon (CLP ~
Ps e9ot13

Table of Contents
U Spnm ft" • East LaMmeadaw, MA 01028 " PAX 413MM64MOS • TEL 413K25 2M
CER7IRICA7t8pii<fI
CordW And7m bctmcbd fo thh WPM
Aaalyte CarlMeatlow
EPA 166621 IN we&?
oil & cra,o CM24) C17)".�=C.W VA
EP.f MA1 fm Worr
TuNdity NC
Si1Q1-2s 2500 in Own
Total 8ugpm6ed Softds CT,MA,NfLNYAWC.MRi VA
SWI-22 45W HB to Wags
pH CTMA Rl
Tho CONJEST E-bosaaewsl labmt operalaa wader 1¢e folkwn caftmahow and soaediudoms:
Cods
D-aiptim
Number
Bvbu
ADIA
AiRA-LAP,LLC- ISO I7MS2=
100033
ozn/2018
MA
M DFP
M.MA100
060=17
CT
Caone U- Depwbneat of Publik Huhh
PH-0567
M9012017
NY
New York Ststo i gwbnc at of 0=101
108" NELAP
0U112017
NH-S
New Hompallhe BoArommCned Lab
2516 NELAP
GVVM17
RI
Rhode ldfaA Dqn msem of Health
LA000112
12f30/2016
NC
North Carolina M. of Water Quality
652
12/3 im 7
NJ
New; may DEP
M4007 NEW
W30M17
m
Florida Depupueut of Health
EV1027 NELAP
06/3Q' M
VT
VerpoutDvuftpmiofHealmLend L bm"
LL0IS036
07I30f2017
mm
Slate ofmaw
201 Ion
061914p17
VA
Cammo4arwa th of Vbgiaia
460217
12l14rZ017
Paw
New Nadu, EuvBaamratal IAb
2M7 NELAP
OP/W2017
Page 10 of 13

0
CHAIN OF CUSTODY RECORD
conmtesr "Wow", VOL-1044
ANALYTICAL LABMATOfl1f �PJl�wrn.�stlabs oem
ova ; har ✓ rale�nor,e: Y 7 T. 3
Q
Z
project Ftiopotaf Rwidedi (For b%bq wpoml
Oros propmmdota
Can -Test lah iD I Cllent Sampfe ID / bmceWm
f�r;a• r
39 Spruce Street page of
fast Langmaado+a, MA U1028
►.
0 Lob W Mir
M•c�e_oeec-.
U`
"Sac . I
ST�iatik
t-vw
Saffurmm
4
Twtedisrbas
rftaRill s to kt Con-Un kmW d a soecft monk rmV be aid
In eoecwmthm in maututo c code scow
.M- L-tare C•pW. U-Unknown
naae/lima. 11
O s-0av onatrr.
` o s.7ow o a p ma p MR orpftncd LandfiEi
,r GWPc O swttandfilr O UST O atc
0 PAM O oftr:
O '2a H. 'ts-►�0 OTHER
r r
O '72-wr'44)aY
1
i�
ftti �isTA1RiATtk�A.M-�1tEOArAFtiAlAfl1/i[�SS1F1lREA1�QLllST�Olt40M�U7lQU1pR.
Oti:±ri pCAiTL1oM1tiSELTORtSQ VirAPMMTWMVRLLeMVMWUNMALLQUMMAPAANWOMW
ll!A
=ate,
I - toed .
lfa"a .. .
MQjfi**jw-
R e tYltriCllrid
3 w Udhw c Acfd . - :
8 a SOdlm blpAt'. - :
x a Fla hj►drmdde
T a No lWasuffaee
a@tatlfe. -- .
al n sllydp
O = other�„w
NELAC & AIHA C N tified
PLLME 84 CAfSMX NOT TO MWAMMAT9 TOM OOCUKUNT

Table of Contents
so SPUN &L
East Laegetsedow, tW1 e1e28
P. 44UM= 14"
AN/►s_r/T�Ow1 �.ABORATppY
Fr 41 4204406 pap 1 of 2
*WW IDrIti COrrl
CUENT
RECEIVED BY:
DATE:
r
1) Waa the chain(s) of c.=Wdy rWhKulslted and elped?
— l
Yes No No COC Ind.
2) Does the chain agree with the samples?
Yes No
tl not, expteln:
8) Are all the m nnplas In good amwiltlon?
Yes x No
H not, explain:
4) How were the awnples remshred:
On Joe Direct from Samplirq­_ Ambient
_ In Cooler(s)
Were the aemples roceitned in Temperature Compifaaroe of (24'C)? Yes No WA
Temperakne 'C by Temp bleak Temperature -C by Temp gun
5) Are flrere Dissolved amples far the lab to filter?
Yes No
Who was notified Date Time
8) Are #we soy RUSH orJMRT HOLDING TIME awnples?
Yea No
Who waa notified OO'N Date-IDate-lapil& Tuna iLioo
Permisalan to oubowdract samples? Yes No
7) I.ocaden where awnpha are sba ed:
(Walk -In cUenffi only) If rot already approved
8) Do all samples have the proper Acid pH: Yes No
plerrt Slgttabtre:
NIA
9) Do off samples #rave the proper Base pH: You No
NIA X
101 Was the PC nodfad of env dhorenwrche wMh do CoC ra the aemale:: Ves NIA
Containers received at Con -Test
# of containers
d corrtalners
1 Liter Amber
18 Ox wnber
I500 mL Amber
8 o¢ amberldear
260 ml_ Amber flat ember
4 at embed dear jar
1 Liter P loch
2 am am
600 ml P'Iasttc
Plastic 1 O
SOC lot
Permrate KIf
250 ml. c
40 rnl Vlal - listed below
Cofisure 1 bacterlg bolds
bathe
Dls6olr►ed O bottle
Other glass IK
f
40 mL Web: # MCI
I :::::::: # Bfsutfate
12Q1.9 ::: # ThiosOMe
# Med all
# DI Water
Unpvserved
n"" � tuw fin.
F
Page 12 of 33

Table of Contents
Pape 2 of 2
i
(ReJaation CrNet Lhtbgl • lfalne Sample Acceptance Policy)
Any False statemerit wlll be brought to the aitterMan of Own
Dos GVT Rev. 4 AApust 2013 L*94n Taman Inbiafa: -t'�J�4A, MOM":
inba: >~lp j% J G 1 .-2:1
Page 13 of 13

�'��t
fill Amyma tAsoPAYMY
30 Spn= Street' East Longmeadow, MA 01M •PAX41SW54 W'TFi 41
November 4, 2016
Soap Martino
Carolina Sumoeic, Ux
200 Horizon Drive, Suite 100
Raleigh, NC 27615
Project Location. Butner Quarry
Client Job Number.
Project Number. [uone]
Laboratory Work Order Numbs: 1631350
Enclosed are results of analyses for samples received by the laboratory on September 29, 2016. If you have any questions
concerning this report, please feel free to cooped me.
Sincerely,
4tx, VO�6�
Lisa A. Worthington
Project Manager
Table of Contests
P t31 of 14

Table of Contents
Table of Contents
Sample Summary 3
Casa Narmfwe 4
Sample Results 5
1611350-01 b
1611350-02
6
1611350-03
7
Sample Prepara#on Information
e
QC Dam
9
Conventional ClcemMy Parameters by EPA/APHA/SW-846 Methods (Total)
9
B159631
9
13169774
9
$159866
9
Flag/Quatifier Summary
10
Certifications
11
Chain of Custody/Sample Receipt
12
Page 2 of 14

Table of Contents
con" r`®
MUMALUMBRArow
39 Spnx* Sb" " EoW Lon9moadav, MA 0102E • FAX 4131b294MM - T EL 413MI-M
Cawing Smmod4 LLC
200 Hofimm Dri+c, Soil.100 RKMT DATE: 11/ =ld
NC 27615 PURCHAMORD11R NU1t1BEL 106000
ATTN: SwU Mardoo
FAOJ®CT NLOM B L [n=j
ANALYTICAL Eii11D18ARY
WORK ORDER NL MM- 16i1M
M result. or.nalyrm pata®ed on tee fbUDWtng umpka FAA tme to tee CON -rear AnOydai Labwawy am &=d m tebt repmi-
PROJBCr LOCATION: Batoa Q-n
F]ffia SAMPLE 0
LAB m:
MAT= SAMPU IIESCRU 77ON
TBST MM LAB
'9
1611350-01
Qronad Water
EPA 1660
EPA 18D.1
SM21-22 2S40D
SWIM 2S40F
l0
19113S0.02
Otwmd Water
EPA 180.1
SM21,22 2540D
S1 I-= 23WF
6
1611330.03
Otmmd Wata
EPA 110.1
SM I-22 2540D
SM I-22 254OF
Page 3 of 14

40 - M-mlwk--a
39 Spmxo SU W • East Longmumdw, AAA 0102B • FAX 41SMS-04M 'TEL. [phone]
CASE NARRATIVE gammum
All repawd rem ae whin de5nod fabaratay genifty OenftTll oltjecdves mileaa IEatod below w otbarwfts gaall5ed 10 tAda repmL
71a: taanlb of andym npomd only relste to amq:les submitted to the Con Too Analydcal ]Abaatery for eeaiay.
t o rdfj that tbo =*. Uatd atm., unlm specifically tied as mboonhact4 if any. were pwf mid trader my dkcWm according to the apluoued atdhodo OWS tined
in dh dorummt, and dtar band upon my inquiry of tbam individuals fwmed;aaely responsible fan obhf ft the h6madon. the mmrld cold in Wa tepat is, to the
bW of my kwwtdp and bdicY mcmats and complete.
'4,,4, 'AIWW-A�—
lie A. woreinglon
Table of Contents
Page 4 of 14

Table of Conterds
All
Mull UWUPATW
39 Sprtwo Sbsaf • East Longmeadow, MA MOB • FAX [phone]M • TEL 41SWS- 852
Pmjca L.oeadon: ButnerQaaoy Semple D-oiptlaa: Walk OAW. 1611350'
Dow Raeeived; 9/29R016
n" Bampk M: 9 Sampled: WZM16 12.00
Baa1ale M. lf[1UM
Samok Matrix [hound Water
Cwmvndmd Cry Fn mdm by BtAIAPRAISW416 MdelSa b (r*&Q
Dula
Da4R1ma
Aaabta
Ra urb
ILL DL
Uelh Dun" ro~
Madw
P 1;,
Aaabad
At1d/+tk
Betde" Solidi
M
0.10
n A I
B RI-2225W
9/30116
9/301d"
LL
TabdSop®dedSolldt
$5
5.0 42
MVL I
SUMI-422MW
IQWJ6
IWM614M
IL
re6wiity
91
10
WTU 20
EPA 190.1
00116
91MI516:00
DRA
Oil a Oren (NBASj
ND
I A 1.2
ell. 1
EPA 16640
IWY16
IW6 13:13
U
Page 6 of 14

tTable of Cantante
��0
MAL
MW
LASt3Ali
20 Spruce SftW • Es3d Loromsedow. MA 01= • FAX 419152'5ddGS - T0. 413=11-2=
Pf*aLomtlmi: BuMerQoany SampIcDaWipdam Wwkozdw. HOUR
Dau Receivad 949=6
Film SmWk fk 19 S-Epka: 9/"16 1230
Samob m Hill -02
Seadla madx: [3ro�md Wader
C®v-donO Chuddry To mdm 6y ZPA/AFRAlSW-6661Mefsoda goiso
Daft Dmhfr w
A -a * k"ab RL DL Uo1zr DDatlQa F4pAQa d Me" Plqm AwAlmd AG*O
somm el Soft ND 0.10 mUL 1 S ]-n 25M *M6 OM612M LL
Told Snapaaded Sollda 87 5.0 41 Qua I SICI-22ISM 1MWJ6 IGM6 I&M LL
Ttiuhf t 1S0 SO WTU 100 EPA 180.1 1VM6 w30J16 1690 Dim
-Page 6 ,Df

Table of ContentB
DW
30 Spnroe Suaw * East !Longmeadow, AAA OIOM • FAX 4%G25a d • TEL 41MMUn
Avjecl Loc"m Bnmc QUmry S. wk Dnaipd-: Wads o d.c 1611350
D:m Received: 9179MI6
FhM SRpfe pi 6 Sampled; 9)29112D16 133o
8.=pkED. f61050-03
S mnla Mmuix: Onuad Water.
Canraat and Cbemk" Pam = by EPA/AFHMSW46f M.OMh (ToftO
Dds 1»
An.bft ResatD ELL DL Unth Dd4 sm rw~ 1q~ Ft+a" Ac*ud An 1 #
SadamblaSON& AID OAO m1JL 1 MM] 222SWF 9/M6 "M61225 IL
TOW amp=" SOtida 16 5.0 42 mvL 1 SMI-22 2540D 1o4116 104014..05 LL
Twbu ty 12 2.5 NTU 3 EPA 190.1 WM6 95Ol1616ro0 DIM
1. Page 7of14

p Table of Co *wft
39 Spruce Sbrtet • Eaa1 LorWneadow, MA 01078' FAX 41=26.040 * TEL 41SM25 2M
Semple Ev&atdm Data
SPA 16640
LabNo-be [Ndd m] Balu6 ludlw INA4 Dui
1611350-01 [91 B1S"66 1000 10106116
SPA 180.1
Lwb Nundw WAM ID1
Burt
ludtw Im14
Fhw Im11
Drab
161135"1 191
815%31
25.0
2.5.0
09JM6
1611250,02 [101
B[5%31
25.0
25.0
09/30/16
1611350-03 [61
B1S9631
25.0
2.0
0w[6
8M142 2540D
Lb N®bet MhW ID1
Bwueb
Iddd [mL]
Daft
16113$0.01[93
B1S9774
100
10104l16
1491350-M (101
Biswn4
100
IOW16
16113SI"3 (6)
131"M
100
I010V1b
SM2142 Isw
Lab Number 1P4M MI
!laecb Id1w [mL1
Dab
1611330-01193
B159M I000
09MI6
16113S0442 [101
B159600 1000
09/3N16
1611350-03 (61
B159M 1000
09mid
Page 8 of 1a

Table of Contents
AM I
M :kSt
�LL" IMW
N%U AWL Y"CM LA13DRATOW
39 Spn= Street' Ent Longnmdow, MA 01028 *FAX 413RQS.04M* TEL 41W525=
QUAUTVCONnM
Cmvcwd=M Cbcmb&y FAMUMny by KPAIAPHANW-M Mcgt*& (ftfto - Q=ft Cm b
Rq-timv Spew Rpm— %RBC JLPD
Aaflyte RcvA Unit Unity LAM Ri>mft %REC Unft RPD Lhaft ydMat
Bmkh B139631 - EPA ISM
MimkMISMI-SLID) Pnpnd & A=bo& 09 M4
TuAwify CAM 030 NTU I
Lco(pt""i-MI) Ptcpmmd3AndyM:OM16
LCS Dtkp MIS96N4=0
Prqmnd & Audy=d: 09WI 6
4.1
O.SO NTU
480 102 WHO 0245 5
RIfth DISM4 - uni-n n"D
Mak(81697744M)
hap" A AnOyo& IQW16
Total Suqxuded SoM
ND
2.5 Mali,
LcS (6t5m4-wI)
Ppqwod & Aid 1 &NO
Tow B=pw&d BOB&
142
1 D 0*1
200 71.0 70.1-116
Batch JBISM6 - grA 1664IB
Malak (B;S"66-")
PMNM& 1WO54n6 A=b=& I0/M6
m & am" (KEM)
ND
I A UVIL
L4C8 @3109866-M)
hMma IWM6 A=4aD& 10/ON16
cm A Or=" OMW)
19
WZJL
20.0 ".5 72-114
I Page 9 of ED

Table of ConWt8
LABORATORYAWYMM
SB Spruce Street' East Lonameadaw, MA M28' FAX 41811i254MM *TM 4/81526-2932
n A13/3 QUALMU 8U98dABY
QC ream[ is outside ofombliabod Imo.
1
Wtds recovery HnAts establlsbcd for difficult oompotmd.
2
Wide RPDtunic eaabti hod tar difcub eampoaad.
d
Date exceeded cliew rsoemmmded or regulstary level
ND
Not Detected
RL
Rgmrtmg Liapt
DL
Method Ddredoa Limit
MCL
M=mmo CmIan ram Laval
Pm=w ramveriea andselative ptaceal diftemncea OLM) am datanmioed by the softwore min; valoee m the
ealcaladon winch have r oa been rounded.
No Faults have bow bkd subcaetod rmlosa epeei&W is ate cm narrative section.
1 Dcmmd but below the Rtpmtin; Llmlt (lowwt tali mim stamdmd}; thaefoae, rtmh is an ridded
coauatratieo (CLP "iag).
Pa e10of14

Table of Ca dew
411101
r
39 Spruce Street' East Lmign dow, AAA OtO291 FAX 41SM5440$ • TEL. 41S1b25,2332
CmR77FDC4TKm
C.ened Arrayaes Included In Ob Report
Ana" C"Ileadont
EPA 166l1J in Wets
Oil A Cvoase (HEM) CT,MA NH.NYALNC.MLr,VA
EPA I$&I in Water
7%Aidity NC
SU21-2225011 in Warr
Total Suspended SoWh Cr MA,NH.NYAI.NC,MIVA
The CON-7UT Environmental! Labmtmy operatea under the followlrrg =dFWadons and uertdStadow
Code
Description
Numbea
Expirrr
AEH A
AMA -LAP, L.LC - ISOI7025:2005
10=15
02/1/2018
MA
MamwhasettsDEP
M•h1A100
06rAM17
Cr
Caunw&vt Department of PubHJr Health
PH4$67
09130I2017
NY
New Ymtr State Department of Health
109" NELAP
0411/2017
NWS
Now ilewpshite Envnonmeotel LAb
2516 NELAP
0215/2017
RI
Rhode Ialard Department of Health
LA000112
12/30)7016
NC
North Carolina Div. ofWeterQus*
632
12/3112016
NJ
New Juaey DEP
MA007 NELAP
061311/2017
FL
Rorids Dgmrtraent ofIioalth
E871027 NELAP
0613012017
VT
Vermont Department of Health Lead Laboratory
LL.015036
07/3012017
ME
State of Maine
201 W28
061grM17
VA
Commonweekh of Virginia
460217
12114/2016
NH-P
New Hampsbim Environmental Lab
2557 NELAP
091612017
0
Page 1 i of 14

cQ n mNsto
ANALY"CAL LABCOATIOW t,
Company lame: f%,5'(,�i�'t�� Telephoee:
-
Address: E Project A
mqmd
Project MwoW Provided? {tar b0ftvavaml
O ns .�. pmpm* dm
Co
Can -Test ldb ID oJem Sample ID / Description "a
CHAIN OF CUSTODY RECORD
r�
arm
O art%a
O "Enheu w om Psd
�#Natrbc Cent
Comsaaxes -Grata eaae Coodr
3s 5 Street
East LwWneadaw. MA 01028
use the fdJmM nE codes mkt Can -Test imow of ■ specific sample maybe
Meoommadas to9AWb4TAoac.Coda9we
n- rt4vr. m
MTMMM
is ittfstaronnd
, Drawn
Q 5-0" Nrrtb:�
rc} Dartel rbne: ! SW51
2&Hrr'48-ilr OMER
l7attjiinte: O �72�Itr'4 Gh�r---�9 =f5- R.n�rkaa tab'PW Q dmV0 ARTSATa doAAi, TM CAT An =6+ttY M teWNI tsW=7"M AM aeut3'rst]M! CWVOM CHOW
Wt iitMW OUT Otf WWMY CM 5 RTOOiAt Wr, ltiR1TANC M V1W g1pJ,SM MW LO MAiL 4t#S WM ARE Ate.
0 UWA 0 read orphaned twwon
0 MLwofla 0 UST 0 fmc
Pap—o-
0hu*adkfeWh
O Rem tT Wed
Ot.btnaker
A�asnber�ss
P•ptmtic
ST.stwile
V= Tlaf
S-wxnms an
t-"ar bag
CoOther
..A,,
f • hxd
H s HCL
M = hA oumm
N a nitric Acid
S StMurtc Add
B a Sodium bisulfate
X th hydroxide
T = tilt thiasnlfMe
O a Other-
fiat:
W WP wAstewatdr
Vwx drtnldns water
A+alr
S = soillsottd
SL4 skodp
Qadtlwf�
0 ocher:
--I
NE LAC & AIHA Certified
o
WaE/bBE Certified
0
PLMR BE CARMVL"C i TO CMAWMTE THIS DOOMtE a
y

39SpfYg8L
SON I.oegrnasdow, IAI� 01028
ME
c�-nwbest®
P: 4134254M
e..•. awe ..wa
ANALV'"aAL LABORATORY
CLIENT NAME:
^aka 1 of 2
Table of Contents
a4lFfltY^.:�i9.'i�.Y�Yi �:]eG� �WRtltleiw,'�
RECEWED BY: rC.$ DATE: 30
11) Was the chains) of custody relinquished end signed? Yes �/_ No
2) Does the chain agree with the samples? Yes �� No
U not, explain:
3) Are all the samples In good condition? Yes ,/ No
If not, explain:
4) How were the samples received:
On bed% Direct from Sampling-- Ambienl In Cooler(s)
Were the samples received In Temperature Compliance of (24 rC)? Yes
Temperature °C by Temp blank
Temperature'C by Temp gum
No COC Incl.
,]1-01-
No NIA
;?. 9
5) Are there Dissoh ed samples for the lab to Alter? Yes No ✓
Who was rK Mled Date Time
Are there any RUSH or O lNanE ples? Yes No
Who was notified �-� Date Time
Permission to subcontract samples Yes No
7) Location where Samples are stored: r = (Walk-in clients only) If not already approved
Client Signature:
S) Do all samples have the proper Acid pH: Yee No NIA
9) Do all samples have the proper Bede pH: Yes No NIA ✓
10 Was the PC notified of any with the CoC vs the earn les: Yes NIA
Containers received at Con -Test
1 Liter Amber
SM mL Amber
# of
4 oz
2 oz
500 mL
250 mL
40 rnL Vial - tvi
77
40 mL vials: # M0 # Methanol
# Bisulfate # DI Water
Thbsuifete Unpreserve
1
X
and

Table of Contents
Page 2 of 2
Lain &Male Reee1,41 Ch"Mat
(Rejection Criteria Listing - Using Sample Acceptance Policy)
Any False statement will be brought to the attention of Client
Quest r uruefraj
T/FMA
1 The cooler's custody seal, If present, Is intact.
e GOM
2) The comer or samples do not appear to have
been compromised or tempered with.
3 Sam were received on Ice.
?'
q Cooler Tern2oture Is aweable,
T
5 Cooler Temperature is recorded_
2A wJh
6CDC Is NO out In Ink and Nible.
7 COC is filled out with all pertinent Information.
B Field SampWs name preseN on COC.
T
9) There are no discrepancies behmeen the
sam a IN on the contalner and the COC.
T'
10 Samples are received within Hoidin Time.
11 Sam a oontainers have leglIble labels.
Z'
12 Containers are rot broken or leakl .
18 At Cassettes are not broken/ n.
AJ
14).Sample collection daWtimes are pmIded.
15A e sample containers are used.
1 6 PropE collection media used.
17 No heWspooe sample bottles are oompletelyflIed.
r
18) There Is sutficlent volume for all requsted
anabMn, Including rewasted MS/MSDs.
I OLTrIp blanks provided if applicable,
20) VOA sample vista do not have head space or
bubble is c6mm (1/41 in diameter.
ri jig
21 Samples do not Mire itft or com i .
Doc 0277 Rev. 4 August 2013
Who notified of False etKernente7
Log -In Technician Initials: E5
DataMme:
Dawtime: 9 C 3 o M,
Page 14 of 14,

Allfilrnwksto
88 Spn= Street' EaM Longmmdaw. AAA 010291 FAX 41 9J62S4MW • TF3. 41&a2r
July 11, 2016
hay Sample
Catalina Su =04 LLC
200 Horizon Mve, suite 100
RAcigh, NC 27615
Project Location: 8ataer Quarry
Client Job )Number:
Pmjoa Number: [none]
Laboratory Work Order Number: 1600013
Enclosed are results of analyzes for samples received by the laboratory an June 30, 2016. If you have any questions concerning
this n park please feel free to contact me.
Smxrely,
4,� vo,"�
Use A. Wvrthingtan
Mampr
Table of Contents
Page 1 of 13

Table of Contents
Sample Summary
Case Narrative
Sample Results
1600013-01
1600013-02
Sample Preparation Information
QC Data
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
5152932
B153303
Flag/Cualiiier Summary
Certifications
Chain of Custody/Sample Receipt
Table of Contents
3
4
5
5
6
7
8
8
8
B
9
10
11
Page 2 of 13

Table of Contents
ikst
,m
N Spn" street - East Lanwmadm, MA Of 028 • FAX 413WS.84M • TEL. [phone].=
Grolma smmxdk LLC
200 AorlEm Drive, Salle 100 REPORT DATE: 711lrJO16
Raldah, NC 27615 PURCHASE ORDER NUMRK-
ATTN: Tcay Sampk
ANALYTICAL SLINWARV
WWORR ORDER NUNMM- 16MI3
The msWta of amdres pertarraod ea the fhllowits gmOcs fuEemlred tD the CON-TIESC Aaalylkal LAbaratary am fm m this er,Pmf.
YRiOIBcr LOCATION: But= Qu:ny
FLEA] SAWLE 0 LAD ID: MATRIX WOMB DESCRU'FLON TEBr SUB LAB
Bolt 7- Cmek cmui,,j I60wV-0I Water BUI-22 25M
POI -22 254OF
Buis W Trailer Park 16OW13-02 Wtror EPA 1664D
SM21 22 25401)
SW 1,22 2%OF
Page 3 of 13

All I I OtEsto
39 Sptuoe Street' East Longmeadow, MA OIOn' FAX 418ttiYB "OS "!EL 41BM26-,ZM
CABS NARRAME SUNWARY
All reported mmb art widiin defined 6bvse4y gosltty combo) objativm — U" below or otherwise gaddad in min report.
HW)9
t;mtple M= ved by Wmrnmy wM Jomffieicat time remaining to perftmm aa*m wiehlm the reommtmded halms time.
Asrayet & Sweplesp) QnaBMdr
Sdtltabla Bath
l tiOW13.01 (limn v_ tpeek Cromind 16=134nplin 10- Tftilc PC&)
The remulw of amalyaet reposed only mtaa w taarplm mbrmuod to the Caa-Tat Analytlaf iabmstory ibr testtos.
1 ccz f that dw natym listed sbova, unka rpoal8eally fisted es aboambacted, if ray, wan perfomaed corder nq direction a cw&sg to the approved methodologies HOW
in cols dommmst, and that bmW apm my Wqmy of hone individuals imma& oely rule fee obta>oSng Ow I fi zdm <be met ri l combed 4a Ada report * to do
Isms of my lnmwledge sad belief, acconsm nod compbde.
—7;@ k� i
Tod KerisclasH
Tabia of Canterlts
F'sge4of13

Table of Contents
co/ A i--tr
r
30 Spruce Steel' East Longmeadow, MA 01020 • FAX 41M/ O-0405 - TEL 413M25-2M
project L ohm Bamrr Qoany Sample Dcsaz*b-: Bark Onto 16M13
Date Received: 6rJQW16
Pldd Sucpb 0% Bate 7- [reek Cimdcg Samplod: WZ%2016 00:00
Sample M 16GN1341
Ssmpk Mehim %Wbm
C.oa.eadowd Cary Pwimtkn by 6PAlAPEAXW4W6 MOM& (TOW
Date DaldTmte
Aodne Rrialta RL DL Iladb DBotlom PhQ/Qrtd Mdbad PrgmW Ambztd A-"
sascabicSclldt DID 0.10 29JL 1 H-09 SMI-22254OF 71V16 71111616+45 DJM
Mal Stud Salldt 64 5.0 42 MJVL, I SMI-22 2540D WIG WNW 14:10 VAK
Page 5 of 13

"=R�r� Table of Contents
A OW
U Spnme &treed' Eae1 Lothar, MA 01020 • FAX 413lS 49%' TEL. 413MS-2332
PnJoa Locatkm: Hama Qmny Sale Dcxi# dm: Vlat Ordv: 16OW13
Dsh R=dve3: 613OW16
Pw 6iample k Hrdn 10- rmu r Putt S®pled: 6l2AQO16 OM
SomW@ IDs 16G OO13-C
SamnL Matrix: Wadr
CanrradmW Cb--I*ry Parmoun by EPA/AP11A/SW4W6 MdM& alld)
Dah
DxtwT me
Aadyae
Reml4 RL OL
unlfa
Deno" Fb & Qml Mediad Ptq—W
ApaWW. AnOW
Seak"SaUdr
m 0.10
MUL
1 H-0Y UM1-222MF ?An6
7/1/1616:45 DIM
TOW Sum=dcd Sdi&
72 6J 5.6
me/L
I DOI-222540D 71VId
7191616:1a VAK
011 & Grew (light)
ND IA 1-2
MA
I EPA 1664E 711I/16
WI U1612:45 LL
Page B of 13

Table of Contents
AIIII,con-,Nste
AMMAIL LABORATORY
39 Spruce Street' East Longrneulm, MA 01028 ' FAX /131&M-606' TEL. [phone]
Semple Bzfroctlen Data
IPA 16M
Lab NI Pud ml Babes IatLl IMLI bats
160"1342 [Bahr 106 nun" Puk] B153303 100D 07111/16
SM21.22 2540D
Lab Number I?W MI
Bald
into 1caL1
Do"
MGM 3A1 [Basin 7- Greelr CmWo11
B 152932
100
07AQ/16
16GOD] 3.02 [Basin 10- Tmiler Park]
B152932
75.0
07/00 6
RM1-222WF
La<b Number IFW MI
Batcb lattblIMLI
Data
16OW13-01 [Basta 7• [Seek CronhW B132216 low 07Ai/l6
16MO13-03 IBasio 10. 7tailcr Padr] B152111 1000 07/01/16
e7of19

Table of Contents
+4gALYT1 Lfi8
39 Spruce Sb*W • East Lorgmeadow, M4 01028 • FAX 41WO256WS • TEL. 411%252332
QUAL1lY COMMUL
Coovendmiti Cacmhfry Parawmtm by BPAMPEMAM8 f M iT&A1) - QuOty CoorM
RII-ft SPA SOW= %RBc RPD
wlyre Rmdr Limn Units LAM Resoh %RRC Limit RFD Lhnh Noce:
Savd BISZ932 - OM142 2516D
83m* (M§2932,N&l)
Prwpsrsd A Analymd: 07AW16
Tow Su - I I Salida
— ND 2-5 MA
LC8 (B1529324m)
—
Prepared &Aaayam& 0710SA6
^ w
Tatal Sid Safids
200 10 nwL
200 IOD 70.1-IJ6
Baaeh 8JMW - 6PA 1664B
Bleak (B1S330$41m)
- —
Prepsmd &A=bzed: 07/11/16
�_..._. - - --
oil or"" �
ND 1.4 men
US (B1S,3303-B31) _
Frq%ad & A®l�d: 09111n6
_ --- —
OR do (twat (IE"
22 WVL,
20.0Y..,._
M 70414
Page 8 of 13

. - - . 9 d � 9 1

Table a? Contents
AMVYMM YOW
S6 Spnm Sfte * EM LonWneadow. MA 01028 • FAX [phone]M ' TF1.. 413)SZ5• =
CZR77FICATION8
Caro d Anab m hadnded In thb Report
Am" CsrlOintlsaa
EPA J661B & NO*,
Oil R omar (HEM) Cf,L1AjMXY,RI.NC.WVA
SM.?I-1 2MOD OR Rrraer
Too Supeaded Sods C .MA.M.NYALNC,ME VA
The CDN•TEST 9vvImameotd Laboratory opetaaa Wlfa dm followlAB mama sad accteditetiwK:
Code
Detasiprioa
N=bcr
Evh"'
AIKA
AIHA.IAP, II.0
100033
MW2018
MA
Msuaehruetts DEP
M-MA100
OW300016
CI
Cow Drpm meW of PnbHk HtyWr
PH-OS67
0913W"17
NY
New Yor4Sbt OupathaentofHeath
10999NEIAP
04/it"17
NI"
New Hatt *o Envi wolow Lb
2316 NEI AP
02/S 17
RI
Rhode hlmd DgmrbnW of HaaleS
I.A000112
12/30f2016
NC
Nmlh Cnvlim Div. of WaW QW ty
652
12131/2016
N)
New Jersey DEP
MADD7 NEAP
06f3N2017
FL
FEarida Dspmmcat of Heath
E871027 NELAP
OWM017
VT
VammttDtmkucntofHeathI.esdLsbmtfmy
L1AIS036
07/3W2017
ME
State of Maine
2011028
06"17
VA
Casnmonweatb of Vinmia
460217
12/1402026
NH-P
Now Hampshire Pavb==eAW Lab
2557 NELAP
MOM
Page 10 of i3

CHAIN OF CUSMY RECORD 39 sawm Stmft
Add�_ :� -.7 �' �. Zv_ a w*,,to
O mx C paR cwmsfE
Fax A
Pr+*a Pro mal P-o dvdi (for bMnsourpmes1 Forret0 CMW CJom Oars
Q 1es _ pow. dBtt O Qmil
on O 321>,nee OM
can -rest lab l0 I Ctlent sample lD / Desufph4an
F
Pm___�_at_.1__
okmPow"
Of idd F1sEnea
otobw Arbr
"Moot o"
A• mAw lm
em9tasf
ST-sane
w vlal
om ntmcnn
Tbtedtsr bit
omothw
«gtmklcom
l•laed
M-HQ
M a lAothw led
PI.NRrIcAdd
S-SAUftAdd
S • 5odhan btcufhft'
x - "a toy* Ode
T . Na tMouffm
d a cfl
Aa'
b wummum
fenaerM�
Plesws �e trre foAowtde cads ea 1st Con`Taxt 4avw M a saedRc mw be
owo 1Ya er
w i�eaatle;r Itr 1Wtrhdlbrrf: t�ede sor
A i air
tf ^ M `lMedhMrS L -tow C-Chan; U - Ue*mmm
SL' dude&
AjAmpotwd 6r: wpoure)
MIMMMA
mmmimomm=a"
Caw
o
sow
Prvgrane
R
O
Sa-ow 0 X
0 WA o mocrpf rmdLmww
om"m
cwpc
0 $mum= o tw o mc
'U-Mrr'4&*
RED f i�
Q
0 MAP
* •� •ee���6� �IIfM�
•
Ma AC&AINACer"ied
7 Ol
r Le
E
[wtmw
prase s vary liiutts a �rrx srrC onr Faille s4efr� fa0Et7r1t711[i>t 7HAf! AttF On t otgl GNIIr1 pq M W CsfMnft WW'M CCWrMWM"
Tree 00CU MBfr
s rrese�oe>a�e a lror*4lE�anaorrtvscs�►aea�oomoeer.�w+wworsrwaviereaw�au�s ruar+�wea�:

as-
neatest
.M Mil Fast
LonQr»otdowOf028Nit
I
P:M94264M
APOALYTIGAL LARORATIORV
CUEMT
Pegs I of 2
Table of Contents
'N11;r�^hFihroy'�N V�YV+41117. +s,ipa�. �.
RECEIVED BY: �� DATE:/
1) Was the chains) of custody relinquished and signed? Yes V No No COC Ind.
2) Does the chain agree with the samples? Yea No
If not. explain:7
3) Are all the samples In good condition? Yes No
If not, explain:
4) Now the samples received: V
On !oe Dired from Sompflr4„ Amblerd . In Coolers)
Were the aerr-pies rscehrsd In Temperature Comoanoe of (24rQ? Yes V Na WA
Tempemkoe °C by Temp biank Temperature °C by Temp gun
8) Are there Dissolved samples for the lab to filter? Yea
Who was notated Date Time
8) Are time any RUSH or SHORT HOLDING TIME samples? Y*s
Who was no4ffled Date Time
Permission to subcontract samples? Yes No
7) Location where samples are stoned: � (� (,A) 1 V (Walk -In diertts o*) If not already approved
Clt m St mature:
8) Do all samples have the proper Acid pit: Yes No NIA
0 Do all samples have the proper Base H: Yes no MA V1
} P R Pef P
10) Was the PC nodfibu of anydiacre"ndes with the CaC vs the sue: Yes = _ MIA
No
No V
Containers received at Can -Test
# of containers
# of containers
t Liter Amber
16 of amber
6W mL Amber
8 or ambeNdear '
260 mi. Amber ft amber
4 oz iat !dew
1 Lber Plastic
2 az amber/dear r
ti00 mL tstic.
PiaC 1 oC
260 mL setts
SOC Kff
40 mL Via! - listed below
Parcliorste Kit
Cokisure 1 bWgft boft
Mae boa
Dissolved OxM bathe
Other
Encore
Other
40 mL vials: 0 HC1
# BliulfMe
�' ti :: -.' ' Thlosulfate
# Methanol
# DI Water
Unpreserved
Th 'sad Dab Pna=:
Page 12 of 13

Page 2 of 2
(Ra)eation Cdtwb L bdn8 - (using Semple Acceptance Pollay)
Any False statement will be brought to the attention of client
1) The cooler's custody seal, ff ent, Is Intact
2) The cooler or samples do not appear to have
Cooler Temwabrre Is
Is tied out In ink 41
Is filled out with all
e Feld Samplees name EEEM on COC. T
9) Thera are no discrepancies between~ the
ramnfw Ins en ftw enetut "and 1Ma r:nc:_
11 Sample contWnera tsarre labels. 1
12) Conishu n are not broken or Ieaklnn. I **MAT
16 Wple contemners are usd.
1S) Prover colbcdon medla used.
18) There Is scent volume for at♦ requsted f
sMbeg, Indud nested MS/MSDs. r} ,
I ?I Trip blanks provided it icable. rv�
20) VOA sample vials do riot have head space or /W
bubble is.<Smm (183 In dlameter.
21) Samples do not mulre aplitUna or cornDmItli a. 7-
Who noUMW of Fels nfa7
Doc 02" Rev. 4 August 2013 L cg4n Technician tnl Wb.- W-7
Table of Contents
mime: 7 I D �, I
D Q
Pape 13 of 13

39 Spruce Street' East Longmeadow, MA 01028 " FAX [phone]-S10li • TEL [phone]-=
Febnmry 15. 2016
Tony Sample
Carolina Sumock, LLC
200 Hodwn drive, Suite 100
Raleigh, NC 27615
Project Location: Quarry
Client Job Number.
project Number: [nariej
Laboratory Work Order Number:16BO432
Enclosed am results of andyaca for samples mcoived by the labmWwy on February 9, 2016. If you have any questions
conarnmg this report, please feel free to contact me.
Smceaoly,
40L, VOW�
Lisa A. Worthington
Project Manager
Table of Contents
Page

Table of Conts"
IAMUTOW
30 Bpruos 81 mW Fast LtutO MBftw. MA 010n' FAX 41&S25 440E ' TEL 413=5.2332
Carotirm Smuuck LLC
200 Hwimn Drive. Suitt 100
Ra1diA, NC 27615
ATTN: 'Eby S=W o
PURCHASE ORDER NUMBER:
PROJECTNUMBEW G—]
ANALYTICALBUNMURV
REPORT DAME: 211 &2016
WORK ORDER NRJMI3BR: 16E0432
Tho results of=Wym patavmea cm me following sunp1m wbmitted to the OOM-TEST AndydW tebmtwy sm amd to 6b repmt.
PROJECT LOCATION; Q-m
FIELD SAMPLE 0 LAB ID: MA3XM SAWLE DESGREMON TEST SUB LAB
Tmaer Park 1680432.01 Wttm EPA 190.1
smal-22 2540D
SM2142 2S40P
Crook Cloning 16BD432-02 Watu EPA 1664E
EPA 180.1
SM21,22 2540D
on].22 2540E
Page 3 of 13

Table of Conhwiffi
A TO
32 SWUa Street' Eaa1 LaV nwdow. MA 010211' FAX 413MM-6406' TEL. 413l525.2392
PMjaw Locatioms Qmery Semple Descripbn: %t Order. IC30432
Mete Recaiv &' MOM
INN goon a A: Tmftr Fork Sampled: 2ffiMI6 l6c26
Sample W. 16801R I
Sunni* TVae
Caartude al Ghazdary Paramrion 1y EPAMPRANW-41" Metbods OMD
Boo D"Ortold
Aaalyta
Resolb RL DL
Uotls Bola lmm V11411MINd
Mslbod Pr4-W AndyW Audyst
Settleable, $.lids
Alt) 0.10
MM 1
SM I-22 2%W 2110116 2110116 1430 DIM
Total m apaadnd S.tfds
42 S9 31
mg/L 1
Mal-22 2S40D 2/11/16 2A U1613:10 YAK
TleMdity
49 10
MTJ 20
EPA 190.1 7AW16 2/1Mf1615=25 DIM
Page 5 of 13

Table of Caalt4lnts
con4ao
awoirTlc�a mart
39 SWUM Shear' Eeaf Latpmsaday. MA 01020' FAX 41&W&6406 • TEL 412MV�2832
Sam[rte Fxbucdon Dab
ZPAl664B
Lab Flumbor [lldd ID[ Blab laltw (MI4 Date
16DO432-02 [Cm* CmubW B142133 Imo 02/13/16
EPA ISM
Lab Nei aw 1pkm mj
Sateh
hdtw [OIL]
17ad [mff4
nuts
16WU2.01 [r=UaPak]
B141269
23.0
234
02/10/36
16BO432.02 Pm* CM291P 4
B1418"
25A
15.0
0011N16
SM I-212S40D
Lab Ncmber pm ml Soft, Inuhl lmL[ Date
16BO432-01 [71aUaPads] B141%4 87.0 02/11/16
16804u-w (Ctoeh cmubi1 B141964 100 02/11/16
SM2142 2"W
Lab Nwnber P%M IN Bairb ladtlal [mL1 Date
I6BM32.OI frrWIaPadt] B141867 low 02Awld
16BO432A2 [Gust CmsdnS] U141867 loop MAW16
Page 7 of 13

Table of Contents
"U®
MMYnM MOMTORY
38 SPR= Street' EoW Largme low. MA01028' FAX [phone] * TEL 41316?&Z=
PLAQQUAL R4LR SUMMARY
'
QC mum is o-hids of arsabHehed Umiu
1
VxW mwvay hwu estabditbad for ddk uh aompo md.
j
Wide RPD thniu cMbUdW for diffimb CaVo®d.
d
ban exoeedsd clime reommmeoded or resuhtmy kvd
ND
Nol Dolled
RL
Rep uffus Limit
DL
Metbod D Limb
MQ
Mauo-m Cmtmaimma L.evet
Peromt recovaies smd relative pmuo di8'cmoea (RPDm) are dehmned by dw software ui" valoet in the
odvdmom wbd hm nd bum fo wiled.
No retails bare bean blank sabtrsdcd --tees specified fo the one oarratfve .
Page 9 of 10

Table of Contents
3e Spruce sc cci n -te s t East Lengmeadow, (4A 41428
P: 413-525.2332 ANI►1-YTS AL L1%M10nA-r0F:Y
F: 413.525-605 Page 1 of 2
ww„r.contesaabscam Sample Receipt Checklist
CLIENT NAME: Carolina Sunrock RECEIVED BY: RLF DATE: 2/0118
1) Was the chaln(s) of custody relinquished and signed? Yes A_ No No COC Incl.
2) Does the chain agree with the samples? Yes X No
If not, explain:
3) Are all the samples In good condition? Yes X No
If not, explain:
4) Now were the samples received:
On Ice X Direct from Sampling Ambient In Cooler(s) X
Were the samples received In Temperature Compliance of (2 -SIC)? Yes X No NIA
Temperature 1✓ by Temp blank
Temperature C by Temp gun
5) Are there Dissolved samples for the lab to filter?
Who was notified Date . Time
B) Are there any RUSH or SHORT HOLDING TIlIkE samples?
Who was notified Alex Date Time
Yes No X
Yes X No
3.5
Permission to suboontract samples? Yes No
7) Location where samples are stored: (Walk-in clients only) If not already approved
Client Signature:
8) Do all samples have the proper Acid pH: Yes No NIA X
9) Do all samples have the proper Base pH: Yes No NIA X
10) Was the PC notified of any discrepancies with the Coc vs the samples: Yes NIA X
Containers received at Con -Test
# of containers
'�' -
�;
# of containers
i Liter Amber
1
16 oz ember
500 mL Amber
8 oz ember/clear'ar
250 mL Amber 8oz amber
4 oz ember/dear ar
1 Liter Plastic
4
2 oz amber/clear jar
500 mL Plastic
Plastic Sag / ZI ioc
250 ml- plastic
2
SOC Kit
40 mL Vial - bpe listed below
Perchlorate Kit
Collsure / bacteria bottle
Ftwhpoint bottle
Dissolved Oxygen bottle
Other glass jar
Encore
Other'
40 mL vials: # HCI
# Methanol
ume ana osee Frozen:
Y:. ....
# Bisutfate
# DI Water
# Thlosulfate
Unpreserved
Page of 13

Co n wt sr
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ANAL.YTiCAL L.ABORATOW
http;Jlwww.mrlcetelaha-eere
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Company Name: �''i�lili`afG�wY[/i
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Project Proposal ProMed7 ffw bIWnE;purmsesl
O vas proposal date
Con -Test Lab ID Client Sample ID / Description
'1 t I -q--'! -n- _%_
CHAIN OF CUSTODY RECORD
1 r 1F,
mat CASof OExt:El _0M
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emang
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Compaulte
Grab
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Code
LL 114
&
39 spruce Street
East LonlpTradow. MA 01029
1
Dhsvlvcd Metals
0 FieW FUterad
0 Lab to Filter
_ fi
A=ambet Etas
G=glass
P--plank
ST=sterile
Y= uwl
S=summa can
Tptedtar bag
O*Ckher
'"pM4ntalli m
1 - Iced
H = HGL
M = Methmnal
N = Nitric Acid
S* SuffuricAcid
g: Sodium Iaisultate
X - Ala hydnudde
T - Na thlowHate
p ■ Quist
GW- groundwater
WW= wastewater
use the fadlerrinE codas to tat Con -Test know Ifa spedtic carrWla nary he hlgh OW. drtinirirzg Water
in concentraclon In datrbAom Code tiwe A a air
5 a soil/solid
d-F!
35 e-
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H - M - Aledlmo: L - taw; C -Clean; U - trnlarewn
u =sludge
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O =other_ —
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91
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OTHER
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DattJThna:
O '72-Hr r'4-pay
`
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.COD
0, 1 73 Sf
I t h Apprarat
WOE/DOE Certified
TURNAROUNDTi11ES (hus3neys days) SUM
AT WMAAL nM DAY AFM SAMWf MUM WRM6TWMM ARE OM YOUR CHAIN.
PLEAM BE CARERft NOT TO CONTAMINATE THIS DOCUM W
0TH15 FOM tS NOS FILLED GUT WIMLOOLY OR 15 btt DUCT, AMNARDINW Ttlin WNL MOT START UNTIL ALL WSn= AItB AbLtlltElM