NCG500608_Regional Office Physical File Scan Up To 6/1/2020 Part 3

ATTACHMENT B
Discharge Water and Groundwater Infiltration Flow
Measurements and Calculations
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ATTACHMENT C
Punch Lists (7)
3
Purchase Orders
Boiler Stearn Receivers
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Chiller Room Cooling Tower 058 Pump
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Cooper Cooling Tower Pump
Water Flow Sensors/Dataloggers
Dechlorination System
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11/19/2017 Virginia Tech Mail-FW Motion Quote Customer RFQ#:PAT WELLSMEFP DAVIS OCN NG59378366
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MOTION INDUSTRIES Date:08/29/17
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PHONES 831P5
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Note:This estimate is v.Ind for 30 days anoints date shovm above
Prices quoted are for quantities shown.Stock is subject to prior sale.
j MTO quantities considered complete 105 underloverunless noted.
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To:BONAR INC QUOTE NUMBER: NC59-378366
j CANDLER,NC 217'.s-4508
CUSTOMER RFQ: PAT WELLSIJEFF DAVIS
j PO: PAT WELLS/JEFF DAVIS
F0.6.: FOB ORG,FRT PP8A00
7 REL: CONDENSATE PUMPS 460V
t QUOTE SENT BY: LARRY COOPER
1 TERMS: 1%10&25TH NET 30
DELIVERY: STOCK UNLESS NOTED
3
SHIPPING:
3
j Description Manufacturer QuanOty Unit Unit Price: Amount
LINE ITEM: 001 CUSTOMER LINE NO:1
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315GV6.1-114FCIPN:-22FH00 1 EA $794.670 $794.67
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3 1-112HP CONDENSATE PUMP 460/3/60
ITEM NO: 99999999 BURKS PUMPS
1
DELIVERY: 3 TO WEEKS AFTER RECEIPT OF ORDER, TO SHIP.
3
SHIPS FROM PIQUA, OHIO.
LINE ITEM: 002 CUSTOMER LINE NO:2
https://mall,google.mm/mail/ul0l?ui=2&ik=a59eO7bBd8&jsverCS87NgUoRx4.en,&New-pt&q=pat.wetls%40lowandbonscmm&gs=tme&search=query... 3/5

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} 11119/2017 Virginia TmJBMail-
FW:Motion Quote Customer RFQ#:PAT WELLSIJEFF DAVIS DON NC59-378366
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320GV6.1-114FCIPN:-26FH00 1 EA $794.670 $794.67
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2HP CONDENSATE PUMP 46013160
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? ITEM NO: 99999999 BURKS PUMPS
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LINE ITEM: 003 CUSTOMER LINE N0:1
330GV6.1-1I4FCIPN:-30FH00 i EA $858.970 $858.97
# 3HP CONDENSATE PUMP 46013160
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ITEM NO: 99999999 BURKSPUMPS
- Subtotal: $2,448.31
's Sales Tax: $0.00
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Total: $2,448.31
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- All Prices in USD
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Copyright©2001 -2017 Motion Industries, Inc. -All Rights Reserved. Legal Disclaimer, Privacy Policy,
Terms And Conditions, Provide Feedback
Motion Industries 1B0"Alton Rd. Birminahan-, Al- 35216, USA {2C61956-1142
BUYER UNDERSTANDS AND AGREES THAT GOODS PRESENTED TO BUYER PURSUANT TO THIS INVOICE ARE BEING TENDERED CONTINGENT UPON
BUYER'S AGREEMENT TO ALL OF MOTIONS TERMS AND CONDITIONS RELATED TO SALES.MOTIONS TERMS AND CONDITIONS ARE AVAILABLE AT
I THE MOTION BRANCH DRAT J'M.BUYERS ACCEPTANCE OF THE DELIVERY OF THE GOODS ARAI CONFIRM BUYERS
AGREEMENT TO UL OF MOTION'S TERMS AND CONDITIONS,
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This Mrrommo gon may contain confidential,proprietary or legal,privileged iMonnagon.It is imsederl for the m.(s)to whom fi is addressed only.If you ere
not an intended Haddam yen may net read.use,Namemal,disseminate ortake any merlon in reliable upon e.Pleaae noti,the sender by return e-mail thatyou
have received it in anerand immediately delete the enbm Communicagon,mousing any attachments.from your system.This e-mail has been sent in the course of
the business of a member of the Low&Boner group.In the Contmn ofttbe monitoring of professional emails this email and any responae to it or any other email
j sent to this address may he need by Chet MmPanR including in its Mpaaly se ea employer.
Mlpsl/mail.google.mm.aiVu/O77ui=2&ik=a59eO7b8d8&jsver-CS87NgUORx4.en.&Neer-pt&q=pat. lls%401owandbonanwm&qs--True&search query... 415

j ORIGINAL
Purchase Order
i Order Number 990000S
Vendor MOTION INDUSTRIES,INC. SH'p To Lo GBU!Sonwlnc.
P08OX 404130 A/P Emdl:0pnaI0sUcWandbonar.com
ALTANTA GA 30384 1301 Send Hill Read
Candler NC 287IS
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FA% 828 6843842 Contact Reeves,Yelmo
828 66 5035 eu9ness
828 6655051 FAX
Orderetl 08-02-17 height HarrtlknB Terms Prepay and Atld Paymentleims Net 30 Days
3 Requested 0-29-17 Delivery Ina.iom DELIVER REEVES/JEFF DAMS
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Currency Code USD
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...PURCHASE ORDER NUMBER MUST BE SHOWN ON ALL INVOICES AND PACKAGING THUS""
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SHIPPING LABEL REQUIREMENTS:
LOW& BONARPO%: 2900005
ANN:REEVES/IEFF DAMS
.......nw.................u....num.«............. ................
««««
PACKAGING REQUIREMENTS:MUST CLEARLY IDENTIFY PRODUCT
Line Rev Ilem Number Descnplion OrdWetl UOM Ural Pnce Extended Poce Due Dote
LQOJ 0 99999 G26FHT0F320GV6L-IM PC PUMP/ 1.0 EA 896A000 696.00 09.29-17
MOTOR 2 HP S75/3/60
2.0000 99999 22018GASKET,FLAL COMP, 160 EA 5.1500 82.40 09-29-17
4X5,56
3.0000 99999 22334 FLOAT ASSY 40 EA 1266003 50&. 09-29-12
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5 40000 99999 9038CG32 FLOAT SWITCH 20 EA 478.6000 957.20 09-W-17
ALTERNATOR
7
500l)0 99999 903>1+532 FLOAT SWITCH 2.0 EA 244.0400 488.05 09-29-17
� Nvoice Addmss Page I
Low and Bona Inc
130I Sand Hill Road
Asheville NC 28506
UNUTel
53
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ORIGINAL
Purchase Order
Line Rev Item Nambe, Descnalion Ordered UOM Unli Pnce Edended Pnce Due Dale
ERE QUOTE NO.NC59J76968 DATED 812/17.
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Total 2.930.W
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,9 Page 2
Invoice Address
Low and Bonar Inc,
1301 Sand!Hill Road
`j AfieNSe NC 288D6
United Stales
3

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ORIGINAL
I Purchase Order
Order Number 29001 OS
€ Vendor MOTION INDUSTRIES.INC. SNP To Low and Bones Be,l
PO BOX 404130 A/P Ema1:opeolasNbWandbonor.com
3 ALTANTA GA 30384 13ol Send Hill Road
Candler NO 28715
1
1
FAX 828 Sell Contact Reeves.Wlmo
°j 826 66S-5038 Business
828 665-505t FAX
Ordered 0802-17 Pongblsomdinglerms PreWyontl Add P aymenl iemss Nei pap
Requesletl 09Q9-IJ DeAvery lnslmcliorls DELIVER REEVES/JEfF DAVIS
I Curency-ace USD
i
1-1PURCHASE ORDER NUMBER MUST BE SHOWN ON ALL INVOICES AND PACKAGING LISTS."`
3 SHIPPING LABEL REQUIREMENTS:
S
tOWB BONAR PO#: 79001 OS
ATTN:REEVES/JEfF DAVE
.aria......................w«4uuuwuuu............
PACKAGING REQUIREMENTS:MUST CLEARLY IDENTIFY PRODUCT
Line Rev Item Number Description Ordered TOM U"t Price NoMed Price Doe Data
10000 99999 G26FH00F3XTGV6I-i/4fC PUMP/ 4.0 EA 896.0000 3,58400 09-29-17
j MOTOR.2 HP 575/3/60
Il REF: QUOTE NO,NC59-376968 DATED 812/I7.
`E3 Intel �- - --X584.00
5
j Invdce Addres_ Page I
ILow and Boner He.
1301 Sand Hill Road
Asl i®e NO 28®36
United States
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ORIGINAL
I Purchase Order
Order Number ]899]OS
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Vendor MOTION INDUSTRIES,INC. SNP to Low and Sonarlun.
3 PO BOX 4041W AIR Emal:apm1uda,and Vno,.com
ARANtA GA 30384 1301 Sand Hill Road
t CandlerNC28O5
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FAX [phone] Contact Reeves.Wilma
828 66550.98 Business
'1 828 6655051 FAX
Ordered 08'02-1I FreighlHanding Terms Prepayond Add Payment I. Net 30 Do,
RmmeMod 09-29-17 Delivery lmi.ciiom DELIVER REEVES/JEFF DAMS
3 C.yCodeUSD
S
--PURCHASE ORDER NUMBER MUST BE SHOWN ON ALL INVOICES AND PACKAGING LISTS—'
SHIPPING LABEL REQUIREMENTS:
LOW 8 SONAR POB: ]899]OS
ATTN:REEVES/JEFF DAVIS
««««e«...m.w..u.«.«««n..««........«...........e..««wm.«..........
? PACKAGING REQUIREMENTS:MUST CLEARLYMENTIFY PRODUCT
1 ❑ne R.Y Ile.Number Descdpiion Ordered UOM Unit Price Extended Price Due Dale
1.0000 99999 G22FHOOF315GV&1�1/4 PC PUMP/ 1.0 EA 896.0000 M6A0 w-29-17
MOTOR,1-1/2 HP,515/3/60
2.0000 99999 G30FH00F330GVb1-1MFC PUMP/ 20 EA 110100300 2,020.00 W-29-17
I MOTOR
7
HER QUOTE NO.NC59-376968 DATED 8/2/I7.
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- Yale 2.91600
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{ Invdce Address Page I
1 Low and Bonor In,
IWl Sand Hill Road
AshAVi NC 28806
Wuied Stales
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ALL BIDDERS
Phone
ward
Fax: SERVICES
' Bill TO Sales Quotation
7
t Fred Bailey
I Low&Bonar
1301 Sand Hill Road
Candler,NC 28715
f Ship to information
"Must Complete New BP Form" Quotation Number 5772
USA Sales Quote Amt. 15,800.00
Customer Code C10000
Document Date 09/29/17
Valid Until 10/29/17
Hem/Part# Material/Description Delivery City Unit Prim Ext.Amount
HachFlowMetering Hach SC200 Ultrasonic Flow Meter with 3 Wks ARO 1 $15,800 $15,800.00
10 foot cable
HachFlowMetering Hach SC200 Ultrasonic Flow Meter with 3 Wks ARO 1
a
50 fool cable
Custom Weir V-Notch,5 It weir plate,
Miscellaneous 304SS 3 Wks ARO 1
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2101-A Cambridge Beltway Dr. -Charlatte,NC 28273-Phone:[phone]-Fax: [phone]-mvrv.heyward.net

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BHC Utilities
QUOTE: 100
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25 Lavonia Ave.
Greenville SC 29609
Carolina cowbov03(aemai Lcom
PH: 864-304-3123
= Dear Fred,
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Thank you for the opportunity to quote the fallowing services:
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• Install(2)Ultrasonic Flowmeters and Hardware
• Install(1)Weir and Hardware
• Provide all Confined Space Entry,Safety Equipment and Gas monitoring
i e All Tools and materials for Job completion
3 • Project is coordinated with Equipment Supplier
• Price will include all Installation, materials,Safety and Supplies
• TOTAL-$3874.00
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Please let me know of an� Y questions.
Sincerely,
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Brent Epps
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ALL BIDDERS
PhoneXnevrward
Fax. Js E R V I C E S
Bill To
Sales Quotation
Fred Bailey
Low&Better
1301 Sand Hill Road
Candler,NC 28715
Ship to Information
j "Must Complete New BP Form" Quotation Number 5772
( USA Sales Quote Amt. 15,800.00
Customer Code C-10000
Document Date 09/29/17
Valid Until 10/29/17
hem/part# Material/Description Delivery Cty Unit Price Ext.Amount
Programming it Calibration
= Programming coordinated with conimed space i
nstaller
Paces do not include tax and are valid for a period of 30 days,after which time they are subject to
review.
1 -----------'-__..._....------
Freight
will be FOB facto Sub Total di prepaid antl added Atsi invoice.Terms are Net 30 days.received
before
ore an $15,800.00
ruder castandarn
Terms and.Credit
Cans rd
apply.a,signed purchase,Discover)
must be quote
be sign an
ruder can b r entered.CrekN Cartl orders(Visa,M1Aastemard,Discover)require quote to be signed
end faxed or e-mailed back.
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We appreciate the opportunity to be of assistance. If the above quotation -----------
results in an order,please address it to: Total Amount $15,800.00
7
Heyward Services
2101-A Cambridge Beltway Drive
Charlotte,NC 28273
{
If we can be of further assistance,feel free to contact us.
l Best regards,
Oudzinski,Sheila
[e-mail]
Heyward Services
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Signature Date '..
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3 2101-A Cambridge Beltway Dr. -Charlotte,NC 28273-Pbome 7041583-2305-Fax:[phone]-uewm.heyrvaM.net

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EQUIPMENT AND CHEMICAL PROPOSAL (PI off)
Stephen Jenkins
i Low and Bonar
PO Box 1057
Enka, NC
I 28728
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I Date: 17w October 2017
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RE: Chlorine Monitoring Apparatus
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I —Supply of dechlorination and free chlorine monitoring system as described $ 11,358.00
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• Includes supply of all equipment and tanks in scope above
• Includes one day of on site start up tech
• Pipework installation by others
• Power Supply and Electrical installation by others
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2—Supply of GC Formula 6600 dechlorination treatment $ 1,270.00
' • I x 55 gallon drum (60016)
• Price includes delivery, transfer to chemfeed unit and removal of empty drum
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CONFIDENTIAL-NOT FOR DISTRIBUTION
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Low&Boner PO Box
Enka,NC 28728
Progrear through performance lowandbanar.eom PUYChq$@ Order
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{ Order Number Bar OS
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j Vendor Gorrafl Callahan Company _ ShpTA Gewga lNkbwcic
045 COn4AERCE CIRCLE SW 6 CrI MDunlan Ridge
1 ATLANTA GA 3W36 - Ashevild NC WEBB
}
FAX [phone] Cool Ci Lowond Bonorinc.
BVuness
FAX
3
Ortlered 1D-18.0 Freight lion ngdims Prepoid PDymenl terms Net JD Days
Requested 10-18-17 Dow"In51mclion5 FOR:SIEVE JENKINS
- CUeency Code USD
E SPECIAL NOTE TO SUPPLER:THE ONLY LOW&BONAR,INC IL&BI PERSONNEL AUTHORIZED TO ACT AS PURCHASING AGENTS FOR L&B AND FINANCIALLY COMMIT OLT
1 TO WRITTEN OR VERBAL PURCHASE ORDERS ARE GEORGE THLOWCIC,ANA REESE,IVA SCHOLZ AND WILMA REEVES,L&B DOES NOT RECOGNIZE AND WILE NOT
3 HONOR,ANY VERBAL OR WRITTEN PURCHASE ORDER THAI IS NOT EXECUTED BY THESE INDIVIDUALS
j CONTACT GEORGE MKLOWCIC AT 838665-SOM WITH ANY QUESTIONS OR CONCERNS REGARDING THIS STATEMENT.
3
Z .. - .
i LOW&BONAR'SATTACHED TERMS&CONDITIONS ARE AN INTEGRAL PART OF THIS PURCHASE ORDER.FORMAL OBJECTION N HEREBY MADE BY LOW&SONAR INC TO
ANY ADDITIONAL OR DIFFERENT TERMS 5EILER MIGHT PROPOSE IN SELLER'S ORIGINAL PROPOSAL OR ACCEPTANCE OF THIS PURCHASE ORDER.
S —'PURCHASE ORDER NUMBER SHOULD BE SHOWN ON ALL INVOICES AND PACKAGING EISTV"
NO REVISION TO THIS PURCHASE ORDER SHALL BE EFFECTIVE UNLESS EVIDENCED IN WRITING BY LOW S BONAR CHANGE ORDER
NOTE: tOWANDRONAft 'TOBACCOUSAGE' BULLETIN APPLIES TO THIS PURCHASE ORDER
f
j Une Rev loor,Umbin DoieripBGn Osdeeed UOM JIM Ptice ENended GNA One DDIa
r I(r)0 OvOr- MONUORING SYSTEM. - —� IN EA 11,1581,00) - 1135809 ILo&I1
i OECHLORINATION AND FREE CHLORINE MONITORING SYSTEM
230001 99999 GC FORUMLA 66W IN EA 1,27NOKDo LDD.ID J1 L_17
3
j 55 GA ORUM6W LBSt OF GC FORMULA t6W 0ECLORINAl10N TREATMENT '.
R F NC R 1t-ChLAHAN PROPOSAL DATED OCIOBER I].201J '.
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Poge I
- AV PIEED SIGNTiVPE '
- AVIHwtIZEDSIGNANRE '.

ATTACHMENT D
Sampling Records
L&B Weather Records: October 2017
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Field Sampling Data
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Purchased Water Records
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Low&Banat—NPDE$Wastewater
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Combined Services Statement SERVICE ADDRESS BILL NUMBER
I City of Asheville and Metropolitan Sewerage District 1301SM011A LM 3193850
RECEIVED
ACCOUNT NUMBER - CUSTOMER NUMBER
CITY OF ASHEVILLE tl(}� 1010648 2155269
VresaiMPes� i7!
eo eex r3a ,US Pes4ge
i asxenu[xczesormaa me E _t
ADDRESS SERVICE REQUESTED Afi s� LAST PAYMENT POSTED 10/30/2017
j Permitr4zz LAST PAYMENT AMOUNT - $13373.59
I COLBOND INC CURRENT BILL DATE 11/15/2017
f PO BOX 1057 PAYABLE ON OR BEFORE 1 2/0 512 01 7
ENKA, NC 28728-1057 CURRENT CHARGES $11262.87
i g11•l.•14P Il,dl'i1lhPrrglP'h°hlPgallhlllll..111 — - — - _
[ BALANCE FORWARD $0.00
$112sz.a7
,3
' If you have any questions concerning this bill call Customer Services 1828)251-1122
1
Service Service Period Days Meter Number Current Previous Consumption
' WATER 1011WO17 to 11/13/2017 33 28140183 169012 164660 4352 CCF
DET MT( 10/11/2017 to 11/13/2017 33 76313643 950 950 0 CCF
fu tI - Total Consumption 4352 CCF
Ogg
WATER CONBUMPTION CHARGE $902.88
CAPITAL IMPROVEMENT FEE $1158.89
DETECTOR METER $0,00
a FREUNE $60A2
FIRELINE $114,69 _
BASE FEE $6.09 7FU]C�, �fSdS
I Total Oily $1126287 9 7
Mc '3 0t} 012
i wwtv.ashevillenc. ov • 828 251-1122 www.msdbc.or�' • 828 254-96A6
i Visit www.ashevikenc.9ov and click Online Services,Online Services Menu,then Utility Bill Payment for access.
Or enter the following web address in your browser https:llwlfservice.ashevillenc.gov/MSS/cilizens/default.aspx.
The City of Asheville will be dosed for Thanksgiving November 24-25.Holiday closings are December 22,25 and 26&for New Year's January
1,2018.
' Retain this person frewur records. Please tear below onp ffoonlon. See reverse side for Customer orcessuen.
PLEASE RETURN THIS PORTION OF STATEMENT WITH YOUR PAYMENT COLBOND INC
I USING THE SEND AND RETURN ENVELOPE. 1301 SAND HILL RD
PAYABLE ON OR BEFORE 12/05/2017
ACCOUNT NUMBER 1010648
t
CUSTOMER NUMBER 2155269
r
'BIU-NUMBER 3193850
CITY OF ASHEVILLE BALANCE FORWARD _ $0.00
P.O.BOX 733 CURRENTAMTDUE $11262,87 '..
ASHEVILLE,NC28802-0733 - -
TOTAL AMT DUE $11262.87
I IIIIIhIP'ulhiH'dPllu•IhIPIIIP9lll'•Illgl'il•hllhll AMOUNT OF PAYMENT
' Make Check Payable to:City of Asheville
I
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000060420180031938509E0011262870

2
3
ATTACHMENT E
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Equipment Information
i
Flow Meters
Dechlorination System
3
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Low&sonar—NPDES Wastewater
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HH P 6 pa tens
UNIVERSAL
-1339
. ER �. .
WITH ULTRASONIC
FLOW SENSOR
The SC,27-00 Universalk. Controller with
Ultrasonic Sensor is assigned to give highly accurate
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(
;�t,20J uc,usia) Specification, UltraSon;c Flow Sensor
Display Graphic dot matrix LCD with LED Flow Rate 0-9999,0-999.9.0-99.99 with
bacWighting,TransreHecfive selectable How rate units
Display Size 48 x 68 man(1.89 x 2.67 in.) Volume 0-9,999,999 with selectable volume
Display Resolution 240 x 160 pixels units
Heightx Width 144x 144 x 181 rareDepth 0.25 m(10 in.)to6m(20 ft.)
x Depth (5.7 x 5.7 x 7.1 In.) Measurement t1 mm(0.04 in.)
Range/Resolution
Weight 1.70 kg(3.751b)
Power 100-240 Vac tl0%,50/60 Hz; Air Temperature -40 to to 90°C(-40 to 194"F)
Requirements 24 Vdc-15%+20% - t0,1°C(0.18-H
Operating -20 to 60°C(-4 to 140-H, j Input Fitter 999 sec
Temperature 0 to 95%RH non-condensing Totalizers 8-digit reachable LCD software totalizer
Storage -20 to 70°C F4 to 158-H, Totalized Flow Gal.,its,acre-ft.,lit.,ms,ins
Temperature 0 to 95%RH non-condensing
Analog Output Signal Totalizer may be set to auto or manual
Two 0/4 to 20 m4 isolated current outputs,max 5000 mode.
Operational Mode (Menu option to reset is available in
F Primary or secondary measurement or calculated value manual mode only)
(dual channel only) ! Accuracy t0.5%of span
Functional Mode Repeatability x0.1%of span
Linear,Logarithmic,Bi-linear,PID Sensor Cable 10 on(33 ft.),20 an(66 ft.),
Optional 4 additional 4/20 mA isolated cunent outputs, pntegmq Lengths 50 an(164 fly),or 100 on(326 fly)
maz 5000®18-24 Vdc(customer-supplied power source)
Calibration Cal Depth 1 point;Cal Depth 2 point
Security Levels Twopassword protected levels Methods
j Enclosure Materials Polcarbonate,Aluminum(powder Operating - 75kHz
j coated),Stainless Steel Frequency
Mounting Wall,pole and panel mounting Construction NEMA 6P(IP68)potybulyene
Configurations temphthalate(PBn body with integral
1 Enclosure Rating NEMA 4X/IP 66 temperature sensor
Conduit Openings 112'NPT Conduit Weight -0.6 kg(1.1 fib)
Relays
Four electromechanical SPDT(Form C)contacts,1200W, Select from the Following Gauge Types:
5 A,250 Vac V Notch Weir
Operational Mode Rectangle Weir
' Primary or secondary measurement,calculated value '.. Rectangle Flume
(dual channel only)or timer
( Round Bot Flume
Functlonel Mode Cipolletti Weir
Alan,Timer,Feeder Control,PVVM or FM Control,
' System Alan Neyipic Flume
Digital MODBUS RS232/RS485, " Parshall Rome
Communication Profbus DPVi optional PFawns Rome
Memory Backup Flash memory Khafagi Flume
I Electrical EMC:CE compliant for conducted and L Lagco Flume
Certifications radiated emissions CISPR 11 (Class H Type Flume
A limits),EMC immunity EN 61326-1
' Qndustdai limits) - Trapezoidal Fume
User Defined
Safety:General Purpose UUCSA ':.
61010-1 with cE1Lus safety mark
- Data Logging Secure Digital Card(Maximum
recommended capacity 8 GB)or '..
j special RS232 cable connector for
data logging and performing software '..
3 updates.
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Dimensions
The S0200 controller unit can be installed on a surface,pared,or pipe(horizontally or verticaly). No tools are needed to connect the
controller unit to any Hach digital sensor.NOTE;Dimensions are in inches[millimeters].
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5.67
- [123.5] [43.11j
4.86 i]2
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Old U53 Sensor
4f 7 u, d .uli-r and Nloddi S r s Par`,. Nm bol rig Systcm 0 .0 ?3 -0 i2
1 LXV404 X -% �X A
i No power cord !0
No power mrtl Type-O-inatalletl sham reliefs i
T With Ed power cord installed with cord grip 2------------
` ---
WiithUKpowersendinstalledwithcardgdP
With US power send installed wfth card ghp _ __ _ 5
_ __sense.. _
24VCD power supply with no cord or cord grips 7 �
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' _Standard
t (two 4-20mA outputs)
MODBUS 232&485 ':'1—'':
Profibus DP 3
-,_ ---
HART+four4-29mA anaog autPWs
F Four additronal 4-20mA analog outputs '9
PH&00
Contlucttvfy 2
_Flow '._3
m Ainput
Digital 15 _—
None 0
PH&DO
Cord!uctivi_N_____. .. . ._._ 2 —..
� Flow __. _ 3
nWinput — d
Digital
Hach 2
u. ¢'IiGBt I 'Gis A cocs so I,
U53S010 Ultrasonic sensor vdth 10 R.cable 9220600 SC200 Weather and Sun Shield
U53s030 Ultrasonic sensor with 30 0.cable with UV Protection Screen
i
U53S100 Ultrasonic sensor with 100 ft.cable 8809200 S0200 UV Protection Screen
10001313088-001 Weather Protection Cover
9218M SD card reader(USB)for connection to PC
J 9202900 SC200 power cord with strain relief,125 Vac 92181OD 4 GB SD card
9203000 SC200 power cord Win strain relief, 9012700 Flow Module
j 230 Vac,European-style plug 9013100 Module for 4 additional analog mA out
(passive)
9013200 Modbus module
F
YAB104 Profibus DP kit
!. L.ZX887 Data coin cable
:3 3004A0017-001 Flow sensor mounting Wit
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5 Printed In IISA®NaM 2017 Nl n9fife mserwd.
- Mlip 'xeSlINmproh9bWWYb9Mpv'M�*hIN�AreselezlM ryYJfaeYaspaP'aMru(o a';uM�l&s'/[x ..
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Stephen Jenkins
Low and Bonar
PO Box 1057
Enka, NC
28728
s 17� October 2017
I
i RE:Chlorine-Ma Ao aratus
i
$ Dear Mr.Jenkins,
Thank you for considering Garratt Callahan for your project to monitor the free chlorine levels of the waste water
leaving your facility and the system to dechlorinate the stream before hitting the state waterways.
We have prepared the attached proposal based on information gathered during our visit.
3
E it you have any questions,please do not hesitate to get in touch with any one of your Garratt Callahan team.
Best Regards,
i
Matt Rose Mark Strudwick
1 Territory Manager Business Development Manager
(cell)—336.500.1346 (cell)—478.550.6496
j mrose@g-ccom [e-mail]
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3 CONFIDENTIAL-NOT FOR DISTRIBUTION
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Project Scope
Low&Bonar are required to monitor the free chlorine level in their wastewater discharge and remove any free
chlorine residual from the water prior to it leaving the site.
i
Currently free chlorine levels are in the 0,5— I.Sppm range leaving the site with a projected flow rate of
7 approximately 55,000 gallons per day.
All waste streams have been directed to a 250 gallon break tank before they overflow to a larger 500 gallon sump,
fro where they weir over to the site discharge line. Measurement of the free chlorine level upon entry to the tank,
dechlorination in the tank and sump and subsequent verification of the drop in free chlorine level is required in order
to meet the project goals.
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Proposed Equipment
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6660 N r wv
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259 CuJoe ymge Tank
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Picture 1 —Schematic drawing of proposed dechlorination and monitoring station
j
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j CONFIDENTIAL—NOT FOR DISTRIBUTION
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j ATTACHMENT
jSafety Data Sheets
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` C N O) ANSAFETY DATA SHEET
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SECTION I -PRODUCT IDENTIFICATION
PRODUCT NAME: FORMULA 6600
PRODUCT USE: DECHLORINATION
S RESTRICTIONS ON USE: Refer to label,available technical information,and other appropriate
sections of this SDS.
UN NUMBER: 2693
PROPER SHIPPING NAME: BISULFITES,AQUEOUS SOLUTIONS,N,O.S. (SODIUM BISULFITE),
j 8,PGIII
MANUFACTURER'S NAME: Garratt-Callahan Company
ADDRESS: 501ngold Road,Burlingame,CA 94010-2206
EMERGENCY PHONE: North America:CHEMTREC: 1-800-424.9300
Outside North America:+1-703-527.3887
BUSINESS PHONE: Product Information:6SO-697-5811
SDS NUMBER: SD6600
DATE OF REVISION: 11/30/2015
1
SECTION 2-HAZARDS IDENTIFICATION
i
j SIGNAL WORD:DANGER
HAZARD STATEMENT: P�yn
{ H314:Causes severe skin bums and eye damage, IC.
i
H335:May cause respiratory irritation. 3 -
PRECAUTIONARY STATEMENTS:(PREVENTION)
PIOI:If medical advice is needed,have product container or label at hand.
PI02:Keep out of reach of children.
PI03:Read label before use.
P260:Do not breathe dust/fume/gas/mist/vapours/spray.
P264:Wash all exposed skin hair thoroughly after handling.
P271:Use only outdoors or in a well-ventilated area.
` P280:Wear protective gloves/protective dothing/eye protection/face protection.
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NFPA RATING
HAZARDOUS MATERIAL IDENTIFICATION SYSTEM FLAMMABILITY
1 Haurd Scale
[ 0.Minimal
1=Slghe
2=Moderate HEALTH I
3-Serous INSTABILITY
t I PHYSICAL HAZARD(YELLOW) i I 4=Severe
* Chronic hanM '..
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OTHER
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WATER TREATMENT EXPERTISE SINCE 1904
FORMULA 6600 www.garrattcallahan.com Page I of

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SECTION 3• COMPOSITION/INFORMATION ON INGREDIENTS
Hazardous Ingredients CAS F!'Jt 1 S Yff
SODIUM BISULFITE 7631-90Z 231-548­0 NA 38-44
1
SECTION 4-FIRST AID MEASURES
Exposed individuals must be taken for medical attention if any adverse effect occurs.Take a copy of this SDS to the health professional with the
s Individual.P310:Immediately call a POISON CENTER or doctor/physician.
1
DANGER:Causes severe skin burns and eye damage.May cause respiratory irritation.Also refer to Section I I for symptoms,effects,and likely
routes of exposure for this product.
TARGETORGANS:
ACUTE:Irritation of skin,eyes,respiratory and gastrointestinal systems.
j CHRONIC:irritation of skin,eyes,respiratory and gastrointestinal systems.
SKIN EXPOSURE:P303+P361+P353:IF ON SKIN(or hair):Remove/take off immediately all contaminated clothing.Rinse skin with watedshower.
Minimum Bushing time Is for 15 minutes.P363:Wash contaminated clothing before reuse.P310:Immediately call a POISON CENTER or
doctor/physician.
t
EYE EXPOSURE:P305+P351+P338:IF IN EYES:Rinse cautiously with water for several minutes.Remove contact lenses if present and easy to
do—continue rinsing. Use sufficient force to open the eyelids. Have the exposed individual"roll"their eyes. Minimum Bushing time is for 15
minutes.P310:Immediately call a POISON CENTER or doctor/physiclan.
s
INHALATION:P304+P340:IF INHALED:Remove victim to fresh air and keep at rest in a position comfortable for breathing.May cause severe
lallergic reaction in some asthmatics and sulfite sensitive individuals.P310:Immediately call a POISON CENTER or doctor/physician.
t INGESTION:P301+P330+P331:IF SWALLOWED:Rinse mouth. Do NOT Induce vomiting.Never induce vomiting or give diluents(milk or water)
by mouth to someone who is unconscious,having convulsions,or unable to swallow.May cause severe allergic reaction in some asthmatics and sulfite
sensitive individuals.P310:immediately call a POISON CENTER or doctor/physician.If conscious,give plenty of water or milk.induce vomltting(if
conscious)by touching back of throat.
MEDICAL CONDITIONS AGGRAVATED BY EXPOSURE:Skin and respiratory disorders,as well as conditions involving the"Target
Organs"may be aggravated by prolonged exposures to this product.Exposed Individual must seek immediate medical attention B any adverse effect
s
occurs.
NOTES TO PHYSICIAN: Treat symptoms as demonstrated by signs and distress in the patient.
j SECTION 5 • FIRE FIGHTING MEASURES
SUITABLE(AND UNSUITABLE) Product is non-flammable.Use water spray,dry chemical,CO2,or foam.Use extinguishing
EXTINGUISHING MATERIALS: measures that are appropriate to local circumstances and the surrounding environment.
f
SPECIFIC HAZARDS ARISING FROM THE This product is non-flammable and nonexplosive under normal conditions of use. At high
CHEMICAL temperatures this product can decompose to give off toxic fumes.
SPECIAL PROTECTIVE EQUIPMENT AND Firefighters should wear Polly protective clothing(chemical impermeable,fully encapsulated suit)
I PRECAUTIONS FOR FIREFIGHTERS: and positive pressure self-contained breathing apparatus.Do not release run off from fire control
jmethods to sewer or waterways.
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WATER TREATMENT EXPERTISE SINCE 1904
} FORMULA 6600 www.garrattcallahan.com Page 2 of 5

i
SECTION 6-ACCIDENTAL RELEASE MEASURES
PERSONAL PRECAUTIONS,PROTECTIVE EQUIPMENT,ENVIRONMENTAL PRECAUTIONS AND EMERGENCY
PROCEDURES.
WARNING:Any container expansion or rounding Indicates pressure build-up. Use extreme caution.When opening,release pressure slowly
through opening.
SPILL AND LEAK RESPONSE:Uncontrolled releases should be responded to by appropriately trained personnel using pre-planned
S procedures.Proper protective equipment should be used,refer to Section 8-exposure controls.
Small Spill:Mop up,or absorb with an inert dry material and place in an appropriate waste disposal container.P391:Collect spillage.
Large Spill:Restrict access to the area.Provide adequate protective equipment and ventilation.Stop leak if without risk Remove chemicals which
can react with the spilled material.Add dry inert material to contain and absorb spilled material.Prevent entry into surface waters,sewers,
basements or confined areas,dike if needed.Ensure that exposure to product is not at a concentration exceeding regulatory limits. Decontaminate
j the area thoroughly.Decontaminate all response equipment with soapy water before returning to service.Place all spill residue in a suitable
container and seal.P391:Collect spillage.
i
SECTION 7-HANDLING AND STORAGE
PRECAUTIONS FOR SAFE HANDLING: Keep out of reach of children.All employees who handle this material should be trained to handle
it safely.Open containers slowly on a stable surface. As with all chemicals,avoid getting this product ON YOU or IN YOU.Avoid direct or
prolonged contact with skin or eyes.Do not ingest Wash thoroughly after handling this product Do not eat.drink,smoke,or apply cosmetics
while handling this product. Avoid breathing vapors,dusts or mists generated by this product Use in a well-vemilated location. Remove
contaminated clothing immediately.Use only as directed.Refer to Section 8 for exposure controls,
i
j CONDITIONS FOR SAFE STORAGE: Containers of this product must be properly labeled.Storage areas of this product should be Beady
1 identified,well-illuminated,clear of obstruction and accessible only to trained and authorized personnel.Store containers in a clean,cool,well
I ventilated,dry location,away from direct sunlight,away from incompatible materials at temperatures between 50°F(10°C)- 100°F(37"C). Keep
3 container tightly closed when not in use.P405:Store locked up.Do not ingest Do not breathe vapor mist Wash hands after handling.Refer to
3 Section 10 for incompatibilities P403+P233:Store in a well ventilated place.Keep container tightly closed.
t
SEG710N 8-EXPOSURE CONTROLS-PERSONAL PROTECTION
VENTILATION AND ENGINEERING CONTROLS: Use with adequate ventilation.Eyewash/safety shower station is recommended to be
available near where this product is used/stored,
EXPOSURE LIMITS/GUIDELINES: EXPOSURE LIMITS IN AIR
............................................................
3
j CHEMICAL NAME CA ACGIH TLV OSHA PE L OTHER
3 TWA STEL TWA
3
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SODIUM BISULFITE 7631-90-5 5 mp/m' NE NE NONE
t
NE=Not Established
INGESTION: P264:Wash all exposed skin/hair thoroughly after handling.P280:Wear protective gbves/protective
clothingleye protection/lace protection.
1 RESPIRATORY PROTECTION: P260:Do not breathe dust/Fume/gas/mistNapours/spray.P271:Use only outdoors or in a well-ventilated area.
Maintain airborne contaminant concentrations below guidelines listed above,ifapplicable. Air-purifying
respirators with dusmalstHume/spray fikers are recommended it operations may produce dusts,mists or
sprays from this product with concentrations at or above levels posted above.
't EYE PROTECTION: P280:Wear protective gloves/protective clothing/eye protectiondface protection.Wear chemical safety
goggles or safety glasses with side shields.A face shield may also be necessary for splash protection.
SKIN PROTECTION: P264:Wash all exposed skindhair thoroughly after handling.P280.Wear protective gloves/protective
j clothing/eye protection/face protection.Use chemically-resistant gloves and skin protection,when handling
this product Use body protection appropriate for task(e.g.,lab coat,overalls).
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WATER TREATMENT EXPERTISE SINCE 1904
FORMULA 6600 www.garrattcallahamcom Page 3 of 5

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SECTION 9- PHYSICAL AND CHEMICAL PROPERTIES
APPEARANCE and COLOR: Clear to pale-yellow solution VAPOR PRESSURE,mm Hg @ 20°C: Not established
ODOR: Slight sulfur VAPOR DENSITY(Air=1): Notestablished
ODOR THRESHOLD: Not established RELATIVE DENSITY@20°C(water-1): 1.32- 1.345
a pH: 3.0-5.0 SOLUBILITY IN WATER: Complete
MELTING/FREEZING POINT: Not established PARTITION COEFFICIENT(moctanollwater): Notestzblished
j BOILING POINT: > 104°C(2191) AL/TOIGNITION TEMPERATURE: Not applicable
FLASHPOINT: Non-0ammable DECOMPOSITION TEMPERATURE: Not established
} EVAPORATION RATE(n-SuAc=1): Not established VISCOSITY: Not established
FLAMMABILITY(SOLID/GAS): Not applicable VOLATILE ORGANIC COMPOUNDS(%):Not established
77 FLAMMABLE LIMITS(in air by volume,%):Not applicable
3 SECTION I0-STABILITY AND REACTIVITY
REACTIVITY: Product is not reactive under standard ambient temperature and pressure.
STABILITY: Stable under normal condition of use and storage.
POSSIBILITY OF
HAZARDOUS REACTIONS: See incompatible materials.
j CONDITIONS TO AVOID: Avoid heat sparks and open flames.
INCOMPATIBLE MATERIALS: (Oxidizers,acids and alkalis).Oxidizers:may cause strong exothermic reactions.Acids:releases sulfur dioxide
gas which is toxic,corrosive,and potentially deadly.
HAZARDOUS
DECOMPOSITION PRODUCTS: Generates toxic and irritating gases at high temperatures.
' SECTION 11 -TOXICOLOGICAL INFORMATION
TOXICOLOGICAL EFFECTS: Sulfite salts cause gastric irritation by liberation of sulfurous acid. The sodium salt is basic and may be
Irritating to corrosive tissues depending on the concentration.
LIKELY ROUTES OF EXPOSURE: Skin,and eye contact inhalation.
[ RELATED SYMPTOMS: Skin,eye,respiratory and gastrointestinal irritation.May be harmful if swallowed.
- DELAYEDIIMMEDIATEfCHRONIC
EFFECTS FROM SHORT AND
LONG TERM EXPOSURES: Skin,eye,respiratory and gastrointestinal irritation.May be harmful if swallowed.
NUMERICAL MEASURES OF
TOXICITY: Not established for this product.
CARCINOGENICITY:None of the components of this product are listed by the NTP,IARC,or regulated by OSHA as carcinogens.
SECTION 12-ECOLOGICAL INFORMATION
ALL WORK PRACTICES MUST BE AIMED AT ELIMINATING ENVIRONMENTAL CONTAMINATION.
1 ECOTOXICITY:
Published literature(US EPA ECOTOX)provide a range of values:
Daphnia magne 48hr LCSO:72A to 149 mg/I.
Fathead minnow 96hr LC50:26.2 to 75.9 mg/l.
Aquatic ecotox data:240 ppm/24,48&96 hr./mosquito fish/rindfresh water(100%basis).
j PERSISTENCE AND DEGRADABILITY:No data available for this product.
BIOLOGICAL ACCUMULATION POTENTIAL:No data available for this product.
MOBILITY IN SOIL:No dam available for this product
OTHER ADVERSE EFFECTS(i.e.,hazardous to the ozone layer):No data available for this product.
BIOLOGICAL EXPOSURE INDICES: Currency,Biological Exposure Indices(BEls)have not been determined for this produ¢
SECTION 13•DISPOSAL CONSIDERATIONS
( DISPOSAL: P501:Dispose of contenWconbiner in accordance with local/regional/national/International regulations.Rinse empty containers with
water and use the rinse water to prepare the working solution. Refer to Section 8 for exposure controls-personal protection.
1
i
WATER TREATMENT EXPERTISE SINCE 1904
FORMULA 6600 www.garrauczllahan.com Page 4 of 5

SECTION 14-TRANSPORTATION INFORMATION
j PROPER SHIPPING NAME
'- DOT: UN2693,BISULFITES,AQUEOUS SOLUTIONS,N.O.S.
(SODIUM BISULFITE),8,PGIII
Emergency Response Guidebook,Guide No.: 154 y
! Passenger Aircraft Cry:SL
' Cargo Aircraft Qty.60L
IMDG/IMO: UN2693,BISULPHITES,AQUEOUS SOLUTIONS,N.O.S.
(SODIUM BISULFITE),8,PGIII
IATA/ICAO: UN2693,BISULPHITES,AQUEOUS SOLUTIONS,N.O.S.
(SODIUM BISULFITE),8,PGIII
1
ENVIRONMENTAL HAZARDS
i (i.e.,MARINE POLLUTANT): None known.
' TRANSPORT IN BULK(according to
J annex 11 ma of 73/78 and the IBC code)
:)• Not applicable.
i SPECIAL PRECAUTIONS FOR USER: None known.
4
PRODUCT REQUIRES CORROSIVE LABEL
t
3 SECTION IS- REGULATORY INFORMATION
1
i United States and International Regulations
United States Regulatians: U.S.SARA REPORTING REQUIREMENTS: The components of this product are subject to the
reporting as listed below,requirements of Sections 302,304,and 313 of Title of the Superfund Amendments and
Reauthorization Act:
{ CHEMICAL NAME
I SODIUM BISULFITE SARA 302(40 CFR 355,Appendix A)-NO
t SARA 304(40 CFR Table 302A)-YES
- SARA 313(40 CFR 372.65)-NO
7 U.S.Regulations
U.S.SARA THRESHOLD PLANNING QUANTITY:There are no specific Threshold Planning Quantities for the components of this product
The default Federal SDS submission and Inventory requirement filing threshold of 10,000 Ibs(4,540 kg)therefore applies,per 40 CFR 370.20.
U.S.CERCLA REPORTABLE QUANTITY(RQ): SODIUM BISULFITE(CAS#7633-90-5):5.000 Ibs(2270 kg).
U.S.TSCA INVENTORY STATUS: The components of this product are listed on the TSCA Inventory,
SARA TITLE 31 I/312 HAZARD CATEGORY:ACUTE:YES CHRONIC: NO FIRE: NO REACTIVITY:NO SUDDEN RELEASE OF
PRESSURE:NO
California safe drinking water and toxic enforcement act(proposition 65)s No component of this product is on the Proposition 65
List
PA REQUIREMENT-3%or greater
NJ REQUIREMENT- 1%or greater
International Regulations '..
CANADIAN REGULATIONS: '..
CANADIAN DSL INVENTORY STATUS: The components of this product are on the DSL Inventory or are exempt from listing. '..
CANADIAN WHMIS CLASSIFICATION:None.
SECTION 16-OTHER INFORMATION
PREPARED BY: GARRATT CALLAHAN
j DATE OF REVISION: 11/30/2015 Supercedes: 10/27/2015
s Formula 66001s registered with the NSF to the Nationally Recognized Health Effects Standard(ANSI 60)for chemicals which are used to treat
drinking water;with NSF DCC#DA06620.
Although reasonable care has been taken in the prepara lon of this document we¢rand no warrmmes and make no representadom as to the accuracy or
j completeness of the information contained herein,and assume no responsibility regarding the suitability of this information for the users intended purpme or for the
conaequmcea of its use. Each indindualshonld make a determination as e,de suitability of the informadon for their particular purpose.
I
WATER TREATMENT EXPERTISE SINCE 1904
FORMULA 6600 www.garrattcallahan.corn Page 5 of 5

ATTACHMENT G
North Carolina Surface Water Standards
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1
DISCHARGED WATER STUDY
REPORT 2
FOR
f Low&
Bonar
Low & Bonar Inc.
1302 Sandhill Road
Enka, North Carolina 27105
� Prepared For:
Landon Davidson, Regional Supervisor, Division of Water Resources
Linda Wiggs, Environmental Senior Specialist, Division of Water Resources
North Carolina Department of Environmental Quality
Water Quality Regional Operations Section
2090 US Highway 70
Swannanoa, NC 28778
3
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Date:
August 31, 2017
I
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Table of Contents
3
EXECUTIVE SUMMARY-DISCHARGED WATER STUDY.............................................I
CHRONOLOGY............................................................................................................................3
i WASTEWATER SAMPLING RESULTS..................................................................................4
DISCHARGE WATER FLOW RATES.....................................................................................5
x
CONTACT VS. NON-CONTACT COOLING WATER...........................................................7
FACILITY IMPROVEMENTS...................................................................................................8
BOILER CONDENSATE.............................................................................................................8
CHILLER COOLING TOWER 058 SYSTEM...............................................................I.......I
COOPER COOLING TOWER SYSTEM................................................................................11
[ SLIM TANK—NEW COMPLIANCE POINT.........................................................................11
1
ROOF STORMWATER DRAIN PIPING................................................................................11
1 FLOW METERS.........................................................................................................................11
SCHEDULE TO COMPLETION..............................................................................................12
1
SCOPE OF FUTURE TESTING...............................................................................................12
fCONCLUSION............................................................................................................................13
I
Figures
1. Low&Bonar Inc. Site Diagram
2. Low&Bonar Inc. Discharge Water Sampling Point Diagram
i
3. Lowy&Bonar Inc.Boiler Condensate Receiver Diagram
I Tables
i
I. Calculation of Discharge Water and Groundwater Infiltration
2. Boiler Condensate Receiver Status
j
3. Boiler Steam Receiver and Drip Line Piping Upgrades
4. Boiler Steam Receiver and Drip Line Piping to MSD or Stormwater System
i
5. Discharge Water Sampling Analytical Results—August 2, 2017
i I
6. Daily Average Pollutant Discharges by Process Point
Low @ Bonar Inc.—NPDES Discharged Water Report 2 i
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DISCHARGED WATER STUDY
REPORT 2
I
FOR
Low&
B©nar
Low & Bonar Inc.
1302 Sandhill Road
Enka, North Carolina 27105
I Prepared For:
i
Landon Davidson, Regional Supervisor, Division of Water Resources
Linda Wiggs, Environmental Senior Specialist, Division of Water Resources
s
I North Carolina Department of Environmental Quality
i
1 Water Quality Regional Operations Section
i 2090 US Highway 70
Swannanoa, NC 28778
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Date:
August 31, 2017
i
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Appendices
A. Pace Analytical Laboratory Analysis Report
7 B. Exhibits
! C. Discharge Water and Groundwater Infiltration Flow Measurements and Calculations
D. Purchase Orders
E. Calculations
F. Sampling Records
G. North Carolina Surface Water Standards
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Low&Bonar Inc.—NPDES Discharge Water it
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EXECUTIVE SUMMARY-DISCHARGED WATER STUDY
Based upon recent phone discussions between the North Carolina Department of Environmental Quality's
Water Resources Section and Low&Bonar Inc. contractors,we have compiled additional information
regarding our water discharges to surface waters of the State for your review. This information comprises
1 a comprehensive water discharge evaluation developed from several internal staff meetings representing
Engineering,Facilities,Maintenance,and Environmental divisions with our environmental consultant
Pisgah Environmental Services.
Additionally,two previous Low&Bonar Inc. staff from Facilities and Drafting were engaged to assist the
effort. In particular,Mr. Howard Early—the Facilities Engineering Manager from 1968 to 2013—was
i engaged to provide facility-wide institutional knowledge of the site and to direct current Low&Bonar
Inc. staff and other contractors. Overall,Mr. Earley has over 45 years of experience at this facility;thus,
he is a very appropriate and valuable resource for this evaluation.
This repot substantially describes current water discharges from Low&Bonar Inc. This is a complex
facility that has had several ownership changes and two spit-off facilities that remain on-site over the past
88 years. Thus,this report does not purport to be the final water discharge evaluation. But, it does
j provide a basis for discussions that will lead to a final understanding of Low&Bonar Inc.'s discharged
water situation.
This report provides discharge water pollutant concentrations from nine(9)sources or intermediate points
and City Water collected during an August 2, 2017,sampling campaign.
Based upon a volume balance of discharged water from various sources and using several pollutants as
' surrogates of pollutant concentrations,we performed a modified Monte Carlo calculation of groundwater
infiltration rates into various water collection systems and a total discharge rate to surface waters. This
allows as to calculate preliminary mass pollutant discharge rates. Again,this information is not the final
i evaluation,but it allows us to draw some conclusions about the situation and serve as the basis for
discussions about a path to compliance for Low&Bonar Inc.
This report—and all previous reports—show that water discharges from the Low&Bonar Inc. facility
substantially comply with North Carolina 15A NCAC 02B Surface Water Standards and Protective
Values. Exceptions to this statement are addressed below.
a
I. Two metals—copper and zinc—are discharged from multiple sources at values exceeding
regulatory limits.
a
4
` Copper and zinc concentrations in the new discharge compliance point(i.e.,Slim Tank)are at
') concentrations of 0.0076 and 0.220 milligrams per liter(mg/L)respectively;the acute regulatory
I
7 limits are 0.0036 and 0.036 itlgiL respectively. Of note are the City Water copper and zinc
concentrations of North Fork reservoir water of 0.0076 and 0.210 milligrams per liter(mg/L)
respectively.
7
Both copper and zinc are considered to have water system supply and infrastructure sources
_7 rather than process sources.
I
Another metal—molybdenum—is also discharged from the facility. Molybdenum's only source
is a water treatment chemical used in the Cooling Towers fo'the Chiller Room. Our water '..
] treatment supplier of this chemical uses molybdenum as a tracer(i.e.,as concentration values for
7
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Low& Bonar Inc.—NPDES Discharge Water t
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3
molybdenum decrease the supplier adds more of the entire formulation). The water treatment
chemical supplier has been directed to remove molybdenum from this formulation.
2. Total Residual Chlorine is discharged from multiple sources; some are once-through cooling
waters that discharge essentially City Water(e.g.,extruders)and some are cooling tower
i
blowdowns.
Total Residual Chlorine concentrations in the new discharge compliance point(i.e.,Slim Tank)
are at a concentration of 0.8 milligrams per liter(mglL);the regulatory limit is 0.017 mg/L. The
City Water Total Residual Chlorine concentration is 1.4 milligrams per liter(mg/L).Recently,at
the East Ditch compliance point for sampling and analysis campaigns on July 6 and August 2,
Total Residual Chlorine has been at concentrations of<0.2 and<0.2 mg/L respectively(see
Figure 2 for sampling locations).
i
= The differences between the Slim Tank and New Stonmwater Sampling Point Total Residual
Chlorine concentrations are due to dilution. The measured discharged water flow at the Slim
I Tank is 38,253 gallons per day and the calculated New Stormwater Sampling Point ranges
11 from]33,250 to 211,958 gallons per day.
Our conclusion is that Low&Bonar Inc. is in compliance with the Total Residual Chlorine
standard in the New Stonmwater Sampling Point but not at the Slim Tank;which is an internal
sampling point that is being proposed as the new"compliance point". For comparison,the Total
Residual Chlorine concentration in the East Ditch—the previous"compliance point'—is<0.2
mg/L.
While we do want to use the Slim Tank because it represents undiluted waters used forcooling
and other legitimate purposes within the processing areas,we also do not want to be penalized—
s by having an individual permit condition that requires substantial monitoring,recordkeeping,and
reporting of Total Residual Chlorine results that without treatment option will result in
continuous Notices of Violation.
The options,therefore, are three:
a
o Reduce or remove the use of chlorinated City Water for once-through cooling,
o Treat the chlorinated water to remove chlorine, or
' o Continue to use the East Ditch as the`compliance point".
1
3. Discharge water flow rates in this report are based upon instantaneous measurements;which vary
greatly on a daily basis. Until totalizing flow meters are installed in the system these
measurements and calculations will be considered preliminary. This uncertainty of flow volumes
must be resolved before the final permit application is complete; as those values are necessary for
Wasteload Allocation calculations.
4. Boiler steam condensate water is discharged in several locations. To Low&Bonar this is an
expense. That water has been purchased,treated with specialty boiler chemicals,and heated. To
minimize costs—and to minimize effluents—our first discharged water action has been to return
boiler condensates to the boiler.
Low&Bonar Inc.—NPDES Discharge Water 2
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' CHRONOLOGY
I
On May 22,2017,Low&Bonar Inc. conducted a Low&Bonar-facility-wide requested inspection with
3 North Carolina Department of Environmental Quality staff concerning compliance with stormwater
t regulations.
During that inspection,several other discharged water issues arose. As a follow-up to that inspection Ms.
Linda Wiggs of tie Division of Water Resources seat to Low&Bonar Inc. in a June 12 email an
j Information Request for water discharge sources,rates,and pollutant concentrations. A response to DWR
from Low&Bonar was dated June 15.
.3 On June 19,the Water Resources Section issued a Notice of Violation and Intent to Assess Civil Penalty
3 (NOV-2017-DV-0148, Incident No.: 201701034)to Low&Bonar Inc.
i
1 Low&Bonar inc. attended a meeting with Water Resources Section staff on June 23. During that
meeting Water Resources Section staff clarified the scope of Ms.Wiggs' requested information and Mr.
} Landon Davidson identified other tasks in an Information Request dated June 23. Those data, including
I estimates of the volume of wastewater discharged daily, list of biocides and any other additives in
1 wastewater,biocide worksheets,wastewater analytical data,facility-wide wastewater audit,cost to pump
and haul current wastewater discharge,metropolitan sewerage district policy on non-contact wastewater,
and current wastewater discharge quality or quantity changes to NCG500608 were conveyed to Mr.
Davidson in a letter from Low&Boiler dated June 26.
i
Ms. Wiggs conducted a Water Resources Section facility-wide inspection of the Low&Bonar Inc. site on
July 6. During that inspection samples were collected from three sources: Slim Tank,Jarden Steam
Heating Condensate,and the East Ditch. On July 13,Low&Bonar Inc.collected samples front three(3)
additional sources: Manhole 3,Manhole 25,and the Cooper Compressor as well as from one(I
stonnwater source: Poly Cooling Building. The results of those two evaluations were conveyed to the
Water Resources Section in a letter report dated July 25.
i
This report describes the results of a sampling and analysis campaign conducted August 2. Samples were
collected from ten(10)sources:Chiller Room Cooling Tower Blowdown,Manhole 3,Manhole 3
Upstream(off-site contribution),Cooper Cooling Tower Blowdown, Slim Tank,Production Line Ml/M4
t Condensate,Production Line M5 Condensate,Manhole 25,Basement Groundwater Pump,and the New
Stormwater Sampling Point, For comparison,City Water was also sampled,
Also,to evaluate Boiler Steam Condensates that are to be recycled to the Boiler system or discharged to
the Metropolitan Sewerage District as blowdowns,we tested a representative Condensate Receiver.
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Low&Bonar Inc.-NPDES Discharge Water 3
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WASTEWATER SAMPLING RESULTS
Table I lists the analytical results from samples collected on August 2,2017. The preceding 96 hours to
1 sampling were dry(i.e.,no measurable rainfall). Copies of the site weather station records for July and
3. August are included in Attachment F. Table I sources and discharges are in the order of flow to Surface
s Waters. Figure 1 shows the sampling locations. Figure 2 shows how each sampling location is linked in
j the discharge water flow to Surface Waters.
Table I pollutants in most cases are less that the North Carolina 15A NCAC 02B Surface Water
Standards and Protective Values. Of particular note are the copper and zinc concentrations. Based upon
a review of water treatment chemical Safety Data Sheets and raw materials used at L&B we conclude that
?_ the source of copper and zinc are from infrastructure. Our professional judgement is that supplied City
Water in concert with building and water conveyance materials contribute most of these metals to
t discharge waters.
l Our judgement is based in part upon the copper and zinc concentrations of less than(<)0.005 and 0.210
milligrams per liter(mg/L)respectively in City Water within the building. Copper is monitored by the
jCity of Asheville and their annual report of April 2017 lists a maximum system-wide concentration of
0.005 mg/L. Although zinc is not addressed in the report, conversations with Mary Grimes of the
_ Asheville Water Department revealed that distribution system zinc concentrations ranged from 0.20 to
0.17 mg/L on July 28 and August 2 respectively at the North Fork Water Treatment Plant. Thus, it is
conceivable that the zinc concentration in the inlet water is 0.210 milligrams per liter and that
concentration is not related to infrastructure. If so,we should correct all discharge water zinc
concentrations by the`background' concentration of approximately 0.20 mg/L. That correct is not
included in this report.
t
- Molybdenum is in discharge waters due to its use as a `tracer chemical' in our water treatment chemicals
supplied by Garrett-Callahan. This metal has biocide properties that were evaluated in the Toxicity
evaluations later in this permitting process and in the wasteload allocation process to be conducted by the
State. We have contacted Garrett-Callahan to modify their water treatment formulation to not include
molybdenum. Future discharge water analyses should reflect this change.
i Chloroform is in City Water at a concentration of 0.0195 mg/L and in the Cooper Cooler System at
0.0023 mg/L. However,chloroform is not detected in any other discharge source.
1
Table 1 does not include the Pumphouse Standing Water addressed in our July 13 campaign. L&B
facilities staff revealed that chlorine in the water was there due to their mosquito control efforts. Some
production staff had complained about mosquitos during the Zika scare of the summer of 2016. Facilities
staff chlorinated the Pumphouse Standing Water with two(2)swimming pool HTC tablets. Apparently,
( some residual chlorine is still in the water. Moreover,the Pumphouse standing water observed in July has
evaporated and the floor is dry(see Exhibit 8).
3 Other pollutants tested are less than State 02B Surface Water Standards or are at concentrations less than
the analytical detection limits.
Figure I is a site diagram that shows the eleven(I I)August 2 sampling locations. Tables 4 and 5 address
t only those pollutants that were detected in any of the I 1 discharge samples. All other pollutants were
t reported by the laboratory at"less than the analytical method detection limit". Pace Laboratories'report
is included in Attachment A.
7 "Fable 2 lists pollutant discharge rates from the new compliance point(i.e.,the Slim Tank in the
j DowTherm Room),the new stormwater sampling point(i.e, flood gate at head of East Ditch), and the
�-- previous compliance point(i.e,the East Ditch)(see Figure 2). These discharge rates demonstrate that—
Low&Bonar Inc.—NPDES Discharge Water 4
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considering instantaneous flow variations—the Slim Tank discharge rates are in the same concentration
range as the other two points.
1
DISCHARGE WATER FLOW RATES
L&B has continued to refine our process discharge water production evaluations. Table I is our current
calculated range of discharge water contributions—including groundwater—to L&B's discharge to
Hominy Creek. Table 5 incorporates some measured actual water contributions to L&B's discharges.
(€ Ranges are necessary in these calculations because the measured water flows are instantaneous values.
.{ These are dynamic flows that vary throughout the day depending on work load,temperature,humidity,
and a host of other production factors. For example,during our recent sampling campaign discharge
$ water flows from only the extruders into the Slim Tank varied by a factor of three(3)over a 20-minute
j period. Other inputs to the Slim Tank varied as well. Thus, until totalizing flow meters are installed in
the discharge water system any calculations of flow must be expressed as ranges.
Calculations of Groundwater Infiltration also vary due to rainfall amounts at the site and upstream in the
Hominy Creek drainage. These factors are beyond our control. However,with better discharge water
data we will be able to evaluate Groundwater Infiltration more accurately.
Three conditions are of note in our calculations:
o The process wastewater values of maximum discharge were taken from measured discharge
a rates during periods of high production, high summer temperatures,and high humidity during
mid-Augurs[.
3 o Groundwater is at a low point;no rainfall events at the facility for the 96 hours preceding
- sampling and flow measurements(see Attachment FL
o Several wastewater streams must be re-routed from their current discharge pathways to
Hominy Creek via the Fast Ditch so that they pass through the `Slim Tank'. This will allow
all process cooling waters to be sampled from a single point.
Based on zinc,phosphorus,hardness,and Total Dissolved Solids data from the August 2 sampling
campaign we used a `volume balance' to calculate.groundwater infiltration amounts. The results are
surprising. We calculate that on average, 148,052 gallons of water per day are discharged from the
j storrawater collection system to Hominy Creek via the Fast Ditch. Appendix C contains a calculation
' summary and calculation example.
i
Below is an example calculation of values in Table 1:
9t
} Manhole3 = Cooling Tower 058+Groundwater: ZINC
"s
(0.416 mg(L x X gal/d)=(1,67 mg/L x 8,818 gal/d) + (0 mg/L x Y gal/d)
1 X = (14726 + 0)/0.416
X = 35,399 gal/day
i
Manhole 3 water flow was calculated using the Volume Balance method for the other three pollutant
concentrations. The average of the four calculations(i.e.,a modified Monte Carlo simulation)averaged
34,442 gallons per day.
- Low&Bonar Inc.—NPDBS Discharge Water 5
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- Table 1. Calculation of Discharge Water and Groundwater Infiltration
Low Measured High Average
Source : al/D aUD aUD ( aVD
! CoolingTower 058 8,818
Groundwater' 25,624
.i SUBTOTAL—Manhole 32 35,399 34,442 62,131 43,991
Manhole 3 Upstream' 4,000
'= Slim Tank - 38,018
Coo er S•stem 15,517
- MI-M4 Room! uench 490
M5 Roond uench III
SUBTOTAL—Manhole 25 88,573 92,578 165,338 115,496
Groundwater 6,366
SUBTOTAL—New Stormwater 133,253 98,944 1211,958 1 148,052
'Groundwater"Measured Flow'is calculated by subtracting the Cooling Tower 058 flow-a true measured flow rate-from the
- totalflov in Manhole 3;which is avolume balance calculation.
2 Manhole 3"Measured Flow"is an average of flows calculated using the average of Zn,P.thadness,and TDS calculations;it is
a volume balance.
77 a Manhole 3 Upstream"Measured Flow"is an estimated Flow.
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( CONTACT VS. NON-CONTACT COOLING WATER
i L&B has determined that discharged waters to Hominy Creek are primarily"non-contact cooling water"
and"once-through cooling water"or they are air condensates from creature comfort,room cooling for
heatimoisture sensitive electronics equipment,or oil-less air compressor systems. Some are boiler or
? cooling tower blowdowns.Each type of discharged water is discussed below.
At L&B extruders are an example of once-through cooling water. City Water is piped tin ough an
extruder head or gear box to cool the mechanism or to prevent the product from becoming too hot. This
a is a type of non-contact cooling water. Water used in cooling the extruder throat and gear boxes is 'once-
through cooling water'. Its residual chlorine is equal to that of City Water and other chemical
characteristics are the same. Thus,extruder cooling waters impart chlorine to discharged waters. L&B is
considering two avenues to address residual chlorine:
7
o Deehlorination. Either sodium thiosulfate or sodium metabistdfite can be added to extruder
z water either in the Slim Tank itself or in another dedicated treatment tank.
3
I o Closed Loop Cooling System. Extruder water can be re-circulated through a chiller rather
than being discharged. This option has several rewards:
'_- - Reduced cost of cooling water. The use rate of 15,000 per day equates to$28,000 of
defrayed purchase costs per year.
- No treatment chemical costs are incurred.
- Instead of using a chiller system to cool extruder cooling water, L&B is exploring using ground water
- stored in three large flooded ventilation tubes under the Fleecing Department Floor to cool the water. This
- option would only require the purchase of a pump and installation of some piping;and several tin-used
- ' heat exchangers around the plant could be put into service for this application.
We believe this option would not require a groundwater pumping or treatment permit. The cooling action
3
is non-contact,and groundwater remains in the basement.
In this evaluation,yarn quench and room cooling air condensates were classified as"process water". For
i example,quenching the recently formed yarn strands with cool air releases nylon or PET monomers to
room air. This air is then mixed with room cooling air. Although these monomers are not in
concentrations to be detected as total suspended solids they are still"process water". Consequently,these
3 waters were replumbed to MSD.
Condensates from compressed air systems are classified as non-process water. Although compressed air
I is used,for example,to move thread through tubing or to spread thread on the Fleecing table,the
j condensed water in the pressurized lines is never in contact with product(s)or raw materials. Moreover,
- this air is produced by"oil-less"compressors;thus,no oil can be in the water- Therefore,condensate
S from these lines is considered"non-contact"and is permitted to be discharged to surface waters.
i Compressed air system water is directed to the Slim Tank and hence to Hominy Creek
L&B has identified several true"contact"process water discharges and has re-routed them to the
Metropolitan Sewerage District(MSD)of Buncombe County sewerage system instead of Hominy Creek.
3 This identification and plumbing process is on-going.
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Low&Bomar Inc.—NPDES Discharge Water 7 '..

FACILITY IMPROVEMENTS
Facilities,Engineering,and Maintenance staff identified several water issues that must be changed to
bring the facility into total compliance with NC Surface Water regulations. These issues and tasks were
ranked by: 1)Impact on surface water quality,2)Schedule to completion,3)Availability of motors and
pumps,and 4) Availability of L&B staff or contract staffing. First among issues is to return all treated
and heated boiler condensates to the boiler system. Losing boiler condensate to the East Ditch or to MSD
is a waste of water h eatment chemicals,heat energy, and purchased water. L&B estimates that every 100
gallons of water lost daily from the system costs about$456 per year,
sLow&Bonar Inc. is committed to installing or performing the actions described in the following
sections. Purchase orders have been approved for equipment totaling approximately$9,400 for motors,
pumps, floats,and switches to repair or replace Boiler Condensate Receiver parts and another$12,900 for
pumps and motors to replace the Chiller Cooling Tower and the Cooper Cooling Tower parts. Flow
i meters are estimated to be$9,000 for six(6)units.
Purchase Orders are included in Attachment D. None of the above costs include labor;these are only
j equipment costs.
'fhe following sections describe actions L&B has embarked upon to minimize impacts to surface waters.
!!! Table 3 provides a schedule for completion.
S
j BOILER CONDENSATE
t
# Over the years the L&B Boiler Condensate System has developed many connections and discharges to
jthe stonmvater system that flows to Hominy Creek via the East Ditch or to the Metropolitan Sewerage
District(MSD)system, Neither discharge reflects the condensate system's initial design. The Boiler
j — Condensate System was designed to capture and recycle all boiler steam condensate. To this end 10
i condensate receivers were installed around the facility.
The system was originally designed to work in the following manner: Boiler steam condenses in transfer
piping and flows via gravity to a receiver. These receivers store the condensate until the container is full
and then pump the liquid to a height that allows it to flow by gravity to the boiler condensate storage in
3 the boiler room. The condensate is heated again in the boiler and the process repeats.
In order to repair/replumb and once again capture and recycle all boiler steam condensates,the following
tasks have been identified:
j
o Repair or replace motors, floats,and switches as necessary(see Table 2).
3 o Remove all boiler steam receiver and drip line piping connections to MSD or to the
'. stormwater system(see Table 3)and Exhibits 4 and 5.
i
o Install bypass piping upstream of receivers for maintenance activities(see Exhibit 3).
o Fabricate a wheeled metal tank to collect boiler condensates during maintenance activities.
' Tank contents will be returned to the boiler condensate system or to MSD via a dedicated
drain.
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Low&Bonar Inc.—NPDES Discharge Water 8

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CHILLER COOLING TOWER 058 SYSTEM
i
- Repair the Chiller Room Cooling Tower 0-58 water pump. Re-attach the effluent line to the piping system
to the Slim Tank central discharge point in the DowTherm room. This repair re-routes the Chiller Cooling
Tower blowdown to the stormwater collection system via the Slim Tank rather than directly to the
stormwater collection system. This change is necessary to have all stormwater collection system discharges
from a single point.
A purchase order for a replace pump/motor is included in Attachment D.
3
COOPER COOLING TOWER SYSTEM
Repair or replace the Cooper Cooling Tower water pump. Re-attach the effluent line to the piping system to
3 the Slim Tank central discharge point in the DowThenn room This iepah're-routes the Cooper Cooling
Tower blowdown to the stormwater collection system via the Slim Tank rather than directly to the
stormwater collection system. This change is necessary to have all stormwater collection system discharges
from a single point.
S A purchase order for a replace primp/motor is included in Attachment D.
SLIM TANK—NEW COMPLIANCE POINT
3 Replumb the central discharge point-the Slim Tank- in the DowTherm room so that all inputs are on the
upstream side of the weir. [Two lines must be moved;one PVC line and one galvanized line must be moved
j about 3 feet upstream.] In the future,all permit compliance monitoring for water discharged to Hominy
Creek via the East Ditch will be conducted at the Slim Tank discharge point.
a
ROOF STORMWATER DRAIN PIPING
t
Low&Bonar Inc.intends to replumb the stormwater drain system in the main processing areas—all six(6)
levels of the tower,winding, fleecing,Enkamat,and Colback—so that drains contain only rain water and
3 condensates from creature comfort cooling—NO PROCESS WATER. Abandoned lines have been spray
painted orange and tags attached to direct our contractor to"cut and cap"all the marked lines(see Exhibits 4
and 5).
FLOW METERS
Low&Bonar Inc. intends to install discharged water flow,monitors in the follow locations:
t
o Install water volume metering devices at:
t
3 o Central water discharge point in the DowThern room.
o Upstream of the DowThenm room
i o Stormwater pipes in the flood gate near the head of the East Ditch-two discharge points.
t o Stormwater pipe in the line through the old Basofil plant near Manhole 8.
'j o One other location to be determined.
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Low&Bona Inc.—NPDES Discharged Water Repon 2
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I
SCHEDULE TO COMPLETION
i
_ Facility hnprovements: Schedule to Completion
- Approximately 12 weeks from August 10:November 3,2017
I
Actions:
o Boiler Condensate—Reroute condensate receivers to Boiler
o Chiller Cooling Towers—Replace pump, reroute to Slim Tank
o Cooper Cooling Towers—Replace pump,reroute to Slim Tank
o Slim Tank—Re-position drain lines to behind weir
o Roof Stormwater Drain Lines—Re-plumb all process waters to MSD. Creature comfort
condensate lines to remain
j o Flow Meters—Discharge point and main trunk lines
i
SCOPE OF FUTURE TESTING
i
Low&Boost Inc. has evaluated its water discharge sources,their pollutants,and volume balances in order to
calculate mass effluent rates in terms of pounds or pollutant per day. We would like to schedule a discussion
on the scope of future sampling and analysis campaigns. This discussion would address:
o Number of sampling points
o Number of sampling campaigns
o Pollutant analysis list
i o Mass effluent rates
i
S Ultimately,this discussion would lead to a decision of whether an Individual or a General Permit is more
appropriate for Low&Bonar.
Biocides are added to cooling tower waters in various locations. Our letter report of June 26 described our
initial calculations of biocide impacts on Hominy Creek. This work will be finalized once the water flows
from each process are correctly categorized and flow rates finalized.
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Low&Bonar Inc.—NPDES Discharge Water 12
j

CONCLUSION
Low&Bonar intends to comply with all State and Federal discharge limitations. This second report
demonstrates that pollutant concentrations in the current compliance point effluent and the future compliance
7 point effluent are both below any Division of Water Resources regulatory limit. North Carolina Surface
j Water Quality Standards are included in Attachment E.
Table 5 compares mass discharge rates of pollutants from the new compliance point—the Slim Tank—to the
previous compliance point—the East Ditch. The Slim Tank exhibits consistently lower pollutant discharge
rates. This circumstance is likely due to the calculated volume of discharged water and contributions from
off-site sources, The same can be said of the comparison of the Slim Tank discharges to the new Stormwater
s
Compliance point in the Flood Gate structure.
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ATTACHMENT4
jPace Analytical Laboratory Analysis Report
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} _v_Inc.—NPDES Discharge Water
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i Pace Analytical Services,LLC
'{ /� 2225 Riverside Or.
aceAnalyt(cal NC 28604
ntvrv.M�eda.<cm
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August 22, 2017
i
Mr. Dan March
Pisgah Environmental Services
9 Woodvale
Asheville, NC 28804
4
f
RE: Project: Low& Bonar Inc 1210140
Pace Project No.: 92350243
Dear Mr. March:
Enclosed are the analytical results for sample(s) received by the laboratory on August 03, 2017. The
} results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
t
' Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
3
a
Enclosures
t
t
3
} vwwrll
REPORT OF LABORATORY ANALYSIS
Thr,e"o shall not he reproduced ept
exc -NII,
wllhowthewtlnenconsem or PacoAealybcal ser roes.LLC, Page 1 of W
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Pace Analytical Services.LtG
aceAnalVical Rivers tle er.
xxxA+ a0.cmm Asheville,NC 28804
3 (82g2M 7176
3
CERTIFICATIONS
Project: Low&Donar Inc 1210140
Pace Pocket No: 92350243
I
Charlotte Certification IDs
s 9800 Kawy Ave.Ste 100,Huntersonge,NC 28078 South Carolina Certification#:99006001
S North Carolina Drinking Water Certification#:37706 FloudafNELAP Certification#:E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification at 12 MuglmenVELAP Certification# 460221
Asheville Certification IDs - -
2225 amends Drive,Asheville,NC 28804 North Carolina Wastewater Certifcafon#:40
FkaidoUNELAP Certification#:E87648 South Carolina Certification#:99030001
' Massachusetts Codification if:M NC030 vaginiaNELAP Certification#'460222
{ North 1-nofna Drinking Water Certification if.3➢712
3
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£3
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REPORT OF LABORATORY ANALYSIS 1.
TMs report shall not 6e repm4uceC,except in fun,
jwithow Ne written consent of Pace Malylical S-1—Ir LIC. Page 2 of 96

Pace Analytical Services.LLC
aceAnalytical e 2225 Riverside 2
wxa�k6nttcn ASM1eville,NC 28604
- [phone]
SAMPLE ANALYTE COUNT
Project: Lew&Bonar Inc 1210140
i Pace Project No.: 92350243
Acolytes
Lab 10 Sample ID Method Analysts Reported Laboratory
92350243001 Chiller Room(0-68) EPA 1664E JMS 1 PASI-C
EPA200.7 SHt 14 PASI-A
EPA245A KAL 1 Ral
EPA625 RES 62 PASI-C
EPA624 SAW 36 PASI-C
SM 2540C SLB 1 PASI-A
SM 2540D MVC 1 PASI-A
TKN+NO3+NO2 Calculation EWS 1 PASI-A
EPA 350.11993 Rev20 BRJ 1 PASI-A
- EPA 351.2 AES2 i PASI A
EPA353.2 CJH1 1 PASI-A
EPA 366.1 CJHt 1 PASI-A
t' SM 5220D NAL 1 PASI-A
82360243002 Slim Tank EPA 16648 JMS 1 PASI-C
EPA 200.9 SH1 14 PASI-A
EPA245A KAL i PAS!A
EPA625 RES 62 PASI-0
i
_ EPA624 GAW 36 PASI-C
SM 2540C SLB 1 PASI-A
SM 2540D MVC 1 PASI-A
TKN+NO3+NO2 Calculation EWS i PASI-A
EPA 350.11993 Rev 2.0 8RJ 1 PASI A
EPA351,2 AES2 1 PASI-A
j EPA353.2 CJHi 1 PASI-A
j EPA 365.1 CJHi 1 PASI-A
SM 5220D NAL i PASI-A
' 92350243003 Cooper Cooling System EPA 16648 JMS 1 PASI-C
1
7 EPA2007 SHt 14 PAS-A
EPA245A KAL 1 PASI-A
EPA625 RES 62 PASI C
EPA624 GFlW 36 Poll
SM 2540C SLB 1 PASI A
I SM 2540D MVG i PAS)A
TKN+NO3+NO2 Calculation EWS i PASI-A
t EPA 350.41993 Rev 2.0 8RJ 1 PASI-A
EPA351.2 AES2 1 PASI-A
f
EPA353.2 CJH1 1 PASI-A
{[ REPORT OF LABORATORY ANALYSIS
t This report shall not be reproaurea,eaci lm full,
1 without the written consent of Pace Malyroctl 5ers ces,LLC Page 3 of W
i

i
Pace Analytical Serv"mes,LLC
aceAnalytical a 2225 Rivera0r.
_ an
w�fol Ashev828)2 C 28806
( 28)2549t]a
I `a
SAMPLE ANALYTE COUNT
i
j Project: Low&Bonar Inc 1210140
jPace Project No.: 92350243
Analytes
Lab1D Sample ID Method Analysts Reporned Laboratory
EPA 3651 CJHi 1 PASI-A
SM 5220D NAL i PASI-A
92360243004 MI&M4 Room Quench EPA 16UB JMS i PASI C
EPA200.7 SH1 14 PASI-A
�.3 EPA2451 ML 1 PASI-A
EPA625 RES 62 PASI-C
EPA624 GAW 36 PASI-C
SM 2540C SLB 1 PASI-A
SM 2540D MVC 1 PASI-A
TKN+NO3+NO2 Calculation EWS 1 PASI-A
EPA 350.11993 Rev 20 BRJ i PASI-A
3 EPA351.2 AES2 i PASI-A
I
{ EPA 353.2 CJHi 1 PASI-A
EPAW5.1 CJHi 1 PASI-A
SM 5220D NAL 1 PASI-A
92350243005 MS Room Quench EPA 1664B JMS i PASI G
EPA200.7 SHi 14 PASI-A
3 EPA245.1 KAL 1 PASI-A
EPA625 RES 62 PASI-C
EPA624 GAW 36 PASI-G
SM 2540C SLB i PASI A
SM 2540D MVG 1 PASI-A
TKN+NO3+NO2 Calculation EWS 1 PASI-A
EPA 350A 1993 Rev 2.0 BRJ 1 PASI-A
EPA 3512 AES2 1 PASI-A
I EPA363.2 GJH1 i PASI-A
EPA365A Writ i PASI-A
SM 5220D NAL 1 PASI-A
92350243008 Boller Contlensate EPA16648 JMS 1 PASI-C
EPA 200 SH1 14 PASIA
S
EPA 245.1 KAL i PASI-A
EPA625 RES 62 PASI-C
j EPA624 GAW 36 PASI-C
= SM 2540C SL8 1 PASI-A
SM 2540D MVC 1 PASI A
TKN+NO3IN02 Calculation EWS 1 PASI-A
EPA 350A 1993 Rev 20 BRJ i PASI-A
j
REPORT OF LABORATORY ANALYSIS
This repatl shall not be reprotluced,except in full, '.
wunnut the wrinen consent of Pace Analytical 5emces,LLC. Page 4 of 96

Pace Analytical Services.LLo
aceAnalytical6 2225 Rive,itle 0r
Asheville,NC 28804
1 / ..'anceseas (828)254-]1]6
1
~13
SAMPLE ANALYTE COUNT
Project: Low&Bonar Inc 1210140
Pace Project No.: 92350243
t
( Analyses
Lab ID Sample ID Method Analysts Reported Laboratory
j
EPA 3512 AES2 1 PASI-A
EPA353.2 CJHl 1 PASI-A
EPAW5A WHi 1 PASI-A
j SM 5220D NAL 1 PASLA
i 92350243007 Basement Groundwater EPA16648 JMS 1 PAR C
EPA 2007 SRI 14 PASI-A
EPA245.1 KAL 1 PASLA
EPA625 RES 62 PASI C
- EPA624 GAW 36 PASIC
SM 2540C SLB i PASI-A
E
SM 26400 MVC 1 PAS4A
TKN+NO3+NO2 Calculation EWS 1 PASI-A
EPA 350A 1993 Rev 2.0 BRJ 1 PASI,A
EPA351,2 AES2 i PASI-A
EPA353.2 GJHi 1 PAShA
-... ' EPA365.1 CJH1 1 PASI-A
SM 5220D NAL 1 PASI-A
92360243008 Demarcated @Manhole 25 EPA 1664E JMS i PASI-C
EPA2007 SH1 14 PASLA
' EPA245.1 ML 1 PASI-A
EPA625 RES 62 PASI C
j EPA624 GAW 36 PASI-C
3 SM 2540C SLB 1 PASI-A
SM 25400 MVC 1 PASLA
i
- TKN+NO3+NO2 Calculation EWS 1 PASI-A
EPA 350.11993 Rev 2E BRJ 1 PASI-A
EPA 351.2 AES2 i PASI-A
EPA353.2 CJH1 1 PASLA
1 EPA365.1 CJHi 1 PASLA
SM 5220D NAL 1 PASI-A
ii- 92360243009 New Stormwaler,Point EPA 1664E JMS 1 PASLC
3 EPA 2007 SER 14 PASLA '..
EPA245.1 PAL 1 PASI-A
EPA625 RES 62 PASI C
EPA624 GAW 36 PASI-C
SM 2540C SLB 1 PASI-A
SM 2540D SLB i PASI-A
f%
j REPORT OF LABORATORY ANALYSIS
This revon shall net be rePmaawa,except in m8,
Without the wdnem mcsem of Pecomely[al SerWcea.LLC. Page 5 of 96
i

Pace Analytical Sw,ncea,LLC
Asheille,NC 28804
aceMalytical4 P225 Rivoil sDr
I
- xwnP' aAcam (828)2547176
SAMPLE ANALYTE COUNT
I
Project: Low&Sonar Inc 1210140
Pace Project No.: 92350243
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
TKN+NO3+NO2 Calculation EWS 1 PASI-A
i
EPA 350.11993 Rev 2.0 BRJ 1 PASI-A
EPA 351.2 AES2 i PASI-A
EPA3532 CJH1 1 PASI-A
j EPAWSA CJH1 1 PASI-A
l SM 5220D RAT 1 PASTA
T 92350243010 East Ditch EPA1664B JMS i PASI-C
{ EPA200.7 SER 14 PASI-A
EPA245.1 SAL 1 PASI-A
EPA625 RES 62 PASLC
- EPA624 GAW 36 PASI-C
SM 2540C SL8 1 PASI-A
j SM 2540D SLB 1 PASI-A
TKN+1103+1,102 Calculation EWS 1 PASI-A
EPA 350.11993 Rev 2.0 BRJ 1 PASTA
EPA 351.2 AES2 1 PASLA
EPA 353.2 CJH1 1 PASI-A
EPA3651 CJHI 1 PASI-A
SM 5220D NAL 1 PASTA
92350243011 City Water EPA16648 JMS 1 PASI-C
i EPA200] SER 14 PASI-A
EPA 245.1 KAL i PASTA
EPA625 RES 62 PASI-C
EPA624 GAW 36 PASTC
I
SM 2540C SLB i PASTA
SM 2540D SLB i PASI-A
TKN+NO3+NO2 Calculation EWS t PASI-A
3
EPA 350.11993 Rev 20 BRJ 1 PASI-A
ERA351.2 AES2 i PASTA
EPA 353.2 CJHi i PASLA
EPA 365.1 CJH1 i PASTA '.
SM 5220D NAL 1 PASI-A
I 92350243012 Manhole EPA 16MB JMS 1 PASI-C
l
EPA2003 SER 14 PASTA
¢ EPA245.1 KAL i PASIA
EPA625 RES 62 PASI C
EPA624 GAW 36 PASI-C
st
- REPORT OF LABORATORY ANALYSIS
This report shot not os nepr00000r,except in fun,
"'Tout Te—ron mneem of Pace Analytcai S.—,LLC, Page 6 of 06

Pace Analytical Senlces,LLC
ill_ aceMalytical® a, Riv ASM1eville,NCG 28 28804
nwn�NalLLo-in04
[phone]
SAMPLE ANALYTE COUNT
Project: Low 8 Banar Inc 1210140
1 Pace Project No.: 92360243
Analytes
Lab ID Sample ID Method Analysis Reported Laboratory
I
t SM 2540C SLB 1 PAShA
{ SM 2540D SL6 1 PASI-A
TKN+NO3+NO2 Calculation EWS 1 PASI-A
EPA 350.11993Rev2.0 BRJ 1 PASI-A
'7 EPA3512 AES2 i PASI-A
EPA353.2 CJH1 / PASIA
EPA365.1 CJH1 1 PASI-A
SM 5220D NAL 1 PASI-A
j 92350243013 Manhole 3�1.1 EPA 16648 JMS 1 PAS6C
i EPA 200.7 SER 14 PASI-A
{ EPA245.1 ML i PASI-A
EPA625 RES 62 PASI-C
EPA624 GAW 36 PASI-C
SM 2540C NAL 1 PASI A
SM 2540D SLB 1 PASI-A
3
� TKN+NO3+NO2 Calculation EWS 1 PASI-A
EPA 350.11993Rev2.0 BRJ 1 PASI-A
' EPA3512 AES2 1 PASI-A
EPA 3532 CJH1 i PASI-A
EPA 365_i CJH1 1 PASbA
SM 5220D NAL 1 PASI-A
3 92350243014 Stamey EPA2003 SER 14 PASI-A
SM 5220D NAL 1 PASI-A
3
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REPORT OF LABORATORY ANALYSIS
i
TM1is report she:I not M1e reprotluceQ except in full,
- wllhoul the written consent of Pace Analytical Sources,LLC. Page 7 of 96

`. Pace Analytical Services,LLC
aceAnalXlcal a 2225fe,NC 2e 04
mvxNmaSimm Asheville,NC 266o4
(828)2547176
f
ANALYTICAL RESULTS
i
Project: Love&Bonar Inc 1210140
Pace Project No.: 92350243
Sample: Chiller Room(0-58) Lab ID: 92350243001 Coliectis] 08/02/17 12:32 Received: 08/0311716:47 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
HEM,Oil and Grease Analytical Method:EPA 1664E
Oil and Grease NO m91L 5.0 1 0811711705:09
S
{ 200.7 MET ICP Analytical Melhotl:EPA 200] Preparation Method:EPA 2007
- Antimony ND ug/L 50 1 0810711721:50 0810811721:19 744036-0
4 Arsenio NO ug/L 'To 1 08107/1721:50 0810811721:19 744038-2
Beryllium ND mill. 10 1 081071172150 0810811721:19 7440-41-7
Cadmium NO ug/L LO 1 08/07/1721:50 08108/1721:19 744043-9
Chromium ND mull- SO 1 081071172150 08108/1721'19 744047-3
Copper 52.5 ugd- 5.0 1 0810711721:60 0810811721:19 744050.8
j Lead ND add- 5.0 1 0810711721:50 0810811721:19 7439-92-1
I Molybdenum 1700 ugl- 5.0 1 0810711721:50 08/0811721:19 7439-98-7
Nickel NO m/L 5.0 1 0810711721:50 0810811721:19 7440-02-0
3 Selenium NO uglL 10.0 1 0810711721:50 0810811721:19 7782.49-2
Silver NO ug/L 50 1 081071172150 0810811721:19 7440-22-4
Thallium NO ugA- 100 1 08107/172150 08/12/172028 744028-0
Hardness,Total(SM 2340B) 48500 mill. 662 1 08/07/1721:50 08/08/1721:19
i Zinc 1670 bg11 10.0 1 08107/1721:50 08/0811721:19 7440-68-6
3 245.1 Mercury Analytical Method.EPA 245A Preparation Method:EPA 245.1
Mercury ND ug/L 0,20 1 0810811701:20 08109/17 he 16 743997-6
3_
_ 625MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
Acenaphthene NO um- &D 1 08107117 12 30 0810911723'09 83-329
Acenaphthylene ND ugh, 5.0 1 08107/171230 08109/17 23 09 208-96-8
1 Anfhracene NO ug/L 50 1 08107117 12 30 0810911723:09 12012-7
Benzo(a)anlhracens ND ugh- 50 1 08107/17 12 30 08/09/172309 56-55-3
Bernso(a)pyrene NO mill 5.0 1 08/07/1712:30 OW09/1723:09 50-32-8
Benzo(b)Ouoranthene NO ug1L 5.0 1 08/07/1712:30 08/0911723,09 205-99-2
g Benzo(g,h.gperyfene NO uglL 5.0 1 08107/1712:30 081091172309 191-24-2
I
Benzo(k)Buoranlhene ND mill. 5.0 1 08107/1712:30 08109I1723:09 207-08-9
4-Bromophenylphenyi ether NO ug1L 5.0 1 0810711712,30 0810911723:09 101553
Butylbenzylphlhalate ND ugl- 5.0 1 08/0711712:30 0810911723:09 8568-7
i 4-Chia.3 methylphemoi NO mTL 5C 1 0810711712:30 081091172309 59-50-7
bis(2-Chlomothncy)methane NO ugh, 100 1 08107/1712:30 081091172309 111-91-1
bis(2 Chloroethyl)ether ND ugh, 50 1 08107/1712:30 08/09/1723 aD 11144-4
i 2-Chloronaphlhalene ND ugh, 50 1 0810711712,30 0810911723'09 91-58-7
2-Chforopheno1 NO ug/L 50 1 0&07/1712:30 OW09/172309 95-57-8
4-Chlorophenylphertyl ether NO uglL 50 1 08/07/1712:30 08/09/1723:0) 7005-72-3
Chrysene NO ug1L 50 1 08107/1712:30 08/091172109 218-01-9
1 glosm (a,h)arnmacene NO uga- SO 1 08/0711712:30 0810911723:09 53-70-3
j 1,3-Dichloodarooene ND uglL 5.0 1 08107/1712:30 08109/1723:09 541-73-1
1,4-Diehlorobenzene NO ug/L 5.0 1 0810711712:30 0810911723:09 10646-7
1 3,3'-Oichlombeazidme ND uglL 25.0 1 0810711712:30 081091172309 91-94-1
2,4-Dichlomphenol ND ug/L 50 1 08A0711712:30 0810911723:09 120832
DiCthylphlhalate NO rd;T 5C 1 0810711712:30 0810911723:09 84-66-2
2,4-Dimethylphenol NO uglL 10.0 1 08/071171230 0810911723:09 10567-9
I
- REPORT OF LABORATORY ANALYSIS
This report shall not be reprodt000d except In for,
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Asheville,NG 28e04e4
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[phone]
43
ANALYTICAL RESULTS
i
j Project Low&Bomar Inc 1210140
{ Pace Project No.: 92350243
Sample: Chiller Room(0.58) Lab ID: 92360243001 Collected, 0810211712:32 Received' 08103/1716:47 Maldx'.Wets,
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method:EPA 625 Preparation Method EPA 625
Dimethylphlhalate ND ail 5.0 1 0810711712:30 0810911723:09 131-11-3
Din-butylphlhalale NO ug/l 5.0 1 08107/1712:30 0810911723:09 84-74-2
4.6 Dinitro-2-methylphenol ND ug/L 20.0 1 08107/1712:30 08/0911723:09 534-52-1
- 2,4-Dincrophenol NO ug/L 500 1 0810711712:30 081091172109 51-28.5
2A DiniteAduene NO ugh- 5.0 1 08/07/1712:30 OW0911723:09 121-14-2
2,6-Dinitudoluerle NO uglL 5.0 1 0810711712:30 0810911723:09 606-20-2
Din-oc(ylphlhalate ND ug/L 5.0 1 081071171230 0810911723:09 117-84-0
12-Diphenylhydrazine NO ugr- 5.0 1 08107/171230 0&09/172309 122-66-7
INS(2-Ethylhexythunhalale NO ugh- 50 1 0810711712:30 08/091172309 117-81-7
Fluoranthene NO ugll 50 1 0810711712:30 08/09/172309 20644-0
Fluorene NO ug/L 50 1 0810A1712:30 0810911723:09 86-73-7
Hexachom-L3-butadiene NO LVL 5.0 1 08107M712:30 0&09/1723:09 87-683
Hexachlonmenerne NO ago- 5.0 1 08JO711712:30 0810911723:09 118-74-1
HeMmIrorocychmusithiene NO Igo- Lou 1 08107/17 12 30 08109/1723:09 77-47-4
Hebachloroethaoe NO age- 50 1 0810711712:30 08/091172309 67-72-1
j Indeno(1,2,3-cd)pymre ND ug/L 5.0 1 0810711712:30 08/0911723:09 193-395
Isopharone ND ug/L 10,0 1 08107/1742:30 08/0911723:09 78-59-4
}3&4 Methylphenol(m&p Cresol) NO ug1L Igo 1 08107/1712:30 0810911723:09 15831-10-4
3 Naphthalene NO mg[L 5.0 1 08/0711712:30 0&09/1723:09 91-20-3
- Nitubereene ND mg/L 5.0 1 0810711712:30 0&091172309 98-95-3
S 2-1,11traphenol NO ug1L 5.0 1 08107/171230 08109/1723:09 88-75-5
4-Nitraphenol NO ugh- 500 1 08/07/1712,30 081091172109 100-02-7
N-Nitrosodimethylamine ND Led- 5A 1 0810711712'30 08/09/1723:09 62-75-9
N-Moose thn pmpylamioe ND ug1L 5,0 1 0810711712:30 0810911723:09 621-64-7
- N Nttmsbliphenylamine NO uga- Igo 1 0810711712:30 0819911723:09 86-306
i 2,2'-Oxybis(1-chompropane) NO ug1L 5.0 1 08107/1712:30 0810911723:09 108-60-1
Pentachlorophenol NO ug/L 10.0 1 08107/1712'30 0&0911723:09 87-86-5
[ Phenanlhrene NO ug/L 50 1 081071171230 08/091172309 85-01-8
Phenol NO uglL 5.0 1 08107/1712:30 08109/172309 108-96-2
j Pyrene ND uglL 50 1 08107/1712:30 0810911723:09 129-000
1,24-Trallmobenzene ND ug/L 5.0 1 08107/1712:30 0010911723:09 12082-1
2,4,6-Trichlompheool NO dM/L 10.0 1 081071CT 1230 0810911723:09 88062
Surrogates
Nitrobenzene d5(S) 69 % 10120 i 0 810 7/1 7 1 2:30 0810911723'09 416560-0
,l 2-Fluorobiphenyl(S) 69 % 15-120 1 08107/171230 OW09/1723:09 321-608
Terphenyl d14(S) 69 % 11-131 1 08107/1712:30 08/09/172109 9718-51-0
Phenol d6(8) 24 % 10-120 1 08/07/17 12:30 08109/17 23:09 13127-88-3
2-I'momphenol(S) 35 % 10-120 1 08/07/17 42:30 08/0911723:09 367-12-4 '..
7 2,4,6Tuthromophenol(S) 84 % 10-137 1 08107M712:30 0810911723:09 118-796
624 Volatile Organics Analytical Mother:EPA 624 '..
i
Austein ND mill 50 1 0810811723:24 107-028 L1 '..
I Aerylonildle NO ugo- 500 1 081OW1723:24 107-13-1
3 Benzene NO uglL 20 1 0810811723:24 71-43-2
j Bromodichlembethane ND u911- 20 1 08108/1723:24 75-27-4
Bromoform NO ug/L 20 1 0810811723:24 75-252
I Bromomethane NO uga- 2.0 1 0810811723:24 74839
}
REPORT OF LABORATORY ANALYSIS
This report shell nor be reproduced,except in tell,
Date:08221201710,12 AM ,nhete the ndtten mneent of Pace Analytical Services,LLC. Page 9of 93

i Pace Analytical Services,LLC
1 aceAnalp/ical6 2225 RIvetsitla D[
funewshaJ' Mn Hsheville,NC 28a04
[phone]
ANALYTICAL RESULTS
i
Project: LovtB Boner Inc 1210140
Pace Project No.: 92350243
Sample: Chiller Room(0-58) Lab ID: 92350243001 Collected 08/02/17 12:32 Received: 08/03/17 16:47 Manor Water
Parameters Resulls Units Report Limit OF Prepared Analyzed CAS No, Chat
I
624 Volatile Organics Analytical Mother:EPA 624
Carbon telrachlonde ND ug1L 20 1 0W0811723:24 56-23-5
Chiorobenzene ND ug/L 20 1 08/08/1723:24 108-90-7
Chioroethans NO ugh- 2.0 1 08/0811723:24 75003
Chloroform NO U91 2.0 1 08/0811723:24 67-663
Chloromethaoe ND argil. 2.0 1 08/0811-72324 74-87-3
Dibromochloromeihane ND ug1L 20 1 08108/1723:24 124-48-1
1,2-Dichlorobenzene ND ugR 20 1 0810811723:24 95-504
1,3-Dichloobenzene ND no& 2'0 1 08/0811723'24 541-73-1
IA-Dief-drobenzene NO till. 2.0 1 0810811723'24 106-46-7
1,1-Dicdoao.manA ND uglL 2.0 1 08108/1723:24 7534-3
1,2-Dichloroethane ND ugg- 20 1 08/0811723:24 107-06-2
1.1-Oichlomethene ND ugll 20 1 0810811723:24 75-354
i cis-Ig-Dichioroethene ND ug/L 20 1 08/0811723:24 156-59-2
trans4,2-Dichforoethoe NO ugt 2.0 1 08/08/1723'24 1 Sit 60-5
1,2-Dichtoropropane NO ug/L 2.0 1 0810811723'24 7887-5
cis-1,3Dichloropropene ND add- 20 1 08108/172324 10061-01-5
trials-1,3-Dichloropropene ND ug/L 20 1 08/08117 23 24 10061-02-6
"'.Emyllatmone ND ug/L 2.0 1 0810811723:24 10041-4
Methylene Chloride ND u f- 2.0 1 0810811723:24 7509-2
1,1,2,2-Tetrachioroelhane NO ug/L 2.0 1 0WOW1723:24 79-345
Telrachloroelhene ND ug/L 2.0 1 08108/172324 127-18-4
Toluene ND ug1L 2.0 1 08108/172324 108-88-3
1,1.1-Trichlodelhane ND ugll 20 1 0810811723:24 71-556
L1,2-Tdchloroethene ND rage- 2.0 1 0810811723:24 79-00-5
Tochloroelhene NO ug/L 2.0 1 08/0811723:24 79-01-6
i Tochloro0uommethane NO upl- 2.0 1 0810811723'24 7569-4
3 Vinyl chloride NO ug/L 2.0 1 08/0811723:24 7501-4
1 Surrogates
4-Bromofforobenome(S) 106 % 70-130 1 08108/1723:24 46000-4
Toluene-dig(S) 114 % 70130 1 0810811723:24 2037-26-5
1.2-DichlOroethane d4(S) 86 % 70-130 1 081081172324 17060-070
i
2540C Total Dissolved Solids Analytical Method:SO 2540C
Total Dissolved Solids 642 and- 250 1 0810811709:34
2540D Total Suspended Solids Analytical Method:Slid 2540D '..
Total Suspended Solids 4.9 mgd 2.8 1 08/08/171706
Total Nitrogen Calculation Analytical Method:TKN+NO3+NO2 Calculation
Total Nitrogen 4.4 milt. 0,12 1 08109/1718:11
350.1 Ammonia Analytical Method:EPA 350A 1993 Rev 2.0
j Nitrogen'Ammooia ND mg1L 0,10 1 0810911702:47 766441-7.....Total Kj...ahi Nitrogen Analytical leaned:EPA 351.2
Nitrogen,Kjeldahl,Total 1.6 grill. 0,50 1 08109M71653 7727-37-9
I
REPORT OF LABORATORY ANALYSIS
t TiN report chat no,be repmnuee l exoavtm mn,
Dale:0W2 212 017 10:12 AM without the wdnen coosenmf Paeennalylical Servlces,LLC Page 10 of 96
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Pace Analytoal NC Services.LLC
3
I aceAnalytical 2225 Ri 2e D1.
a»w�urTm asnevne,rvc 28e04
(62e)254-717e
( ANALYTICAL RESULTS
( Project: Lose&Boor Inc 121040
Pace Project No.: 92350243
i
3 Sample: Chiller Room(0-58) Lab ID: 92350243001 Collected: 08102/17 12 32 Received: 08103/17 16:47 Matrix.Water
13 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Cost
353.2 Nitrogen,NO2IN03 pres. Analytical MelhW:EPA 353.2
Nitrogen.NO2 plus NO3 2.7 dg/L 0020 1 0W0911712'03
365,1 Phosphorus,Total Analytical Method:EPA 365.1
Phosphorus 10.9 raga- 0,25 5 08/0811708:44 7723-140
? 5220D COO Analytical Method:SM 5220D
l
Chemical Oxygen Demand 67.0 mglL 25.0 i 08/07/17 18:4/
Sample: Slim Tank Lab ID: 92360243002 Collected 08102/1715:bar Received: 08103/1716:47 Maps, Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
I
HEM,Oil and Grease Analytical Method EPA 16648
i
Oilantl Grease NO mglL 5.0 i 08/17/1705'09
]` 200.7 MET ICP Analytical Method:EPA 200.7 Preparation Method:EPA 200.7
Antimony NO ug/L 5D 1 08/0711721:50 08/08/172122 7440-36-0
---Arsenic NO add- 10.0 1 0810711721:50 08108/472122 744038-2
Beryllium ND muL 1.0 1 08107/1721:50 08108/1721'22 7440-41-7
' Cadmium NO ug/L 1.0 1 08107/172150 0810811721:22 7440-43-9
Chromium NO ug1L 5.0 4 08107/172150 08/0811721'22 744047-3
Copper 7.6 ug/L 50 4 08/0711721:50 081081172122 7440-508
Lead NO ug/L 50 1 0810711721:50 08/081172122 7439-92-1
Molybdenum NO ug1L 5D 1 0810711721:50 08108/172122 7439987
Nickel NO ugh- 50 1 0810711721:50 08108/1721:22 7440-02-0
Selenium NO rag/L 100 1 08107/1721:50 081081172122 7782-49-2
- Silver NO ug/L 5.0 1 08107/172150 08/081172122 7440-224
Thailand NO ug1L 10D 1 08/0711721:60 08/12/1720:31 7440280
i Hardness,Total ISM 2340B) 5790 rag/1- 662 1 0810711721:50 08/0811721:22
Zinc 220 ugd- 1(0 1 0810711721:50 08108M72122 7440-e68
246.1 Mercury Analytical Method:EPA 245.1 Preparation Method:EPA 245.1
aMercury NO rag/L 0.20 1 08108117 01 20 0810911706:18 743997-6
L
- 625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
Acenaphthene NO ug1L 5.0 1 0810711712,30 081081170348 83-32-9
f Acenaphlhylene NO rapid- 50 1 08/0711712:30 081081170348 208-9"
Andracene ND uglL 50 1 0810711712:30 08/08117 03 48 120-12-7
Benze(a)anthracens NO ug/L 50 1 0810711712:30 08/081170348 56-55-3
:j Bemaddpyrene NO ug/L 5D 1 08/0711712:30 081OW1703AB 50-32-8
F Beezodamoranlhene NO ui 5.0 1 08107/1712:30 TY0811703:48 205-992
Benzo(g.gi)perylene ND ugh- 5D 1 08/07/1712:30 08/08/17 WAS 191-24-2
Benzo(k)flumandene ND ug1L 5.0 1 08/07/1712:30 0810811703:48 207-09-9
4-Bromophenylphenyl ether NO rapid- 5.0 1 08107/1712:30 081081170348 101-55-3
Butylberaylphthmale NO ug(L 50 1 0810711712:30 0810811703:48 85-68-7
3
t "
REPORT OF LABORATORY ANALYSIS
This report shall net be reproduced,except N fe0.
Date:0 812 212017 10A 2 AM Wuhout Re wIten emsent of Pace Analasel Services,LC, Page 11 of 96
f{7
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firPane Analytical ServlCes,LLC
�CUn„a .yical® 2225 ft,NO 2e Or.
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ANALYTICAL RESULTS
t
Project: Low&Damon Inc 1210140
- Pace Project Na: 92350243
I Sample: Slim Tank Lab ID: 92350243002 Collected: 08102M715:00 Received: 0W0311716:47 Matrix:Water
Parameters Results Units Report Limit DE Prepared Analyzed GAS No, Qual
625 MSSV Analytical Method:EPA 625 Preparation hlelhod:EPA 625
4 Chloro-3 methylphenoi NO ug1L 5.0 1 0810711712:30 08108/17 03 48 59-50-7
j bis(2-Chioroethoxy)methane NO ugiL 10.0 1 08107/1712:30 0810811703:48 111-94-1
bis(2-Chioroethyl)ether NO mill 5.0 1 0810711712:30 08/08/17 WAS 111444
2-Ghloronaphthalene NO ug/L 5.0 1 081071171230 08/08/1703:48 9158-7
2-Chlorophenol NO ugL 50 1 0810711712:30 08108/170348 95-57-8
4-Chlorophenylphenyl ether NO ugiL 50 1 0810711712:30 08108/1703:48 7005-72-3
Chrysene NO ugL 50 1 08107/1712:30 08108/1703:48 218-01-9
famenz(a,h)anihracene NO ugL 50 1 08/0711712:30 08108117 03 48 53-70-3
13 Dichlorobenzene NO ugiL 5.0 1 0810711712:30 08/0811703:48 541-73 1
1A Dichlooleenzene NO ug1L 5.0 1 0810711712:30 08/0811703:48 106AG-7
3,3'-Dichlorobenzidine NO ugiL 250 1 08107/1712:30 081081170318 91-94-1
2,4-Dichloomianol NO ugL 50 1 0810711712:30 08/0811703:48 12083-2
j Diethylphthalate NO ug/L 5.0 1 0810711712:30 0810811703:48 84-66-2
2,4-Diametelpheool NO uglt 10.0 1 08107/1712:30 0810811703:48 105-67-9
1 Dimethylphthalate NO mpl- 5.0 1 0810711712:30 08ION1703:48 131-11-3
Di inbutylphthalate NO ugL 5.0 1 0810711712:30 08ION1703:48 84-74-2
- 4,6-Dinifro-2-methylphenoi NO ugL 200 1 0810]Ii712:30 08/08/1703:48 534-52-1
- "- 2.4-DInieophenol NO ugL 500 1 08107/171230 08108/1703:46 51-28-5
2,4-Dinitrotoluene NO ugL 5.0 1 0810711712:30 08108/1703:48 121-14-2
2,6-Diniimto1uene, NO ugL 50 1 08107/1712:30 OBI08/1703:48 606-202
Di N octylphthalate NO ugll. 50 1 08/07/1712:30 0810811703:48 117-84-0
1,2-Diphenylhydrazine NO ugiL 50 1 08107/1712:30 0810811703:48 122-66-7
bis(2-Etbylhexyl)phthalate NO ugiL 5.0 1 08107/1712:30 OBI0W1703:48 117-81-7
Fluoranthene NO ugiL 5.0 1 0810711712:30 08/08/1703:48 20 44-0
Humerus NO ugiL 50 1 08107/1712:30 0810811703:48 B6-73-7
Hexachloro-i,&bulamene NO ug1L 5.0 1 08/07/1712:30 081081170348 87-68-3
Hexachlorobenzene NO ugiL 5N 1 08107/1712:30 0810811703:48 11874-1
Hexachlorocyclopenladiene ND ugiL INN 1 0810711712:30 08108/170348 ]]-47-4
Hexachloroethane NO ugL 5.0 1 0810711712:30 08A)8/1703:48 67-72-1
indeno(1,2,3-cd)pyrene NO ugiL 5N 1 08f0711712:30 081081170348 193-39-5
i Rophorone NO ugiL VON 1 08107117 12 30 081OW170348 78 59-1
3 384-Melhylphenol(m&p Camino) NO ug/L 10.0 1 08107I1712:30 08/08/1703:48 15831-10-4
Naphthalene NO ugL 50 1 08/071171230 081081170348 91-20-3
_ Nitrobenzene NO ugL 5.0 1 0810714712:30 08108117 03 48 98-95-3
2 Nitmphenal NO ugiL 5.0 1 0810711712:30 08108/1703:48 88-75-5
4-Nihophenol NO ugL 500 1 0810711712:30 08108/170348 100-02-7
N Nitio (olnuothylamme NO ugL 5D 1 0810711712:30 08/08117 03 48 62-75-9
N-Nitroso-di-n-propylamine NO ugiL 50 1 0810711712:30 0810811703:48 621-64-7
I N-Nilmo odipheaylwarsu NO ugL 100 1 08/0711712:30 081081170348 86-306
2,2'Oxybis(Lchlompropane) NO ugiL 5.0 1 08/07/1712:30 0810811703:48 108-60 1
perrachl0rophenol NO ugiL 100 1 08/07/1712:30 08/0811703:48 87-86-5
[ Phenanihimne NO ug/L NO 1 OBJ07/1712:30 081081170348 85 01-8
1 Phial NO ugiL 5.0 1 0810711712:30 0810811703:48 108-95-2
Pyume ND ugiL 5.0 1 0810711712:30 0810811703:48 12900-0
L2,4-Tdchlorobenzene NO ugiL 60 1 0810711712:30 08/081170348 12082-1
2,4,6-Tdchlorophenol NO mg1L lao 1 08/07/1712:30 08/0811703:48 80-M2
i
~� REPORT OF LABORATORY ANALYSIS
The report snot not be reproduced,except in fA,
Date:08/22/201710:12 AM 11th.c me wdtean-..art of Pace Analytcal Services,LLC. Page 12 of 96

3 Pace Analytical j Serv.ices,L LC
225RNetstleOracqpAnalyticale Ache le
NC 2SU04
n»w aan [phone]
I
t
i ANALYTICAL RESULTS
i
Project: Law&Bomar Inc 1210140
Pace Project No.: 92350243
Sampla: Slim Tank Lab1D: 92350243002 Collected: 0810211715:00 Received 0810 311 7 16:47 Matrix Water
7
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
I
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA625
Surrogates
3 Nitrobenzene-d5 Cd 31 % 14120 1 08(07/1712:30 OW0811703:48 416560-0
2-Fluorobiphenyl(S) 34 % 15-120 1 08/07/1712:30 0810W1703:48 321-60 8
# TeMhenybd14(S) 61 % 11-131 1 0810711712:30 0810811703:48 1718-51-0
t` Phenobd6(S) 11 % 16120 1 0810711712:30 08101111703:48 1312T883
1 2-Fluorophenol(S) 18 % VL 20 1 0810711712:30 08/0811703:48 307-12-4
5 2,4,6-Tubromophemol(8) 56 % 10-137 1 08107/1712:30 0810811703:48 118-796
624 Volatile Organics Analytical Method:EPA 624
- Acrolein NO ug1L SB 1 OW0811722:13 107-02-8 11
Acrylonitdle NO ug/L 50.0 1 08108/1722'13 107-13-1
Benzene NO mill 20 1 0810811722'13 4443-2
Bmmodichlommethane NO ug/L 2.0 1 081OW1722:13 75-27-4
Bramoform ND uglL 2.0 1 OW081472213 75-25-2
Bromomelhane NO ug/L 20 1 0810811722:13 7483-9
3 Carbon tetrachloride ND eg/L 20 1 OW0811722:13 6623-5
Chlorobenzene NO uglL 20 1 0810811722:13 108-90-7
Chlormthane ND ug/L 20 1 0810811722:13 7500-3
modicum NO mill- 2B 1 08/08/1722:13 67-66-3
.: 61bloromethane NO cB1 20 1 08/08(l722:13 74-87-3
Dibromochimromethane NO ugn- 2B 1 08108/1722:13 12448-1
1,2-Dichlor06enzene NO ugf- 2.0 1 081OW1722:13 95-50-1
1.3 Dichioro0enzene ND ug1L 2.0 1 OBIOW1722:13 541-73-1
1,4-Dichlorobenzene NO uglL 20 1 0810811722:13 106467
1,1-Dichdoroethane ND ug1L 2.0 1 08/0811722,13 75-34-3
{ 1,2-Dichieroethane ND ug/L 20 1 0810811722:13 107-062
y 1,1-Diohloroethene NO ugll. 20 1 08108I1722:13 75-354
cis-1,2-Dichlorcethene NO ug1L 2.0 1 08/0811722:13 16659-2
_ hams-1,2-Dichloroemene ND ugr- 2.0 1 OW0811722:13 156-60-5
1,2-Dichlompropane NO ugn- 2B 1 DWOW1722:13 78-87-5
cis 1,3�Dichioropwpene ND ug0. 2B 1 08/DW1722:13 10061-01-5
trans-1.3,DiOloropropene ND Lira- 20 1 0810811722:13 10061-02-6
Ethylbenzene ND ug1L 2B 1 08108/1722:13 100-41-4
Methylene Chloride NO ug& 2.0 1 OBIOW1722:13 7509-2
1,1,2,2-Tetrachlorcethane ND ug/L 20 1 08/0811722:13 79-34-5
Telachloroethene ND ug1L 2.0 1 OW0811722:13 127AB-4
Toluene NO ug/L 20 1 0810811722'.13 10888-3
LLI-TrlchlmoeUane ND ug1L 20 1 0810811722:13 71-556
1,1,2-Tdchlomethane ND ug/L 20 1 0810811722:13 7900-5
Tdchloroethene NO mbl- 20 1 0810811722:13 7901-6
Tad1orolluoromeihane NO ug1L 2.0 1 OW0811722:13 7569-4
Vinyl chloride NO ug/L 2B 1 08/08/1722:13 7501-4
3 Surrogates
4-Bromo(loorobemzene(S) 101 % 70-130 1 0810811722:13 460-004
- Toluene 18(5) Ill % 70-130 1 08/08/1722:13 2037-265
1,2-Dichloroetimm,d4(S) 83 % 70-130 1 081OW1722:13 17060073
S
REPORT OF LABORATORY ANALYSIS
jThis report char na1 be u,,aeducetl,except io full,
Date:0812 212 017 10A2 AM w.mon the women consent at Pace Anaqucat Semicec,LLC Page 13 of 96 '..
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ANALYTICAL RESULTS
Project: Low&Sonar Inc 1210140
j Pace Project No.: 92350243
Sample: Slim Tank Lab ID: 92350243002 Collected 08/02/17 15:00 Received: 08/03/17 16:47 Matrix:Water
i Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Coal
}
2540C Total Dissolved Solids Analytical Method:SM 2540C
I
1 Total Dissolved Solids 63.0 mill- 25A 1 08W1709'35
2640D Total Suspended Solids Analytical Method:SM 2540D
Total Suspended Solids NO mg/L 2S 1 08/08/1717,07
{_ Total Nitrogen Calculation Analytical Method:TKN+NO3aNO2 Calculation
Total Nitrogen 0.37 mg/L 0.12 1 08/09/17 18:11
I
350.1 Ammonia Analytical Method:EPA 350.11993 Rev 2.0
i
Nitrogen Amorous NO roil- 010 1 08109/1702:49 7664 41-7
351.2 Total Kjeldahl Nitrogen Analytical Method:EPA 351.2
Nitrogen,Kjeldahl,Total NO Toga- OSO 1 OW0911716:56 7727-37-9
i
353.2 Nitrogen,N0VN03 pros. Analytical Method:EPA 353.2
- Nitrogen,NO2 plus NO3 0.11 roil- 0,020 1 08/09/17 12:04
365.1 Phosphorus,Total Analytical Method:EPA 365.1
1jhosphorus 0.76 mgd- 0.050 1 01310811707:44 7723-14-0
5220D COD Analytical Method:SM 5220D
j Chemical Oxygen Demand ND regal- 25.0 1 081071171841
Sample: Cooper Cooling System Lab ID: 92350243003 Collected 0 810 211 7 14:04 Received: 0 810 311 7 16:47 Matrix:Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM,Oil and Grease Analytical Method:EPA 16646 s
r Oil and Grease 36.3 m9/L 5A 1 08I17/1705:09
200.7 MET ICP Analytical Method:EPA 200.7 Preparation Method:EPA200-7
Antimony NO TPI 5.0 1 0810711721:50 OW0811721:34 7440-M0
- Arsenic NO ugh- 10A 1 0810711721:50 0810811721:34 7440-38-2
Beryllium NO ug/L 1.0 1 0810711721:50 081081172134 744041-7
Cadmium NO mtl 10 1 0810711721:50 08108/172134 7440439
Chromium NO ug/- 50 1 0810711721:50 08108/1721-34 7440-47-3
Capper 28.6 uglL 5.0 1 08I07/172150 0810811721:34 7440-508
Lead NO ug1L 5.0 1 08/07/172150 0W0811721:34 743992-1
Molybdenum NO ug/L 5.0 1 08/0711721:50 081081172134 7439-987 '..
,j Nickel ND ug/L 5.0 1 08107/1721:50 08/0811721:34 7440-02-0
Selenium NO mill. 100 1 0810711721:50 08/0811721:34 778249-2
Silver NO mpL 5.0 1 08107/1721:50 0810811721:34 7440-22-4
# Thallium ND high- 10.0 1 08107/1721:50 08112/172034 7440-280 '..
Hardness,Total(SM 23401g 6660 cm- 662 1 08a0711721:50 08108/17 2134
3
1
REPORT OF LABORATORY ANALYSIS
This repair shall not be reproduced.except in rum.
Date:0812 212 017 10:12 AM 'cled me"'Iten cm.sat of Pace Analyr tSemces,uc Page 14 of 96
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i
ANALYTICAL RESULTS
1 Project: Low?,Sonar Ina 1210140
i
j Pace Project No.: 92350243
3 Sample: Cooper Cooling System LablO: 92350243003 Collected: 08/0211714:04 Received: 08/03/171647 Matrix:Water
Parameters Results Units Report Limit DF Prepared AniWed CAS No. Coal
t
I 200.7 MET ICP Analytical Method:EPA 200.7 Preparation Method:EPA 2007
/
Zinc 2" opE 10.0 1 08IG7117 21:50 08/08/17 21:34 7440 66 6
I
245.1 Mercury Analytical Method:EPA 245.1 Preparation Method:EPA 245.1
Mercury NO ug& 0.20 1 081081170120 0810911706:32 7439-97-6
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
Aceaaphthene NO ug/L 5.0 1 08/0711712:30 O80081170417 83-32-9
Acenaimmylene NO ug/L 5.0 1 08107/171230 08108/1704:17 208-96-8
Anthracene NO halt, 50 1 08107/171230 08/0811704:17 12012-7
i
Benzo(a)anthracene NO ug/L 5.0 1 08107/1712:30 0810811704:17 56553
� Benzo(a)pyrene NO ug1L 60 1 08/07/1712:30 08IOBI170417 50-32-8
Benzo(b)Ouoranthene NO uglL SO 1 0810711712:30 08108/1704:17 205-99-2
Senzo(9.h.i)perylene NO h91L &0 1 08/0711712:30 0810811704:17 191-24-2
8enzo(k)0uoommene NO ug/L 5.0 1 08/0711712:30 08/081170417 207-08-9
4-Bromophenylphenyl ether NO ug/L SA 1 08107/1712:30 0810811704:17 101-553
Butylbenzylphthalete NO opt- 5.0 1 08107/1712:30 08/0811704:17 85-68-7
4 Chiom-3-methylphenol ND pg/L 50 1 08107/1712:30 081OW1704:17 59-50-7
,.ns(2-Chlorosthoxy)melha e, NO ug/L 10A 1 081071171230 08108I1704:17 111-91-1
or(2-Chloroethy)ether NO halt, 5R 1 081071171230 08108I1704'17 111-444
3 -"2-Chlomnaphthalene NO uglL 5.0 1 0810711712:30 08108/1704:17 91-58-7
2-Chlomphenol NO uglL So 1 08I0711712:30 08/0811704:17 95-578
t 4-Chlorophenylphenyl ether NO plot, 5.0 1 08/071171230 0810811704:17 7005-72-3
Chrysene NO ng/L 50 1 08107/1712:30 081OW1704:17 218-01-9
Diberz(a,h)aothracene NO ug/L 5.0 1 08107/171230 0810811704:17 53-70-3
1,3-Diedlorobenzene NO ug/L 50 1 08107/1712:30 0810811704:17 541-73-1
1,4-Dichlorabenzene NO ugp- 50 1 0810711712:30 08108/1704:17 106-46-7
' 3,T-Dichlopmeormine NO ug1L 25.0 1 0810711712:30 OBIOW1704:17 91-94-1
2,4 Dichlorophenol NO halt, 5.0 1 08/0711712:30 08108117 04 17 120-83-2
Diethylphthalate ND ug/L 50 1 0810711712:30 0810811704:17 8466-2
2.4-Dlmethylphenol NO imlL t0.o 1 08107/1712:30 0910811704'17 10567-9
- Dimethylphthalate NO ug/L Ro 1 08107/1712:30 0810811704:17 131-113
Di-n-butylphthelale NO ug/L 5.0 1 08107/1712:30 08/0811704:17 84-742
4,6-Dinitro-2-methylphenol NO hg/L 20.0 1 08/0711712:30 081081704'17 534-52-1 '..
1 2,4-Dinitrophenol NO ug/L 500 1 08107/1712:30 08I08/1704:17 51-285
2,4-Dinilro,durne NO ug1L 5R 1 0810711712'30 0810811704'17 121-14-2 '..
2,6-Dinilrotomene NO uglL 5.0 1 0810711712:30 08/0811704:17 606-20-2
Di-n-octylphlhalate NO uglL 5.0 1 0810711712:30 08108I1704:17 117840
1,2-Diphenylhydrazine NO ug/L 5.0 1 08107A712:30 0W0811704'17 122-66-7 '..
t mr(2-EthyliesgIghthalate NO hg/L 50 1 08107/1712:30 08/08/1704:17 117-81-7 '..
? Fluoramhene NO ugh- 50 1 08107/1712:30 081OW1704'17 20644-0
Fluorene NO rppL 50 1 0810711712,30 08/0811704,17 86-73-7
Hexantom1,3 botadiene NO ug/l 50 1 0810711712:30 0810811704:17 87-683
7 Hexachloomoreene NO ug1L 50 1 0810711712:30 081MV1704'17 118-74-1
Hexachlowcyclopentadiene NO uq/L 10.0 1 08107117 12:30 0810811704:17 77-47-4
( Hexachlomeman, NO uglL SA 1 0810711712:30 0810811704:17 67-72-1
r Indeno(1,2,3-od)pyrene NO hall- 5.0 1 0810711712:30 08/0811704:17 193-395
t
i
REPORT OF LABORATORY ANALYSIS
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j ANALYTICAL RESULTS
project: low&Bomar Inc 4210140
i
Pace Project No.: 92350243
Sample: Cooper Cooling System Lab I0: 92350243003 Collected: 08/02/1714:04 Received: 08I0&1]164] Matrix:Water
parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
Isommose NO ug4 100 1 08/07/1712:30 0810811704:17 78-591
3&4-McNylphenol(mBp Cresol) NO USAF 10.0 1 08107/1712:30 0810811704:17 15831-10-4
Naphthalene NO uga_ 5.0 1 0810711712:30 0&0&170417 91-20-3
[ Nitrobenzene NO ug/L 5,0 1 08107/1712:30 08108117 04 17 98-95-3
2-Nihophenol NO ug1L 50 1 08107/171230 081OW1704:17 8875-5
4-Nihophenol NO ug/L 50.0 1 08107/1712:30 0810811704:17 10002-7
N-Nitrosodimethylamine ND ig/L 50 1 08107/1712:30 0810811704:17 62-75-9
N-Nitrosodi-a,emylamine NO ug& SA 1 0810711712:30 08/08/17 o4:17 621 64-7
N-Wousidiphenylamine ND ug/L had 1 0810711712:30 OW0811704'17 86-30 6
z 2,2'-Oxybls(1-chloropropane) NO ug/L 5.0 1 08107M712:30 0&0&170417 10860-1
Penlachlorophenol NO ug/L 10.0 1 08107/171230 0810811704:17 87-86-5
Phenanthrene ND ugo- 50 1 0810711712:30 0810811704:17 85-01-8
Phenol NO ug/L 50 1 08107/1712:30 OMOW170417 108-95-2
j Pyrene NO ug/L 5.0 1 0810711712:30 08I081V 04:17 129-00-0
1,44-TrichImebenzene NO USAF 5.0 1 08/0711712:30 0&0811704:17 120-82-1
j 2,4,6-Trichloropheno1 ND ug/L 10.0 1 08/0711712:30 08108/170417 88-06-2
Surrogates
Nihbenzene-d5(8) 74 % 10120 1 081071171230 OW0811704:17 416560-0
"2-Fluombiphenyl(8) 74 % 15-120 1 0810711712:30 0810811704:17 321-60-8
_ „Wpheryl N14(S) 49 % 11-131 1 08107/1712:30 0810811704:17 1718-51-0
Phenol-d6 Rd 25 % 10-120 1 08107/1712:30 OW08/1704:17 13127-88-3
2-Fluorophenol(S) 43 % 10-120 1 0810711712:30 0810811704:17 367-12-4
2,4,6-Tribromophenol(S) 87 % 10.137 1 0810711712:30 08/0811704:17 118-09-6
624 Volatile Organics Analytical Method EPA624
Anatole NO ug/l. 50 1 08108/1723:42 107-02-8 Ll
Awynoni0ile ND ug/L 500 1 08108/1723'42 107-13-1
7 Benzene NO ugh. 20 1 0810&172342 71-43-2
j Bromodichlommethane ND ugAL 2.0 1 0810811723:42 75-27-4
Bromoform ND ug/L 2.0 1 0&0&1723'42 75-25-2
Bromomethane NO nee- 2P 1 08AMM723:42 74-83-9
3 Carbon tetrachloride NO mpl_ 2.0 1 08/08/1723:42 56-23-5
` Chlorobenzene NO mi 20 1 08/081172342 108-90-7
i Chi oroelhane NO ug/L 20 1 081081172342 75-003
I Chloroform 2.3 ug/L 20 1 081081172342 67-66-3
Chlommethane ND Ug1L 20 1 0810&1723:42 74-87-3
Ddonertctloromethane NO uglL 2.0 1 081081172342 124-48-1
1,2.Diohlorobenzeme ND .,at 2.0 1 0&08/1723:42 95-50-1
1,3Dichlorobenzene NO ugh. 2.0 1 08108117 23 42 541434 '..
14-Dichlumbeneene NO ug/L 2P 1 08108/172342 10646-7
1,1-DichlUroelhane NO USAF 20 i 0 810 8117 23:42 75-34-3
j 1,2-Dichmcbrdhane NO nPL 20 1 081081472342 107-062
1,1-Dichloroelhene NO ug/L 20 1 08/0811723A2 75 35 4
7 cis-1,2-Dichloroelhene NO USAF 2.0 1 0810811723:42 156-59-2
I trans-1.2-Dichloroelhene NO add 20 1 08108,172342 15660-5
i 1,2-Dichloroprepane ND ug/L 2.0 1 0MOW172342 78-87-5
I cis-1,3-Dichloropropene NO umL 2.0 1 0810811723:42 1006101-5
REPORT OF LABORATORY ANALYSIS
3 Trc report shall not be mpmdueeU,except In but,
Date:081221201710,12 AM -bout the written consent of Pace Analyw,at Services LLC Page 16 of 96
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t Pace Analytical 80-ices,LLC
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aceAnalytical Ashevelle,NC 28804
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7 I
ANALYTICAL RESULTS
Project: Low&Boost Inc 1210140
Pace Project No.: 92350243
Sample: Cooper Cooling System Lab1D: 92360243003 Collected: 08/02/1714:04 Receive! 08/03/171647 Ma1mc Water
i
l Parameters Results Uni(s Report Limit OF Prepared Analyzed CAS No. Qual
3 524 Volatile Organics Analyliwl Method:EPA 624
3 trans-1,3-Dichlompropene NO uEL 20 1 OW0811723:42 10061-02-6
Ethylbenzene ND ug/L 2.0 1 081OW1723:42 10041-4
Methylene Chloride NO ug/l 2.0 1 08108/1723'42 75-09-2
1,1,2,2-Tetrachloroel rms, NO ug/L 2.0 1 08108117 23 42 79-34-5
Telrachloroefhene ND ug/L 20 1 08108/1723:42 127-184
i Toluene NO ug/L 20 1 0810811723:42 108883
- 1,1,1-Tdchloroethane NO ug/L 2.0 1 08/0811723:42 71-55.6
1,1,2-Owhloroeihane NO ug/L 2.0 1 081OW1723'42 79-00-5
Tdchloroethene ND ug/L 2.0 1 081OW1723:42 7901-6
Tdchloro mwomeihane ND ug/L 2.0 1 08hdV1723'42 75-69-4
Unyl chance ND ug/L 20 1 0810811723:42 75-01-4
Surrogates
3 4-Bmmonuorobenzene(S) 103 % 70-130 1 08/09/1723:42 460-00-4
Tolueal(S) 113 % 70130 1 OW081172842 2037-26-5
- 1,2-Dichloroethaoe-d4(S) 86 % 70-130 1 08/0811723:42 17WO 07-0
2540C Total Dissolved Solids Analytical Method:SM 26400
{
Total Dissolved Solitls 57.0 ral 25.0 1 0808117 09 35
a--400 Total Suspended Solids Analytical Method:SM 2540D
Total Suspended Solitls NO mmL 2.5 1 WOW 717:07
Total Nitrogen Calculation Analytical Mother:TKN+NO3-NO2 Calealalion
Total Nitrogen 0.85 mpi- 0,12 1 OW09/1718,11
- 350.1 Ammonia Analytical Method:EPA 350.11993Rev20
{ Nitrogen.Ammonia ND all 0,10 1 0810911702,50 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Moment:EPA 35L2
j Nitrogen,Kleldahl,Total 0.61 mgl- 0.50 1 ON09/17 16,57 7727-37-9
353.2 Nitrogen,N021NO3 pros. Analytical Method:EPA 353,2 '..
Nitrogen,NO2 plus NO3 0.24 tr,a& 0.020 1 081091171208 '..
365.1 Phosphorus,Total Analytical Method:EPA 365.1 '..
t
j Phosphorus 0.82 all 0050 1 0811011706:30 7723140
i
5220D COD Analytical Method SM 5220D '..
Chemical Oss do Demand NO mg/L 25A 1 0810711718'41
i
"1
i
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5 REPORT OF LABORATORY ANALYSIS
£ This repon short not ce repcclueec,except In full,
Date:08I221201710:12 AM without the written consent of Pace Analytcal Se,c ,LLC. Page 1]of 96
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Ashriale,NC 28804
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ANALYTICAL RESULTS
3
Project Low&Bond, Inc 1210140
Pace Project No.: 92350243
s
Sample: MI&M4 Room Quench Lab ID: 92350243004 Collected: 0810211717:05 Received 08JO31171647 Muni trader
jParameters Results Units Report Limit DF Prepared Analysed CAS No, Qual
1 HEM,Oil and Grease Analytical Method:EPA 16646
p Oil and Grease 8.6 mgll 5.0 1 08/17/1705:10
t
200.7 MET ICP Analylical Method:EPA2007 Preparation Method:EPA2003
Milli NO ug/L 5A 1 08JO711721:50 08/08117 21 38 7440-360
Arsenic NO ug/L 10.0 1 08107/1721:60 WORD 72138 7440-38-2
3 Beryllium NO di 1.0 1 0810711721:50 08/081172138 7440-41-7
i Cadmium NO uglL I'd 1 08/0]/1]2150 0810811721:38 744043-9
Chromium NO ugll. SO 1 0810711721:50 0810811721:38 7440-47-3
Copper 54.5 ug/L 5.0 1 08107/1721:50 0810811721:38 7440-60-8
Lead ND ug/L 5.0 1 08/071172150 08101 7439-92.1
Molybdenum NO ug/l 5.0 1 010711721:SO 08/08/1721:38 7439-98-7
Nickel NO ug/L 5.0 1 08/0711721:50 OW0811721:38 744002-0
Selenium ND ugll 10.0 1 08/0711721:50 0WOW1721:38 7782-49-2
Silver ND uglL 5A 1 08107/172150 081081172138 744022-4
Thallium NO ug/L 10A 1 08/0711721:60 081121172037 7440-28-0
Hermosa,Total(SM 23408) NO uglL 662 1 08107/1721:50 08/081172138
} Zinc 170 ugh- 10,0 1 08107/1721:50 081081172138 7440-66-6
45.1 Mercury Analylical Method,EPA 245.1 Preparation Method:EPA 245A
'-'iNercury ND uglL 0.20 1 08/08/1701:29 08I09/1706:34 7439-97-6
i
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
3 Acenapdhene NO rap- 50.0 10 0810711712:30 08/0911723:38 83-32-9
- Acenaphthylene ND ug/L 50.0 10 08/0711712:30 ON0911723:38 208-968
Anlhracene NO ug/L 50A 10 081071171230 08/09/i]23:38 120-12-7
Benzo(a)anlhracene NO uglL 51 10 WV07A712:30 08/09117 23:38 56-55-3
Benzo(a)pylene ND upl- 500 10 081071171230 08/09/1723:38 50-32-8
BenzoRtmoranfhene NO ug/L 500 10 08107/1712:30 08109/172338 205-99-2
I BenzoRbunpoRdene NO ug/L 50D 10 08107/1712:30 08109/1723:38 191-242
Benzoggiluorenthene NO uglL 50D 10 08107/1712:30 08/09/172338 207-08-9
4 Bromophenyiphenyl ether NO ug/L 500 10 08/07/1712:30 081 2338 101-553
Butylbenzylphlhalafe NO ug/L 50.0 10 08107/171230 08/0911723:38 85-68-7
4-Chiom-3-mefhylphenol ND uglL 50.0 10 0810711712:30 08109117 23 38 59.50-7
bis(2-Chlorcellumshrelhanc ND uglL 100 10 08107/1712:30 U810911723:38 111-91-1
I WW2-Chmeefhyi)ether NO ei 50.0 10 08107/1712:30 OW0911723:38 111-44-4
S 2 Ghlorommulnalens NO umrL 50.0 10 08AT11712:30 OW0911723:38 9158]
2 Chlorephenol ND ug1L 50.0 10 OB/ni 12:30 0810911723:38 95-57-8
4 Chlomphenylphenyl ether NO ugLL 50.0 10 08107/171230 (1723:38 700S72-3
Chrysene NO ugg- 50.0 10 08112:30 OW0911723:38 218-01-9 '..
Dihenz(a,labodhracene ND uga4 50.0 10 08/071171230 0810911723:38 53-70-3
1,3-Dichlorobenzene ND ug,L 500 10 08107/1712:30 0810911723:38 541-73-1
14-Dichlorobenzene NO ugh- grab 10 08/W/fl 12:30 0810911723:38 106-46-7
3,3'-Dichlorobenzidine NO ug/L 250 10 0810711712:30 ON09/1723:38 91-94-1
24 Dichiolophenai NO .91 500 10 0810711712:30 08109/1723:38 12083-2
Diethylphlhalate NO mpL 500 10 081W/1712:30 OW091172338 84-66-2
P 2,4-Dimelhylphenol NO upl- 100 10 08107/1712:30 08109/172338 10567-9
E
-"` REPORT OF LABORATORY ANALYSIS
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Date:OW2212017 10A 2 AM wimom be will .consent of Pace Msilis,at Servees.LLC. Page 18 of 96
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ANALYTICAL RESULTS
Project: Low&Bone, Inc 1210140
Pace Project No.: 92350243
I Sample: MI&M4 Room Quench lab ID: 92350243004 Collected: 08/02/17 17:05 Received' 08103/17 16:47 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Quaff
1
625 MSSV Analytical Method:EPA625 Preparation Method:EPA 625
Dimethylphihalate NO ug1L SON 10 0810711712:30 0&091172338 131-11-3
Di-n-butylphlholate ND ugh. 50.0 10 08/07/1712:30 08/0911723:38 84-74-2
4.6 Dinilro-2-melhylphenol NO MIL 200 10 08107/171230 08109117 23 38 534-52-1
# 2.4 Dinilrophenol ND eg1L 500 10 08/07/1712:30 0810911723:38 51-28-5
2,4-Dinitrotoluene ND ug/L 50.0 10 08I07/1712:30 0810911723:38 121-14-2
2,6-Dinitrotoluene NO ug/L 500 10 08/0711712:30 0&09/1723:38 606-20-2
Di-noc(ylphlhalate NO uglL 50A 10 0810711712:30 08109117 23 38 117-84-0
1,2-Diphenylhydrazioe NO uglL 50.0 10 0810711712:30 08109117 23 38 122-66-7
bis(2-Elhy1h,xdphtha1ale NO ug/L 50.0 10 08107/1712:3008/0911723:3811781-7
Fluomothene ND ug/L 50N 10 08107/1712:30 0810911723:38 206-44-0
i Pluorene ND ugLL 500 10 08107/171230 08/0911723:38 86-73-7
Hexachlom-1,3 butadiene NO ual 500 10 Oil 12:30 0810911723:38 87-68-3
' Hexachlorobenzene NO ug/L 50N 10 0810711742:30 O&09/172338 118-74-1
3 Hexachlorocyclopentadene NO uglL 100 10 0810711712:30 08109117 23 38 77-47-4
Hexachloroethane ND had- 50.0 10 0810711712:30 081091172338 67-72-1
_ Indeno(1,2,3,cd)pyrene ND ug/L 500 10 08107/171230 0810911723:38 193-39-5
Isophorone ND ug/L 100 10 08/07/1712:30 0810911723.38 78-59-1
3&4-MCNylphenol(mBp Cresol) ND uq/L 100 10 0810711712:30 0810911723:38 15831-104
`��'u33aphlhalene NO ug/L 50.0 10 08107/1712:30 08109/1723:38 91-20-3
.--Nitrobemene NO Lad- SON 10 0810711742:30 0810911723:38 98-95-3
t 2-shemphenol ND uglL 50N 10 08107117 12 30 08109/17 23 38 88-75-5
j 4Numphenol NO ug1L 500 10 0810711712:30 0809172338 100-02-7
- N-Nitr05odimethylamine ND ug1L 50.0 10 08107/1712:30 08/0914723:38 62-75-9
14-1,11tr0sodi mpmpylemine ND ug/L 50.0 10 0810711712:30 0810911723:38 621-64-7
j N-Nilrosodlphenytimine ND ng1L 100 10 08107/1712:30 08/0911723:38 86-30-6
? 2,70aalbis(1-chloropropanum NO ug/L 500 10 08107/1712:30 O&0911723:38 10860-1
1 Pentachrimphenol NO ug/L 1W 10 0810711712:30 08/09/1723:38 87-86-5
Phenomenons NO uglL SON 10 081071171230 08/091172338 8501 8 '.l Phen01 ND ug/L 50.0 10 0810711712:30 08/09/172338 108-952
Pyrene NO ug/L 50.0 10 08107/171230 0&0911723:38 129-00-0
1,2,4-Tdchlorobenzene ND ug1L 500 10 08107/171230 08109/1723:38 12082-1
2,4,6-Trehlomphenol NO ug/L 100 10 08/0711712:30 08/0911723:38 88-06-2
Sunngates
Nitrobenzene-d5(S) 0 % 10-120 10 08/071171230 0810911723:38 4165-60-0 D3,54
2-Ommbiphenyl(8) 0 % 15-120 10 0810711712:30 08109117 23 38 321-6" S4
Terphenyl-014(8) 0 % 11-131 10 08/0711712:30 08109117 23 38 1718-51-0 S4
3 Ehan0l d6(S) 0 % 10-120 10 0810711712:30 08MOM72338 13127-883 S4
2-Fluorophenol(S) 0 % 10-120 10 08107/1712:30 0&09/1723:38 367-12-4 84
2,4,6-Tribmmophenol(S) 0 % 10-137 10 08107/1712,30 081091172338 118-796 54
l 624 Volatile Organics Armylicai Method:EPA624
Acrolein NO ug/L 5A 1 081O&1723:59 107-02-8 Ll
Actylonllrile NO uglL SON 1 0810811723:69 107-13-1
Benzene NO rqA- 2.0 1 0810&172359 71-43-2
i 6romodichloromethane NO uglL 2.0 1 0&08(172359 75274
j 8rom0form ND ML 2.0 1 0810811723:59 75-25-2
i Bmmomelhane NO ug/L 20 1 0810811723:59 74-83-9
s' S
- REPORT OF LABORATORY ANALYSIS
mis repod shall not ee mproduced,except in full.
Date:O&22/201710:12 AM without the—tueo consent of Pace Analytical Service¢,LLC. Page 19 of 96
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Pace Analytical Services,LEG
aceAnajfytical a 2225 Riverside ur
Asheville,NC 2e8e4
sespecabraose
(82d254-7176
I
ANALYTICAL RESULTS
Project: Low&Sonar Inc1210140
- Pace Project No, 92350243
! Sample: Ml&Me Room Quench Lab ID: 92350243004 Collected: 0810211717:05 Received: 0 810311 7 16 47 Matrix:Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Quel
624 Volatile Organics Analytical Method:EPA624
3 Carbon tetrachloride NO ug/L 2S 1 0810811723:50 56-23-5
Chlorobenzene ND ug/L 2.0 1 08108117 23 59 108-90-7
j Chloroethane NO upl- 2.0 1 08/08/172359 75-00-3
-1 Chloroform NO uglt. 20 1 081081172359 67-66-3
Chloromethane NO ug/L 2.0 1 08/08i1723'59 74-87-3
1 Dibromochloromethane NO ug/L 2.0 1 0810811723:59 124-481
E 1,2-Dichiorobenzene NO tall 2S 1 08/0811723:59 95-50-1
1,3-Dichlorabenzene ND ug& 2D 1 0810811723:59 541-931
1,4-Dichlorabenzene ND ug/1. 20 1 garnet 72359 106-46-7
- 1,1-Dichloroathane NO un/L 20 1 08108117 23 59 75-34-3
1,2-Dichloroethans NO ug/L 20 1 0810&1723:59 107-05-2
1,1-Dichloroethens NO "go- 2.0 1 08/08/1723:59 75-354
i cis-1,2-Didtloroethene ND mull. 2S 1 0810811723:59 156-59-2
Trans-1,2-Dichiomelhene NO ugll. 2S 1 08/0811723:59 15660-5
1,2-Dishioropropane ND ug/L 2.0 1 0810811723:59 78-87-5
' cis-1,3-Dichloropropene ND ug/L 20 1 0810811723'59 10061-01-5
trans-1,3DichlompmfmrA NO ug1L 20 1 0810&1723:59 10061-02-6
? Ethylbemnom ND un1L 20 1 0810811723:59 10041-4
')ethylene Chlaride NO un1L 2.0 1 08/081723:59 75-09-2
- (,,1.2,2-Torachloroethane NO ug/L 2.0 1 08/0&1723:69 79-34-5
Tionchiomethene ND ug/L 2A 1 0810811723:59 127-18-4
Toluene NO unit- 2.0 1 0810W4723:69 108-88-3
1,1.1-Trichloroeihane ND ug/L 2.0 1 0810811723:59 71-55-6
1,1,2-Trichloroeihane NO ug/L 20 1 08ID&172359 7900-5
_ Trichloroethene NO ago- 20 1 0&081172359 7901-6
Trichiorogoaromethane NO ug/L 2.0 1 08/0&1723:59 75-69-4 '..
Vinyl Chloride NO unit- 20 1 OW08/1723:59 75-01-4
Surrogates
4 DramoBuorobenzene(S) 109 % 70-130 1 08/0811723:59 460-00-4
Toluene-d8(S) 110 % 70-130 1 08108117 23'59 2037-26-5
1,2 Dichlomethane d4(8) 97 % 70-130 1 08108/17 23 59 17060 O7-0 '..
2540C Total Dissolved Solids Analytical Method'SM 2540C '..
Total Dissolved Solids NO mg/L 25S 1 0810811709,38
2540D Trial Suspended Solids Analytical Method:SM 2540D
Total Suspended Solids ND mg1L 2.5 1 0810811717:07
Total Nitrogen Calculation Analytical Method:TKN+NO3+NO2 Calculation
3 Total Nitrogen 68.6 ni 0.12 1 08/0911718'if
350.1 Arguments Analytical Method EPA350.11993 Rev 2.0
Niorgen,Ammonia 3.7 add- 0.10 1 0810911702:52 766441-7
351.2 Total Kjeldahl Nitrogen Analytical Method.EPA 351.2
- Nitrogen Kjeldahl.Total 68.5 mg/L 5D 10 08109117 4732 7727-37-9
i
"f REPORT OF LABORATORY ANALYSIS
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E
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_ Pace Anatyticdl ServiOee,The
i
aeeAnalytleai 2225 Rivers28ich,04
nuwp' xum Nshe(826)2C26804
(82a)254-]P6
I
ANALYTICAL RESULTS
i
I
Project Lmv&Bomar Inc 1210140
Pace Project No: 92350243
Sample: MI&M4 Room Quench Lab ID: 92350243004 Collected: 0810211717:05 Received: 08103/4716:47 Matrix: Water
' Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Goal
i
353.2 Nitrogen,NO21NO3 pres. AnalNical Mother:EPA 353.2
Nitrogen.NO2 plus NO3 0.059 mdd- 0,020 1 OW091171211 Mt
365.1 Phosphorus,Total Analytical Method;EPA365.1
aPhosphorus NO mill 0050 1 08/10117 06 32 7723-14"0
i 5220D COD Analytical Methotl;SM 5220D
5 Chemical Oxygen Demand 1150 mill 25.0 1 08101117 18:41
3
Sample: MS Room Quench Lab ID: 92350243005 Collected: 08IO2/1718:10 Received; 08103/1716:47 Matrix:Water
Parameters Results Units Report That OF Prepared Analyzed CAS No. Qual
HEM,Oil add Csrease Analytical Method:EPA 1664E
Oil and Grease NO mill 5.0 1 08/1711705:10
_ 200.7 MET POP Analytical Method:EPA yell Preparation Method:EPA 200]
Antimony ND hill 5.0 1 0BAT117 2150 081081172141 7440360
j sseme NO ug/L 10-0 1 08/0711721:50 08/08/1721:41 744038-2
Beryllium NO ug/l 10 1 081O1/1121:50 081081172141 7440-41-7
Cadmium NO uglL 10 1 0810711721,50 08/08/17 2141 7440-439
Chromium NO ugA- 50 1 081071172LM OS/0811]21:41 7440-47-3
- Copper 44.1 hill 5'0 1 08107/1721:50 081081172141 7440-50-8
Lead ND Trill SO 1 08107/1721;50 0810811721:41 7439-92-1
Molybdenum NO uglL SO 1 0810711721:60 08108/1721:41 7439-98-7
Nickel NO mill- SO 1 08107/1721:50 081081172141 7440-02-0
Selenium ND ug/L 10.0 1 08107/1721:50 0810811721:41 ]]82-49-2
Silver NO ugd- 5.0 1 08107/172150 08/081172141 7440-22-4
Thallum ND mid. 1OO 1 08107/172150 0W1811719:25 7440-28-0
Hardness.Total(SM 2340B) 2220 ugll 662 1 08107/1]2150 08108/172141
j Zinc 85.3 ugh- 10) 1 0810]I1]2150 081081172141 7440"66-6
245.1 Mercury Analytical Method:EPA 245.1 Preparation Method:EPA 245A
Mercury ND uglL 0,20 1 0810811701:20 0810911706:36 7439-97-6 '..
625 MSSV Analytical Method;EPA 625 Preparation Method:EPA 625 '..
3 Acenaphthene NO u91L 500 10 0810711712:30 Oa/1 Oil 7 OOT)6 83-32-9 '..
AcenapMhylene NO uglL rich 10 08,A)l 12:30 0811 Oil 700:06 208-96-8
Anthmoene NO hill 50.0 10 08107/1712:30 08/1011700,06 120-12-7
Benzo(a)anlhracene ND ug/L 50.0 10 08107/1712:30 081101170006 56-55-3 '..
Benzc(a)pyrene ND upt- 50.0 10 08107/1712;30 08I1011]00,06 50-32-8
Benzo(b)Ouoraoften. NO ug1L 50.0 10 08107/171230 081101II 00:06 205-99-2 '..
-_ Benzo(g,h,i)perylene ND ugh- 50.0 10 08107/171230 0811011700:06 191-24-2
Beizo(k)Brchanfhene ND ug1L 50.0 10 08/0]I1]12,30 08/10117 Ol 207-08-9
4-8romophenyiphenyl ether NO uglL 500 10 0810711712:30 0811011700:06 101-55-3
Butylbewylptimalate NO uglL 50.0 10 08/0711712:30 08110/170006 85684
i
3
REPORT OF LABORATORY ANALYSIS
This reform shaft not be reproduced,except in On,
Date:081221201710:12 AM meow the warren consent of Paw Analytical Srwi a,LLC. Page 21 of 96
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Pace Analytfeai Smcfees,LLC
_ aceAllaly ical a 2225 R"erstle 0,
Ash.11,NG 28804
(828)2U-7170
3
ANALYTICAL RESULTS
E Project: Lmv&Sonar Inc 1210140
Pace Project No.: 92350243
l Sample: MS Room Quench Lab ID: 92350243005 Collected 0810211718:10 Received: 0810 311 7 16:47 Matrix: Water
# Parameters Gel Units Report Limit OF Prepared Analyzed CAS No. Qual
] 625 al Analytical Method:EPA 625 Preparation Method.EPA 625
} 4 Chlool onedulphenol NO u911. 50.0 10 08107/1712:30 08/1 OIL 700'.06 59-50-7
I bIs(2-Chloreemoxy)melhane NO uglL 100 10 081071171230 GOO G1700,06 111-91-1
t bis(2-Chloroethyl)ether NO upt- 50-0 10 08107I171230 081101170006 1t144-4
2-Chloronaphlhalene NO ugll 60.0 10 OB1W/1712:30 0811011700:06 91-58-7
3 2Chlorophenol ND ug/l 50.0 10 0810711712:30 08/40/1700:06 95-57-8
4 Chlomphenylphenyl ether NO ug1L 500 10 08/071171230 0811011700:06 709572-3
Chrymme NO ug/L 500 10 08/0711712,39 0811011700:06 218-01-9
DANnz(a,h)anNrre ne NO ug1L 500 10 0810711712:30 081101170006 53-703
1,3-Dichlombenzene NO ug/L 50.0 10 0810714712:30 08/10I1700:06 541-73-1
1A Dichlorobenzene NO uglL 50.0 10 0810711712:30 0811011700,06 106-46-7
3,3'-Dichlorobenzidine NO uglL 250 10 08107/1712:30 08/1011700:06 91-94-1
j 2,4-Dichlmophenol NO uglL 50.0 10 OB/OM 12:3008/1Off 7 00,06 120 83-2
Dielhylphlhalate ND upt. 50.0 10 08107/1712:30 08110ft 700,06 84-66-2
#` 2,4DImethylphenol ND ugh, 100 10 08107117 12 30 08/1011700:06 105-67-9
}_ Oimethylphlhalate ND ti ll 50.0 10 08/0711712:30 0811011700:06 131-11-3
Di-n-butylphlhalate NO ul 50D 10 0810711712:30 0811011700:0 84-74-2
4,5Dinilro-2methylphenol NO ug1L 209 10 0810711712:30 08110117 MOO 634-52-1
2,4-Dinilrophenol NO uglL 500 10 0810711712:30 0811011700:06 51-28-5
_. .�7,4 Dinitroteluene NO uglL 50.010 0810711712:3p 0811011700:06 121-14-2
d,6-DinilroloWene NO ug1L 500 10 0810711712:30 08/10/170006 606-20-2
j OLmoclylphlhilate NO ell 50D 10 08107/1712:30 0811 OIL 700.06 117-84-0
1,2-Diphenylhydrazine NO ugd- 500 10 08107/1712:30 08I10O 70006 122-66-7
3 bis(2-Elhy1haxyl)phlhaete NO uglL 50.0 10 08107/1712:30 08/1011700:06 117-81-7
Fluoranlhene ND fol 500 10 081071171230 08/10/17 GOES 20644-0
H mone ND ug/L 50.0 10 08107/1712:30 0811011700,06 66-73-7
Hexachloro-1.3 buladene ND uglL 50.0 10 08/071171230 0811011700:06 87-68-3
- Hexachhhobenaene NO ug/L 50D 10 081071171230 08/1011700:06 118-74-1
HexachlorocyclopeMadiene NO ug/L 100 10 08107/1712:30 08/1011700:06 7747-4
Hexachloroelhane NO uglL 50A 10 08107/1712:30 0811 Off 700:06 67-72-1
7 Indeno(1,2,3-cOpyrene ND ug/L 500 10 0810711712:30 081101170006 193-39-5
17 Isophorone NO Odd 100 10 08/0711712:30 0811011700:08 78-59-1
3&4-Melhylpheool(m&p Cresol) NO ug1L I 10 081071171230 081101170006 15831-104
Naphthalene NO u911- 500 10 08107/1712:30 06110H 700:06 91-203 '..
Nineturrene NO red- 500 10 08107/171230 0811011700:06 98-953 '..
d 2-Nietphenol NO uglL 500 10 0810711712:30 0811011700,06 88-755
! 4-Nitephenol NO ug1L 500 10 08107/1712:30 08I1 Oil 70006 10002-7 l
N Nilrosoduchtrylamine NO ug1L 50D 10 08107/1712:30 0811011700:0'0 62-75-9 1,
N Nitmse di n-pmpylamine NO ug/L 500 10 08107/1712:30 08110117 00 06 621-64-7
N-Nilmsodiphenylamine NO uglL 100 40 08107/1712:30 Oot GO700,06 86-306 1.
2.2-0xybis(1-chloropropane) NO milk 50.0 10 0810711712:30 08/10/1700:06 108-601 1.
Pardethlorophenol NO cut- 100 10 081071171230 0811011700,06 87-86-5
Prommuhrene ND ug/L 60.0 10 08/07/1712:30 08110/1700:06 85-01-8
Phenol ND mfll 50.0 10 08/07/1712 30 08/10117 00:05 108-95 2 1.
S Pyrene ND ug/L 50.0 10 0810711712.30 08/10/170005 129-000
1,2,4-T rhlombenzene ND ugll 50.0 10 0810711712:30 08110117 00 06 120-82-1
2,4,6drichlorophemn NO til 100 10 0810711712:30 08110117 00 06 8806-2
REPORT OF LABORATORY ANALYSIS
This report shall not in,monstrous,except in full,
- Date:081221201719:12AM where the wooden consent of Pace Anelylloal$B,Ts,TLC, Page 22 of 0

t Pace Analytical Services,LLb
` 2225 a,NC 28 04
3 aceAnalyticai be(82 NC -7176
I -" nfvxiavn ta2a)254„]6
�3
ANALYTICAL RESULTS
Project: Low&eonar Inc 1210140
Pace Project No.: 92350243
Sample: M5 Room Quench Lab ID: 92350243005 Collected: 0810211718:10 Received: 08/03117 16:47 Matrix:Water
jParameters Results Units Report Limit OF Prepared Analyzed CAS No, Coal
625 MSSV Analytical Moment EPA 625 Preparation Method:EPA 625
t Surrogates
Nitrobenzene-d5(S) 0 % 10-120 10 08107/1712:30 081101170006 4165-60-0 DTS4
2-Pluombiphenyl(S) - 0 % 15120 10 08107/1712:30 (SMO1700:06 321-60-8 54
Terphenyl dl4(S) 0 % 11-131 10 08107/171230 0811011700:06 1718-51-0 54
Phenol-d6(S) 0 % fill 10 0810]/t]12:30 0811011700:06 1312788-3 S4
2-Fluorophenol(8) 0 % 10120 10 0810711712:30 0811011700:06 367-12-4 84
2,4S-Tribromopheal(S) 0 % 10-137 10 08107/1712:30 08/10ff 7(005 118-79-6 S4
i
624 Volatile Organics Analytical Method:EPA 624
Acamein NO igh- 5.0 1 0W0911700:17 107-02-8 IT
Acrylooitmo NO u94 50.0 1 0810911700'17 107-13-1
Benzene NO ug/L 2.0 1 0810911700:17 71-43-2
Bromodichloromelhane NO bill. 20 1 08109/1700:17 75-27-4
Bromoform NO ug1L 20 1 08109/17 00:17 75-25-2
Bromomelhane NO high, 2) 1 0810911700:17 74-83-9
Carbon tetrachloride ND uglL 2.0 1 08/09/170017 56-23-5
Chloomenzene NO ug1L 2.0 1 Oonthly 00:17 108-90-7
( Chloroethane NO ug/L 2.0 1 0810911700:17 75-00-3
'r=filorotorm NO ug& 2.0 1 0810911700:17 67-663
>9hloromethane NO bill. 2.0 1 0810911700:17 74.87-3
Din
o
no fulmomelhane NO uglL 20 1 plural 124-48-i
1.2-Dichlorobenzene NO ug1L 20 1 0810911700:17 9550-1
1,bDichlombeniene NO ugiL 20 1 OW0911700:17 541-73-1
1.4-11chlorobenzene NO bg/L 2.0 1 08109/1700:17 106-46-7
1,1-Oichtoroelhene NO ugll- 2.0 1 08/0911700:17 75-34-3
- 1,2-Dichtoroethane NO ug/L 2.0 1 08/09/1700:it 107-06-2
i 1.1-DicMomethene NO uglL 2.0 1 0810911700:17 75-354
cs-1,2-Dichloroethene NO ugl, 2.0 1 0810911]00:1] 156-59-2
trans-12-Dichlmoethene NO bill. 20 1 0810911700:17 156-60-5
1,2-Dichleaclagane NO bill. 20 1 08109/1700:17 78-87-5
f cis-1,&Dichlmopropene NO ug/L 20 1 0810911700:17 10061-01-5
(3 Var l,3-Men...proper. NO bull. 2.0 1 08109/1700:17 10061-02-6
t Emyltenzene NO muL 2.0 1 0810911700:17 100-41-4
{ Methylene Chloride NO bg1L 2.0 1 0810911700:17 7509-2 '..
i LL2,2-Tebachlemethane NO bill 2.0 1 08/0911700'17 79-34-5
Tenschloroethene NO ugh, 2.0 1 OW0911700:17 127-184
j Toluene NO uglL 20 1 0810911700:17 108-BS3
7 1,1,1-Tnchtoroethan. NO ugll. 20 1 08/09/1700:17 71-56-6
1,1,2-Trichlomethane NO ti lL 20 1 OW0911700"17 7900-5
3 Trichtomethene NO uglL 20 1 0810911700,17 79-01-6
s Trichlorofluoromelhane NO ughL 2.0 1 handful 00 17 75-694
3 Unyl chloride NO ug/L 2.0 1 08/0911700:47 7501A
I Surrogates
4-6romofluorobenzene(S) 107 Ti 70-130 1 08/0911700:17 460004
i Toluene-do(8) 114 % 70-130 1 0810911700:17 2037-26-5
1,2-Dichloroethane-d4(S) 94 % 70-130 1 08/09/1700:17 1706007-0
i
-"' REPORT OF LABORATORY ANALYSIS
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' Date:081221201710:12AM without us winners consentnl Pace Analylical SeMces,LLG Page 23 of 96
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Pace Analytical Services,LLC
Wereide Rr.
aceAna(ytical® 2225 R
Ashe,ens,NC 28804
(I 'aamse. [phone]
4
t
ANALYTICAL RESULTS
Project: LmvB Bona. Inc 1210140
Pace Project No.: 92350243
( Sample: M5 Room Quench Lab ID: 92360243006 Collected 0810211718:10 Received: 08103/1716,47 Matrix:Water
€ Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Carl
2540C Total Dissolved Solitls Anal)4ical Mother:SM 25400
j Total Dissolved Solids NO "s- 25.0 1 08I08/170938
i 26400 Total Suspended Solids Analytical Method:SM 2540D
j
Total Suspentletl Solitls ND mglL 2S 1 0810811717:08
Total Nitrogen Calculation Analytical Method:TKN+1,03+1,102 Calculation
Total Nitrogen 24.3 rap- 0.12 1 0810911718:11
360.1 Ammonia Analytical Method:EPA 350.11993 Rev 2.0
Nitrogen,Ammonia 3.3 mglL 0A0 1 0810911702:53 766441-7
351.2 Total Kjeldahl Nitrogen Analylicai Method:EPA 351.2
Nitrogen,Kleldahl,Total 24.2 mg/L 1.0 2 0810911717:33 7727-37-9
j 353,2 Nitrogen,NO2/NO3 pass. Analytcal Method:EPA 353.2
Nitrogen,NO2 plus NO3 0.11 mgA- 0020 1 OW0911712:14
i
-365.1 Phosphorus,Total Analytical Method:EPA 365A
phosphorus ND mg/L OT50 1 0811011706:36 7723-14-0
52200 COD Analytical Method SM 5220D
I Chemical Oxygen Demand 422 calk 250 1 08/0711718:41
] Sample: Boiler Condensate Labib: 92360243006 Collected: 08102/1713,00 Received: OW03117 16 47 Matrix: Water
Parameters Results Units Report limit OF Prepared Analyzetl CAS No. Oual
HEM,Oil and Grease Analytical Method:EPA 16646
9 Oil and Grease NO mg/L 50 1 08/17117 05 10
7 200.7 MET ICE Analytical Method:EPA 2W.7 Preparation Method EPA20C7
ji
3 Antimony NO ug1L Co 1 0810711721:50 08/08/17 2 1:44 7440-36-0
] Arsenic NO ug/L 10.0 1 0810711721'50 081081172144 7440-38-2
I Beryllium NO ug/L id / 0810711721:50 081081172144 7440-41-7
Cadmium ND ug11. 1A 1 0810711721:50 08108117 21 44 7440-43-9 '..
Chromium NO ug/L 50 1 (AW07/1721:50 08/08/172144 7440-47-3
Copper 38.4 uglL &0 1 08107/1721:50 08108Ii 72144 7440-50 8
1 Lead ND ugp- 5d 1 08/07/1721:50 08108/1721:44 7439-92-1
Molybdenum ND ug/L 5.0 1 0810711721,50 08108117 24 44 7439-987
Nickel NO end- 5.0 1 08107/1721:50 08108/17 21 44 7440-02-0
Selenium NO uglL 10.0 1 0810711721:50 08/081172144 7782-49-2
Silver NO ug/L 5.0 1 0810711721:50 08108/1721'44 7440-22-4
Thallium NO add- 10.0 1 0810711721'50 08118117 19 54 7440-280
Hardness,Total(SM 2340H) NO ug/L 662 1 08I07/1721:50 08/081172144
s
REPORTOP LABORATORY ANALYSIS
This reld shall not be repmtluceq except In full,
Data 08/22/201710:12 AM without me wrinen consent of Pace Analytcal services,uA Page 24 o196
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Pace Analytical Servlces,LLC
i e 2225 Rlverelde Or.
aceAaalytical ASM1eville,NC 28804
o,,ros`a c ceal [phone]
3
j
ANALYTICAL RESULTS
S Project: Low&Sonar Inc 1210140
1 Paw Project No.' 92350243
i
Sample: Boller Condensate Lab ID; 92350243006 Collected 0810211713:00 Received: 0810311716:41 Matrix;Water
Parameters Results Units Report limit DF Prepared Analyzed CAS No. Coal
j
200.7 MET ICP Analytical Method:EPA 2007 Preparation Method:EPA 2007
Zinc 13.4 ugA- 10.0 1 08107/17 21:50 08/08117 2144 7440666
t
245.1 Mercury Analytical Method:EPA245-1 Preparation Method:ERA245A
:3 Mercury NO ug/L 0.20 1 081081170120 0810911706:39 7439-99-6
625 Al Analytical Method:EPA625 Preparation Method:EPA625
Acenaphlhen , NO u91L 5.0 1 0810711712:30 OW0811705:43 83-32-9
i Awnaphlhylene ND u9ll. 5.0 1 0810711712:30 0810811705:43 208-958
Anlhmwne NO opt. 50 1 0810711712:30 08108117 05 43 120-12-7
Bmeo(a)anlhracene NO ug111 50 1 0810711712:30 0810811705:43 5655-3
Benzo(ajpyrene NO ug/L 50 1 08107/171230 081081Tl 05:43 50-32-8
BenamInflumanthene NO ugh. 5d 1 08107/1712:30 0pplet 705:43 205-99-2
Benzo(g,h.i)peonene NO ugLL 5.0 1 08107/1712:30 08/0811705:43 191-24-2
3 Benzogollumandene ND ug1L 5.0 1 0810711712:30 0810811705.43 20708-9
_ 4 BromOphenylphems ether NO u /L. 5.0 1 0810711712:30 081081170543 101-55-3
Butylbenzylphlhalate, NO mill- 50 1 08107/1712:30 0810811705:43 8568-7
- 4Chlorc-3 methy;phenel ND mill- 50 1 08107/1712:30 08/08/1705'43 59-50-1
.:fie(2-CNoroelhoxy)melhene NO ugA, 10-0 1 08107/1712:30 08108/1705:43 111-91-1
- Ns(2 CMomelhyl)ether NO ug/L 5A 1 0810711712:30 081080705:43 111 44-4
'2-Chloronaphthalene NO off- 5d 1 0810711712:30 08108/1705:43 91-58-1
2-Chloophouse NO ug1L 5.0 1 08/07/1712:30 0810W1705:43 95-57-8
4 Chlorophenyiphenyl ether NO ug1L 5.0 1 0810711712:30 0810W1705:43 1005-72-3
Chrysene NO ugA- 5d 1 0810711712:30 081081170543 218-01-9
Dibenz(a,h)anlhracene NO uglL 50 1 08/07/1712:30 0810811705:43 53-70-3
1,3 Dichlorobenzene NO ug/L 50 1 081071171230 08/ON1705:43 541-73-1
L4-Otchlorobenzene NO mill- 50 1 08(07/111230 0810811705'43 106-46-7
3,3-Dichlmohenzimne NO ug/L 25.0 1 0810711712:30 08108/110543 91-94-1
j 2,4-Dichlomphenol NO up- 5d 1 08107/1712:30 08108/1705'43 120-83-2
Olethylphthalate NO ugh- 5P 1 0810711712:30 08/08/1705A3 84-66-2
2,4-Dimethylphenol NO u91L 10.0 1 0810711712,30 0810811705:43 105-67-9
Dimethylphthalate NO u91 5.0 1 08101117 12:30 0810811705:43 131-11-3
Di-n-butylphlhalate NO ago. 50 1 O1/07117 12:30 08108117 05 43 84-74-2
4,6-Dinit.2-methylphenol NO uglL 200 1 08107/1712:30 0810811706:43 534-52-1
2,4-Dinilmighenol NO upi- 500 1 08/0711712:30 O&O811705'43 51-28-5
2,4 Dlndmoluene NO ug/L 5.0 1 08107/1712:30 08/08/170543 121-14-2
1 2,6(grin cloluene NO ugh- 5d 1 08/0711712:30 08108/1705'43 606-20 2
Of moctylphNalate NO ug/L 50 1 08107/1712:30 08/08/1705'43 117-84-0
1,24notteny1hydrazine NO ug11- 6d 1 08107117 12:30 0810811705:43 122-657
bis(2-EthylhexyI)phthdate NO opt- 5P 1 08107/1712:30 08/08117 G543 117-81-2
Fimnalsome, NO upl. 5N 1 08107/1712:30 0810543 20644-0
f Fluorene ND ugIL 5.0 1 08107/1712:30 0131,01705'43 8673-7
Hexachlm,L3-butadiene NO mill, 50 1 08/0711712:30 OW081170543 87-68-3
I Hexachlorobenzene NO uglL 5.0 1 08107/1712,30 081081170543 118-74-1
HexachloneWdopenladiene ND ug1L 10.0 1 0810711712:30 08108/1705:43 77-47A
1 Hexachforoelhane NO ug1L 5.0 1 08/07/1712:30 08108(1]05:43 61-22-1
mdeno(1,2,3-cdjpyrene NO mill- 50 1 08/W/1712:30 01110811705:43 193-39-5
)
-` REPORT OF LABORATORY ANALYSIS
Tors repen shall not oe reprodmeo,e. u m ma,
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Project LowB eonar Inc 1210140
Pace Project No- 92350243
Sample: Boiler Condensate Lab ID: 92350243006 Collected: 0810211713:00 Received: OW0311716'47 Matrix:Water
Parameters Results Units Report Limp OF Prepared Analyzed CAS No. Oual
,3 625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
i Isophorone ND ug/L 10.0 1 0810711712:30 0810811705:43 78-59-1
384-Melhylptlenol(m&p Cresol) ND uglL 10.0 1 08107/1712:30 081081170543 1583110-4
Naphthalene ND ug/L 5.0 1 08107/1712:30 08/08/170543 91-20-3
Nitrobenzene ND ug/L 50 1 08107/1712:30 08108/1705:43 98-953
-� 2-Nitrophenol ND Ug/L SO 1 0810711712:30 08/0811705:43 88-755
4-Nitrophenol NO uglL 50.0 1 08/071171230 081081170543 100-02-7
N-Nibosodimelhylamine NO hi SP 1 0810711712:30 08/0811701 62-75-9
- N-Nittvso-all n-propylamine ND ug/L 5.0 1 08/07/1712:30 0810811705,43 621-64-7
N-Nitroiodiphenylamine ND uglL 10.0 1 08107/1712:30 08/08I1705:43 86-30.6
_ 2,2'-01 c,hloropopane) ND ug/L 50 1 08107/1712:30 081OW170543 108-60-1
Pentachlorophenol ND ug/L 100 1 08/07/1712:30 08(0811705:43 87-86-5
1 Phenanthrene NO us/1- fro 1 081071171230 08/08/170543 85-01-8
7� Phenol NO ui SO 1 08/0711712:30 081081170543 108-952
i Pyrene NO 1 5.0 1 0810711712:30 08/08/17 05 43 12900-0
- T24-Tdchlorobenzene ND ri 5.0 1 081071171230 08/0811705:43 12082-1
- 2,4,6-Trichloophenol ND ug/L 10.0 1 0810711712:30 OW0811705'43 88-06-2
Surrogates
141trobereene-d5(S) 73 % 10-120 1 0810711712:30 08/081170543 416560-0
yHoorobiphenyl(S) 76 % 15-120 1 08fi 12:30 0810811705:43 321-60-8
- 5 ophenyl-014(8) 86 % 11-131 1 0810711712,30 0810811705:43 1718-51-0
Phenold6(S) 19 % 10-120 1 0810711712:30 081081170543 13127-883
2-Fluomphenol(S) 22 % 10-120 1 0810711712:30 08/0811705:43 367-12-4
2.4,6-Tdbromaphenol(ST 43 % 10-137 1 0810711712:30 OW0811705:43 118-79-6
624 Volatile Organics Analytical Method EPA624
Acrolein ND ug/L 50 1 0810911700:35 107-02-8 Li
Acrylonitriie ND uq/L 500 1 OW091170035 107-131
Benzene ND ug1L 2.0 1 OW09/170035 7143-2
Bromodichloromethane NO uglL 20 1 08/09117 00 35 75-27-4
Bromoform NO uglL 2.0 1 08/0911700,35 7525-2
Bromomethane NO ug/L 2.0 1 081091170035 74-839
Carbon tetrachloride NO ugll- 20 1 0810911700:35 5623-5
Chtorobenzens ND ug/L 2D 1 OW0911700:35 108-90-7
- Chi oroethere ND ug/L 20 1 08/09/170035 75-003
Chloroform NO, ug1L 20 1 08109117 00 35 67-66-3
Chloromelhane NO u91L 2.0 1 08108/170035 74-87-3
Dibromochloromethane NO ug1L 2.0 1 08109/170035 12448-1
1,2-Dichlorobenzenc ND uglL 2P 1 081091170035 95-50-1
j 1,3-Dichiorobenzene NO ug/L 2P 1 0810911700:35 1
1,4-Dichlorobenzene NO ogg- 20 1 OW0911700'35 106-467
1,1-DirbIsoelhane ND ug/L 2.0 1 0810911700:35 7534-3
1,2-Dichloroethere ND ugh- 20 1 ON0911700:35 107-06-2
Li-Dichloroethene ND Ug1L 20 1 08109/1700:35 75-35-4
cis-1,2-Dichtoroethene NO ug/L 2.0 1 08/09117 0035 156-59-2
tans 1,2-Dichloroa hene NO ug/L 2,0 1 08109M7 00 35 156-60-5
1,2-Dichlompropane NO ui 2) 1 0810911700:35 78 87-5 '..
- cis-1,3-Dichleropropene NO ug/L 2.0 1 0810911700:35 10061-01-5 '..
t
REPORT OF LABORATORY ANALYSIS '
This most shall not be reproduced,except is full.
Date:08122/2 01 7 10:12AM wimom the wdase consenl of Pace Analytical SmY.ces,LLC Page 26 of 96
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Pace Analytical Services,LLC
i aceAnalyticals Rivera ide
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1
1
i
ANALYTICAL RESULTS
Project: Low&Bantu Inc 1210140
Pace Project No.: 92350243
Sample: Boller Condensate LabiD: 92350243006 Collected: 0810211713:00 Received: 0 /0N17I6:47 Matrix:Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Coal
s
624 Volatile Organics Analytical Method:EPA 624
j lra r-1,3-Oichloropropene NO ug1L 2.0 1 0810911700:35 1006102-6
tj Ethylbenzene NO ug/L 2.0 1 0810911700:35 100-41-4
3 Methylene Chloride ND ug1L 2.0 1 0810911700:35 75-09-2
l 112,2-1fielrachloroethane ND min- 20 1 08109117 00 35 79-34-5
Tetrachloroe(herle ND Ug/L 2.0 1 08109117 00 35 127-18-4
j Toluene ND ugl 2A 1 08109117 0035 108883
I 1.1,1-Trichlomethane NO ug/L 2A 1 08/09/1700.35 71-55-6
1,1,2-Tdchloroethane ND ug/L 2.0 1 081091170035 7900-5
Turtilamethene NO ug1L 2.0 1 0810911700:36 79-016
Tochlouo0ooromethane ND ug1L 2.0 1 08/0911700:35 75-69-4
Vinyl chloride ND ug/L 2.0 1 08109I1700:35 75-01-4
Surrogates
4 BromoOuorobenzene(S) IN % 70-130 1 0810911700:35 460-00-4
't Toluene-d8(S) 113 % 70-130 1 OW091170035 2037-26-5
1.2-Dichimoethano&(8) 81 % 70-130 1 08/091170035 17060-07-0
1
2540C Total Dissolved Solids Analytical Method:SM 2540C
Total Dissolved Solids NO mg/L 25R 1 0810811709:39
,S401)Total Suspended Solids Analytical Method.SM 25400
Total Suspended Solids 4.2 mg/L 2.5 1 0810811717:08
Total Nitrogen Calculation Analytical Method:TKN+NO3+NO2 Calculation
Total Nitrogen 1.7 mga- 0,12 1 08109/17 18 11
# 350.1 Ammonia Analytical Method:EPA 350.11993 Rev 2.0
J
s Nitrogen,Ammonia NO ri51L 0,10 1 08109/170255 ]664-41-]
j
351.2 Total Kjeltlahl Nitrogen Analytical Method EPA 351.2
Nitrogen.Kjeltlahl.Total 1.7 mg1L (50 1 08/09117 17:00 ]]2]-3]-9
353.2 Nitrogen,N021NO3 puts. Analytical Method:EPA 353.2
Nitrogen,NO2 plus NO3 ND mglL 0,020 1 0810911712:15
365.1 Phosphorus,Total Analytical Method:EPA 365.1
i
Phosphorus NO mg/L 0.050 1 08I10Ii]06:3] ]]23-04-0
5220D COD Analytical Method:SM 5220D
Chemical Oxygen Demantl NO MAL 25.0 1 08107/171841
1
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i
REPORT OF LABORATORY ANALYSIS
Thia report shall not ca reproduced,except in full,
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Pace Analytical Services,LLC
aceAnalytical a 2225 Rivers de Or
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ANALYTICAL RESULTS
I
3 Project: Lmv&Boner inc 1210140
Pace Project No.: 92350243
Sample: Basement Groundwater Lab ID: 92350243007 Collected: 08102117 15:30 Recanted: 08103/17 16:47 Main, Water
Parameters Results Units Repan Limit DF Prepared Analyzed CAS No, Dual
HEM, in and Grease Analytical Method:EPA 1664E
Oil and Grease NO moll- 5.0 1 08117/1705:11
I
ZOOS MET ICP Analytical Melhotl:EPA 200.7 Preparation Method:EPA 2007
_ Antimony NO uqA- 5.0 1 081071172150 081081172147 7440-W-0
Arsenic NO ugiL 10'0 1 0810711724:50 08/0811721:47 7440-38-2
Beryllium NO m/L 1.0 1 08107/1721:NO 081081172147 744041-7
Cadmium NO ug1L 1.0 1 08107/1721:60 081081172147 7440-43-9
Chromium NO ug/L 50 1 08/07/1721:50 08108/172147 7440-47-3
Copper NO uPA- 50 1 08107/1721:50 081081172147 7440-50P8
S Lead NO ug/L 50 1 08/07/1721:50 08108117 21 47 7439-92-1
Molybdenum NO ug/L 5'0 1 08107/1721:50 08/081172147 7439-98-7
} Nickel NO 1911- 5.0 1 0810711721:W 081081172147 7440-02-0
Selenium ND uglL 10.0 1 0810711721'50 081081172147 7782-492
a
a Silver NO moll- 6.0 1 08/07/1721:50 08/08/1]214] 7440-22-0
% Thallium NO ugiL 10.0 1 08107/1721:50 08/18/1719:58 7440-28-0
Hardness,Total(SM 23408) 26500 uq/L 662 1 08/0711721:50 Output 72147
I Zinc NO uga- 10.0 1 0810711721:50 OBIOW1721:47 7440-66-6
- -"`1y154 Mercury Analytical Method:EPA245-1 Preparation Method:EPA 245.4
I Mercury NO uglL 0.20 1 08108117 01:20 0810911706:41 7439-97-6
3 625 MSSV Analytical Melhic:EPA 625 Preparation Method:EPA625
Acenaphlhene NO ug& 50 1 08107/1712:30 0WOW1706:12 83-32-9
Acenap)Rhylene NO u91L 50 1 0810711712:30 081OW1706:12 208968
Anthracene NO moll- 50 1 0807/1712:30 08/08117 05 12 120-12-7
eenzo(ahouturacene NO ugiL SIP 1 08107/1712:30 08/08/170612 5655-3
8.tO,cp)pyrene ND milt- 5.0 1 08107/1712:30 08108/17 SO 12 50-32-8
j Benzo(b)Ouounthene NO cold- 5.0 1 08107/1712:30 ONOW1706:12 205-99-2
Benzo(gL.i)peryien, NO ugiL 5.0 1 08/07/1712:30 0810811706:12 191-24-2
Benzo(k)Ouoranlhene NO ug/L 5.0 1 0810711712:30 08/08/1706:12 20708-9
4-Bromophenylphenyl ether NO ug/L 50 1 08107/1712:30 08ION170612 101-55-3
I ButyibenzyIdethalate NO milt- &0 1 08/07117 12 30 0810811706:12 85-68-7
4-Chlom-3 melhylphenol NO ugiL 5'0 1 0810711712:30 0810811706:12 59-50-7
bis(2-Chloroelhesomelhane NO milt- 10.0 1 08107/1712:30 08108117 he 12 111-91-1
bis(2 Clueroelhyl)ether NO .91 5.0 1 0810711712:30 0810811706'42 111-44-4
2-Chloronaphthalene NO cold- 50 1 0810711712:30 0810811706'12 91-584
2 Chlorophemel NO ugh- 50 1 08/07/1712:30 0810811706:12 95-57-8
i 4 Chicrophenylphenyl ether NO u9dL 5.0 1 06107/171230 08/081170612 700572-3
Chrysene NO u91L 50 1 0810711712:30 08108117 06 12 218�01-9
1 Dmenz(a,b)anthracene NO uglL 50 1 0810711712'.30 08108/1706:12 5370-3
r
3 1,3-Dichlorobenzene NO ugh- 5.0 1 08I07/1]12:30 08I0811706:12 541-73-1 '.
14-Dichlorobenzene NO ugiL 50 1 08/07/17 C?30 0810811706:12 106467
3,T-Detcorobenrdine NO ugiL 25.0 1 0810711712,30 0810811706:12 91-94-1
1 2,4-Dichierophenol NO ugiL 5.0 1 08107/1712:30 0810811706:12 120-83-2 '..
E Dielhyiphthalate NO ug/L 5.0 1 0810711712:30 081OW1706:12 84-662
- 2,4-Dimethylpheno1 NO ugiL 10.0 1 0810711712:30 08/08/1706:12 105-67-9
i
` REPORT OF LABORATORY ANALYSIS
[ This`¢part abst net be reproduceq except in lu'l,
Date:0 8/2 212017 10:12 AM wchow mewnnen conyemof Pace Analytical Services,LLc. Page 28 of 96

Pace Analytical Services,LLC
aceAnalytical® ,eview Riv Dr.
Alle.NC C 2880i
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i3 ANALYTICAL RESULTS
7 Project: Low&Bona, Inc 1210140
Pace Project ND.: 92350243
Sample: Basement Groundwater Lab ID: 92350243007 Gollecled: 08/02/17 15.30 Received: OW03/1716:47 Matrix:Water
Parameters Results Units Repod Limit OF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method:EPA 625 Preparation Methed:EPA 625
t Dimethylphihalate NO ug/L 5 I 1 0810/171230 0810811706:12 131-11-3
Oin-butylphthalate NO ui 50 1 0810711712:30 0810811706:12 84-74-2
4,6-Dicdo-2 methylphenol NO iri 20.0 1 08/0711712:30 0810811706:12 534-52-1
2,4-Dinihophenoi NO ug/L 50.0 1 08107/1712:30 0810811706:12 51-28-5
2,4-Dinitrotoluene NO ugr. 5.0 1 0810711712:30 08/0811706:12 121-14-2
2.6-0initrotoluene NO ug/L 5.0 1 0810711712:30 0810811706:12 606-20-2
i Dim oclylphthalate NO uga- 50 1 081071171230 08/08/1706:12 11784-0
1,2-Diphenylhydaums, NO ugf- 5.0 1 08107/1712:30 081OW1706:12 12266-7
his(2-Elhylhexy0phthafine NO MIL 5R 1 0810711742:30 08/081170612 117-81-7
I'moranthene NO ug/L 5.0 1 08107/1712:30 08/0811706:12 206-44-0
Roseau NO ug1L 5.0 1 08107/1712:30 0810811701 86 73-7
Hexachloro-1,3-butadiene NO ug/L 50 1 08/0711712:30 0810811706'12 87-68-3
Heeachiorobeezene NO ug7L 50 1 08107117 12 30 08108/1706:12 118-74-1
Hexachio,ocyclopentadieoe NO di 10.0 1 OBIG711712:30 08108/1706:12 77474
Hexachloroelhane NO ue1L 5.0 1 08107/1712:30 08/0811700:12 67-72-1
7 indeno(1,2,3 empyrens NO no& 5.0 1 08107/1712:30 0810811706:12 193J9-5
j Belmopan NO ug/L 10.0 1 08107/171230 0810811706'12 78-591
3&4-Melhylphermorn pCresol) NO ughi 100 1 0810711712:30 OW0811706'12 15831-104
3 'ttaphlhalene NO uge- 50 1 08/0711712'30 08/08/1706:12 91-20-3
.Jitrobenzene NO ogr- 5.0 1 0810711712:30 OW08/1706:12 98-95-3
2-Nllrophenoi NO tied- 5.0 1 08107/1712:30 08/0811706,12 88-75-5
4-Nilrophenol NO uml- 50.0 1 08107/1712:30 08108/1706:12 10002-7
N Nitosodimethylarnme ND ug/L 5.0 1 08107/1712:30 0810811706'12 62-75-9
j N-Nitroso-di-mpmpylamins NO ug1L 5.0 1 0810711712:30 0810811706:12 621-64-7
N-Nilrosodiphenylamine NO ug& 100 1 08/0711712,30 08/08/1706:12 86-30-6
2.2-Oxybis(l-chlocadopane) NO ugi 50 1 0810711712:30 08108/1706:12 108-604
ti Pentachlorophenol NO tied- 10.0 1 08107/1712:30 08108/1706:12 87-86-5
Phenanih,ene ND ug/L 5.0 1 0810711712:30 08108/170612 85,01-8
- Phenol NO ug/L 5.0 1 08/07/1712:30 0810811706:12 108�95-2
f Pyrene NO ug/L 5,0 1 08107/1712:30 0810811706:12 129-01
LZA-Tdchlorabessum. NO ug1L 50 1 0810711712:30 0810811706:12 120-82-1
2.4,6 Trichlorophenol NO ug1L 10.0 1 0810711712:30 0810811706:12 86-06-2
Surrogates
Nilrobenzeres us(8) 80 % 10120 1 0810711712:30 0810811706:12 416560-0
1 2-Flumalephenyl(S) 73 % 15-120 1 08107/1712:30 0WOW1706:12 32"08
t Teryhenyl-d14(S) 62 % ll-131 1 0810711712:30 0810811705:42 1718AI-0
Phene no(S) 28 % 10-120 1 0810711712:30 08/0811708:12 13127-88-3
2-Fluorophenol(S) 45 % 10120 1 08/07/1712:30 0810811706:12 367-12-4
2,4,6-Tribromophenoi(S) 89 % 10137 1 0810711712:30 08ION1706:12 118-79-6
624 Volatile Organics Analytical Method:EPA 624
Acrolem NO eg/L 5.0 1 0810911700'53 107-02-8 Ll
Acrylonilrile ND ugA- 50.0 1 08/09/900:53 107-13-1
Benzene NO 1 2.0 1 081091170053 71-43-2
Bromodichlommelhane NO ug11- 20 1 0810911700:53 75-27-4
- Biederman NO ug1L 20 1 081091170053 75-25-2
Bromomelhene NO hi 2.0 1 08109/1700:53 7483-9
v
REPORT OF LABORATORY ANALYSIS
This repod shay not he intercom",except in lu'd,
Data 08/22/201710:12 AM Iteaut me"'rinse consent of Pace Aee1,1a1 Services,LLG Page 29 of 96

Pace Analytical Services,LLC
aeeAnalytical a A 26 R, 8 Dr
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(828)254-]1]6
ANALYTICAL RESULTS
Project: Los,&Sonar Inc 1210140
Pace Project No.: 92350243
j Sampie: Basement Grountlwater Lab ID: 92350243007 Collecletl: 08IO2I17 15:30 Received: 0 810 3111 16:47 Matrix:Water
Parameters Results Units Report Limit DE Prepared Analyzed CAS No, Coal
624 Volatile Organics Analytical Method EPA624
Carbon tetrachloride NO ug/L 20 1 0810911700:53 56-235
Chimobenzene NO mill 20 1 08109/1700:53 108-90-7
Chloroencom NO ug1L 2.0 1 08109117 00 53 75-00-3
Chloroform NO uga- 20 1 081091170053 6766-3
l Chlommethane NO ugl- 20 1 OW0911700:63 74-BZ3
Dibromochlommelhane NO ug1L 2A 1 0810911700:53 124-48-1
1,2-Dichlorobenzene NO mare, 2.0 1 0810911700:53 95-50-1
1,3-Dichlorobenzene NO hard- 2.0 1 0810911700:53 541-73-1
1,4-Oichimolrenzene NO ugh. 2.0 1 OW0911700:53 106-46-7
>_ 1,1-Dichicaoethene NO ug& 2.0 1 0&09/1700:53 75343
12-Dichloroethane NO uglL 20 1 0810911700:53 107-06-2
1,1-Oichloroeprobe NO Una- 20 1 OW0911700:53 25-35-4
cis-1,24dortmoelbene NO ug1L 20 1 08I09I1700:53 156-53-2
trans-1.2-Dichlonothene ND mill- 2.0 1 08/0911700:53 15660-5
1,2-Dichlompropane NO ONA. 2P 1 0810911700:63 7887-5
cisAS Dichlorapropene NO ug1L 2P 1 0810911700:53 10061-01-5
Iran-1.3 Dichimopropene NO eg/L 2.0 1 0810911700:53 10061-02-6
j Elhylbenzene NO ugf- 20 1 0810911700:53 100-414
3jethylene Chloride NO uga 2.0 1 0W09/1700'53 75-09-2
t '1,2,2-Tetrachloroelhane NO marl- 20 1 081091170053 79-34-5
Telrachlomethene NO ug/L 20 1 0810911700:53 127-18-4
Toluene NO ug/L 20 1 0810911700,53 108-88-3
1 1,1,1-Trichimaethane NO ug/L 2.0 1 0810911700:53 71-55-6
1.1,2-Trichloroelhane NO ug1L 2.0 1 U810911 7 0 0:53 7900-5
Tdchloroelhene NO UgA. 2.0 1 0810911700.53 7901-6
Trichloro0uoromethane NO ugA. 2.0 1 0810911700:53 75-69-4
Must chloride NO ug/L 2.0 1 0810911700:53 75-01-4
Surrogates
4 Bromofluorobenzene(S) 103 % 70130 1 0&09117 00 63 460-004
Toluene d8(S) 113 % 70-130 1 08109117 00 53 2037-265
1,2-DichloOethaned4(S) 79 % 70430 1 0810911700:53 17060-070
2540C Total Dissolved Solids Analytical Method:SM 2540C
Trust Dissolved Sogds 66.0 mglL 25.0 1 08/0811]09:39
I
2540D Total Suspended 501itls Analytical Method:SM 2540D
Total Suspended Solids NO mgo. 3A 1 0810811717'08
Total Nitrogen Calculation Analytical Method:TKN+NO3+NO2 Calculation
Total Mangan 0.17 mgl- 0,12 1 08109/1718:11
350.1 Ammonia Analytical Method:EPA 350A 1993 Rev 2.0
j
Nitrogen,Ammonia NO mglL 0.10 1 0810911705:04 7664-41-7
E 351.2 Total Kjeldahl Nitrogen Analytical Method:EPA351.2
Nitrogen,Kletdahl,Total NO mgdL 0,50 1 08/09/17 17:02 ]]27-37-9
i
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in fear
Date:08122/2017 10:12 AM without Ue wdnen conaentot Pace Anabi( lServices,LLC. Page 30 of 96
3
i

Pace Analytical Services,LLC
aeeAnalytil l a 2225low lowness,0r.
Wmsa�Ycmen ASM1eville,NC 28864
(828)254-]1]6
I
j ANALYTICAL RESULTS
Project: Low&Boner Inc 1210140
Pace Project No.: 92350243
Sample: Basement Groundwater Lab ID: 92350243007 Collected: 0810211715:30 Received: 081031171647 Matrix:Water
i Parameters Results Units Report Limit OF Prepared Analyzetl CAS No. Dual
j
! 353.2 Nitrogen,NOZ/NO3 pres. Analytical Methotl:EPA 353,2
Nitrogen,NO2 plus NO3 0.17 mglL 0.020 1 08/0911712:17
365.1 Phosphorus,Total Analytical Method:EPA 365A
3 Phosphorus 0.080 mill 0050 1 08/1011706:37 ]]23-14-0
5220D COD Analytical Methotl:SM 5220D
Chemical Oxygen Demand NO mglL 25.0 i 0810]/1]1641
Sample: Downstream @ Manhole LAID: 92350243008 Collected: 0810211716:20 Received; 0810311716:47 Main. Mt.,
25
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Dual
HEM,Oil and Grease Analytical Method:EPA 1664E
Oil and Grease NO mil 5.0 1 OW1711705:11
i
I 200.7MET ICP Analytical Method:EPA 2007 Preparation Method EPA 200]
:;'alimony NO UgIL 50 1 08/0]/1]21'50 08IOBI1721:50 7440-360
- "Arsenic NO ug/L 100 1 0810711721:50 081081172150 7440-38-2
Beryllium ND ulL 10 1 0810711721:50 08/0811721:50 ]440-41-]
Cadmium NO uglL Lo 1 0810]/i]21:50 0810811721:50 7440-43-9
Chromium ND uglL 5.0 1 0810711721;50 0810811721:50 ]440-4]-3
Copper 8.7 uglL SO 1 08/0711721:50 OW081172150 7440-50-8
Lead NO uglL 5.O 1 08107/1721:50 0910811721:50 7439-92-1
Molybdenum 12.3 uglL SO 1 08107/1721:50 081081172150 ]43TEa-]
Nickel NO mpl- 5.0 1 081071172150 081081172150 7440-02-0
Selenium NO eg/L 10.0 1 081071172150 OW08/17 2150 ]]82-49-2
j Silver NO ug4 5.0 1 0810710'21:50 08108/1721:50 7440-22-4
Thallium ND no& 100 1 081071172150 0811 WI720,14 7440-280
j Hardness,Treat ISM 2W13) 12500 ug/L 662 1 08107/17 24 50 08/08/17 2150
Zinc 177 Truth- 10R 1 08/07117 21:50 08108117 21:50 7440 66 6
245.1 Mercury Analytical Method:EPA 24L1 Preparation Method:EPA 245.1
Mercury NO UeL 0,20 1 08/08/1701:20 0810911706A4 7439-97-6
I 625 MSSY Analytical Method:EPA 625 Preparation Methotl:EPA 625
Acenaphtheoe ND TgIL 5.0 1 08107/171230 08108/170641 83-32-9
Acenaphthylere ND ug/L 5.0 1 08107/1712'.30 08108/i70641 208-9L8
3 Anthracene, NO eg& 5.0 1 0810711712:30 08108N706,41 120-12-7
Benzo(ocre scene ND Ug/L 50 1 08/07/17 12:30 08108/1706'41 56-55-3
Benzo(a)pyrene ND uglL 50 1 08a0?11712:30 OW081170041 50-32-8
Bencodelumanthene ND uglL 50 1 08/0711712:30 08108/1706:41 205992
Benzo(g,h.l)perylene ND uglL 5.0 1 08/0711712:30 08/0811706:41 191-24-2
Beuar.du r,renthene ND uglL 5.0 1 0810711712:30 08108/17 06 41 207-08-9 '..
4 Bramophenylphenyl ether NO se lL 5.0 1 08107117 12:30 08/08117 WAl 101-55-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except In full,
' Data 081221201710:12 AM w,mout fire wntlen wncem of Pace analytical Services,ua Page 31 of 96
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Pace Analytical senmaa,LLC
e 2225 Riverside 0r.
ace Analytical Ashevda,NC 28804
[phone]
t
ANALYTICAL RESULTS
Project: Law&Bru ar too 1210140
I Pace Project No.: 92350243
Sample: Downstream@Manhole Lab ID: 92350243008 Collected: 08102/1716:20 Proeised: 081031171647 Mont :Water
25
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
a
625 MSSV Analytical Method:EPA625 Preparation Method:EPA 625
Butylbenzyiphthalate NO red- SO 1 0810711712:30 0810811706:41 85-68-7
4-Chlom3 methylphenol NO um/L 5.0 1 08/0711712:30 OW0811700:41 59-50-7
bis(2-Chloroethoxyjmelhane NO uglL 10.0 1 0810711712:30 08/08/17 IS 41 411-91-1
} bis(2-Chloroelhyl)ether NO ug1L 5.0 1 08107/1712:30 0810811706:44 111-44-4
2 Chlonamphlhelene NO ug/L 5.0 1 08107117 12 30 0&0&170641 91-58-7
2-Chlarophenol NO U91 50 1 08107/171230 08/08M 706:41 9557-8
3 4Chlarophenylphenyl ether NO ug11- 50 1 08107/1712:30 0810811706:41 700572-3
Chrysene NO opt- 5A 1 0810711712:30 081081170641 218-01-9
' Diame(a.h)anilrecene NO uglL 5L 1 0810711712:30 OBI0X1706:41 53-703
I 1,3-Dichlorobenzene NO ugg- 5A 1 08107M712:30 081OW170641 541-73-1
1.4-Dichlorobenzene NO ogR 5.0 1 0810711712:3D 0810817 06.41 106-46-7
3,3'-Dichlombenzidine NO ugh- 25.0 1 08107M712:30 08108117 06 41 91-94-1
2,4Dlchlomphenol NO red- 5.0 1 0810711712:30 08/08/17 GSAI 120-83-2
Diethylphthalate NO ugl- 5.0 1 08/07/1712:30 0810817 W 41 84-66-2
2,4-Dimethylphenol NO ugrL 10.0 1 08107/1712:30 08108117 IS 41 10567-9
Dimethylphlhalate NO ug1L 5.0 1 08/07/171230 0810811706;41 13141-3
Din-butylphthalate NO uglL 50 1 0810711712:30 08/081706:41 84-74-2
"i 6-Oinitro-2-melhylphenol NO uglL 260 1 08107/1712:30 08/081170641 534-52-1
�,4-Diuitrophenol NO ug1L 500 1 08107/1712:30 0810811706:41 51-285
( 2,4 Oinilrotoluene NO ug/L 5A 1 08/07/1712:30 08/08/170 et 121-14-2
26-Dinilrololuene NO uglL 50 1 08/07/1712:30 081081170641 606-20-2
Di-n-0ctylpmhalate NO ugll 5R 1 08/0711712:30 OBIOW1706:41 117-84-0
- 1.2-Dipheny1hydwroe NO ug/L Ed 1 0810711712:30 081081170641 122-6&7
bed2-Elhylhexyljphtha1ate NO ugh- 5.0 1 08/0711712:30 0810811706:41 117-81-7
Fluoranlhene NO Red- 5.0 1 08/0711712:30 08108L 706,41 206-44-0
Flu eme NO ug1L 5.0 1 0810714712:30 08108/1706AI 86-73-7
Hexachloro-1.3 butadiene NO ugd- 5.0 1 0&07/1712:30 081OW17 MAI 87-68-3
Hexachlombenzene NO ug1L 5.0 1 08107/1712:30 08/08117 W41 118-74-1
Hexachlomcyclopentadlene NO ugh- INN 1 08/07/1712:30 08108/1706'41 77-474
Hexachlolncaame NO ug1L 5.0 1 08107/1712:30 0810811706:41 67-72-1
Inden0(1,2,3 ohayrene NO ug/L 50 1 08J07/171230 08/0811706:41 193-39-5
Isophorone NO ogd. 100 1 08107/17 12 30 08/0&1708:41 78-59-1
3&4-Methylphenol(m&p Cresol) NO ug/L 100 1 08107/1712:30 0&O&170641 15831-104
- Naphthalene NO uglL 5A 1 0810711712:30 mutual 706:41 91-20-3
Nitrobenzene NO ug/L 50 1 08AV/V 12:30 08/0811706:41 98-95-3
&Nlhophenol NO o9/L 50 1 08107/1712:30 081081706:41 88-755
4 Ndorphenol NO ugd- 50.0 1 081071171130 081081170641 100-02-7
N-Nitrosodimethylamine NO ugl 5.0 1 08/0711712:30 0810811706:41 62-759 '..
N-N0ros0 or mpropylamine NO ugh- 50 1 08107117 12:30 08108117 06'41 621-64-7
N-Nilrosodiphenylamine NO ugh- 10.0 1 08107/1712:30 08/08/170641 86-306
2,2'-Oxybis(Lchloropropane) NO ug/L 5.0 1 081071W 1230 08108117 06 41 IOB-60-1
Pentachlorophenol NO ugh- 10.0 1 08107/1712:30 081081170641 87-86-5
Phenanthrene NO red- 5.0 1 08107/1712:30 0810811706:41 8501-8
j Phenol NO ug/L 5.0 1 0810711712:30 0810811706:41 108-95-2
J Pymme NO ug11- 5N 1 0810711712:30 081081170641 129000
1,2,4-Tdchimmixnzene NO oglL 50 i WIDOW 12 30 08108117 06 41 12082-1
t
'A REPORT OF LABORATORY ANALYSIS
jmla rap0n OWI not be reproduced,exeapl ia f W.
Dale:08122/201710:/2AM wchaWdoldaeocarasatol Pace Analytlral sem�a,LLG Page 32 of 96
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a Pace Analytical Services,LLC
aceAnalXical a 2225 RivereNa Or.
Aahaville,NG 28304
} awnpaC¢'aAxMn (92A2547176
1
ANALYTICAL RESULTS
Project: Low&Sonar Inc 1240140
Pace Project No.: 92350243
Sample: Downstream @ Manhole Lab ID: 92350243008 Collected: 08J0211716:20 Received: 0810 311 7 16:47 Matrix'Water
25
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Coal
3
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
24,6-Trichlorophenol ND ngiL 10.0 1 08/07/1712:30 08108/1706'41 88-06-2
SnRogmes
,? Nitrobenzedi(S) 72 % 10-120 1 0810711712:30 081OW1706:41 4165-60-0
1` 2-Fluoroblphenyl(8) 71 % 15120 1 08/0711712:30 0810811706:41 321-608
i Terphenyl-d14(S) 55 % 11-131 1 08/0711712:30 OW0811706'41 1718-51-0
Pendell(S) 28 % 10-120 1 08107/1712:30 081081170641 1312788-3
s 2-Fluomphenol(S) 44 % 10420 1 08107/1712:30 08108/i 706:41 367-12-4
2,4,6-Tabromophenol(S) 87 % 10-137 1 08107/1712:30 08/0811706'41 118796
624 Volatile Organics Analytical Method:EPA624
i
' Acroleln NO dill- 5.0 1 08/08/1722:31 107-02-8 Li
Acrylonildle NO ug1L 60.0 1 0810811722'31 107-13-1
Benzene NO ug1L 2D 1 OBI0W1722:31 71-432
Bromisichloromelhane ND and- 2D 1 08/081172231 ]52]-4
- Woodland NO mid- 2D 1 0810W172231 75-25-2
Bomemethane ND u91L 2.0 1 08108/1722:31 74-83-9
Carbon letrachlome NO ugf- 2.0 1 ONOW1]22:31 56-23-5
Ehloomearn ene ND ug/L 2.0 1 08/08/17 22:31 108 90-]
]Zhlomethane NO ug/L 2.0 1 08108/1722:31 75-00-3
Chloroform NO dg1L 20 1 08117 67-66-3
Chlommethane NO ug1L 20 1 OBIOW172231 ]4-8]-3
Dibromochlommethane NO ug/L 2.0 1 08/0811722:31 124A8-1
i 1,24achbmbenzene ND ng/L 2D 1 08/0811722:31 95-50-1
1,301ohlorobemene ND ug/L 20 1 0W0811722:31 541-73-1
1.4-Dichlombenzene ND ug1L 2.0 1 0810811722:31 10646-7
1,1-Dichloroethene NO ug/L 2D 1 08108/1722:31 75-34-3
1,2-Dichlomethane NO dill- 20 1 0810811722:31 107-06-2
i 1,1-Dichloroethene NO dg/L 20 1 08/0811722:31 7535-4
cis-12-Dirtneroethene NO ng1L 20 1 081081172231 156-59-2
trans4,2-Dichloroelhene ND ug/L 2'0 1 OSIOW172231 156SP5
1.2-Dichlompropane ND ng/L 2.0 1 OWO81112231 ]88]-5
ins-1,3-Dchloropropene ND ug/L 2.0 1 08/0811722:31 10061-01-5
trans-1,3-Dichloropropene ND ug/L 2P 1 0810811722:31 10061-02-6
tI Ethylleamene ND ug/L 20 1 0810811722:31 10041-4
I Methylene Chloride NO rii 2.0 1 08108/1722:31 7509-2
- 1,1,2,2-Tetrachloroethane ND ug1L 20 1 081081172231 79-34-5
Tetrachloroethane NO ago- 20 1 0810811722'31 127-184
Toluene ND ug& 2D 1 U810 8117 2 2:31 108-88-3 '..
1,1,1-Trichlomethane NO ug/L 2.0 1 OW0811722:31 71-55-6
1,1,2-Oichloroetbane NO ugi 2.0 1 0810811722:31 79&00-5 '.
Trichlomethene ND ug/L 2.0 1 O8/08/II 22:31 79-01-6
Trichlom0onromethane NO u,F 2.0 1 08/0811722:31 7569A
- Vinyl chloride NO opt- 20 1 00108/1722:31 7501-4
Surrogates
4-Bromno0uorelamorae(S) 105 % 70-130 1 081081172231 460-00-4
Toluene48(S) III % 70-130 1 08108/172231 2037-265
5, 1
REPORT OF LABORATORY ANALYSIS
Thia farm act not be reprodowi,except in full,
Date:0 812 212 01]10:12 AM vrithon he wdnen oci of Pace Anaill—I Services,LLC. Page 33 of 96
1
t
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s Pace Analytical services,LLC
aeeAnalytieal RNeretle 0r
} - Asheville,NC zeeaa��
(828)2544176
3
ANALYTICAL RESULTS
Project: Low&Bona, Inc 1210140
Pace Project No.: 02350243
i Sample: Downstream@Manhole Lab Oh 92350243008 Collected: 08102117 16 20 Received: OW0311716:47 MaMx:Water
25
Parameters Ril Units Report Limit DF Prepared Analysed CAS No, Chat
624 Volatile Organics Analytical Melhotl:EPA 624
Stimogafes
1.2-Dlohlemelhane-04(3) 86 % 70-130 1 0WOW172231 17060070
i
2540C Total Dissolved Solids Analytical Method:SM 2540C
Total Dissolved Solids 58.0 Trill- 25D 1 0810811709:39
2540D Total Suspended Solids Analytical Method:SM 25400
Total Suspended Solids NO "L 8.3 1 08/0811717:09
Total Nitrogen Calculation Analytical Method.TKN+N0S+NO2 Calculation
Total Nitrogen 1.7 uni 0,12 1 0810911718:11
350.1 Ammonia Analytical Method:EPA 350.11993 Rev 2.0
Nitroger4Ammacia 0.31 pri 0,10 1 OW0911705:06 7664-41-7
351.2 Total Kjoidahl Nitrogen Analytical Method:EPA 351.2
-...Nitrogen,Kjeldahl,Total 1.6 hi lL 0,50 1 08109117 17:03 7127-37-9
353.2 Nitrogen,N021NO3 pros. Analytical Melhed:EPA 353.2
Nitrogen.NO2 plus NO3 0,092 Trial- 0,020 1 081091912:18
366.1 Phosphorus,Total Analytical Method:EPA 365A
Phosphorus 0.71 mg1L 0.050 1 0811011706:38 7723-140
i
5220D COD Analytical Method:SM 5220D
Chemical Oxygen Demand ND mg& 25D 1 OW0711718:41
Sample: New Stormwater Point Lab ID: 92360243009 Collected: OW021171130 Received: 081031171647 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Cual '..
HEM,Oil and Greasy Analytical Method:EPA 16648
- Oil and Grease NO Trill- 5.0 1 0811711705:12 '.
1s
200.7 MET ICP Analytical Method:EPA 200.7 Preparation Method:EPA 2003
i Antimony NO ug/L 50 1 08113117 22,05 08116117 03 22 7440-36-0
- Afamic NO Rini T10 1 08113/1722:05 0811511703:22 7440-38-2
Beryllium ND ri 1.0 1 0811311722:05 08/1511703:22 7440-41-7
Cadmium NO ug/L 1.0 1 08/13/II 22:05 0811511703:22 744043-9
' Chromium NO ugs- 6D 1 0811311722:05 0811511703:22 2440-47-3
I Copper 6.8 red- 50 1 0811311722:05 08115/17 03 22 7440-508
Lead NO uglL 50 1 0811311722:05 08115117 03 22 7439-92-1
Molybdenum 9.9 hill- 50 1 08/1311722:05 0805M703:22 7439-98-7
t
i
t
REPORT OF LABORATORY ANALYSIS
This report shall not be repmduwd.except in run.
Dale:081221201710:12 AM rmtnout tnewdnen consemot Paceensly[(Services.LC Page 34 of 96

i
Pace Analyttcal Services,LC
I 2a rside or
aceAnalytcai Ashe,ff , G2e804
xecTo,cafteas (828)2!9]1]6
o�
ANALYTICAL RESULTS
Project: Low&Sonar Inc 1210140
Pace Project No.: 92350243
Sample: New Stormwater Point LAID: 92350243009 Collected: 08102/1717:30 Received: OW0311716:47 Matrix:Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Coal
j 200.7 MET ICP Analytical Method:EPA 200.7 Preparation Methotl:EPA 2001
I Nickel NO uglL fro 1 0811311722:05 0811511703:22 744002-0
Selenium ND ug& 100 1 08113M722:05 08f1511703:22 7782-49-2
Silver NO ugA_ 5.0 1 0811311722:05 08115117 03 22 7440-22-4
Thallium ND ug1L 40.0 1 081131172205 0811511703'22 744028-0
Hardness.Total(SM 2340B) 14400 mpt, 662 1 08/1311722.05 0811511703:22
j Zinc 161 uga- 100 1 0811311722:05 ON1511703:22 744066-6
# 245.1 Mercury Analytical Method:EPA245.1 Preparation Method:EPA245A
Mercury ND ug1L 0,20 1 0810911705:35 08/1111700:38 7439.97-6
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
5 Aeenaphthene NO ug/L 5.0 1 0810711712:30 08/08/1707:10 83-32-9
Acenaphthylene NO red- 5.0 1 08/0711712:30 08/08/17 W:10 208-96-8
Anthracene ND ug/L 5.0 1 08107/1712:30 08/0811707'10 120-12-7
Benzo(a)anthracene ND ug/L 5.0 1 08107/1712:30 08109/17 07'10 56-55-3
' Benzo(a)pyrene NO ug1L 50 1 08/07/1712:30 OW0811707:10 50-32-8
Benzopplooranthene NO ug/L 50 1 08107/1712:30 OW0811707:10 20599-2
.-.Benwdg.h,h,,aene NO upt. SO 1 08/0711712:30 0810811707:10 191-24-2
3enzo(k)fluoranthene ND ug& SO 1 0810711712:30 08f08/1707:10 207-08-9
4nomophenylphenyl ether ND ug1L 5.0 1 08/07/1712:30 0810811707:10 101-55-3
13mylbenzylphthelate ND uglL 5.0 1 08107/1712:30 O8I08/1707:10 8568-7
4 Chlom-3-melhylphenol NO ug1L 5.0 1 08107/1712:30 OW0811707:10 59-50-7
3 bis(2-Chlamcthon )methane NO ug/L 10.0 1 08107/1712'.30 0810814707:10 111-91-1
bis(2-Chloroethyl)ether NO upt- 50 1 0810711712:30 OW0811707'10 111-44-4
2-Chloronaphthalene ND ugA 5.0 1 0810711712:30 08mWl707:10 91-58-7
2-Chlomphenol NO ug1L So 1 0810714712,30 08108/1707'10 95-57-8
t 4-Chlorophenylphenyl ether ND ug1L 5.0 1 0810711712:30 08108/1707'10 700572-3
Chrysene NO ugh- 5.0 1 08107/1712:30 0810811707'10 21801-9
Dibenz(ab)and racene NO ug1L 50 1 08/07/1712:30 08/0811707:10 53-70-3
L3-Dichloomenzene NO ug/L 50 1 08/07/1712:30 08108/1707:10 541-73-1
[ 1,4 Dichimobenzene NO ug/L 5.0 1 08107/1712:30 08108/1707:10 106-46-7
3.T-Dichloromoreine NO ug& 250 1 0810711712:30 ON0811707:10 91-94-1
2,4-Dichlorophenol NO ug4 50 1 0810]/1]12:30 08TIVI707'10 12083-2
Diethylphlimade ND age- SO 1 0810711712,30 08/0811707:10 8466-2
2,4-Dimelhylphenol NO ug1L 400 1 0810711712:30 08108/1707:10 105-6T9
Dimethylphlhalate ND ug/L 50 1 08107/1712:30 0810811707:10 131-11.3 '..
1 Oi-n-butylphthalate NO uglL 50 1 0810711712,30 0810811707:10 64-742
4,6 Dinilm-2-melhylphenol ND uglL 200 1 0810711712:30 08108/1707:10 534-52-1
I 2.4-Dmitrophenol NO mpL 50.0 1 08107tl712:30 0810811707:10 51-28-5
2.4 Dinihotoluene NO ug/l. 5.0 1 0810711712:30 08f08/1707:10 121-14-2
y 2,6-Dinitmloluene NO ug/L 5.0 1 0810711712:30 0810811707:10 606-20-2
Ol-n-octylphthaine, NO ug1L 5.0 1 08107/1712:30 06108/1707:10 117-84-0
L2-Diphenylhydrazine ND opt, 50 1 081071171230 08108/17 07:10 122-66�7
bis(2-Ethylhexy1h,mralate NO mPL 50 1 08107/17 12 30 08/081170710 117-81-7
Elooranthene NO ugll 50 1 08107/171230 OW0811707:10 206-44-0
Plumene ND ug& 50 1 0810711712:30 0&0811707:10 86-73-7
REPORT OF LABORATORY ANALYSIS
Tbie report shall not be reprotluce4,except in lull,
Date:081221201710:12 AM without the written..sent of Pace Analytcl Service,LLC. Page 35 of 96
j
i

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j Pace Analytical Services.Lte
iIy "Ana jdical® 2 owhro, C 28 04
ASM1eville,NC 28804
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I ANALYTICAL RESULTS
Project: Law&Boner Inc 1210140
Pace Project No.: 92350243
I Sample: New Stormwater Point Lab ID: 92350243009 Collected: 08/02/1717:30 Received 08/031171647 Matrix:Water
)
j Parameters Results Units Report Limp DF Prepared Analyzed CAS No. Oral
625 MSSV Analytical Method:EPA625 Preparation Method:EPA 625
Hexachloro-1,3-butadiene NO uglL 50 1 0810711712:30 08108/17 07:10 8768-3
Hexachlorobenzene NO ug/L 50 1 08107/171230 08108/1707:10 118-74-1
Hexachlorocyclopernadiene NO ugiL 10.0 1 0810711712:30 081081170710 77-47A
Hexechloroettene ND Tg/L 5.0 1 0810711712:W 0 8/0 8117 07:10 67-72-1
Indeno(1,2.3-cd)pyrene NO Tall- 5.0 1 08107/1712:30 0810811707:10 193-39-5
Isophoforte NO uglL 10.0 i 08107/1712:30 OW0811707:10 71 591
3&4-Melhylpheno1(m&p Cresol) NO ugll- 100 1 08107/1712:30 08108/1707:10 15831-10-4
Naphthalene NO uglL 50 1 0810711712:30 08IOB1 707:10 91-20-3
Nitrobenzene NO Tg/L 50 1 08/07/1712:30 0810811707:10 98-95-3
2-Nitrophenol NO ugh 5.0 1 0810711712:30 0810811707:10 88-75-5
4-Nitrophenol ND Tall- 50.0 1 0810711712:30 0810811707AO 100-02-7
N-Nituchadimethyrurins NO Tall- 5.0 1 08107Y1712,30 0810811707:10 62-76-9
37 N-Nitese,di-n-proplannine NO ug/L 5.0 1 0810711712:30 08/0811707'10 621-64-7
N Nitrosotliphenylamine NO ugA- 10.0 1 0W0711712:30 081OW1707:10 86-30-6
$2'-Oxybis(1-chympmpane) NO u9/L 5.0 1 08107/1712:30 0WOW170710 108-60-1
I Peatachlorophenol NO ago- 100 1 08/0711712:30 OW0811707:10 87-86-5
j Phenanthrene NO ago- 50 1 0810711712:30 0810811707:10 8501-8
Phenol ND ug1L 5.0 1 0810711712:30 0810811707:10 10895-2
17 1yran. NO ug/L SO 1 08/07/1712:30 081081170710 129-00-0
7,2.4-Tdchlombenzene NO Tall- SO 1 08IG711712:30 08108117 07:10 120-82-1
2,4,6-Tdchlorophenol NO ug/L 10.0 1 0810711712:30 OB/081170710 88 06 2
Surrogates
_ Nitrobenzene-65(S) 66 % 10120 1 08107/171230 08108/1707:10 416560-0
2-Fluorobiphsnyl(S) 68 % 15120 1 0810711712:30 08/08/170710 321-60-8
Euphenyl-d14(S) 62 % 11-131 1 08/0711712:30 08108117 07 10 171851-0
Phenol d6(S) 27 % 10 120 1 08107/1712:30 08108117 07:10 13127-88-3
i 2-Fluarephenol(8) 44 % 10120 1 0810711712:30 0810811707:It) M7-12-4
ff 24,6-Tribromophenol(S) 87 % 10-137 1 0810711712:30 0810811707:10 418-79-6
624 Volatile Organics Analytical Method:EPA624
Acrolein NO u,a- 50 1 08109/1701:10 10702-8 -1
Acrylonilrile NO ug/L 50.0 1 08109/1701:10 107-131
Benzene NO ug/L 20 1 08109/1701:10 71A3-2 '..
Bromotlichloromethane NO r91L 2.0 1 DW09/4701:10 75-274
Sromoform NO uglL 2.0 1 08/09117 Or 10 75-25-2
Bromomethane NO ugl6 20 1 0810911701:10 74�83-9
Carbon tetrachloride NO ugh 2.0 1 0810911701:10 56-23-5
Chlorobenzene NO ug(L 2.0 1 0810911701'10 108-90-7
`[ Chloroet ere, NO ug/L 20 1 0810911701:10 75-00-3
Chloroform NO u911- 20 1 OW0911701:10 67-66-3
Chloromethane ND Tall- 20 1 0810911701:10 74-87-3
Dibromochloromethane NO raft- 20 1 08109/17 OL10 124-48-1
t 1,2-Dichlorobenzene ND ug1L 2.0 1 0810911701:10 95-50-1
1,3 Dichlorabenzene NO ug/L 2.0 1 0810911701:10 541-73-1
1,44oharombenzene NO ug/L 2.0 1 08/0911701:10 106467
1,1-DicMoroe(hthe ND Ug/L 2.0 1 0810911791'10 75-34-3
1,2-Dichloroelhane ND ug/L 20 1 OW0911701:10 107-06-2
7
s
REPORT OF LABORATORY ANALYSIS
This report ehan not be reproduced,except in roll,
Date:OS1221201710:12 AM -imam the whole,ce,sem of Pace Analycced services,LLC_ Page 36 of 96

Pace Analy46a1 Services,LW
3
2225 s Riverside Or.
aeeAnalytiea( NC 298e4
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j ANALYTICAL RESULTS
i
Project Low&sonar Inc 1210140
Pace Project No.: 92360243
Sample: New Stormwater Point Lab ID: 92350243009 Collected: 08102/1717:30 Received 081116,47 Matrix:Water
{
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Coal
624 Volatile Organics Analytical Method:EPA624
1,1-Dichloroethene ND mid- 2.0 1 08109/17 ONTO 75-354
cis-1,2-Dichlomelhene ND ug]L 2.0 1 0N0911701:10 156-59-2
Irons-1,24ichlorcethen, NO ugi 2.0 1 0810911701:10 156-60-5
i 1,2Oichlomproproe NO u9IL 20 1 0810911701:10 78-87-5
- cis-1,3-Dichloropr0pene ND ugl 20 1 0810911701:10 10061-01-5
tmns.1.3-Dichlompropene NO opt- 20 1 08/0911701:10 10061-02-6
Ethydrom,ene ND Li 2.0 1 08/0911701:10 100-41-4
' Methylene COal ND u9/L 2.0 1 0810911701:10 75-093
1,1,2,2Taluseliorcethane NO ug1L 2.0 1 0810911701:10 79-34-5
Tourchloroethene NO uglL 2.0 1 08109/1701:10 127-18-4
Toluene NO uglL 20 1 0810911701:10 108-88-3
1,1,1-Trichl.a ethane NO uel- 20 1 0810911701:10 71-556
j 1,1.2-Trichlomelhane NO coil- 20 1 OW0911701.10 79-00-5
SS Trichlomethene NO ug/L 2R 1 0810911701:10 79-01-6
j Trichlore0camo lhone ND ugfi 2.0 1 08/0914701:10 75-694
Vinyl chloride ND ugn- 2R 1 OW0911701'10 75-01-4
Surrogates
4-Bonammor0heezene Ch IN % 70-130 1 08109/1701:10 460-00-4
pluenede(8) 114 % 71T130 1 08109117 01 10 2037-26-5
_., 2-Dichloreethane-d4(S) 86 % 70-130 1 08109/1701:10 1706007-0
251 Total Dissolved Solids Analytical Method:SM 2540C
Total Dissolved Solids 64.0 mglL 25R 1 08/0811709:40
2540D Total Suspended Solitls Analytical Method:SM 2540D
rTotal Suspended Solids ND
3 mg/L 50 1 O8108117 13:49
Total Nitrogen Calculation Analytical Method:TKN+NO3+NO2 Calculation
Total Nitrogen 1.1 all 0.12 1 0810911718:11
350.1 Ammonia Analytical Method:EPA 350A 1993 Rev 2.0
j
Nitrogen,Ammonia 0.41 molt 0.10 1 08109IV O5:07 7664-41-7 '.
351.2 Total Kjeldahl Nitrogen Analytical Method:EPA351.2
,j Nitrogen.Kjeldahl,Total 1.0 mgk 0,60 1 08/09/17 1704 7727-37-9
353.2 Nitrogen,N021NO3 pres. Analytical Method:EPA 353.2
1
1 Nitrogen,NO2 plus NO3 0.078 mg/L 0.020 i 08109/1712:19
365.1 Phosphorus,Total Analytical Method:EPA 365.1
Phosphorus 0.67 m94 0050 1 OW10/170039 7723-14-0
j 5220D COD Analytical Methotl:SM 5220D
Chemical Oxygen Demand ND molt 250 1 08107117 18 41
i
3 #
REPORT OF LABORATORY ANALYSIS
This report spell not the reproduced! a oept in full,
3 Dale:06122/201710:12 AM ,,[hurt the wane.consent of Pace Anini Services,LLC. Page 37 of 96
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j Paco Analytical Services,LLC
aeeAnalytieal a 2225 RivetSitle Or.
i ( _ IX� Asheville,NC 28804
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ANALYTICAL RESULTS
Project Law&Bona. Inc 1210140
a Pace Project No.: 92350243
i Sample: East Ditch Lab IO: 92360243010 Collected: 08/02/1717,00 Received' OW0311716:47 Matrix:Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Goal
- HEM,Oil and Grease Analytical Method:EPA 16648
! Oil and Grease NO ou lL 5.0 1 08/17/1705:12
200]MET PUP Analytical Merootl:EPA 200.7 Preparation Method:EPA 200.7
Antimony NO ug/L SO 1 0811311722:05 0811511703'26 7440L36-0
Arsenic NO ug/L fell) 1 08/13/1722:05 08115117 03 26 7440.38-2
Beryllium NO age- 1.0 1 0 /13/1722:05 0811511703:26 7440-41-7
Cadmium ND u911- 1.0 1 081131172205 (Not 511703:26 7440-43-9
Chromium NO d,d- 50 1 0811311722,05 Thai 5/1703:26 7440-47-3
Copper flip ha/L 5.0 1 08/1311722:05 08/16/1703:26 7440608
- Lead NO ug/L 5.0 1 08113/1722:05 0811511703:26 7439-92-1
Molybdenum 22.6 ugh- 5.0 1 08113/1722:05 OW1511703:26 7439-98-7
f Nickel NO offer- 50 1 0811311722:05 08/1ITT 70326 744002-0
Selenium NO ug/L IOR 1 0811311722'05 0&1511703:26 7782-49-2
Silver NO upi- 50 1 081131172205 part 511703:26 7440-22-4
Thallium NO ha/L 10-0 1 0811311722,05 08116/1703:26 7440-28-0
's Hardness,Total(SM 23408) 19700 ug/L 662 1 08OW17 22,05 98116117 03:26
Zinc 135 and- 10.0 1 08/1311722:05 0811511703:26 7440-666
"F'))45.1 Mercury Analytical Method:EPA245.1 Preparation Method:EPA2454
5
- Mercury NO ug]L 0.20 i 08/09/1705:35 0801/1700A0 7439-976
1
625 MSSV Analytical Method:EPA 625 Preparation Method EPA 625
Acenaphthene NO ug1L SO 1 0810811710:00 08/1011702'28 8"2-9
Acenaphlbylene NO hg/L 50 1 0810811710:00 0811011702:28 208-96-8
`t Maracene NO ug/L 5.0 1 08108/171000 08/101170228 12012-7
Benzo(a)anthracene NO ug/L SO 1 0810811710:00 0811011702:28 56-55-3
Benzopupyrene NO ug/L 5.0 1 081081171000 08/1 Oil 702:28 50-32-8 '..
8enzo(b)Ovookehene NO gall- 50 1 0810811710.00 OWIGI1702:28 205-99-2 '..
Benzo(9h,i)perylene NO ad- 50 1 0810811710,00 0811011702:28 191-24-2
i Benzouguluoranthene NO uga SO 1 08108/1710:00 0811011702:28 207-089 '.
j 4 Bromophenylphenyl ether NO ug/L 50 1 08108/1710:00 081f011702:2B 101-55-3 '..
Bulyhenzylphthalate NO ug/L 5.0 1 08/08/1710:00 hot 0/170228 85-687 '..
# 4-Chlon,3 methylphenal NO upt- 5.0 1 0810811710'00 0811011702:28 59-507
s
l bis(2-CMercelhoxy)methane NO offer- 10.0 i 0810811710:00 08/10/1702;28 111-91-1
bis(2Chloroethyl)ether NO ug1L 50 1 OW081171000 0811011702:28 111-44-4
2-Chloronapichalene NO MIL 50 1 0810811710.00 0811011702:28 91-58-7
2-Chloophenol NO ago- 50 1 0810811710,00 081401170228 95-57-8
4-CMoraphenylphenyl ether NO ug4 5.0 1 0810811710:00 0811011702:28 7005-72-3
Chrysene NO urge- So 1 08108/1710'00 0811011702'28 218-01-9
` Dibenz(ah)anthracene NO ad- 5.0 1 (MANY1710:00 unit Oil 702:28 53-70-3
1,3Dichlorobenzene NO ug/L 5.0 1 08/08117 TTW 0811011702'.28 541-731
LA DicMombeenae NO hall- 50 1 0810811710:00 PAT Off 702:28 10646-7
3,3-Dichlonfl enzidine NO hall 250 1 08/081171000 08/1011702:28 91-94-1
3 2,4-Dirseoraphenal NO ug/L SO 1 08108/1710'.00 0811011702'28 120-832
Dielhyiphthalate NO ug1L SO 1 0810811710:00 08110117 02 28 84-66-2
2,4-Dimelardlenol ND ugfL 10.0 1 08M811710:00 0811011702:28 105-67-9
REPORT OF LABORATORY ANALYSIS
This sport shall not he reproduced,except in full,
s Ddc¢08122/201710:12 AM w4hout the wnaen concern of Pare Analytical services,uc Page 38 of in
i
1

Pace Analytical SeMces,LLC
NC
aeeAa80cal A 2225 Riverside Dar
shevipe,NC 2a80404
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ANALYTICAL RESULTS
j Project Low&Boner Inc1210140
# Pace Project No.: 92350243
3 Sample: East Ditch LablDe 92360243010 Collected: 08102/1717:00 Received: 08103/1716'47 Mahix Waled
l
Parameters Resuiis Units Repod Limit OF Prepared Analyzed CAS No, Qual
+ 626 MSSV Analytical Method:EPA 625 Preparation Method.EPA625
j Dimethylphlhilate ND ug/L 5.0 1 081081171000 08110/1702:28 131-11-3
Di-n-butyiphihalate ND ug1L 5.0 1 08108117 10:00 08/1011702:28 84-74-2
4,6 141111ro-2-melh ighnnnol NO uglL 20.0 1 0810811710:00 081101170228 534-52-1
- 24 Oinitrophenal NO dill 500 1 08108/17 10 00 OW fill 702'28 51-28-5
2.4-trinitrotoluene NO ugdL fro 1 OB/08/1710:00 0&i 0/1702:28 121-14-2
2,6-Dirnaloluene NO uglL 5.0 1 08108/1710:00 O1102:28 606-20-2
j Di-n-octylphthalate NO ugal fro 1 081081171000 08/1011702:28 11784-0
1,2-Dipheny1hydrazine ND uglL 5.0 1 (pool 10 00 0811011702:28 122-66-7
bis(2-Ethyihexyl)phthalale ND ugA- 50 1 0810811710:00 0811011702:28 117-81-7
s Fluoranlhene NO upl. 5.0 1 0810811710:00 08110/1702:28 206-440
Huorene NO uglL &0 1 (diffi 171000 poll got 70228 86-73-7
i Heochioro-1.3 brothers NO fig& 5D 1 08108/171000 grant fill 702:28 87-68-3
Hexaehlorobenzeoe NO ugll 5.0 1 08/08/1710:00 0811011702:28 118-74-1
Hexachlorocyclopentadiene ND dg/l 10.0 1 08/0811710:00 08/1011702:28 7747A
Hexachloroelhane ND ugnL 5.0 1 0810811740:00 0W101170228 67-72-1
indeno(1,2,3 Whymne ND ug/L 50 1 0810811710:00 0811011702:28 193-39-5
isophorone NO uglL 100 1 08108/171000 O8/1 fill 702:28 78-59-1
_ 3&4-Methylphenol(m&p Cresol) ND dill 100 1 08/08/171000 0811011702:28 15831-40-4
`aphlhalene NO aid- 5A 1 08/08117 10 00 0811011702:28 91-20-3
9ilrobenzens NO fig/L 5.0 1 08108/1710,00 0811011702:28 98-95-3
2-Nilrophenoi NO find- 5.0 1 08108/1710:00 08/1011702:28 88-75-5
- 4-Nilrophenoi ND ug/L 501 1 0810811710:00 0811011702:28 10002-7
N Nitersodimelhylamine ND ug11- 5.0 1 08/0811710:00 OW1011702:28 62-95-9
N Nilroso-di-n-propylamine NO upl- fro 1 0810811710:00 0811011702:28 621-64-7
N Nilrosodiphenylamine NO dill 100 4 0810811710,00 OB/1011702:28 86-30-6
2,2'Oxybie(1-chlowpropane) NO dill 50 1 0810811710:00 08/10117 02 28 108-60-1
y Penlachldephenol NO ug/L 10.0 1 0810811710,00 0811011702:28 87-86-5
Phenanthrene NO dill 5.0 1 0810811710:00 0811011702:28 85-01-8
Phenol NO Land- 50 1 08108/1710:00 0all702:28 108-95-2
Physics ND dial 5.0 1 081081171000 all 02:28 129000
1,2,4-Trichlorobenzene ND ug/L 5.0 1 0810814710:00 0N1011702'28 120-82-1
2,4,6-Trichiomplat NO uglL W.0 1 0810811710:00 0811011702:28 88-06-2
Surrogates
Nitraheneane-d5(S) 60 % 10-120 1 08108/171000 08110117 02 28 416560-0
2-Ff.dethiphenyl(S) 59 % 15-420 1 0810811710,00 08/101170228 321-60-8
Terphenyl did(S) 53 % 11-131 1 0808/1710,00 08110117 02 28 1718-51-0
Phenol off 22 % 10-120 1 0810811710:00 08/1011702:28 13127-88-3
2-Fluorophenol(S) 32 % 10-120 1 08/0811710:00 0811011702:28 367-12-4
3 2,4,6-Tdbromophenol(S) 68 % 10-137 1 08/08/1710:00 0811011702:28 118-79-6 '..
624 Volatile Organics Analylioai Method:EPA624
j Acralien NO uglL 50 1 08/08/1722:48 107-02-8 L1,Mo
Acrylarlble NO unlL 500 1 081081172248 107-13-1
Benzene NO dill 2.0 1 0810811722:48 71-43-2 -
j Bmmoeichloronoth rn, NO dill 2D 1 08/0814722:48 75-27-4
Bromol0on NO dgh- 20 1 0810811722:48 75-25-2
Bromomelhane ND dgll 2.0 1 0810811722:48 74-83-9
y
7 REPORT OF LABORATORY ANALYSIS
1 This repot shall not No reproduced,except in fall.
1 Date:O8i222/20t]10.12 AM wimow he lenit coneem of Pace Analytical Scov. ,LLC Page 39 of 96

T Pace Analytical Services,LLO
zazs eraraae Of aceAnalytical Ashosine.NC 28804
hHwJeSxavn Ie281254a176
i
a ANALYTICAL RESULTS
Project: Lrnv&BomP Inc 1210140
Pace Project No, 92350243
j Sample: East Ditch Lti 92350243010 Collected: 0810211717:TO Received 08103117 1647 Matrix'Water
' Parameters Results Units Roper!Limit OF Prepared Anrlyzed CAS No. Qual
3 s
624 Volatile Organics Analytical Method:EPA 624
Carbon tetrachl®ritle ND ug/L 2B 1 0810811722:48 6623-5
- Chlombenzene NO ugal 2.0 1 08108/172248 108-90-7
Chloroethane NO ug/L 2D 1 08/08/1722A8 7500-3
-j Chloroform ND ug/L 20 1 08/081172248 67-66-3
- Chlommelhane NO rill- 20 1 0810811722:48 7487-3
i Dihromochloromethane ND ug/L 20 1 0WON172248 124-48-1
j 1,2-Dichlombenzene NO ug/L 20 1 08/08/1722:48 95-50-1
1.3 Dichlormhenzene ND ug/l 2A 1 Oought 722:48 541-731
Lal-Dichlombenzene NOT ugh- 2.0 1 G81081172248 106-46-7
1,1-Diohioroethane NO ugh- 2.0 1 08/0811722A8 75-34-3
( 1,2-Dichlofoethane NO rill- 2.0 1 0810811722:48 107-06-2
IJ-Dichloroelhene NO rill- 2.0 1 0810811722:48 75-35y
- cis4,2-0ichioroethene ND ug/L 20 1 081OW1722'48 156-59�2
- transl,2Dichlomethene NO ug/L 20 1 08/0811722:48 156-60-5
1.2-Dichlompropane NO offal 2B 1 08108/1722'48 78-87-5
ds-L3 Diohlompropene NO ugi 2.0 1 08/08/172248 10061-01-5
trans-l.3-Dichlaroprmpene NO rglL 2.0 1 08I08/172248 10061-02-6
Ethylbenzene ND ug/L 2.0 1 0810811722:48 100-01-4
jemyiene Chloride ND rill- 2S 1 ON0811722:48 7509-2
S ',1,2,2-Tehachlormethane NO opt, 20 1 08/0811722:48 79-34-5
I Tetrachlomelhene NO ug/L 20 1 08/0811722'48 127�18.4
Toluene NO ui 2.0 1 0810811722'48 108-88-3
1,1.1-Tdchlmroithane ND ug4 2D 1 08108/172248 71-556
1,1,2-Tnchlmirmthane ND uglL 20 1 08/08117 22 48 79-00-5
- Trichl usamene NO rill- 2B 1 0810811722:48 79-01-6
i Trichlorogummuremane NO ug1L 2.0 1 D81081172248 75.69-4
Vinyl chloride NO mill- 2.0 1 0810811722'48 7501-4
Surrogates
4-Bromo(luorobenzene(8) 103 % 70-130 1 0810811722:48 460-00-4
Toluene 18(S) 111 % 70-130 1 08108/1722:48 2037-26-5
i 1,2-Dichloroemane off(SO 87 % 70.130 1 081081172248 1706007-0
I
3540C Total Dissolved Solids Analytical Method:SM 2540C
i
- Total Dissoivetl Solitls 73.0 mill- 25.0 i OB/OBIT]0941
25400 Total Suspended Solids Analytical Method:SM 2540D
Total Suspended Solids NO mg/L 30 1 08/0811713'50
Total Nitrogen Calculation Analytical Method TKN+NO3+NO2 Calculation
I
- Total Nitrogen 1.3 mill 0.12 1 0810911718:11
j 350.1 Ammonia Analytical Method:EPA 350.11993 Rev 20
Nitrogen,Ammonia 0.44 mglL 0,10 1 081091170509 7664-41-7
361.2 Total Kpidahl Nitrogen Analytical Method:EPA 351.2
1
Nitrogen,Kjeltlahl,Total 1.1 mill- 050 1 08109/1717:07 7727-37-9
REPORT OF LABORATORY ANALYSIS
I This room shall not be repmtluceQ except in full.
[] Date:0812 212 017 10:12 AM -then me corium consent of Pace Analytical sh,oee.LLC Page 40 of 96
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I Pace Analytical Services,LLC
aceAn lXtcal® A 2R5aFevAls. 04
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ANALYTICAL RESULTS
Project Loi Boner Inc 1210140
1 Pace Project No.: 92350243
Sample: East Ditch Lab ID: 92360243010 Collected: 08102/1717:00 Received: 081031171&47 Matrix:Water
I
Parameters Results Units Report Limit OF Prepared Analysed CAS No. Goal
i
_t 353.2 Nitrogen,N021NO3 pros. Analytical Method:EPA 353.2
Nitrogen,NO2 plus NO3 0.19 mg/L 0020 1 08/09117 12 20
1 366.1 Phosphorus,Total Analytical Method:EPA365.1
Phosphorus 0.58 mg/L 0.050 1 0811011706:40 7723-14-0
5220D COD Analytical Method:SM 5220D
Chemical Oxygen Demand ND Tagil- 250 1 08/0711718:41
Sample: City Water Lab IO: 92350243011 Collected 0810211713:32 Received: 0810311716'47 Matrix:Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Coal
HEM,Oil and Grease Analy8ca1 Method:EPA 1664B
} Oil and Grease NO might. 50 1 08/17117 05:12
200.7 MET Ella Analytical Method EPA2007 Preparation Method:EPA 200.7
Antimony ND uglL 5.0 4 0811311722:05 08115/1703:29 7440-36-0
;d'aenlc ND ug/L 10.0 1 011311722:05 081151170329 7440-36-2
Beryllium NO uglL 10 1 08113/1722:05 08/1511703:29 7440-41-7
Cadmium NO ug/L 10 1 08/13/172205 0811511703:29 7441L43-9
Chromium NO O91L 50 1 08113/1722:05 08115/1703:29 7441147-3
Copper NO ug/L SO 1 08M311722,05 0811511703:29 7440-hit 8
a Lead NO ugl 50 1 08113/1722:05 OW15R703:29 7439.92-1
Molybdenum NO ug/L SO 1 0811311722:05 08/1511703:29 7439-98-7
Nickel NO 0i 5.0 4 0811311722:05 0811511703:29 7440-02-0
Selenium NO uglL 10.0 1 0811311722:05 08115117 03 29 7782-49-2
Silver ND uglL 50 1 08113/172205 0811511703'29 7440-22-4
Thallium NO Tied- 10.0 1 0811311722:05 0811 AM70329 7440-28-0
1 Hardness,TOtal(SM 2340B) 5470 ugd- 662 1 08113/172205 OW1511703:29
- Zinc 210 ug/L 100 1 081131172205 Not 5117 03 29 7440-65-6
245.1 Mercury Analytical Methotl:EPA 245.1 Preparation Method,EPA 245.1
3
Mercury ND ugiL 020 i 08/09/1705:35 08111/170043 7439-97E
1 625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
t
Acenephthene ND ug/L 5.0 1 08108/1710:W 0et 011708:34 83-32-9
] Acenaphlhylene NO uglL 50 1 08108/171000 08/10/170834 208-96-8
Anlhracene NO upt- 50 1 08108/I71000 0WOR70834 120-12-7
- Brorxid )anthrecene NO uq/L 5.0 1 0810811710,00 0911011708:34 56-55-3
J eenzoOdpyrene NO ug/L 5.0 1 0810811710:00 OWIOI1708:34 50-32-8
Benzo(b)hmahlhene NO ug1L SO 1 08108/1710:00 0811011708:34 205-99-2 '..
Bere,fuhh,i)perylene NO ugd- 5.0 1 08108/1710:00 0811011708:Set 191-24.2
j Ben T,thfiuoranlhene ND ug1L 5.0 1 08/0811710:00 0811011708:34 207-98 9
4-Bromophenyiphenyl ether NO ug/L 50 1 08/0811710'00 08110/1708:34 101-55-3
Butymenzylphoclale NO, ue/L 50 1 0810811710:00 08110117 08 34 8568-7
' REPORT OF LABORATORY ANALYSIS
j This repot shell not 6u repmtluced except in lull,
Date:0812212017 10:12 AM without the chose mnecni of Pace Analytical Services,LLC Page 41 of 96

Pace analytical Services.LlC
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I ANALYTICAL RESULTS
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- Project: low 8 Donar Inc 1210140
{ Paw Project No. 92350243
Sample: City Water Lab ID: 92350243011 Collected 08102/17 13:32 Revived: 0810311716:47 Matrix:Water
Parameters Results umts Report Limit OF Prepared Analyzed CAS No, Qual
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA625
4-Chlom-3-methylphenol ND u9/1 5D 1 08/08/1710,00 08/1011708:34 59-50-7
bis(2-Chloroethoxy)memane ND ug/L 100 1 0810811710:00 08110117 08:34 111-91-1
- bis(2-Chloroelhyl)ether NO ug1L 5D 1 08/08/17 10:00 08140117 08:34 111444
2-Chlormigifihalene NO ug1L 5.0 1 08/08/17 10:D0 08110/17 08:34 91-58-7
2-Chlorophenol NO ug/L 5.0 1 0810811710:00 0IN0/1708:34 95-57-8
4-Chlorophenylphenyl ether ND ug/L 5.0 1 0810811710:00 DWI Oil 708:34 7005-72-3
Chrysini NO ug/L 5.0 1 0810811710.00 08/10117 08 34 218-01-9
Dibenz(a,h)anthrawne ND ug/L 50 1 08/08/17 IODO OW10117 OB 34 53-70-3
1,3-Dic1,lorobenzene ND uglL 5D 1 08108/1710.00 08110117 08:34 54b73-1
1A Dichlorobefrzene NO ug1L 5.0 1 08/08117 10:00 08/10117 08:34 108.16 7
3.3'-Dichimobenzidine NO ug/L 25.0 1 0810811710:00 08/10117 08:34 91-94-1
- 2,4-Dichlorophenol NO ug/L 5.0 1 08108/1710:00 OW1011708:34 12083-2
Diethylphthalate NO ug1L 5.0 1 08/08/17 10'00 08110/17 08'34 84-66 2
2.4 Dimethyiphenol NO uglL 10.0 1 0810811710:00 0811011708:34 105-67-9
Dimethylphthalate NO ug/L 5D 1 08/08/17 10:00 08/1 fill 7 08:34 131-11-3
Di-a butylphthalate NO ug/L 50 1 08108/17 10DO O8/10117 08:34 84-74-2
4,6-Dinilro-2-methylpheno1 ND ug/L 20D 1 08108/1710:00 08110I170834 534-52-i
2,4-Dinitrophenol NO ugA- 50D 1 081081171000 08110117 08:34 51-28-5
'4-DinitrotoWene NO ug1L 5D 1 08/08/17 10:00 08110117 08:34 121-14-2
15-DiNtrot.hone NO uglL 50 1 08/08/1710:00 0811011708:34 606-20-2
Di-n-octylphthalate NO ug/L 5.0 1 OB/08117 10:00 08/10117 08:34 117-84-0
1,2-Diphenylhydrazine NO uglL 5.0 1 08/08/17 10:00 08110/17 08:34 122-66-7
bisM-Elhylhexy0phthalate NO ug/L 5.0 1 08108/1710:00 0811011708:34 11781-7
3 Fluoranthene NO uPh 50 1 08108117 10 00 0811011708:34 206-440
j Floored ND ug1L 5.0 1 08108/17 1000 08110117 08 34 86-73-7
j( Hexachloro-13buladlene NO ug/L 50 1 0810811710:00 08110/17 08 34 87-68-3
3 Hexachloroben¢ene ND ug/L 5A 1 081D81171000 013/1011708:34 118-741
3 HexachlorocyGopentadiene NO ug1L 10D 1 08/08117 10:00 0a/t Olt 7 08:34 77-47-4
1 Hexachloroethane NO ug/L 5D 1 08/08117 10:00 08110/17 08:34 67-72-1
Inden0(1,2,3-W)pyrena NO ugl 5.0 1 08/08/17 10,00 08110/17 08 M 193-39 5
Isophomne NO M/L ION 1 0810811710:00 0811011708:34 78-59-1
384-Methylphenol(m&p Cresol) NO uglL 10D 1 081081171000 0811011708:34 15831-10-4
# Naphthalene NO ugd- 5.0 1 08/0811710,00 0811011708:34 91-20-3
Nitrobenzene NO ug/L 5.0 1 081081171000 08/1011708:34 98-963
2-Nitrapheno1 NO ugn. 50 1 081011710,00 081101170834 88-75-5
4 Nitrophenol ND ug/L 500 1 0B108/1710,00 080 fill 708:34 100-02-7
N-Nihosodimethylamine ND ug/L 50 1 08/081171000 08/10ff 708:34 62-75-9
E N-Nitroso chI-propylamine NO ugl 5D 1 08/08117 10:00 08/10/17 08'34 621-64-7
tt' N-Nitrosodiphenylamine NO ug1L 10D 1 08108/17 10,00 08110117 08,34 86-30-6
t 2,2'-O,bls(1-chlompr0pane) NO ugh- 5D 1 08108117 10 00 0811014708:34 10880.1
3 Pentachiorophenol NO ug/L 10.0 1 08/08117 10 00 08110/17 08:34 87-86-5
j Phenanthrene NO ug1L 5D 1 0810811710:00 08110117 08:34 8501-8
Phenol ND ug/L fro 1 08108117 10 00 0811011708'34 108-95-2
Pyrene NO rMIL 5.0 1 081081171000 ON1011708.34 129-000
1,2A Tdchlombenzene ND ugh. 50 1 08108/1710DO 0811 Off 7 08 34 120-82-1
1 2,4,6-Trich1orophenol ND ug/L 100 4 0810811710,00 08/1011708:34 8806-2
- 1
REPORT OF LABORATORY ANALYSIS
This report shall not be repmtluwq except in full.
Date:08122I201710:12 AM without the—O.aconeentof Pace Analytical 5e1mas,LLC Page 42 of 96
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Project: Low&Sonar Inc 1210140
Pace Project No.: 92350243
Sample: City Water Lab10: 92350243011 Collected: 08/02117 13 32 Received: 0810 311 7 16:47 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method EPA 625 Preparation Method EPA625
Surrogates
Nitrobenzene-d5(S) 63 % 10-120 1 0810811710:00 08110/170934 4165-600
2-Fluombiphenyl(S) 63 % 1S120 1 08/08/17 ISM 0811014708:34 321-60-8
,. Eophenyid14(5) 61 % 11-131 1 08/O1/1710:00 0811011708:34 1718-510
Phenol-d6(S) 17 % 10-120 4 08108/171000 OW1011708:34 13127-88-3
3 2-Fluomphenol(S) 31 % 10-120 1 08108117 10 00 Plot 0/170834 367-12-4
i 2,4,6-Tribom ichenoi(S) 67 % 10137 1 08108117 TDA0 081101170834 118-79-6
3
$24 Volatile Organics Analytical Method:EPA624
)
Acralein NO ug& 5.0 1 0810911701:28 107-02-8 Li
Acrylooiidle NO ug1L 500 1 0810911701:28 107-13-1
i Benzene NO ug/L 20 1 08109117 01 28 71A32
£ Broundichloromeihane 2.8 mill- 20 1 081091170128 ]52]-4
Brommorm NO u911 2D 1 08/09/170128 75-25-2
Bromome(hane NO ug/L 2B 1 081091170128 74-83-9
Carbon househlold. NO dig/- 2B 1 OWO911701:28 56-23-5
{ Chlorobenzene NO ug/L 2S 1 0810911701:28 108-90-7
Chlannounce NO one- 20 1 0810911701:28 75003
' hlomform 19.5 mill- 20 1 0810911701:28 67-66-3
E;Horomethane NO mill- 2.0 1 Tell 70128 ]4-8]-3
_ Dibromochloromethane NO mill- 20 1 08/09/170128 124-48-1
1,2-Oichlorobervene NO ug1L 20 1 08/0911101:28 95501
1,3-Dichlorobermene NO ug/L 20 1 OW091170128 541-731
1,4-Dichlombenzene NO died- 20 1 08/l704:28 108467
1,1-Dichloroelhane NO ugLL 2S 1 G8109117 04 28 75-34-3
' 1,244chioroelhane ND ug/L 2S 1 08I09117 01:28 107-062
IJ-Didtloroelhene NO ugA- 2B 1 0BI0911101:28 75-35-4
j cic-1,2-Diahlomethen, NO u91L 2S 1 081091170128 156592
Trans-1.2-Dichlomethene NO mill- 20 1 ON0911701:28 156-60-5
1.2-DichImam pane NO dig/L 20 1 08/091170128 ]88]-5
ds-1,3 Dichlompropene NO ug/L 20 1 OW0911701,28 10061-01-5
trans-1,3-Dichloroprapene NO ugh 20 1 0810911701:28 10001-02-6
3 Ethyllmor ne NO ug/L 2B 1 08/09/170128 10041-4
Methylene Chloride ND ugdL 2B 1 08109117 01:28 75-09-2
1,1.2,2-Tetrachioroelhane NO ug/L 20 1 08/0911701:28 79-34-5
Tetrachloroelhene NO dig& 2.0 1 0810911701:28 127-184
- Toluene NO uge- 20 1 08109/170128 108-88-3
{ 1,1,1-TricNoroe1hane NO ug/L 20 1 0810911701'28 71-556
1 L1,2-Trolsoroethane NO uglL 20 1 081091170128 79-00-5
Oichlisondhene NO uglL 20 1 081091170128 79-016
{ Trichloro0uoromerane NO died- 2.0 1 integral 701:28 75694
3 Vinyl chloride NO ugh- 2.0 1 08109/1]0128 ]S-OIA
Surrogates
4-Bromo0uorobenzene(5) 104 % 70-130 1 08109117 01 28 460004
Toluene-08(S) 108 % 70-130 1 0810911701:28 2037-26-5
1,2-Dichlomelhane-d4(S) 91 % 10-130 1 08dd1701:28 1706007-0
j REPORT OF LABORATORY ANALYSIS
Thls report shan not re reproduces,ex Pt in full,
Dale:08/22/201710:12 AM without de wrnten consam of Pace Analytical Services,LLC. Page 43 of 9&
7
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ANALYTICAL RESULTS
Project: Low&Banar Inc 1240140
Pace Project No.: 92350243
Sample: City Water Lab ID: 92350243011 Collected 0810211713:32 Received: 08/0311716'47 Manx:Water
7
Parameters Results Units Repot Limit OF Prepared Analyzed CAS No, Quid
2540C Total Dissolved Solids Analytical Method:SM 2540C
-j Total Dissolved Solids 36.0 mglL 25D 1 081081170941
2540D Total Suspended Solids Analytical Method:SM 2540D
1
`I Total Suspentletl Sofltls ND Tend- 25 1 08IO8117 13:50
Total Nitrogen Calculation Analytical Method:TKN+NO3+NO2 Calculation
Total Nitrogen NO Tend- 0,12 1 08/09/17 18:11
350.1 Ammonia Analytical Method:EPA350.1 1993 Rev 2.0
t
Nitrogen,Ammonia NO mg4 0.10 1 08109l17 05:10 ]66441-]
351.2 Total Kjeltlahl Nitrogen Anelylicel Method:EPA 351.2
Nitrogen,Kjeltlahl,Total NO mglL 0.50 1 0810911717'08 7]27-3]-9
I
` 353.2 Nitrogen,N021NO3 pres. Analytical Method:EPA 353.2
Nitrogen.NO2 plus NO3 Lo54 Tend- 0020 1 08109117 12 21
- -.366.1 Phosphorus,Total Analytical Method:EPA365.1
-.,vhruphorus 0.58 mg/L 0.050 1 OW101170640 ]]2314-0
5220D COD Analytical Method:SM 5220D
j Chemical Oxygen Demand ND mg/L 25D 1 08/07/1718:41
1
t
j Sample: Manhole 3 LabiD: 92360243012 Collected: 081021171410 Received: 081031171647 Matrix:Water
Parameters Results Units Repot Limit DF Prepared Analyzed CAS No. Coal
3
{ HEM,Oil and Grease Analytical Method:EPA 16648
Oil and Grease NO mg4 So 1 OW17/1705:13
{ 200.7 MET ICP Analytical Method:EPA 200] Preparation Method:EPA 200.7
Antimony ND ugl- 5T 1 0811311722:05 0811511703:32 7440-36-0
Arsenic NO ago- 10.0 1 0811311722:05 0811511703:32 7440-38-2
Beryllium ND ug4 1.0 1 0811311722:05 0811511703:32 ]440-41-]
Cadmium NO ug/L 10 1 08/1311722:05 08/15117 03 32 7440-43-9
Chromium ND ug/L 50 1 0611311722:05 0811511703'32 ]440-4]-3
Copper 19.6 ug1L 5.0 1 0811311722:05 0805/170332 7440-50-8
Lead NO uga- 5D 1 0811311722:05 081191703,32 743992-1
Molybdenum 291 .,at 5.0 1 0811311722:05 0811511703:32 ]439-98]
-1 Nickel NO upl- 5A 1 0811311722:05 0811511703,32 7440-02-0
Selenium NO ug/L 10.0 1 0811311722:05 08116/1703:32 ]]82-49-2
Silver ND ugdL 5.0 1 081131U 2205 OW1511703:32 7440-22-4
- Thallium ND ugh- 100 1 08/131172205 OW1511703:32 7440-28-0
Hardness,Total(SM 23 OB) 17400 agdL 662 1 08113/17 22'.05 08/15/17 03:32
t
REPORT OF LABORATORY ANALYSIS
i This report shall not be mpmtluw4 except In 1.51, '..
Date:0812212017 10:12AM without the wnneoconcentof Pace Analy6cel Sences,LLc. Page 44 of 96
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3

Pace Analythel6ervices,LLC
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ANALYTICAL RESULTS
I i Project Low&Boner Inc 1210140
Pace Project No.: 92350243
Sample: Manhole Lab ID: 92350243012 Collected: hill 714:10 Received: OW0311716'47 Matrix',Water
Parameters Results units Report Limit OF Prepared Analyzed CAS No. Qual
( 200.7 MET ICP Analytical Method:EPA 200.7 Preparation Method:EPA 200.7
3 Zinc 416 ug5 10.0 1 08113/1722:05 0811511703:32 7440666
3 245.1 Mercury Analytical Method:EPA245.1 Preparation Method:EPA245.1
r Mercury NO ug/L 0.20 1 0810911705:35 OArl Ill 700'45 7439&97-6
625 MSSY Analytical Method:EPA625 Preparation Aleihod:EPA625
Acenaphthene NO mall 5.0 1 08/0814710SO 08110117 03 25 83-32-9
Acenaphthylene NO ug/L 5.0 1 0810811710:00 08/101170325 208-96-8
Anteroom, NO uglL IS 1 081081171000 ON10/1703:25 120-12-7
Benzopeanlhracene NO ug/L 50 1 0810811710:00 08/1011703:25 5655-3
a Benzo(a)pyrene NO ug5 50 1 0810811710:00 08e10/170325 50-32-8
Senzo(Oflumanlhene ND ug5 5.0 1 08108/1710:00 (pi 03:25 205-99-2
Benzo(g,h,i)perylene ND uglL 5.0 1 0810811710:00 0811011703:25 191-24-2
Bearsehalluoranihene NO ug/L 5.0 1 08108/171000 08/1011703:25 207-08-9
4 Bromophenylphenyl ether NO hall- 5.0 1 0810811710:00 OW1011703:25 101-55-3
Buryibenzylphthalate NO ug/L 5.0 1 08/081171000 08/10/1703:25 8568-7
j 4-Chlom-3-methylphenol NO Inge- 50 1 0810811710:00 08110117 03 25 59-50-7
j ble(2-Chiomethexy)methane NO ug1L 10A 1 0810811710:00 Ofel 0/1703:25 111-91-1
a(2-Chloroethy0 ether ND ug5 5'0 1 08110:00 08110/1703:25 111-44-4
2-Chlommaphlhalene ND ug5 6P 1 08/08/17 When 0 811014 7 03:25 91-587
2 Chiomphenol NO ug/L 5.0 1 0810811710'00 08110/1703'25 95-57-8
t 4 Chiorophenytphenyl ether NO ball 5.0 1 08108/171000 0811011703'25 701
Chrysene NO Still- 50 1 081081171000 08/10/1703:25 218-01-9
Dibenz(a,h)anthracene NO uglL 5.0 1 08/08/1710:00 0811011703:25 53-70-3
-_ LlLDichlopmenzene NO ugh- 5.0 1 08/0811710:00 08110117 03 25 541-73-1
14 DICMOfObenzene NO no& 50 1 08/0811710:00 0811011703:25 40646-7
1 3,T-Dichlonmenzidine ND ug5 250 1 08/08/1710:00 0811011703:25 91-94-1
2,4-Dichiorophenoi ND ug/L 5'0 1 0810811710:00 08/10/1703:25 120-83-2
} Olethylphlhaiate NO mill- 5.0 1 08/0811710:00 0811011703:25 84-66-2
2,4-Dimelhylphenol NO ug/L 10.0 1 081081171000 0811011703:25 105-67-9
Dimethylphlhalate NO Ina/L 50 1 0810811710:00 08110/1703'25 131-11-3
Or n-bNyiphthalate NO ug/L 50 1 0810811710,00 0W1011703'25 84-74-2
4,6-Dinitro-2-methylphenol NO ug1L 200 1 0810811710:00 0WIOI1703:25 534-52-1
2.4 Dinhrophenol NO ug1L 50.0 1 08108/1710:00 08110117 03 25 51-28-5
2A Dinewtoluene ND ug5 50 1 0810811710:GO 0811011703:25 121-14-2
t
2,6-Diniftmoluene NO ug11- 50 1 081081'1710:00 0811011703:25 606-20-2
On aclylphthalate NO hpL 5,0 1 08I0811710:00 0811011703'25 117-84-0
1,2-Dipheny1hydrazine NO ug/L 5.0 1 081081171000 0811011]03'25 122 66-7
bis(2-Efhy1hmcyhphh I.P NO IN& 50 1 0810811710,00 08110/170325 117-81-7
Fluoranthene NO ug/L 50 1 081081171000 0811011703:25 206-44-0
Floorene ND ug5 5.0 1 0810811710:00 08110117 03 25 86-73-7 '..
Hexachlom-1.3-lam diene ND ug5 50 1 081080710:00 OB11011703:25 87-68-3
Hexachlorobenzene NO ua1L 5.0 1 0810811710:GO 0811011703:25 118-74-1
Hexachiorocyclopentadiene NO ug5 IL0 1 08/08/1710:00 08/1011703:25 77-47-4
Hexachtomethane NO uglL 5.0 1 (NIANY1710:00 08110/1703:25 67-72-1
Indmm(1,2.3 Opp,arm NO ugo- 5.0 1 08108117 10 00 0811011703:25 193-395
i
REPORT OF LABORATORY ANALYSIS
t
This report sham net 6e repmeucem,exaevt in rum,
Date:0812 212 017 10:12 AM wine.,the"een consent of Pace Antirecal Services,LLG Page 45 of 96
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Pace Analytical3ervices,LLC
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ANALYTICAL RESULTS
? Project Law&Bomar Inc 1210140
t Pace Project No.: 92350243
Sample: Manhole Lab1D: 92350243012 Collected 08/02/1714:10 Received: 08/0311716:47 Matrix Wale,
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual
625 MSSV Analytical Method:EPA625 Preparation Method:EPA 625
Dophomne NO ug/L 10.0 1 08108/17 Wig 08110/17 03 25 78-59-1
_ 3&4-Methylphmmdm&p Cresol) ND milt 10.0 1 08108I17 10:00 0811011703:25 15831-10-4
Naphthalene NO ug1L SO 1 0810811710:00 0811011703:25 91-20-3
Nitrobenzene ND u9/1- 5.0 1 081081171000 OW1011703'25 98-953
2-NOrophenal ND u91L 5.0 1 0810811710:00 08110117 03 25 8875-5
1 4-Nitrophenoi ND reglL 50B 1 08/0811710,00 0811011703:26 100-02-7
N NihosodimeNylamins ND Tge- 50 1 0810811710:00 0811011703:25 62-75-9
N-Nitroso of mpropylamine ND ug/L 5.0 1 W10811710:00 08110/1703:25 621-64-7
N-Nitersodipheny dame ND TgA- 10B 1 08I08117 food 08110/1703:25 86-306
2,2'-Oxybis(i-chloropropmed NO ugll- fro 1 0810811710:00 OB/1 Oil 703:25 108-60-1
= Pentachlorophenol NO ug/1 10.0 1 08/081171000 OW1011703:25 87-86-5
Phenanthren, ND mill- 50 1 08108117 10 00 08110/17 03 25 8501-8
Phenol ND hill- 50 1 0810811710,00 08110/1703:25 108-95-2
r Pyrene NO Tgd- AT) 1 0810811710:00 08110/1703:25 129000
7 1,2,4-Trichloomenzene ND TOIL 5B 1 0810811710:00 08140/170325 120-82-1
7 2,4,6-Tdchloreephenoi ND TgI 10.0 1 0810811710:00 0811011703:25 8806-2
Surrogates
Nitrobenzene-d5(S) 60 % 10-120 1 0810811710:00 0811011703:25 4165-600
` Fam obiphenyl(S) W % 15-120 1 08JO811710 00 OB/1 Oil?03:25 321-60-8
j 2rphenyhd14 Nd 53 % 11-131 1 081081171000 08110117 03 25 1718-51-0
j Phenol-d6(S) 25 % 10-120 1 0810811710'.00 08110/1703'25 13127 88-3
2-Firaropheno1(S) 34 % 16120 1 08/08/1710,00 0811011703:25 367-124
j 2,4,6-Tdbromophenoi(S) 75 % 10-137 1 08/0811710:00 0811011703:26 118-79-6
s
! 624 Volatile Organics Analytical Method:EPA 624
Acralein ND milt 5.0 1 08I0811723:06 107-02-8 Li
$ Acrylonilnle NO ug/L 50-0 1 081OW1723:06 407-13-1
Benzene NO ug/L 20 1 0&0811723:06 71-43-2
Bromodichlommelhane NO fed- 2.0 1 0810811723'00 75-27-4
Bromoform ND hilt 2,0 1 08/08/17 23:05 75 26 2
I Brournmed are NO Tgd- 20 1 OBIOW1723:06 7483-9
Carbon tetrachloride ND rig/1 20 1 OBIOW172306 56-23-5
Chlombenzene ND Tg/L 2.0 1 0810811723:06 108-90-7
Chlomethane ND ug/L 2.0 1 08/0811723,06 7500-3
s Chloroform 3.5 TO& 2.0 1 08108/1723:06 6760-3
Chimomethane ND milt- 2.0 1 08/0811723,06 74-87-3
Dibromochloromelhane ND uglL 2.0 1 08/08/l723:06 124-48-1
1,2-Dichiothernzene NO ug/L 2.0 1 0810811723:06 95-50-1
L3-Dichlorabenzene ND ug/L 20 1 08/0811723'06 541-73-1
- to Dichlorabenzene ND Tg1L 20 1 08108N723:06 10646-7
1,1-Dichloroethane ND mid- 20 1 081OW1723:08 7534-3
1,2-Dichloroethane ND old- 20 1 08108/47 23 06 107062
I 1.1-Dichlooethene ND TgIL 2.0 1 08108/1-72306 7535-4
6s-1,2-D1c1ioroethene ND ugh 2.0 1 081081172306 156-592
Irons-1,2-Dichioroethene ND ug/L 2.0 1 0810811723:06 15660-5 '..
1,2-Dichiompropane NO TOOL 2.0 1 0810811723:06 7887-5
cis-1,3 Dichlorepropene NO .,T 2.0 1 081081172306 10061-04-5
7
REPORT OF LABORATORY ANALYSIS
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Date:08/22/201710:12 AM munccul the wbmen hosenlor Pace Analytmel 6ervkei LLC Page 46 of 96
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Pace Anal6cal Services,LLC
aceAnaly tcal e 225 Hsbeville,NC,NC 28804
'
/ _ wmv{a'a'rvhxrm
(828)26a7116
ANALYTICAL RESULTS
Project: Lmv&Bonar Inc 1210140
Pace Project No.: 92350243
Sample: Manhole Lab ID: 92360243012 Collected 0810211714:10 Received: 0810311716:47 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed GAS N, Qual
624 Volatile Organics Analytical Mother:EPA 624
- bans-1,3 Dichlompropene ND ug1L 20 1 08/0811723:06 10061-02-6
- Ethylbenxene ND ug/L 20 1 09108(172306 100-41-4
j Meihyleoe Chloritle ND ugh- 2.0 1 08108/ 723:06 75-09-2
1,1,2,2-Tetrachlomethane ND uglL 2.0 1 08108/1723:06 79-34-5
Telrachimoethene NO M/L 2.0 1 0810811723:06 127-18-4
Tomme NO ug/L 2.0 1 0810811723:06 108-88-3
1,1,1-Trichlorcelhane ND ug0 20 1 0 ARV1]2306 71-55-6
1,1,2-Trichimoethane NO ug/L 2) 1 081081172306 79-00-5
Tdchloroethene ND had- 2.0 1 0810811723:06 79-01-6
Tnchlorolluoromethane ND ug/L 2.0 1 08/0811123'06 75-694
Vinyl chlorride NO ug/L 20 1 OW0811723t06 75-01-0
Surrogates
4-Brommurimbenzene(A) 101 % 70-130 i 08/08/11230G 46000-4
Toluene-tl8(S) 109 % 70-130 1 081OW1723:06 2037-26-5
1,2-Dicbioroet rruPA4(8) 93 % 70-130 1 08/08117 23 06 17060-07-0
I
2540C Total Dissolved Solids Analytical Method:SM 2540C
Total Dissolved Solids 166 mg1L 25C 1 0Y081170941
s
� '.e540D Total Suspended Solids Arralylical Method:SM 2540D
Total Suspended Solids 2.5 mi 25 1 08108117 13 50
Total Nitrogen Calculation Analytical Method:TKN+NO3+NO2 Calculation
Total Nitrogen 4A mg1L 0,12 1 0810911718'11
350.1 Ammonia Analytical Method:EPA 350A 1993 Rev 2.0
Nitrogen.Ammonia 0.32 mg/L 0.10 1 08109/170512 ]664-41-]
351.2 Total Khaki Nitrogen Analytical Method:EPA 351,2
3
Nitrogen,Keidahl,Total 39 mglL 0.50 i 08109/1]1]:09 ]]2]-3]-9
I
j 353.2 Nitrogen,NO2IN03 pres. Analytical Melhotl:EPA 353.2
Nitrogen,NO2 plus NO3 0.36 RAPT 0,020 1 08109/171224
365.1 Phosphorus,Total Analytical Method:EPA 365A
Phosphoms 2.2 mi 0050 1 08/101170641 ]]23-14-0
52200 COD Analytical Method:SM 5220D
a Chemical Oxygen Demand 72.0 mg/L 250 1 08107/1718:41
3
3
j
REPORT OF LABORATORY ANALYSIS
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(828)2594176
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ANALYTICAL RESULTS
Project: Low&Sonar Inc 1210140
Pace Project No.: 92350243
( Sample: Manhole 3-U Lab ID: 92350243013 Collected 0810211714.29 Receivad. 08/03/17 16 4 7 Matrix:Water
Parameters Results Dole Report Limit DF Prepared! Analyzed CAS No. Goal
HEM,Oil and Grease Analytical Method EPA 16648
1
Oil and Grease ND mglL 5.0 1 08/17I1705'13
200.7 MET ICP Analytical Methotl:EPA 20O7 Preparation Method:EPA 200.7
Antimony NO ugo- 50 1 0811311722,05 0811511703:35 7440-360
Arsenic NO mpL Too 1 08/13/1722:05 08/15117 03 35 7440-38 2
Beryllium ND ug/L 1'0 1 0811311722:05 08115117 03 35 744041-7
Catlmium NO Intl 1.0 1 08/43/1722R5 081151170335 7440-43-9
Chromium NO Ug/L An 1 081131172205 OW1511703:35 7440-47-3
Copper ND ugl- 50 1 0811311722:05 08/15/1703:35 7440-508
Lead ND ugn- 50 1 08/1311722:05 98115M703:35 7439-92-1
- Maibdenum ND ug/L 5.0 1 0811311722:05 0811511703:35 743998-7
Nickel NO uge- 5.0 1 08113/1722:05 08115/170335 744D02-0
1 Selenium ND Ugn- 10.0 1 08113/172205 0811511703:35 7782-49-2
Silver ND Ug/L 5.0 1 081131172205 08/1511703:35 7440-224
Thallium ND ug/L 10.0 1 0811311722:05 0811511703'35 7440-28-0
Hardness,Total(SM 2340B) 46100 uglL 662 1 OW1311722:05 0811511703'35
Zinc ND ugll 10.0 1 08113/1722:06 08115117 03 35 7440.66-6
'45.1 Mercury Analytical Methotl:EPA 245A Preparation Method:EPA 245.1
{ "'Mercury NO ug1L 0.20 1 08109117 05 35 08/1111700:47 7439-97-6
625 MSSV Analytical Methotl:EPA625 Preparation Method:EPA 625
Acenaphthene ND ug/L 50 1 08/08/1710:00 08110117 03 63 83-32-9
Acenaphthylene ND ug1L 5.0 1 0810811710:00 081101170353 208-96-8
Anthracene ND red- 5.0 1 08/08/17 10:0 081TY1703:53 120-12-7
BenzoThanthracene NO uglL 5.0 1 0810811710:00 OW1011703:53 56-55-3
eenema)pyeaus ND uglL 50 1 0810811710,00 08/1011703:53 50-32-8
eenzo(bp1mearnmene ND uglL 50 1 0810811710:00 0811011703:53 205-99-2
Senzo(Thri)perylene ND ugn. 50 1 08/0811710:00 0811011703!53 191-24-2
Benzo(kplumanthene NO ug1L 5.0 1 08108117 10: 0 081401170353 207-089
3 4-Bmmophenylphenyl ether ND ug1L 5.0 1 081081171000 08110/1703:53 101-55-3
Butylbenzylphthalate ND UgIL 5.0 1 08108/171000 0811011703:53 85-68-7
4-Chlom-3 methylphemn NO Ug/L 5E 1 08/081171000 08/1011703'53 5950-7
b1s(2-Chloroethoxy)methane ND uglL 100 1 0810811710:00 08110/1703:53 111-91-1
bis(2-Chlomethyl)ether ND ugA- 50 1 08108/1710:00 0811011703:53 It 444
2-Chloronaphthalene ND ug& 50 1 0810811710:00 081100703:53 91-58-7
2-Chlarophenol NO
add-5.0 1 08/0811710:00 08110117 03 53 95-57-8
3 4Chlomphenylphenyl ether NO Ug/L 5.0 1 06108/17 Won 0811011703:53 7005-72-3
ChrySene NO Ugo- 5.0 1 08/081171000 OW1011703:53 21801-9
Dibenz(a,h)enthracene NO uglL 5.0 1 0810811710:00 08/1011703:53 53-70-3
1,3 Dichtombeaene NO ugh- 50 1 0810811710,00 0811011703'53 541-73-1
1.4-Dichiorobenzene ND mTL 50 i 081OW1710,00 08/101170353 106-46-7
3.3'-Dichiorabenzitline ND ug1L 25.0 1 08/08/1710:00 081101170353 91-94-1
2,4-DichIcemotenol ND ugA 50 1 08/08/1710:00 08110117 03 53 120832
Dfethylphthalate NO ug/L 5.0 1 0810811710:00 08/10M703,53 M 0-2
44-Mme(hyiphenol NO ug1L 10.0 1 08/08117 1000 08/10117 03:53 105-67-9
7 REPORT OF LABORATORY ANALYSIS
t
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Date:08122/201710:12AM vmhout the wdtlen consent of Pace Analy0oei Servic5,LLC- Page 48 of 96
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Pace Analytical Services,LLO
aeeAnalytieal a 2225e,NC 2e 0r
Asheville,NC 28e04
1 renx am D28)2544176
j
ANALYTICAL RESULTS
Project: low&Boom Inc 1210140
i Pace Project No.: 92350243
7
Sample: Manhole 3-U Lab ID: 92350243013 Coliecletl: 08/02117 14:29 Received; p8103/1716'47 Matrix:VJaler
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Goal
625 MSSV Analytical Method:EPA625 Preparation Method:EPA 625
Dimelhyiphlhalete NO ug/l 50 1 08/0811710:00 0811011703.53 131-11-3
Di-n-butyiphlhalate NO ug/L SO 1 0810611710 DO 0811 DO703:53 84-74-2
46-Dinith,2-melhylphenol NO ug/L 20.0 1 0810811710:00 OWIOI1703:53 53452-1
2,4-Dinilo phenol NO DOL 50.0 1 0810811710,00 08/1011703:53 51-28 5
2,40inithdoluene NO Dg1L 6.0 1 08108/1710,00 0811011703:53 121-14-2
' 2,GOin odoluene NO ug1L 5.0 1 0810811710:00 08110117 03 53 606-20-2
1 Obn-octylphthaiate NO ugll 5.0 1 08108/171, 00 0811011703'.53 117-84-0
1,2-Diphenylhytlmzine NO uga- SO 1 08/0811710:00 08/10/1703:53 422-66 7
bis(2-Ethylhexyl)phlhaAte NO ug1L 5.0 1 08/08/171000 Deal OIL 703'53 117-81-7
Flmmmthene ND ugh- 5.0 1 0810811710;00 0811011703:53 206-44-0
i Flporene NO ug/L 6.0 1 08/08117 IUD 0811011703:53 86-737
Hexachforo-1,3 buladene NO Drift- 5.0 1 0810811710,00 08110117 03 53 67-683
j Hexachiorobenzene NO ugh. 50 1 08/0811710:00 081101170353 118-74-1
Hexachlorocyclopentadiene ND ug/L 100 1 08108117 10: 0 OW1011703:53 7747-4
HexanNoroelhane ND uglL 5.0 1 W10811710:00 DWI D1703:53 67-72-1
Indeno(1,2,3-crigyrene NO ug/L 5.0 1 081081171000 0811011703:53 193-39-5
isophomne NO ug1L Uro 1 0810811710:00 08/1011703:53 7859-1
384-Melhylphenoi(m&p Goad) NO ug1L 10.0 1 0810811710:00 0811011703:53 15831-104
'.3aphlhalene NO u911- 5.0 1 0810811710,00 08/10/170363 91-203
j =iailrobemene NO Dglt- 50 1 0810811710:00 08110/170353 98-95-3
3 2-Nilropheno1 NO ugh- 50 1 0810811710,00 0811011703'53 88-75-5
3 4-Nilrophenol NO age- 50.0 1 08/0811710:00 0811011703:53 100-02-7
N-Nlrosotlimethylamine NO uglL 6.0 1 08108/17 1000 0811011703:53 62-75-9
N-Nilrosodi-n-propylamine NO uga- 5.0 1 08/0811710:00 08/1011703:53 621-54-7
_ N-Nitrosel iphenylamine ND ug/L OLD 1 081081171000 0811011703:53 86-306
2,2'-Oxylos(1-cMmopropane) NO ug/L 5.0 1 0810811710:00 08/1011703:53 108-60-1
Pentachlorephenol NO Dg1L 100 1 08108/1710DO 0811011703:53 87-86-5
Phenanthrene NO Dg/L 50 1 0810811710,00 08110117 03 53 8501-8
Phone l NO uqA- 5.0 1 08/08/17 LTW 08N011703:53 108-95-2
f Pyrene NO ug/L 5.0 1 08108/1710:00 0811011703:53 129000
1,2,4-Tdchlorobeazene ND ug1L 5.0 1 0810811710:00 08/101170353 12082-1
t
2,4.6-Tdchlorophenoi NO Drift- 100 1 08/081171000 OB/1011703.53 8806-2
Surrogates
Nitrebenzene-05(S) 66 % 10-120 1 081081171000 08/10/i703'53 4165-60-0
7 2-Frimrobiphenyl(8) 65 % 15-120 1 0810811710,00 0811011703:53 321-608
Terphenyl d14 IS) 36 °/u 11-131 1 WOOD 08/10/1703'53 1718-51-0
Phenol DO(S) 23 % 10-120 1 0810811710:00 OW101170353 13127-883
2-Fliximphenol(S) 33 % 10120 1 08108117)0:00 08110/1703:53 367-12-4
' 2,4S-Tdbromophenoi(9) 73 % 10-137 1 0810811710:DO 0811011703:53 118796
624 Volatile Organics Analytical Method:FPA624
Acrolein NO u9/1- 5,0 1 0810911701:46 10702-8 L1
Acrylonilrile ND ugll, 50.0 1 081091170146 107-13-1
Benzene NO ug/L 2.0 1 08109117 01 46 71-432
Bromotlichloromethane NO ugaL 20 1 06109/170146 7527-4
Bromolonn NO ug/L 20 1 081091170146 75-25-2
Bromemelhane NO uglL 2.0 1 08/09117 WAS 74�83-9
1
1 REPORT OF LABORATORY ANALYSIS
S mie report char not be reprotlucea,except in felt
Date:0 8/2 212017 10:12 AM aimout the wnuen wnsent of Pace A.11t.l Servaes,LLc. Page 49 o196
7
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Pace Analytical Services,LLC
1 pp 2225 Riverside or.
aceAnalytieal As„evip¢,NO 28804
mxp�.tb` Amer odounl54-7176
a ,
ANALYTICAL RESULTS
project; Low&Boner Inc 1210140
Pace Project No.: 92350243
r Sample: Manhole 3 U Lat i6: 92350243013 Collected: 0BIOD1714:29 Received 081031171647 Matrio,Wme,
Paremeiers Results Units ReportLimit OF Prepared Analyzed CAS No. Qual
j 624 Volatile Organics Analytical Melloul EPA 624
Carbon tetrachloride NO uga- 20 1 08/09/1701:46 56-235
Chlorobenzeer NO ug4 20 1 08/09117 01 46 108-90-7
l Chlomethane NO ug1L 20 1 08/091170146 15-00-3
Chloroform NO ugh. 20 1 0810911701:46 61-663
Chio,omethene NO ug4 2.0 1 0W091170146 74-8I-3
- Dibromochloramethane NO ug4 2.0 1 0810911701;46 124-48-1
1,2-Dichtorobenzene NO ug4 2.0 1 0810911701:46 95-50-1
1.3-Dichlorobenzene NO uglL 2.0 1 08/0911701:46 Ml-734
? 14-Dichlarabenzene NO ug/L 20 1 081091170146 10646-7
1,1-Dichlomethane NO uglL 20 1 08/09/170146 75-34-3
_ 1.2-Dichloodolorne NO uglL 2.0 1 081091170146 107-06-2
1,1-Dichloroethe0e NO ug4 2.0 1 08/09/17 Of 46 75-354
cis-1,2-Dic torcethene NO ug4 2.0 1 OW0911701:46 156-59-2
Inns-4.2-0inhoroelhens NO ug/L 2.0 1 081091170146 15660-5
12-Dichloropropene NO uglL 20 1 081091170146 78-87-5
cis-1,3-DichloroProduce NO uglL 2.0 1 08/09117 01 46 10061-01-5
trans-1,3-Dichloropropene NO uglL 20 1 08109117 Of 46 10061-02-6
Ethylbenzene NO uglL 20 1 081(pul 0146 100-41-4
( (methylene Chloride NO ug/L 2.0 1 0810911701:46 75-09-2
�.1.2,2-Talochimaddl me NO Thin- 2.0 1 081091170146 79-34-5
Teirachloroemene NO ug4 2.0 1 OW091170146 127-184
Toluene NO ug4 2.0 1 0810911701:46 408883
1,1,4-Tdchliamethane NO ug4 2.0 1 081091170146 71-556
1,1,2-Trichloroethane NO uglL 2.0 1 081091170146 7900-5
Trichoroelhene NO hod- 20 1 0W0911701:46 790
- TrichlorolluoromeNane NO uglL 20 1 OW091170146 75E9A
? Mnyl choside NO ug4 2.0 1 08/0911701:46 7501-4
Surrogates
4-Bromofiuorobenzene(S) 102 % 70130 1 08/091170146 460004
peaene-d8(S) Of % 70T30 1 08/091170146 2037-26-5
} 1,2-Dichloroethane ed IS) 86 % 70-130 1 0810911701-46 17060 07-0
71 2540C Total Dissolvetl Solitls Analytical Method:SM 2540C
Total Dissolvetl Solids 83.0 mg4. 25.0 1 08IONI717:53 D6
3
{ 2540D Total Suspended Solids Analytical Method SM 2540D
f
3 Total Suspended Solids NO ou lL 2.5 1 0810811713'51
Total Nitrogen Calculation Analytical Method:TKN+NO3+NO2 Calculation '..
Total.Nitrogen 0.94 hi 0,12 1 0810911718it
350.1 Ammonia Analytical Method EPA 350.11993 Rev 20
Nilrogen,Ammonia NO mg4 0,10 1 0810911705:13 7664-41-7
g
351.2 Total K1 9 eldahl Nitro en Analytical Melhatl:EPA 351.2
I
Nitrogen.Kleldahi,Total NO mglL 0,50 1 08109/1717:10 1727-37-9
1 REPORT OF LABORATORY ANALYSIS
This report shall net be reponfroad,except in full,
Date:0 812 2/2 011 1 0:12 AM winner the wdnen consent of Pace Aaalyrood Asoices,LLC Page 50 of
S

1
} Pace Analytical Services.LLC
t ® 2225 Riv ef4r,0r.
aceAnaly6cai At„n„ne.NC 2e6o4
/ onOvenot ove (828)2M.7176
ANALYTICAL RESULTS
S Project: Lmv&Sonar Inc 1210140
Pace Project No.: 92350243
Sample: Manhole3-U Lab ID: 92350243013 Collected 081021171429 Received: 08103/1716:47 Maldx:Waler
3
� Parameters Results Units Report Limit OF Prepared Analyzetl CAS No. Qual
353.2 Nitrogen,NO2/NO3 pros. Analytical Method:EPA 353.2
Nitrogen,NO2 plus NO3 0.85 mglL 0.020 i 08109117 12:25
365.1 Phosphorus,Total Analytical Method:EPA 365A
1
Phosphorus NO dri 0,050 1 OW101170642 7723-14-0
5220D COD MalNicai Method:SM 5220D
I Chemical Oxygen Demand NO mglL 250 1 08/0711718:41
s
I
Sample: Stamey Lab ID: 92360243014 Collected: 0810211713:06 Received: 08103/171647 Ma(rix:Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
1 200.7 MET ICP Analylicai Method:EPA 2001 Preparation Method.EPA200.7
Antimony NO ug/L 50 1 0811311722:05 08/1511703:38 7440-360
T Arsenic ND USA- 100 1 0811311722,05 0811511703:38 7440-38-2
Beryllium NO ug/L 1.0 1 0811311722:05 DWI 51170338 744041-7
--,cadmium ND ug1L I'D 1 08/1311722:05 0811 out 703:38 744043-9
- 2hromium NO ug/L 5.0 1 08/13/1722:05 0811511703'38 7440�47-3
j - Copper ND ug/L 5.0 1 08113/1722:05 0811511703:38 7440-508
Lead ND W1 Sp 1 0811311722:05 08/1511703:38 743992-1
- Motybdenum NO add- 50 1 0811311722:05 0811511703:38 7439-98-7
- Nickel ND ug/L 50 1 0811311722:05 08/15/1703:38 744002-0
s Selenium NO ug/L 100 1 0811311722:05 08115/1703:38 7782-49-2
Silver NO ug/L 50 1 0811311722:05 081151170338 7440-22-4
Thallium NO ug/L 100 1 0811311722,05 DWI 61170338 7440-28-0
Hardness, total ISM 23408) 53200 USA- 662 1 08/1311722:05 DWI 511703:38
Zinc 22.4 USA- 10.0 1 0811311722:05 0811 Sit 703:38 7440-66-6
5220D COD Analytical P,lelhcdT SM 5220D
Chemical Oxygen Demand ND mg/L 25.0 1 0&07/1718:41
3
7
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REPORT OF LABORATORY ANALYSIS
Talc report than not be reproduced.exeptm ruu.
j Date:08122/201710:12 AM without he written consent or Pace Analytical services.LLC. Page 51 of 96
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Pace Analytical Services,-W
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aeeAnalytieal 2225 R.NO 28 04
Asheville.NO -7176
(a281254-'1196
QUALITY CONTROL DATA
Project: Law 8 Boner Inc 1210140
Pace Project Ni 92350243
QC Batch: 373777 Anatysis Method: EPA 1664E
QC Batch Methori: EPA 1664E Analysis Description: 1664 HEM,Oil antl Grease
Associated Lab Samples: 92350243001,92350243002,92350243003,92350243004.92350243005,92350243006,92350243007,
92350243008,92350243009,92350243010,92350243011,92350243012.92350243013
J METHOD BLANK: 2071021 Matrix: Water
Assodated Lab Samples: 92350243001,92350243002,92350243003,92350243004,92350243005,92350243006,92350243007.
92350243008,92350243009,92350243010,92350243011,92350243012,92350243013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 OB/17/170508
j
� LABORATORY CONTROL SAMPLE: 2071022
Spike LCS LCS %Rec
1 Parameter Units Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 40 38.9 97 78-114
MATRIX SPIKE SAMPLE: 2071023
iP 35329392002 Spike MS ME %Rec
} Parameter Units Result Conc. Result °/b Rec Limits Qualities
$ Sit and Grease mglL 3.3d 40 41.1 95 78-114
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I
REPORT OF LABORATORY ANALYSIS
This soon sba'I not be reproduced,except a full,
Date:0 8/2 212017 10,12 AM mimeet me writes re-weof Pace Anayfical SA,xcs,tic. Page 52 of 96
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Pace Analytical services.LLC
aceMalyttcal a Rrversbe
nafv}wa'aC.zam Fshe»Ile,NC 28a86
(82e)250.]1]6
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QUALITY CONTROL DATA
l Project: Low&Bonar Inc 1210140
I Pace Project No.: 92350243
QC Balch: 372256 Analysis Method: EPA245A
QC Balch Melhotl: EPA 245.1 Analysis Description: 245.1 Mercury
Associated Lab Samples: 92350243001,92350243002,92350243003,92350243004,92350243005,92350243008,92350243007,
i 92350243008
METHOD BLANK: 2062253 Matrix: Water
Associated Lab Samples: 92350243001,92350243002.92350243003,92350243004.92350243005,92350243006,92350243007,
92350243008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0,20 08109/1705,02
7
3
LABORATORY CONTROL SAMPLE: 2062254
Spike LCS LCS %Rec
Parameter Units Conc. Result %Res Lies Qualifiers
i Mercury ug/L 25 26 104 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2062265 2062255
MS MSD
92349975002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone Conc. Result Result %Rau %Rec Limits RPD Qual
I - Mercury ug/L ND 25 2S 0,24 0.28 8 10 70-130 16 M1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2062257 2062258
MS MSD
92350107001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Come. Result Result %Rec %Rec Limits RED Cuts
Mercury ug/L ND 2.5 2.5 24 2.2 94 86 70-130 9
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ree=m�sPre=emea on mis Peeearemma nmislmmmaa nrrne^umisaowmn except where an mlerama valua preeomm to aam Dune rssml.
_ REPORT OF LABORATORY ANALYSIS
This consul shall act be mpmtlu-d.except in On,
Date:0812212017 10:12 AM without the whiten conaanl of Pace Analytical Service,LLC. Page 53 of 96

i
ff Pace Analytical Servloes,LLC
aeeAnalytical o 2225 Riverside Or
1 Asheville.NC 26809
xu'rvsam
p2m254]t]6
I
QUALITY CONTROL DATA
Project: Lmv&Sonar Inc1210140
Pace Project No.: 92350243
QC Batch: 372458 Analysis Method: EPA245A
QC Batch Method: EPA245.1 Analysis Description: 245.1 Mercury
{ Associated Lab Samples: 92350243009,92350243010,92350243011,92350243012,92350243013
3
METHOD BLANK: 2063511 Matrix: Water
Associated Lab Samples: 92350243009,92350243010,92350243011,92350243012,92350243013
i Blank Reporting
3
Parameter Units Result Limit Analyzed Qualifiers
� Mercury uglL ND 0.20 08/1011723:43
3
t LABORATORY CONTROL SAMPLE: 2063512
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Mercury ugll 2.5 2.6 105 pLH5
3
5
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2063515 2053516
i MS MSD
92350367014 Spike Spike MS MSD MS MSD %Rec
I Parameter Units Result Coma Cook, Result Result %Rec %Rec Limits RPD Qual
4ercvry uglL ND 2.5 2.5 2] 26 107 103 ]4/30 3
3 3
1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2063596 2063597
has MSD
92350367005 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cora Can, Result Result %Rec %Rec Limits RED Qual
Mercury ug/L NO 2.5 2.5 20 26 103 102 70-130 0
1
1
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i
REPORT OF LABORATORY ANALYSIS
This report shall ot he reprmuce4 except in fall,
i Date:081221201710:12AM fives Me when consent of Pace Analytical Sconces,LLc. Page 54 of 96
3
1

1
EPace Analytical Services,Lc
' /I/�/�a er �/�/� a 2225 Riversch.0r.
^ceAnalyic2� Asheville,NC 28804
(82m254-]196
i
3
I
QUALITY CONTROL DATA
Project. Low&Borar Inc 1210140
Pace Project No.: 92350243
QC Balch: 372225 Analysis Method: EPA 200.7
i QC Balch Method: EPA 2007 Analysis Description: 2007 MET
Associated Lab Samples: 92350243001,92350243002.92350243003,92350243004,92350243005,92350243006,92350243007.
92350243008
METHOD BLANK: 2062099 Matrix: Water
Associated Lab Samples: 92350243001.92350243002,92350243003,9235024300Q 92350243005,92350243006.92350243007,
l 92350243008
'3 Blank Reporting
Parameter Unils Result Limit Analyzed Qualifiers
Antimony ug/L ND 5.0 0810811720:13
Aroenlc u pl- ND 10.0 08/08/17 20:13
Beryllium upl- ND 1.0 0810811720a3
j Cadmium uglL ND L0 0810811720:13
Chromium ug/L NO 50 0810811720:13
j Copper ug/L ND 50 08/08117 20:13
Hardness,Total ISM 23408) ug/L ND 662 08/08/17 20:13
Lead ug/L NO 5.0 0810811720:13
- Molybdenum ug/L ND 5,0 0810811720:13
Nickel ug/L ND 5.0 08/08/17 20:13 -
Selenium ug/L NO 10B 08/08/17 20:13
Silver ug1L ND 5S 08108/17 20:13
_ Jim ium u91L NO 10) 0811211720:18
1-inc uglL ND 10 0 08/08117 20:13
3
LABORATORY CONTROL SAMPLE: 2062100
3 Spike LCS LCS %Res
7]7$ Parameter Units Cone. Result %R. Limits Qualifiers
Antimony ug/L 500 504 101 85115
Arsenic u911- 500 485 97 85-116
Beryllium ug/L Soo 516 103 85-115
Cadmium u91L 500 509 102 85115
Chromium ug/L 500 500 100 85115 '..
Copper ug/L 500 622 404 85-115 '..
Hardness,Total ISM 23408) ug/L 32000
Lead mpl- 500 492 98 85115
Molybdenum ug/L 500 515 103 85115
Nickel ug/L Soo 510 102 85-115
Selenium ug1L 500 496 99 86115
Silver ug/L 250 233 93 85 US
Thallium ugll- 500 490 98 85TI5
Zinc met- Soo 514 103 85-115
3
't
1 Reaelta presented on this page are lathe units Indicated by the'Vnils'colace except More an alternate unit Is presentee'.the passing,re cut,
REPORT OF LABORATORY ANALYSIS
This report shall not be coproduwQ except in full.
Date:08122/201710a2 AM ',hat'melath..consent of Pax Analye:al Services,LLc. Page 55 of 96
(

)
j
s Pace Analytical5ervices,LLC
aceAnalytical 24,;]c,N 2104.
3 nwnN�'ases. ASFevi!Ie,NC2Ba04
i (e2a)254,]ll8
13
I QUALITY CONTROL DATA
t Project: Levi&Bona. Inc 1210140
Pace Project No.: 92350243
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2062101 2062102
MS MSD
I 92349912OD2 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cane. Cons, Result Result %Rec %Rec Limits RPD Chat
Antimony ug(L 86 500 500 437 395 86 77 70-130 10
{ Arsenic ug/L ND 500 500 445 400 89 80 70130 11
I Beryllium ug/L NO 500 500 433 388 87 78 70-130 11
Cadmium uglL NO 500 500 436 392 87 78 70130 11
Chromium ugli- 9.0 500 500 434 393 85 71 70-130 10
Copper ug/L 312 500 500 778 727 93 83 70-130 ]
Hardness,Total ISM 23408) ug/L 108000 131000 133000 2
j Lead ugh- ITA 500 500 415 375 81 73 90-130 10
I Molybdenum upt, 12.2 500 500 471 426 92 83 70-130 10
j Nickel ugl- 104 Soo 500 415 376 81 73 70-130 10
Selenium ug/L NO 500 500 471 422 92 82 70-130 11
3 Silver ugll NO 250 250 218 196 87 78 70-130 10
Thallium ug/L ND 500 500 167 147 33 29 70-130 13 MO
Zinc ui 214 500 500 634 608 84 79 70-130 4
S
1
MATRIX SPIKE SMATRIX SPIKE DUPLICATE: 2082103 2062104
MS MSD
j 3 92350183001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cana Cmm. Result Result %Rec %Rec Limits RPD Coal
Antimony mpl- ND 500 500 401 407 80 81 70-130 1
Arsenic ug/L NO 500 500 389 392 ]] 78 70-130 1
Beryllium ug/L ND 500 600 397 401 79 80 70-130 1
@; Cadmium ugh- ND 500 500 389 395 78 79 90-130 2
9 Chromium ug/L 19.2 500 500 395 406 75 27 70-130 3
13 Copper ug/L ND 500 500 408 419 81 83 70-130 3
j Hardness,Total ISM 23406) ugd. 6670 31600 32200 2
i Leatl ug/L ND 500 500 385 392 77 78 70-130 2
t Molybdenum uq/L NO 500 500 408 416 81 83 70130 2 1.
Nickel ug/L 13.2 500 500 396 402 76 78 1P130 2 '..
Selenium ug/L ND 500 500 398 404 79 80 70-130 1
t
Silver bad- ND 250 250 202 203 81 81 70130 1
3 Thallium uglL ND 500 500 393 393 79 79 70.130 0 '.
Zhu, upl- 39.7 500 500 424 434 ]] 79 70-130 2 l
t
I
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3
�.
REPORT OF LABORATORY ANALYSIS
} This report shall not be reproduced.c—pl in full,
iDate:08122e017 10:12 AM wimomthe wren consent m Pace Analytical Services,LLC. Page 56 of 96
1
s

1
Pace Analytical Services,LTC
j s 2225 ov...We Or.
ytieal Asheville,NC 28804
11� aceAnal
mrw e'db%am [phone]
i
f
i
QUALITY CONTROL DATA
Project: Low 8 Broad Inc 1210140
Pace Project No.: 92350243
PC Batch: 372446 Analysis Method: EPA 200.7
I QC Batch Method: EPA200] Analysis Description: 200.7 MET
` Associated Lab Samples: 92359243009,92350243010,92350243011,92350243012,92350243013,92350243014
t
METHOD BLANK: 2063458 Matrix: Water
Arceraled Lab Samples: 92350243009.92350243010,92350243011,92350243012,92350243013,92350243014
3 Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1 Antimony ug/L NO 5A 08115/1702:54
Arsenic ug/L NO 100 0811511702:54
Beryllium UgIL ND LB 0811511702:54
Cadmium ug1L ND LB 0811511702:54
Chmmlum ui ND 6B 0811 511 7 0 2:54
Copper ug/L ND 5.0 08115/1702',54
{_ Hardness,Total(SM 2340B) ug/L ND 662 0811611702:54
Lead ug/L NO 5.0 0811511702:54
Molybdenum ug/L ND 5B 0 811 611 7 02:54
Nickel right. ND 5B 0811511702'54
3 Selenium uri ND 10B 0811511702:54
Silver ug/L NO 5.0 0811511702:54
Thallium rig/L ND 100 0811511702:54
. Zinc ug/L NO 10A 0811511702'54
i LABORATORY CONTROL SAMPLE: 2063459
Spike LCS LCS %Rea
q Parameter Units Conn Result °o Rea Limits Qualifiers
3 Antimony mph- 500 480 96 85-115
Anoints ugh. 500 466 93 85TH5
Beryllium ug1L 500 484 97 85-115
Cadmium ug/L 500 494 99 85-115
Chromium ui 500 487 97 8&115
Copper moL 500 484 97 85-115
Hardness,Total ISM 2340B) ugi 32500
1 Lead ago- 500 489 98 85-115
Molybdenum uglL 500 504 101 85-115
S Nickel ug1L 500 488 98 85115
Selenium rig/L 500 487 97 85-115
Silver trg/L 250 246 98 85-115
- Thallium rig/L 500 474 95 85115
Zinc UgIL 500 499 100 85-115
I MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2063460 2053461 '..
MS MSD
( 92350079002 Spike Spike MS MSD ME MSD %Rec
j Parameter Units Resell Conn. Cone. Result Result %Rec %Rec Limits RPD Cars
3 Antimony ug& 157 500 Soo 499 498 97 96 70130 0
Reaullapresente0 on 101s pagearcin the ueib ln0lcale0 hylhe'Unlle"coluTn¢xupl Mlere an allemaleuni119 pmRnte4blhe tlg0l otlhe res Wl.
REPORT OF LABORATORY ANALYSIS
TM1ie report shall not be rep/rmo d,except in of,
Date 0812 212 017 10:12 AM without the wtinen conscet of Pace Analytical Serwres,uc Page 57 of
1

i Pace Analytical Services,Dec
s 2225 Riverside Dr.
aceAnaXical Asheal ,NC 2ae04
QUALITY CONTROL DATA
Project: Low&Touch Inc 1210140
Pace Project No: 92350243
I
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2063460 2063461
MS MSS
j 92350079002 Spike Spike ME MSD MS MSD %See
I! Parameter Units Result Cone Cone. Result Result %Rec %Rec Limits RPD That
s Arsenic ug/L NO 500 500 494 494 99 99 70-130 0
Beryllium ug1L ND 500 50D 477 479 95 96 70-130 0
i Cadmium ug/L ND 500 500 494 495 99 99 70-130 0
i Chromium calp 139 5w 500 627 627 98 98 70-130 0
Copper ug/L ND 500 500 490 492 97 98 70-130 1
= Turmoil,Total(SM 23406) ui 33800 64800 65100 0
} Lead ug1L ND 500 500 442 444 88 89 70-130 1
Molybdenum ug1L ND 500 500 504 507 100 101 70130 1
Nickel ug/L ND 500 Sao 455 466 91 91 70130 0
Selenium ug/L ND 500 500 527 528 103 104 70-130 0
Silver no& ND 250 250 256 257 102 103 70-130 0
Thallium ugiL ND 500 Soo 391 396 78 79 70-130 1
Zinc ug/L 635 500 500 559 561 99 400 70130 0
f}
x�
1
3
I
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tl
j
E
j
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3
I
1
mmupapreaenfed on this page are in the hale Indicated by the"Units-column except vh—an apernale unlpa pen-odlorhe a", fee'a'a"
I
j REPORT OF LABORATORY ANALYSIS
This tepotl shall not be reproduced,except in lull,
Date:0 812 212017 10:12AM without the wnnen consent of Pace Analybeal services,LLC. Page 58 of 96
I
j

{ Pace Analytical SaM6eS,LLC
6 2225 Rlcered.9r.
j aceAnaptcal Aahamna,NC 28804
be,ey`sce. [phone]
t
I �1
QUALITY CONTROL DATA
Project Low&Bmmr Inc 1210140
Pace Project No.: 92350243
i
J OC Batch: 372395 Analysis Method: EPA624
DC Batch Method: EPA624 Analysis Description: 624 MSV
! Associated Lab Samples: 92350243001,92350243002,92350243003.92350243004,92350243005.92350243006,92350243007,
92350243008.92350243009,92350243010,92350243011.92350243012,92350243013
METHOD BLANK: 2063075 Matrix: Water
! Associated Lab Samples: 92350243001.92350243002,92350243003,92350243004,92350243005,92350243006,92350243007,
92350243008.92350243009,92350243010,92350243011,92350243012,92350243013
'i Blank Reporting
Parameter Units Result Limit Analyzed OmbiOers
L1.1-Trichloroethane fig/L ND 2,0 08/08/17 20:09
TL2,2-Tetrachbroethane ugiL ND 2B 08/08/17 20:09
1,1,2-Trichloroethane ug/L ND 2B 08/08/17 20:09
1,14nchlmcelhane ugiL ND 20 0810811720,09
IT-Dichlo bethene ug1L ND 2 0 08108/17 20:09
T2 Dichlrbenzene ugiL ND 2.0 081081172009
1.2-Dichlor0 otems, ug1L ND 2B 08108/17 20:09
1,2-Oichioropropane ug)L ND 2.0 0810811720:09
L3-Dichbrobenzene fig/L ND 20 0810811720:09
= L4-Dichbrobenzene fig/L NO 2B 08/08/17 20 09
Acrolein ug1L ND 5.0 08108/17 20S9
Acrylonildle upt. NO 50.0 08108117 20:09
s �genzene ugiL ND 2.0 0810811720:09
)roreodichlorometheme ug/L NO 2.0 0810811720:09
'Br0moform fig/L ND 2P 08/08/17 20:09
Bromomethane ug/L ND 20 08108/1720:09
i Carbon tetrachloride mpl- ND 2.0 08/08/17 20:09
Chiomlanzene ugh- NO 20 081081172009
Chamethane ug1L NO 2A 08/08/17 20:09
Chloroform g1L u NO 2B 08/08117 20:09
3 Chloromethane ugiL NO 2.0 08/08/17 20:09
7 cis-1.2-Dichlaroethene ug/L ND 2.0 08/081172009
cis-1,8-Diohloropropene ug/L ND 2P 08108/17 20:09
Diearmehioromethane ug15 ND 2.0 08AP/1720:09
Ethyleanzene ugh- ND 2.0 08/08/17 20:09
Methylene Chloride ugiL NO 2.0 08108117 20 09
Tehacbioroethene ugiL ND 2B 08/08/17 20:09
3
Toluene ugiL ND ZO 08108117 20:09
( hans-T2-Dichlomethene uWL ND 2.0 08I081W 20:09
t trans-1,3 Dichlompropene find- ND 2.0 08108/17 20:09
1 Tnchlorcelhene find- ND 2B 08/08/17 20:09
j Trichiorofrommelhane ugiL ND 2D 08/08/17 20:09
li Vinyl chloride ugh- NO 2B 08/08/17 20 09
3 L2-Dichloreehlane 14(S) S 87 70-130 08/08/17 20 09
4-Bramoiluorobenzene(6) % 100 70-130 08/08/17 20,09
Toluene-08(S) % 109 70130 08108117 20:09
I
Rssulm Preeeme4 on lee pare are mare umu lnemtme Crme-umis'eammn e.ceyl on—eo nerna€e car to Wesomee to the ne„mime rases
1
REPORT OF LABORATORY ANALYSIS
This r,en e„at not be reyma had,except in miL
Date:081221201710:12AM Ne whnen comae of Pace Analytical seraxaa,llG Page 59 of 96
3

Pace Analytical Services,LLC
r Rives de
_ aOAnayical Ashanho,NC 288 04
onegoicartence
(828)254->t>6
i
7 4
QUALITY CONTROL DATA
Project: Low&Behar Inc 1210140
E Pace Project No.: 92350243
3
LABORATORY CONTROL SAMPLE: 203076
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1 1-Trichlorcelhane ugh- 20 21,6 108 52-162
T1,22-Tetrachloroelhane ug1L 20 187 94 46 157
1.1,2-Towifrraeihane ug1L 20 189 95 52-150
1,1-Dichloroethane uglL 20 21S 107 59-155
1,1-Dichlosafthene ug/L 20 19.6 98 1-234
ii 1,2-Dichlorobenzene ug/L 20 18.5 93 i&190
# 1,24lichloroethane ug/L 20 20.4 102 49-155
I 1.2-Dichloropropane ug1L 20 21.2 106 1-210
1,3-Dich1orobenzene ug1L 20 19.5 97 59-156
1.4 Dichlorobenzene ug/L 20 18.5 92 18-190
Acrolein ug/L 100 165 165 15-152 L1
Awlonilrtle ug)L 100 101 101 75-132
1# Benzene hpl- 20 2T6 103 37-151
Bromodichlommelhaoe ug/L 20 22.0 110 3&155
8mmoform ug/L 20 16.7 84 45-169
€ Bramomethans ug/L 20 23.4 117 1-242
Carbon tetrachloride ug1L 20 21.8 109 70-140
3 Chlombereene ug1L 20 196 99 37-160
Chi oroel isle uglL 20 195 98 14230
{ >-Chloroform wit- 20 21.8 109 51-138
S �hlommelhane ug/L 20 21.9 110 1-273
_ cis-1,2-Dichloraethene ug/L 20 20.9 104 68-146
cis-1,3-Dichlompropene ug/L 20 21.9 109 1-227
Rbri moch1werfa thane ug/L 20 20.4 102 53-149
Elhylbenzene uglL 20 20.7 103 37-162
Melhylens Chloride upt. 20 21.3 10/ 1-221
- Telrachlomelhene ug1L 20 170 85 64-148
Toluene ug1L 20 200 100 42-150
Irons-1,2-Dichlonothene, ug/L 20 22.2 111 54-156
7 Iran-1,3-Dichlompropene og/L 20 19.8 99 17-183
1 Tochloranthene ug/L 20 19.8 99 71-157
# Trichlomfluoromethane u91L 20 21.3 107 17-481
Vinyl chloride uglL 20 18.9 94 1-251
1,2-Dichlomelhaned4(S) % 108 70130
- 4-Bromofluombenzene(S) % 101 20-130
Toluene-d8(S) % 101 70-130
MATRIX SPIKE SAMPLE: 2063078
92350243010 Spike MS MS %Rec
{ Parameter Units Result Conc. Result %Rec Limits Qualifiers
1 —
3 1 1,14richioroelhane uylL NO 20 24.3 121 46-171 '.
1 2,2-Tetrachloroelhane ug/L ND 20 21A 106 73-159
i 1,2-TricMoroelhane ug/L NO 20 20.3 101 64-152
1,1-Dichloroelhane uTI- NO 20 22.0 110 43172
IJ-Dichloroethene uglL NO 20 22.2 111 48 189 '..
rcouva insesneo on mis pegs inhehic.maltatea brine^one,-1umn oxcefe in.an enema.unit is Presentee to the right of the reams
3
" REPORT OF LABORATORY ANALYSIS
This repotl snarl not he reproduced,except in ron,
3 Date:08122120171 T12 AM without the written consent of Pace Analyfcai Services,LLC Page 60 of 96
j

3
' Pace Analytical Services,LLC
aeeAnalytical a RiveWltle or
fseNIIe.NC 28804
7 mvrcp;w.'adscwn A
ff (628)254d17e
j QUALITY CONTROL DATA
I Project: Low&Boner Inc 1210140
Pace Project No.: 92350243
MATRIX SPIKE SAMPLE: 2063078
92350243010 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Lines Qualifiers
j 4,2-Oichlorobenzene eg/L ND 20 20.1 101 54-154
i 1,24ichloroethane ug/L ND 20 22,3 111 42-171
1,2-Dichtoropropane ug)L ND 20 22,9 115 55-157
1,3-Dichlorobenzene ug/L NO 20 21J 108 57-148
i 40ichlorobanzene ug/L ND 20 21.2 106 58-149
'. Aentein uglL ND 100 171 171 70-130 MG
Acrylonitrite ug/L ND 100 109 109 10-130
( Benzene ug/L NO 20 22.3 111 54-163
Bromotlichloromethane ug/L ND 20 241 123 56-152
_ Bromoform ugll- NO 20 183 92 53-151
Bromomethane rapt. ND 20 224 112 10-200
Carbon letraou,aide ug/L ND 20 26R 125 41-175
Chlourbureene uga- NO 20 21.5 108 67-152
- Chloroethane uglL NO 20 198 99 23-200
Chloroform ug/L NO 20 22 8 109 51-166
Chlommethane ug/L NO 20 215 108 40-175
cis-1,2-0ichlowe toes, ra/L ND 20 23.2 116 45174
cis-1.3-01chloropropene ug/L ND 20 22.9 115 38-146
Dibromochloromethane ug(L NO 20 22.0 110 65-144
1 Elhyfbereene eg/L ND 20 21,5 108 51-152
9 Methylene Chloride ugl- NO 20 20.5 103 40-167
Iblrachloroethene uglL ND 20 20.1 100 59-155
Toluene uglL ND 20 228 114 47-162
trans-1,2-0101ofoethene ugJL NO 20 24A 122 47-178
trans-1,3-Oichloropropene ug/L NO 20 23.3 117 39 148
Trichloroethene uglL ND 20 22,5 113 60-153
Tnchloronuoromethane ugs- ND 20 22B 115 42-199
Vinyl chlofitle uglL ND 20 192 96 46-176
q 1,2-Dichlomethane-d4(S) % 107 70-130
} 4-Dial ctuorobeluene(S) % 101 70-130
Toluene-tl8(8) % 100 TO 130
j
SAMPLE DUPLICATE 2063077
92350243008 Cup
j Parameter Units Result Result RPD Qualifiers
11,1-Trichi methane uglL NO ND
1,1,2,2-Teirachloroethane qWL ND NO
f} 1,1.2-Tfichlotoethane ug/L NO NO
t 1,1-Dichforoelhane rglL NO ND
1.1-Dichtoroethene eg/L NO ND
33 124icbtambenzeoa uglL ND ND
3 L2-Dlchlofoethane upl- ND NO
L2-Diehlofaprepane uglL ND ND
- 1,3 Oichlofobenzene uglL ND NO
j L4-Dichlorobenzene upl- ND ND
i
Results pre—we on rko' geareln lM1e volts lnYlcale0 el we"rnifs"column ercepleTem analfernate unitlspresenied to the dgMoflOe revolt
i
-'_-' REPORT OF LABORATORY ANALYSIS
3 Thi.repoM1 shall not be reproduced,except I.tali
3 Date,0812212017 10:12 AM Wnhoat the written concur of PaceMatytlmal Services LLc. Page 610196
t

Pace Analytical Services,LLC
' aceAnalytical® Riverside Of
Asheville,NC 28804
conelemeareace [phone]
I
QUALITY CONTROL DATA
- Protect: Low&Sonar Inc 1210140
Pace Project No.: 92350243
3 SAMPLE DUPLICATE: 2063077
92350243008 Dun
Parameter Units Result Result RPD Qualifiers
Acrolein uglL NO NO
Acrylonitlile ug/L NO ND
? Benzene ug)L ND NO
Bromodichlormnelnane, ug1L ND NO
i Diameter. uglL NO NO
' Bfommrrelhane uglL NO ND
Carbon telonlitedde gL NO ND
- Chlorobenzene uglL NO NO
Chloroelfane, ug1L ND ND
Chforofmm uglL ND 21
Chloremethane uglL NO NO
cis-1,2-Dichlmoelhene uglL NO ND
_ ds-1,3 Dichloropropene ug)L ND NO
Dibro.ochloro.elhane ugo- NO NO
Ethylbenzene ug1L ND ND
Methylene Chloride ugl NO NO
- Telrachloroethene uglL NO ND
- Toluene ug/L NO NO
j bans-1,2-fichloroethene ug/L NO NO
fans-1,3-Dichlompropene uglL ND NO
dchloroethane uglL NO ND
S Tdchlorolluoronlethane uglL NO ND
i Vinyl chlonde uglL NO ND
1 1.2-Dichloroethane-d4(S) % 86 86 0
4-BromoOuorohenzene(5) % 105 102 3
TOluene-de,(S) % 111 112 1
i,j
i
{
i
i
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3
Results ptes¢Oletl On th is pa8earein the uni151n 01caletl 0y the"one."-facinexcept xTaman anemaleunit is Presented to the tight or the result.
REPORT OF LABORATORY ANALYSIS
This repot shall not be reproduced,except in full,
Dale:081222017 10:12 AM lure.me written consent of Pace Anelyliwal Services,LLC Page 62 or 96

Pace Analytical Services,LLC
aceAnalj4wal b 2225 Rrvers tle Dr.
mvn' attvn Asha(82 )2 7176
8804
I (828)25d-0t>6
QUALITY CONTROL DATA
1
Project: Low&Sonar Inc 1210140
Pace Project No.: 92350243
QC Batch: 3721M Analysis Method: EPA625
QC Batch Method: EPA625 Analysis Description: 625 MSS
Associated Lab Samples: 92350243001,92350243W2.92350243003,92350243004,92350243005,92350243005.92350243007,
92350243008,92350243NO
3
METHOD BLANK: 2081603 Matrix: Water
Associated Lab Samples: 92350243001,92350243002,92350243003,92350243004.92360243005,92350243006,92350243007,
92350243008,92350243009
[ Blank Reporting
Parameter Unite Result Limit Analyzed Qualifiers
1,2+TrmhRmhenzene ug➢. ND 5B 08/07/1720:35
tyDiphenylhydrazine uglL NO 5B 0810711720:35
1.3 Dichlembenzene rml- ND 5.0 0810711720:35
1A Dichlombenzene moo- ND 5.0 08107/1720'35
- 2,T-Oxybis(i-chrompropane) uglL ND 5B 08107/1720:35
2.4.6Trichlorophenol uIRL ND 10.0 08107/1720:35
2,4 Dichlorophenol ohl- NO 50 0810711720:35
2,4-Dimelhylphenol ug/L NO 10.0 08107/1720,35
- 2,4-Dinitmphenol uglL NO 50B 0810711720:35
2,4-Dinilrotoluene ug1L ND 5P 0810711720:35
2BDinilrotoluene ug/L ND 5.0 0810711720:35
2 Chloronaphthalene ug l- NO 5.0 0810711720:35
2-Chloropera l hi ND 5.0 081071172035
�a-Nilrophenol ug/L ND 5B 08/0711720,35
- 3&4 Methylpherol(m&p Cresol) ug/L ND 100 0810711720:35
3,S-Dichlownenzidine ug/L NO 250 08107117 20 35
_ 4,6-Dinilmo-2-melhylphrumh ug/L NO 200 08107/1720:35
4-Bromoplepilphenyl ether ug/L NO 50 08107/1720:35
4 CMom 3-methylphenol ug1L ND 5A 08107117 20:35
j 4 CMolnphenylphenyl ether ugh- ND 5.0 08/0711720:35
4 Nitoophenol ug/L ND 50B 08107117 20 35
$ Acenaphlhene ag1L ND 5.0 08/0711720;35
3t Acenaphlhylene ug)L ND 5.0 0810711720:35
Anlhracene ug/L NO 5.0 08/07/1720,35
Bencubdanthracene u91L ND 50 0810711720:35
Benzo(a)pyrene ug/L ND 5B 08107/1720:35
Benzopufluoranthene ug1L NO 50 08A)711720:35
Senzo(g.h,i)perylene ugh- ND 5B 08107/1720:35
} Senzo(k)Oumanlhene ug/L NO 5B 0810711720:35
bis(2-Chloronfeco Jmethane tmL NO 10.0 08107I1720:35
I bis(2-Chlomethyl)ether ug/L ND 5.0 0810711720:35
bls(2-Ethylhesttgn lhalale ug/L NO 5.0 08107117 20 35
Butylbenzylphlhalale it NO 5.0 08/07/1720,35
Chrysene ug/L ND 5.0 08/0711720:35
i Dl-rt-bulylphthalate ug/L NO 50 p8/07/1720:35
7 Di-noctylphthalate ugfL NO 50 0810711720:35
Dibenz(a,h)anlhracene ug1L ND 5A 08107/1720:35
J Diethylphlhalale uglL ND 5B 0810711720:35 '..
Dirrcthylphlhalate ug1L ND 5B 08107/1720:35 '..
Pluoranthene ug1L NO 5.0 0810711720'35
Results areaemed on this Roos are in the uMs r ece ce or lbe'9ntts"c sout n exe.RI ser.an entTate tell is presouhs rmne damm1 Inc rezW.
REPORT OF LABORATORY ANALYSIS
I
"a Thls report she not be reproducM,except In lull,
Dale:0812 212 017 10:12AM without the written corsets of Pace AnalyIXal Rervlces,LC. Page 63 of 96
i

Pace Analytical Services,LLC
® 2225 Riverside 0r11� .
aceAnalAcat
Asheville,NC 28804
mfwluca'aQ°a+r' (829)254-]1)6
QUALITY CONTROL DATA
Project: Low&Bonar Inc 1210140
III€ Pace Project No.: 92350243
j METHOD BLANK: 2MI603 Matrix: Water
Associated Lab Samples: 92350243001,92350243002,92350243003,92350243004,92350243005,92350243006.9235024300].
1 92350243008,92350243009
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
3 Fluorene ug1L NO 5.0 081071P7 20:35
Hexachiero-1,3-butadtene upl- ND 80 08107/17 20:35
Hexachlorobenzene uglL NO 5.0 08107117 20:35
Hexachlorocyclopentadiene ug)L NO 10.0 08/07/17 20:35
Hexechloroelh nto ug/L ND 5A 08/07/17 20 35
indenc(1,2,3-cd)pyome ug/L NO 50 08107/1720:35
Rophorone ug/L NO 10.0 08/07/17 20:35
j N-NiVoso-di a-propylamine ug/L NO 5.0 08I0711720:35
N-Nitrosodimethylamine uqT ND 6.0 08/07117 20:35
N-Nilrosodiphenylamine ug/L ND 10.0 0 /07117 20:35
j Naphthalene ug/L NO 5.0 08107117 20:35
Nitrobenzene ug1L NO 5,13 08/07/17 20:35
Penlachlorophenol ug/L NO 10.0 08/07/17 20:35
Pbenanthrene ug/L ND 5.0 08/07/17 20:35
Phenol ug/L NO 5A 08107117 20:35
7 Pyre. apt. NO 5.0 0810711720:35
- 2,4S-Tdbramophenol(S) % 81 10-137 08/07117 20,35
>-.z Fluorobiphenyl(S) % 71 15-120 08107117 20:35
Nib Flarroph nol(S) % 40 10-120 081WI1720:35
- irobenzene-d5(S) % 70 10120 08107117 20:35
Pheno1-46(S) % 27 10420 08101/17 20:35
Terphenyl-d14(S) % 87 11-131 0 /0711720,35
3
j
LABORATORY CONTROL SAMPLE: 2061604
Spike LCS LCS %Rem
j Parameter Units Cone, Result %Rec Linch. Qualifiers
1,2,4-Tdchlorobenzene ug/L 50 32.4 65 44-142
3 1,2-Diphenylhydrazine ug/L 50 42.9 86 25-150
1,3-Dichiorobenzene ug/L 50 28 0 56 1-122
IA-Diehl...benzene ug/L 50 28 6 57 20-124
2,2'-Oxybis(l,m1ommopane) upL 50 29] 59 36-166
2,4,64richior damol uglL 50 41.2 82 37-144
7 2,4-Dlcal.ophenoi uglL 50 39D 78 1-191
2,4-Dimethylphenol mdL 50 38.6 ]] 32-119
j 2,4-Dinitrophenol add- 250 188 75 1-181
2A Dindrololuene ug/L 50 42A 85 39-139
2,8-Dinitroloiuene u91L 50 40.9 62 50-158
2-Chlcronaph h.lene u,T 50 38.8 78 60-118
2-Chlorephenol ug1L 50 34.2 68 23-134
bNihophenoi ug1l- 50 37.B 76 29-182
3&4-Mothylphencl(m&p Cresol) ug/L 50 26.0 52 25-150
3.T-Dichlorobenzidine ug/L 100 72.3 72 1-262
j 4,6 Dinitro-2 melhylphenci ug)L 100 96D 95 1-181
t
} Remlla lla—le4 oa no.Pageare ln(he cites In al.lea LylOe"Units"sole mn except xTerean allemale unit ispresenletl to lM1e tlgOr of trye reaull.
REPORT OF LABORATORY ANALYSIS
j This report shall not be repmaucea,except in W,'I.
I Date:0812212017 10:12 AM wimou[Mewnttemmnsentol Pace Anatyti IB—ces,ua Page 64 of 96

Ior I Pace Anatytical Services,LLC
aceAnalytical 222s Rr ecow 0,
Hshevive,Nc 28504
j www'ParPornIXNP [phone]
1
i
QUALITY CONTROL DATA
i
PmJecl: row&Sonar Inc 1210140
Pace Project No.: 92350243
I
IABORATORY CONTROL SAMPLE: 20616N
l Spike LCS LCS %Rec
I Parameter Units Cons. Result %Rec Limits Qualifiers
4-Bromophenylphenyl ether ug/L 50 36,0 72 53127
4-Chloro-3-melhylphenol ug/L 100 69.2 69 22-147
4 Chlomphenylphenyl ether M/L 50 36.2 72 25-158
4-Nilrophenol uglL 250 %0 40 1-132
Acenaphlhene ug/L 50 39.2 78 47-145
Acenaphthylene ugfL 50 40.3 81 33-145
Anlhracene uglL 50 454 91 1-166
- Benzo(a)anthracene ug/L 50 45 9 92 33-143
Senzo(agapene uglL 50 42.6 86 19-163
7 Benzo(b)fluoranthene ug/L 50 43S 88 24159
Benzogfh,pperylene ug/L 50 35.7 71 1-219
Beez6(Mlluc a thene ug)L 50 44.9 90 11-162
ths(2-Chloroathoxy)melhane right- 50 34.6 69 33-IM
bis(2 Chloroelhyl)ether ug/L 50 33.2 66 12-158
bis(2-Elhylhexyl)ph1halale ug/L 50 43.3 87 8-158
8utylbenrylphthalate ug(L 50 43 9 88 1-152
Chrysene, uglL 50 4T8 96 12-168
3 Di-mbutylphlhalate uglL 50 453 91 1-118
Of moctylphlhalate right- 50 38A 78 4-146
3 13ithenz(a,10anthracene ug/L 50 35,2 20 1-227
_:.JDielhylphlhalate night, 50 39.8 80 1-R4
Dimelhylphlhalate ug/L 50 39.2 78 1-112
Hu.nu here rig/L 50 60.4 101 26-137
Fluoreto ugh 50 41A 83 59-121
- Heleachloro-1,3-bNadiene it 50 30.3 61 24-116
Hexachlofobenzene uglL 50 41 9 84 1452
q Hexachlorocyclopenletliene ug/L 50 325 65 25-150
3t Hexachloroethane ug/L 50 26.0 52 40-113
Indeno(1.2,3 cd)pymne ug/L 50 35.8 72 1-171
tsophorone ng)L 50 38A ]] 21-196
3 N-Nilrose di-n propylamine ug)L 50 31.0 62 1-230
N-Niteandlmethylamine rig/L 50 267 53 25150
N-Nitheraliphenylamine rig(L 50 433 89 25-150
1 Naphthalene ug/L 50 35.3 71 21-133
- Nitrobenzem ug/L 50 40.1 80 35-180
Pentachlorophout uglL 100 105 105 14-176
Phenanlhrene ug/L 50 44.E 89 54-120
Phenol uglL 50 16.8 34 5-112
Pyrene ughL 50 41C 83 52-115
2,4,6-Tribromophenol(S) % 98 10-137
{ 2 Fluorabiphenyl(S) % 85 15-120
2-Fluoraphenol(S) % 48 10-120
Nitrobenzene d5(S) % 78 10-120
- Pheno1-0(S) % 30 10-120
Terpl i-d14(S) % 79 11-131
i
Results prasenleO an lhls page am in lM1e unlls intlicaletl bylpe`UNIs"calumneawpl wfieie an allemale unll is presenletl lolM1e tlgM ollOe result '.
}
j REPORT OF LABORATORY ANALYSIS
i
This repop shall not Ce reproducer,except in full
Dale:0 812 212 017 10:12 AM without the wnaen ocrewt of Pace Analytical Services,LLc, Page 65 of 96

Pace Analytical Services,LLc
8 2225 Riverside Or
aceconalwearo.
AshevP!e.NC 28809
x»"Hp'fttdA4M'1
(828)25941I6
F QUALITY CONTROL DATA
Project: Lmv&Sonar Inc 1210140
Pace Project No.: 92350243
MATRIX SPIKE SAMPLE: 2061605
92349969001 Spike MS MS %Ron
Parameter Unite Result Per.. Remit %Rec Limits Qualifers
1,24-Tdchlorohenzene mint. NO 50 32.7 65 44-142
1,2-Dipheny1hydrazine ug/L NO 50 30.4 61 25-150
1,3-Oichl.mbenzene ug/L NO 50 26.5 53 1-112
1,4-Dichlombenomi, ug/L NO 50 26.8 54 20-124
2.2'-Oxybis(1-chloropropane) ug/L NO 50 26.9 54 36-166
3 2,4,6-Tdchlmophenol mint, ND 50 41.0 82 32-144
44-Dichloropheoal uglL ND 50 47.5 95 1-101
44-0imethylphenol ug/L NO 50 47,4 95 32-119
2,4-Dinilrophenol ug/L NO 250 184 74 1-181
2.4-Dmitrololuene ug/L NO 50 43.3 87 39-139
} 2.6 DinNotolvene ug/L NO 50 392 78 50-158
2-Chlompapinnalma, ug(L NO 50 290 60 60-118
2-Chlorophenol uggL NO 50 30.7 61 23-134
2 Nilrophente ug/L NO 50 42.1 84 29-182
384 Memyiphenvl(m&p Cresol) hint. NO 50 23.3 47 25-150
3.3'-Dichlorobenzidine ug/L NO 100 31.7 32 1-262
4,6-Dimloo-2-melhylphenol ugh- NO 100 660 66 1-181
4-Bmmophenylphenyl ether ug/L NO 50 27.0 54 53-127
3 4-Chioro-3-melhylphenol ug/L NO 100 ill to 22-147
"`-Chlorophenylphenyl ether ogt- NO 50 351 I0 25-158
WNllrophenol ag/L ND 250 136 54 1-132
Acemphlheoe ug/L NO 50 319 68 47-145
j Acenaphlhylene ugg- NO 50 342 68 33-145
- Anthracene ugo- NO 50 38.1 76 1-166
j Benzo(a)anlhracene umL NO 50 373 75 33-143
Behairpepyrene ug/L NO 50 34 2 68 17-163
Benzc(b)fuoranihene ug/L ND 50 34.3 69 24-159
Benz.g h,g,,Pyene ugh- NO 50 337 67 1-219
Benzo(k)fooranthene upt- NO 50 34.9 70 11-162
bis(2-Chlorocihoxy)methane mpL NO 50 37.1 74 33-184
- bis(2-Chloroethy0 ether ug/L NO 50 28.7 57 12-158
bis(2-Ethylhexyl)phlhalale vg/L NO 50 418 88 8-158
- Bulylhenzylrehmalate, ug1L NO 50 42A 84 1-152
Chrysene milt. NO 60 37,2 74 17-168
Oi-mbutylphlhaiate ug/L ND 50 40.0 80 1-118
- Di octyiphlhalale ug/L NO 50 388 78 4-146
Dibenz(&h)an@racene ng/L NO 50 34.1 68 1-227
i Dlelhylphlhalate ug/L NO 50 42A 84 1-114
Dimelhylphlhalate ugg- NO 50 37S 75 1-112
Fluoranleene ugfL NO 50 466 93 26-137
Fiuorene, mpL NO 50 388 78 59-121
p Hewu hlom-l.8-bulatliene ug/L NO 50 355 71 24-116
Hexachlorobenzene milt. NO 50 28A 57 1-152
HexachioroWdopereadiene ugh- NO 50 16.5 33 25-150
HexacMoroelhaoe ug/L NO 50 26,7 53 40-113
Indeno(1,2,3-cd)pyrene ug/L ND 50 34.2 68 1-171
£ Isophorone high NO 50 40 0 80 21-19B
I re"Irs Presentee on this Pa9<are In the units hale ce by ins'max
"<alumn¢xcePl nBm<an alfemale unit is Pr<aenleJ to lM1e d9hl otlh</¢soil.
1
J
REPORT OF LABORATORY ANALYSIS
d
This report sha!I not be reproeucetl,except in toll,
i Date:081221201710:12 AM viithom the wren consent of Pace Analytical Services,LLC Page 66 of 96
(
't

Pace AxelyWou Services,LLC
Analytical' R"efS'de°`
xwnyazeaAcmm Asheville.NC 28fio4
[phone]
1
i -
QUALITY CONTROL DATA
i
j Project: Low&Bona, Inc 1210140
j Pace Project No.: 92350243
S
MATRIX SPIKE SAMPLE: 2061605
t 92349969001 Spike MS MS %Rae
j Parameter Units Result Conn. Result %Ran Limits Qumhgers
N Nithoso-diT,propylamine unt, NO 50 26.7 53 1-230
N-Nitrosohimelhylamine ug/L NO 50 224 45 25-150
&NiVosodiphenylamine rig/L NO 50 34.1 fib 25-150
Naphthalene TRIAL ND 50 35.5 71 21-133
;.l Nitrobenzene uglL ND 50 44.3 89 35-180
} Pentachlorophenol Mil- NO the 97.2 97 14-176
j Phenanthrene ug)L NO 50 355 21 54-120
Phenol mpl- NO 50 15.5 31 5-112
Pyrene rig/L ND 50 45.0 90 52-115
24,6-Tribromophenol(S) % Be 10-137
2-Hmalog iphenyl(S) % 46 15120
- 2-Flumaphenol(S) % 40 10-120
Nitrobenzene 1(8) % 83 10-120
} rpmea a.(S) % 26 10-120
Terphenyt-d14(S) % 71 11-131
3
SAMPLE DUPLICATE: 20616W
92350073002 Dup
Parameter Units Result Result RED Qualifiers
.2.4-Trichlorobenzene ughL NO NO
1,2-Diphenylhydrazine ug/L ND ND
1,3-Oichlmobenzene mpl. ND ND
1,4-Oichlorobenzene Tg/L ND NO
2,2'-Oxybis(1-chleropropane) uRI/L ND ND
t 2,4,6-Trichlomphenol uni NO NO
' 2,4 Dichlomplumol uglt NO ND
2.4-Dlmethylphenol rig/L ND NET
2.4 Dinitrophenol ug/L NO NO
9 2,4-DlnRroto1uene rig/L NO NO
2,6 Dinitrotcluene ug/L ND NO
2 Chloronaphlhatene ug/L ND ND
j 2-Chlorophenol upr- ND NO
1 2 Nitraphenol ug1L NO ND
t 3&4-Methylptnumm&p Cresol) uglL NO ND
3.3'-Oichlmobenziaine upl- NO NO
4.6 Dioitro-2 methylphenol ugll ND NO
4-Bromophenylphenyl ether ug/L ND NO
4-Chloro3-methylphenol ug/L NO NO
4-Chlorophenylphenyl ether rig/L ND ND
( 4-Nitrophenol ugg. NO ND
[ Acenaphthene uglL NO ND
Asenaphthylene mjT NO NO
Anthracene ug/L NO NO
3 Benzo(ramthracene ughL ND 1AJ '..
Z Benze(a)pyrene right ND 1AJ
t ae<mm araaemaa oo lws aeue.remme oRn.ma¢alea er ms-uou:.owmne.,RfuseeeeR surnereemlla erensool to as ruff elms ..IT '..
REPORT OF LABORATORY ANALYSIS
- This each shall Rol The reproduced.except in full.
Date:0 812 2/2 011 10:12 AM wimom the wrnen conaem of Pac^Analy[(Services,UPC. Page 67 of 96
i

Pace Analyllcal Services.LLL
aceAnalyticat RWerSNe Or
xnwpze:'aNmm Ashevtle,NC 28804
[phone]
i
QUALITY CONTROL DATA
Project: Low&parer Inc 1210140
I Pace Project No.: 92350243
[ SAMPLE DUPLICATE: 20616M
92350073002 OUR
_ Parameter Units Result Result RED Qualifiers
Benzo(b)fluoranthene ug/L ND 1.8J
Benzo(g,niheerylene uglL NO 4,7J
Benzo(k)goomethene u 11- ND LW
bis(2-Chloroethoxy)methane uglL NO NO
j bis(2-Chloroethyl)ether uglL NO ND
bis(2Ethylhexyl)phthalale ug/L 11.0 3.2J
j Butylbanzylphfhelate ug/L ND NO
Chnoone gglL NO 1.4J
Di n-butyfphthatate uglL ND ND
i Di-o-ortylphthalate uglL ND L2J
Dibenz(a,h)anfhracene ug/L NO 1.3J
Oielhylphthalate ug/L ND NO
_ Ungethylphlhalafe ug/L ND NO
_ Fluoranlhene ug/L NO NO
Fiuorene og/L NO NO
Hexachlom1,3 butedlene ug/L NO ND
- Hexachlorobenzene age- NO ND
S Hexachlorocyclopenladiene uglL ND NO
} HexachloroeUane uglL NO NO
^"1ttleno(L2,3-chwhere ug/L NO i.6J
_ iophorone ug)L NO NO
' N-Nitc so-di-n-propylamine ug/L NO NO
N-hatesodimethylarane uglL NO NO
N-Ni eshodipheny1 ine upl- NO ND
Naphthalene ug1L NO ND
Nitrobenzene ug/L NO NO
Pentachlorophenol uglL ND ND
Phenanfhrene ug/L NO NO
3 t Phenol ugJL ND NO
` Pyrene uglL NO NO
3 2.4,6-Triereaphenol(S) % 46 71 45
2 Fluorobiphenyl(S) % 21 59 15
2-Fluorophenol(8) % 18 31 55
Nilrobenzened5(S) % 29 61 76
Phone us(S) % ii 22 62
3 Tarphenyl 114(S) % 44 44 0
I
i
S
1
aaamt,praaemea on ml:paaaare mm—mu mmnmea ermrunnr<omnin e,«pt where anal—re unit l=aree.meamma crease,resort.
REPORT OF LABORATORY ANALYSIS
Tai,,hped chat not be reproduced,except in full.
7 Dale:081221201710:12 AM without the written wusent of Pace met"ical Sweces,MC, Page 68 of 96
1

' Pace Analytical Services,LLC
S & 2225 Rivetslu
a0 s pr.
j Analgical
- Asheville,Nc 2860a
) Kwp.Pa��aittan (82B)254-]1]6
j QUALITY CONTROL DATA
Project: Low&Bonar Inc 1210140
Pace Project No.: 92350243
QC Batch: 372288 Analysis Method: EPA625
1 QC Batch Method: EPA625 Analysis Description: 625 MSS
a
j Associated Lab Samples: 92350243010,92350243011,92350243012,92350243013
S
METHOD BLANK: 2062362 Matrix: Water
i Associated Lab Samples: 92350243010.92350243011,92350243012,92350243013
i
` Blank Reporting
[ Parameter Units Result Limit Analyzed Qualifiers
l
1,2.4-Trichlowbenzene uglL NO 5B OW0911722:12
1,2-Diphenylhydrazine ug1L NO 5B 08109/17 22:12
j 1,3 Dichlorobenzene ug1L NO 5.0 68109/17 22:12
1A Dlchlorobenzene ug/L NO 5.0 08/09117 22:12
2,2--Oxybis(1-chlompropane) ug/L NO 5,0 08109117 22'12
2,4,6 Trichlorophenal ug/L NO 10 0 08/)9/17 22:12
2ADawhlorophenol ugd- NO 5.0 0810911722A2
2,4-Dimelhylphenal uglL NO 10.0 08109/1722:12
2,4-faintopirmed u911- NO 5(10 08/09/17 22:12
2.4-Dinilrotoluene mill- NO 5.0 08109/17 22:12
s_ 2.6 DInibutoluene uglL NO 6.0 08109117 22:12
2-Chloronaphthalene uglL NO 50 08109/17 22:12
2-Chlorophenal mill- NO 50 08109/17 22:12
2-1,10rophenol ug/L ND 50 0810911722:12
�&4-Methylphenol(m&y Cresol) ugll NO 100 08/09/17 22'12
=
S - IT-Dichlorobirmidine ugh- NO 25.0 08/09/17 22:12
4B-Dinitro-2-ruethylphenol uglL ND 20.0 OW09/17 22:12
4-Bromophenylphenyl ether ugll- NO 5.0 08109/17 22:12
4 Chlom-3 melhylphenol ug1L NO 5.0 08109/1722'12
4-Chiamphenylphenyl ether ug/L NO 50 0810911722:12
4-Nitmphenol ug/L NO 500 08109/1722'12
Acenaph(bene ug/L ND 50 0810911722'12
Acommiduhyllow ug/L NO 50 08109117 22:12
- Anthracene uglL NO 5B 08109/17 22:12
6enzo(a)anthracene ugd- NO 5.0 08/09/17 22,12
Benzo(iggorene ug1L NO 6.0 08/09/17 22:12
i Benzo(b)fluoraNhene upt- NO 5.0 08109/1722:12
Bragedg,h,i)perylene ug/L NO 5.0 08/09117 22,12
Benzod luoranthene uglL NO 5.0 08109117 22:12
bts(2-Ghloroetboxy)methane, unit. NO 10.0 08/09117 22:12
bis(2-Chloroethy1f ether uglL NO 5 0 08/09/17 22:12
t bis(2�Fthylhexy1gghthalate add- NO 5,0 08109/17 22:12
Butylbenzylphthalate unit. NO 50 08/09/17 22,12
Ghryseng bg/L NO 50 08109117 22:12
Pro butylphthalate Igo- NO 5.0 08/09/17 22:12
I Di-n-octylgahal.t. ug/L NO 50 08/09/17 22:12
Dibenz(a,h)anthracene ug1L NO AB 08109/17 22:12
Diethylphthalate ug/L ND 5.0 08/09/17 22:12
Dinnethylphthalate ug/L NO 5.0 08109117 22:12 '..
3 Fluoranthene ug/L NO 5.0 08109117 22:12 '..
Farrere uglL NO 50 0810914722:12
i
8a%nn%vre%emea on Ibis page are in the lnaa mammeo by in,-unite omamn except»Here an atamme onus we%emsa to the asm onn%rearm.
REPORT OF LABORATORY ANALYSIS
This threat ah r not be reprodeem,except in of
Data 08I221201710:12 AM avithout the Walter consent of Pate eatytical Services,LLC. Page 69 of 96
I

Pace Analytical Services,LLC
Analytical aee g 2225 RiverSHe Or.
t rrnw(yreadcgvn ASheville.NC 28804
(628)25487176
QUALITY CONTROL DATA
Project: Low 8 Bomar Inc 1210140
t Pace Project No.: 92350243
i
METHODBWVK: 2062362 Matrix: Wales
Associated Lab Samples: 92350243010,92 3 5 0 24 3 011,92350243012,923SON3013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
3 Hexachloro 1,3-butadiene ug/L NO 50 0810911722:12
Hexachlorobenzene ug/L ND 50 0810911722:12
Hexachlorocyclopentadiene age- ND TOB 0810911722:12
Hexechlomethane ug/L ND 5.0 0810911722:12
T Indeno(1,2.3-cd)pyrene ug1L ND 5.0 08/0911722:12
( Isophorone apt. ND 10.0 0810911122:12
N-Nitroso of n-propylamine ugT NO 50 0810911722'12
j N-Nitrosommelhylamine ugo- NO 5D 0810911722:12
N-Nilrosodiphenylamme, ug/L ND 10B 0810911722:12
_ Naphthalene ugo- ND 5.0 08/09/1122:12
Nprobenzene call. ND 50 0810911722:12
# Pentashlorophenol ug)L ND 10.0 08/0911722'12
Phenanthrene ug/L NO 50 0810911722:12
( Phenol ug1L ND 50 0810911722:12
Pyrene ug/L ND SO 0810911722:12
- 2,4,6-Tribromaphenal(S) % 74 10,137 0810911722:12
2-Fluorobiphenyl(S) % 66 15-120 0810911722:12
2-Pluamphenol(S) % 37 10-120 08109/1]22:42
5 e Wmbnowmar-15(S) % 67 10420 08/0911722:12
1 .,4Phenol d6(8) % 26 IR120 08/0911722'12
Terphenyl-d14(8) % 70 11-131 0810911722:12
LABORATORY CONTROL SAMPLE 2062383
Spike LCS LCS %Res
j Parameter Units Cons. Result %Rea Limits Oualifiers
I,24-Tdchlorobenzene ug)L 50 263 53 44-142
1,2-Diphenylhydrazine ug/L 50 380 76 25-150
3
1,3-Dichlorobenzane call. 60 243 49 1-172
14-Dichlombenzene ug/L 50 251 51 20}124
2,2'-OxybisH chlommapane) u,T 50 31.8 64 36-166
2,4,64tichlommorol ug1L 50 322 64 37-144
2,4-Dichlorophenol and- 50 36.5 73 1491
2,4-Dimethylphenol ug1L 50 NS 70 32-119
2.4-Dinibophenol mpL 250 800 32 1-181 '..
I 2,4-Dinitrotoluene og/L 50 38.2 76 39-139
2,6-Dinitrotoluene uglL 50 39A 78 50-158
2 Chloronamthalene ugh- 50 330 66 60-148 '..
2-ChImophenol ugT 50 34A 68 23-134 '..
2 Nipophenol ug/L 50 35.9 72 29182
W-Melhylphenol(m&p Cresol) ua1L 50 28.8 58 26-150
3,3'-Dichloomenzidme apt- 100 ]]4 ]] 1-262
4.6-Dinite-2-methylpheao1 ug/L 100 53S 54 1-181
4-Bromophenylphenyl ether call. 50 31.3 63 53-127
4-Chloro-3-methylphenol uglL 100 705 71 22-147
t RqullS pre-+enl¢O Cn lhLL pagearelnlhe unil3 intliCeleE by lM1C"UN1a"cClumnexcepl xOereaa alternate uniU9 preaen1e41C @erlgbto(Ihe result.
f
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REPORT OF LABORATORY ANALYSIS
This o pon aha8 ret ac repmeuced,exwpt in fro,
Dale:OW2212UI 710:12 AM withool the wen-ccr,,M at Pace Analytical Scnicee,TO Page]0 of 96
S
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1
( Pace Analytical Sereces,LLC
E _ aceAnaljftals 2225 RA'erage Dr_
Asheville,NC 28804
stearseseceam
(e28)259-1116
QUALITY CONTROL DATA
Project: Low&Boner Inc 1210140
Pace Project No.: 92350243
LABORATORY CONTROL SAMPLE: 2062363
7 Spike LCS LCS %Rec
Parameter units Conc. Result %Rec Limits Qualifiers
-i 40TIGrophenylphenyl ether uglL 50 32.3 65 25-158
4 NAmphenol ug/L 260 60.2 24 1-132
Acenapblhene uge- 50 35.0 70 47-145
Acenaphthylene ug1L 50 35.5 71 33 145
Anthmcene uglL 50 37.6 75 1-166
} Benzo(manthracene ugh- 50 40.2 80 33-143
Benzo(a)pyrene ug/L 50 37A 74 17-163
Benzopeftoranthene ug/L 50 37S 75 24-159
Benzo(g,h,hperylene ug/L 50 38.2 76 1-219
Bence(Milumanthene ugh- 50 37.2 74 /1-162
bis(2-Chloroetme hpiethane uglL 50 33.5 67 33-184
bis(2-Chlorcethyl)ether ug/L 50 332 66 12-158
bls(2-Eihylhexyl)phlhalate og/L 50 393 79 8-158
i Butytbenrylphthalate ugfL 50 38.9 78 1-152
' ;nrympo ug/L 50 40.9 82 17-168
Or butylphthatate uglL 50 37.9 76 T-118
3 DI-n-octylphlhalate uglL 50 40.6 81 4-146
Dibenz(a,h)anlhracene ug/L 50 37.5 75 1-227
Diethylphthatate ug/L 50 36A 73 1-114
"91methylphthalate uglL 50 Us 70 1-112
;jiumanlhene ug/L 50 381 77 26-437
3 Fluarene uglL 50 36.6 73 59-121
Hexachlom-93-butatliene uglL 50 234 47 24-116
Hexerchlombenzene uglL 50 368 74 1-152
Hexachlomcydopenlatlfene ug/L 50 265 51 25-150
1 Hexachloseethrne ug/L 50 23.7 47 40-113
mJmo(1,2,3-Whymne ugh- 50 38S 77 4-171
Isophoome, ug/L 50 38.9 78 21-196
N-Nilroe-di mpropylamine u9IL 50 4T7 83 1-230
N-Ni eemimethylamine ug/L 50 23.6 47 25-150
( N-Nibwoniphalwamine ug/L 50 37.3 75 25-150
Naphthalene uglL 50 31.5 63 21-133
Nibobenzene uglL 50 36A 73 35-180
Pen(achlorophenol ugh- 100 44A 45 14-176
i Phenantmene u,T 50 37.3 75 54-120
j Phenol uglL 50 17.0 34 5-112
Flamm uml- 50 37.3 75 52T 15
f 2,4,&Tnbromlphenol(S) % 75 10-137
2-Plumobiphenyl(8) % 72 15-120
2-Plamopheno1(S) % 42 10-120
Nitumenzene-05(8) % 73 10-120 '..
Pill his(S) % 31 10 120 '..
Terph eryl 114(6) % 72 11-131
i
Hetmr:preaemee un sirs page are In me umrs lnaleelea ormrumlr cousin except Where na owartale unit is presentee m me supreme result.
i
REPORT OF LABORATORY ANALYSIS
- This report shall not he repromiep except In fall,
I Data 08/22/201710:12 AM mil the eritten wn5ent of Pace Anahecal Services,LLC Page 71 of 96
1

I
j Pace Anaty6ca15ervices,LLC
U25aceAna jicalo Ache. Rivers28 04
[ _ ate,NC 26eoa
(e28)254-]476
QUALITY CONTROL DATA
Project: Low&Bona, Inc 1210140
Pace Project No.: 92350243
7
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 20623M 2062365
t MS MSD
92350391001 Spike Spike MS MSD MS MSD %Rae
I Parameter Units Result Cone. Con, Resell Result %Rec %Rec Limits RPD Qual
1,2,4-Trichlorobenzene ug/L NO iW 100 653 596 65 51 44-142 25
1.2 Diphenylhydrazine Gilt, NO Too 100 78.3 67.6 78 68 25-150 15
I 1.3 Dichlorobenzene 0911- NO 100 100 57A 482 58 48 1-172 18
1,4-Dichlorobenzene ug/L ND 100 100 60.1 413 60 48 20-124 22
2,2'-Oxybis(hchioropropene) GOAL NO 100 100 66.4 550 66 55 36166 19
! 2,4,6-Trichlomphenol uglL NO 100 100 29.7 GOA 80 66 37-144 19
2,40chlomphenol uglL NO 100 100 791 664 80 66 1-191 18
2,4-Dimelhylphenol ug/L NO 1OR 100 76.7 62.2 27 62 32-119 21
2,4-Dinilrophenol uglL NO 5g0 500 443 396 89 80 1-181 11
24 Diailmiolmene ug/L NO 100 100 821 710 82 72 39-139 13
2,6 Dioilrololume, mg/L NO 100 Too 821 710 83 71 50-158 15
2-Chlomnaphthalene uglL NO 100 100 72.5 587 72 59 60-118 21 Ml
2-Chlorophenol ug/L NO 100 100 772 600 ]l 61 23-134 24
2-Nilrophenol ugll, NO 100 100 784 632 78 63 29182 21
3&4-Methylphenol(m&p uglL ND 100 100 ]3.] 57.5 74 57 25-150 25
Cresol)
3,3'-Dichicmbenzifto, uglL NO 200 200 111 15.33 6 8 1-262
4,600102-melhylphenol ug/L NO 200 200 189 169 95 84 1-181 11
--.4-Bmmophenylphenyl ether Gga NO 1OR 100 668 57.1 6 57 53127 16
j -Chlo,o-3-melhylphenol ug/L NO 200 200 160 136 80 68 22-147 17
4 Chlorophenylphanyl ether uglL NO 100 100 GOA 590 70 59 25458 it
4-Nilrophenol GOAL NO 500 500 235 199 47 40 1-132 17
[ Acenaphlhene ug/L NO 100 100 75.9 62.9 76 63 47-145 19
3 Acenaphthylene uglL NO 100 100 77.2 621 A 63 33-145 21
Anlhraceoe ug/L NO 100 100 79.0 68.5 79 68 1-166 14
Benzo(a)anthracene ug/L NO 100 100 784 697 78 70 33-143 12
aenzopOpyrene ug/L NO 1GO 100 ]2] 66.9 73 67 17-163 8
Benzo(b)8umanathene uOL NO 10O 100 738 67.9 74 68 24-459 8
Benzo(g,gi)perylene ughL ND iW 100 784 732 78 73 1-219 y
Renzo(k)guomnthene ug/L NO 100 100 729 67.8 73 68 11-162
bis(2-Chloroethoxy)melhane ug/L NO 100 100 7Z7 580 73 59 33184 21
bis(2-Chlomethyl)ether ug/L NO 100 100 72.0 5Z5 72 58 12-158 22
1 bk(2-EthylhcxypphlGMm GgIL NO 100 100 80,5 752 81 75 9-158
j Butylbenzylphlhalate GglL NO 100 100 790 71A 79 72 1-152 10
- Chrysene ug/L NO 100 WO 79.3 928 79 73 17-168 9
Oi-n-butylphthalate ug/L NO 100 Rio 80.4 71.9 80 72 1-118 11
j Di-moclylphihalale ug/L NO 100 100 81A 74S 82 75 4-146 9
i Dlbenz(a,h)anthraaene high- NO 100 100 768 72.5 72 73 1-227 6 '..
Oielhylphlhaiate ug/L NO 1GO 100 791 69.2 79 69 1-114 13 '..
Dimelhylphthalale uglL ND 100 100 75.3 64.3 25 64 1-112 16
Flumanlherm GOAL NO 100 100 79.3 72.2 79 72 26-137 9
Fluorem, ugll. NO 100 100 78.8 664 79 66 59121 17
Hexachioro-1,3-butatliene GgIL NO 100 100 607 48.5 61 48 24-116 22
Henmhio,obenzene mill, NO 100 100 76.6 66.3 77 66 1-152 14
S Hexachlomcyclopentatliene uglL NO 100 100 63.5 488 63 49 25-160 26 '..
Hexachloroelhane uglL NO 100 100 58.5 47.5 58 48 40 03 21
i
� aaemta preaemee an tm.va9e.mmthe Imt:mammm or the'Gans column oxeeptwM1ere ao aeemmeom fe v,e..:mee tome nom oun=res.n.
7 }
REPORT OF LABORATORY ANALYSIS
a
This repoM1 sha!I net be reprptlucetl,except in fu!I,
Data 081221201710:12 AM W,Ihc0 the wnthea consent of Pace Analytical Services,LLC Page 72 of
t

Pace Analytical services,LLe
aceAnalytical4 2225 mythical,0r.
xrvapambDxmn Asheville.NC 28804
[phone]
I
I
QUALITY CONTROL DATA
Project LowB Bonar Inc 1210140
Pace Project No.: 92350243
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 20623M 2062365
I MS MSD
! 92350391001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cane. Cone. Result Result %Rec so gee Limits RPD Ones
IodenoI12.3-ed)pyrene ugi NO 100 100 77.6 73.3 78 73 1-171 6
j Ismmusene TgIL NO 100 100 83-1 67.6 83 68 21-196 20
N-Nites0-di-n-propylamine hg/L ND 100 100 89.8 72S 90 73 1-230 21
7 N Nibosodimethylamine mglL NO 100 100 654 502 65 50 25150 26
t N-Nitrosodiphenylamine uglL ND 100 100 ]8.] 68.5 79 69 25150 14
y Naphthalene TILL NO 100 100 70,6 57.4 ]i 57 21-133 21
Nitrobenzene ug/L NO 100 100 766 621 ]] 62 35-180 21
Pervachlomphenol ugLL ND 200 200 155 141 ]] ]i 14-176 9
Phenanthree, ui ND 100 too 780 68.3 78 68 54-120 13
3 Phenol Tell- NO 100 100 485 362 49 36 5-112 29
Pyrene uglL NO 100 Too 954 67.2 75 67 52-115 12
2,4,6-Tnbromophenol(8) % 88 79 10-137
} 2-Fluorobiphenyl(8) % 75 60 15120
P 2-Flumaphenol(S) % 55 42 10-120
I NiVobenzene-d5(S) % 74 60 10-120
- Phenol d6(S) % 46 35 10-120
I Terphe0yld14(S) % 62 43 11-131
:1ATRIX SPIKE B MATRIX SPIKE DUPLICATE: 2062366 2062367
MS MSD
j 92350391002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Can. Cone, Result Result %Rec %Rec Limits RPD Coal
1,2,4-Trichlombenzene ugrL NO 100 100 627 58A 63 58 44-142 8
12-Diphenylhydra¢ioe uglL NO 100 100 73S 70.2 74 70 25-150 5
1,3-Dichlorobenzene upL NO 100 100 58.1 55.1 58 55 1-172 5
1.4 Dichlombennene mill, ND 100 too 59A 554 59 55 20124 6
2,2'-Oxybis(1-rnloropropane) Tell- NO 100 100 61.6 57.5 62 57 38-166 ]
2,461dchlorophenol upt. ND 100 100 747 754 75 75 37-144 1
2.4-Dichlorophenol uglt ND 100 100 76.7 710 ]] 72 1-191 6
2,4-Dimethylphenol Tgi NO 100 100 726 69.1 73 60 32-119 5
2,4-Dinitrophenal ui ND 500 500 453 441 91 88 1-181 3
2.4-Dinitrotoluene ui NO 100 100 ]].2 ]].6 ]] 78 39-139 0
- 2,6-0initrosImme upL NO 100 100 78.8 79.9 79 80 50-158 1
2-Chloronaphthalene mill- NO 100 100 672 66.0 62 66 60-118 2
2 Chlorophenol u,I- NO 100 too 702 61.2 70 67 23-134 4
2-144mphenol hurt ND 100 100 73-1 704 73 70 29-182 4
I 384-Methylphenolerri TgIL NO 100 100 1 59.9 67 60 25150 it
Cresol) '..
3.3'-Dichlorobenzidine ug1L NO 200 200 8.5J WATT 4 5 1-262 '..
4.6-Dinitro-2-methylphenol TpL NO 200 200 189 179 94 90 1-181 5 '..
3 4 Bromapherylphenyl ether ugn, ND 100 100 64A 60.5 64 61 53-127 6 '..
4 Chloro-3 methylphen el u i NO 200 200 155 146 78 73 22-147 6 '..
4-Chlomphenylphenyl ether ugi ND 100 100 66.2 645 66 65 25-158 2
4 Ndrophenat right, ND 500 500 234 228 47 45 1-132 3 '..
i
ftesulls presented on this page are In the unns lshiose46ylhe'Tnle column exeeptweere in sicall, lairs press. to the heht eRM1e result
j
REPORT OF LABORATORY ANALYSIS '..
This report shall not be reproduced,assets in hil.
Date;0812212017 10,12 AM without the wines consent of Pace analytical Services,LLC Page]3 of 96

Pare Analytical Services,LLC
e 2225 Riverside Dr.
aeeMalytieal Ashoea e,NG 28804
humW
[phone]
i QUALITY CONTROL DATA
i
S
Project lmv8 Bonar Inc 1210140
Pace Project No: 92350243
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2062366 2062367
j MS MSD
92350391002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Conc. Result Result %Rec %Rec Limits RPD Qual
Acenaphthene ug/L NO 100 10D 70.7 70.0 71 70 47-145 1
Acenaphthylene uqT NO 100 100 71.9 70.1 72 70 33-145 2
Anthracene vol- NO 100 100 74.8 71.9 75 72 1-166 4
- Benzopotummacene uglL NO 100 100 771 756 78 76 33143 3
Y Benzo(a)pyrene upl, NO 100 100 72.2 71.1 72 71 17-163 2
6enzo(Ommarr a s, ug/L NO 100 100 74.3 706 74 71 24-159 5
Benzo(g,h,i)perylene ug/L ND 100 100 77S 74.0 77 74 1-219 5
Benzo(k)1luoranthene ug4 ND 1110 100 72.9 72A 73 72 11-162 1
t ble(2-Chloroethoxy)methane ug1L NO Into 100 686 6,L2 69 64 33-184 7
bis(2-Chloroethyl)ether u911- NO 100 100 657 GOT 66 63 12-168 4
Ns(22Ethylh,g,pphthalate ug/L NO 100 100 824 786 82 79 8-158 5
Butylbenzylphthatate GOT NO 100 100 79A 756 79 75 1-152 5
Chrysene toll- NO 100 100 78.9 768 79 77 17-168 3
Di-n-butylphthelate upt- NO 100 100 77A 742 77 74 1-118 4
Dim-octylphthalate upt- NO 100 100 83.5 805 84 81 4-146 4
- Dibenz(olOanthracene ug/L NO 100 100 77,6 759 78 75 1-227 3
Diethylphthalate ug/L ND 100 100 75.2 74.2 75 74 1-114 1
£ Dlmethylphlhalate, ug/L ND 100 100 70.6 740 71 71 4-412 4
,Flumanlhene ug/L NO 1GO 100 773 75.2 78 75 26-137 3
nFluorene toll- ND 100 100 736 721 74 73 59-121 1
Hexacharo-1,3-butadiene ug/L NO 100 100 60A 57,2 60 57 24-116 5
Hexachlorobenzene uqT NO 100 100 73,1 686 73 69 1-152 6
i Hexachlorocydopentadlene uPIF NO 100 100 60.0 56.7 60 57 25-150 6
Hexachloroelhane uglL NO 100 100 MIX 54.4 58 54 40-113 7
Indeno(L2,3 ccupyrene upl- ND 100 100 77S 745 77 75 1-174 4
Isopbmone ug/L NO 100 100 79.0 733 79 73 21-196 7
N-Istroso-di n-propylamine, ug/L ND 100 100 82S 74.9 83 75 1-230 10
N-Ngmsodimethylamine ago, NO 100 100 59.3 547 59 55 25-150 8
I N Nitrosodiphenylamine UOL NO 100 100 74A 714 74 71 25-150 4
Naphthalene ug0. NO 100 100 684 642 68 64 21-133 6
Nitrobenzene uGL NO 190 100 716 68.6 71 69 35-180 3
j Pentachlorophenol ug/L NO 200 200 155 148 78 74 14476 5
PhommthesK, b,F NO 100 100 743 70A 74 71 54-120 5
Phenol muL NO Into Into 44.0 39.5 44 40 5-1t2 11
Pyren, ugF NO 100 100 72.2 68.8 72 69 52-115 5
24,6-Tdbmmophenol(S) % 83 82 10137
2-Fluambiphenyl(8) % 70 69 t5120
2-Flumophenol(S) % 51 47 10-120
Nibobenzerle45(S) % 71 68 10-120
Pheno1-d6(S) % 43 37 10-120
Terphenyl-d14(SO % 56 59 11-131
Reaulla"camueuon@Is macerate shorn la Indicated by the'9nits'column except Ware an allemalench tapmee om mm.n9hlorlmy'res.
1
REPORT OF LABORATORY ANALYSIS
Tms report=_hall not be rePmauced,except m ruq
Date:0 8/2 212017 10012 AM without lhewdtmrmmmrm.f Pace Analytical smv:ces,LLG Page 74 of 96
i

I Pace Analytical Services,U-C
e 2225 Riverside[M
AnalVieal Ce.,ill NC 28804
— a ee cer
[phone]
1
QUALITY CONTROL DATA
i
Project: Low&Banner inc 1210140
I Pace Project No.: 92350243
QC Batch: 372287 Analysis Method SM 2540C
OC Batch Method SM 2540C Analysis Description: 2540C Total Dissolved Solids
Associated Lab Samples: 92350243001,92350243002,92350243003,92350243004.92350243005,92350243006,92350243007,
{ 92350243008,92350243009,92350243010,92350243011,92350243012
1
METHOD BLANK: 2062358 Matrix Wafer
Associated Lab Samples: 92350243001,92350243002,92350243003,92350243004,92350243005,923502430W.92350243007,
92350243008.92350243009,92350243010,92350243041,92350243012
Blank Reporting
Parameter Units Result Limit Amlyzed Qualifiers
Total Dissolved Solids mglL NO 25 0 08/08/17 09,27
's
LABORATORY CONTROL SAMPLE: 2062359
j Spike LCS LCS %Rec
Parameter Deals Come. Result %Rec Limits Qualifiers
- Total Dissolved Solids ri 250 234 94 90-110
}
SAMPLE DUPLICATE: 2062360
92350128001 Cup
Parameter Units Result Result RPD Qualifiers
�olal Dissolved Solids mglL 187 183 2
3
SAMPLE DUPLICATE: 2062361
92360243003 Oup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids UET 570 59B 3
j
7
t
I
3
i
t
P Resullaprea¢nour an lOis pagearein Ina ep115 inJI<aled 4y lM1e'Ilnlla"column extepl..,a an allemale until lspreaenl¢E I¢111¢dust Of lM1[resull.
I
-' REPORT OF LABORATORY ANALYSIS
This repent shal rat be reprodeeed.except in lull,
Date:OW2212017 1012 AN without Vie wdflen consent of Pace Analytical 6ervlWs,LLC. Page 75 of 96
7

EPace Analytical Service.,LLC
a
aceMalytical225 Riva,eep
f _ ASM1aville,NC 2a804
xuwf elswm04
[phone]
t
QUALITY CONTROL DATA
Project: Lay.&Senator Ina 1210140
Pace Project No.: 92350243
DC Batch: 372409 Analysis Method: SM 2540C
QC Batch Method: SM 2540C Analysis Description: 25400 Total Dissolved Solids
Associated Lab Samples: 92350243013
METHOD BLANK: 2053178 Malrix: Water
Associated Lab Samples: 92350243013
Blank Reporting
# Parameter Units Result Limit Analyzed Qualifiers
j Total Dissolved Solids mgfL ND 25.0 08I08fi]i]'S2
3
- LABORATORY CONTROL SAMPLE: 2063179
- Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Clothes
Total Dissolved Solids mgfL 250 238 95 go 110
i
SAMPLE DUPLICATE: 2063180
92350243013 cup
i Parameter Units Result Result RED Qualifiers
- Total Dissolved Solids mgfL 830 94B 12 D6
SAMPLE DUPLICATE: 2063181
92350232ON Our
Parameter Units Result Result RED Qualifiers
3 Total Dissolved Solids mglL ND NO
3
,1
ji
fj
S
I
I
(
i
ReaellepresenfeJ on lhla pageam In lha oohs lntllcafeJ Lylhe'Ilnits"column except xfiere an a0ernate unit is presenfeJ to lOe nBaf ollM1e result.
i
REPORT OF LABORATORY ANALYSIS
' The reperc snen not he reproaeeea,except in twl,
Dale:08122f2017 10:12 AM without theemihen Consent of Pace Analytical Semrea,LC Page]6 of 96
j
t
ti

] Pace Analytical Senator,LLC
Ii
Riv Or
aceAnapicalB Acrole NO 28904
narepewe son
(828)254-I116
't
^1
QUALITY CONTROL DATA
i
Project Lmv&Sonar Inc 1210140
I Pace Project No.: 92350243
QG Batch: 372272 Analysis Method: SM 2540D
' QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
' Associated Lab Samples: 92350243001,92350243002,92350243003,92350243004,92350243W5,923502430W.9235024300],
s 92350243008
METHOD BLANK: 2062327 Matrix: Wale,
Associated Lab Samples: 92360243001,9235024302.92350243003,92350243004.92350243005,92350243006,92350243 W],
92350243008
Blank Reporting
- Parameter Units Result Limit Anatyzed Qualifiers
Total Suspended Solids nggl- NO 2.5 0810811716:57
LABORATORY CONTROL SAMPLE: 2062328
_ Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Litnils Quafrters
j Total Suspended Solids mglL 250 274 110 90-110
(j
SAMPLE DUPLICATE 2062329
b 92350123001 Dup
Parameter Units Result Result RED Qualifiers
jotal Suspended Solitls mg/L NO NO
9
SAMPLE DUPLICATE: 2062330
92350141001 Dup
Parameter Units Result Result RED Qualifiers
Total Suspended Solids mglL NO NO
j
1
assunspresenled on this page are Inner units Indicated ulgh.-oohs"c.Nuor elang wLere an all¢mala unit is preseneal(o are target the result.
}
REPORT OF LABORATORY ANALYSIS
t1 This pand'hug'at be reproduced,dre"a in full
! Data 0812212017 10:12 AM whom the wdnen consent of frock Akabscal Serires,LLC Page 77 of 96

I
Paco Analytical Services,LLC
aeeAnalytieal o eca s,Nf 28 04 i Polecats,NC 2aae4
I
QUALITY CONTROL DATA
t
Project: Low&Sonar Inc 1210140
Pace Project No.: 92350243
OC Bateh: 372363 Analysis Method: SM 2540D
t
QC Balch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92350243009.92350243010,92350243011,92350243012,92350243013
METHOD BLANK: 2062857 Matrix: Water
Associated Lab Samples: 92350243009,92350243010,92350243011,92350243012,92350243013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 25 081081i)t3:49
f
_ LABORATORY CONTROL SAMPLE: 2062858
Spike LCS LCS %Rec
- Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mglL 250 232 93 90-110
SAMPLE DUPLICATE: 2062859
j- 92350243009 Pop
9 Parameter Units Result Result RPD Qualifiers
I Total Suspended Solids ren- NO NO
i
SAMPLE DUPLICATE: 2062860
3 92350369001 Dup
Parameter Units Small Result RPD Qualifiers
Total Suspended Solids mgll 227 180 23 D6
1
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S
7#
S
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E
3
'i exer" pttsenled on lhla Page are l a lie units lunica@J to 1be'Va.,—fumnevRpl noerea,chances unit la Prevented to the right arms result.
l
t REPORT OF LABORATORY ANALYSIS
i
This report shall be rtl,except in tell,
j Date:0822120D ID:12 AM waCoul Me written consent
Pace A ce
nt of Pace natyCral Services,ILG Page 78 of 96
l
j

® Pace Analytical Services.LUG
aeeAnalytieai 2225 RiversNe Or.
a»wCacteen wn ASM1eville,NC 29804
(828)2M-7176
i
QUALITY CONTROL DATA
Project Levy&Bonar Inc 1210140
Pace Project No.: 02350243
I OC Batch: 372455 Analysis Method: EPA 350.1 1993 Rev 2U
3
QC Balch Method: EPA 350.11993 Rev 20 Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92350243001,92350243002,92350243003,92350243004,92350243005,92350243006.92350243007,
92350243008,92350243009.92350243010,92350243011,92350243012,92350243013
METHOD BLANK: 2063497 Matrix: Water
Associated Lab Samples: 92350243001,92360243002,92350243003,92350243004,92350243005,92350243006,92360243007,
_ 92350243000,92350243009,92350243010,92350243011,92350243012,92350243013
Blank Reporting
{ Parameter Units Result Limit Analyzed Qualifiers
Nitrogen,Ammonia mglL NO 0.10 0810911702:37
3
LABORATORY CONTROL SAMPLE: 2063498
Spike LCS LCS %Rec
Pafameter Units Cone. Result %Rec Limits qualifiers
j Nitrogen,Ammonia mglL 5 4.7 95 90110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2063499 2063500
MS MSD
92350183901 Spike Spike MS MSD MS MSD %Rec
s Parameter Units Result Cone, Cone,. Result Result %Rec %Rec Limits RPD Coal
-
i Nitrogen,Ammonia mglL NO 5 5 47 4.8 95 95 90-110 0
$
7 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2063501 2063502
MS MSD
92350243OW Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Con, Con, Result Result %Rec %Rec Limits RED Dust
Nitrogen,Ammonia raga- NO 5 5 4.8 5.0 96 100 90-110 4
1
3
3
3
S
3
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Reaulle Presenlal on vio pageare In IM1e units iurnere l by ILe-Uni a column exeepl xTere an attemale unit is porchro010 the right or vie reach.
1
REPORT OF LABORATORY ANALYSIS
i
mis report sM1a!I not reproduced,exists n fml.
]j Date:08122I201210,12 AM cement Pro wrihes consem of Pace Analytical Servlcee,ua Page 79 of 96
#

' Pace Anatytinal Service.,LLC
2225 Mercado Oc
aeeAna yieal Asbev:Ile,NC 28804
J wwwf 3PM g2m2Ct 7476
i
1 QUALITY CONTROL DATA
i
j Project Low&Boner Inc 1210140
Pace Project No.: 92360243
i
j QC Batch: 372344 Analysis Method: EPA 351.2
( OC Batch Method: EPA35L2 Analysis Description: 3512 TKN
Associated Lab Samples: 92350243001,92350243002,92350243003,92350243004.92350243005,923502430W.92350243007,
92350243008,92350243009,92350243010,92350243011,92350243012,92350243013
j METHOD BLANK: 2062669 Matrix: Wafer
1 Associated Lab Samples: 92350243001,92350243002,92350243003,92350243004,92350243005,923502430W,9235024300],
92350243008,92350243009,92350243010,92350243011,92350243012,92350243013
Blank Reporting
Parameter Units Result Limit Analyzed Cautious
Nitrogen,Kjetdahl,Total mg/L ND 0.50 08/09I1]16:45
LABORATORY CONTROL SAMPLE: 2062670
Spike LCS LCS %Rec
Pummeler Unite Cone. Result %Rec Limits Qualifiers
Npmgeo.Kjeltlahl,Total Mgt 10 10.1 101 9IT 0
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2062671 2062672
MS MSD
3 92350447001 Spike Spike MS MSD MS MSD %Rec
_ 1 Parameter Units Result Cons. Cone. Result Result %Rec %Rec Limits RPD Coal
Nitrogen,Kjeltlahl.Total mglL ND 10 10 10A 110 102 107 90-110 5
MATRIX SPIKE S MATRIX SPIKE DUPLICATE: 2062673 2062674
MS MSD
923502430M Spike Spike NIS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result %ftec %Ron Limits RED Coal
Nitrogen,Kjeltlahl,Total mglL 1] 10 10 12 G 12.4 109 107 90-110 1
S
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}
REPORT OF LABORATORY ANALYSIS
This repop shall set be reprotlucetl.except in full.
Date:08122/201710:12 AM without the written cchnsent of Pace Analytical Services,LLC Page 80 of 96
i
3

Pace Analytical Services,LLC
aceAnalVical s 222a Rive`31ae 0,
_ AsnevOe,NC 26804
ack leee case (821A254-7176
i QUALITY CONTROL DATA
j
Project: Low&Boner Inc 1210140
Pace Project No.: 92350243
OC Batch: 3724M Analysis Method EPA353.2
OG Balch Method EPA 353.2 Analysis Description: 353.2 Nitrate r Nitrite,preserved
Associated Lab Samples: 9235)243001,92350243002,92350243003
METHOD BLANK: 2063547 Matrix: Water
Associated Lab Samples: 92350243001,92350243002,92350243003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
j Nitrogen,NO2 plus NO3 mg/L NO 0.020 0W09117 11:34
I
i LABORATORY CONTROL SAMPLE: 2063548
j Spike LCS LCS %Rec
Parameter Units Cone. Result %Rec Limits Qualifers
Nitrogen,NO2 plus NO3 mg/L 2S 2.5 101 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2063549 2063550
1 MS MSD
92350049003 Spike Spike MS MSD ME MSD %Rec
Parameter Units Result Conc. Coma Result Result ARec %Rec Limits RED Coal
Nitrogen,NO2 plus NO3 mglL 0.48 25 25 30 3.0 100 100 75-125 0
- MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2063551 2063552
t h1S MSD
92350118001 Spike Spike MS MSD MS MSD ARec
j Parameter Units Result Cone, Come, Result Result %Rec %Rec Limits RED Oual
Nitrogen,NO2 plus NO3 mg11 Bla 2.5 25 26 2.6 97 97 75-125 0
i
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}
} REPORT OF LABORATORY ANALYSIS
]ma repon shall net be repmaaced,excep)m rw,
Date:0812212017 R A2AM w0bomthewrfffen nonaemof P—Aoelyfl,al SerNces,LLC- Pepe 81 of 95
3

}
Pace Analytical Services,LLC
aceAnaXjcal` Ri"areda°`
3 Asheville,NC 28804
j [phone]
3 F
QUALITY CONTROL DATA
j "eject: Lmv 8 Sonar Inc 1210140
Pace Project No: 92350243
QC Batch: 372467 Analysis Method EPA353.2
QC Balch Alethod: EPA353.2 Analysis Description: 353.2 Nitrate 4 Nitrite,preserved
1 Associated Lab Samples'. 92350243004,92350243005,92350243006,9235024300],92350243008.92350243009,92350243010,
92350243011.92350243012,92350243013
- METHOD BLANK 2063553 Matrix: Water
j Associated Lab Samples: 92350243004,92350243005,92350243006,9235024300].92350243008,92350243009,92350243010,
? 92350243011,92350243012.92350243013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen,NO2 plus NO3 mglL ND 0.020 0810911712:07
LABORATORY CONTROL SAMPLE. 2063554
- Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen,NO2 plus NO3 mgfL 2.5 2.5 101 90-110
3
- MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2063555 2063556
MS MSD
92350243ON Spike Spike MS MSD MS MSD %Rec
Pummel¢, Units Result Conc. Conc, Result Result %Rec %Rec Limits RPD Qual
- 'Nilmigen,NO2 plus NO3 mglL 0059 2.5 2A IA 1.4 54 54 75-125 0 M1
j MATRIX SPIKE&MATRIX SPIKE DUPLICATE 2063557 2063558
_ MS MSD
92350460002 Spike Spike MS MSD MS MSD %Rue
Parameter Units Result Conc, Conc. Result Result %Rec %Rec Limits RPD Qual
Nitrogen,NO2 plus NO3 mg/L 261 2.5 2S 28.5 284 69 64 75-125 0Me
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REPORT OF LABORATORY ANALYSIS
- This report scar al be reproduced,
Analycacentvi roe,
Dale:08122I201710:12 AM without the wnsem of Paw Analy(ISenzes.LLG Page 82 o196
j

Pace Analytical 3ervices,LLC
' r�/+QAA '/}/. 2225 Fawicitle 01
ZeA
I �alcata AcheNlle,NO 28804
(828)25491]6
I
QUALITY CONTROL DATA
Project: LOW 8 Bona, Inc 1210140
l
Pace ProjeG No.: 92350243
QC Batch: 372248 Analysis Method: EPA 365.1
QC Batch Method EPA365.1 Analysis Description: 365.1 Phosphorus.Total
Associated Lab Samples: 92350243001,92350243002
METHOD BLANK: 2062222 Matrix'. Water
Associated Lab Samples: 92350243001,92350243002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
t Phosphams mg)L NO 0050 08108/170723
LABORATORY CONTROL SAMPLE 2062223
Spike LCS LCS %Rec
Parameter Units Cone. Result %Rec Limits Qualifiers
j Phosphorus mg/L 2S 2.5 101 90.110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2062224 2062225
MS MSD
92350024001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone Cone. Result Result %Rec %Rec Limits RED Dual
'jhosphoma ned, 4.1 2.5 2.5 ].0 68 115 109 90-110 2 M1
's
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2062226 208222]
t MS MSD
92350049011 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cane. Cone, Result Result %Rec %Re. Limits RPD Quad
Phosphorus mglL 0.060 25 2.5 26 2.6 103 101 90-110 2 '..
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REPORT OF LABORATORY ANALYSIS
This report luau not be reprotlucetl,except in lull,
i Date:08122/201710:12 AM wAom thawratenoonsentol Pace AnalycPsl Services LLG Page 83 of 96
E
1

Pace Analytical Services,LLC
E
aceAnalytical Riversi201
( _ Asheville,NC 28 804
(828)2544176
QUALITY CONTROL DATA
I
Project: LowB Boner Inc 1210140
Pace Project No.: 92350243
7
QC Batch: 372619 Analysis Method: EPA 365.1
( QC Batch Method: ERAMS1 Analysis Description: 365.1 Phosphorus,Total
Associated Lab Samples: 92350243003
METHOD BLANK: 2064851 Matrix: Water
Associated Lab Samples: 92350243003
j Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
j Phosphorus mglL NO 0,050 08/10/17 Gl
1
LABORATORY CONTROL SAMPLE: 2054852
"( Spike LCS LCS %Rae
Parameter Units Cone. Result %Rec Limits Qualifiers
Phosphorus mg1L 2.5 2.7 106 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2064853 2064854
MS MSD
- 92348822001 Spike Spike MS MSD MS MSD %Rec
5
Parameter Units Result Cona Conc. Result Result %Rec %Rec Limits RPD Qual
s,hospholna mglL ZB 25 2.5 70.M1 10.8 113 141 90410 1 Mi
7
- MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2064855 2064856
MS MSD
92350792001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Gone Conc, Result Result %Rec %Rec Limits RPD Qual
Phosphorus mgd- 0,069 2.5 2.5 2.8 2.9 109 113 90-110 4 MI
I
3
T
1
3
i
I Resulla Presenletl an tals PaBa ar¢inlM1e unite in0lcatetl 4Y t0e"Ilnils'column¢[rePtwM1er¢an allemate unl(IS Presenletl to lee naatollFe reaufl.
j REPORT OF LABORATORY ANALYSIS
This repoe.bar net be reprotluced except a sell
On(e:0812212 01 7 10:12 AM wimom the nRes consent of Pace Analy(tal ts, ,LLC. Page 94 of 96

Pace Analytical Services.LLC
Analytically 2225 moored,Dr.
j Ashav,a NC 26804
rowers apron ki28d!r1-]176
1
3
QUALITY CONTROL DATA
Project: Low&Boner Inc 1210140
Pace Project Na,: 92350243
1
QC Batch: 372680 Analysis Method EPA 385.1
DC Batch Method: EPA 365.1 Analysis Descfiption: 365.1 Phosphorus,Total
( Associated Lab Samples: 92350243004,92350243005,92350243006,92350243007.92350243008,92350243009.92360243010,
92350243011,92350243012,92350243013
METHOD BLANK: 2064857 Matrix: Water
Associated Lab Samples: 92350243004,92350243005,92350243006,92350243007,92350243008,92350243009,92360243010,
92350243011,92350243012,92350243013
Blank Reporting
- Parameter Units Result Limit Analyzed Qualifiers
Phosphates m911- NO 0050 081101
t
S
LABORATORY CONTROL SAMPLE: 2064858
Spike LCS LCS to Rae
Parameter Units Conc. Result %Her, Limits Qualifiers
Phosphorus mg/L 25 21 108 90-110
1
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2064859 2064860
j MS MSD
92350243ON Spike Spike MS MSD MS MSD %Ree
Parameter Units RAWL Gonc. Conc, Result Result %Rec %Rec Limits RPD Qual
Phosphorus mpl- NO 25 2.5 21 26 106 104 90-110 2
3
MATRIX SPIKE&MATRIX SPIKE 20 K DUPLICATE. 2069862
a MS MSD
92350581007 Spike Spike MS MSD MS Wit %Rec
i Parameter Units ftesM Conc. Cone Result Result %Rec %Rec Limits RPD Oral
Phosphatesmg/L 0.077 25 2.5 2.8 2.9 TH 111 90110 0 M1
9
1
S
s
S
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a
Results peesenletl on Iry15 page artln 0a unI151ntllcateJ Oylhe'Unils"volume except"ere an partner real Is pmsented to the eight of the result
j
REPORT OF LABORATORY ANALYSIS
i
This report shall rite ne repmaucea,except n ten,
- Data 0 812 212 01 7 1 0:12AM without the written consent of Pace Arelyrcal 8ersces,LLC. Page 85 of 96

or
Pace Analytical Services,LLC
' 2225 Reg-rune 0,
aceftlAcal® Asheville,NC 206W
jxnw�.S6iam (828)254-)1]6
I
I
j
QUALITY CONTROL DATA
Project Low&Sonar Inc 1210140
Pace Project elo: 92350243
QC Balch: 372202 Analysis Method: SM 5220D
QC Balch Math.d: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92350243001,92350243002,92350243003,92360243004,92350243005.92350243006,92350243007.
92350243008,92350243009.92350243010.92350243011,92350243012,92350243013,92350243014
METHOD BLANK: 2061991 Matrix: Water
Associated Lab Samples: 92350243001,92350243002,92350243003,92350243004,92350243005,92350243005,92350243007,
92350243008,92350243009,92350243010,92350243011.92350243012,92350243013.92350243014
Blank Reposing
Parameter Units Result Limit Analyeed Qualifiers
Chemical Oxygen Demand buT ND 25.0 08107/1718:41
I
t LABORATORY CONTROL SAMPLE: 2061992
Spike LCS LCS %Rec
Parameter Units Con.. Result %Rec Limits Daughters
Chemical Oxygen Demand m uL 750 749 100 90-110
t MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2061993 20619M
I MS MSD
92350153001 Spike Spike MS MSD MS MSD %Rec
Parameter Ungs Result Cone. Conc, Result Result %Rec %Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 8750 750 750 8590 8410 -21 45 90110 2M6
- MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2061995 2061995
MS MSD
j 92350243005 Spike Spike MS MSD PAS MSD %Rec
Parameter Units Result Gone Conc. Result Result %Bee l Bee Limits RPD Qual
Chemical Oxygen Demand mglL 422 750 750 1170 1190 100 102 90-110 1
f
3
I
3
3
a Reaupa p@s¢pl¢tl on lM4 Page arelnthe uni141n01caleJ by IM1e"an114"column except Waere an allemal¢unitla pr¢4¢nletl to the tlgM of the result.
REPORT OF LABORATORY ANALYSIS
s
- This repmR shall not he reprotluced,except in(a!I,
Dale:09I22I2017 10:12 AM vrmovt the emblem consent at Pace Amar,beal Serioea,TO Page 860196
i

I Pace Analytical Services,LLC
2225 Flversae or.
/_ aceAnalytical Aehevilla.NC 28804
as
I (s20)250.]1]6
1 QUALIFIERS
Project: Low&Sonar Inc 1210140
Pace Project No,: 92350243
3 DEFINITIONS
OF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
NO-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J�Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit,
PQL-Practical Cohabitation Limit.
RL-Reporting Limit
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Amicahzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrmorded data are displayed and have been used to calculate°h recovery and RED values.
i LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
OUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
y SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
AGd preservation may not be appropriate for 2 Chlomethylvinyl ether,
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
- Method 8280,
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for
each analyle is a combined concentration.
Pace Analytical is TNl accredited.Contact your Pace PM for the current list of accredited analyfes.
TNI-The NELAC Institute.
I
LABORATORIES
- PASI-A Pace Analytical Services-Asheville
l PASIC Pace Analytical Service.-ChrrhAte
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non target analytes or other matrix interference. '..
3 D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
L1 Analyte recovery in the laboratory control sample(LCS)was above QC limits, Results for this analyte in associated
samples may be biased high
me Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
' Mt Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovi
i
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against conirci limits due to sample dilution. '..
3 S4 Surrogate recovery not evaluated against control limits due to sample dilution,
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REPORT OF LABORATORY ANALYSIS
This report shall not be reProduoed,.—,l I.hill,
t Date:08122!2017 10:12AM without me writer consentol Pace Ana;ytical Service,LLC. Page 87of 96
i
i

Pace Analytical Services,LLC
i 5ceAna[Xlca' 2225 R NC 2e Dr.
I wxearn ASM1eville, 2B804
(828)254-]1]6
1
QUALITY CONTROL DATA CROSS REFERENCE TABLE
i
j Project: Law&Bonar Inc 1210140
{ Pace Project Nor: 92350243
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92360243001 Chiller Room(0-58) EPA 1664E 373777
92350243002 Slim Tank EPA 1664E 373777
j 92350243003 Cooper Cooling System EPA 1664E 373777
92350243004 MI&M4 Room Quench EPA 1664E 373777
3 923:024300: MS Room Quench EPA IW48 373777
9230243006 Boiler Condensate EPA 16648 373777
I 92350243007 Basement Groundwater EPA16648 373777
92350243008 Downstream @ Manhole 25 EPA 1664E 373777
7 92360243009 New Stormwater Point EPA 1664E 373777
92350243010 East Ditch EPA 1664B 373777
92350243011 City Water EPA 16MB 373777
1 92350243012 Manhole 3 EPA 1664B 373777
s
92350243013 Manhole 3-11 EPA 1664E 373777
92350243001 Chiller Room(0-58) EPA200.7 372225 EPA2001 372380
92350243002 Slim Tank EPA2007 372225 EPA200.7 372380
92350243003 Cooper Cooling System EPA 200.7 372225 EPA2009 372380
92350243004 MI&M4 Room Quench EPA2003 372225 EPA2009 372380
92350243005 MS Room Quench EPA2001 372225 EPA200.7 372380
i 92360243006 Boiler Condensate EPA2001 372225 EPA2007 372380
92350243007 Basement Groundwater EPA200] 372225 EPA200.7 372380
}2350243008 Downstream @ Manhole 25 EPA200.7 372225 EPA200.7 372380
I
92350243009 New Stormwater Point EPA 200] 372445 EPA 200.7 373139
92350243U1U East Ditch EPA2007 372445 EPA2001 373139
92350243011 City Water EPA200.7 372445 EPA200 7 373139
j 92350243012 Manhole 3 EPA200.7 372445 EPA2003 373139
92350243013 Manhole 3-U EPA200.7 372445 EPA200] 373139
92350243014 Stamay EPA 200.7 372445 EPA2001 373139
92350243001 Chiller Room(0-58) EPA245.1 372256 EPA245.1 372316
92350243002 $lim Tank EPA 245A 372256 EPA245A 372316
92350243003 Cooper Cooling System EPA 245-1 372256 EPA245.1 372316 '..
92350243004 MI&M4 Room Quench EPA24&I 372250 EPA 245.1 372316
92350243005 MS Room Quench EPA245A 372256 EPA245.1 372316 '..
92360243006 Boilar Contlensate EPA2451 372256 EPA 245.1 372316 '..
} 92360243007 Basement Groundwater EPA245.1 372256 EPA 245.1 372316
92350243008 Downstream @ Manhole 25 EPA24SI 372256 EPA246A 372316
92360243009 New Stormwater Point EPA245.1 372458 EPA 2451 372520 '..
i 92350243010 East Ditch EPA245.1 372458 EPA 2451 372520
92360243011 City Water EPA245A 372458 EPA245.1 372520
92360243012 Manhole 3 EPA245.1 372458 EPA245.1 372520 '..
i
92350243013 Manhole 3-1.1 EPA 245A 372458 EPA245A 372520
92350M3001 Chiller Room(0-58) EPA625 372134 EPA625 372231
3 9235ON3002 Slim Tank EPA625 372134 EPA625 372231
92350243003 Cooper Cooling System EPA625 372134 EPA625 372231
92350243004 MI&M4 Room Quench EPA625 372134 EPA625 372231
92350243005 M5 Room Quench EPA625 372134 EPA625 372231
j 92350243006 Boiler Condensate EPA625 372134 EPA625 372231
i
3
—" REPORT OF LABORATORY ANALYSIS
- This laical shall not tre o produced.except In full,
Date:0812212017 1O:12 AM without thewnnen consent of Pace Anal10ral Senecas,LLC. Page 88 of 96
I
i
l

3
i Pace Analytical Services,LlC
aceAnaiytical a 2225 R—otta 0,
_ rvwxpasea'c,. Ash eWIe,NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project Low&Bonar Inc 1210140
3 Pace Project No.: 92350243
Analytical
# Lang) Sample ID QC Batch Method QC Batch Analytical Method Batch
j 92360243007 Basement Groundwater EPA625 3721N EPA625 372231
92350243008 Downstream @ Manhole 25 EPA625 372134 EPA625 372231
92350243009 New Stormwater Point EPA625 372134 EPA625 372231
E
92350243010 East Ditch EPA625 372288 EPA625 372653
92360243011 City Water EPA625 372288 EPA625 372653
)f 92350243012 Manhele3 EPA625 372288 EPA625 372653
i 92350243013 Manhole 3-U EPA625 372288 EPA625 372653
92350243001 Chiller Room(0-58) EPA624 372395
92350243002 Silm Tank EPA624 372395
92350243003 Cooper Cooling System EPA624 372395
92360243004 Mil&M4 Room Quench EPA624 372395
92350243005 M5 Room Quench EPA624 372395
92350243006 Batter Condensate EPA624 372395
92350243007 Basement Groundwater EPA624 372395
92350243008 Downstream @ Manhole 25 EPA624 372395
92350243009 New Stormwater Point EPA624 372395
92350243010 East Ditch EPA624 372395
923SOU3011 City Water EPA624 372395
j 92350243012 Manhole 3 EPA624 372395
-`-112350243013 Manhole 3-1.1 EPA624 372395
62350243001 Chiller Room(0-56) SM 2540C 372287
92350243002 Slim Tank SM 2540C 372287
92350243003 Cooper Cooling System SM 2540C 372287
92350243004 MI&M4 Room Quench SM 2540C 372287
92350243005 M5 Room Quench SM 2540C 372287
7 92350243006 Boiler Condensate SM 2540C 372287
92360243007 Basement Groundwater SM 2MOC 372287
92350243008 Downstream @ Manhole 25 SM 2540C 372267
92350243009 New Stormwater Point SM 25400 372287
92360243010 East Ditch SM 2540C 372287
92360243011 City Water 5M 2540C 372287
g 92350243012 Manhole 3 SM 2540C 372287
i
92350243013 Manhole 343 SM 25400 372409 '..
92350243001 Chiller Room(0-58) SM 2640D 372272
92350243002 Sllm Tank SM 2540D 372272
92350243003 Cooper Cooling System SM 2540) 372272
92350N3004 MI&M4 Room Quench SM 25401) 372272
92350243005 MS Room Quench SM 254013 372272
( 12350243006 Boiler Condensate SM 2540D 372272
( 92350243007 Basement Groundwater SM 2540D 372272
92360243008 Downstream @ Manhole 25 8M 2540D 372272
92350243009 New Stormwater Point SM 2540D 372363
92350243010 East Ditch Ski 2540D 372363
92350243011 City Water SM 254013 372363
92350243012 Mardian,3 SM 254011 372363
92350243013 Manhole 3-U SM 25400r 372363
'3
f
REPORT OF LABORATORY ANALYSIS
tThis report stair not ac evWrOad.O.P o rml,
Data OW221201710:12 AM nimom me wntten consent of Pace Analytical SeMcea LLC' Page 89 of 96
1

( Pace Analytical Services.LLC
aeeAnalyleal s 2225 R,TIC 28 2ae4 0
mramaves mn HSFeville. 25
porL
� 4-7176
QUALITY CONTROL DATA CROSS REFERENCE TABLE
i
t
Project: Low&Boner Inc 1210140
Pace Project No.: 92350243
i
Analytical
3 Lab ID Sample ID QC Balch Method QC Batch Analytical Method Batch
92350243001 Chiller Room(0.58) TKN+NO3+1,102 372661
Calculation
92350243002 Slim Tank TKN+NO3+NO2 372661
Calculation
92350243003 Cooper Cooling System TKN+NO3+NO2 372661
Calculation
923502430" MI&M4 Room Quench TKN+NO3+NO2 372661
s Calculation
92350243005 MS Room Quench TKN+NO3+NO2 372661
Calculation
92350243006 Boiler Condensate TKN+NO3+NO2 372661
Calculation
j 92350243007 Basement Groundwater TKN+NO3+NO2 372661
Calculation
92350243008 Downstream @ Manhole 25 TKN+NO3+NO2 372661
Calculation
92350243009 New Stormwater Point TKN+NO3+NO2 372601
= Calculation
92350243010 East Ditch TKN+NO3+NO2 372661
} Calcolation
92350243011 City Water TKN+NO3+NO 372661
i Calculation
92360243012 Manhole TKN+NO3+NO2 372661
Calculation
y j2350243013 Manhole3-U TKN+NO3+NO2 372661
Calculation
- 92350243001 Chiller Room(0-581 EPA350.11993 Rev 2.0 372455
92350243UO2 Slim Tank EPA350A 1993 Rev 20 372455
92350243003 Cooper Cooling System EPA350.11993 Rev 20 372455
92350243004 MI&M4 Room Quench EPA350.1 1993 Rev 2.0 372455
92350243005 M5 Room Quench EPA350.11993 Rev 2.0 372455
9235024J006 Better Contlensate EPA 350.11993 Rev 2.0 372455
92350243007 Basement Groundwater EPA350A 1993 Rev20 372455
92360243008 Downstream @ Manhole 25 EPA350.11993 Rev 2.0 372455
- 92350243009 New Stormwater Point EPA350.11993 Rev 20 372455
92350243010 East Ditch EPA350.11993 Rev 20 372455 '..
92350243011 City Water EPA350.11993 Rev 2.0 372455
- 92350243012 Manhole EPA350A 1993 Rev 20 372455
92360243013 Methods 3 U EPA350A 1993 Rev 20 372455
92360243001 Chiller Room(0-58) EPA3512 372344
1 92350243002 Slim Tank EPA351.2 37244
] 92360243003 Cooper Cooling System EPA351.2 372344
92350243004 MI&M4 Room Quench EPA351,2 372344
92350243005 M5 Room Quench EPA351.2 372344
92360243006 Boiler Contlensate EPA35L2 372344
92350243007 Basement Groundwater EPA351 2 372344
92350243008 Downstream @ Manhole 25 EPA 351.2 372344
92350243009 New Stormwater Point EPA351.2 372344
92350243010 East Ditch EPA35L2 372344
° 92350243011 City Water EPA 351.2 372344
92350243012 Manhole EPA351.2 372344
i
REPORT OF LABORATORY ANALYSIS
This ropon shag not be reproduced,eseept in mu,
i Data 0812 21201 7 10:12 AM wnhoW the mrace coc,chl.f Pace Analytical Services,LLG Page 90 of 96
1

I Pace Analytical Services,LLC
i ppq pq 2225 RNerssle Dr.
a 4y V Analytical Aah.,11,,NC 28804
11�3 (828)2547175
i
3
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Low&Sonar Inc 1210140
I Pace Project No.: 92350243
1
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92350243013 Manhole 3-U EPA35L2 372344
92350243001 Chiller Room(068) EPA 353.2 372466
( 92350243002 Slim Tank EPA353.2 372466
I 92360243003 Cooper Cooling System EPA353.2 372466
92360243004 MI&M4 Room Quench EPA353.2 372467
_ 92360243005 M5 Room Quench EPA 353.2 372467
92350243006 Boiler Condensate EPA353.2 372467
92350243007 Basement Groundwater EPA353.2 372467
92350243008 Downstream @ Manhole 25 EPA353.2 372467
92360243009 New Stormwater Point EPA 353.2 372467
- 92350243010 East Ditch EPA353.2 372467
92350243011 City Water EPA353.2 372467
- 92350243012 Manhole 3 EPA 353.2 372467
92350243013 Manhole 3-U EPA353 2 372467
92360243001 Chiller Room(0.58) EPA 365A 372249
[ 92350243002 Slim Tank EPA365A 372249
92360243003 Cooper Cooling System EPA365.1 372679
92350243004 MI&M4 Room Quench EPA365.1 372680
12350243005 M5 Room Quench EPA365.1 372680
`92350243006 Boiler Condensate EPA365.1 372660
3 92350243007 Basement Groundwater EPA 365A 372680
_ 92350243008 Downstream @ Manhole 25 EPA365.1 372680
92350243009 New Stormwater Point EPA365A 372680
92350243010 East Ditch EPA365.1 372680
92350243011 City Water EPA365.1 372680
92360243012 Manhole 3 EPA365A 372680
92350243013 Manhole 3-U EPA365A 372680
92350243001 Chiller Room(0-58) SM 5220D 372202
92360243002 $lim Tank SM 5220D 372202
92350243003 Cooper Cooling System SM 52200 372202
j 92350243004 MI&M4 Room Quench SM 5220D 372202
7 92350243005 M5 Room Quench SM 5220D 372202
92350243006 Boiler Contlensate SM 5220D 372202
92350243007 Basement Groundwater SM 5220D 372202
92360243008 Downstream @ Manhole 25 SM 5220D 372202
92350243009 New Stormwater Point SM 5220D 372202
92350243010 East Ditch SM 5220D 372202
92350243011 City Water SM 5220D 372202 '..
92360243012 Manhole 3 SM 5220D 372202
92350243013 Manhole 3 U SM 5220D 372202
j 92350243014 Stamoy SM 5220D 372202
I
t
I
"J REPORT OF LABORATORY ANALYSIS
i
TMs report span not be repmauaee,except in mIL.
- Date:08122/201710:12AM ximom the wrinen consent of Pace Analytcal Benkes,uc. Page 94 of 96

t
7— Document Name: Document Revised:Sept 21,2016
aC2/h/r7jn/C2I Sample Condition Upon ReceiptlSCURI _ Page 1 of 2
f Y' Document No.: Issuing Authority:
F-[AR-CS033-flev.01 Pace 4uali[y Office
i Laboratory receiving sample
Asheville —Eden[] - Greenwood — HuntersvilleEl Raleigh Mechanicsville[]
j [Rent Name: Project) W0# : 92350243
^ ❑UDSL 11 V ❑USPS Client �I'II'I I fIIIII III �I�
Courier. I]FedE
! ❑Commercial ❑pace ❑Other.
923Sp243
Custody Seal Present? ❑Yes �fio Seals Intact? ❑yes .�jNo l ( ^^iN``
' Date/Ininal5 rton F aMningtonfents �
Packing Material: ❑Bubble Wrap ubble Bags ❑None Other._
Th¢rmom¢ten [� --.Qyet ORlne ❑None ❑Samples on ice,coating process has begun
❑IR Gun ID: Type of l[e:; Cf
Correction Factor: Cooler Temp Corrected(°C): L �,5 ri- li f 5�'9 ologisal Tivue Frozen? QYes ❑ N/A
f Temp should be above ffr�reffzing to VC
3 USDA Regulated 5o11(,lJ N/A,water sample)
Did samples Dili in a quarantine One within the United States:CA,NY,or SC(check maps)? Did tamphsoriginate(roma foreign source(internationally,
QYes QNo including Hawaii and PUMO RICO)?Oyce ❑?Jo
Comments/Discrepancy:
i
Chain of Concede Present? Yes QNo ON/A 1.
i
Samples Arrived within Hold Time? E011 No ON/A 2. ,
Short Hold Time Analysis(U2 m.)?
Rush Turn Around Time Requested? OYesN/A 4.
Sufficient Volume? 0,6' No ON/A 5.
Correct C.Ofty4 h,used? .—LJ�reS �Offa DA/A 6.
-Pace Containers Used? ❑Yca ONa QN/A
Cisculancro,Intent? es ON. ❑N/A ?.
Sample,Field Filtered? OYes No N/A S. Note if sediment is visible in the dissolved container
j Sample Labels Match COC? Ycs ONO ON/A
-nmwa¢s DaL¢1Ti:nMw/AnaWtis maNix,- \i v
Headspace in VOA Vials('5 5mm? OYes ,�.,.N�oo ON/A 10.
Trip Blank Present? Oyes ,lijOa ONJA 11,
I
Trip Blank Custody Seals Present? Oyes Oflo '/A
CLIENT NOTIFICATION/RESOLUTION Field Data Required? QYes []No
1
I Rome.Contacted: Date/Time: _
Comments/Sample
Discrepancy:
1 _ —
Protect Manager SCURF Revievr. _ Date:
( Project Manager SRF Review: /I Date:
3
Run; Whenever here i5 a discrepancy affecting North Carolina wmpCance smines.acony of the form vll be sent to lire North Camllno DEHNR Corrugation Office Re.
I Out of hotel,incorrect pmterva con,out of temp incorrect containers)
i
Page 92 of AT
i

Uocument Name: Document Revised:Sept 21,2016
Sample Condition Upon Receip[ISCURI Page 2af2
_7 8 6 naljtical Document No.: Issuing authority:
i F-CAR-CS-033-Rev.01 {{}j Pace Quality Office !p
*Check mark top half of box if pH and/or dechlorination Project W®!T : 9235®243
is verified and within the acceptance range for
i preservation samples.
PM: COS Sue Dale: 08/17/17
j
3 **Bottom half of box is to list number of bottles CLIENT: 93-PisgahEnv
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Somplel0 Typeofpreservative PH upon recehu Date preservation adjusted Time preservation Amount of Preservative tote
3 adjusted added
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Page 93 of 96
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Document Name Document Revisetl:Sept,21,2016
' f1 - Sample Condition U on RecedaiSCURI Page 2 of 2
ieAnalytical Document No.: @sui Issuing Authority:
F-CAR.CS-033-Ree01 Pace Quality Office
*Check mark top half of box if pH and/or dechlorination Project
is verified and within the acceptance, range for
preservation samples.
-*Bottom half of box is to list number of bottles
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ATTACHMENT D
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3 � Boiler Steam Receivers
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Chiller Room Cooling Tower 058 Pump
Cooper Cooling Tower Pump
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Ti0e: Purchase Order Requisition Poem Revision Level 3 Rev. Date 12-14-01
Number 406-11
PURCHASE REQUISITION
Page 1 of 1
Purchase Order No. 8/28/2011
j Ship To EENKA, NC
1 Motion Industries ROAD
3865 Sweeten Creek Rd.
-- Arden, NC 28704 8
z
arty Cooper
Contact Pat Wells
828 684 3180 828 665 3532
828 684 3842 i� Fax [phone]
S Payment Terms
s (or see below)
fF,O.B.
t ASAP Conf cram =Yes D No
` Printed F.O.Req'd by Vendor? 0-ye; - D No
15322.4848.1 0 Yes iD so
- Chentic i?,
Item Qt /UOM Unit Price Total price
Duplex pump system for cooling water pit behind cooper
1 cooling tower per attached quoted $4,209.00
3
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Prepared ByiDate Approva / e zg // A proval 3: IT/R&D $4,209.00
i
)
The only controlled copy of this document is on the network. Printed copies are on regular paper and become
i ouality records when completed.

3
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MOTION INDUSTRIES Date:08124117
i 3865 SWEETEN CREEK ROAD
ARDEN,NO 28704-0000
i PHONE:[phone]
FAX:[phone]
1
3
Note:This estimate is valid far 30 days from the date shown above.
Prices quoted are for quantities shown.Stock is subject to prior sale.
MTO quantities considered complete 109;undadover unless noted.
I
To:SONAR INC QUOTE NUMBER: NC59-378148
I # 13015AND HILL RD CUSTOMER RFD: PAT WELLS
CANDLER,NC 25715-4508 F.O.B.: FOB ORG,FRT PP&ADD
1 PO: PATWELLS
QUOTE SENT BY: LARRY COOPER
REL: COOLING TOWERSUMP
TERMS: 1%10&25TH NET 30
DELIVERY: STOCK UNLESS NOTED
SHIPPING:
:
Dgs�gp60n MaHviactu�r-- = Quan4ty llalt Uo2Pnce 'AmD[
LINE ITEM: 001
G-165 CAST IRON SUMP PUMP 480V 3P 1 2 EA $1,120,870 $2,241.
ITEM NO: 04663753 ZOELLER
DELIVERY:7 DAYS TO SHIP, FROM LOUISVILLE, KY
LINE ITEM: 002 CUSTOMER LINE NO:2
j 10-1106 DUPLEX CONTROL PANEL 460V 3PH 1 EA $1,673.410 $1,673. '..
I NEMA 4X WITH ALARM _
! ITEM NO: 99999999 ZOELLER
STOCK AT ZOELLER,LOUISVILLE, KY
LINE ITEM: 003
10-14584-FLOAT TREE ASSEMBLY 1 EA. $293.880 $293.
ITEM NO: 99999999 ZOELLER
1
I
i

3
I i
3
�i
STOCK AT ZOELLER, LOUISVILLE, KY
Subtotal: $4,209.•
Sales Tax: $0.
Total: $4,209.
All Prices in Ii.
i
Call. 800526-9328
; Click wv:vtmotlonindusLfie;.mm
5c i Visit. Over 550 Locations
7
j Copyright©2001-2017 Motion Industries, Inc.-All Rights Reserved. Legal Disclaimer, Privacy Policy,
Terms And Conditions, Provide Feedback
Motion Industries 1605 Alton Rd. Birmingham,AL 35210, USA(205)956-1122
9 BbYfR UNOERSR.IioS KMe AGREES itIAi GGUaS I1j MOTIONSS£flMS CmoHSRE iCPSRllfSESEN T.on5TER SAD CONDITIONS
DI l N ARE AVAILABLE
AT THE KAOTIMCONTIY WAITED
F UiPS
BrlACCEPiAN<F OF ME DELIVERY OF ME GOODS MAIL(OWNED lamal5iGNUMENT TO ALI ME MOP09S TERMS
OAND
OVYFtR�S A6RNfEJ(EH_p.iE5MrI OixOgACIOt eV},F CO.4al➢ONS,
3
z
ibis commpnmetion may contain mnpdessid,proprietary,or legally privileged inforemoom It is intended for the parsons)to vlrlom it
is addressed only.If you are not an Intended recipient you may not read,use,retransmit disseminate or take any action in reliance
> 't upon it.Please notlty the sander by return email that you have reeei,.dit in error antl immediately delete the entire oommumczlion,
Ludt any attachments,from your system.This e-mail has been sent in the course of the business of a member of Ute Lowe&
{ Bonn,group.In Me context of me deritodng of professional omens Nis e-mail and any response to it or any other e-mail sent to
g this address may be read by that company.including in its capacity as an employer.
tdembers of the Lai&Sonar group do not encrypt and cannel ensure the confidentiality or integrity of extemat email
_ wmmumsearns and,therefore,cannot be held responsible for any unauthorized access,disGosure,use or tampering Nat may
occur during transmission.This communisation is not intended to create or modify any obligation,contract offer,=(too,,
acceptance of aconlrad offer or warranty of members of the Lee,&Sonar group.unless that member smarty expresses such an
intent This email does not constitute consent to the use of the sender's contact information far direct marketing purposes or for
transfers of data to third pares.
Low&Boner PLC is a limited liability company registered in Scotland with registered number SC008349.Our registered office is
Whitehall House,33 Ye mM.Shore,Dundee DDt 48J.
3
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i

Title: Purchase Order Requisition Form Revision Level Rev. Date 12-14-01
F Number 406-11
i
- , PURCHASE REQUISITION
Page 1 of 1
s
Purchase Order No. 8/28/2017 �
- i Ship To I� Low and Bonar
Motion Industries 1301 SAND HILL ROAD
3865 Sweeten Creek Rd. PO BOX 1057
Arden, NO 28704 ENKA, NO 28726
c
I Larry Cooper Contact Pat Welis
l
828 684 3180 828 665 3532
828 684 3842 Fax [phone]
Payment Terms
(or see below)
F.O.B.
ASAP Conflrmin ElYes PI No
Printed P.O. Rea,'d by Vendor? D Yes r Ns
15322.4848.1 r7 Yes '-1 No
Ches,nc.si
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Item t /UOM Unit Price Total Price
1 Duplex pump system for cooling water drain tank from the
1 chiller cooling towers per attached quoted $8,768.95
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Prepared B /Date A royal ate /r A b8,768.95
Pre Approval
P Y P 3: IT1R&D
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OTIOW
INDUSTRIES QUOT
F-a€/+u+R Irr[Lrstn+be MaRau
1 �
MOTION INDUSTRIES Date:08128/17
3865 SWEETEN CREEK ROAD
ARDEN,NC 28704-0000 is
PHONE:[phone]
Note:This estimate is valid for 30 days from the date shown above.
4 FAX:[phone] Prices quoted are for quantities shown.Stock is subject to prior sale.
a
MID quantities considered complete i0°h undercover unless noted.
To:BONAR INC QUOTE NUMBER: NC59-378034
1 1301 SAND HILL ED i
CANDLER,NC 28715-4508 CUSTOMER RkQ: HOWARD EARLEY
PO: HOWAAD EARLEY F.O.B.: FOB ORG,FAT PP&ADD
REL: DEMING PUMPS QUOTE SENT BY: LARRY COOPER
3 TERNIS: 1% 10 S 25TH NET 30
DELIVERY: STOCK UNLESS NOTED
SHIPPING:
d
I
Description Manufacturer Quantly Unit Unit Price Amoy
LINE ITEM: 001 CUSTOMER LINE NO: 1
4011-133-10-031 PUMP 1-114S STANDARD 2 EA $3,689.210 $7,378.
i ALL IRON 7"DIAMETER IMPELLER
ITEM NO: 99999999 DEMING PUMPS '..
3 40I1-133-10-031 CRANE DEMING END SUCTION CENTRIFUGAL PUMP,STANDARD FPPTFA
3 ALL
j IRON CONSTRUCTION,
SIZE 1-Il4S, WITH BFI Ct SEAL, IMPELLER TRIMMED TO,7" DIAMETER.
UNIT MOUNTED ON CARBON STEEL BASEPLATE WITH FALK T SERIES 1020TIO
} COUPLING,
FALK COUPLING GUARD, AND BALDOR
EM3546T MOTOR I HP 175ORPM 143T FROAME 208-230/460 VOLTS,3 PHASE, 60 CYCLES
TEFL ENCLOSURE,.
.1 DELIVERY: ONE PUMP N 3 TO 4 WEEKS
SECOND PUMP 7 WEEKS TO SHIP, AFTER RECEIPT OF ORDER.
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LINE ITEM: 004
j 3221W00lH3A6A17A19F CONTROL PANEL 1 EA $1,390,530 $1,390,
DUPLEX ALTERNATING WITH ALARM
ITEM NO: 99999999 SJ ELECTRO
1. ENCLOSURE MEASURES 14 X 12 X 6 INCHES (35.56 X 30.48 X 15.24 CM)
NEMA 4X(ULTRAVIOLET STABILIZED THERMOPLASTIC WITH REMOVABLE MOLNTIN(
'.. FEET FOR OUTDOOR OR INDOOR USE).
2. IEC MOTOR CONTACTORS CONTROL PUMPS BY SWITCHING ELECTRICAL LINES_
.; 3. MULTI-TAP TRANSFORMER(208/240/480 VAC PRIMARY)PROVIDES 120V
CONTROL/ALARM VOLTAGE. OR 600VAC PRIMARY TRANSFORMER.
4. MOTOR PROTECTIVE SWITCHES PROVIDE ADJUSTABLE OVERLOAD, BRANCH
3 CIRCUIT
PROTECTION AND PUMP DISCONNECT.
5. ALTERNATING CIRCUIT BOARD PROVIDES PUMP CONTROL AND ALTERNATION
`) (U.S. PATENT A 5,909,532).
6. GREEN PUMP RUN INDICATOR LIGHTS (MOUNTED ON CIRCUIT BOARD).
7. ALARM/CONTROL FUSE (MOUNTED ON CIRCUIT BOARD).
8,FLOAT STATUS INDICATOR LIGHTS (MOUNTED ON CIRCUIT BOARD).
- 9. FLOAT SWITCH TERMINAL BLOCK (MOUNTED ON CIRCUIT BOARD).
10, INPUT POWER TERMINAL BLOCK
11. GROUND LUGS
12. HOA SWITCHES FOR MANUAL PUMP CONTROL(MOUNTED ON CIRCUIT BOARD).
_ 13. CONTROL ON/OFF SWITCH (MOUNTED ON CIRCUIT BOARD).
NOTE: SCHEMATIC"WIRING DIAGRAM IS LOCATED INSIDE THE PANEL ON ENCLOSURE
t COVER.
3 STANDARD ALARM PACKAGE
14, RED ALARM BEACON PROVIDES 360' VISUAL CHECK OF ALARM CONDITION.
15.ALARM HORN PROVIDES AUDIO WARNING OF ALARM CONDITION (83 TO 85 DECIBI
RATING).
16.EXTERIOR ALARM TEST/NORMAL/SILENCE SWITCH ALLOWS HORN AND LIGHT TO
BE
TESTED AND HORN TO BE SILENCED IN AN ALARM CONDITION. ALARM
3 AUTOMATICALLY
j RESETS ONCE ALARM CONDITION IS CLEARED.
17. HORN SILENCE RELAY (MOLNTED ON CIRCUIT BOARD).
NOTE: OTHER OPTIONS AVAILABLE.
- FEATURES
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ENTIRE CONTROL SYSTEM(PANEL AND SWITCHES) IS UL LISTED TO MEET AND/OR
)
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EXCEED INDUSTRY SAFETY STANDARDS
s DUAL SAFETY CERTIFICATION FOR THE UNITED STATES AND CANADA
t
STANDARD PACKAGE INCLUDES THREE 20'SIGNALMASTER®CONTROL SWITCHES
3A ALARM FLASHER
6A AUXILIARY ALARM CONTACT,FORM C
17A SJE SIGNALMASTERO!PIPE CLAMP
' 19F FOURTH FLOAT TO SEPARATE ALARM FUNCTION FROM LAG
l
COMPLETE WITH STEP-BY-STEP INSTALLATION INSTRUCTIONS
N FIVE-YEAR LIMITED WARRANTY
DELIVERY: SHIPS IN 3 TO 5 WORKING DAYS AFTER RECEIPT OF ORDER,
PRICING PER TYLER AT SJE RHOMBUS 8128i17 BY PHONE QUOTE,
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1
Subtotal: $9,7681
Sales Tax: SO.l
- Total: S8,768_'
All Prices in US
s
MOTION f,aiF. 800 526-9328
a r INDUSTRIESi `:ucl,- w,w.motiorundustrics.com
visit, Over 550 Locations
Copyright Chi 2001 -2017 Motion Industries,Inc. -All Rights Reserved, Legal Disclaimer,Privacy Policy,
Terms And Conditions, Provide Feedback
Motion Industries 1605 Alton Rd. Bumingharn,AL 35210,USA(205)956-1122
BUYER UNDERSTANDS AND AGREES THAT GOODS PRESENTED TO BUSER P.RSUANT'IO YNIS INVOICE ARE.BLIND T NDERBDCON71N.UT ORON
BUYPAtSAGREPIBENT TO ALL OF NIOTION'STERgiSANDCONDITIONSRrIAnU TO SALES VOTICNS FERNIS AND C08ENRON ARE AVAILABLE AT THE
l ,fOTION BRnNCH OR AT N\5-li`l.tngONMDUSlRIE�r�I.S,BUYER'S ACCEPTANCE OF THE DELIVERY OFTHE GOODS SHALLCONPIRNI BUYER'S
AOREFNENTTO ALL or OUT IONS T@AIS AND CONDITIONS
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ORIGINAL
Purchase Order
--;1 Ord,Nvmber 7899705
Vender MOTION INDUSTRIES,INC. Step To LOW and Bona,lac,
} PO BOX 404130 A/P NOTE opnalasbwandbonaccom
ATLANTA GA 3QB 4 130;Sand Hai Road
$ Candler NC 28715
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3
FAX [phone] Contact Reeves,Wilmo
828 665-50M Business
828 6655051 FAX
Ordered 0S02-V deighl Handing ietms Prepay and Add Paymeal Terms Net 30 Days
3 RegaeAed OR29-I) Delivery ya,.Iiaes DELIVER REEVES/JEFF DAVIS
{ Onceney Code USD
3
'—PURCHASE ORDER NUMBER MUST BE SHOWN ON ALL INVOICES AND PACKAGING LISTS"'s
SHIPPING LABEL REQUIREMENTS:
V& SONAR POR: 78997 OS
? "CTLE REEVES/JEFF DAVIS
n....<.........<.0...............—,...e..<....u..<u......„..„<.......<............<
j PACKAGING REQUIREMENTS:MUST CLEARLY IDENTIFY PRODUCT
one Rev Born Number [a,,Fd.d Ordered TOM Unit PAce Extended RIEP Oae Data
3
IWOO 99999 - -- G22FHWF315GV&1-1/4 FC PUMP/ ---- - IO EA -- 89600W ---- 896W WRY IJ
'3 MOTOR.I-I/2 HR 575/3/60
20W0 99999 G3CRIW F330GVbt-I/dFC PUMP/ 20 EA 1R10 WW 2020LW G9-29-0
j MOTOR
I
REF: QUOTE NO,NC59-SOWN DATED 8 WX/
Top] 2,91603
3
I Pape 1
Inve Ce ANN,,.
E LOWond Bonarinc
3
T H Stled Mil Rood
-ev,a NC BO06
j Umled Stole,
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ORIGINAL
` Purchase Order
OrdEP Namber 79030 OS
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Vender MOTION INDUSTRIES,INC. Slip To Low and Bonor Inc.
PO BOX 404133 AIR Em Yl:opLoId?0owandbonas.com
ATLANTA GA 30384 1301 Sand HIT Road
CanNerNC 28715
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FAX 826 E84-3842 Conlod fte9ves.WlmO
828 6655038 Bus•ness
828 6655051 FAX
Ordered OBU2-17 Freight Hactling Terms Prepay and Add Payment Terms Net 30 Days
f
j Requazied FLY-29-] Ueivery mimMons DELIVER RFF/ESfJEFPDAVIS
j Currency Code USD
!
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PURCHASE ORDER NUMBER MUST BE SHOWN ON ALL INVOICES AND PACKAGING LISTS•^x
- .SHIPPING LABEL REQUIREMENTS:
)WB BONARPO=: 79"OS
ALEX:REEVES/IEFF DAVIS
PACKAGING REQUIREMENTS:MUST CLEARLY IDENTIFY PRODUCT
❑ne Rev Rem Numbar Description Ortlered LOU Unit Poce 6londed Pita LOU Palo
L 1.090 99999. G26fHC0 f320GVb-i-I/4 fC'PUMP/ 10 EA 59$CC'.Xi 89600:09-29=17
{
MOTOR 2 HE 57513/60
3 20000 99999 22018 GASKET,FLAT.COMP, 160 EA 5.i51X1 82,40 M29-V
j 4 X 5.56
F
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3B)..3' 0 99999 22334 FLOAT ASSY 40 EA 126,60IXJ 506,40 09-29-19
4JEGI0 99999 90MCG32 FLOAT SWITCH 10 EA 478.6000 95I20 W-29-17
'j ALTERNATOR
l &CW O 99999 903IHG32 FLOAT SWITCH 20 EA 244.0d00 e88.03 0929-V
age 1
( Invoice Atl@ess
t L.,and BWarinc
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sold HIT Paco
j -41evi La NC 28806
i UNied sates

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ORIGINAL
I
Purchase Order
'Fne Rev Itym rvumber NU'cU'tion Ord.,.d i Unit He Dlentled We Due DATA
REF. QUOTE NO,NCSRB]6968 DATED 812117,
I
iota: 29:A88
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ORIGINAL
Purchase Order
Otaer Number 79WI OS
1
ventlw MOTION INDUSTRIES,INC. 5Mp To Low and Bono,Inc.
I PO BOX 4041 Ed A/P EmaPn opnalaslowanbbonoccom
ALTANTA GA 30384 1301 Sand HiT Road
I Candler NC 28715
3
FAX [phone] Conrad Reeve"Arra.
828 6655038 Business
828 665-5051 FAX
2
j Ordered 0802-17 Freight Hand'ng Terms Prepay and Add Payment Terms Net 30 Days
od,relea 09-29-1I Delwery FOILLclbns DELIVER REEVESGEFF DAVIS
(Vrrendy Code USD
—PURCHASE ORDER NUMBER MUST BE SHOWN ON ALL INVOICES AND PACKAGING URS""
SHIPPING LABEL REQUIREMENTS:
)N& EQUAL!PER: 79MI OS
'ANN:REEVESIJEFF DAVIS
PACKAGING REQUIREMENTS:MUST CLEARLY IDENTIFY PRODUCT
K
- Line Rev tram NUmbe, Drocrplian Ordered UOM Unll Pace Extended PI One Dale
- I.DED0 99999 G26FHW F320GV6-1-1/4 PC PUMP/ 40 EA 8960000 3584W 09-29-17
6 MOTOR,2 HE 57513160
' REF: QUOTE NO.NC59-3I696B DATED 8/2/I7.
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FIND 3,584.00
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JIeVNe NC 2EGA
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North Carolina Surface Water Standards
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