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Home My WebLink AboutNC0021962_Method 625 Scan_20200520Action History (UTC-05:00) Eastern Time (US & Canada) Subrrit by Anonymous User 5/20/2020 12:21:39 PM (Supplemental Submittal) Submit by Thedford, Wren 5/20/2020 2:54:24 PM (Supplemental Info Submittal) • Thedford, Wren assigned the task to Thedford, Wren 5/20/2020 2:54 PM • The task was assigned to Thedford, Wren, Bennett, Bradley 5/20/2020 12:21 PM Initial Review Information Updated ID#:* IWORTANf:FEVIBAERSHOLLDVERIFY and revise here ifnecessary. NC0021962 How should this project be handled?* r File r Discard Information Submitted on 5/20/2020 Submitter Information Name: James Utke Vft is subrritting the inforrretion? Email Address:* jutke@citgo.com Submittal Information The Division of Water Resources (DWR) is providing this site to allow for the upload of required supplemental information associated with discharge monitoring reports (DMR). All DMR data is required to be submitted electronically through the eDMR system and should not be submitted here. Division staff will reviewall uploaded documents and will only maintain required information. Documents such as laboratory reports are not required to be submitted and will not be maintained in the system. Project Information: Rease SUDDly the Dernit nun ber for this Existing ID#* PerrritNurrber NC0021962 Exarrples: NOKxxxxxx or NO&xxxxx Facility Name:* CITGO Petroleum Corporation County: Mecklenburg Please upload all files that need to be submited. * dick the upload button or drag and drop files here to attach docurrent NPDES625april2020.pdf 6.79MB Only pdf files are accepted. Comments about the attachments: 625 Compound Scan Sumittal * V By checking the box and signing box below, I certify that: o I have given true, accurate, and complete information on this form; • I agree that submission of this Supplemental Information form is a "transaction" subject to Chapter 66, Article 40 of the NC General Statutes (the "Uniform Electronic Transactions Act) • I agree to conduct this transaction by electronic means pursuant to Chapter 66, Article 40 of the NC General Statutes (the "Uniform Electronic Transactions Act'); • I understand that an electronic signature has the same legal effect and can be enforced in the same way as a written signature; AND • I intend to electronically sign and submit the Supplemental Information form." Full Name: James Earl Utke Signature: Date Submitted: 05/20/2020 aceAnalytical° ANALYTICAL REPORT i National Center for Testing & innovation April 23, 2020 ON 3 Ss CITGO-Charlotte, NC Sample Delivery Group: L1209532 Fn Samples Received: 04/16/2020 Sr Project Number: SEMIANN Description: treated stormwater EQc To: FReport Mr. Jim Utke 7600 Mount Holly Road E Charlotte, NC 28214 E Entire Report Reviewed By: Stacy Kennedy Project Manager Results relate only to the items tested of calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the Information provided, and as the samples are received. Y ACCOUNT: PROJECT: SDG: DATE/TIME: Porr TABLE OF CONTENTS ONE LAB NATIONWIDE. V Cp� Page 1 TcTable of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results S Fs OUTFALL0D1 L1209532-01 5 ^--- Qc Quality Control Summary 7 Fn _ Semi Volatile Organic Compounds (G[%K46)byMethod G25.1 7 E G|: Glossary of Terms 12 Al:�4ccneditations&Locations 13 | L�c Sc Sample Chain of Custody 14 �� AocouwT: PROJECT: snn: n^r=mwP =^— OUTFALL 001 L1209532-01 WW SAMPLE SUMMARY Collected by Rob Durham ONE LAB, NATIONWIDE. V Collected date/time Received date/time 04/15/20 09:00 04/16/20 08:30 Method Batch Dilution Preparation Analysis date/time date/time Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1462591 1 04/20/2015:19 04/21/20 02:33 Analyst Location AO Mt. Juliet, TN ..c ACCOUNT: PROJECT: S DG: DATE /TI M F D A r_ M. CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. Stacy Kennedy Project Manager rc s Ss ACCOUNT: PROJECT: SDG: r)ATr/TIAAF. OUTFALL 001 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. . Collected date/time: 04/15/20 09:00 L1209532 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Acenaphthene U 0.0000886 0 00100 1 04/21/2020 02:33 WG1462591 Acenaphthylene U 0.0000921 0.00100 1 04/21/2020 02:33 WG1462591 Anthracene U 0.0000804 0.00100 1 04/21/2020 02:33 WG1462591 Benzidine U 0.00374 0.0100 1 04/21/2020 02:33 WG1462591 Benzo(a)anthracene U 0.000199 0.00100 1 04/21/2020 02:33 WG1462591 Benzo(b)fluoranthene U 0.000130 0.00100 1 04/21/2020 02:33 WG1462591 Benzo(k)fluoranthene U 0.000120 0.00100 1 04/21/2020 02:33 WG1462591 Benzo(g;h,i)perylene U 0.000121 0.00100 1 04/21/2020 02:33 WG1462591 Benzo(a)pyrene U 0.0000381 0.000200 1 04/21/2020 02:33 WG1462591 Bis(2-chlorethoxy)methane U 0.000116 0.0100 1 04/21/2020 02:33 WG1462591 Bis(2-chloroethyl)ether U 0.000137 0.0100 1 04/21/2020 02:33 WG1462591 2,2-Oxybis(1-Chloropropane) U 0.000210 0.0100 1 04/21/2020 02:33 WG1462591 4-Bromophenyl-phenylether U 0.0000877 0.0100 1 04/21/2020 02:33 WG1462591 2-Chloronaphthalene U J4 0.0000648 0.00100 1 04/21/2020 02:33 WG1462591 4-Chlorophenyl-phenylether U 0.0000926 0.0100 1 04/21/2020 02:33 WG1462591 Chrysene U 0.000130 0.00100 1 04/21/2020 02:33 WG1462591 Dibenz(a,h)anthracene U 0.0000644 0.000200 1 04/21/2020 02:33 WG1462591 3,3-Dichlorobenzidine U 0.000212 0.0100 1 04/21/2020 02:33 WG1462591 2,4-Dinitrotoluene U 0.0000983 0.0100 1 04/21/2020 02:33 WG1462591 2,6-Dinitrotoluene U 0.000250 0.0100 1 04/21/2020 02:33 WG1462591 1,2-Diphenylhydrazine U 0.000105 0.0100 1 04/21/2020 02:33 WG1462591 Fluoranthene U 0.000102 0.00100 1 04/21/2020 02:33 WG1462591 Fluorene U 0.0000844 0.00100 1 04/21/2020 02:33 WG1462591 Hexachlorobenzene U 0.0000755 0,00100 1 04/21/2020 02:33 WG1462591 Hexachloro-1,3-butadiene U 0.0000968 0.0100 1 04/21/2020 02:33 WG1462591 Hexachlorocyciopentadiene U 0.0000598 0.0100 1 04/21/2020 02:33 WG1462591 Hexachloroethane U 0.000127 0.0100 1 04/21/2020 02:33 WG1462591 Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 1 04/21/2020 02:33 WG1462591 Isophorone U 0.000143 0.0100 1 04/21/2020 02:33 WG1462591 Naphthalene U 0,000159 0.00100 1 04/21/2020 02:33 WG1462591 Nitrobenzene U 0.000297 0.0100 1 04/21/2020 02:33 WG1462591 n-N itrosod imethyla mine U 0.000998 0.0100 1 04/21/2020 02:33 WG1462591 n-Nitrosodiphenylamine U 0.00237 0.0100 1 04/21/2020 02:33 WG1462591 n-Nitrosodi-n-propylamine U 0.000261 0.0100 1 04/21/2020 02:33 WG1462591 Phenanthrene U 0.000112 0.00100 1 04/21/2020 0133 WG1462591 Benzylbutyi phthalate U 0.000765 0.00300 1 04/21/2020 02:33 WG1462591 Bis(2-ethylhexyl)phthalate U 0.000895 0.00300 1 04/21/2020 02:33 WG1462591 Di-n-butyl phthalate U 0.000453 0.00300 1 04/21/2020 02:33 WG1462591 Diethyl phthalate U 0.000287 0.00300 1 04/21/2020 02:33 WG1462591 Dimethyl phthalate U 0.000260 0.00300 1 04/21/2020 02:33 WG1462591 Di-n-octyl phthalate U 0.000932 0.00300 1 04/21/2020 02:33 WG1462591 Pyrene U 0.000107 0.00100 1 04/21/2020 02:33 WG1462591 1,2,4-Trichlorobenzene U J4 0.0000698 0.0100 1 04/21/2020 02:33 WG1462591 4-Chloro 3-methylphenol U 0.000131 0.0100 1 04/21/2020 02:33 WG1462591 2-Chlorophenol U 0.000133 0.0100 1 04/21/2020 02:33 WG1462591 2;4-Dichlorophenoi U 0.000102 0.0100 1 04/21/2020 02:33 WG1462591 2,4-Dimethylphenol U 0.0000636 0.0100 1 04/21/2020 02:33 WG1462591 4,6-Dindro-2-methylphenol U 0.00112 0.0100 1 04/21/2020 02:33 WG1462591 2,4-Dinitrophenol U 0.00593 0.0100 1 04/21/2020 02:33 WG1462591 2-Nitrophenol U 0.000117 0.0100 1 04/21/2020 02:33 WG1462591 4-Nitrophenol U 0.000143 0.0100 1 04/21/2020 02:33 WG1462591 Pentachlorophenol U 0.000313 0.0100 1 04/21/2020 02:33 WG1462591 Phenol U 0.00433 0.0100 1 04/21/2020 02:33 WG1462591 2,4,6-Trichlorophenol U 0.000100 0.0100 1 04/2112020 02:33 WG1462591 (S) Nitrobenzene-d5 29.6 15.0-314 0412112020 02:33 WG1462591 (S) 2-Fluorob/phenyl 34.6 22.0-127 0412112020 02.33 WG1462591 ACCOUNT: PROJECT: SDG: DATErTIMF anrc OUTFALL 001 SAMPLE RESULTS - 01 Collected date/time: 04/15/20 09:00 L1209532 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 ONE LAB, NATIONWIDE, * Result Qualifier MDL RDL Dilution Analysis Analyte mg/I mg/I Mg/I date/time p -Fer"p henyl-'d 1-4 66.8 29.0-141 0412112020 02.33 (S) Phenol-d5 18.6 8.00-424 0412112020 02:33 (S) 2-Fluorophenol 29.0 10.0-120 0412112020 02.33 (S) 2,46-Tribromophenol 66.5 10.0-153 0412112020 02:33 Batch WG1462591 WG1462591 WG1462591 WG1462591 E F F n I EQC- E E E ACCOUNT: PROJECT: SDG: DATFITIMr-- DArr- [�� U I LL"i0 LIL v (� 110 Ll Mtn F U w O CD CDa J O O o O O O O O O O O O O O Of O O p O O O O O CC O O O O O O o O N O o O. 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O] m GLOSSARY OF TERMS ONE LAB. NATIONWIDE. V Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions MDL Method Detection Limit. RDL Reported Detection Limit. Rec. Recovery. RPD Relative Percent Difference, SDG Sample Delivery Group. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different 1 than is used in this field, the result reported has already been corrected for this factor. Limits These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges.. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. Qualifier This column provides a letter and/or number designation that corresponds to additional information concerning the result reported. If a Qualifier is present, a definition per Qualifier is within the Glossary provided and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was Result no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" (Below Detectable Levels). The information in the results column should always be accompanied by MDL either an (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. Case Narrative (Cn) A brief discussion about the included sample results, including a discussion of any non -conformances to protocol observed either at sample receipt by the laboratory from the field or during the analytical If there process. present, will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. Sample Chain of This is the document created in the field when your samples were initially collected. This is used to verify the time and date of collection, the person collecting the samples, and the analyses that the laboratory is requested to This Custody (Sc) perform. chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. Sample Results (Sr) This section of your report will provide the results of all testing performed on your samples. These results are provided by sample ID and are separated by the analyses performed on each sample. The header line of each analysis for section each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J3 The associated batch QC was outside the established quality control range for precision. J4 The associated batch QC was outside the established quality control range for accuracy. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. 3 Ss a Cn Sr Qc E ACCOUNT: PROJECT: SDG• IIATF/TIMC ACCREDITATIONS & LOCATIONS ONE LAG. NATIONWIDE. ,* Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. State Accreditations Alabama 40660 Nebraska NE-OS-15-05 Alaska 17-026 Nevada TN-03-2002-34 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey—NELAP TNO02 California 2932 New Mexico' Colorado TN00003 New York 117 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina DW21704 Georgia 9 NELAP North Carolina' 41 Georgia' 923 North Dakota R-140 Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky's 90010 South Carolina 84004 Kentucky' 16 South Dakota n/a Louisiana AI30792 Tennessee14 2006 Louisiana' LA180010 Texas T104704245-18-15 Maine TNO002 Texas s LA80152 Maryland 324 Utah TN00003 Massachusetts M-TNO03 Vermont VT2006 Michigan 9958 Virginia 460132 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 9980939910 Montana CERT0086 Wyoming A2LA Third Party Federal Accre'di rations A2LA— ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA — ISO 17025 a 1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA—Crypto TNO0003 ' Drinking Water ] Underground Storage Tanks e Aquatic Toxicity ° Chemical/Microbiological s Mold s Wastewater n/a Accreditation not applicable Our Locations Face National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA rat T N' 1f T 1 �w T rC 5C3 � � ✓i 1 AI'*r WY Pt6 "�,.,......_.... .. v IA�_,..,,'" ✓ �� NV i 4--..._ �. ... W V V [k U "- IL 1 ,t °°33 lit ♦ � ��.... _..µ....»,.. � .,t" �.... `` * .., "S r t©' ICY >, Nvr.T ti mm,,,m„" ........ P , , ► , � y T kdPA SC r)it` AR tr_-;^? ...F„... P11S AL [A _.. TX t.A AK FL { 4 ,ter �•�-�- x HI ... 1 � ACCOUNT: PROJECT: SDG: DATF/TIMF• Arc• E E FS F E E E 0 F