WQ0000838_Modification_20200605

Initial Review
INITIAL REVIEW
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
Is this a complete
application?* Complete App Date
r Yes r No 06/05/2020
Project Number* WQ0000838
Applicant/Permittee Granville Farms, Inc
Applicant/Permittee PO Box 1396 Oxford, NC 27565
Address
Is the owner in BIMS?
r Yes r No
Owner Type Organization
Facility Name GFI RLAP
County
Fee Category
Major
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if
non -application)
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Is the facility in BIMS?
r Yes r No
Fee Amount
395

Admin Reviewer
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notification
Comments for Kendall
Comments for RO
Comments for Reviewer
Comments for Applicant

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
........................................................................................................................................................................................................................................................................................................................................................................
Name * Drew Matthews
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number WQ0000838
currently has project
ApplicantTermittee * Granville Farms, Inc.
Applicant/Permittee PO Box 1396 Oxford, NC 27565
Address*
Facility Name * GFI RLAP
Phone Number*
2528839301
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Paper copy is being mailed
Please attach all information required or requested for this submittal to be review here.
Application Formt Engineering Rans, Specifications, Calculations, Etc.)
GFI WQ0000838 Permit Mod May 2020.pdf 33.02MB
upload only 1 RJF document. NLltiple docurrents must be corrbined into one RJF file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper --polka*-ion is required,
be advised, applications accepted' far pre -review until both the paper and eIect-c-,i_ co1)ies nave been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments (calcs, soils report, specs, etc.)
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
MallinE address:
❑iuision of Water Resources1 Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center 1 Aft: Nathaniel Thornburg, 91° Floor, Cfice #942W
----------------------------------------------------------- -----------------------------------------
Raleih, NC 27699-1617 512 N. salisbury St.
Far questions or problems contact Tessa Monday [e-mail] or 919.707.3560.
* W By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
0- �
Submission Date 5/28/2020

GRANVILLE FARMS, INC.
PERMIT MODIFICATION
CLASS B PROGRAM
WQ0000838
Submitted by:
Soil Plus, LLC
PO Box 1396
Oxford, North Carolina 27565
May 28, 2020
SOIL PLUS

SOIL PLUS
May 28, 2020
NCDEQ-DWR
Non -Discharge Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Attention: Mr. Nathaniel Thornburg
Reference: PERMIT MODIFICATION
Granville Farms, Inc. Residual Biosolids "Class B" Program
Permit # WQ0000838
Mr. Thornburg:
Soil Plus, LLC (Soil Plus) is submitting one paper copy and one electronic copy of this
permit modification application package for Granville Farms, Inc. (WQ0000838). This
package includes:
1. Completed Residual Land Application Program Application
2. Completed Residual Source Certification Attachments
a. Hominy Creek WWTP (New)
b. Oxford WWTP (New)
This package is designed to add (2) new facilities. A check for $395 is enclosed with this
package per the Division of Water Resources Land Application Unit's fee schedule for a
major modification to a major non -discharge permit.
Soil Plus will be responsible for completing this permit application for Granville Farms,
Inc. If there is any further information required or questions regarding this permit
application, please do not hesitate to contact me for assistance.
Respectfully,
Drew Matthews, Soil Plus
Cc: Jason Smith, Granville Farms, Inc.
Andy Smith, Granville Farms, Inc.
PO Box 1396
Oxford, NC 27565
[phone]
dmatthewsgsoilplus. ne t
www.soilplus.net

Granville Farms, Inc.
Permit Modification
WQ0000838
Granville County, NC
Residual Land Application
Program Application
Weighted Source PAN Calculations
Revised O&M Plan
Residual Source Certification
Attachment
Hominy Creek WWTP
Field Loading Calculations
Analytical
Residual Source Certification
Attachment
Oxford WWTP
Field Loading Calculations
Analytical

APPENDIX 1
2020 PERMIT MODIFICATION
Granville Farms, Inc. (WQ0000838)
Residual Land Application Program Application
Weighted Source PAN Calculations
Revised O&M Plan

State of North Carolina
DWR
Department of Environment and Natural Resources
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM
FORM: RLAP 03-15
L APPLICANT INFORMATION:
1. Applicant's name: Granville Farms, Inc.
Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
❑ Federal ❑ State ❑ Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: Jason Smith
Applicant's mailing address: P.O. Box 1396
City: Oxford State: NC Zip: 27565-
Telephone number: [phone] Email Address:
2. Consultant's name: Drew Matthews License Number (for P.E.): _
Affiliation: ❑ On Staff ® Retained (Firm: Soil Plus, LLC)
Title: Vice President
Consultant's mailing address: P.O. Box 1396
City: Oxford State: NC
Zip: 27565-
Telephone number: [phone]
Email Address: dmatthewsksoilplus.net
3. Agronomist's name:
License Number:
Affiliation: ❑ N/A ❑ On Staff
❑ Retained (Firm: )
Agronomist's mailing address:
City: State:
Zip: -
Telephone number: (_) _-
Email Address:
4. Soil Scientist's name:
License Number:
Affiliation: ❑ N/A ❑ On Staff
❑ Retained (Firm: )
Soil Scientist's mailing address:
City: State:
Zip: -
Telephone number: (_) _-
Email Address:
5. Fee submitted: $395.00 (See Instruction B)
IL PERMIT INFORMATION:
1. Application is for (check all that apply):
❑ new, ® modified, ❑ renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00000838
Date of most -recently issued permit: 10/11/2016
Date of most -recently certified Attachment A (if different than the permit): 12/9/2019
Date of most -recently certified Attachment B (if different than the permit): 04/20/2018
FORM: RLAP 03-15 Page 1 of 5

III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. Residuals Processing Facility's physical address: NA
City: State: Zip: -.
Coordinates: Latitude: ° '
Datum:
ff Longitude: _°
Level of accuracy:
Method of measurement:
County where residuals land application program is headquartered:
1. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their
certification numbers, and their affiliations in the following table:
Designation
Name
Affiliation
Certification Number
ORC
Jason Smith
Granville Farms, Inc.
13266
Back -Up ORC
Bryan A. Smith
Granville Farms, Inc.
13265
Additional Back -Up
ORCs
if applicable)
If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide
the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training
school and certification test:
2. Complete the following tables regarding management of the residuals land application program:
a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals
source -generating facilities as currently certified and proposed for certification with this application and list the results in
the following table:
Maximum amount of residuals to be certified: 11,538 dry tons per year.
PAN
Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface
Incorporation
or Injection
Surface
Incorporation
or Injection
First -Year
36.41
51.17
420,103
590,444
Five -Year Maximum Adjusted
52.55
63.61
606,360
733,950
b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified
and proposed for certification with this application:
Category
Use
Acres
Comments
Crops
Forest or Plantation
Row Crops
Hay
2,199.91
Pasture
2,199.91
Total:
2,199.91
Methods
Surface
2,199.91
Incorporation or Injection
0
Total:
2,199.91
FORM: RLAP 03-15 Page 2 of 5

c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently
certified and proposed for certification assuming the scenarios listed in the following table:
Assumed
Application Rate
(lbs PAN/ac yr)
Acres Required Using
First -Year PAN Concentrations
Acres Required Using
Five -Year Maximum Adjusted PAN
Concentrations
Surface
Incorporation or
Injection
Surface
Incorporation or
Injection
50
8,402.06
11,808.87
12,127.21
14,679.01
100
4,201.03
5,904.44
6,063.60
7,339.50
150
2,800.69
3,936.29
4,042.40
4,893.00
200
2,100.51
2,952.22
3,031.80
3,669.75
6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed
residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector
reduction practices not in place, etc.): Many of these sources will also maintain their current land application program in
conjunction with this one. Basicallv for most sources this Dennit will not serve as an exclusive land aDDlication Droaram_ but
rather as a supplement
7. Specify type of residuals program (See Instruction F): ® Non -dedicated ❑ Dedicated
If Dedicated, specify the following (check all that apply):
❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than
agronomic rates, explain;
❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop
production is of secondary importance, explain;
❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or
irrigation facilities fed through a fixed supply system, explain; -M
IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the following Residuals Source Certification and all associated documentation.
Residuals Source
Certification
V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site)
Complete and submit the following Land Applications Site Certification and all associated documentation.
Land Application Site
Certification. doc
FORM: RLAP 03-15 Page 3 of 5

Applicant's Certification (signing authority must be in compliance with 1.5A NCAC 02T .0106):
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without
proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with
any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
Yes IN No, Explain;
I, Jason Smith Vice President
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for Granville Farms, Inc.
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water
Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes
unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate
enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the
Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this
application are not completed and that if all required supporting information and attachments are not included, this application
package will be returned to me as incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any
false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine
not to exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature: JC9<9 (r<. Date:
FORM: RLAP 03-15 Page 4 of 5

Source
Dry Ton
Avg
%Solids
Weighted Avg
tat Y,.PAN(Su)
Weighted Avg.
lba/Dt
tat Yt PAN(Inj)
Weighted Avg
lba/Dt
SthY PAN(S-&-)
Weighted Avg
lba/DT
Sth Yt PAN(Inj)
Weighted Avg
lba/DT
Amherst Subdiwlslon V WPP
10.00
0.09%
0.09%
0.26%
0.09%
0.09%
0.09%
0.09°/n
0.26%
0.26%
0.65%
0.09%
0.09%
0.17/n
0.09%
0.09%
0.35%
0.09%
0.09%
0.43%
0.87%
0.87%
2.76%
0.35%
0.43%
0.69%
13.87/
17.33°/n
0.87/n
2.76%
1.73%
0.09%
0.09%
0.13%
0.09%
0.09%
0.17%
1.30%
0.13%
6.85%
0.17%
1.30%
0.13%
8.67%
4.33%
0.09%
0.17%
0.09%
0.09%
2.76%
5.63%
0.13%
2.76%
6.93°/n
2.76°/n
0.65%
2.76%
1.73%
0.43%
2.76%
0.09%
0.09%
0.13%
0.13%
0.09%
0.22%
1.79%
2.04 %
1.34 %
1.91%
0.57%
2.15%
1.21%
1.36%
1.50%
1.71%
5.19%
2.50%
0.59%
1.85%
0.49%
1.29%
1.77%
2.08%
1.13%
1.80 %
2.121
3.26%
0.59%
1.83%
1.39%
5.37%
26.10%
2.16%
2.03%
0.85%
1.73%
1.04%
1.13%
4.01%
2.77%
0.64%
2.03%
1.79%
2.40 %
0.81 %
2.11 %
1.50 %
3.67%
3.56%
0.20 %
1.79%
1.44%
1.44%
3.28%
3.03%
0.47%
3.00%
1.20%
5.40 %
1.40 %
2.37%
7.40 %
3.32%
5.43%
2.07%
1.46%
1.75%
2.35%
1.95%
1.95%
2.89%
0.002%
0.002%
0.003°/n
0.002%
0.000%
0.002%
0.001%
0.004%
0.004°/n
0.011%
0.004°/n
0.002%
0.001%
0.002%
0.00M
0.004%
0.002%
0.002%
0.005%
0.016%
0.018%
0.090%
0.002%
0.008%
0.010°/
0.745%
4.524%
0.019°/
0.056%
0.015%.
0.001%
0.001%
0.001%
0.003%
0.002%
0.001%
0.026%
0.002%
0.164%
0.001%
0.027%
0.002%
0.318%
0.154%
0.000%
0.003%
0.001%
0.001%
0.091%
0.171%
0.001%
0.083%
0.083%
0.149%
0.009%
0.066%
0.128°/
0.014°/n
0.150%
0.002%
0.001%
0.002%
0.003%
0.002%
0.004%
7.23%
19,455
18,314
19,382
17,634
21,070
15,262
24,374
14,003
20,507
2,039
5,146
10,304
45,353
17,994
14,096
9,939
18,249
17,417
1,006
9,221
19,718
8,015
22,214
12,168
13,788
33,805
4,249
19,055
13,676
1,870
17,039
21,918
20,009
10,211
7,065
49,435
14,725
17,492
26,535
20,670
3,422
67,377
27,028
20,668
17,890
13,408
22,259
22,259
508
6,180
2,527
237
52,946
120
26,133
3,758
23,316
14,407
16,308
17,483
46,754
17,198
10,027
16,305
21,291
16.86
15.87
50.40
15.28
18.26
13.23
21.12
36.41
53.32
13.25
4.46
8.93
78.62
15.60
12.22
34.46
15.82
15.10
4.36
79.92
170.90
221.60
77.01
52.73
95.60
4,687.81
736.52
165.15
378.11
32.41
14.77
19.00
26.01
8.85
6.12
85.69
191.43
22.74
1,816.84
35.83
44.49
87.59
2,342.52
895.65
15.51
23.24
19.29
19.29
14.05
348.15
3.29
6.55
3,671.07
3.32
169.87
103.90
404.16
62.43
450.88
15.15
40.52
22.36
13.04
14.13
46.13
18,205.18
0.03
0.03
0.10
0.03
0.04
0.03
0.04
0.07
0.11
0.03
0.01
0.02
0.16
0.03
0.02
0.07
0.03
0.03
0.01
0.16
0.34
0.44
0.15
0.11
0.19
9.38
1.47
0.33
0.76
0.06
0.03
0.04
0.05
0.02
0.01
0.17
0.38
0.05
3.63
0.07
0.09
0.18
4.69
1.79
0.03
0.05
0.04
0.04
0.03
0.70
0.01
0.01
7.34
0.01
0.34
0.21
0.81
0.12
0.90
0.03
0.08
0.04
0.03
0.03
0.09
M 41
420,103
20,801
22,824
20,877
24,519
21,947
17,207
26,994
14,997
25,807
2,560
5,306
12,864
45,761
18,669
14,351
10,466
22,484
20,398
1,127
9,499
19,737
10,410
25,799
12,913
14,356
45,105
7,199
22,525
15,466
2,570
17,276
22,107
26,734
12,316
8,375
50,216
16,940
23,163
30,270
27,420
6,313
69,020
38,477
27,468
17,944
14,358
23,182
23,182
710
6,481
3,782
409
96,612
203
34,333
4,534
30,616
17,797
20,353
29,383
56,103
19,320
11,242
18,145
27,470
18.03
19.78
54.28
21.25
19.02
14.91
23.40
38.99
67.10
16.64
4.60
11.15
79.32
16.18
12.44
36.28
19.49
17.68
4.88
82.33
171.06
287.81
89.44
55.96
99.54
6,254.81
1,247.88
195.22
427.60
44.55
14.97
19.16
34.76
10.67
7.26
87.04
220.23
30.11
2,072.57
47.53
82.07
89.73
3,334.81
1,190.33
15.55
24.89
20.09
20.09
19.63
365.11
4.92
11.31
6,698.70
5.61
223.17
125.36
530.70
77.12
562.72
25.47
48.62
25.12
14.62
15.73
59.52
25,586.91
0.04
0.04
0.11
0.04
0.04
0.03
0.05
0.08
0.13
0.03
0.01
0.02
0.16
0.03
0.02
0.07
0.04
0.04
0.01
0.16
0.34
0.58
0.18
0.11
0.20
12.51
2.50
0.39
0.86
0.09
0.03
0.04
0.07
0.02
0.01
0.17
0.44
0.06
4.15
0.10
0.16
0.18
6.67
2.38
0.03
0.05
0.04
0.04
0.04
0.73
0.01
0.02
13.40
0.01
0.45
0.25
1.06
0.15
1.13
0.05
0.10
0.05
0.03
0.03
0.12
51.17
590,444
30,669
27,346
30,500
25,413
29,466
23,123
37,406
21,661
30,433
3,034
8,095
15,271
53,834
28,524
22,379
14,903
27,272
26,850
1,006
13,309
28,723
11,744
32,868
17,428
21,257
50,227
5,655
28,797
18,959
1,870
27,184
34,192
28,960
15,408
10,549
77,382
22,724
25,573
40,967
29,713
4,078
106,711
39,275
30,639
28,611
20,656
24,645
24,645
508
9,506
3,432
237
69,757
120
38,893
5,712
34,793
21,639
23,848
23,485
71,040
26,792
15,267
25,455
31,520
26.58
23.70
79.30
22.03
25.54
20.04
32.42
56.32
79.13
19.72
7.02
13.24
93.32
24.72
19.40
51.67
23.64
23.27
4.36
115.35
248.94
324.70
113.95
75.52
147.39
6,965.09
980.24
249.58
524.17
32.41
23.56
29.63
37.65
13.35
9.14
134.13
295.42
33.25
2,804.99
51.50
53.02
138.73
3,403.97
1,327.74
24.80
35.81
21.36
21.36
14.05
535.53
4.46
6.55
4,836.68
3.32
252.81
157.92
603.10
93.77
659.34
20.35
61.57
34.83
19.85
22.06
68.30
26,276.67
0.05
0.05
0.16
0.04
0.05
0.04
0.06
0.11
0.16
0.04
0.01
0.03
0.19
0.05
0.04
0.10
0.05
0.05
0.01
0.23
0.50
0.65
0.23
0.15
0.29
13.93
1.96
0.50
1.05
0.06
0.05
0.06
0.08
0.03
0.02
0.27
0.59
0.07
5.61
0.10
0.11
0.28
6.81
2.66
0.05
0.07
0.04
0.04
0.03
1.07
0.01
0.01
9.67
0.01
0.51
0.32
1.21
0.19
1.32
0.04
0.12
0.07
0.04
0.04
0.14
52.55
606,360
31,669
30,695
31,610
30,526
30,117
24,568
39,352
22,399
34,369
3,421
8,213
17,172
54,137
29,025
22,568
15,295
30,417
29,063
1,127
13,515
28,737
13,522
35,530
17,981
21,679
58,618
8,083
31,374
20,289
2,570
27,360
34,333
33,954
16,971
11,522
77,962
24,369
29,784
43,741
34,726
6,225
107,931
47,777
35,688
28,652
21,361
25,331
25,331
710
9,729
4,363
409
102,182
203
44,982
6,288
40,213
24,156
26,852
32,322
77,982
28,368
16,169
26,821
36,108
27.45
26.60
82.19
26.46
26.10
21.29
34.11
58.24
89.36
22.24
7.12
14.88
93.84
25.16
19.56
53.02
26.36
25.19
4.88
117.13
249.06
373.85
123.18
77.92
150.31
8,128.69
1,401.11
271.92
560.95
44.55
23.71
29.76
44.14
14.71
9.99
135.14
316.81
38.72
2,994.92
60.19
80.93
140.32
4,140.84
1,546.54
24.83
37.03
21.95
21.95
19.63
548.09
5.67
11.31
7,084.90
5.61
292.39
173.85
697.05
104.68
742.40
28.01
67.59
36.88
21.02
23.25
78.24
31,805.79
0.05
0.05
0.16
0.05
0.05
0.04
0.07
0.12
0.18
0.04
0.01
0.03
0.19
0.05
0.04
0.11
0.05
0.05
0.01
0.23
0.50
0.75
0.25
0.16
0.30
16.26
2.80
0.54
1.12
0.09
0.05
0.06
0.09
0.03
0.02
0.27
0.63
0.08
5.99
0.12
0.16
0.28
8.28
3.09
0.05
0.07
0.04
0.04
0.04
1.10
0.01
0.02
14.17
0.01
0.58
0.35
1.39
0.21
1.48
0.06
0.14
0.07
0.04
0.05
0.16
63.61
733,950
Arbor Hills XIHP
10.00
Asbky Hills W WTP
30.00
Avocet WWTP
10.00
Barclay Downs WWTP
10.00
Beachwood WWTP
10.00
Birchwood RV Pads
10.00
Bear Chapel Development
30.00
Bnanvood Farms WWTP
30.00
Carolina Meadows WWIP
75.00
Chapd Ridge
10.00
Cole Pads Plaza WWFP
10.00
Consolidated Dme d WWFP
20.00
Colvard Farms
10.00
Cottonwood/Ba3wood
10.00
Crooked Creek WWPP
40.00
Cross Creek Mobile Estates
10.00
Deerchase WWFP
10.00
Enfield WPP
50.00
Enfield W WPP
100.00
Fearnn n Utility W WTP
100.00
Franklin County W WTP
319.00
Govemoi s Club V WPP
40.00
Hasentree Golf Community
50.00
Hawthorne Subdiwision V WPP
80.00
Henderson WRF
1,600.00
Hominy Creek WRF
2,000.00
Johnston County WWPP
100.00
Kehly Re i-d V WPP
319.00
Kerr Lake Regional WFP
200.00
Kings Grant Subdivision W WPP
10.00
Kittrell Job Corp Center
10.00
Knlght,Wl XIHP WWFP
15.00
Lake Ridge WWPP
10.00
Lake Royale
10.00
Legacy atj-d-Lake
20.00
Little Creek W WPP
150.00
Mallard Crossing WWPP
15.00
ll.Umd rodt W WFP
790.00
Nature Trails XIHP V WPP
20.00
Nevse Colony V WPP
150.00
Nevse River Village V WPP
15.00
Nevse River V WPP
1,000.00
Oxford WWPP
500.00
P e Industrial Park
10.00
Preserve at Jordan Lake
20.00
River NIM WWPP
10.00
Rockbndge
10.00
SGWASA WFP
319.00
SGWASA WWFP
650.00
Shearon Hares NPP
15.00
SvnsetWPP
319.00
Tar River Regional W;TP
800.00
Tar River WPP
319.00
T- of Bunn W ;TP
75.00
T-of LouisburgW ;TP
319.00
Town of Pittsbom W WLP
200.00
Town of Spring Hope WWPP
50.00
Town of Waaenton WWFP
31200
Tradewinds WWFP
10.00
WestOVV)PP
10.00
Wlvppoorwill Valley V WPP
15.00
Wddwood Goren WWFP
15.00
Willowbrook WWFP
10.00
Woodlake Country ClW vb WPP
25.001
11,538.00
PAN Rate Acres Requited Acres Requited Ates Required A- Requited
50 8,402.06 11,808.87 12,127.21 14,679.01
100 4,201.03 5,904.44 6,063.60 7,339.50
150 2,800.69 3,936.29 4,042.40 4,893.00
200 2,100.51 2,952.22 3,031.80 3,669.75

GRANVILLE FARMS, INC.
OPERATION AND MAINTENANCE PLAN
LAND APPLICATION OF CLASS B RESIDUAL BIOSIOLIDS
WQ#0000838
Revised May 2020

1.0 SUMMARY
Granville Farms, Inc. (GFI) is a privately owned company that is contracted to haul and land apply nutrient enriched
by-products such as Biosolids from Wastewater Treatment Plants, Residuals from Water Treatment Plants, Animal
Waste from Animal Production Facilities, and certain Construction Debris from Road Work (i.e. slurry water from
diamond cutting of concrete). GFI is unique in that it does not participate in the generation or treatment of the by-
products generated by any of the source types listed above. At times GFI is requested to provide lime stabilization
of Biosolids by smaller operating facilities, but this quantity is normally very small. GFI's main role is to provide
transportation and operational equipment to spread the nutrient enriched by-products listed above.
Another unique characteristic about GFI is that it owns and maintains permits to land apply these by-products. Given
that most generators are issued their own land application permit, they have direct oversight of the preparation,
removal, and application of their by-products. This creates some operational and permit challenges for GFI since
standard, state issued permits are typically issued to generators not land application companies. This Operation and
Maintenance Plan (O&M) addresses how GFI is able to manage by-products produced by multiple, independent
generators and land applies under their own land application permit.
Revised 06/19 OGranville Farms, Inc. Operation and Maintenance Plan

GRANVILLE FARMS O&M PLAN
SAMPLING & ANALYTICAL

2.0 ANALYTICAL REQUIREMENTS
Prior to the hauling and land application event being schedule the generator must provide analytical results
documenting that all parameters listed in Condition IV. 2 — 4 and at the frequency listed in most recent copy of this
permit. If GFI does not collect the sample then it DOES NOT own the responsibility of the integrity of the sample
and the method it was collected, transported, submitted, and analyzed. Should the generating source elect to have
GFI collect the sample prior to land application, then it will be done in the following manner:
Four factors that may ultimately affect the integrity of reported data include: 1) obtaining a representative sample, 2)
preventing contamination of the sample, 3) providing legal documentation of the sampling event, and 4) protecting
the sample from chemical, physical or biological change prior to analysis.
A sample will be collected according to the schedule provided in the most recent copy of the Attachment of this
permit and prior to land application one composite sample should be pulled from a designated location from the
generating source. GFI has identified Meritech, Inc based in Reidsville, NC to be used as the Certified Laboratory.
The composite sample should be analyzed for:
• % Solids,
• Nitrogen Series (TKN, Ammonia, Nitrate, Nitrite, and Organic Nitrogen),
• Phosphorus,
• Potassium,
• Sulfur,
• Calcium,
• Magnesium,
• Sodium,
• Iron,
• Aluminum,
• Manganese,
• Copper,
• Zinc,
• and Remaining 503 Metals (i.e. Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel,
Selenium)
Approximately 2 quarts of residual should be collected. The sample containers should be clean and sterile. They
should also be labeled so that they are easily identifiable in the lab. The samples should be pulled using the method
listed below:
❖ Collect one sample from each digester(s) from which the material will be land applied using a "swing sampler"
o The swing sampler must be used with a sterile, plastic 960 ml container
❖ Combine each sample in a stainless steel bucket
❖ Mix thoroughly using a fiberglass rod
❖ Collect each sample from the top of the access point at each digester. This access point is obtained by climbing
the installed ladder on the side of the digester.
Revised 06/19 OGranville Farms, Inc. Operation and Maintenance Plan

Once the sample is pulled, it should be placed in medium size cooler packed with ice. The sample should be collected
with an enough time so that it can be delivered to the laboratory.
Once per calendar year a sample should be collected and analyzed for:
• Full TCLP
• Ignitability, Corrosivity, and Reactivity
• Requires 5 Liters
A third should be submitted for a 30-Day Scale Bench test and Fecal Coliform Density Test. The 30-Day Scale Bench
Test also requires 1 quart of "clear" water from the Clarifier for Dilution if necessary. This sample would be analyzed
for:
• 30-Day Scale Bench Test (4 Quarts of Residuals and 1 Quart of Clarifier water)
• Fecal Coliform Density Test (seven samples)
The contact information for the lab is:
Mailing Address
Meritech, Inc.
642 Tamco Rd
Reidsville, NC 27320
[phone] (Phone)
Sampling frequency will be conducted in accordance with the Table listed in the most recent Attachment A of this
permit. The sample will be collected by a representative of Soil Plus, LLC. For further information please contact:
Drew Matthews
P.O. Box 1396
Oxford, NC 27565
252-883-9301
Revised 06/19 OGranville Farms, Inc. Operation and Maintenance Plan

GRANVILLE FARMS O&M PLAN
OPERATION, SPILL CONTROLL, & TRAINING

3.0 BIOSOLIDS REMOVAL, TRANSPORT, AND APPLICATION
Biosolids will be transported from the generators to suitable, permitted land application sites. Transport equipment
will be inspected, licensed and appropriately marked, as required, for the purpose of transporting biosolids. Biosolids
will be delivered to the application sites between sunrise to sunset.
Both liquid and dewatered biosolids distribution on the land application sites will be uniform throughout the
application area. To ensure adequate control of the application rate for each site, the equipment used for spreading
the sludge will be calibrated by measuring the amount handled on a known square footage. While the rate of discharge
from the application vehicle is fixed, the speed of the equipment can be adjusted to maintain the flow rate needed to
achieve specific application rates. Spreading operations will be discontinued during periods of inclement weather and
will not be resumed until sufficient drying of the fields has occurred. This allows equipment access without causing
excessive soil compaction or rutting. To prevent adherence of the biosolids, transport vehicles will be equipped with
rear mud flaps, thereby preventing biosolids from being tracked onto roadways. Biosolids adhering to the mud flap
will be scraped off in the field before the truck returns to the roadway. Examples of our application tracking and
summary form/reports can be provided upon request.
4.0 SITE OPERATION
Biosolids will be surface applied at the properly -calculated agronomic rate and in strict accordance with any state and
federal regulations for the land application of the biosolids. Buffer zone distances will be observed in accordance with
applicable state and federal regulations. Buffer zones will be flagged and no biosolids will be applied within those
areas. The most restrictive buffer will apply in combined situations. Operational provisions will be taken to prevent
soil loss through erosion. Provisions will include contour application and avoidance of areas where surface drainage
patterns result in concentrated flow of runoff from rainfall. In accordance with sound, industry standard agronomic
practice, areas which are unseasonably wet (and would produce rutting or damage to the field) will not be utilized for
biosolids application operations during those periods. Operations will be discontinued when soils are saturated and
will not be resumed until the field has sufficient dried. The amount of biosolids applied will not exceed the hydraulic
capacity of the soil at the time of each application. If a subsequent pass across a field is necessary to achieve the
desired application rate, sufficient drying time will be allowed between passes.
5.0 PROJECT CONTROL
To ensure biosolids are continuously applied at the correct application rate and in a manner consistent with the
Operations Plan, a GFI Project/Field Manager will be in direct charge of the field operations, controlling the amount
of biosolids delivered to each field, and conducting daily field inspections. Field inspections will include ensuring that
flags are in place, biosolids are applied uniformly at the designated application rate, setbacks are observed, trucks are
unloading at best location, trucks are not driving over biosolids, trucks are cleaned before leaving the field and the
land application equipment is maintained in working condition.
6.0 TRANSPORTATION SYSTEM ROUTING
Per the specifications, GFI transportation vehicles will be equipped with GPS devices that will guide drivers to the
land application sites. Transportation routes will follow primary highways and avoid residential areas where possible.
Designated routes are followed unless a detour is specified. In the event of a detour route, it shall be taken as specified
by the detour authority. There shall be no unscheduled stops when loaded. Transportation vehicles will be inspected,
licensed and appropriately marked as required with identification numbers for the purpose of this contract. All units
will be equipped with spill guards and full mud flaps. This will prevent the biosolids from adhering to the tires and
undercarriage of the transport vehicle, thereby preventing biosolids from being tracked onto roadways. Biosolids
adhering to the mud flap will be scraped off in the field before the truck returns to the roadway. All federal OSHA
Revised 06/19 OGranville Farms, Inc. Operation and Maintenance Plan

and DOT laws and regulations are complied with for the protection of our clients, the community and our drivers.
Examples of vehicle and driver transportation logs and inspection forms can be provided upon request.
7.0 DEWATERED BIOSOLIDS
Dewatered biosolids will be transported in standard end dump trailers. The dump trailers will be loaded per the
generator's specifications and standard protocols. The dump trailers used for transportation of dewatered cake
biosolids will be equipped with sealed tailgates and will be completely sealed to prevent leakage. All trucks will be fully
covered and will be fitted with positive lock tailgates.
8.0 LIQUID BIOSOLIDS
Liquid biosolids will be transported using liquid tankers that will be pulled by standard road tractors. The tankers
will be loaded per the generator's specifications and standard protocols. The tractor/tanker unit will transport its
load to a designated staging area inside the buffered area of a permitted land application site.
9.0 APPLICATION (SPREADING) — DEWATERED BIOSOLIDS
At the staging area each load will be unloaded in a designated area within the land application site. Biosolids will be
loaded into our Side Slinger cake box by a GFI employee using a front-end loader. This unit is capable of delivering
an accurate, calibrated application of dewatered biosolids over the application site. The uniform spread pattern ensures
that biosolids are applied at proper agronomic (nutrient) and hydraulic loading rates. The application rates for each
site, and its corresponding crop, will be determined based on the Plant Available Nitrogen (PAN) content of the
biosolids, or other limiting factors. Typical applications will deliver between 75 and 100 percent of a crop's annual
PAN requirement.
10.0 APPLICATION (SPREADING) — LIQUID BIOSOLIDS
At the staging area each load will be transferred into a 4,000-gallon capacity pull behind or TerraGator for subsequent
land application. This unit is capable of delivering an accurate, calibrated application of liquid biosolids over the
application site. The uniform spread pattern ensures that biosolids are applied at proper agronomic (nutrient) and
hydraulic loading rates. The application rates for each site, and its corresponding crop, will be determined based on
the Plant Available Nitrogen (PAN) content of the biosolids, or other limiting factors. Typical applications will deliver
between 75 and 100 percent of a crop's annual PAN requirement.
11.0 SPILL AND EMERGENCY RESPONSE PROGRAM
In the unlikely event of a spill, GFI will take the following actions immediately.
• Halt Source of Spill. Use of any leaking or damaged unit which is causing the spill will cease immediately. The
unit will be repaired before resuming its use.
• Contain Spill. In the event large quantities of biosolids have been spilled, straw bales will be used where
available and as necessary to either form a barrier or absorb biosolids.
• Clean -Up. Depending on the type and amount of biosolids spilled, a variety of equipment may be used to
remove the biosolids: front-end loader, shovels and brooms and vacuum equipment of a liquid biosolids
applicator. Any biosolids removed from the spill site will be spread on an approved application site, returned
to the WWTP, or disposed of in an approved landfill.
• Final Clean -Up. Flush roadways with water or sweep as necessary to clean. Allow to dry and incorporate if
spill occurs on non -paved and tillable area. In the event a spill occurs on private property, final clean-up
should be completed immediately to the satisfaction of the owner.
Revised 06/19 OGranville Farms, Inc. Operation and Maintenance Plan

• Management of Clean -Up Efforts. The Operations Manager will take immediate charge and initiate clean-up
activities. GFI labor will be used, with additional labor secured as needed. The Operations Manager will also
communicate with the public on the scene, answering questions and advising of clean-up activities.
• Reporting. All spills will be reported immediately to GFI offices and the client. State and local agencies will
be notified in accordance with their notification requirements. Within 24 hours of the spill, the Operations
Manager will send GFI office a written report detailing how the spill occurred and remedial action taken. This
report will be provided using the enclosed Spill Report form.
• Spill Prevention. The Operations Manager will implement the following spill prevention measures:
o Ensure truck drivers watch trailer while loading and do not overload;
o Ensure trailer hatches are closed and latched while transporting;
o Ensure trailer seals are inspected on a daily basis and replaced as necessary; and
o Ensure unloading operations in the field are conducted to minimize any potential runoff or tracking.
All employees receive safety and spill response training as part to their new hire training and thereafter participate in
our monthly safety and spill response training program. In addition to our internal training and protocols, we also
contract with a regional emergency response firm - HEPACO - available to respond to an incident in the Central and
Eastern North Carolina area within two hours. A copy of our agreement with HEPACO can be provided upon
request.
Names and Titles of Inspection Personnel
Andy Smith, Area Supervisor
Jason Smith, Area Supervisor
JT Bryant, Regional Supervisor
Jay Bryant, Project Supervisor
Matt Foster Project Supervisor
BJ Bryant, Field operators
Jeff Bumpass, Field operators
Tammy Walston, Field operators
12.0 PREVENTION
The goal of a compliance assurance system is to prevent compliance issues from occurring. Prevention involves:
• Ensuring personnel understand their role in assuring compliance;
• Identifying compliance requirements at the federal, state and local levels;
• Implementing a system where compliance tasks are scheduled, assigned and tracked to completion;
• Developing standard operating procedures where appropriate; and
• Reviewing the compliance task list and standard operating procedures on an ongoing basis and modifying
them as appropriate to account for changes in regulations/requirements and operating methods, and to
address compliance deficiencies.
GFI ensures employees understand their role in assuring compliance through new employee orientation programs
and on the job training.
Revised 06/19 OGranville Farms, Inc. Operation and Maintenance Plan

13.0 Standard Operating Procedures (SOP's)
GFI develops and implements SOPS to ensure compliance tasks are completed consistently across the company.
The SOP provides standard forms to use, approved biosolids analytical methods, frequency of monitoring
information, etc. Another key SOP relative to preventing compliance issues from occurring is the use of a "Pre -
Operating and Buffer Checklist".
The Pre -Operating and Buffer Checklist ensures federal, state and local regulations and permit requirements are met
prior to initiating biosolids applications at field sites. Compliance items on the Checklist include:
• The field is permitted and suitable for the biosolids/residuals type being applied;
• Pre -application requirements are met;
• Farmer and landowner agreements are current and the crop to be grown has been verified;
• The field is flagged to prevent applications in buffer zones and restricted areas;
• The appropriate application rate and field capacity is calculated; and
• Any special permit or local requirements are met.
• A listing of the buffer zones and restricted areas where biosolids/residuals cannot be applied
• A listing of operating requirements including notification requirements,
• application method requirements, and inclement weather operating requirements
14.0 ASSESMENT
To help ensure compliance requirements are being met and the compliance assurance system is implemented and
working, periodic, consistent, objective and documented assessments of a project/facility's compliance status are
conducted. GFI personnel have clearly -defined compliance assessment responsibilities and time to conduct such
assessments. GFI conducts informal site inspections and formal audits on an ongoing basis.
15.0 CORRECTIVE ACTION
Once compliance issues have been identified during the course of day to day business and through internal audits and
inspections a system must be in place which ensures that appropriate and timely corrective action is taken, the cause
of the compliance issue is identified and actions are taken to prevent recurrence of the issue.
GFI's goal is to have no instances of non-compliance. However, issues and incidents may occur and when this
happens employees work to correct the incident in a timely and thorough manner. When compliance issues are
identified, the situation is examined to determine the root cause of the problem and the corrective and preventive
action that must be taken. The preventive action must address the root cause with the goal of preventing a recurrence.
Depending on the nature of the compliance issue, it is assigned to one or more responsible parties to ensure that the
corrective and preventive actions are implemented. A deadline for completion of the task is assigned and the issue is
tracked to completion by regional and corporate compliance personnel.
Revised 06/19 OGranville Farms, Inc. Operation and Maintenance Plan

16.0 TRAINING
An effective compliance training program involves:
• Identifying training needs and requirements;
• Assigning personnel to provide training and providing them the resources they need to conduct training;
• Documenting and tracking that mandatory t raining has occurred; and
• An employee's training needs and requirements, as well as their training responsibilities, are based on
his/her position within the company.
Revised 06/19 OGranville Farms, Inc. Operation and Maintenance Plan

GRANVILLE FARMS O&M PLAN
PROCESS FLOW DIAGRAM

GRANVILLE FARMS CLASS B SOURCES (WWTP)
Amherst Subdivision
Knightdale MHP
Arbor Hills MHP
Lake Ridge
Avocet
Lake Royale
Ashley Hills
Little Creek WWTP
Barclay Downs
Mallard Crossing
Beachwood
Mallinckrodt
Birchwood MHP
Nature's Trail
Briar Chapel Development
Neuse Colony
Briarwood Farms
Neuse River Village
Carolina Meadows
Neuse River WWTP
Chapel Ridge
Oxford WWTP
Cole Park Plaza
Pope Industrial Park
Colvard Farms
River Mill
Consolidated Diesel
Rock Bridge
Cottonwood/Baywood
SGWASA WWTP
Crooked Creek
Shearon Harris NPP
Cross Creek
Tar River Regional WWTP
Deerchase
The Legacy at Jordan Lake
Enfield WWTP
The Preserve at Jordan Lake
Fearrington Village
Town of Bunn
Franklin County WWTP
Town of Louisburg
Governor's Club
Town of Pittsboro
Hasentree Golf Comm.
Town of Spring Hope
Hawthorne Subdivision
Town of Warrenton
Henderson WRF
Tradewinds
Hominy Creek WWTP
Westfall
Johnston Co. WWTP
Whippoorwill Valley
Kenly Regional WWTP
Wildwood Green
King's Grant Subdivision
Willowbrook
Kittrell Job Corp.
Woodlake Country Club

Influent Box
J
GRANVILLE FARMS CLASS B WWTP RESIDUAL BIOSOLIDS FLOW SCHEMATIC
Grit & Trash Aeration Basin
Removal
Ea)a
6
(ifQcn
Solids
Aerobic Digester/Storage
i 0 Crop Planting
& Growing
Transport
to Field
Land Applied
Clarifier
Discharge
Water
Disinfection
Harvesting,
I

GRANVILLE FARMS CLASS B SOURCES (WTP)
Enfield WTP
Kerr Lake Regional WTP
SGWASA WTP
Sunset WTP
Tar River WTP

GRANVILLE FARMS CLASS B WTP RESIDUAL BIOSOLIDS FLOW SCHEMATIC
Raw Water Chemical Mixer
Clear Well
i
Filter
Flocculators
Disinfection
Filter Backwash
Harvesting
Somlids
Reoval
Solids Storage
Liquid Truck
Loading
Transport
to Field
I
,,. • Ts 5 CropPlantin
suswrndble g
amtn� & Growing
Land Applied

GRANVILLE FARMS O&M PLAN
MAXIMUM PRODUCTION
QUANTIFICATION & JUSTIFICATION

AVERAGE
.of
Forecasted Requested
Gallons
Dry Tons
years Counted
Production DT
38,938
2.43 Amherst WWLP
3
Amh-WWP
4.97 SOAO
13,350
1.14 Arbor Hill MHP
1
Arbor Hill MHP
2.28 30Ao
210,375
10.82 Ashley Hills WWFP
2
Ashley Hills WWFP
21.63 30.00
43,017
3.56 Avocet WWFP
3
Avocet P
7.12 30A0
20,163
0.55 Barclay Downs WWFP
8
Barclay Downs WWFP
1.10 30A0
21,508
1.56 Beachwood WWFP
6
Beachwood WWFP
3.11 30A0
48,950
2.47 Birchwood RV Park
1
Birchwood RV Park
4.% 30A0
237,793
18.63 Briar Chapel Development
3
Briar Chapel Development
37.25 30.00
72,8W6
4.57 Briarwood Farms WWFP
9
Briarwood Farms WWFP
9.13 30.00
378,2%
33.58 Carolina Meadows WWFP
9
Carolina Meadows WWFP
67.17 75A0
18,450
3.99 Chapel Ridge W WFP
1
Chapel Ridge W WFP
7.98 30A0
70,706
6.33 Cole Park Plaza
9
Cole Park Plaza
12.66 30A0
36,667
2.25 Colvard Farms
3
Colvard Farms
4.50 30A0
1 W,66]
7.51 Consolidated Diesel W WFP
6
Consolidated Diesel W WFP
15.02 20.00
-
0.W Cottonwood/BaywoodW P
1
Cottonwood/BaywoodW P
0.00 30Ao
118,033
10.35 Crooked Creek W WFP
9
Crooked Creek W WFP
20.69 40.00
44,783
2.05 Uoss Creek Mobil a IF-
9
Uoss Creek Mobil a IF-
4.10 30Ao
66,956
3.12 Deerchase P
9
Deerchase P
6.24 10Ao
113,306
13.09 Enfield WFP
9
Enfield WFP
26.18 50.00
191,779
19.66 Enfield W P
9
Enftld W WFP
39.32 300A0
247,333
30.17 Fearrington Utility WWFP
9
Fearrington Utility WWFP
60.34 300A0
981,556
120.% Franklin County WWFP
9
Frankl in County WWFP
241M 319.00
178,988
].% Govenor's Club WWFP
8
Govenor's Club WWFP
15A9 40.00
37,2W
3.27 Hasentree Golf Comm unity
2
Hasentree Golf Comm unity
6.53 50.00
285,528
23.32 Hawthorne Subdivision WWFP
9
Hawthorne Subdivision WWFP
46.63 80.00
3,116,167
546.21 Henderson WRF
9
Henderson WRF
1092A2 1600.00
1,481
483.12 Hominy Creek WRF
4
Hominy Creek WRF
966.25 2000A0
234,000
33.18 fohnston County WWFP
1
fohnston County WWFP
66.35 300A0
888,422
76.17 Kenly Regional WWFP
9
Kenly Regional WWFP
152.34 M9A0
216091444
103.29 Kerr Lake Regional WFP
9
Kerr Lake Regional WFP
206.58 ZOo..
26,7W
1.49 Kings Grant Subdivision
9
Kings Grant Subdivision
2.98 30A0
18,056
1.49 Kittrell lob Corp
8
Kittrell lob Corp
2.98 30A0
66,750
5.43 Knightdale Mobil a Home Park
9
Knightdale Mobil a Home Park
1oA6 -
16,688
1.59 Lake Ridge WWFP
8
Lake Ridge WWFP
3.18 ..o
-
0.W Lake Royale WWFP
1
Lake Royale WWFP
0.00 30A0
28,3W
1.52 Leg.W tlordan Lake
2
Leg.W at lordan Lake
3.03 Z0.00
928,6a4
88.96 Little Creek W WFP
6
Little Creek W WFP
177.92 150.00
85,017
6.70 Mallard Crossi ng WWFP
9
Mallard Crossing WWFP
13A0 15A0
-
0.W MallinckrodtW P
1
MallinckrodtW P
0.00 790A0
132,388
5.53 Nature Trails MHP WWFP
8
Nature Trails MHP WWFP
11.06 Z0.00
1,026,000
70.95 Neuse Colony WWFP
8
Neuse Colony WWFP
141.91 150.00
76,267
3.% Neuse River Vill age
9
Neuse River Vill age
7.97 15A0
3,%S,642
562.83 Neuse River WWFP
]
Neuse River WWFP
1125.67 3000.00
3,600,133
489.20 Oxford WWFP
3
Oxford WWFP
978A0 500A0
10,383
0.26 Pope Industrial Park
3
Pope Industrial Park
0.52 ..o
128,783
7.20 Preserve at lordan Lake
3
Preserve at lordan Lake
14.39 Z0.00
4,450
0.50 Rives Mill W WTP
1
Rives Mill WIXTP
1.00 10A0
49,210
3.19 Rock Bridge WWFP
5
Rock Bridge WWFP
6.38 30A0
1,796,667
129.19 SGWASA W P
9
SGWASA WFP
258.38 319A0
2,302,329
313.30 SGWASA WWFP
9
SGWASA WWFP
626.59 650A0
347,129
3.41 Shearon Harris NPP
]
Shearon Harris NPP
6.82 1 0
495,408
87.55 Sunset WFP
6
Sunset WFP
175.10 319A0
2,146,444
227.29 Tar River Regional WWFP
9
Tar River Regional WWFP
454.58 800A0
8a4,667
1W.30 Tar River WFP
9
Tar River WFP
2W.20 319A0
32,SW
1.% Town of Bunn
1
Town of Bunn
3.79 75A0
1,160,667
135.47 Town of Louisburg
9
Town of Louisburg
270.% 319A0
527,000
96.% Town of Pittsboro W WFP
1
Town of Pittsboro W WFP
193.W 200A0
86,775
9.W Town of Spring Hope WWFP
6
Town of Spring Hope WWFP
19.59 50.00
909,9a4
146.31 Town of Warrenton W WFP
9
Town of Warrenton W WFP
292.62 319A0
75,750
3.89 Tradewin&s P
9
Trad-inds W WFP
7.77 30A0
44,]]5
3A0 Westfall WWFP
2
%V sW ll WWFP
6.79 30A0
41,383
1.88 Whippoorwill Valley WWFP
9
Whippoorwill Valley WWFP
3.76 15A0
80,217
6.93 Wildwood Green WWFP
9
Wildwood Green WWFP
13A6 15A0
66,263
3.20 Willowbrook WWFP
8
Willowbr 1,k P
6A0 10A0
106,575
9.77 Woodl C..Iy Q� W WTP
4
Woodl Co-t, Q� W WTP
19.54 25.00
31,634,SU
4,106
8,212.56 11,638.00

GRANVILLE FARMS O&M PLAN
SOURCE VICINITY MAPS

TABLE OF CONTENTS
SOURCE
FIGURE
SOURCE
FIGURE
Amherst Subdivision
1
Lake Ridge
18
Arbor Hills MHP
38
Lake Royale
29
Avocet
25
Little Creek WWTP
19
Ashley Hills
40
Mallard Crossing
20
Barclay Downs
2
Mallinckrodt
8
Beachwood
2
Nature's Trail
4
Birchwood MHP
38
Neuse Colony
21
Briar Chapel Development
5
Neuse River Village
2
Briarwood Farms
3
Neuse River WWTP
16
Carolina Meadows
4
Oxford WWTP
42
Chapel Ridge
39
Pope Industrial Park
22
Cole Park Plaza
5
River Mill
23
Colvard Farms
6
Rock Bridge
16
Consolidated Diesel
7
SGWASA WTP
24
Cottonwood/Baywood
40
SGWASA WWTP
24
Crooked Creek
1
Shearon Harris NPP
25
Cross Creek
2
Sunset WTP
26
Deerchase
8
Tar River Regional WWTP
27
Enfield WTP
9
Tar River WTP
28
Enfield WWTP
9
The Legacy at Jordan Lake
36
Fearrington Village
5
The Preserve at Jordan Lake
36
Franklin County WWTP
10
Town of Bunn
29
Governor's Club
4
Town of Louisburg
30
Hasentree Golf Comm.
37
Town of Pittsboro
39
Hawthorne Subdivision
11
Town of Spring Hope
31
Henderson WRF
12
Town of Warrenton
32
Hominy Creek WWTP
41
Tradewinds
8/20
Johnston Co. WWTP
13
Westfall
4
Kenly Regional WWTP
14
Whippoorwill Valley
33
Kerr Lake WTP
15
Wildwood Green
11
King's Grant Subdivision
16
Willowbrook
34
Kittrell Job Corp.
17
Woodlake Country Club
35
Knightdale MHP
2

SR-s
c�W E-
�083
s
$
v
SR-1593
SR-1568
_39
"�SR-1579
SRSR-1553
SR-4766
-n
w
SR-3942
w
Cary
0
rr SR-�1390 vti
s
c
SR 1504
Q
v,
0
Holly Springs
/NN�
uquay-
�A"
ruquay- vanna
7� R 1� ro
�I
S`7$�3
SR-2811
N
c
�P4
SR-4737
SR3997 Fuduav-Va]
i
s
( Creek
SR-2724
c
� �
SR- 5006 o
S
�33
I
s�Ql
�a
Fuquay-Varina
SR-3952
�s
sl�
3�5�
�•
13 ,3 Fuquay-Varina
S SR_3�
o
SR-3959
SR-403g
x
o°
s �S�oti N
SR-2752
S ti
Fuquay-Varina
Legend
SR-3730 �
a
u�
Source Location
Terrible Creek
Fuquay-Varina
o
— Road
��
SR,37 56
51
sR
Stream
sR 15
Fu
L_jCounty Boundary
SR_4813
Municipal Boundary
N
0.5 0.25 0
0.5
39
Miles
SR 48ni
Scale: 1 inch = 0.5 miles
T
LOCATION MAP
Figure
Drawn by: CSC
�- T
P
SOIL 1L J f lJ s
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Fuquay-Varina, North Carolina
1
Date: Sept'16
Soil Plus Project # 200705.G10

N
tW E
S
6
WAKE
Raleigh
Carolina Lak
VL
SR-2680
SR-2625
t�
R
SR
�-2946
--F�
SR-4102
1
Neuse River
Zs1�-,
J
SR-2671
�N
0
SR-2515
1
N'
`� 3'" 007
Knightdale MHP Cross Creek
J
jI
L2p�21]C�
n
Source Location
x
,
— Road
U s
Stream
,L_JCounty Boundary
SR_2678
Municipal Boundary
0.5 0.25 0
0.5
Miles
Scale: 1 inch = 0.5 miles
LOCATION MAP
Figure
Drawn by: CSC
PLUS �- T
SOIL 1L J f lJ S
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Raleigh, North Carolina
2
Date: Sept'16
Soil Plus Project # 200705.G10

N
i
\W E
S
ti
ti(3
SR-1
Apex
SR-1448
\'J
130� C \
d
SR�5429 0.
WAKE SR--
N Brian
S -545
SRC-583�2
Cary
S R-3934
\ch
St 39
n
Sg39�� 9��/ SR-1484
N
Legend
S
Source Location Holly Springs �� 3
S�
— Roads
o �
Stream SR-1390
A� o
LJCounty Boundary
Municipal Boundary o 0.5 0.25 0 3- 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC Cary, North Carolina 3
Date: Sept'16 Soil Plus Project # 200705.G10

/ N p
v
W E
S \
a�
ORANGE
l 198
CHA
� II
� O�1
ti
Nature
1 6
1832 1 ��
1753
AM CD
M CD
o N
r
Home Par WWTP
i
O
O
' 0O
a
11
Y
N
?
U
I�SS 1736
I,
mod;
n
�C
T
�h
1740
Cr
I --ek I>"_
3120
0
Legend
cr,
0 Source v 761 174�
Water m� 00 1'°'
o
Stream tip° WAKE W
rig �
Road Y
County Boundary ^�
0 1 0.5 0 1
Municipal Boundary
Miles
n 17
—11-11
Scale: 1 inch = 1 miles SOURCE LOCATION MAP
Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: Chapel Hill, North Carolina 4
Date: Nov'17 Soil Plus Project # 200705.D10

f c 1602 ^tit`
0
1532 Cole Park Plaza
� %rC.
1584
00 " 1 SGS
�n
00
00
�n
1530
Ln cl~
011
�~�
` 1721
Briar Chapel Development
G
1606
o •'
4
1634 `r 1719
o Dogwood Veterinary Hospital
CHATH�
1717
166 j
�
Legend 1618
NC Sources ~ 1Q3 Fearrington Village
`n 1
Stream Nc 1�6`� 1779 ASS
— Road ) 1 w c 1803
NHDWaterbody h % 52� 1805 180
<all other values> 1 1+718 st
6g� 1g15 �� 1802
FType 1 ��1so 1836
Estuary GO �
Ice Mass 1 ~ 1818
❑ LakePond w�
Playa
Reservoir
0
nSwampMarsh 00
ti
i J!CountyBoundary
�MunicipalBoundaries_polys 0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP
Figure
Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ000838)
Reviewed by: CSC Chapel Hill, North Carolina 5
Date: April'17 Soil Plus Project # 200705.G10

DURHAM
1103
______---------------
- Colvard Farms
G
Durham
l �
s
Legend °
Cary
Source Location
— Road ���G� Cary
Stream
r- �
County Boundary North/}eaa'st Creek
-J
M Municipal Boundary rgan Creek Arm of New H�op�e River Arm of B. Everett Jo I \
Surface Water I 0.5 0.25 0 0.5
Miles y
1-1organ ree(including t e organ Creek Arm of New Hope River Arm of B. Everett Jordan Lake `�
Scale: 1 inch = 0.5 miles T T LJ r LOCATION MAP Figure
Drawn by: CSC SOIL L• PL S GFI Land Application Permit (WQ000838)
Reviewed by: CSC Durham, North Carolina 6
Date: Sept'16 Soil Plus Project # 200705.G10

N
W E
S
\J
r
SR�1�1
SR-1519
0
a
ti
NC-33 /
Whitakers NC-33
i
i
/
/
S�V — 4
NASH
55z
Cons6lidated Diesel
SR-1516 /
;ZAP
Creek
EDGECOMBE
Legend
Source Location
/
— Road
i
Stream i
L_JCounty Boundary
Municipal Boundary �1 0.5 0.25 0 0.5
Surface Water i g
j 1N19 Miles
/c
Scale: 1 inch = 0.5 miles LOCATION MAP
P T r T Figure
Drawn by: CSC SOIL 1L J f lJ s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Whitakers, North Carolina 7
Date: Sept'16 Soil Plus Project # 200705.G10

N 2� Q
W E
Wake Forest
S 2JJs 2045
CG ~
°Op Gb
0 Q
0 Wake Forest Smith Creek WWTP Smith Creek WWTP
ti
a
Mallinckrodt
M
Oo
a°
D a
2043 0
a
\00G I
0
3663
c,
'064 o
N
Deer Chal
e
Forest
5170 00
0
N
pp1
N
/� N
Raleigh
Raleigh
WAKE
-'
O
0
�
cV A2GI
Legend
GNC Sources
Dc1' St2s WL �
Stream
�6�1 —4914 49
0
— Road
4622 c c1�
ND
NHDWaterbody
° o w
No8
Tradewinds
fff
all other values>
2930
FType
2�82
❑ Estuary
❑ Ice Mass
❑ LakePond
o
po
❑ Playa
❑ Reservoir
222%
7SwampMarsh
i J!CountyBoundary
2�$�
4308
ElMunicipalBoundaries_polys
0.5 0.25
0
0.5
Miles'
Scale: 1 inch = 0.5 miles
LOCATION MAP
Figure
Drawn by: CSC
SOIL
PL Us
GFI Land Application Permit
(WQ000838)
Reviewed by: CSC
Raleigh, North Carolina
8
Date: April '17
Soil Plus Project # 200705.G10

N
W E
\\ s
NC-481
Coat
SR 123^231i
sR-1223
�s
�C_481-$L
tiV
/Unfi
sR-1220
HALIFAX
WWTP
I B
ee�h Ska
mp
0
o,
NC-481
Legend
Source Location
— Road
Stream
i_JCount Y Boundary
,00 Municipal Boundary
N1 Surface Water reed. 0.5 0.25 0 0.5
� Miles
Scale: 1 inch = 0.5 miles r V T LOCATION MAP Figure
Drawn by: CSC SO S GFI Land Application Permit (WQ000838)
Reviewed by: CSC 494supbwo,Enfield, North Carolina 9
Date: Sept'16 FSOTplus Project # 200705.G10

\ NN N �
ti
E ti
5�
S
ti
h'
ti
Franklinton
N
Y
SR-1157
N r
SR-1163
\ SR-1159
�a
ERANKLIN
Franklin County VWJF
Cedar Creek
SR-1133
0
s�
Creek
N
i
Legend
Source Location
Ion
— Road
Stream
L_JCounty Boundary sRi964
sR_ Municipal Boundary
Surface Water �1130.5 0.25 0 0.5
Miles
"a•�•ymg t,reek
Scale: 1 inch = 0.5 miles LOCATION MAP
OIT�T� r 11J T Figure
Drawn by: CSC S �l� s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Franklinton, North Carolina 10
Date: Sept'16 Soil Plus Project # 200705.G10

s s
^N SR 4230
SR-4281 SR-4633 s��c �Q2 SW:I.,
W E SR-1899
s
4 SR-4483 SR-4984 S�
s
O�
k
t; g rr sr �6 FC
9
63 SR-4976 v'
� x gg 1� SR-5619
� '
4Q —w
R �
/ SR-4689 S� s
SR-5686
Hawthorne Subdivision
NC)'S 3599 l
SR-498) ��tj � SR 3452 s� s6�3 n SR-3594
2 P Q 0 \
n h S ,59
SR-1834 s� 4j R 3 3
3
S3382 �� N
R
SR-3286
94SR-3591 SR-3590
o �+, SR-3589
MC, S fi
R-4695 w°
18 SR-3467 ��� SR-3588
SR-3379
SR-4909
sR-183Y WAKE � �"
.�
Raleigh s
kQ
I-540 SR-1898
6
�2
tiC� m�C�
3g54 SR!4276 RN1RL201 ��
51Z SR-
ti�asx-322s x s��o Wildwood,Green SR-3447
1 Raleigh °"'
SR-3445
s
s� Raleigh ? � � M
J838
SR 42�9 1
SR-3289�
SR-1829 w S�
Raleigh
N
s SR-3236 SR
SR-3450 �N
SR SR-3256 r1,
46Z3
SR-3241
LegendroA
Source Location
Raleigh
— Road Cggo�
4 s
Stream SR-3305
i_JCounty Boundary SR-3363 7 SR-3303
Municipal Boundary Raleigh
Surface Water leigh p ,� 0.5 0.25 0 0.5
s� Miles
inV�
Scale: 1 inch = 0.5 miles LOCATION MAP
P Figure
Drawn by: CSC SOIL 1L L US GFI Land Application Permit (WQ000838)
Reviewed by: CSC Raleigh, North Carolina 11
Date: Sept'16 Soil Plus Project # 200705.G10

N
W E
s
'-1-1309
SR-1453
� o
a
SR-1429
S�'77
h
sR-14zS )Henderson WRF sR_1 s� sR-1001
31z �
VANCE �1ti s
ll�
sR,1 5�
N .t� 1 �6
NO PWP-2113 �N SR,� 184
RMP-2110,-2111
1JS-158 � ti
n` a cA
1 �
5� 5oN
S�1
4� c
5�
SR-1518 a9
Henderson N
Legend
s a
Source Location
— Road
Stream
3J
LJCounty Boundary
Municipal Boundary N �R 1F22
Surface Water
S 0.5 0.2-5 0 0.5
Miles
SR-1148
Scale: 1 inch = 0.5 miles LOCATION MAP
P Figure
Drawn by: CSC SOIL 1L L Us GFI Land Application Permit (WQ000838)
Reviewed by: CSC Henderson, North Carolina 12
Date: Sept'16 Soil Plus Project # 200705.G10

N �
a�
N
W E
0�
616
o I Johnston County WWTP
P�I
SR-1340
11%
JO
0
f
V�10
S�1341
� n�h
1343
Legend
Source Location
— Road
Stream
Smithfield xlS Smithfield
�_JCounty Boundary
s�
Municipal Boundary
0.5 0.25 0 0.5
Surface Water
Miles
Scale: 1 inch = 0.5 miles
LOCATION MAP
Figure
Drawn by: CSC
T
PLUS
SOIL L V S
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Smithfield, North Carolina
13
Date: Sept'16
Soil Plus Project # 200705.G10

N 21�a
S�
W E SR-2147
s u v
N sv.
o Ui
0
w
0
SR-2146
Kenly Region
N
a
SR-2162
\.U,
i�
1� A
ti
D
S$-2143
h'.
Kenly
_ � SR-2346
�F Mill Creek
S\3g5
SR 2142
5�' Kenly
T,
Kenly
�0
SR-2343
4
Legend
Source Location
S,R��
SR-2341
o0o—
Road
J'
Stream
�y� SR_2414
L_JCounty Boundary���
Municipal Boundary
Surface Water
0.5 0.25 0 0.5
Miles
Tj
Scale: 1 inch = 0.5 miles
LOCATION MAP
Figure
Drawn by: CSC
P �- T
SOIL L V s
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Kenly, North Carolina
14
Date: Sept'16
Soil Plus Project # 200705.G10

N � �/ SR-1366
W E
(below n.
N 7 L
Kerr Lage
))fir •/
Swamp,Creek,below normal pool elevation
SRR-1,446
h Creek Arrr
SR-1418
SR�13�8
SR-1403
Ste.
ft MSL')
VANCE
SR 13 5
WTP
,-,-1400
Mill Creek
Legend
Source Location
Middleburg
— Road
sx-
Stream
r--
�_JCounty Boundary
RM13-2130 �T
Municipal Boundary
Surface Water
0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles
LOCATION MAP
Figure
Drawn by: CSC
n T T
SOIL 1 L LJ s
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Middleburg, North Carolina
15
Date: Sept'16
Soil Plus Project # 200705.G10

R �
SR_4114
33
5�SRti�S�g�_26
41 red SR-5
N� �
�
Wendell0 SR-5241US64,264
w e SR=41'55Knightdale
SR-2671 SR-2685 �
s -2674
N v 0C CJ
SR -
Rock Bridge 1111
SR-2507
SR-2511
C/� W
WAKE
o s? z
�o
AlZ9
5� SR-2509
Kings Grant
o �y� SR-2508
S,'
S� 473
SR-4198 6
c�
igh Neuse River WWTP
e
Legend
Source Location
— Road
i
i
Stream
JCounty Boundary %� -%� JOHNSTON Clayton
Municipal Boundary tz��
0.5 0.25 0 0.5
Surface Water4t
�t Miles
Scale: 1 inch = 0.5 miles j LOCATION MAP Figure
Drawn by: CSC SO' Int, 4i�J s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Clayton, North Carolina 16
Date: Sept'16 Soil Plus Project # 200705.G10

i
N
w
S
SR-1107
s
�2
9Q �5
5R_12
SR-1573
SR-1262 v
U
4
0
a
VANC--E 0 Kittrell Job Corp
��1ti3-SR-1588
xl �
SR-1105 0
Kittrell SR-1551
x
SR-1240
� � o
V �
V�
C
UJ.
SR-1556 i
Legend
_
Source Location
— Road
Stream
r
i_JCount Y Boundary
Municipal Boundary
0.5 0.25 0 0.5
Surface Water
Miles
Scale: 1 inch = 0.5 miles
LOCATION MAP
Figure
Drawn by: CSC
T T LJ r
SOIL L• PL s
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Kittrell, North Carolina
17
Date: Sept'16
Soil Plus Project # 200705.G10

I SR-1214
N �\
Bu)ne
w e %I SR-1100
S ! ,_
PFlater (neluding the Flat Riv
c
5R1633 ����-----------------------------------
M �
C-
Gam/
SR"
i
1 ti
1
1
7637
1
Tj
Lake Ridge
=Neuse River (Falls Lake below normal�Po (elevation),
WAKE
DURHAM
5�
3
GYeek
4a�t�e�
Legend
0
.Source Location
a
— Road
SR-1893
— Stream
3County Boundary
Municipal Boundary
—�10.5
SR-1893 IlkSurface
0.25 0
0.5
Water
Tiiiiiiiiii
Miles
ur am urrham
Scale: 1 inch = 0.5 miles
SOIL PL U s
LOCATION MAP
Figure
18
Drawn by: CSC
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Durham, North Carolina
Date: Sept'16
Soil Plus Project # 200705.G10

i
N
bN`
W E
S
Sg-2320I
. SR-24'6
\�s
WAKE
SR-234()
SR-2347
SR-5417
SR-1726
JOHNSTON
y
SR-2100
s�
cj
a
tr
US-264-A1-T
NASH
Legend
Source Location
— Road
Stream i
L_JCount Y Boundary
Municipal Boundary SR-1723 sR,,
Surface Water 0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PL U s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Zebulon, North Carolina 19
Date: Sept'16 Soil Plus Project # 200705.G10

N N SR-2224
x SR-4914 �
`" N
�W E/S4-4657� N
SA4622
� L
S� Raleigh W _ Tradewi�ds
s2 N
s�
SR-2223 � SR_433`�
SR-2217
SR"2�a� SR-4 OS
SR-2296
�> c
Mill Creek
Raleigh sR-295s s�.A33�
N
N
N
Mallard Crossing
J� �s sR-2972
Raleigh
Is
�A N
Raleigh
Raleigh
�M
N
N
SR'�3 SR-4313
Legend
Source Location
— Road
— Stream
i_JCount Y Boundary
Municipal Boundary
R, 0.5 0.25 0 0.5
Surface Water y
Miles
ightdale "igntaaie
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PL U s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Raleigh, North Carolina 20
Date: Sept'16 Soil Plus Project # 200705.G10

N
W E
�I S
1 Clayton
Clayton
Gs
Clayton
Jo
5t
Clayton
Archer Lodge
r
r
c4
0
SRC 3� SR72693
�N N DNS
ti � ti
I
M
-42
Neuse-Colony
0
Clayton
SK=1903
897
M
l~
nj
Legend C L0)
Source Location ��oN
sR�
— Road layton
c
Stream o
Count Boundary
o
i_ J y y o SR-1913
Municipal Boundary
Surface Waterzt
0.5 0.25 0 0.5
t 600� Miles
US-�o "r - x
Scale: 1 inch = 0.5 miles j T LOCATION MAP Figure
Drawn by: CSC soy � l J s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Clayton, North Carolina 21
Date: Sept'16 Soil Plus Project # 200705.G10

SR-1473
9
SR-1450
SR-3933 SR-1375
N
c�
r,
r
SR-3881
a a
n SR 2-,--
N
c4
I -- r
SR-14,46 � d*N
SR-1466 SR
Raleigh
c
�I i
SR-1374 SR-2797
ti
c
a
SR-2720
cc
a
SR-2719 SR-2798 2
Pope Industrial Park
M� SR-2833
SR-2782 SR-2792
�� Uf SR-277_'
i�
L sR 21190
-2852 WAKE /
SR-2819
<3
N s�
SR-282,5
Garner
715
2857 `J
Garner11
sR
SR-3703
�'
Legend
n111
Source Location
N�
S�
— Road
Stream
o�
CJCounty Boundary
sR
J
Municipal Boundary
48
64
sR-
Surface Water
s 0.5 0.25 0
Rs3j9
0.5
5�
Miles
SR-2891
Scale: 1 inch = 0.5 miles
T
LOCATION MAP
Figure
Drawn by: CSC
�- T
P
SOIL 1L J f lJ s
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Garner, North Carolina
22
Date: Sept'16
Soil Plus Project # 200705.G10

N s� 1967 s��l Wake Forest
N C-98
W E
S ^^ A JI ww
_ 1 \
5� "o
SR-3625
ti
SR-3509 Sg-362:4 R1Ver Mill
Neuse River (Falls Lake below normal pool elevation v
SR-5169 w
..q
77U
� W
4 3 WAKE
sk ti Raleigh
�v
c�23
M
NEUSE RIVER
`
Wake Forest
ti
572� SR-5107 s� SR-2045
sR,2oo
2 �
ti
SR 3697
Legend
Source Location
Wake Forest D
— Road
Stream
�o
L_JCounty Boundary '6
` Municipal Boundary
0.5 0.25 0 0.5
Surface Water
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PL U s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Raleigh, North Carolina 23
Date: Sept'16 Soil Plus Project # 200705.G10

I
1112
NS1Z-
Q
vW E
s � picture
Greek
I SR, eels\ ZZ
R
map of SgAN � SGWASA WTP
! S�
I G5b
I s� tititi� �
� I
II
s
titi ti
SG SA WWTP
G
Butner
Legend /
er (including the Flat Riv I/
Source Location
SR-1234
— Road
— Stream
Count Boundary
i_J Y Y /
Municipal Boundary
Surface Water 0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PL U s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Butner, North Carolina 24
Date: Sept'16 Soil Plus Project # 200705.G10

11 �
W E` �. U
® �� O
dd
r", 3;
off`
Shearon Ha ris uclear Power Plant Q�tai
120
115
1394
°
k
0
1 s
TP
1395
1114
4 4024
1 96
s
1 01
1126
WAKE 0ta�o 1113
127
m
a 1 11
ti g
1�2s 1112 Twin L ke T
242
vocet P
yo 2
titi 2
1110
N
Q
1123
1104
N �
1103 /I
1274 /L J1
Ix 1114, 1122 �
CHATHAM zz
ti
O h M
V
1h�h ti ��01
.$J
ti
1405
N a
� 145
1451 ti
Legend ek 68
0 Source 5
Water
Stream G �ee� �
bets u' Sent rs t o
Road .
County Boundary , A02o 1 0.5 0 1
0 Municipal Boundary
14t� Miles
1411
Scale: 1 inch = 1 miles SOURCE LOCATION MAP
Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: 4900W
Holly Springs, North Carolina 25
Date: Nov'17 Soil Plus Project # 200705.D10

N
W
\✓r
R1\1P-172
Rocky Mount
r
f <h,
i
�Ic 133
o �
O
N �
SR 1
WTP
ti
S�
SR-1599
SR-1542
o�
O/ LOG915 y
US-64
Horn B
RMP_1 �1
E
sg'
s
G G�
Leg
end d LOC-914
� N
� o
Source Location p� i
% o
— Road m j
Stream CokeY 5°'amp / mottle
L_JCounty Boundary
Municipal Boundary SR-1727
Surface Water 0.5 0.25 0 0.5
i=6 Miles
u
Scale: 1 inch = 0.5 miles T T LJ r LOCATION MAP Figure
Drawn by: CSC SOIL L• P� • s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Rocky Mount, North Carolina 26
Date: Sept'16 Soil Plus Project # 200705.G10

N
W E
s
SR-1404
EDGECO'MBE
Rocky Mount
Legend
Source Location
— Road
Stream
_ r
i_JCount Y Boundary
Municipal Boundary
z
Surface Water
N
Tar River
0 I
gional WWTP
SR-1414
v
a
0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP
PLUS Figure
Drawn by: CSC SOIL 1L PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC Rocky Mount, North Carolina 27
Date: Sept'16 Soil Plus Project # 200705.G10

N
S
N
I
SR-1707 v
V
460lobat� SR-1710
94
SR-1709 °h
Tar River WTP
slJ
SR-1749
a
NASH
s�
Rocky Mount
Sg�
�334
SR-1733
Legend I `
Source Location ass
— Road
Stream
County Boundary
Municipal Boundary
s 0.5 0.25 0 0.5
Surface Water �,1��
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP
P �- T Figure
Drawn by: CSC SOIL L V s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Rocky Mount, North Carolina 28
Date: Sept'16 Soil Plus Project # 200705.G10

N
S� J,JJ
W E
S
1� NC-98
O
O/
\s�
Town of
0
FRANKLIN
1609
ti
M y
Legend Lj1
l�
2 Source Location SR-1 736
— Road
Stream
i_JCount Y Boundary
Municipal Boundary sR��4�
Surface Water 0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP
�T � r Figure
Drawn by: CSC � () IT L L L J s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Bunn, North Carolina 29
Date: Sept'16 Soil Plus Project # 200705.G10

N
W E
s
—.lC'��Creek
_N
a �
� �SR n
_ N
TKLIN
122E
SR' 12�2
SR-1256J
SR-1231
va,
SR-1645
1 sR-12,3
Sly
z6o� Sg 1�
burg
14j1
<rl
Legend
Source Location
— Road
Stream
Count Boundary
i_J Y Y
Municipal Boundary
Surface Water ��� 0.5 0.25 0 0.5
SR-1604 Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PL U s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Louisburg, North Carolina 30
Date: Sept'16 Soil Plus Project # 200705.G10

i
N
J�
W E��
S
SR
SR-1331
SR-1314
SR,1
t
11146
� sr
U
0
0
V7
Spring Hope
ks Creek
Jam'
j
�[ 5�64�US-64�200
Rmp-401
S�-114-5
SR- 1180
SR-1915
1
Legend C'e
Source Location
s�
— Road TAR RIVER
Stream
i_JCount Y Boundary
F—Imunicipal Boundary
Surface Water 0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PL U s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Spring Hope, North Carolina 31
Date: Sept'16 Soil Plus Project # 200705.G10

N
W E
S
0
Fishing
SR-1332
SR-1107
N
SR-11.19 �S
�N SR-1326
SR-115(
n
i
0
SR-1601
SR-1142
7
cC
x
0
n
fD Warrenton
SR'16�2
IZ/
21 5�2.
ell,Legend
Source Location °
— Road
Stream
i_JCount Y Boundary
Municipal Boundary -
Surface Water 0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SO S GFI Land Application Permit (WQ000838)
Reviewed by: CSC Warrenton, North Carolina 32
Date: Sept'16 Soil Plus Project # 200705.G10

N SR,
i
W E
ti
119 I�22 S¢,11 �ti5
FRANKLIN
1
1
_ Whippoorwill -Valley
SR_ -�
2447 I
cn �
m Si S� S$-1826
N �
\+b"
SR-1724
titi��
g1R 2311
5� M
WAKE SR-2313
�
N
W
Legend
Source Location
— Road
e
— Stream
SR-2309 Oil
\
r CountBoundary9
Y
Municipal Boundary
0.5 0.25 0
0.5
Surface Water
Miles
SR-2315
Scale: I inch = 0.5 miles
LOCATION MAP
Figure
Drawn by: CSC
SOIL PLUS
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Zebulon, North Carolina
33
Date: Sept'16
Soil Plus Project # 200705.G10

,® {
/#s #�
© E SR-524 ®77
�
s
^
;
«
WAKE »
\
r
°
G
« caSR-
m!!4
Will owbrook
d
�
}
y f \ }
\ d
s�
/ + $�
\
y
y
/,
» w&!77(
i\
\
* �
/ y
+ �
�
»
�
S` ©78
�
±
JOHNSTON
IS,
�
�R,k2;
ƒ s& 1615
\
Silr77
Cats
y»
\ s Ic
, Legend
aSourceLocGBn
— Road
Steam
s#59
\\ Coun& Boundary
5 F-1 municipal Boundary
Surface Water
« 0.5 0.2 O
0.5
Sys
Scale: 1 inch s 0.5nii1e
SOILPL s
LOCATION MAP
Figure
34
Drawn by: CSC
Gq Land A piationPrmil 99000838)
Reviewed by: CSC
Garner, North Carolina
p#w Se t' 6
Soil Au Project # 200705.G10

N {,
W E
N
S `0/
SR-2016
IN
MOO
SR-2176
0%0
� O7
�� 0
SR-2019
I
I
I
I
I
N
Legend N cG
Source Location
— RoadHO
Stream 01 ICE
♦�
L_JCounty Boundary
Municipal Boundary
0.5 0.25 0 0.5
Surface Water
Miles
IF
Scale: 1 inch = 0.5 miles LOCATION MAP
P T r T Figure
Drawn by: CSC SOIL 1L J f lJ s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Vass, North Carolina 35
Date: Sept'16 Soil Plus Project # 200705.G10

N
W E
S
The Preserve at Jordan Lake
0
The
0
N
0
Jordan_Lake SRA - Parkers Creek Q
CHATHAIVI 1746
0 0
Oq D cp
Legend O
0 NC Sources
Stream
0
— Road
NHDWaterbody
L <all other values> p
FType e64 64
JordaneL-ake-SRA=_Seaforth
Estuary
Ice Mass °
LakePond
Playa o
Reservoir
nSwampMarsh O
i J!CountyBoundary --
�MunicipalBoundaries_polys 0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP
Figure
Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ000838)
Reviewed by: CSC Pittsboro, North Carolina 36
Date: April'17 Soil Plus Project # 200705.G10

N oo `� 1909 �
N QN
W E Qs� a
S 4592
�s�8 T�Tc �S88 0^0 5704 �5F721
5720 Wake'Forest
CN
n M
4565 4521 4577
c
148 4$73 Hasentree Golftommunity
4523 cV 7t
�Hasentree Golf Community, Phase 1 & 2A ��„� 26
rr
D o
4Sj8
Ncb
U 4583
� 1988
4560
4517
l�
98
00
gslp
Legend
1
4408
NC Sources
°`
Wake Forest
"
T�
�oo�
Stream
c5p
— Road
1961
NHDWaterbody
5165F—I
SGo
9 98,98
<all othervalues>
4
FType
❑ Estuary
O
❑ Ice Mass
❑ LakePond
❑ Playa
Raleigh
Reservoir
446
2
3
DSwampMarsh
i !CountyBoundary
�MunicipalBoundaries_polys
0.5 0.25 0
0.5
Miles
Scale: 1 inch = 0.5 miles
LOCATION MAP
Figure
Drawn by: CSC
SOIL PLUS
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Wake Forest, North Carolina
37
Date: April '17
Soil Plus Project # 200705.G10

61 Q
N
'' 1449
1563
16
I
S
1570
1556 0 �
1V4
O�, Z6g2 1402 I�1.3
5
ti
0
1888
Ar r s 8728 e Ho Pa
ti 00
158(
85 St to P WTP 1494 J
� 4U)
812
1710 �Ukti
2 � o��
ti3 1721 73 45 rbe Cree
I
901
ORANGE 720
24
1 9 89
78
19
32
1g74 DURHAM
z�7z
Ne 0 e 1718
20
61 N 84 ( n
p 1 Y
c m N
nN' I U
227 od Mobil me k to
d
2290 �A
2219 1880
172
illtop Mob e P k zzs> 1731 M
136_
N 1303
2G N N ti Bran h
2 1835 4 1331 1205 27�2
ti
�ti 2 ti
ti
Legend
0 Source 1��
oa � 904 N
Water 1^11 N 1146
Stream
Road
3 01
County Boundary �tio
1 0.5 0 1
0 Municipal Boundary �o �' Miles
1� NQ 38 2220
Scale: 1 inch = 1 miles SOURCE LOCATION MAP
Figure
Drawn by: DM SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: Durham, North Carolina 3 8
Date: June '19 Soil Plus Project # 200705.D10

1546
N
1547
W E
— s
Dry Creek
Lo 9 Branch °co
Chapel Ridge
0
1680
160
0
r�rl
<a
1346 *5 Uee4
O
�n
w CHATHAM
C-1
1
q N N
C-
00
159
s
1649
1648 2� � _
1564
�n
m
m
N �
N
.P
ti
ti9
ittsbor W
1523 871 <m
V
159 1658
2059
N 91
01
226 1967 1943
Pi sboro W TP P c
19,
N �
N 2159 N 6
0
o�
Legend IO
0 Source
C Water 1 Doti
eA
Stream
Road
County Boundary
0 1 0.5 0 1
Municipal Boundary
Miles
NN
Scale: 1 inch = 1 miles SOURCE LOCATION MAP
Figure
Drawn by: DM SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: Pittsboro, North Carolina 39
Date: June '19 Soil Plus Project # 200705.D10

N
2
0
N 22 2 3 of v
13
W E
43a�
4313
guar D Corn Jj
3
N
IV
74 1�
Q
2235
n
232
ti
298
5446
W
�
ac
N
0
216 2946
`O¢�
tih
1
� 4102
�n
B c o
WW
N
�
N
,d G
14
) 1 7 i J�
WAKE mm
25
N s� �
JJ
`� Q13$ 4
N'
55
h
r 30
n
6 4<
t o
w �
2671 �
4133
Ashle Hills
2
WWTP m
Rivervi
obile
m Park
1007
dal Estates M P WWTP m
2505
�Na1
Cross
ile states
m
t
creek2
�G
?
o
N�
2 7
52 3
J�
o
N
2634
S
9
2511
2 7
�s
416
vision WWTP
2508
n,¢
�V
ERIVER
ti
52(
J, V
euse
Legend
of
0 Source
�o
Water
Stream
IV
Road
= County Boundary
TOHNSTON
0 Municipal Boundary
0 1 0.5 0
N
1
N
5204
1
Miles
Scale: 1 inch = 1 miles
SOURCE LOCATION MAP
Figure
Drawn by: DM
S OIL
PLUS
GFI Land Application Permit (WQ000838)
Reviewed by:
Raleigh, North Carolina
40
Date: June '19
Soil Plus Project # 200705.D10

N
D
SR-1328
W E
n
S
s� o
SR-1428
4
s�®
Q
Toisriot W`I'P
9�
Sg1
o
SR- 136
C�,
S4`
SR-1184 Wilson
-1211
p
NC -
O
a
s
SR116
p�
® D Q 607
�wiggins Mill WTP �a
WILSON
R16 9 CP
SR-11 3 _
c
s� SR-1 Wilson WWTP
SR-1174 C,C
Us 264 Us-26¢
N -
SR-1(a95
- -169
IAA • -1697
c
S 3�1 SR-1615 SR-1614
0
ti SR 1616
Legend
LUCama _ o SR-1619 SR- 1623
Sources
® 115 9
IL Stream
SR-164s sR 172o i Stream 0ti5
r.� a s� Road
�8 Waterbody
Black Creek SR-1621 n Lake Pond
1 0.5 0 I 1 0 County Boundary
h o
MilsR_162s 0 Municipal Boundary
es �
�643 SR-16
Scale: 1 inch 1 miles SOURCE LOCATION MAP Figure
Drawn by: CSC GFI Land Application Permit (WQ0000838)
SOIL LUS Reviewed by: Wilson, North Carolina 41
Date: Aug'17 Soil Plus Project # 200705.A10

N
O
W E �d N
•`
4
1 06 S 1541 6
s �m� o s
1301
SSA C0�
<v
N
9 1 39 ¢
158 J 1
G�
G �
4 c
iv
teems 11 I6o2 ��� 161
1670 1673
1656 1660 e
1162di
ti T
667
1605 1606
m
m� ti 1601
GR AIWIRT .F,
F°V 1607
m
^�
1609 1
6
16 7.
I
7
G�
211
113
�
O�
16�6
1156
W
°
0-
1614
n
N
5�
N
(D
(D
^
I",7
b�
G).
Legend
6n
0 Source
Water
Stream
Road
1643
County Boundary
AiL
1 0.5 0 1
0 Municipal Boundary
��'
1618
W
s
Miles
Scale: 1 inch = 1 miles
SOIL PLUS
SOURCE LOCATION MAP
Figure
42
Drawn by: DM
GFI Land Application Permit (WQ0000838)
Reviewed by:
Oxford, North Carolina
Date: May'20
Soil Plus Project # 200705.D10

APPENDIX 2
2020 PERMIT MODIFICATION
Granville Farms, Inc. (WQ0000838)
Residual Source Certification Attachment
RS CA
Hominy Creek WWTP
Field Loading Calculations
Analytical

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: Granville Famrs, Inc.
Status
Code a
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current b
Proposed
N
City of Wilson
Hominy Creek WWTP
Wilson
NCO023906
-
2,000
N
City of Oxford
Oxford WWTP
Granville
NCO025054
-
500
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

State of North Carolina
DWR
Department of Environment and Natural Resources
Division of Water Resources
l?ivision of hater Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 11-13
L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: LomiM Creek WWTJ
2. Facility permit holder is: I[] Federal, 0 State, 0 Local Government, or 0 Private.
Facility permit issued by: IL Div. of Water Resources, Div. of Environmental Health,
or L Other (explain: _).
3. Facility contact person and title: Jimmy Pridgen, a�irerclamation Mang
Complete mailing address: PO Box 10
City:_ State: NC Zip: 27894-0010
Telephone number: M) 399-2491 E-mail address: jpridgengwilsonnc.org
4. Facility physical address: 3100 Old Stantonsburg Rd.
City: Wilson State: NC Zip: 27894-
Coordinates: Latitude: b° 41' 15.4" Longitude: 77° _5j' 40.3"
Datum: � Level of accuracy: Sub -Meter
Method of measurement: GIS
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: E MGD and facility average daily flow: 4.14 MGD
8. Average amount of residuals being generated at this facility = dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type volume of residuals treatment: conventional activated sludge with biological nutrient removal and tertiary
treatment
Type and volume of residuals storage (i.e., outside of residuals treatment units): 4 anaerobic digesters with a total volume
of 2,346,500, belt press with a covered 32,000 square ft storage pad holding approximately 216,000 cubic ft
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 0 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological 0 Non -Biological
FORM: RSC 11-13 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: _ erican Testing Technologies. Inc. and Date of analysis: _
Passed corrosivity test: ® yes ❑ no. pH: 6.8 s.u. (2 < pH < 12.5)
Passed ignitability test: 0 yes ❑ no. Flashpoint: - OF (> 140°F)
Passed reactivity test: Eyes pno. HCN: M mg/kg (<250) & H2S: M mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(mg/1)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
Arsenic
5.0
< 1.0
Hexachlorobenzene
0.13
< 0.05
Barium
100.0
< 10
Hexachloro-1,3-Butadiene
0.5
< 0.05
Benzene
0.5
< 0.1
Hexachloroethane
3.0
< 0.05
Cadmium
1.0
< 0.5
Lead
5.0
< 1.0
Carbon Tetrachloride
0.5
< 0.1
Lindane
0.4
< 0.005
Chlordane
0.03
< 0.005
Mercury
0.2
< 0.02
Chlorobenzene
100.0
< 0.1
Methoxychlor
10.0
< 0.1
Chloroform
6.0
< 0.1
Methyl Ethyl Ketone
200.0
< 2.0
Chromium
5.0
< 1.0
Nitrobenzene
2.0
< 0.05
m-Cresol
200.0
< 0.5
Pentachlorophenol
100.0
< 0.5
o-Cresol
200.0
< 0.5
Pyridine
5.0
< 0.05
p-Cresol
200.0
< 0.5
Selenium
1.0
< 0.5
Cresol
200.0
< 0.5
Silver
5.0
< 1.0
2,4-D
10.0
< 1.0
Tetrachloroethylene
0.7
< 0.1
1,4-Dichlorobenzene
7.5
< 0.05
Toxaphene
0.5
< 0.1
112-Dichloroethane
0.5
< 0.1
Trichloroethylene
0.5
< 0.1
1,1-Dichloroethylene
0.7
< 0.1
2,4,5-Trichlorophenol
400.0
< 0.5
2,4-Dinitrotoluene
0.13
< 0.05
2,4,6-Trichloropheno1
2.0
< 0.5
Endrin
0.02
< 0.005
2,4,5-TP (Silvex)
1.0
< 1.0
Heptachlor and its Hydroxide
0.008
< 0.005
Vinyl Chloride
0.2
< 0.2

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Meritech Inc. and Date of analysis: -
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mg1kg)
Arsenic
75
41
<1.92
Cadmium
85
39
0.498
Copper
4,300
1,500
195
Lead
840
300
16.6
Mercury
57
17
0.038
Molybdenum
75
n/a
4.56
Nickel
420
420
16.1
Selenium
100
100
<1.92
Zinc
7,500
2,800
835
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: = and Date of analysis: =
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
M > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: a %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: 14eritech, Inc. and Date of analysis: 1/16/2020
Parameter
Result
(mg1kg)
Aluminum
6,780
Ammonia -Nitrogen
5,900
Calcium
12,900
Magnesium
1,540
Nitrate -Nitrite Nitrogen
<38.3
pH (Standard Unit)
5.7
Phosphorus
21,800
Potassium
927
Sodium
759
Total Kjeldahl Nitrogen
12,200
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 0.86
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 20 %. This
rate is a (check one): JW default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: ia
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (11) Year PAN
Five -Year
Maximum Adjusted PAN
(mg/kg)
(mg/kg)
Surface
4,249
5,655
Injection/Incorporation
7,199
8,083
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: None Kno

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
C1 A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
id A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
14 Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
EJ Alternative 2 [15A NCAC 02T.I 106(b)(3)(13)] - Alkaline Treatment.
Alternative 3 [15A NCAC 02T. 1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
E] Alternative 4 [15A NCAC 02T. 1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: composting, A heat drying, 71 heat treatment,
thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, I
air drying, ❑ anaerobic digestion,
El composting, or lime stabilization.
c. For Surface Disposal:
rl Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
J Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
J Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
J Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
El Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
E] Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
E] Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
El Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
E] Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
E] Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
E] Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
El Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
El Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
q Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
id Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.

AGMAN FIELD LOADING ESTIMATES
Facility Hominy Creek WRF
Sampling Date 1/16/2020
Solids 26.1
Mineralization Rate 0.20
Wet Tonsper DT 3.83
pH 5.7
Sodium Absorpotion 0.86 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 12,200
lbs./WT 6.37
Ammonia Nitrogen (mg/Kg) 5,900.00
lbs./WT 3.08
Nitrate -Nitrite (mg/Kg) 38.80
lbs./WT 0.02
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 4,249
lbs./WT 2.22
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 7,199
lbs./WT 3.76
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
Potassium lbs./WT
0.48
Phosphorus lbs./WT
11.38
Calcium lbs./WT
6.73
Magnesium lbs./WT
0.80
Manganese lbs./WT
0.55
Sulfur lbs./WT
16.70
Molybdenum lbs./WT
0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
1.92
Cadmium (mg/Kg)
0.50
Copper (mg/Kg)
195.00
Lead (mg/Kg)
16.60
Mercury (mg/Kg)
0.04
Nickel (mg/Kg)
16.10
Selenium (mg/Kg)
1.92
Zinc (mg/Kg)
835.00
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
12,200
4,249 8.50
7,951
12,200
7,199 14.40
5,001
7,951
795 1.59
7,156
5,001
500 1.00
4,501
7,156
358 0.72
6,798
4,501
225 0.45
4,276
6,798
170 0.34
6,628
4,276
107 0.21
4,169
6,628
83 0.17
6,545
4,169
52 0.10
4,117
Arsenic lbs./WT
0.00
Cadmium lbs./WT
0.00
Copper lbs./WT
0.10
Lead lbs./WT
0.01
Mercury lbs./WT
0.00
Nickel lbs./WT
0.01
Selenium lbs./WT
0.00
Zinc lbs./WT
0.27
Equations
1st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 5,655 11.31
Total 8,083 16.17

Meritech, Inc.
z ,� Environmental Laboratory
Laboratory Certification No.165
Contact: Andrew Mlot
Client: City of Wilson
3100 Old Stantonsburg Rd
Wilson, NC 27893
Page 2
Revised Date. 313012020
Report Date: 1/30/2020
NPDES #: NC0023906
Project: Hominy Creek Class B Sludge
Date Sample Rcvd: 1/16/2020
Meritech Work Order #
011620223 Sample: Hominy Creek Class B (A-437-7) Grab
1/16/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
22.9 %
1/21/20
0-100 %
SM 254013
Fecal Coliform (Sludge)
127,857 col/g dry wt
1/16/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
011620224 Sample: Hominy Creek Class B (A-437-8) Grab
1/16/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
26.1 %
1/17/20
0-100 %
SM 2540B
Chloride
<192 mg/kg
1/27/20
192 mg/kg
SM 4500 Cl B
Ammonia, Nitrogen
5900 mg/kg
1/27/20
0.1 mg/kg
EPA 350.1
TKN
12,200 mg/kg
1/23/20
0.20 mg/kg
EPA 351.1
Nitrate, Nitrogen
<38.3 mg/kg
1/22/20
38.3 mg/kg
EPA 353.2
Nitrate/Nitrite, Nitrogen
<38.3 mg/kg
1122120
38.3 mg/kg
EPA 353.2
Aluminum, total
6,780 mg/kg
1/24/20
0.050 mg/kg
EPA 200.7
Arsenic, total
<1.92 mg/kg
1/24/20
1.92 mg/kg
EPA 200.7
Cadmium, total
0.498 mg/kg
1/24/20
0.200 mg/kg
EPA 200.7
Calcium, total
12,900 mg/kg
1/24/20
0.100 mg/kg
EPA 200.7
Chromium, total
30.5 mg/kg
1/24/20
0.005 mg/kg
EPA 200.7
Copper, total
195 mg/kg
1/24/20
0.002 mg/kg
EPA 200.7
Iron, total
265,000 mg/kg
1/24/20
0.025 mg/kg
EPA 200.7
Lead, total
16.6 mg/kg
1/24/20
0.010 mg/kg
EPA 200.7
Magnesium, total
1,540 mg/kg
1/24/20
0.005 mg/kg
EPA 200.7
Manganese, total
1,050 mg/kg
1/24/20
0.005 mg/kg
EPA 200.7
Mercury, total
0.038 mg/kg
1/21/20
0.02 mg/kg
EPA 245.1
Molybdenum, total
4.56 mg/kg
1/24/20
0.500 mg/kg
EPA 200.7
Nickel, total
16.1 mg/kg
1/24/20
0.010 mg/kg
EPA 200.7
Phosphorus, total
21,800 mg/kg
1/24/20
0.020 mg/kg
EPA 200.7
Potassium, total
927 mg/kg
1/24/20
1.00 mg/kg
EPA 200.7
Selenium, total
<1.92 mg/kg
1/24/20
1.92 mg/kg
EPA 200.7
Sodium, total
759 mg/kg
1/24/20
0.100 mg/kg
EPA 200.7
Sulfur, total*
32,000 mg/kg
1/29/20
0.1 mg/kg
EPA 200.7
Zinc, total
835 mg/kg
1/24/20
0.010 mg/kg
EPA 200.7
Cyanide, total
<1.92 mg/kg
1/22/20
1.92 mg/kg
EPA 335.4
pH
5.7 S.U.
1/17/20
1.0 - 14.0 S.U.
SM 4500-HB
* Results not for regulatory
purposes
Nitrate/Nitrite, Nitrogen was added to the report on 3130120
I hereby certify that I have
reviewed and approve these data.1.1kD
ar'
(J
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5-9-2016 Chain of Custody Record (COC)
NPDES#: NCO023906
M E R I TE C H, INC.
Client: City of Wilson Phone:_ 252-399-2491
A'
Address:_ 3100 Old Stantonsburg Rd Fax: [phone]
ENVIRONMENTAL LABORATORIES
Wilson, North Carolina Email:_ [e-mail]
al• 642 Tamco Rd. Phone: [phone]
`
Project:_ Hominy Creek Class B Sludge
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:_ Andrew Mlot Turn Around Time*
WWW.ITIerlteCillabS.COm
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Email (preferred), Fax, Mail st ) 3Das rs
Sampling Dates & Times
Person Taking Sample (Si �iCnt)%��� .
(9 1 Lab Use Only
Sample Location and/or ID #
Date Start Time Date End
Comp? #of Test() Req u i red on Ice? pH OK?
Time _Crab?
Cont.
�s / No Cl OK?
Hominy Creek Class B (ia•y3a-q I L —�
G 1 % Total Solids & Fecal ',
Hominy Creek Class B (A-4I 1-1) I it LoL+ I _�` �=
G 1 % Total Solids & Fecal <) 06
Hominy Creek Class B (A-t0l•)) 11�Iva-o
G 1 % Total Solids & Fecal
Hominy Creek Class B (}j ul) l'�� I �� tp} r ,�!
G 1 % Total Solids & Fecal C
Hominy Creek Class B (AAO-f) I1101=
Ilo Lvtu
a ^ r�
/ G 1 Total Solids &Fecal d
Hominy Creek Class B (A•N3l b) r 1 vt 1 1 0 � _ �
G 1 % Total Solids & Fecal
Hominy Creek Class B (A• ""'?) tto fill _--
G 1 %Total Solids & Fecal
f
Hominy Creek Class B (- �i��•�+) I 1 W ) 3 !_
o a o i s ois ureo a fe aiogen, osp o us an
G 3
Potassium, Ph, Cn-, CI
SLZ: Basic SL3 plus Sulfur, Calcium, Magnesium, Sodium, Iron, AlumlnuW,
Manganese, Copper, and Zinc,
Temperature Upon Receipt:
503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, t, ,
Nickel, Selenium, Copper, and Zinc Nitrogen Series: /Tl/
Total Kjeldahl, Ammonium, Nitrate & Organic Nirtogen
Method of *** Dechlorination (<0.5 m) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Comments: Also send a copy of the result to : Laura Pruitt
Shipment:
Email: [e-mail] Compositor #
❑ UPS
❑ Fed Ex Are these res 4ts for regulatory purposes? Yes ❑
❑ Relinqui ed
Jug #
No ❑ Report results in: mg/L ❑ mg/kg ❑ ug/L ❑
j ate:
Hand Calivery Timei
Received b p Time: //
Other
Relinquis at Time:
oZ .SS
Received b y Date: Time:
e inquished by: ate: Time:
Received by Lab; , n
ake:/*�� Time: )

Waypoint�4'
ANALYTICAL
02/12/2018 14:50:18
Export Batch Report
Export Batch Id : 1995EXP
7621 Whitepine Road, Richmond, VA 23237
Main 04-743-9401 ° Fax [phone]
www.wayoi nta rra lytica l.com
Created' 2/ 12/2018 14: 50: 04
Computer: RVADESK001
User: Morgan Tichacek
Page 1 of 1
mer can Testa.^
To.-9
echolo ie'
9 s
From:
Waypoint Analytical Virginia, Inc.
y , .
1350 Hone Ave.
7621 Whitepine Rd.
Akron, OH 44310
Richmond, VA 23237
330-634-9906
804-743-9401
Report No
Sample Date
Rush Lab No
Method No
Fee Code Description
18-043-0205
02/08/2018 11:18
58572
ASTM D93-80
Ignitabii0/Flash point (ASTM
D93-80)
18-043-0205
02/08/2018 11:18
58572
SW-7.3.3
Cyanide Reactivity
18-043-0205
02/08/2018 11:18
58572
SW-7.3.4
Sulfide Reactivity
18-043-0205
02/06/2018 11:18
58572
SW-9045C
CorrosVty (pH)
18-043-0205
02/08/2018 11:18
58573
SW-1311
TCLP Extraction Method 1311
18-043-0205
02/08/2018 11:18
58573
SW-1311 (ZHE)
TCLP Extraction Method 1311
18-043-0205
02/08/2018 11:18
58573
SW-6010C (TCLP)
TCLP Metals (8 RCRA Metals)
18-043-0205
02/08/2018 11:18
58573
SW-7470A (TCLP)
TCLP Metals (8 RCRA Metals)
18-043-0205
02/08/2018 11:18
58573
SW-8081A (TCLP)
TCLP Pesticides (Pest)
18-043-0205
02/08/2018 11:18
58573
SW-8151A (TCLP)
TCLP Herbicides (Herbs)
18-043-0205
02/08/2018 11:18
58573
SW-82608 (TCLP)
TCLP VOCs (Volatiles)
18-043-0205
02/08/2018 11:16
58573
SVV-8270C (TCLP)
-1 CLP'SVOts (BNAs)
18-043-0206
02/08/2018 17:23
58574
ASTM D913-80
Ignitability/Flashpoint (ASTM
D93-80)
18-043-0206
02/08/2018 12:23
58574
SW-7.3.31
Cyanide Reactivity
18-0,13-0206
02/08/2018 12:23
58574
SW-7.3.4
Sulfide Reactivity
18-043-0206
02/08/2018 12:23
58574
SW-9045L
Carrosivity (pH)
I8-043-0206
02/08/2018 12:23
58575
SW-1311
TCLP Extraction Method 1311
18-043-0206
02/08/2018 12:23
58575
SW-1311 (ZHE)
TCLP Extraction Method 1311
18-043-0206
02/08/2018 12:23
58575
SW-6010C (TCLP)
TCLP Metals (8 RCRA Metals)
18-043-0206
02/08/2018 12:23
58575
SW-7470A (TCLP)
TCLP Metals (8 RCRA Metals)
18-043-0206
02/08/2018 12.23
58575
SW-8081A (TCLP)
TCLP Pesticides (Pest)
18-043-0206
02/08/2018 12:23
58575
SW-8151A (TCLP)
TCLP Herbicides (Herbs)
18-043-0206
02/08/2018 12:23
58575
SW-8260B (TCLP)
TCLP VOCs (Volatiles)
18-043-0206
02/08/2018 12:23
58575
SW-8270C (TCLP)
TCLP SVOCs(BNAs)
Sampled By
Method of Shipment
Blank / Cooler Temp.
C.
Remarks
Rel'
wished By (sign)
Date / Time
Received By (sign)
Date / Time
Relinquished By (sig
Date / Time
Re�eiv d y (sign)
59
Date / Time p
3l® r

ToArtt eracan TestirtgTechncslogies
1350 Hone Ave.
Akron, OH 44310
330-634-9906
Report No Sample Date Rush Lab No Method No
18-039-0203 02/07/2018 11:57 58513 ASTM D93-80
18-039-0203
02/07/2018
11:57
58513
SW-7.3.3
18-039-0203
02/07/2018
11:57
58513
SW-7.3.4
18-039-0203
02/07/2018
11:57
S8513
SW-9045C
18-039-0203
02/07/2018
11:57
58514
SW-1311
18-039-0203
02/07/2018
11:57
58514
SW-1311 (ZHE)
18-039-0203
02/07/2018
11:57
58514
SW-6010C (TCLP)
18-039-0203
02/07/2018
11:57
58514
SW-7470A (TCLP)
18-039-0203
02/07/2D18
11:57
58514
SW-8081A (TCLP)
18-039-0203
02/07/2018
11:57
58514
SW-8151A (TCLP)
18-039-0203
02/07/2018
11:57
58514
SW-8260B(TCLP)
18-039-02.03
02107/2018.11:57
58514
SW-8270C(TCLP)
Sy I Method of Shipment
Relinquished By (sign) x Date / Time
By (sjpn) I Date / Time
rim
7621 Whitepine mead, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Page 1 of 1
,Created:
2/8/2018 14:16: 56
Computer:
RVADESK001
User:
Morgan Tichacek
From;
Waypoint Analytical Virginia, Inc.
7621 Whitepine Rd.
Richmond, VA 23237
804-743-9401
Fee Code Description
Ignitability/Flashpcint (ASTM
D93-80)
Cyanide Reactivity
Sulfide Reactivity
Corrosivity (pH)
TCLP Extraction Method 1311
TCLP Extraction Method 1311
TCLP Metals (8 RCRA Metals)
TCLP Metals (8 RCRA Metals)
TCLP Pesticides (Pest)
TCLP Herbicides (Herbs)
TCLP VOCs (Volatiles)
TCLP SVOCs (Bf As)
Blank / Cooler Temp.
Received By (sign)

•
02/28/2018 American Testing Technologies, ]no,
WayPoint Analytical
7621 Whitepine Rd
Richmond, VA 23237
Report No.: 021318-02 04
Enclosed are the results of the sample(s) submitted to our laboratory on 02/13/2018.
All analyses were performed according to our laboratory's quality assurance program.
All sample results are reported on an "as -received" wet basis unless otherwise noted. The
test results meet requirements of the NELAP standards for methods listed on the
laboratory's current fields of accreditation (EPA 8260, 8082, 8081, 8151, 8270, 6010,
6020, 1010, 9045, 7471, 1010, 1311, 150.1, 200.7, 200.8, and 245.1) except as noted.
Results apply only to the items submitted to the laboratory for analysis. Pursuant to
NELAP, this report may not be reproduced except in fall, and With written approval from
the laboratory.
If you have any questions please contact the laboratory manager at 330-634-9906 or via
email at sam americantestingtechnologies.com
nager
ATT is NELAP-accredited by the State of Florida, #E871084. Other state accreditation include: North
Carolina, #670; Pennsylvania #68-05167; West Virginia, #372.
The results relate only to the items tested. ATT shall have no liability to the client or client's customer with
respect to decisions or recommendations made, actions taken or courses of conduct implemented by either
the client or the client's customer as a result of or based upon the Test Results. In no event shall ATT's
liability with respect to the Test Results exceed the amount paid to ATT by the client therefor.
ToU Free: 877-634-9906
1360 Home Avenue Akron, OH 443:10
Phon f330
Page 1 of 19
e• ) 634 99�D Fax: (4_60) 634-9937 Website: www.AmericanTesting echnologies.com

American Testing Technologies, Inc.
WayPoint Analytical
7621 Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/08/2018
Time Collected: 11:18
Client ID #: 58573
Laboratory ID #: 021318-02
Date of Analysis: 02/15/2018
Certificate of Analysis
Metals-TCLP (EPA 1311)
Parameter
Results
Units
Regulatory
Method
Limits
Number
Arsenic
<1.0
mg/L
5.0
6010C
Barium
<10
mg/L
100.0
6010C
Cadmium
<0.5
mg/L
1.0
6010C
Chromium
<1.0
mg/L
5.0
6010C
Lead
<1.0
mg/L
5.0
6010C
Mercury
<0.02
mg/L
0.2
7470A
Selenium
<0.5
mg/L
1.0
6010C
Silver
<1.0
mg/L
5.0
6010C
6
1350 Horne Avenue Akron, OH 44310 Page 2 of 19
TOO Free: 877-634-9906 Phone: [phone] Fax. [phone] Website:www,ArnericanTestingTechnologles.corn

41D
American Testing Technologies, Inc.
WayPoint Analytical
7621 Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/08/2018
Time Collected: 11:18
Client ID #: 58573
Laboratory ID #: 021318-02
Date of Analysis: 02/16/2018
Certificate of Analysis
Volatiles-TCLP (EPA 1311)
Parameter
Results
Units
Regulatory
Method
Limits
Number
Benzene
<0.1
mg/L
0.5
8260B
Carbon tetrachloride
<0.1
mg/L
0.5
8260B
Chlorobexrzene
<0.1
mg/L
100
8260B
Chloroform
<0.1
mg/L
6.0
8260E
1,2-Dichloroethane
<0.1
mg/L
0.5
8260B
1,1-Dichloroethene
<0.1
mg/L
0.7
8260B
Methyl ethyl ketone
<2.0
mg/L
200
8260B
Tetrachloroethene
<0.1
mg/L
0.7
8260B
Trichloroethene
<0.1
mg/L
0.5
8260B
Vinyl chloride
<0.2
mg/L
0.2
8260B
1350 Horne Avenue Akron, OH 44310 Page 3of19
Toil Free, 877-634-9906 Phone: [phone] Fax: [phone] Website: www.Ames'icanTestingTechnologies.com

�i
1 7r;
Amer can Testing Technologies, Inc.
WayPoint Analytical
7621Wbitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/NI8
Date Collected: 02/08/2018
Time Collected. 11:18
Client ID #: 58573
Laboratory ID #: 021318-02
Date of Analysis: 02/17/2018
Certificate of Analysis
BNA TCLP (EPA 1311)
Parameter
Results
Units
Regulatory
Method
Limits
Number
1,4-Dichlorobenzene
<0.05
mg/L
7.5
8270C
24-Dinitrotoluene
<0.05
mg/L
0.13
8270C
Hexachlorobenzene
<0.05
mg/L
0.13
8270C
Hexachlorobutadiene
<0.05
mg/L
0.5
8270C
Hexachloroethane
<0.05
mg/L
3.0
8270C
Nitrobenzene
<0.05
mg/L
2.0
8270C
Pyridine
<0.05
mg/L
5.0
8270C
o-Cresol
<0.5
mg/L
200
8270C
m,p-Cresol
<0.5
mg/L
200
8270C
Pentachlorophenol
<0.5
mg/L
100
8270C
2,4,5-Trichlorophenol
<0.5
mg/L
400
8270C
2,4,6-Trichlorophenol
<0.5
mg/L
2.0
8270C
reviewed by:
Manager
Page 4of19
1360 Home Avenue Akron, 0H 44310
Toll Free: 877-634-9906 Phone: [phone] Fax: [phone] Website: www.ArnericanTestingTechnoiogies.com

s
AmeEican Testing Technologies, Inc.
WayPoint Analytical
7621 Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/08/2018
Time Collected: 11:18
Client ID ##: 58573
Laboratory ID ##. 021318-02
Date of Analysis: 02/17/2018
Certificate of Analysis
Pesticides-TCLP (EPA 1311)
Parameter
Results
Units
Regulatory
Method
Limits
Number
Chlordane
<0.005
mg/L
0.03
8081B
Endrin
<0.005
mg/L
0.02
8081E
Heptachlor
<0.005
mg/L,
0.008
808IB
Heptachlor epoxide
<0.005
mg/L
0.008
S081B
Lindane
<0.005
mg/L
0.4
8081B
Methoxychlor
<0.1
mg/L
10.0
8081B
Toxaphene
<0.I
mg/L
0.5
808113
1350 Horne Avenge Akron, 0H 44310 Page 5of19
Tall Free: 377-634-9906 Phone. [phone] Fax: [phone] Website: wvvw,AmericarsTestingechnologies.com

•FIFWj
Amer4can Testing Technologies, Inc.
WayPoint Analytical
7621 Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/08/2018
Time Collected: 11:18
Client ID #: 58573
Laboratory ID #: 021318-02
Date of Analysis: 02/27/2018
Certificate of Analysis
Herbicides-TCLP (EPA 1311)
Parameter Results Units Regulatory Methods
Limits Number
2,4-D <1.0 mg/L 10.0 8151A
2,4,5-TP (Silvex) <1.0 mg/L 1.0 8151A
1350 Hume Avenue Akron, OH 44310 Page 6af19
Toil Free: 877-634-9906 Phone: [phone] Fax: [phone] ►hlebsite: www.ArnericanTestingTechnologies.com

WayPoint Analytical
7621Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/08/2018
Time Collected: 11:18
Client ID #: 58572
LaboratoryID #: 021318-02
Q �dd
Arnerican 'besting Technologies, Inc.
Certificate of Analysis
Parameter
Results
Units
Method
Date of
Number
Analysis
Reactive Cyanides
<0.5
mg/kg
7.3.3.2
02/23/2018
Reactive Sulfides
<25
mg/kg
7.3.4.1
02/23/2018
pH (Lab)
3.29
S.U.
9045D .
02/13/2018
Flash point
>140
°r
1010A
02/16/2018
1350 Borne Avenue Akron, OH 44320 Page 7 of 19
Toil Free: 877-634-9906 Phone: [phone] Fax: [phone] Website: www.ArnericarTestingTechnologies.com

•
American Testing Technologies, Inc.
WayPoint Analytical
7621 Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/08/2018
Time Collected: 12:23
Client ID #: 58575
Laboratory ID #: 021318-03
Date of Analysis: 02/15/2018
Certificate of Anal sis
Metals-TCLP (EPA 1311)
Parameter
Results
Units
Regulatory
Method
Limits
Number
Arsenic
<1.0
mg/L
5.0
6010C
Barium
<10
mg/L
100.0
6010C
Cadmium
<0.5
mg/L
1.0
6010C
Chromium
<1.0
mg/L
5.0
6010C
Lead
<1.0
mg/L
5.0
6010C
Mercury
<0.02
zng/L
0.2
7470A
Selenium
<0.5
mg/L
1.0
6010C
Silver
<1.0
mg/L
5.0
6010C
135d3 Home Avenue Akron, Oki 44310 Page 8 of 19
Toll Free: 877-634-9906 Phone: [phone] Fax: [phone] Website: www.AmericanTeFtingTechnologies.com

•
American Testing Technologies, Inc.
WayPoint Analytical
7621 Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/08/2018
Time Collected: 12:23
Client ID #: 58575
Laboratory ID #: 021318-03
Date of Analysis: 02/16/2018
Certificate of Analysis
Volatiles-TCLP (EPA 1311)
Parameter
Results
Units
Regulatory
Method
Limits
Number
Benzene
<0.1
mg/L
0.5
8260B
Carbon tetrachloride
<0.1
mg/L
0.5
8260B
Chlorobenzene
<0.1
mg/L
100
8260B
Chloroform
<0.1
mg/L
6.0
8260B
1,2-Dichloroethane
<0.1
mg/L
0.5
8260B
1,1-Dichloroethene
<0.1
mg/L
0.7
8260B
Methyl ethyl ketone
<2.0
mg/L
200
8260B
Tetrachloroethene
<0.1
mg/L
0.7
8260B
Trichloroethene
<0.1
mg/L
0.5
8260B
Vinyl chloride
<0.2
mg/L
0.2
8260B
reviewed by:
Manager
1350 Home Avenue Akron, OH 44310 Page 9of19
Toil Free: 977-634-9906 Phone: [phone] Fax: [phone]d',febsite:ivww.ArnericanTestingTechnoiogies.com

Ob
American Testing Technologies, Inc.
WayPoint Analytical
7621 Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018.
Date Collected: 02/08/2018
Time Collected: 12:23
Client ID #: 58575
Laboratory ID #: 021318-03
Date of Analysis: 02/17/2018
Certificate of Analysis
BNA-TCLP (EPA 1311)
Parameter
Results
Units
Regulatory
Method
Limits
Number
1,4-Dichlorobenzene
<0.05
mg/L
7.5
8270C
2,4-Dinitrotoluene
<0.05
mg/L
0.13
8270C
Hexachlorobenzene
<0.05
mg/L
0.13
8270C
Hexachlorobutadiene
<0.05
mg/L
0.5
8270C
Hexachloroethane
<0.05
mg/L
3.0
8270C
Nitrobenzene
<0A5
mg/L
2.0
8270C
Pyridine
<0.05
mg/L
5.0
8270C
o-Cresol
<0.5
mg/L
200
8270C
m,p-Cresol
<0.5
mg/L
200
8270C
Pentachlorophenol
<0.5
mg/L
100
8270C
2,4,5-Trichlorophenol
<0.5
mg/L
400
8270C
2,4,6-Trichlorophenol
<0.5
mg/L
2.0
8270C
1350 Horne Avenue Akron. OH 44310 Page 10 of 19
Tall Free. 877-634-9906 Phone: [phone] Fax: [phone] Website: wmv.AmerlcanTestingTechnologies.corn

•
AFT
American Testing Technofogles, Inc.
WayPoint Analytical
7621 Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/08/2018
Time Collected: 12:23
Client ID #: 58575
Laboratory ID #: 021318-03
Date of Analysis: 02/17/2018
CertMeate of Analysis
Pesticides-TCLP (EPA 1311)
Parameter Results Units Regulatory Method
Limits Number
Chlordane
<0.005
mg/L
0.03
8081B
Endrin
<0.005
mg/L
0.02
8081B
Heptachlor
<0.005
mg/L
0.008
80$1B
Heptachlor epoxide
<0.005
mg/L
0.008
8081E
Lindane
<0r005
mg/L
0.4
8081B
Methoxychlor
<0.1
mg/L
10.0
8081B
Toxaphene
<0.1
mg/L
0.5
8081B
1360 Dome Avenue Akron, OH 44310 Page 11 of 19
Toil Free: 877-634-9906 Phone: [phone] Fax: [phone] Website: www, AmericanTesting echnologies.com

WayPoint Analytical
7621Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/08/2018
Time Collected: 12:23
Client ID #: 58575
LaboratoryID #: 021318-03
Date of Analysis: 02/27/2018
Herbicides-TCLP (EPA 1311)
Parameter Results
2,4-D <1.0
2,4,5-TP (Silvex) <1.0
•
American Testing Technologies, Inc.
Certificate of Analysis
Units
Regulatory
Method
Limits
Number
mg/L
10.0
8151A
mg/L
1.0
8151A
1350 Horne Avenue Akron, OH 44310 Page 12ofI9
Toll Free: 877-634,9906 Phone: [phone] Fax: [phone] Website: vuww.ArnericanTestingTechnologies.com

WayPoint Analytical
7621Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/08/2018
Time Collected: 12:23
Client ID #: 58574
Laboratory ID #: 021318-03
a
American Testing Technologies, Inc.
Certificate of Analysis
Parameter
Results
Units
Method
Date of
Number
Analysis
Reactive Cyanides
<0.5
mg/kg
7.3.3.2
02/23/2018
Reactive Sulfides
<25
mg/kg
7.3.4.1
02/23/2018
p14 (Lab)
3.68
S.U.
9045D
02/13/2018
Flash point
>140
OF
1010A
02/16/2018
Toll Free. 877-634-9906
1350 Horne Avenue Akcron, OH 44310 Page 13 of 19
Phone: [phone] Fax: [phone] Website: www.AmericanTes€irlgTechnologies.com

qiD
American Testing Technologies, Inc.
WayPoint Analytical
7621 Whitepine Rd
Richmond, VA 23237
Date Received. 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/08/2018
Time Collected: 12:23
Client ID #: 58575
Laboratory ID #: 0213 18-03
Date of Analysis: 02/15/2018
Certificate of Analysis
Metals-TCLP (EPA 1311)
Parameter
Results
Units
Regulatory
Method
Limits
Number
Arsenic
<1.0
mg/L
5.0
6010C
Barium
<10
mg/L
100.0
6010C
Cadmium
<0.5
mg/L
1.0
6010C
Chromium
c1.0
mg/L
5.0
6010C
Lead
<1.0
mg/L
5.0
6010C
Mercury
c0.02
mg/L
0.2
7470A
Selenium
c0.5
mg/L
1.0
6010C
Silver
<1.0
mg/L
5.0
6010C
reviewed by:
Manager
135O Horne Avenue Akron, OH 44310 Page 14 of 19
Toil Free, 377-634-9906 Phone: [phone] Fax: [phone] Wehsite: www .AmericariTestindTechnologies.corn

American Testing Testing Technologies, Inc.
WayPoint Analytical
7621Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/07/2018
Time Collected: 11:57
Client ID #: 58514
Laboratory ID #: 021318-04
Date of Analysis: 02/16/2018
Certificate of Analysis
Voladles-TCLP (EPA 1311)
Parameter
Results
Units
Regulatory
Method
Limits
Number
Benzene
<0.1
mg/L
0.5
8260B
Carbon tetrachloride
<0.1
mg/L
0.5
8260B
Chlorobenzene
<0.1
mg/L
100
826013
Chloroform
<0.1
mg/L
6.0
8260B
1,2-Dichloroedme
<0.1
mg/L
0.5
8260E
1,1-Dichloroethene
<0.1
mg/L
0.7
8260B
Methyl ethyl ketone
<2.0
mg/L
200
8260B
Tetrachloroethene
<0,1
mg/L
0.7
8260B
Trichloroethene
<0.1
mg/L
0.5
8260B
Vinyl chloride
<0.2
mg/L
0.2
826013
Page 15 of 19
1350 Home Avenue Akron, OH 44310
Toll Free: 877-634-9906 Phone: [phone] Fax. [phone] Website: www.AmericaniTestingTechnoiogies.com

WayPoint Analytical
7621 Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/07/2018
Time Collected: 11:57
Client ID #: 58514
Laboratory ID #: 021318-04
Date of Analysis: 02/17/2018
Certificate of Analvsis
BNA-TCLP (EPA 1311)
Parameter
Results
Ur is
Regulatory
Method
Limits
Number
1,4-Dichlorobenzene
<0.05
mg/L
7.5
8270C
24-Dinitrotoluene
<0.05
mg/L
0.13
8270C
Hexachlorobenzene
<0.05
mg/L
0.13
8270C
Hexachlorobutadiene
<0.05
mg/L
0.5
8270C
Hexachloroethane
<0.05
mg/L
3.0
8270C
Nitrobenzene
<0.05
mg/L
2.0
8270C
Pyridine
<0.05
mg/L
5.0
8270C
o-Cresol
<0.5
mg/L
200
8270C
m,p-Cresol
<0.5
mg/L
200
8270C
Pentachlorophenol
<0.5
mg/L
100
8270C
2,4,5-Trichlorophenol
<0.5
mg/L
400
8270C
2,4,6-Trichlorophenol
<0.5
mg/L
2.0
8270C
1350 kiorne Avenue Akron, ©H 44310 Page Ib of 19
Toll Free: 877-634-9906 Phone: [phone] Fax. [phone] Website: tivmv.AmericenTestinglechnologies.com

43D
AmerficOn Testing Technologies, Inc.
WayPoint Analytical
7621 Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/07/2018
Time Collected: 11:57
Client ID #: 58514
Laboratory ID #: 021318-04
Date of Analysis: 02/17/2018
Certificate of Analysis
Pesticides-TCLP (EPA 1311)
Parameter Results Units Regulatory Method
Limits Number
Chlordane
<0.005
mg/L
0.03
8081B
Endrin
<0.005
mg/L
0.02
8081B
Heptachlor
<0.005
mg/L
0.008
8081B
Heptachlor epoxide
<0.005
mg/L
0.008
8081B
Lindane
<0.005
mg/L
0.4
8081B
Methoxychlor
<0.1
mg/L
10.0
8081E
Toxaphene
<0.1
mg/L
U
8081B
reviewed by:
Manager
Page 17of19
1350 Home Avenue Akron, OH 44310
Toil Free: 877-634-9906 Phone: [phone] Fax: [phone] Wehsite: w v.AmericanTestingTechnoiogies.corn

A
American Testing Technologies, Inc.
WayPoint Analytical
7621Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/07/2018
Time Collected: 11:57
Client ID #: 58514
Laboratory 1D #: 021318-04
Date of Analysis: 02/27/2018
Certificate of Analysis
Herbicides-TCLP (EPA 1311)
Parameter Results Units Regulatory Method
Limits Number
2,4-D <1.0 mg/L 10.0 8151A
2,4,5-TP (Silvex) Q.0 mg/L 1.0 8151A
reviewed by:
Manager
1350 home Avenue Akron, OH 44310 Page 18 of 19
Toll Free, 877-634-9906 Phone. [phone] Fax: [phone] Website: www.AmericenTestingTechnologies.com

WayPoint Analytical
7621 Whitepine Rd
Richmond, VA 23237
Date Received: 02/13/2018
Date Reported: 02/28/2018
Date Collected: 02/07/2018
Time Collected.: 11:57
Client ID #: 58513
Laboratory ID #: 021318-04
4ip
American Testing Technologies, Inc.
Certificate of Analysis
Parameter
Results
Units
Method
Date of
Number
Analysis
Reactive Cyanides
<0.5
ing/kg
7.3.3.2
02/23/2018
Reactive Sulfides
<25
m9/k9
7.3.4.1
02/23/2018
pH (Lab)
6.80
's.u.
9045D
02/13/2018
Plash point
>140
OF
1010A
02/16/2018
1350 Florae Avenue Akron, Off 44310 Page 19of19
Toff Free. 877-634-9906 Phone: [phone] Fax: [phone] Website: www.ArnericarTestingTechnologies.com

Waypointo
ANALYTICAL
02/08/2018 14:17:11
Export Batch Report
Export Batch Id : 1987EXP
To: American Testing Technologies
1350 Hone Ave.
Akron, OH 44310
330-634-9906
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Page 1 of 1
Created: 2/ 8/ 2 018 14 :16: 56
Computer: RVADESK001
User: Morgan Tichacek
From: Waypoint Analytical Virginia, Inc.
7621 Whitepine Rd.
Richmond, VA 23237
804-743-9401
Report No
Sample Date Rush
Lab No
Method No
Fee Code Description
18-039-0203
02/07/2018
11:57
58513
ASTM D93-80
Ignitability/Flashpoint (ASTM
D93-80)
18-039-0203
02/07/2018
11:57
58513
SW-7.3.3
Cyanide Reactivity
18-039-0203
02/07/2018
11:57
58513
SW-7.3.4
Sulfide Reactivity
18-039-0203
02/07/2018
11:57
58513
SW-9045C
Corrosivity (pH)
18-039-0203
02/07/2018
11:57
58514
SW-1311
TCLP Extraction Method 1311
18-039-0203
02/07/2018
11:57
58514
SW-1311 (ZHE)
TCLP Extraction Method 1311
18-039-0203
02/07/2018
11:57
58514
SW-6010C (TCLP)
TCLP Metals (8 RCRA Metals)
18-039-0203
02/07/2018
11:57
58514
SW-7470A (TCLP)
TCLP Metals (8 RCRA Metals)
18-039-0203
02/07/2018
11:57
58514
SW-8081A (TCLP)
TCLP Pesticides (Pest)
18-039-0203
02/07/2018
11:57
58514
SW-8151A (TCLP)
TCLP Herbicides (Herbs)
18-039-0203
02/07/2018
11:57
58514
SW-8260B (TCLP)
TCLP VOCs (Volatiles)
18-039-0203
02/07/2018
11:57
58514
SW-8270C (TCLP)
TCLP SVOCs (BNAs)
Sampled By I Method of Shipment I Blank / Cooler Temp.
Remarks
Relinquished By (sign) Date / Time Received By (sign) Date / Time
Relinquished By (sign) Date / Time Received By (sign) Date / Time

BIOSOLID SAMPLE TR,A XIC" Airy--F A T Y'f"-% 4/41TT
A TILT r-%T' ^T TSTODY
Account#
•
45969
02°3
7621 Whitepine Road N.Chesterfield VA 2323
Illllllllll
� IIII
IIIIII
IIIII
IIIIIII
IIIIIIIIIIIIIIIIIIIIIIIIIIIIIII
45969
02 08 2018 �intanalytical.cofn
TM
City of Wilson WMF
1155:26
Hominv Creek
Copy To
Submitted By
Debra Collins
City of Wilson
of
3
g
I J 4 ��� S �Ndf �'u13 a
P.O. Box 10
3 a
STATE CERT
L t(�J
Wilson, 27854-0010
NC
J L
; J
Phone: Z S " 3 �S" Z'� y
E-mail: [e-mail]
Fax:
tS z - 3� 5 -tz
Package:
Project:
Sample Information
Collection Information
Container Information
Please Write in Desired Tests
Sample ID
Lab Number
(Lab Use Only)
Time
Number
Type
Volume
SL1
SL2
503
METALS
Nitrogen
Series
p H
CCE
ClALK
Volatile
Solids
OTHER
Type
Date
of Bottles
ff
Zl � f
! l T �"
('�
Z Glass
'L Plastic
_ oZ
___pint
X
X
X
X
C/N, A
!}- a I'(,
SO
Composite
—
t �
—
—
Grab
_ Glass
oz
pint
_
_ Composite
_ Plastic
t
Grab
_ Glass
oz
t
_ Composite
_Plastic
_.__pin
Grab
_Glass
oz
_mint
_
Composite
_Plastic
t
Date
Time
ICE: Y
N
D t
Time
Received B (Signature)
Relin uished B Si nature a e
ti1 r6 11 iL ()
Test Package Details
SL1: Total Solids(Moisture) Total Kjeldahl Nitrogen, Phosphorus and Potassium
SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium , Iron, Aluminum, Manganese, Copper, Zinc
503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium,Copper, and Zinc
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen.
TEMP:
Instructions or Remarks
ww� �' C (Y

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: Andrew Mlot
Revised Date:
313012020
Client: City of Wilson
Report Date:
1/30/2020NPDES
#:
3100 Old Stantonsburg Rd
NC0023906
Wilson, NC 27893
Project: Hominy Creek Class B Sludge
Date Sample Rcvd:
1/16/2020
Meritech Work Order #
011620217 Sample: Hominy Creek Class B (A-437-1) Grab
1/16/20
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
26.0 % 1/21/20 0-100 %
SM 2540B
Fecal Coliform (Sludge)
1,433,566 col/g dry wt 1/16/20 130 col/g dry wt
SM 9222D
Meritech Work Order #
011620218 Sample: Hominy Creek Class B (A-437-2) Grab
1/16/20
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
21.4 % 1/21/20 0-100 %
SM 2540B
Fecal Coliform (Sludge)
339,847 col/g dry wt 1/16/20 130 col/g dry wt
SM 9222D
Meritech Work Order #
011620219 Sample: Hominy Creek Class B (A-437-3) Grab
1/16/20
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
22.5 % 1/21/20 0-100 %
SM 2540B
Fecal Coliform (Sludge)
323,232 col/g dry wt 1/16/20 130 col/g dry wt
SM 9222D
Meritech Work Order #
011620220 Sample: Hominy Creek Class B (A-437-4) Grab
1/16/20
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
23.6 % 1/21/20 0-100 %
SM 2540B
Fecal Coliform (Sludge)
194,686 col/g dry wt 1/16/20 130 col/g dry wt
SM 9222D
Meritech Work Order #
011620221 Sample: Hominy Creek Class B (A-437-5) Grab
1/16/20
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
23.0 % 1/21/20 0-100 %
SM 2540B
Fecal Coliform (Sludge)
133,177 col/g dry wt 1/16/20 130 col/g dry wt
SM 9222D
Meritech Work Order #
011620222 Sample: Hominy Creek Class B (A-437-6) Grab
1/16/20
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
34.2 % 1/21/20 0-100 %
SM 2540B
Fecal Coliform (Sludge)
52,684 col/g dry wt 1/16/20 130 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
z ,� Environmental Laboratory
Laboratory Certification No.165
Contact: Andrew Mlot
Client: City of Wilson
3100 Old Stantonsburg Rd
Wilson, NC 27893
Page 2
Revised Date. 313012020
Report Date: 1/30/2020
NPDES #: NC0023906
Project: Hominy Creek Class B Sludge
Date Sample Rcvd: 1/16/2020
Meritech Work Order #
011620223 Sample: Hominy Creek Class B (A-437-7) Grab
1/16/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
22.9 %
1/21/20
0-100 %
SM 254013
Fecal Coliform (Sludge)
127,857 col/g dry wt
1/16/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
011620224 Sample: Hominy Creek Class B (A-437-8) Grab
1/16/20
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
26.1 %
1/17/20
0-100 %
SM 2540B
Chloride
<192 mg/kg
1/27/20
192 mg/kg
SM 4500 Cl B
Ammonia, Nitrogen
5900 mg/kg
1/27/20
0.1 mg/kg
EPA 350.1
TKN
12,200 mg/kg
1/23/20
0.20 mg/kg
EPA 351.1
Nitrate, Nitrogen
<38.3 mg/kg
1/22/20
38.3 mg/kg
EPA 353.2
Nitrate/Nitrite, Nitrogen
<38.3 mg/kg
1122120
38.3 mg/kg
EPA 353.2
Aluminum, total
6,780 mg/kg
1/24/20
0.050 mg/kg
EPA 200.7
Arsenic, total
<1.92 mg/kg
1/24/20
1.92 mg/kg
EPA 200.7
Cadmium, total
0.498 mg/kg
1/24/20
0.200 mg/kg
EPA 200.7
Calcium, total
12,900 mg/kg
1/24/20
0.100 mg/kg
EPA 200.7
Chromium, total
30.5 mg/kg
1/24/20
0.005 mg/kg
EPA 200.7
Copper, total
195 mg/kg
1/24/20
0.002 mg/kg
EPA 200.7
Iron, total
265,000 mg/kg
1/24/20
0.025 mg/kg
EPA 200.7
Lead, total
16.6 mg/kg
1/24/20
0.010 mg/kg
EPA 200.7
Magnesium, total
1,540 mg/kg
1/24/20
0.005 mg/kg
EPA 200.7
Manganese, total
1,050 mg/kg
1/24/20
0.005 mg/kg
EPA 200.7
Mercury, total
0.038 mg/kg
1/21/20
0.02 mg/kg
EPA 245.1
Molybdenum, total
4.56 mg/kg
1/24/20
0.500 mg/kg
EPA 200.7
Nickel, total
16.1 mg/kg
1/24/20
0.010 mg/kg
EPA 200.7
Phosphorus, total
21,800 mg/kg
1/24/20
0.020 mg/kg
EPA 200.7
Potassium, total
927 mg/kg
1/24/20
1.00 mg/kg
EPA 200.7
Selenium, total
<1.92 mg/kg
1/24/20
1.92 mg/kg
EPA 200.7
Sodium, total
759 mg/kg
1/24/20
0.100 mg/kg
EPA 200.7
Sulfur, total*
32,000 mg/kg
1/29/20
0.1 mg/kg
EPA 200.7
Zinc, total
835 mg/kg
1/24/20
0.010 mg/kg
EPA 200.7
Cyanide, total
<1.92 mg/kg
1/22/20
1.92 mg/kg
EPA 335.4
pH
5.7 S.U.
1/17/20
1.0 - 14.0 S.U.
SM 4500-HB
* Results not for regulatory
purposes
Nitrate/Nitrite, Nitrogen was added to the report on 3130120
I hereby certify that I have
reviewed and approve these data.1.1kD
ar'
(J
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

tiA
> 00 T
0 v E
N•
O Y
O
v
1
l /�
C
O
U
cn
N
rq
aJ
Q
0
nUl
xt
m
E
O
N
=
L
❑ \
~a
N
v
O
~
O
Lj
N
c
0
O
M
ai Z
u
%
v `
pal _� O
—
on a; ai
v
C
U
o
a Ln
-1
c
O
n
�J a
yt 9
~� F-
_E
~
m
O
O
a)
Q
c M
v
O
LO O
N
N
y
1
i
0
~
U
n
3
U
3
o .
El
N
of
01
to
O
V
N
N
}
O
_C
E
m 3
E
Z
to
N
Ln
N
E
m
O
2
v�
V
✓�
o c
v to
_
I
I
^,a
, ..
N
"'
N
U
W
`�
° E
° c c
p
c
O
=
m
N
*C
_
•
�,,
ClL u
i v
=_
a
d o
i a
�
z
a
x
w
a
a
t v'
0'
ho
E
LLL
r..
0 E
i .-
w v
c
- _
v
X
i
m.a..+ cl
LL
"
Wto
m to
0 �o
C
•tn
m
O
Q a
d 2
y0 oZJ 0`
E
v c
O
O
L v
io
m
m
m
m
m° —' u
E a Z
m
Q
�.
`/
�
U
U
U
U
U
U
U y U N
:�
L
_
(/�
LL
LL
LL
Ll
LL
LL
LL
U
a s
L
Y E
•`
•�
6S
06
Q$
6 S
�S
cS
06 0 j
U C O
Q
=
C
a--i
O
— W
C
a
/_�
�{/
Ln
"O
of
'Q
V)
Vn
1n
to
to U N a)
c
U E N
y E
Q:
O
_-6 N .UC" a
O O
OE
-� Q
vi
vi
N
(n
N
In
N° N N
in N °
�•
>
Ef
+
a
O
O
O
O
O
O
tO°
c
2.
E�U
v v
>>
a,O
�
E
O
O
O
O
O
O
•.
O N m
U
V U
U
L
I O m
h
O
L
U
c--I
r-I
c-I
ci
r-i
c�
1-1 M
—
in
a
U
IY-
Z
z
O
C
co
Q M1.
H m
❑
4
i
E
U'
C7
C7
C7
C7
U'
U' U'
c
U
Q
Q
a
v° C7
m W
O
z
0
a v
a
�
1, `I�
1`
v
E E
❑
E
N
1
� a
1�(aa
W
00
t 1
O
}
V
^
�
W
I
1
I
U J
CC
���Yf
W
aJ
1
II ,
_
y
N
m
N
C
O
t
E
O o, m
—
Q
m
1
a
.6
M
4-0E
7
Q
� _.
U
O
m
m
ai
M
u
v
�—
C't
L
o a
Q
L
_
�
0
t
M
'L
v!
�Q
��
�'
Cl
y-
2
J
a
LL
a)uj
/E
am•+
Q
d
Z
Wc
v
V)
I.i
.J
u
O(A
m
U
rQ.
p
m2
Z
N
0
.�
=
._i
_
C
++
—
_—ID
C
y
W
LZ
O
z
C
—
_
t VI
L
:
U
U
a
W
O
N '
w
)
O
Nd
ro
H
ee-
e4-
'�
t0
m
m
m
m
m
m
m
m m
c
c
chi)
LnvNi
Lnv`ni
can
Ln
uNi CA
O
U
v v
o z
v
m
=
O
a)
a)
0J
aJ
N
a)
0) a)
N
x OJ L
W
v
U
U
U
U
U
U
U U
O
N
a
�
a
a
�
�•
a
a a
t
� a� �
O
cn
E
E
E
E
E'
E
E
s
=
cn
❑ 0 ElK

p AM
U F;Z
PROM PT•ACCLI RATE -RELIABLE
LABORATORIES, INC
WWW.PARLABS.COM
REPORT OF ANALYSES
Attn: ANDREW MLOT
CITY OF WILSON
PO BOX 10
WILSON, NC 27894-0010
PROJECT NAME: JAN 20
DATE: 03/03/20
SAMPLE NUMBER-
138072
SAMPLE ID- HOMINY
CREEK A-433
SAMPLE MATRIX- WW
DATE SAMPLED-
01/15/20
TIME SAMPLED- 0917
DATE RECEIVED-
01/16/20
SAMPLER- NH
RECEIVED BY- DJ
TIME RECETVED-
1020
DELIVERED BY- FEDEX
TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS
METHOD
DATE
TIME BY
RESULT UNITS
40 DAY BENCHTOP
DIGESTION EPA625R
01/16/20
1550 RE
5.75 %
LABORATORY
DIRECTOR
2217 Graham Park Drive • Charlotte, NC 28273
Phone: [phone] • Fax: [phone]

P.-A.R.-
I.ABORATORIEsr INC
40 Day Bench Scale Extended Aeration Test for Anearobically Digested Solids
Percent Volatile Solids Reduction
Day 0 - Start of Test
A
Empty Dish Wt
21.5769
20.3050
20.5152
24.2898
19.2830
21.2051
B
Initial Sample Wt+ Empty Dish WI
31.4395
32.9300
29.6397
35.0293
30A467
32.1570
C
Doled Sample Wt+Empty Dish Wt
247951
2404411
23.6884
28.1029
23.1161
24.8047
D
Ashed (Burned)SampleAft
23.0863
22.2563
21.9169
20.0528
21.0825
22.8709
L= (B-A)
tl SWd eWt
9.8626
12.5650
9.1245
11.0395
11.5829
10.95119
S = C-A
Dried Slud Wt
3.2182
4,0761
3.0512
3.8131
3.8343
3.5986
V = C-D
Volatile Solids Wt
1.7298
2.1848
1.6495
2.0503
2.05W
1.9338
F = (D-A)
Fbned Solids Wt
1.4894
1.8913
1.4017
1.7628
1.7787
1.6648
V% • B •100
Perim Volatile Solids %
53.719
63.600
54.061
63.770
53.011
53.7522
2
Mass Fraction of Volatile Solids in Liquid Feetl) Slutl eat Start of Test
0.1752885
0.1738798
0.1807770
0.1761502
0.1777755
0,1768
x = FIL
Maas Fracton of toted Sotitls in Li Feed Slud at Start of Test
0.1510149
1 0.150521
1 0.1536194
0.151449a
1 0.1538282
1 0.1521
Day 20 - Mid -Point of Test (CC Cheek)
A
Empty Dish Wt
17.1735
21.9085
22.0101
21,4385
17.6213
20.0300
B
Initial Sam le Wt+Em Dish WI
26.9035
30.6156
30.2435
28.7307
27.0363
28.3059
C
Dried Sam le V. Dish Wt
19.7074
24.76"
24.7345
23.8268
20.7151
22.7496
D
Ashed Burned Sam Wt+Dish Wt
18.3588
23.2571
23.3015
22.5762
19.0939
21.3175
L- B-A
Li Slutl a Wt
7.7300
8.7069
0.2334
7.2942
9.4150
02759
S = (C-A)
Doled Sludge WFCWM
2.5339
2.8559
2.7244
2.3903
3.0938
2.7197
V = C-D
Volatile Solids W[ W
1.3488
1.5073
1.4330
1.2506
1.6212
1.4322
F = (D-A)
Fixed Solids Wt
1.1851
1.3486
1.2914
1.1397
1.4726
1.2875
V%- IS •100
Percent Volatile Solids %
53.230
52.778
52.599
52.320
52.402
52.6658
V% 20 < 0
QC Check of Ana 's: Is 20 da V % less than 0 da V%?
Yea
Yes
Yes
Yes
Yes
Day 40 - End of Test
.,w.��4x avcwsrc
A
Em iah
23.1833
22A941
10,9928
23,0256
22.8281
21.7044
B
Initial Sample Wt+Empty Dish Wt
33.0218
31o222
28.2217
309479
30.9601
30.8347
C
Dned Sam le WI+Ent Dish Wt
26.4015
25.4224
20.6804
25s2 7
25.2746
24AM
D
Ashed Bunted Sam le N+ Dish Wt
24,7448
24.0217
10.7805
24.2924
23.9210
23.1521
L = B-A
LJ uid Slud Wt
9.8385
8.3281
11.2289
7.9223
8.3340
9.1304
S = C-A
Dried Stud a Wt
3.2182
2.7283
3.6876
2.6001
2.6485
2.9765
V • C-D
Volatile Solids Wt
1.6567
1.4007
1.8999
1.3333
1.3536
1.5288
F • D-A
Fixed Solids Wt
1.5615
1.3278
1.7877
1.2688
12949
1.4477
V%= IS•100
Peroem Volatle Solids %
51.479
51.340
51.521
51279
51AGII
51.3454
b • IL
Mass Fraction of Volable Solid. in Liquid (Bottom) Sludgeat End of Test
0.1683895
0.1681896
0.1691973
0.1682971
0.1624190
0.1673
= FIL
Mass Fractlon of Fixed Solids in Liquid Bottom Sludge at End of Test
0.1587132
0.1594121
0.1592053
0.1599031
0.1553756
0.1585
V% 40 < 0
DC Check of Ana : Is 40 da V% less than 0 d V%?
Yea
Yes
Yes
Yee
Yes
VSR (mb) = See Belov Fractional Volatile Solids Reduction (Mass Balance Method) 3.82% 2.81% 7.24% 4.37% 10.49%
Average FVSR (mb) of all vaild replicate results 5.75%
Is Average FVSR (mb) less than or equal to 17%? YES - Sample Passes Requirement
*Calculation: FVSR (mb) _
y = mass fraction of volatile solids in the liquid sludge
x = mass fraction of fixed solids in the liquid sludge
f = indicates feed sludge at start of the test
b = indicates "bottoms" sludge at end of the test
[y(f) " (1 - x(b))] - [y(b) " (1-x(fl)]
[y(f) ` (1-x(b)-y(b))]
P.O. sox 41 I483 a Chulotte, NC 2R241.I "3
Phone: (704) :RN-B333 = Fu: ('ai) SN8-N335

PAR
lA/OM TOMES. INC.
www,partabi.com
Shipping:
2217 Graham Park Drive
Charlotte, NC 28273
CHAIN OF CUSTODY
PAR Laboratories, Inc
Phone [phone]
Fax [phone]
Mailing:
PO Box 411483
Charlotte, NC 28241.1483
It is essential that all Information be recorded on thin Chain of Custody documerrc for acceptance by PAR Laboretorles. Inc. and the North
Carolina De anmont or Environmental and Natural Resources,
Company Name (bllting) Ll
Comments/ Special Instructions
f� n1 lt) .
Address
P u. fox iL)
City, State fx zip code
Wr b toir 0 'C z7g53
Point of Contact It Telephone Number
Z S 2 W- I'4 W
Sample
Taken By: SIGNATURE
PRINTED NAME /tI- It (c 4A
ARE SAMPLES FOR STATE or EPA REPORTING? YES NO X
;Sample Type: ow ww �_ GWMW HW soil Other Y
Sample Tamp at time of snrNo— ° C Sample Temp upon receipt: — ° C
' `Field Preserved: Yes Teflon Liner/Zero Headspace: Yes No n/a
Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (Y/NI: fj4
Client Sample I.O.
(Semple Location / Numbed
Comp
Grab
Preserv.
Set Up
Date/T1me
Collection
DateMma
nalyses
Rsquested
N .,stjj rt 61s, Q
X
I s z�tv
i
Hellnquished b te/TTo r+ecrrve o v■ie. o
fr 1.') L
Relinquished by: Oate/Time Received by: Dete[rime
C a Composite G =Grab OW=Drinking Water WW =Wastewater GWMW =Groundwater Monitoring Well HW aHazardous Waste
" See Other Side

APPENDIX 3
2020 PERMIT MODIFICATION
Granville Farms, Inc. (WQ0000838)
Residual Source Certification Attachment
RS CA
Oxford WWTP
Field Loading Calculations
Analytical

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: City of Oxford WWTP
2. Facility permit holder is: ❑ Federal, ❑ State, ® Local Government, or ❑ Private.
Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: ).
3. Facility contact person and title: Antoine Lewis, WWTP Superintendent
Complete mailing address: PO Box 506
City: Oxford State: NC Zip: 27565-
Telephone number: [phone] E-mail address: alewis&oxfordnc.org
4. Facility physical address: 325 New Commerce Drive
City: Oxford State: NC Zip: 27882-
Coordinates: Latitude: 36' 17' 22" Longitude: 78. 34' 51"
Datum: NAD 83 Level of accuracy: Sub -Meter
Method of measurement: GIS
5. Purpose of the facility:
® treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
❑ treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: __E % industrial and % domestic)
❑ other (explain: ).
6. Does the facility have an approved pretreatment program: ® Yes No
7. Facility permitted/design flow: 3_5 MGD and facility average daily flow: 1_5 MGD
8. Average amount of residuals being generated at this facility —500 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 3-Stage Oxidation Ditch featuring Anaerobic, Aerobic, and Anoxic Zones
Type and volume of residuals storage (i.e., outside of residuals treatment units): 0.5 MG Aerobic Digester
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
M. 40 CFR Part 503 or ❑ 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
® Biological ❑ Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA:
(Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -
municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: e yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well
as those for corrosivity, ignitability, and reactivity:
Laboratory: Summit Environmental Technologies, Inc. and Date of analysis: 6/21/2018
Passed corrosivity test: ® yes ❑ no. pH: 6.8 s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes ❑ no. Flashpoint: Non Flammable OF (> 140°F)
Passed reactivity test: ® yes ❑no. HCN: <0.5 mg/kg (<250) & H2S: <25 mg/kg (<500)
TCLP Parameter
Limit
(mg17)
Result
(mg17)
TCLP Parameter
Limit
(mg17)
Result
(mg17)
Arsenic
5.0
<2.5
Hexachlorobenzene
0.13
<0.08
Barium
100.0
<25.0
Hexachloro-1,3-Butadiene
0.5
<0.032
Benzene
0.5
<0.5
Hexachloroethane
3.0
<0.16
Cadmium
1.0
<0.5
Lead
5.0
<2.5
Carbon Tetrachloride
0.5
<0.5
Lindane
0.4
<0.002
Chlordane
0.03
<0.02
Mercury
0.2
<0.01
Chlorobenzene
100.0
<0.5
Methoxychlor
10.0
<0.002
Chloroform
6.0
<0.5
Methyl Ethyl Ketone
200.0
<2.5
Chromium
5.0
<1.0
Nitrobenzene
2.0
<0.16
m-Cresol
200.0
<0.4
Pentachlorophenol
100.0
<0.4
o-Cresol
200.0
<0.4
Pyridine
5.0
<0.4
p-Cresol
200.0
<0.4
Selenium
1.0
<0.25
Cresol
200.0
<8.0
Silver
5.0
<2.5
2,4-D
10.0
<1.0
Tetrachloroethylene
0.7
<0.5
1,4-Dichlorobenzene
7.5
<0.16
Toxaphene
0.5
<0.04
1,2-Dichloroethane
0.5
<0.5
Trichloroethylene
0.5
<0.5
1,1-Dichloroethylene
0.7
<0.5
2,4,5-Trichlorophenol
400.0
<0.4
2,4-Dinitrotoluene
0.13
<0.08
2,4,6-Trichlorophenol
2.0
<0.4
Endrin
0.02
<0.002
2,4,5-TP (Silvex)
1.0
<0.5
Heptachlor and its Hydroxide
0.008
<0.002
Vinyl Chloride
0.2
<0.2

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate
the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: WMpoint Analytical and Date of analysis: 11/6/2019
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
<13.9
Cadmium
85
39
<2.78
Copper
4,300
11500
461
Lead
840
300
33.9
Mercury
57
17
0.55
Molybdenum
75
n/a
8.94
Nickel
420
420
17.6
Selenium
100
100
<13.9
Zinc
7,500
2,800
1,820
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
❑ > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 3.56 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Waypoint Analytica, and Date of analysis: 11/6/2019
Parameter
Result
(mg/kg)
Aluminum
54,700
Ammonia -Nitrogen
13,600
Calcium
15,400
Magnesium
4,560
Nitrate -Nitrite Nitrogen
<128
pH (Standard Unit)
7.7
Phosphorus
20,300
Potassium
2,920
Sodium
2,310
Total Kjeldahl Nitrogen
59,400
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 0.79
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and
conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate
is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1s) Year PAN
Five -Year
Maximum Adjusted PAN
(mg/kg)
(mg/kg)
Surface
20,668
30,639
Injection/Incorporation
27,468
35,688
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: None Known

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(13)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T. 1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 [15A NCAC 02T. 1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
® Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
c. For Surface Disposal:
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
® Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur
when these residuals are applied and left on the land surface.

FIELD LOADING ESTIMATES
Facility Oxford WW 'P
Sampling Date 11/6/2019
Solids 3.56
Mineralization Rate 0.30
Gallons perDT 6,736.18
pH 7.7
Sodium Absorpotion 0.79 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 59,400 lbs./1,000 gal 17.64
Ammonia Nitrogen (mg/Kg) 13,600.00 lbs./1,000 gal 4.04
Nitrate -Nitrite (mg/Kg) 128.00 lbs./1,000 gal 0.04
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 20,668 lbs./1,000 gal 6.14
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 27,468 lbs./1,000 gal 8.16
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling Class B Ceiling
Limits (mg/Kg) Limits (mg/Kg)
41 75
39 85
1,500 41300
300 840
17 57
420 420
100 100
2,800 7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
Potassium lbs./1,000 gal
0.87
Phosphorus lbs./1,000 gal
6.03
Calcium lbs./1,000 gal
4.57
Magnesium lbs./1,000 gal
1.35
Manganese lbs./1,000 gal
0.17
Sulfur lbs./1,000 gal
2.97
Molybdenum lbs./1,000 gal
0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
13.90
Cadmium (mg/Kg)
2.78
Copper (mg/Kg)
461.00
Lead (mg/Kg)
33.90
Mercury (mg/Kg)
0.55
Nickel (mg/Kg)
17.60
Selenium (mg/Kg)
13.90
Zinc (mg/Kg)
1820.00
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
59,400
20,668 41.34
38,732
59,400
27,468 54.94
31,932
38,732
5,810 11.62
32,922
31,932
4,790 9.58
27,142
32,922
2,469 4.94
30,453
27,142
2,036 4.07
25,107
30,453
1,142 2.28
29,311
25,107
941 1.88
24,165
29,311
550 1.10
28,761
24,165
453 0.91
23,712
Arsenic lbs./1,000 gal
0.00
Cadmium lbs./1,000 gal
0.00
Copper lbs./1,000 gal
0.14
Lead lbs./1,000 gal
0.01
Mercury lbs./1,000 gal
0.00
Nickel lbs./1,000 gal
0.01
Selenium lbs./1,000 gal
0.00
Zinc lbs./1,000 gal
0.54
Equations
1st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 30,639 61.28
Total 35,688 71.38

YTICAL
11/18/2019
Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-312-0007
Project Description: Oxford
Dear Mary Brewer.-
Waypoint
report.
7621 Whitepine Road, R
Main 804-74.3-9401
ichmond, VA 23237
° Fax 804w2-71-6446
www.waypointanalytical.com
Analytical Virginia, Inc. received sample(s) on 11/8/2019 for the analyses presented in the following
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with t
if applicable.
he applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite... ) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this repo.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
poaj�W 661wr
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

Report Number:
ANALYTICAL
19-1312mOOO7
Client Project Description: Oxford
7621 Whitepine Read, Richmond,. VA 23237
Main 804-743-94010 Fax [phone]
wwtn+.waypaiEltanalyfiical.tdm
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
69535 Oxford N &M Solids 11/06/2019 09:30 11/08/2019
69535 Oxford N &M Solids 11/06/2019 09:30 11/08/2019 SM-4500-NH3C WTN
69535 Oxford N &M Solids 11/06/2019 09:30 11/08/2019 9045D WTN
69535 Oxford N &M Solids 11/06/2019 09:30 11/08/2019 450ONO3F-2011 WTN
69535 Oxford N &M Solids 11/06/2019 09:30 11/08/2019 601 OD WTN
69535 Oxford N&M Solids 11/06/2019 09:30 11/08/2019 SW-7471 B WTN
69535 Oxford N &M Solids 11/06/2019 09:30 11/08/2019 SM-4500-NH3C-TKN WTN
69535 Oxford N&M Solids 11/06/2019 09:30 11/08/2019 SM-254OG WTN
WTN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

YTICAL
46478
Synagro Central LLC/
Mary Brewer
284 Boger Road
Oxford
Mocksville , NC 27028
Submitted By: Ryan Copeland
Report Number : 19-312-,0007
Project
Information
7621 Whitepine Road, Richmond, VA 23237
Main 804-743m-9401 ' Fax [phone]
www.waypaintanalyfical.com
Ryan Copeland
Oxford
REPORT OF A MA L VSXS
Report Date
Received
11/18/2019
11/08/2019
Pauric McGroary
Agronomist
Lab No : 69535 Matrix:: Solids
Sample ID :Oxford N&M Sampled: 11/612019 9w530
Test Results Units MQL DF Date I Time By Analytical
Analyzed Method
Ammonia Nitrogen
Nitrate+N
organic N
itrite-N
pH
Total Solids
Total Kieldahl N
Phosphorus
Aluminum
Arsenic
Calcium
Cadmium
Chromium
Capper
Ir4n
Lead
Magnesium
Manganese
Mercury
Molybdenum
Nicke[
Potassium
Selenium
Sodium
itrogen
13600
<128
45800
7m7
3m56
59400
20300
54700
<13.9
15400
<2.78
52o2
461
21500
33.E
4560
564
OX550
�4
<13.9
2310
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
s.u.
°Ia
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg -dry
mg/Kg -dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
mg/Kg - dry
128
6940
139
139
119
6.94
6.94
139
833
139
119
0.406
6.94
139
119
694
1
11/15/19
15:00
JPJ
SM-4500-NH3C
1
11/12/19
14:12
ZBD
450ONO3F-2011
1 11/15/19 12:00 CALCULATION
1
11/12/19
05:08
ISL
9045D
1
11/11/19
16:135
ADM
SM-254OG
i
11/15/19
12:00
JPJ
iM-4500-NH3C-TKP
1
11/13/19
02:34
KKM
1
11/13/19
02:34
KKM
1
11/13/19
02:34
KKM
1
11/13/19
02:34
KKM
1
11/13/19
02:34
KKM
1
11/13/19
02:34
KKM
1
11/13/19
02:34
KKM
1
11/13/19
02:34
KKM
1
11/13/19
02:34
KKM
1
11/13/19
02:34
KKM
1
11/13/19
02:34
KKM
1
11/12/19
14:29
TJS
1
11/13/19
02:34
KKM
1
11/13/19
02:34
KKM
1
11/13/19
02:34
KKM
1
11/13/19
02:34
KKM
1
11/13/19
02:34
KKM
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
SW-7471 B
6010D
6010D
6010D
6010D
6010D
Page 3 of 6

YTICAL
Synagro Central LLC/ Oxford
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Submitted By: Ryan Copeland
Report Number: 19-312-0007
Lab No
69535
Sample ID: Oxford N&M
7621 Whitepine Road, Richmond, VA 23237
Main 804-7434-,94010 Pax 904-771-6446
www.waypointanaly1dical.eo►n
Ryan Copeland
Project oxford
Information ;
REPORT OFANAL YSIS
Report Date : 11/18/2019
Received : 11/08/2019
P.4
awf ce..
I C* 60A AO
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 11/6/2019 9aW30
Test Results Units MQL D F Date / Time By Analytical
Analyzed Method
Zinc
1820
mg/Kg
- dry
34.7
Sulfur
10000
mg/Kg
- dry
139
Moisture 96m4 % 0.010
1 11/13/19 02:34
1 11/13/19 02:34
KKM
qh' I VLU.
1 11/11/19 16:35 ADM
Qualifiers/ B Analyte detected in blank H Beyond holding time
Definitions
6010D
SM-2540G
Page 4 of 6

LrA
"a
ANALYTICAL
0
Customer Number: 46478
Customer Name:
Report Number:
0 Fed Ex
• UPS
7621 Whitepine Road, Richmond, VA 23237
Main 804--74-'311-9401 'Fax [phone]
4'
www.wayp o f nta n a I ytica I. co m
Cooler Receipt Form
Synagro Central LLC/ Oxford
19-312-x0007
0 US Postal
0 Client
Shipping Method
0 0
Lab
Courier
Shipping container/cooler uncompromised?
• Yes
dumber of coolers received � 1
0 Other
Thermometer ID-.
No
Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Required
Custody seals intact on sample bottles? 0 Yes 0 No I* Not Required
Chain of Custody (COC) present? is Yes 0 No
No - MR-*
COC agrees with sample labei(s)? I* Yes 0 No
COC properly completed I* Yes 0 No
Samples in proper containers? • Yes 0 No
Sample containers intact? ID Yes 0 No
%� —
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? IS Yes 0 No
Cooler temperaturein compliance? •Yes 0 No
Cooler/Samples arrived at the laboratory on ice. •Yes 0 No
Samples were considered acceptable as cooling
process had begun'.
Water - Sample containers properly preserved 0 Yes C) N o 9 N/A
Water - VOA vials free of headspace 0 Yes 0 No I* N/A
Trip Blanks received with VOAs 0 Yes No N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No � N/A
F_ High concentration container (48 hr) � Low concentration Encore samplers (48 hr)
� High concentration pre -weighed (methanol -14 d) Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?. 0 Yes 0 No
Comments:
Signature: BrandiWatson Date & Time:
11/08/2019 13-003:03
Page 5 of 6

S
SAMPLING LOG #
F
rv, � p � 1-xti �'-tt"�} f+ry+4-rf.a-ia}K. f.,�v� �. G ti�•41F{ i Sf.��iJi��
PROJECT MANAGER.,
Phone: t 33 6.. }
CUSTOMER
SAMPLEIvDoo
Relinquished by Sampler:
$AMPUtUlf aTt
kP
LOCACJAI
4
A&
762. CentralLC
Svn;acjto
�ICt -d
Oxford
7
OL
T"*E
SAMPLE
D to iirrte
00
Re[Inquished by: _ D
Rellnou'...P d by:
Sp,ECIAL INSTRUC11ONS
For
d
t
monitoring pu oses.
w
dime
Time
coNTAfNERS
Recleved by:
Recleved bu.;
Recleved tajr.
A —N.ALv,f S.WIS REQUEST
-C-0 D
affest that the proper field sampling procedures
were used daring the collection. of e-S6 samples.
SAMPLER
SABfi.P NG
P0#6V
TIME
�lETHOt3
PRESE�.VE�]
REMARKS:
C13CO3 volatile� Mo
eaulviv Solids 4Pt
t
METH 00
SHIPPED
----
coo
LOQZ
4
0
Page 6 of 6

MP
{ I R. ,161 E cl L Ct. PS I -z" :
Lqb av%aho rip.
July 24, 2018
Clay Fi"sackerly
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Oxford TCLP 2018
Dear Clay Fi'sackerly:
Sinninit Envii4oninental Technologies, Inc.
3310 ffl'in St.
Cityahoga Falls, Ohl*o 44223
TEL: [phone] EAY.- [phone]
Prebsite.- h Up-.-Iliviviv. se tie k. cotaz
Order No.:
18061305
Summit Environmental Technologies, Inc. received 1 sample(s) on 6/22/2018 for the
analyses presented in the following report,.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory,.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls., Ohio 44d&Edx=Ed3
Arkansas 88-0735, California 07256CA3 Colorado, C onnectic ut PH-0 10 81 Delaware, Florida NELAC E87688, Georgia E 8 7 6 8 8, Idaho OH00923, Illinois
200061, Indiana C -OH- 13 . Kansas E- 10347, Kentucky (Underground Storage Tank) 3, Kentucky 9 014 6, Louisiana 0406 1, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OHOO 6, New York 117 7 7, North Carolina 39705 and 631, North Dakota R-2 0 1, Oklahoma 994 0, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5,, Utah OH00923201 1-1,, Virginia VELAP 9456, Washington
C891
Page 1 of 27

r�:Ll"IRONMEt4TALTECHNOLOG.1,Es, WC.-
Laboratories
CLIENT. Synagro
Project: Oxford TCLP 2018
WorkOrder Narrative:
18061305: This ref oft in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of- Custody,
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL [phone] FAX- [phone]
Website: httM:11www.settek.cojn
Case Narrative
W0#@9
Date:
18061305
7/24/2018
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies-, Inc., Work Order Number assigned to this report..
Summit Environmental Technologies, Inc., holds the acereditations/certmificatoions listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not ceitified."
The information contained in this analytical
Technologies, Inc. and that of the customer.
Summit Enviromnenta.
report is the sole property of Summit Environmental
It cannot be reproduced i"n any form without the consent of
1 Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received.. Conditions can vary at different
tunes and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data In herein.
All results for Solid Samples are reported on an "as received" or it weight" hasis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
Theis report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Prep Sample Comments:
18061305-OOIA 391811: Prep Comments for MtlPrep TCLP(3010A) Sample 18061305-OOIA:
Sample had a yellow tint, had limited volume, and was filtered after digestion.
18061305 Mod 001A 391857., Prep Comments for S re B ot C P 3510), Sample 18061305-
Ulu ample is a soapy solution, Limited volume
18061305-001 391855: Prep Comments for S re CPest TC P 3510), Sample 18061305m4001A:
Sample is a soapy solution, Original p o sample is acidic; sample was neutralized prior to extraction,
Limited volume
Origi
nal
Page 2 o 7

Ila$
IIISzmamitEnvironnaental Technologies, Ira Qua lfieics a d AcronymsAcronyms3310 Hlin .�
M
I
1kol
INQ Cityahoga Falls, Ohio 442.4' WO#G 18061305
— Anah-of�r81 Ls�h�rs�ut7�� TELL (330) 2.53-8211 FAX: [phone]E
TIVebsirte: httD.-11ivivw.settek.co Date: 7/24/2018
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
i The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
�The result exceeds the Regulatory Limit or Maximum Contamination Limit,
m Manual integration was used to determine the area response.
d manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a. I :1 response.
P The second column confirmation exceeded 25% difference,
C The result has been confirmed by GC/T\4S.
X The insult was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The GCB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL./+ The LCS or LCSD recovery failed low (-) or high (+).
VLK The LUN/LUND RPD was outside of accepted recovery limits.
QM.-,/+
QMR
QV-/+
S
Z
The MS or MSD recovery failed love (-) or high (+).
The MS/N4SD RPD was outside of accepted recovery limits,.
The ITV recovery failed low (-) or high (+).
The spike result was outside of accepted rep
0
Deviation; A deviation from the method wa
additiona
Acronyms
J
I information
ND
Not Detected
QC
Quality Control
MB
Method Blank-
LCS
Laboratory Control Sample
LCSD
Laboratory Control Sample Duplicate
QCS
Quality Control sample
DUP
Duplicate
MS
Matrix Spire
MSD
Matrix Spire Duplicate
RPD
Relative Percent Different
ICV
Initial Calibration Verification
ICB
Initial Calibration Blank
CCV
Continuing Calibration Verification
CAB
Continuing Calibration Blank
RLC
Reporting Limit Check
DF
Dilution Factor
�overy limits.
s performed; Please refer to the Case Narrative for
RIL
MDL
LOD
LOQ
PQL
CRQL
PL
RegLvl
MCL
MinCL
RA
RE
TIC
RT
CF
RF
Reporting Limit
Method Defection Limit
Level of Detection
Level of Quantitation
Practical Qumfitation Limit
Contract Required Quantitation Limit
Permit Limit
Regulatory Limit
Maximum Contamination Limit
Minimum Compound Limit
Reanalysis
Reextraction
Tentatively Identified Compound
Retention Time
Calibration Factor
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Origdo
inal
Page 3 of 27

71 C! I =!; I
F- N, V 1". 0 N M E WfA L I Ew C'.111 U 0 LO N'C:
r
CLIENT:
Project:
Lab SampleID
18061305-001
Synagro
Oxford TCLP 2018
Client Sample 11D
Oxford TCLP 2018
Szonnfit Envii'lonmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX- [phone]
Websi'te.0 htfig.-Ili,i�wii�.settefc.co77i
Tag No Date Collected
6/21/2018 12-YO30:00 PM
Workorder
Sample Summary
WO#:
Date Received
6/22/2018 10:20:00 AA4
18061305
24-Jul-18
Matrix
Sludge
Page 4 of 27

Summit Environmental Technologies, Inc.
3310 Win St.
EMPMRONIal-ENTAL TECON'OLOGIES, INC. CuyahogaFalls, Ohio 44223
.r:r?ZP,�P."ci C.a" TEL: [phone]FAX: [phone]
Website: htt :Ilwww-settek.com
Client: Synagro
Project: Oxford TCLP 2018
DATES REPORT
WO#:
18061305
24-Jul-18
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prey Date Analysis Date
18061305-OOIA Oxford TCLP 2018 6/21/2018 12:30:00 PM Sludge Ignitability of Solids (SW-846: 1030)
pH (SW9045D)
Reactive Cyanide (9014/7.3.3.2)-Solid
Reactive Sulfide (9034)/7.3.4.2
TCLP Herbicides Analysis (SW1311/87/1/2018 6:00:00 PM
TCLP Mercury Analysis (SW1311/7477/l/2018 6:00:00 PM
TCLP Metals Analysis (SW1311/6010-7/l/2018 6:00:00 PM
TCLP Pesticides Analysis (SW1311/8(7/l/2018 6:00:00 PM
TCLP Semi-Volatiles Analysis
(SW1311/8270)
TCLP Volatiles Analysis
7/1/2018 6:00:00 PM
7/3/2018 12:30:00 PM
7/3/2018 10:55:00 AM
7/2/2018 3:20:00 PM
7/2/2018 1:00:00 PM
7/2/2018 11:15:00 AM
7/1/2018 6:00:00 PM
7/23/2018 2:00:00 PM
7/9/2018 5:18:00 PM
6/25/2018 2:29:00 PM
6/25/2018 2:29:00 PM
7/11/2018 7:20:00 PM
7/3/201.8 3:43:00 PM
7/5/2018 8:34:41 PM
7/11/2018 2:30:00 PM
7/9/2018 12:18:00 PM
7/4/2018 2:16:00 AM
Original
Page 5 of 27

CLIENT:
Matrix:
Lab ID:
Project:
Synagro
SLUDGE
18061305-OOIA
Oxford TCLP 2018
Stwunit Envii-loiv7iental Technologies, bic.
3310 Whi St.
Cuj)ahoga Falls, Ohl'o 44223
TEL: [phone] FAA-.- [phone]
Tfl'ebsite.11 http://i,vi,i)it).settelc.coii?
Araalytic�l Report
W0#E0
abase report
1
Date Repoiled:
8061305
7/24/2018
Tag Number:
Collection Date.* 6/21/2018 12:30:00 PM
Client Sample ID Oxford TCLP 2018
Analyses Result RL Qual Units DF Date Analyzed
TCLP ARPTAl��, Nlnr.RNA PF=5T, HFRRnSOLID
TCLP MERCURY ANALYSIS (SW1'31 11
TCLP Mercury
7470)
ND 0.0100 mg/L
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SWI 311/6010)
TCLP Arsenic(As)
TCLP Barium(Ba)
TCLP Cadmium(Cd)
r)
TCLP Chrom'l'um(C
TCLP Lead(Pb)
TCLP Selenium(Se)
TCLP Silver(Ag)
SW601 OD
SW7470A
Analyst: EAM
1 7/3/2018 3-043-MOO PM
SW301 OA
Analyst: KMS
ND
2.50
mg/L
1
7/5/2018
8:34:41
PM
ND
25.0
mg/L
1
7/5/2018
8:34:41
PM
ND
0.500
mg/L
1
7/5/2018
8:34:41
PM
ND
1.00
mg/L
1
7/5/2018
8:34:41
PM
ND
2.50
mg/L
1
7/5/2018
8:34:41
PM
ND
0.250
mg/L
1
7/5/2018
8:34:41
PM
ND
2.50
Mg/L
1
7/5/2018
8:34:41
PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMImVOLATILES ANALYSIS (SWI311/8270)
1,4-Dichlorobenzene
2,4,5-Tri ch I o roph en 0
2,4,6-Trichloropheno
2,4-Dinitrotoluene
o-Cresol
m/p-Cresols)
Cresols, Total
Hexachloro-1 ,
3-butadiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
Surr',- 2-Fluorophenol
Surr Phenol-d6
Surr Nitrobenzene-d5
Surr 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
SW8270D
SW351 OC
Analyst: BJH
ND
0.160
mg/L
2
7/9/2018 12-18-000
PM
ND
0.400
mg/L
2
7/9/2018
12:18-000
PM
ND
0.400
mg/L
2
7/9/2018
12:18-000
PM
ND
0.0800
mg/L
2
7/9/2018
12:18-000
PM
ND
0.400
mg/L
2
7/9/2018
12:18--000
PM
ND
0.400
mg/L
2
7/9/2018
12:186-00
PM
ND
8.00
mg/L
2
7/9/2018
12:18:00
PM
ND
0.0320
mg/L
2
7/9/2018
12:18-000
PM
ND
0.0800
mg/L
2
7/9/2018
12-018-000
PM
ND
0.160
mg/L
2
7/9/2018
12:18-000
PM
ND
0.160
mg/L
2
7/9/2018
12-ml8m-00
PM
ND
0.400
mg/L
2
7/9/2018
12:18:00
PM
ND
0.400
mg/L
2
7/9/2018
12,0,18:00
PM
25.2
10-109
%Rec
2
7/9/2018
12:18:00
PM
27.0
10-109
%Rec
2
7/9/2018
12:18E-00
PM
31.6
19-120
%Rec
2
7/9/2018
12:18:00
PM
33.4
10-120
%Rec
2
7/9/2018
12-18-00
PM
41.8
22-117
%Rec
2
7/9/2018
12:18:00
PM
Qualifiers: * Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC ,Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected 0 RSD is greater than RSD11*m1*t
P Second column confirmation exceeds PL Permit Limit Origiiial
R RPD outside accepted recovery limits RL Reporting Detection Lff'nit
Page 6 of 27

CLIENT,
Matrix:
Lab ID.
�1 -WIRIM
VW qW
Pri 0 '(4 hl E WI-4"t L - .22"dC
0 N 0
Suimifit Em4i-qomnental Technologies, Inc.
3310 Tf/'ij7 St.
0
L G!G' I Pir Czryalaoga Falls, OI710 44223
TEL: [phone] FILK [phone]
TIVahcito0 la ttn -//u�uin) sotto lr rnm
Synagro
SLUDGE
18061305-OOIA
1 0
t ,:eaI -R P-ort
(base report)
W0#0 18061305
liate tceponea: //Z4/ZU15
Tag Number:
Collection Date:, 6/21/2018 12:30-OPOO PM
Project: Oxford TCLP 2018
Client Sample ID Oxford TCLP 2018
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERS -SOLID
TCLP SEMI=VOLATILES ANALYSIS (SW131118270)
Surr.- p-Terphenykd14
FOOTWIDIN
I r.1 P M F TA I !;, VOC, FtmA, pi=sT, 1--ERB-SOLID
TCLP PESTICIDES ANALYSIS (SW13111
Chlordane, total
To x cra kp h e n e
Endrin
gamma-BHC
Heptachlor
Heptachlor epoxide
Methoxychlor
Surr: TCMX
S u rr:
ITy�
8081)
ND
IND
ND
ND
ND
ND
ND
35.1
56.0
TCLP METALS, VOC, RNA.0 PEST, HERBS �OLID
TCLP HERBICIDES ANALYSIS (SW1311/8161)
[cIA=f[*1
0.0200
0.0400
0.00200
�][iI1yz1I87
0.00200
0.00200
0.00200
10-119
10-119
SW8270D
%Rec
SW351 OC
Analyst: BJH
2 7/9/2018 12:18600 PM
SW361 0C
mg/L
9
7/11/
m g/L
1
7/11/
m g/L
'1
7/11/
mg/L
7/11/
mg/L
1
7/11/
Mg/L
1
7/11/
mg/L
1
7/11/
%Rec
1
7/11/
%Rec
1
7/11/
SW8151A SW8151A
214-D
ND
1.00 d
mg/L
1
7/11/
214)5-TP
ND
0.500 d
mg/L
1
7/11/
S u rr.-. D CAA
83.7
20-140
%Rec
1
7/11/
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
SW8260B
SW1 311 M
Analyst: JBN
2018 2:30:00 PM
2018 2:30:00 PM
2018 2:30:00 PM
2018 2:30:00 PM
2018 2:30:00 PM
2018 2:30:00 PM
2018 2:30:00 PM
2018 2:30:00 PM
2018 2:30:00 PM
Analyst: JBN
2018
7-020-000
PM
2018
70020:00
PM
2018 7-0,20-000 PM
Analyst: CTB
11 1-Dichloroethene ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
1,2-Dichloroethane ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
MEK ND 2.50 mg/L 100 7/4/2018 2:16:00 AM
Benzene ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
Carbon tetrachloride ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
Chlorobenzene ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
Chloroform ND 0.500 mglL 100 7/4/2018 2:16*000 AM
Tetrachloroethene ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
Trichloroethene ND 0.500 mg/L 100 7/4/2018 2:16:00 AM
Vinyl chloride ND 0.200 mg/L 100 7/4/2018 2:16:00 AM
Qualifiers: � Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
E Value above quantitation rang
M Manual Iniegration used to determine area response
N Tentatively identified compounds
0 RSD is greater than RSDlimit
PL Peiiiiit Limn Origtnal
n Reporting Defection Limit
Page 7 of 27

CLIENT:
Matrix.
Lab ID.
Project:
17 N�V I ; 10 �l - I I il E N' I A L 1. ip'! C J4 0
Ami ( Crm I L;-j- L ila 0K
Sioninit Envh-coni?iental Technologies, Inc.
Mir 3310 Pfl'in St.
LO, I L �3 ���, � u'Zl)�cr�?Og'C7 .FQ1lS, d�`iro ��.2.�.3
TEL: [phone] FAX." [phone]
Tfl'ebsite: hge.-Ilit)lt)i.v.settelic-coi-ii
Synagro
SLUDGE
18061305-OOIA
Oxford TCLP 2018
Port
(base report)
W0#1h 18061305
Date Reported:
7/24/2018
Tag Number:
Collection Date: 6/21/2018 12:30:00 PM
Client Sample ID Oxford TCLP 2018
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB=SOLID
TCLP VOLATILES ANALYSIS
SW1 311 M
Analyst: CTB
Surr.-
4-Bromofluorobenzene
107
70-130
%Rec
100
7/4/2018
2.1
Sum.
Dibromofluorom ethane
106
70-
130
%Rec
100
7/4/2018.2-11
Sum-
Toluene-cI8
105
70-130
%Rec
100
7/4/2018
2-01
RC1wwS0LID=W/ IGNITABILITY1030
REACTIVE CYANIDE (901417 m3 3.2)vwSO LID
Cyanide, Reactive
RC1mS0LIDwmW/ IGNITABILITY1 030
IGNITABILITY OF SOLIDS (SW=846m. 1030)
Ignitability
RCkSOLID-W/ I
PH (SW9045D)
pH
GNITABILITY1030
RCI=SOLID=W/ IGNITABILITY1030
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
0
ND
non-flammable
M9,001
SW9014
0.500 mg/Kg 1
Qualifiers** value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column conf rn-ta#ion exceeds
R RPD outside accepted recovery limits
SW11 030
1
s.u. @21.7C 1
SW9034
F
25.0 mg/Kg 1
6:00 AM
6-000 AM
6-000 AM
Analyst: MS
6/25/2018 2:29:00 PM
Analyst: AJT
7/23/2018 2:00:00 PM
Analyst: DHC
7/9/2018 5:18:00 PM
Analyst: MS
6/25/2018 2,0290MOO PM
E Value above quantitation range
M Manual Integratian used to determine area response
N Tentatively identified compounds
0 RSD is greater than RSDfirnit
PL Permit Limit original
RL Reporting Detection Limit
Page 8 of 27

I - �. _ Suininit Envirownental Technologies, Inc.
JIVI 10 3310 min St.
N V IH 0 N M E N i-f-k L -IEC R t4 0LO eul I E -510 'N C, Ctijwhoga Faits, UI17'0 442Z3
Accredi'tatt'on Program
A alytes Report
Analytic.0 TEL: [phone] FAX- [phone] WO#w 18061305
Website. httpV'01livivw.settek.coin 24-wJul-18
Client: Synagro State: NW
Project: Oxford TCLP 2018 Program Name. NC WW SCM
Sample ID Matrix Test Name Analyte Status
1110 1 --- I
18061305-OOIA Sludge Ignitability of Solids (SW-846: 1030) Ignitability A
Sludge pH (SW9045D) Hydrogen Ion (pig A
Sludge Reactive Cyanide (9014/7.3..3.2)-Solid Cyanide, Reactive U
Sludge Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U
Sludge TCLP Herbicides Analysis (SWI 311/815 1) 2:,4,5-Tp A
Sludge TCLP Herbicides Analysis (SW1311/8151) 2,4-D A
Sludge TCLP Herbicides Analysis (SW1311/8151) DCAA A
Sludge TCLP Mercury Analysis (SW1311/7470) Mercury A
Sludge TCLP Metals Analysis (SW 1311/60 10) Arsenic A
Sludge TCLP Metals Analysis (SW1311/6010) Barium A
Sludge TCLP Metals Analysis (SW1311/6010) Cadmium A
Sludge TCLP Metals Analysis (SWI 311/60 10) Chromium A
Sludge TCLP Metals Analysis (SW13ll/6010) Lead A
Sludge TCLP Metals Analysis (SWI 311/60 10) Selenium A
Sludge TCLP Metals Analysis (SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis (SW1311/808 1) 232r,3,3 ,4,4r 55,5`,6156 A
NC WW SCM
Decachlorobl"phenyl.
Sludge TCLP Pesticides Analysis (SW1311/808 1) Chlordane,, total
Sludge TCLP Pesticides Analysis (SW1311/808 1) Endrm'
Sludge TCLP Pesticides Analysis (SWI 311/808 1) gamma-BHC
Sludge TCLP Pesticides Analysis (SW1311/808 1) Heptachlor
Sludge TCLP Pesticides Analysis (SW 13 11/8 08 1) Heptachlor epoxide
Sludge TCLP Pesticides Analysis (SW1311/808 1) Methoxychlor
Sludge TCLP Pesticides Analysis (SW1311/808 1) Tetrachloro-m-xylene
Sludge TCLP Pesticides Analysis (SWI 311/808 1) Toxaphene
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) IA-Dichlorobenzene
Sludge TCLP Semi-Volatfles Analysis (SW1311/8270) 2,4,5-Trichlorophenol
Sludge TCLP Seml*-Volat fles Analysis (SW1311/8270) 2,4,6-Tribromophenol
Sludge TCLP Seini-Volatiles Analysis (SW1311/8270) 2,4,6-Trichlorophenol
Sludge TCLP Setni-Volatiles Analysis (SW1311/8270) 2.4-Dinitrotoluene
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2-Fluorobiphenyl
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2-Fluorophenol
Key I{ey
A Accredited NC WW SCM U Unavailable
0
M
M
FAI
0
A
A
0
A
A
A
A
Original 41
Page 9 of 27

F NVI R". Lo I 0A E NTA L ILI E C H N 0 LO 0 1 -F. 5
Siamnif Envii-onmental Technologies, Inc.
3310 Win St.
Cityahoga Falls, Ohio 44223
TEL: [phone] FAX. [phone]
W
���,.� ht�Y.,,,.,,,..,..,ette,�.c,,,,. 24-Jul-18
Client: Synagro State: NW
Project: Oxford TCLP 2018 Program Name: NC WW SCM
Sample ID Matrix Test Name Analyte Status
18061305-001 A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2-Methylphenol A
Sludge. TCLP Semi-Volatiles Analysis (SW1311/8270) 3,4-Methylphenol A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Cresols, Total A
Sludge. TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobenzene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachloroethane A
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
TCLP Semi-Volatiles
Analysis
(SW1311/8270)
TCLP Semi-Volatiles
Analysis
(SW1311/8270)
TCLP Semi-Volatiles
Analysis
(SW1311/8270)
TCLP Semi-Volatiles
Analysis
(SW1311/8270)
TCLP Semi-Volatiles
Analysis
(SW1311/8270)
TCLP Semi-Volatiles
Analysis
(SW1311/8270)
TCLP Volatiles Analysis
TCLP Volatiles Analysis
TCLP Volatiles Analysis
TCLP Volatiles Analysis
TCLP Volatiles Analysis
TCLP
Volatiles
Analysis
TCLP
Volatiles
Analysis
TCLP
Volatiles
Analysis
TCLP Volatiles Analysis
TCLP Volatiles Analysis
Sludge
TCLP Volatiles Analysis
Sludge
TCLP Volatiles Analysis
Sludge
TCLP Volatiles Analysis
ICey Key
A Accredited
NC WW SCM
U Unavailable
Nitrobenzene
Nitrobenzene-d.5
Pentachlorophenol
Phenol-d6
p-Terphenyl-d 14
Pyridine
1-J-Dichloroethene
1,2-D ichloro ethane
2-Butanone
4-Bromofluorobenzene
Benzene
Carbon tetrachloride
Chlorobenzene
Chlorofonn
D ibromofluo ro m ethane
Tetrachloroethene
Toluene-d8
Trichloroethene
Vinyl chloride
0
0
A
0
LAO
0
0
0
0
0
0
0
0
Gl
0
0
Original # 1
Page 10 of 27

ENVIRO IN 11 EINTAL
Client: Synagro
Project: Oxford TCLP 2018
Sample ID mb-32833
Client ID: PBS
Analyte
I 1 1 -Dichloroethene
12-Dichloroethane
MEK
Benzene
Carbon tetrachloride
Chlorobenzene
[fill mes 511711
Tetrachloroethene
Trichloroethene
Vinyl chloride
Sum 4-Bromofluorobenzene
Sum. Dibromofluoromethane
Sum Toluene-d8
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: httl2:llwww.settek.com
SampType-. MBLK
Batch ID.- 32833
Result
IND
IND
IND
IND
IND
ND
ND
ND
ND
50.0
48.7
51.3
TestCode. tc1ph-voc-IMST Units: mg/L
TestNo: SW8260B
I01 -4
0.00500
0.00500
0-0250
0.00500
0.00500
0.00500
0.00500
0.00500
0.00500
0.00200
61MVMff..r%
SWI 311 M
SPK Ref Val
QC SUMMARY REPORT
BatchED.
Prep Date*. 7/1/2018
Analysis Date-, 713/2018
%REC LowLimit HighLimit RPD Ref Val
50.00
100
70
130
50.00
97.5
70
130
50.00
103
70
130
WO#:
32833
RunNo: 86054
SeqNo-. 1616959
18061305
24-Jul-18
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quaaitiotation railge
H Holding Humes for preparation or analysis exceeded � A.7ialyte defected below quan�itaiian limits M Manual �z�.teg�ratzon used to determine
MC Value rs below Minimum Compound Limit.. ND Not Detected a RSD is greater than RSDIft-nit Original
P Second column confiurxnatian exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 11 of 27

%r Q 11011 A F N TA I CHNO LOG
,&r f. La" ra -to r) as
Client: Synagro
Project: Oxford TCLP 2018
Sample ID MB-32833
Client ID: PBS
Analyte
11 1-0ichloroethene
MEK
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chIorEde
Sum., 4-Bromofluorobenzene
Sum Dibromofluorom ethane
Sum- TolueneA8
Stimmit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga,Falls, Ohio 44223
TEL: [phone] FAX. [phone]
Website: httv:11www.settek. coin
SampType.- MBLK
Batch ID-. 32833
Result
ND
ND
ND
ND
ND
211
ND
ND
488
412
509
TestCode: telpmvoemmstr Units-. mg1L
TestNom. SW8260B
0.0500
0.250
0.0500
0.0500
0.0500
1111141I11
iXiM1I11
0.0500
0.0200
y Z! 1kre M ff M^
SW1311M
SPK Ref Val
QC SUMMARY REPORT
W0#0 18061305
BatchlDo
Prep Date: 71112018
Analysis Date: 712/2018
%REC LowLimit HighLimit RPD Ref Val
500.0
97.6
70
130
500.0
82.4
70
130
500.0
102
70
130
24mwJulw 18
32833
RunNo: 85971
SeqNo: 1615558
%RPD RPDLirnit Qual
r
Qualifiers:.* Value exceeds Maximum Contaminant Level. B Analyte detected in the assaciaied Method Blarik E Value above quaiititation1.
range
H Holding t es for preparation or analysis exceeded J .Analyte detected below quantitatl'on 11*mits M Manual hitegration used to determine
1\4C Value is below Minimum ��mp�und Limit. ND Not Detected � RSD is greater than RSDlimit Origi'nal
P Second column confinnatian exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 12 of 27

Summit Environmental Technologies, Inc.ILI JFW-1 f 3310 Win St. SUMMARY�� REPORT
E�G"�I:��?hJMEIVTt�L TE�IN�aC�L���;ES. CuyahogaFalls, Ohio 44223
AnalyHoa � L r) e 5 TEL: [phone] FAX: [phone] W0#0 18061305
Website: httv:llwww.settek.com 24-Jul-I8
Clients., Synagro
Project: Oxford TCLP 2018 BatchEDO 32855
Sample ID MB-32855 SampType: MBLK TestCode: HG TCLP(74 Units: PPM Prep Date: 7/3/2018 RunNo: 86042
Client ID: PBS Batch ID: 32855 TestNo: SW7470A SW7470A Analysis Date: 7/3/2018 SeqNo: 1616624
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua!
TCLP Mercury ND 0.00200
Sample ID LCSm32855 SampType-. LCS TestCode: HG TCLP(74 Units: PPM Prep Date: 7/3/2018 RunNo: 86042
Client ID: LCSS Batch ID: 32855 TestNo'.' SW7470A SW7470A Analysis Date: 7/3/2018 SeqNo: 1616625
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury 0.00363 0.00200 0.00400 0 90-8 80 120
Sample ID 18061322-OOIAMS SampType: MS TestCode: HG TCLP(74 Units: PPM Prep Date: 7/312018 RunNo-. 86042
Client ID: BatchQC Batch ID'.' 32855 TestNo: SW7470A SW7470A Analysis Date-. 7/3/2018 SeqNo: 1616627
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury 0.00391 0.00200 0.00400 0 97.8 75 125
Sample ID 18061322-OOIAMSD SampType: MSD TestCode: HG TCLP(74 Units: PPM Prep Date: 7/3/2018 RunNo: 86042
Client ID: BatchQC Batch ID-. 32855 TestNo: SW7470A SW7470A Analysis Date: 7/3/2018 SeqNo: 1616628
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury 0.00381 0.00200 0.00400 0 95.2 75 125 0.00391 2.59 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank- E Value above quan6tation range
H Holding times for preparation or analysis exceeded J Analyte detected below quanfitafion limits M Manual Integration used to determine
MC Valuel"s below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDII'mit
Original
P Second column confirmation exceeds PL Pem-iit Limit R RPD outside accepted recovery limits
Page 13 of 27

Client:
Project:
�P 4"J F4, Q IN 1 lr-- NTAL T��C014OLOG
A.v-w(t.r(-i`c,ai LHboratcrre,5
Synagro
Oxford TCLP 2018
Sample ID 18061322k-.001AMSD
Client ID-.
Analyte
BatchQC
L
SLIMM
Y �
rt Environmental Technologies, Inc.
3310 Win St.
CuyahogaFalls, Ohio 44223
TEL: [phone],FAX.- [phone]
Website: httg.0
llwww.settelc.com
SampType: MSD
Batch ID-. 32855
Qualifiers: Value exceeds Ma ximum Contaminant Level.
TestCode: HG,TCLP(74
TestNom. SW7470A
IZ7J
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
IV
i
PL
Units: PPM
SW7470A
n-%&W-01
1.
QC SU-IjN.IARY REPORT
BatchIDe
Prep Date: 7/3/2018
Analysis Date: 7/3/2018
%REC LowLimit HighLimit RPD Ref Val
Analyte defected in the associated Method Blank
Analyte detected belo
Not Detected
P e mi it L i'm it
w quantitatIoTi limits
W04:
32855
RunNo: 86042
SeqNom. 1616628
18061305
24o-Jul-18
%RPD RPDLimit Qua[
E Value above quanfitation rage
M Manual hitegration used to determine
0 RSD is greater than RSDIunit
R RPD outside accepted recovery limits
Original
Page 14 of 27

Summi"t Environmental Technologies, Inc. QC SUY-"MARY RIEP���
3310 Win St.
6.
E-N-VIRONME.NTb,L'T,ECOtJOLQGI,=.s, tvC.Cuyahoga Falls, Ohio 44223 WO#. 18061305
AraIYUcaI ���•TEL: [phone] FAX: [phone]
Website: htty:11www.settek. com. 24-Jul-48
Client: Synagro
Project: Oxford TCLP 2018 Batch]]D. 32886
Sample ID mb-32886
I Client ID-. PBS
Analyte
234-D
21415-TP
S u rr: DCAA
Sample ID Icso-32886
Client I D-.
Analyte
214-D
21415-T
S u rr:
LGSS
SampType-. mblk
Batch ID;
32886
Result
TestCode: tcllp-svoc-he
TestNo: SW8151A
r Units: mg/L
SW8151A
Prep Dade
Analysis Dade
71312018
7111/2018
PQL SPK value SPK Ref Val %REC LowLimit HighLimit
N D 1.00 0 0
N D 0.500 0 0
365 500.0 73.1 20 140
SampType: Ics
Batch ID: 32886
Result
TestCode: tcllp-svoc-he
TestNo: SW8151A
r Units: mglL
SW8151A
17�7:�`i�F1
Prep Date: 7/3/2018
Analysis Date-. 7/1112018
PQL SPK value SPK Ref Val %REC LowLimit HighLimit
N D 1.00
0.500
0 72-.9
62.6
125
' N D 0.500
0.500
0 78.9
52.5
128
DCAA 449
500.0
89.9
20
140
Sample ID
Client ID:
I Analyte
2)4-D
21415-TP
18061305m001ams SampType-. ms TestCode
Oxford TCLP 2018 Batch ID: 32886 TestNo
Result PQL
' tGIP=SV0Gwhe
SW8151A
r Units: mg/L
SW8151A
Prep Dade
Analysis Date
RPD Ref Val
7/3/2018
7/11/2018
RunNo
Seq No
86440
1632755
%RPD RPDLimit Qual
RunNo
Seq Na
86440
1632756
%RPD RPDLimit Qual
RunNo
86440
SeqNo-. 1
632760
SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
ND
1.00
0.500
0
ND
0.500
0.500
0
Surr: DCAA 486 500.0
82.7
37
105
86.7
38
106
97.1
20
140
QuaflQualifiers:Value exceeds Maxiin
mum contamant Level. B Analyte detected in the associated Method flank E Value abase quanti*tafion range
H Holding tunes for preparah"on or analysis exceeded J Analyte detected below qua116itaton limits M Manual Integration used to detemi i*ne
MC Value is below Ml*n um Compound Li'mit. ND Not Detected 0 RED is greater than RSDIft-ni't Original
P Second column confizxaa.ation exceeds PL Pem-11"t Lunit R RPD outside accepted recovery limits
Page 15 of 27

Client:
Project:
F T
NVIRr.
L rANN&
Synagro
Oxford TCLP 2018
Sample ID 18061305-001amsd
Client ID: Oxford TCLP 2018
Analyte
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga,Falls, Ohio 44223
TEL: [phone] FAX-.- [phone]
Website: httI2.011www.settek. con?
SarnpType: msd
Batch ID: 32886
Result
TestCode: tclp-svoc-her Units: mglL
TestNo: SW8151A
SPK value
QC SUMMARY REPORT
BatchID:
Prep Date: 7/3/2018
SW81 51A Analysis Date: 711112018
SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
W04:
32886
RunNo: 86440
SeqNo-., 1632761
18061305
24-Jul-18
%RPD RPDL'Imit Qual
274-D ND 1.00 0.500 0 84.9 37 105 0 0 30
27415-TP ND 0.500 0.500 0 89.6 38 106 0 0 30
S u rr: DCAA 502 500-0 100 20 140 D
Q u A ifi e rs Value exceeds Maximum Contaminant Level. B Analyte detected fil the associated Method Blank E Value above qum-ititation range
H Holding times for preparation or analysis exceeded J Analyse defected below quantitation h"mits M Manual Integration used to determine
MC Value is below Minfinum Compound Limit. ND Not Detected 0 RSD is greater than RSDInnit
P Second column confunlaiion exceeds PL Permit LM'II't R RPD outside accepted recovery limits
Original
Page 16 of 27

Client:
Summit Environmental Technologies, Inc.
I%Pl 3310 Win St.
EN V I` ID N F.1FNTA4C"t40Lr4ji�S.it�C Cuyahoga Falls, Uhlo 44225
Analvf$lcaf Lzbcraxo.rie5 TEL: [phone] FAX [phone]
Synagro
Website: http://Www.settelc-con7
QC SUMMARY REPORT
Project: Oxford TCLP 2018 Batch]HD: R85806
Sample ID 18061330-OOIAMS
Client ID:
Analyte
BatchQC
Cyanide, Reactive
SampType: MS
Batch ID: R85806
Result
a
TestCode: Cyanide,Rea
TestNoffi. SW9014
0.500
Units: mg/Kg
SPK value SPK Ref Val
Prep Date:
Analysis Date: 6/25/2018
%REC LowLlmit HighLimit RPD Ref Val
10.00 0 97.4
122
WO#:
RunNo: 85806
SeqNom. 1608659
18061305
24mwJul-48
%RPD RPDLimit Qua[
Sample ID 18061330=OOIAMSD SampType: MSD TestCode-. Cyanlide,Rea Units: mg/Kg Prep Date: RunNo: 85806
Client Id: BatchQC Batch ID: R85806 TestNo: SW9014 Analysis Date: 612512013 SeqNo-. 1608660
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive
9.62
0.500
10.00 0 96.2
81.6
122
9.739
1.20 5
Qualifiers: Value exceeds Maximum Contaminant Level.
B Al-talyte detected in the associated Method Blmik
E
Value above quanti'tation range
H Holding tunes for preparation or analysis exceeded
J Analyte detected below quanfitafion Hmits
M
Manual Integration used to detennm'e
4 MC Value is below Mlnl*lTlum Compound Limit.
ND Not Defected
a
RSD is greater than RSDIlmi't
P Second column confirmation exceeds
PL P e nu it L i'm it
R
RPD outside accepted recovery limits
Original
Page 17 of 27

Summit Environmental Technologies, Inc.
ENVIRONMENTAL TEC"NOL.00.11a&:�L'9�
AIVIy ff=i'.0zoa;ralprl�es TEL: (330)
Client: Synagro
Project: Oxford TCLP 2018
Sample ID MB-RB5806
Client ID:
Analyte
PBW
Cyanide, Reactive
Sample ID LCSwR85806
Client ID:
Analyte
LCSW
cyanide, Reactive
SampTypem MBLK
Batch ID: R85806
Result
ND
SampTypem. LCS
Batch ID: R85806
Result
9.91
3310 Win St.
Cuyahoga Falls, Ohio 44223
253-8211 FAX: [phone]
Website: Attp:llwww.settek.com
TestCode: Cyanide,Rea
TestNo: SW9014
PQL
0.500
Units: mg/L
SPK value SPK Ref Val
TestCode: Cyanidle,Rea
TestNo: SW9014
Units: mg/L
PQL SPK value SPK Ref Val
0.500
QC SUMMARY RIE0P RT
BatchED.
Prep Date:
Analysis Date: 6125/2018
%REC LowLimit HighLimit RPD Ref Val
Prep Date:
Analysis Date: 6125/2018
%REC LowLimit HighLimit RPD Ref Val
10.00 0 99.1 85 115
W0900
RunNo-. 85806
SeqNo: 1608644
18061305
24-JuI48
%RPD RPDLimit Qual
RunNo: 85806
SeqNo.m 1608645
%RPD RPDLimit Qual
Qualifiers: Value exceeds Maxu'num Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H molding times for preparation or analysis exceeded J Analyte detected below quantlotation limits M Manual kitegration used to determine
MC Value is below Minimum Compound Limit. ND Not Defected 0 RSD is greater than RSD11-ml*t Original
P Second colunui confu7mation exceeds PL Permit Ln"ni't R RPD outside accepted recovery limits
Page 18 of 27

ENVIRO NId�h1TAl,�Eai
�MOLfDCiO 1:6.. IFC..6
Armlythzal tar��rs.rari��
Client: Synagro
Project: Oxford TCLP 2018
Sample ID 18061330-001AMS
Client ID:
Analyte
BatchQC
Sulfide, Reactive
SampType: MS
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga,Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
website.- http--Ilwww.settek.com
Batch ID: R85822
Result
4630
Sample ID
18061330-OOIAMSD
SampType:
MSD
Client ID:
BatchQC
Batch ID:
R85822
Analyte
Result
TestCode: Sulfide,React Units: mg/Kg
TestNo: SW9034
25.0
SPK value SPK Ref Val
40.00
TestCode: SuIfffi!de,ReaGt Units: mg/Kg
TestNo: SW9034
PQL
SPK value SPK Ref Val
QC SUMMARY REPORT
BatchlDo0
Prep Date:
Analysis Date: 6/25/2018
%REC LowLimit HighLimit RPD Ref Val
95.6 80 120
Prep Date:
Analysis Date: 6/25/2018
%REC LowLimit HighLimit RPD Ref Val
W0#:
R85822
RunNo: 85822
SeqNo: 1609030
18061305
24-Jul-18
%RPD RPDLimit Qual
RunNo: 85822
SeqNo: 1609031
%RPD RPDLimit Qua]
Sulfide, Reactive 4740 25.0 4800 40.00 97.9 80 120 4630 2.35 30
Qualiffiers. 'k Value exceeds Ma,?Mum Cojitaminajit Level. B Analyte detected in the associated Method Blank E Value above quamfitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual bitegration used to deteni-iine
MC alue xs below MinimumGCompound Limit.NDmat Detected Q RSD is greater thanRSDlunit �OriginalV
P Second column conf rnlatioll exceeds PL Permit Limit R RFD outside accepted recovery limas
Page 19 of 27

E M V 1 6R 0 N fil F H T. L 7 C L �IG IS,
NZ
j
.AnafyU i 4-1--eTI-TtI_J1F9 .1,20 f 0 rl 95
Client: Synagro
Proiect. Oxford TCLP 2018
Sample ID MB-RB5822
Client ID:
Analyte
PBW
Sulfide, Reactive
Sample ID LCS-mR85822
Client ID:
Analyte
LCSW
Sulfide, Reactive
Qualifiers..6
H
MC
P
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website.- htto:llwww.settek.com
SampType: MBLK
Batch ID: R85822
Result
SampType,., LCS
Batch [Do. R85822
Result
TestCode: Sulfide,React Units: mglL
TestNos. SW9034
PQL
25.0
SPK value SPK Ref Val
TestCode: Suffide,React Units: mglL
TestNo: SW9034
PQL SPK value
SPK Ref Val
QC SUMMARY REPORT
Prep Date:
Analysis Date: 612512018
%REC LowLimit HighLirnit RPD Ref Val
Prep D ate:
Analysis Date.- 6/2512018
%REC LowLimit HighLimit RPD Ref Val
4660 25.0 4800 0 97.1 85 115
WO#Wa
Iffoo,W611m,
RunNo: 85822
SeqNo-. 1609015
18061305
24,--Ju148
%RPD RPDL'jm'It Qual
RunNo: 85822
SeqNos. 1609016
%RPD RPDLimit Qua]
Value exceeds Maximum Contamu'lant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
Holding tines for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Value is below Mh-in`num Compound Limit. ND Not Detected 0 RSD is greater Than RSDIH'ui't
Second column confirniation exceeds PL Permit L fini t R RPD outside accepted recovery limits
Original
Page 20 of 27

N". 1k. -
MW W V a
Nhl"7 NTAL� CHt4o LC
Client: Synagro
Project: Oxford TCLP 2018
Sample ID CHECK 7
Client lD:
Analyte
LCSS
SampType: LCS
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] F,4X.- [phone]
Website: httj2,. d, //www.settek.coni
Batch ID: R86179
Result
TestCode: PH S(9045D)
TestNow. SW9045D
PQL
Units: s.u.@22.3C
SPK value SPK Ref Val
%REC
QC SUMMARY REPORT
BatchlD*0
Prep Date:
Analysis Date: 7/9/2018
LowLimit HighLimit RPD Ref Val
pH 7.0 7.0 0 99.6 90 110
Qualifiers,** * Value exceeds Maximum Contamm'ant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyse detected in the associated Method Blank
J Analyse detected below quzaititati'on limits
ND Not Detected
PL Permit Lftnit
1j
W0#:
R86179
RunNo: 86179
SeqNon. 1623498
18061305
24-Jid-18
%RPD RPDLimit Qual
E Value above quantitation range
M Manual hitegrati'on used to determm'e
0 RSD is greater than RSDII'mi't
R RPD outside accepted recovery limits
Original
Page 21 of 27

I
Client:
Proi'eete.
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
VNIFONPAF79TAI. C9NOL04344S, iMCuyahogaFalls, Ohio 44223
F,4X.-W04-0 18061305
��:�. T�L: [phone] 253-4489
website.- httv:llwww.settek.com 24-Jul-18
Synagro
Oxford TCLP 2018
Sample ID CHECK 7
Client ID:
Analyte
LCSW
SampType: LCS
Batch ID: R86179
Result
TestCode: PH OIL(9045 Units: s.u.@22.2C
TestNo: SW9045D
PQL SPK value SPK Ref Val
%REC
BatchID:
Prep Date. -
Analysis Date: 7/9/2018
LowLimit HighLimit RPD Ref Val
pH 7.0 7.0 0 99.3 90 110
SamplelD
18070425=OOIADUP
SampTypem.
DUP
TestCode,.,
pH Oil(9045 Units: s.u.@22.9C
Client ID:
BatchQC
Batch ID:
R86179
TestNo:
SW9045D
Analyte
Result
PQL SPK value SPK Ref Val
%REC
Prep Date:
Analysis Date: 7/9/2018
LowLimit HighLimit RPD Ref Val
pH 5.4 0 0 5.3
RunNo: 86179
SeqNo: 1622920
%RPD RPDLimit Qual
RunNom. 86179
SeqNo: 1623459
%RPD RPDLimit Qual
0.7 10
Qualifiers:�` Value exceeds Max`num Contaminant Level. B Analyse detected in the associated Method Blaiik E Value above quantitafion range
H Holding times for preparation or analysis exceeded J .Analyse detected below quanfitation limits M Manual integration used to determine
0
MC Value is below Minimum Compowid Limit. ND Not Detected 0 RSD is geater than RSDIU'nIt original
P Second colunul confinnafion exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 22 of 27

Client:
Project:
Lz'
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga,Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: hgp:llwww.settek.com
Synagro
Oxford TCLP 2018
Sample ID LCS-R86179
Client ID:
Analyte
pH
LCSW
Sample ID I8061704-w005ADUP
Client ID:
Analyte
pH
BatchQG
SampType: LCS
Batch ID: R86179
Result
7.0
Sam-pType. DUP
Batch ID: R86179
Result
6.9
TestCode: pH,.NPW(450 Units: s.u.@21.8C
TestNo: SW9045D
PQL
SPK value SPK Ref Val
TestCode: pH..P,,NPW(450 Units: s.u.@20.8C
TestNo: SW9045D
PQL
SPK value SPK Ref Val
%REC
QC SUMMAR� I1��'ORT
BatchlDo
Prep Date:
Analysis Date: 7/912018
LowLimit HighLimit RPD Ref Val
�i •
Prep Date:
101.4
Analysis Date: 7/9/2018
LowLimit HighLimit RPD Ref Val
I
18061305
24-Jub-18
R86179
RunNo: 86179
SeqNo-. 1622722
%RPD RPDLlm*lt Qua
RunNom. 86179
SeqNo: 1622724
%RPD RPDLirnit Qua]
0.4 5
Qualifiers: Value exceeds Maxu'num Contamm'ant Level. B Analyte detected in the associated Method Blank E Va1ue above qumititation range
H Holding times for preparation or analysis exceeded J Analyse detected below quantitafion limits M Manual Integration used to detennm'e
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDIMaliot Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery Ii *ts
Page 23 of 27

Summit Environniental Technologies, Inc. QC SUMMARY REPORT
its lytipol 171 3310 Win St.
E�x1�lri�? �J1��'NT.p,I.'��hiE,1�+L4•�l�$. �tVP� Cuyahoga Falls, Ohio 44223
A-reatyUcaf Lzb!ora.roi1eF- TEL: [phone] FAX. [phone] W0#: 18061305
Website. http.-Ilwww.settek.com 24-Julp-4 8
Client: Spiaaro
Project: Oxford TCLP 2018 BatchlD.. R86713
Sample ID LCSmR86713
SampType: LCS
TestCode:
Ignitability_S Units:
Prep Date:
RunNo: 86713
Client ID: LCSS
Batch ID: R86713
TestNo:
SWI030
Analysis Date: 7/23/2018
SeqNo: 1645842
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 7.41 7.240 0 102 70 130
Sample ID 18061305mOOlADUP
SampType: DUP
TestCode:
Ignitabillity_.S Units:
Prep Date:
RunNo: 86713
Client ID: Oxford TCLP 2018
Batch ID: R86713
TestNo:
SW1 030
Analysis Date: 7/23/2018
SeqNo: 1645844
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
SamplelD 18070553mOOlADUP
SampType: DUP
TestCode:
Ignitabillity.­.S Units:
Prep Date:
RunNo: 86713
Client ID: BatchQC
Batch ID: R86713
TestNo:
SW1 030
Analysis Date: 7/23/2018
SeqNo-. 1645846
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
SamplelD 18070827-001ADUP
SampType: DUP
TestCode: Ignitabillity..S Units:
Prep Date:
RunNo: 86713
Client ID: BatchQC
Batch ID: R86713
TestNo: SWI030
Analysis Date-, 7/23/2018
SeqNo: 1645848
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Qualifiers: Value exceeds Maximum Contaminant Level. B Pmalyte detected in the associated Method Blank E Value above qumiti'tation range
H Holding tunes for preparation or analysis exceeded J Analyte detected below quantitafion limits M Manual Intecrrafion used to detennmde
MC Value is below Ml'n'mt�m Compound Limit. ND Not Detected Q RSD is greater than RSDIum-nit Original
P Second column confirmation exceeds PL Permit Limn R RPD outside accepted recovery limits
Page 24 of 27

Client:
Sunimit Environmental Technologies, Inc. QC SUMMARY R PORT
tj I%fk#N k I 1I 3310 Win St.
INVIRON�dFNT�tI. TEC"NOL� ,�:s, 1:.r..,_ Cuyahoga Falls, Ohio 44223
TEL [phone] FAX.- [phone] W04.0 18061305
Website: hqp:11www.settek. com 24o-Ju lo- 18
Synagro
Prjoect: Oxford TCLP 2018 BatchlD...9 R86713
Sample ID 18070827=001ADUP SampType
Client ID: BatchQC Batch ID:
Analyte
DUP
R86713
Result
TestCode: Ignitabillity.S Units:
TestNo: SWI 030
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 7123/2018
%REC LowLimit
HighLimit
V,�l:Z�`iTF11
RunNo: 86713
SeqNo: 1645848
%RPD RPDLimit Qua[
SamplelD
18070849m001ADUP
SampType:
DUP
TestCode:
IgnitabilitY S Units:
Prep
Date:
RunNo:
86713
Client ID:
BatchQC
Batch ID:
R86713
TestNlo:
SWI030
Analysis
Date-. 712312018
SeqNow.
1645850
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua!
Ignitability non-flammable D 01 20
Sample ID
18070849-002ADUP
SampType:
DUP
Client ID:
BatchQC
Batch ID:
R86713
Analyte
Res u It
TestCode: Ignitabillity S Units:
TestNo*. SWI 030
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 7/23/2018
%REC LowLirnit HighLimit RPD Ref Val
RunNo: 86713
SeqNo: 1645852
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Qualifiers: Value exceeds Maximum Contaminant Level. B Analyte detested in the associated Method Blank E value above quantitation range
H Holding limes for preparation or analysis exceeded J Analyte detected below quantitatimon 110mits M Manual Integration used to deten-nm'e
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDII'mit Original
P Second column confirnlation exceeds PL Permit Lunn R RPD outside accepted recovery limits
Page 25 of 27
'N

]EMM-ROMMENTAL TECHNOLMS-91. INOW
3310 VAR Ser+eN
cuw.hO". Pallor Okla 44223
DC;wQACOC33-8 R.cv.0
EffeW ve Dat e: 12AD 911i
Ana IY so ]Zequest lChain of Cust
For Summit En
VIT egaWE Techn-ol+vgies, Inc. use only
age 1 of 1
Page 26 of 27

Sumnil"t Envi"ronmental Teclmologles, Inc.
3310 ff7in St.
MID%# K-im- _91M I I rh4,'VIRONP#IEN'-j'ALTF.CHIYOLOCi-E!'-:ft, Inc.Czryal7ognFalls, Ohio 44223 sample Log -In Check I Ist
Arr3ivt-1r..31 Lsbaralorfes TEL: [phone] FAX.' [phone]
T47ebsite,p & hIU2://tivrviv.settek. cont
Client Name: SYN-oNCw27028 Work Order Number: 18061305 RcptNo: 1
Logged by:
Christopher Livengood
Completed By: Christopher Livengood
Reviewed By:
6/22/2018 10:20:00 AM
6/22/2018 1:47:05 PM
M
I "A epir R..T, am - F., :
Jennifer Woolf A1*2_r%191)1R 19011)EAR PM �+'�'*� ►��"''"'�' +'
Chain of Custod
s chain of Custody complete?
2. How was the sample delivered.?
Log In
3, Coole
rs are present?
4. Shipping container/cooler in good condition?
seals intact on shipping container/cooler?
Seal Date:
attempt made to cool the samples?
Custody
No.
5. Was an
6. VVere all samples received at a temperature of >D° C to 6.0'C
7. Sample(s) in prope
$. Suff icie
r container(s)?
nt sampie volume far indicated tests}?
yu Are samples (except VGA and UNU) properly presented?
10, Was preservative added to bottles?
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
12. Were any sample containers received broken?
13, Does
paperwork match
bottle
labels?
(Note
discrepancies on
chain
of custody)
14. Are matrices correctly identified on Chain of Custody?
1 5, is It clear what analyses were requested?
16:. Were all holding ti
mes able to be met?
(IT nonoTIry cusiomer ror autnorizaiion. )
0
SDectalId Handlina i
170
if applicable
NEENEEPM
Was client notified of all discrepancies with this order?
Yes❑
UPS
No ❑
Yes V N o ❑
Yes N o ❑
Yes ❑ N o ❑
Not Present ❑
NA ❑
Not Present 0
Signed By:
Yes ❑O N o ❑ N A ❑
Yes 0 No I I NA F-1
Yes N o ❑
Yes N o ❑
Yes N o ❑
Yes ❑ N o ❑ NA 0
NA
Yes ❑ N o ❑ No VOA Vials ❑�
Yes ❑ No ❑�
Yes No ❑
Yes No ❑
Yes No ❑
Yes N o ❑
Yes F-1 No ❑ NA ❑�
_ __ .,�...,.
Person Notified: Date
1
_�a.z__ _ -- L_i:sraa�ra�+�� �LQ.ra►�.L.==- •'Y'i: .!~ :_li'�1�
By Whom: Via: eMail Phone Fax I n Person
------- .........
�i
_ � _ _ _�`''�►�,.__—.Ra•��MliYRJ..r,ili'. iiL'3Y.'�1�LiTeVti-.L+AR�S�Of
Regarding:
------------------ ----
W {e. "m;A--.�i{
Client Instructions:
18. Additional remarks:
Additional sample reed an 7-13-18/1 0h.25 via UPS in cooler wl ice temp. of 4.2°
Cooler Information
Cooler No
Temp °C
� Condition
Seal Intact
I Seal No
Seal Date
Signed By
1
423 i
Good
Not Present'
�
Page 27 of 27

i
• • • a a ua�_��. � � aa� • � _ ' a_ � a __ ____ ____'_' �• ��� • � � as a�a � + a _a_. a T_..r fir: ..•__a__l:—.�1: +•_fit.;
.� ti_••l•r•
J •hr.. •{:
• � .~i• �.x••ti.ytC4 �.V1
M1�M1r M r
[� L
v}�
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
MocksvilIe, NC 27028
Meritech Work Order It 11061977
Parameters
Total Solids
Fecal Coliform
Meritech, Inc.
Environmental aboratory
Laboratory Certification No. 165
Results
Sample: Oxford 1 Grab
3,04901r
(SIudge) 1823 col/9 dry wt
Meritech Work Order # 110- 6- 1978
Parameters
% Total Solids
Fecal Coliform
Results
ftmm�
Analysis Date
11/8/19
11/6/19
Sample: Oxford 2 Grab
Analysis Date
3-A6 % 11/8/19
(SIudge) 51255 col/g dry wt 11/6/19
Meritech Work Order # 11061-979
Parameters,
% Total Solids
Fecal Coliform
Results
Sample: Oxford 3 drab
Analysis Date
3.53 % 11/8/19
[Sludge] 6,696 col/g dry wt 11/6/19
Meritech Work Order # 11061980
Parameters
Total Solids
Fecal Coliform
Results
Sample:: Oxford 4 Grab
Analysis Date
332 % 11/8/19
Sludge) 43-9 C 1//9 dY wt 11/6/19
Meritech Work Order # 11061981
Parameters
% Total Solids
Fecal Coliform (Sludge
Results
Sample: Oxford 5 drab
Analysis Date
3.49
7,554 co /g dry wt 11/6/19
Report Date:
Project:
Date SampleRcvd:
Reporting Limit
0-100
508 col/g dry wt
RevertinarLimit
0-100 % 10
508 col/g dry wt
Revortina, Limit
O*Ewl 00 0/f
J0
508 C01/9 dry wt
euorti LI'mit
01MM 110 0
508 C01 /gdrywt
eno ing Limit
0-100
508 col/g dry wt
642 Tamco Road, Reidsville, No Carolina 27320
tel.[phone] fax. 336 342"41522
Page 1
11/19/2019
Oxford
11/6/2019
11/6/19
Method
SM 2540B
SM 9222D
11/6/19
Method
SM 2540B
SM 9222D
11/6/19
Method
SM 2540B
SM 9222D
11/6/19
Method
SNI 2540B
SM 9222D
11/6/19
ethod-
M 2540B
SM 9222D

Contact: Ryan Copeland.
Client: Synagro
284 Boger Road
MocksVI'lle, NC 27028
Meritech Work Order# 11061982
Parameters
Total Solids
Fecal Coli'form
A4eri.' ecit, inco
Envirenmentai Laboratory
Laboratory Certification No. 165
Sample: Oxford 6 Grab
3e5I
(Sludge) 4Y144 1/9 dry wt
Meritech Work Order # 11061983
Parameters
% Total Solids
Fecal Coliform
(Sludge)
Results
Analysis Date
11/-8/19
11/6/19
Sample: Oxford 7 Grab
3.58 OY(o
5,587 col/ligd,11111"Ywt
Aq�lvsis Date
11/8)(19
11/6/19
I hereby certify that I have reviewed and approve these data.
I
Report Date:
Project
Date Sample Rcvd
Renortin
Limit
0-100
508 col/g dry Wt
ReDortill
Limit
0-100011111
�06
494 col/g dry wt
11/19/2019
Oxford
11/6/2019
11/6/19
Method
S
M 2540B
SM 9222D
11/6/19
Method
SN���� 2540B
SM 9222D
LaboratoryReprbsentative
642 Tamco load, Reidsville, No h Carolina 27320
tela(336)342-4748 fax.[phone]
IJ

8/9l18 Chain of Custody Record (COC) �+ NPDES#:
0
Client: J'����"Cs�t� Phone: '>>�'-C�
n
D Address: L5CG Fax:
ENVIRONMENTAL LABORATORIES �/1 oGvIV'� ALL N L EmailA
�'��Log
�„ VP� 642 Tamco Rd. Phone.* 336-342-4748 Project: ri��
Reidsville NC 27320 Fax: [phone] P.O.#:
Email: [e-mail] Attention: IZ�'r� � (�"�I�Ni� Turn Around Time*
*RUSH work needs prior approval,
How would you like your report sent? Cha.r-ges Alopiv
WWW.MeriI'Reci a )SCOM ,std, da s) 3�s 24:4IIFIrs
�---Circle all that apply EEmail preferred) Fax, Mail
afflf�ifd 0i�1 ��'�eS&-��f�ll��� Person Taking Sample (Sign/Print):
�� fZ�r�J o�-� � Lab use Only
Sample Location and/or ID # Start End Comp? #ofIs
Ri� On Ice? pH OK?
Date Time Date Tio�ne Grab? Cont. S � u ���� lu � Yes / No CI 01<?
0 A Th
6
1�
M. I M M
4C if Id
IP
Temperature Upon
Receipt:
Method oDechlorination (<0-.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in -the field prior to preservation.
Comments: Compositor #
Shipment:
❑ U PIS
Jug #
� Fed Ex Are these results for regulatory purposes? Yes � No O Report results in: mg/L ❑ mg/kg ❑ ug/L ❑
Relinquished by; � �' Date: Time: - �� - Received by.Hand Delivery � L�'{ Date: Time:
� Other Relinquished by. Date: Time: Received by: Date: Time:
Relinquished by, Date: Time: Re
_qelved by Lab; a

'W
Meritech,, Inc.
Environmental Laboratory
Laboratory Certification No.:165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Report Date:
Project:
Date Sample Rcvd:
12/12/2019
Oxford
11/6/2019
Vector Attraction Reduction Aerobicallv Digested Sludge (30 Dav Test
Meritech Work Order # 11061976
Total Solids
Sample.* Oxford Grab
Volatile S
Week 1 I-M09 0.6590
Week 2 1w26 Oa730
Week 3 L22 04700
Week4 113 0.650
Week 5 1m03 OM590
Van Kleeck Reduction(%): -12.91 1
I hereby certiy that I have reviewed and approve these data.
11/6/19
ids IN
�o Volatile Solids
La
OF
642 Tamco Road, Reidsville, North Carolina 27320
tei.[phone] fax.(336)342P--v1522
OmS40
0-w577
Ow5 70
Oz572
O*S70
a
ive

5.9.2016 Chain of Custody Record (COC) .� NP
DES#
:
1RClient: �1q1{PhonesV
�7z F. � "o Address: 7-15y �c�(�,�f� Y--�!�� Fax:
_L ENVIRONMENTAL LABORATORIES �I�J% C.ICSAI.Li-C I- Email: ��%�'EVV�� �} S;�N�fr(WF d d. I
• (.����1
r;�• `' ' 642 Tamco Rd. Phone-,,, 336-342-4748 Project; �������{i
lit
Reidsville NC 27320 Fax: [phone]------ ------
P.O.#:
Email: 1*[e-mail] Attention: ��i�'�ti1 Lc:(-�i:�r�1(� Turn Around Time*
[EEE`E�How would you like yallr report sent? *RUSH work needs prior approval.
w w w m e ro�:��;C�i�a�s.CoY'Yl ' Std(10vs)�S 24 - 48 Hrs
Circle all that apply: � Email ( (erred) , Fax, Mail
M(OIIt1� D���'� �t �fl��5 Person Taking Sample (Sign/Print); �� ,� Lab Use OnlyI V
Roml
Sample Location and/or ID # Start End
Comp? # of 10—
����r
��On Ice? Yes pH OI<?
Date Time Date Time Grab? Cont.� � � /N o Cl 01(?
Pow 0
)'9'
0
=i 6-®r �!� 'v2 li_�—Gtu
Temperature Upon Receipt71
*** Dechlorination (<D..5 ppm) of Ammonia, Cyanide, Phenol and TKN sam les must be done in the fieldprior topreservation.Method ofiP
Comments: Compositor #
ipment:
o BPS
Jug tNIEMEN
❑ Fed EX Are these results for regulatory purposes? Yes No � Report results in: mg/L ❑ mg/I<g ❑ ug/L ❑
Relinquished by: N •' ? Date: I Time: F �" Received by; Date: Time:
Hand Delivery t ' l
Relinquished by: Date: Time: Received by:Oti18f Date: Time:
Relinquished by: Date: Time: ReR;Fv7e2dm
by La ,. D
•� T