NC0000019_Regional Office Historical File Pre 2016

Pr
Pat McCrory
Governor
Mr. Butch Howell
United Chemi-Con
185 McNeil Road
Lansing, NC 28643
NCDENR
North Carolina Department of Environment and Natural Resources
SUBJECT:
Dear Mr. Howell:
July 21, 2015
Compliance Evaluation Inspection (CEI)
United Chemi-Con WWTP
NPDES Permit # NC0000019
Ashe County
Donald R. van der Vaart
Secretary
On July 16, 2015 George Smith performed a Compliance Evaluation Inspection. Mr. Gale D. Howell, ORC,
Grade IV, and Mr. John Turner, Back-up, Grade I, were present for the inspection. The inspection is comprised
of an overall evaluation in order to document compliance and noncompliance of. facilities equipment, capability
to meet effluent limits, and NPDES permit terms & conditions.
Permit
Your NPDES permit became effective on January 1, 2012 and expires on March 31, 2016.
The permit identifies the following discharge pipes:
(001) Non -contact cooling water, A/C condensate, boiler blow -down, de -ionizer backwash, assembled product
wash water & process wastewater.
(003) A/C condensate.
(006) Domestic wastewater.
(007) Recycled non -contact cooling water, and filtered surface water during maintenance periods only.
Records & Reports
Mr. Howell maintains a log. Mr. Howell documents phone conversations, calibrations, process control, and all
are done in an excellent manner.
Facility Site Review
The effluent from the Imhoff tank was clear with no visible solids.
The sandfilters were raked and appeared to be clean and in good condition. There was no evidence of ponding
on the surface of the sandfilters.
The dosing lines and concrete pads are intact.
450 W. Hanes Mill Road, Winston-Salem, North Carolina 27105
DKnn 11P 77P WN) \ In#ornc}• nnrionr nnv

"Im
Flow Measurement
The instantaneous flow at Outfall 006 is obtained by measuring the height of the water in a 1-inch parshall
flume then converting it to flow (MGD).
The Stevens, Model 61R flow meter at Outfall 001 was calibrated by B.W. Allen on June 25, 2015.
Laboratory
Mr. Howell performs pH and Temperature; and these tests are recorded on the daily monitoring report.
A field certification for pH and Temperature was issued to Mr. Butch Howell for United Chemi-Con (lab
#5099). All remaining tests are performed by TriTest (Certified Lab #103).
Calibration for pH is performed using Fisher standards of pH 4 and 10, and a check at pH 7.
The temperature is recorded against a NIST traceable thermometer.
Effluent/Receiving Waters
The effluent from Pipe 006 to the North Fork New River, Class C HQW waters of the State was clear, no color,
no solids, or no odor.
The effluent from pipes 001 and 006 do not impact the North Fork New River.
Pipe 001 is discharging clear water with no color.
The manhole with the parshall flume for Pipe 006 has some solids from the river backing -up into the flume.
Effluent pipes 003 and 007 were not discharging.
In conclusion, none of the discharge pipes appear to be impacting the river.
Operations & Maintenance
Mr. Butch Howell, Grade IV is the current ORC. The back-up operator is Mr. John Turner, Grade I.
The facility (pipe 006) with the Imhoff tank is considered a Class I facility.
The facility was well maintained by the staff, and they are considered to perform their jobs in an outstanding
manner. The sandbed is well maintained. The Imhoff tank appears to be well operated & maintained.
Process control tests of pH, ammonia, alkalinity, oil & grease are performed on the influent and Imhoff tank.
These process control tests appear to be successfully used in measuring plant performance.

rSeif-Monitoring Program
A review of the monthly self -monitoring reports from June 2014 through March 2015 did not show any limit
violations.
Grab samples are taken from the end of the pipe 006 at the bank of the river.
The composite sampler at Pipe 001 is time composite at 300 mL every 30 minutes. This time composite sample
is acceptable because the flow only varies related to non -contact cooling water, which is tied to plant production
rates. There are no inflow & infiltration issues.
The chain -of -custody reports were accurate and in good order.
Mr. Howell continues to perform in an excellent manner. The compliance evaluation inspection is considered
satisfactory. If you have any questions please contact George Smith or me at [phone].
Sincerely,
W. Corey Basinger, Regional Supervisor
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
cc: WSRO Files

United States Environmental Protection Agency
Form Approved.
EPA Washington, D.0 20460
OMB No. 2040-0057
Water Compliance Inspection Report
Approval expires 8-31-98
Section A: National Data System Coding (i.e., PCS)
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type
1 IN 1 2 15 1 3 I N00000019 I11 12 15/07/16 17 18 L CJ 19 1 s t 20I
21111111 1111111111111111111111111 11111111111 r6
Inspection
Work Days Facility Self -Monitoring Evaluation Rating B1 QA ---------------Reserved-------------
67
1 -1 70 71 ID I 72 I N I 731 1 174 751 1 1 1 1 1 1 180
LJ LJ t t
Section B: FacilityData
Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include
Entry Time/Date
Permit Effective Date
POTW name and NPDES permit Number)
10:30AM 15/07/16
12/01/01
United Chemi-Con
185 McNeil Rd
Exit Time/Date
Permit Expiration Date
Lansing NC 28643
11:10AM 15/07/16
16/03/31
Name(s) of Onsite Representative(s)/Titles(s)/Phone and Fax Number(s)
Other Facility Data
Gale Dean Howeil/ORC/336-384-6917/
Name, Address of Responsible Official/Title/Phone and Fax Number
Contacted
Gale D Howell,185 McNeil Rd Lansing NC 28643H336-384-6917/
No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit 0 Flow Measurement Operations 8 Maintenance 0 Records/Reports
Self -Monitoring Program 0 Facility Site Review Effluent/Receiving Waters
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date
George S Smith WSRO WQH336-776-9700/
Signature of Management Q A Reviewer Agency/Office/Phone and Fax Numbers Date
l(JL
EPA Form 3560-3 (Revz-94) Previous editions are obsolete.
Page#

Permit: NC0000019
Inspection Date: 07/16/2015
Owner - Facility: United Chemi-Con
Inspection Type: Compliance Evaluation
"IN
Operations & Maintenance Yes No NA NE
Is the plant generally clean with acceptable housekeeping? 0 ❑ ❑ ❑
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable 0 ❑ ❑ ❑
Solids, pH, DO, Sludge Judge, and other that are applicable?
Comment:
Permit
Yes No NA NE
(If the present permit expires in 6 months or less). Has the permittee submitted a new
❑
❑
0
❑
application?
Is the facility as described in the permit?
0
❑
❑
❑
# Are there any special conditions for the permit?
❑
0
❑
❑
Is access to the plant site restricted to the general public?
0
❑
❑
❑
Is the inspector granted access to all areas for inspection?
0
❑
❑
❑
Comment:
Record Keeping
Yes No NA NE
Are records kept and maintained as required by the permit?
M
❑
❑
❑
Is all required information readily available, complete and current?
M
❑
❑
❑
Are all records maintained for 3 years (lab. reg. required 5 years)?
0
❑
❑
❑
Are analytical results consistent with data reported on DMRs?
0
❑
❑
❑
Is the chain -of -custody complete?
M
❑
❑
❑
Dates, times and location of sampling
Name of individual performing the sampling
Results of analysis and calibration
Dates of analysis
Name of person performing analyses
Transported COCs
Are DMRs complete: do they include all permit parameters?
M
❑
❑
❑
Has the facility submitted its annual compliance report to users and DWQ?
❑
❑
0
❑
(If the facility is = or > 5 MGD permitted flow) Do they operate 24/7 with a certified operator
❑
❑
M
❑
on each shift?
Is the ORC visitation log available and current?
M
❑
❑
❑
Is the ORC certified at grade equal to or higher than the facility classification?
0
❑
❑
❑
Is the backup operator certified at one grade less or greater than the facility classification?
0
❑
❑
❑
Is a copy of the current NPDES permit available on site?
M
❑
❑
❑
Page# 3

PV
Permit: NC0000019 Owner -Facility: United Chemi-Con
Inspection Date: 07/16/2015 Inspection Type: Compliance Evaluation
Record Keeping Yes No NA NE
Facility has copy of previous year's Annual Report on file for review? ❑ ❑ N ❑
Comment:
Effluent Pipe Yes No NA NE
Is right of way to the outfall properly maintained? 0 ❑ ❑ ❑
Are the receiving water free of foam other than trace amounts and other debris? 0 ❑ ❑ ❑
If effluent (diffuser pipes are required) are they operating properly? ❑ ❑ 0 ❑
Comment:
Flow Measurement - Effluent
Yes No NA NE
# Is flow meter used for reporting?
N
❑
❑
❑
Is flow meter calibrated annually?
0
❑
❑
❑
Is the flow meter operational?
0
❑
❑
❑
(If units are separated) Does the chart recorder match the flow meter?
N
❑
❑
❑
Comment. -
Effluent Sampling
Yes No NA NE
Is composite sampling flow proportional?
M
❑
❑
❑
Is sample collected below all treatment units?
0
❑
❑
❑
Is proper volume collected?
N
❑
❑
❑
Is the tubing clean?
0
❑
❑
❑
# Is proper temperature set for sample storage (kept at less than or equal to 6.0 degrees
0
❑
❑
❑
Celsius)?
Is the facility sampling performed as required by the permit (frequency, sampling type
0
❑
❑
❑
representative)?
Comment:
Page# 4

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Reference NC NPDES NC0000019
United Chemi-Con, Inc.
28 January 2015
TO WHOM IT MAY CONCERN:
Based on my inquiry of the person or persons directly responsible for managing compliance with the
permit limitation for total toxic organics, I certify that, to the best of my knowledge and belief, no
dumping of concentrated toxic organics into the wastewater has occurred since the filing of the last
discharge report.
Gale D. Howell, Jr
Environment/Safety Manager

Pat McCrory
Governor
I.
II.
TWA
A �
,A
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Resources
Donald R. van der Vaart
WATER QUALITY PERMITTING SECTION Secretary
This form is for ownership changes or name changes of NPDES wastewater permits.
• "Permittee" references the existing permit holder
• "Applicant" references the entity avvlvin2 for the ownership/name change.
NPDES Permit No. (for which the change is requested: N C 0 0 0 0 0 1 9
or
Certificate of Coverage #: N C G 5
Existing Permittee Information:
a. Permit issued to (company name):
b. Person legally responsible for permit:
c. Facility name:
United Chemi-Con, Inc
Yoshi Narita
First MI Last
Vice President of Operations
Title
185 McNeil Rd.
Permit Holder Mailing Address
Lansing NC 28643-
City State zip
[phone] [phone]
Phone Fax
United Chemi-Con, Inc
d. Facility's physical address: 185 McNeil Rd
Address
Lansing NC 28643
City State zip
e. Facility contact person: Gale D. Howell, Jr [phone]
First / MI / Last Phone
III. Applicant Information:
a. Request for change is a result of ❑ Change in ownership of the facility
❑ Name change of the facility or owner
If other please explain: Change of staff assignment
b. Permit issued to (company name): United Chemi-Con, Inc
c. Person legally responsible for permit: Steve V Katz
First MI Last
Plant Manager
Title
185 McNeil Rd
Permit Holder Mailing Address
Lansing NC 28643-
City State zip
[phone] [e-mail]
Phone E-mail Address
Page t of 2 Revised 710112014

d. Facility name: United Chemi-Con, Inc
e. Facility's physical address: 185 McNeil Rd
Address
Lansing NC 28643
City State Zip
f. Facility contact person: Gale D Howell, Jr
First MI Last
Environment Health and Safety Manager
Title
[phone] [e-mail]
Phone E-mail Address
IV. Will the permitted facility continue to conduct the same commercial/industrial activities conducted prior to
this ownership or name change?
® Yes
❑ No (please explain)
If applicable, the applicant shall submit a major permit modification request to DWR. A major modification shall be
defined as one that increases the volume, increases the pollutant load, results in a significant relocation of the
discharge point, or results in a change in the characteristics of the waste generated.
V. Required Items: THIS APPLICATION WILL BE RETURNED UNPROCESSED IF ITEMS ARE
INCOMPLETE OR MISSING:
1. This completed application is required for both name change and/or ownership change requests.
2. Legal documentation of the transfer of ownership (such as relevant pages of a contract deed, or a bill of sale) is
required for an ownership change request. Articles of incorporation are not sufficient for an ownership change.
Applicable regulations: 40 CFR 122.41, 40 CFR 122.61 and 15A NCAC 02H .0114
.....................................................................................................................
The certifications below must be completed and signed by both the permit holder prior to the change (Permittee), and the
new applicant in the case of an ownership change request. For a name change request, the signed Applicant's Certification
is sufficient.
PERMITTEE CERTIFICATION (Permit holder prior to ownership change):
I, , attest that this application for a name/ownership change has been reviewed and is accurate and complete to the
best of my knowledge. I understand that if all required parts of this application are not completed and that if all required
supporting information is not included, this application package will be returned as incomplete.
Signature
APPLICANT CERTIFICATION
Date
I, S. Katz, attest that this application for a name/ownership change has been reviewed and is accurate and complete to the
best of my knowledge. I understand that if all required parts of this application are not completed and that if all required
supporting information is not included, this application package will be returned as incomplete.
Signature
**************************
Date
PLEASE SEND THE COMPLETE APPLICATION PACKAGE TO:
Division of Water Resources
Water Quality Permitting Section
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
NPDES PERMIT NAME/OWNERSHIP CHANGE REQUEST
Page 2 of 2 Revised 710112014

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YXX
NCDENR
FV North Carolina Department of Environment and Natural Resources
Division of Water Resources
Water Quality Regional Operations Section
Pat McCrory John E. Skvarla, III
Governor Secretary
June 4, 2014
Mr. Butch Howell
United Chemi-Con
185 McNeil Road
Lansing, NC 28643
SUBJECT: Compliance Evaluation Inspection (CEI)
United Chemi-Con WWTP
NPDES Permit # NC0000019
Ashe County
Dear Mr. Howell:
On May 30, 2014 George Smith performed a Compliance Evaluation Inspection. Mr. Gale D.
Howell, ORC, Grade IV, and Mr. John Turner, Back-up, Grade I, were present for the
inspection. The inspection is comprised of an overall evaluation in order to document
compliance and noncompliance of. facilities equipment, capability to meet effluent limits, and
NPDES permit terms & conditions.
Permit
Your NPDES permit became effective on January 1, 2012 and expires on March 31, 2016.
The permit identifies the following discharge pipes:
(001) Non -contact cooling water, A/C condensate, boiler
assembled product wash water & process wastewater.
(003) A/C condensate.
(006) Domestic wastewater.
(007) Recycled non -contact cooling water, and filtered
periods only.
Records & Reports
blow -down, de -ionizer backwash,
surface water during maintenance
Mr. Howell maintains a log. Mr. Howell documents phone conversations, calibrations, process
control, and all are done in an excellent manner.
Facility Site Review
The effluent from the Imhoff tank was clear with no visible solids.
585 Waughtown Street„ North Carolina 27360
Phone: [phone] Fax: [phone]
Internet:: www.nmateraualitv.orn
An Eaual ODDortunhAffirmaBve Action Emolover

Compliance Evaluation Inspection
June 4, 2014
Page 2 of 3
The sandfilters were raked and appeared to be clean and in good condition. There was no
evidence of ponding on the surface of the sandfilters.
The dosing lines and concrete pads are intact.
Flow Measurement
The instantaneous flow at Outfall 006 is obtained by measuring the height of the water in a f-
inch parshall flume then converting it to flow (MGD).
The Stevens, Model 61 R flow meter at Outfall 001 was calibrated by B.W. Allen on June 12,
2013. Remember that flow calibration to be accurate within 10% of the true flow is required
annually.
Laboratory
Mr. Howell performs pH and Temperature; and these tests are recorded on the daily monitoring
report.
A field certification for pH and Temperature was issued to Mr. Butch Howell for United Chemi-
Con (lab #5099). All remaining tests are performed by TriTest (Certified Lab #103).
Calibration for pH is performed using Fisher standards of pH 4 and 10, and a check at pH 7.
The temperature is recorded against a NIST traceable thermometer.
Effluent/Receiving Waters
The effluent from Pipe 006 to the North Fork New River, Class C HQW waters of the State was
clear, no color, no solids, or no odor.
The effluent from pipes 001 and 006 do not impact the North Fork New River.
Pipe 001 has some foam discharging, but it dissipates before reaching the river.
The manhole with the parshall flume for Pipe 006 is free of debris
Effluent pipes 003 and 007 were not discharging.
In conclusion, none of the discharge pipes appear to be impacting the river.
Operations & Maintenance
Mr. Butch Howell, Grade IV is the current ORC. The back-up operator is Mr. Allan Miller is in
training.

ompliance Evaluation Inspection
June 4, 2014
Page 3 of 3
The facility (pipe 006) with the Imhoff tank is considered a Class I facility.
The facility was well maintained by the staff, and they are considered to perform their jobs in an
outstanding manner. The sandbed is well maintained. The Imhoff tank appears to be well
operated & maintained.
Process control tests of pH, ammonia, alkalinity, oil & grease are performed on the influent and
Imhoff tank. These process control tests appear to be successfully used in measuring plant
performance.
Self -Monitoring Program
A review of the monthly self -monitoring reports from June 2013 through March 2014 did not
show any limit violations.
Grab samples are taken from the end of the pipe 006 at the bank of the river.
The composite sampler at Pipe 001 is time composite at 300 nil, every 30 minutes. This time
composite sample is acceptable because the flow only varies related to non -contact cooling
water, which is tied to plant production rates. There are no inflow & infiltration issues.
The chain -of -custody reports were accurate and in good order.
Mr. Howell continues to perform in an excellent manner. The compliance evaluation inspection
is considered satisfactory. If you have any questions please contact George Smith at (336) 771-
4968.
Sincerely,
W. Corey Basinger
Regional Supervisor
Water Quality Section
Division of Water Resources
cc: WSRO Files

P!7
United States Environmental Protection Agency
Form Approved.
EPA Washington, D.C. 20460
OMB No. 2040-0057
Approval expires 8-31-98
Section A: National Data System Coding (i.e., PCS)
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type
1 L2 J 31 NC0000019 111 121 14/05/30 117 18J 191LSJ I 20
Remarks
21111111111111111111111111111111111111111111111116
Inspection Work Days Facility Self -Monitoring Evaluation Rating B1 QA ----- — —Reserved---- ---
671 1 69 70) 3 71 I D I 72 (N 73 I 174 751 1 1 1 1 1 1 180
�--� L -I W
Section B: Facility Data
Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include
Entry Time/Date
Permit Effective Date
POTW name and NPDES permit Number)
United Chem! -Con
10:45 AM 14/05/30
12/01/01
Exit Time/Date
Permit Expiration Date
185 McNeil Rd
Lansing NC 28643
11:50 AM 14/05/30
16/03/31
Name(s) of Onsite Representative(s)/Titles(s)/Phone and Fax Number(s)
Other Facility Data
Gale Dean Howell/ORC/336-384-6917/
Name, Address of Responsible Officialfritle/Phone and Fax Number
Contacted
Gale D Howell,185 McNeil Rd Lansing NC 28643//336-384-6917/ No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit 0 Flow Measurement Operations & Maintenance N Records/Reports
Self -Monitoring Program 0 Facility Site Review Effluent/Receiving Waters
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date
George S Smith WSRO WQH336-771-5000/
Signature of Management Q A Reviewer Agency/Office/Phone and Fax Numbers Date
ICA
EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete.
Page # 1

PV
Permit: NC0000019
Inspection Date: 05/30/2014
Owner - Facility: United Chemi-Con
Inspection Type: Compliance Evaluation
Operations & Maintenance Yes No NA NE
Is the plant generally clean with acceptable housekeeping? ■ ❑ ❑ ❑
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable Solids, pH, DO, Sludge ■ ❑ ❑ ❑
Judge, and other that are applicable?
Comment:
Permit Yon NA NA up
(If the present permit expires in 6 months or less). Has the permittee submitted a new application? ❑ ❑ ■ ❑
Is the facility as described in the permit? ■ ❑ ❑ ❑
# Are there any special conditions for the permit? ■ ❑ ❑ ❑
Is access to the plant site restricted to the general public? ■ ❑ ❑ ❑
Is the inspector granted access to all areas for inspection? ■ ❑ ❑ ❑
Comment: acute toxicity, eposodic
Record Keeping
Yes No NA NE
Are records kept and maintained as required by the permit?
■ ❑ ❑ ❑
Is all required information readily available, complete and current?
■ ❑ ❑ ❑
Are all records maintained for 3 years (lab. reg. required 5 years)?
■ ❑ ❑ ❑
Are analytical results consistent with data reported on DMRs?
■ ❑ ❑ ❑
Is the chain -of -custody complete?
■ ❑ ❑ ❑
Dates, times and location of sampling
■
Name of individual performing the sampling
■
Results of analysis and calibration
■
Dates of analysis
■
Name of person performing analyses
■
Transported COCs
■
Are DMRs complete: do they include all permit parameters?
■ ❑ ❑ ❑
Has the facility submitted its annual compliance report to users and DWQ?
❑ ❑ ■ ❑
(If the facility is = or > 5 MGD permitted flow) Do they operate 24/7 with a certified operator on each shift?
❑ ❑ ■ ❑
Is the ORC visitation log available and current?
■ ❑ ❑ ❑
Is the ORC certified at grade equal to or higher than the facility classification?
■ ❑ ❑ ❑
Is the backup operator certified at one grade less or greater than the facility classification?
■ ❑ ❑ ❑
Is a copy of the current NPDES permit available on site?
■ ❑ ❑ ❑
Page # 3

Pr
Permit: NC0000019 Owner - Facility: United Chemi-Con
Inspection Date: 05/30/2014 Inspection Type: Compliance Evaluation
Record Keeping Yes No NA NE
Facility has copy of previous year's Annual Report on file for review? ■ ❑ ❑ ❑
Comment:
Flow Measurement - Effluent
Yes No NA
NE
# Is flow meter used for reporting?
■ ❑ ❑
❑
Is flow meter calibrated annually?
■ ❑ ❑
❑
Is the flow meter operational?
■ ❑ ❑
❑
(If units are separated) Does the chart recorder match the flow meter?
❑ ❑ ❑
■
Comment:
Sand Filters (Low rate)
Yes No NA
NE
(If pumps are used) Is an audible and visible alarm Present and operational?
❑ ❑ ■
❑
Is the distribution box level and watertight?
■ ❑ ❑
❑
Is sand filter free of ponding?
■ ❑ ❑
❑
Is the sand filter effluent re -circulated at a valid ratio?
❑ ❑ ■
❑
# Is the sand filter surface free of algae or excessive vegetation?
■ ❑ ❑
❑
# Is the sand filter effluent re -circulated at a valid ratio? (Approximately 3 to 1)
❑ ❑ ■
❑
Comment:
Page # 4

Cover Sheet from
Staff Member to
Regional Supervisor
DMR Review Record
Facility: , —111a, rA - L, Pernut/Pipe No.: N000600 i y Month/Year T l �013
Monthly Average Violations
Parameter Permit Limit DMR Value
Date Parameter
Weekly/DaiIy Violations
Permit Limitf vpe
DMR Value
% Over Limit
% Over Limit
Monitoring Frequency Violations
Date Parameter Permit Frequency_ Values Reported # of Violations .
7' 3l Ro D .2x rno, Z—A. I
7- 3 1 775,5
Other Violations
RPc (%O ( It-' e[S S d Mev'iL) a ij Coad 4or S4t"ple
Completed by: Date: 111 a f li 3
Regional Water Quality 5 +�
Supervisor Signoff: Date: 2
�.✓l�t�i

Smith, George
From:
Butch Howell <[e-mail]>
Sent:
Tuesday, July 16, 2013 9:41 AM
To:
Smith, George
Cc:
John Turner
Subject:
UCC Outfall 006
George,
UCC outfall 006 (the sand filter system) is submerged. This condition has persisted all the way through July. Our permit
requires two samples (grab) for BOD and TSS, and one for NH3-N. Representative samples with a ten day separation
appears highly unlikely. Any advice?
-butch

Ashe
NCO000019
Monitoring Violation
United Chem! -Con
Frequency Organics, Total Toxic Milligrams
Violation 2013 3 001 (TTO) 03-31-2013 Quarterly per Liter
Frequency Organics, Total Toxic Milligrams
Violation 2013 3 006 (TTO) 03-31-2013 Quarterly per Liter
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ats 2 V1oltVIcn
1n QIMf

PV
Pat McCrory
Governor
Mr. Butch Howell
United Chemi-Con
185 McNeil Road
Lansing, NC 28643
4
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Charles Wakild, P. E. John E. Skvarla, III
Director Secretary
June 3, 2013
SUBJECT: Compliance Evaluation Inspection (CEI)
United Chemi-Con WWTP
NPDES Permit # NC0000019
Ashe County
Dear Mr. Howell:
On May 31, 2013 George Smith performed a Compliance Evaluation Inspection. Mr. Gale D. Howell, ORC,
Grade IV, was present for the inspection. The inspection is comprised of an overall evaluation in order to
document compliance and noncompliance of. facilities equipment, capability to meet effluent limits, and
NPDES permit terms & conditions.
Permit
Your NPDES permit became effective on January 1, 2012 and expires on March 31, 2016.
The permit identifies the following discharge pipes:
(001) Non -contact cooling water, A/C condensate, boiler blow -down, de -ionizer backwash, assembled product
wash water & process wastewater.
(003) A/C condensate.
(006) Domestic wastewater.
(007) Recycled non -contact cooling water, and filtered surface water during maintenance periods only.
Records & Reports
Mr. Howell maintains a log. Mr. Howell documents phone conversations, calibrations, process control, and all
are done in an excellent manner.
Facility Site Review
The effluent from the Imhoff tank was clear with no visible solids.
North Carolina Division of Water Quality, Winston-Salem Regional Office
Location: 585 Waughtown Street, Winston-Salem, North Carolina 27107
Phone: [phone] FAX: [phone]
Internet www.ncwaterouality.om
Nne
orthCarolina
APaturallr�
An Equal Opportunity 1 Affirmative Action Employer

CEI
June 3, 2013
Page 2 of 3
The sandfilters were raked and appeared to be clean and in good condition. There was no evidence of ponding
on the surface of the sandfilters.
The dosing lines and concrete pads are intact.
Flow Measurement
The instantaneous flow at Outfall 006 is obtained by measuring the height of the water in a 1-inch parshall
flume then converting it to flow (MGD).
The Stevens, Model 61R flow meter at Outfall 001 was calibrated by B.W. Allen last year and is scheduled for
calibration June 5, 2013.
Laboratory
Mr. Howell performs pH and Temperature; and these tests are recorded on the daily monitoring report.
A field certification for pH and Temperature was issued to Mr. Butch Howell for United Chemi-Con (lab
#5099). All remaining tests are performed by TriTest (Certified Lab #103).
Calibration for pH is performed using Fisher standards of pH 4, 7, 10.
The temperature is recorded against a NIST traceable thermometer.
Effluent/Receiving Waters
The effluent from Pipe 006 to the North Fork New River, Class C HQW waters of the State was clear, no color,
no solids, or no odor.
The effluent from pipes 001, 003, 006, and 007 do not impact the North Fork New River. The manhole with the
parshall flume for Pipe 006 is free of debris
Effluent pipes 003 and 007 were not discharging.
Operations & Maintenance
Mr. Butch Howell, Grade IV is the current ORC. The back-up operator is Mr. Allan Miller is in training.
The facility (pipe 006) with the Imhoff tank is considered a Class H facility.
The facility was well maintained by the staff, and they are considered to perform their jobs in an outstanding
manner. The sandbed is well maintained. The Imhoff tank appears to be well operated & maintained.
Process control tests of pH, ammonia, alkalinity, oil & grease are performed on the influent and Imhoff tank.
Process control tests appear to be successfully used in measuring plant performance.

rPageof3
3
Self -Monitoring Program
A review of the monthly self -monitoring reports from June 2012 through February 2013 did not show any limit
violations.
Grab samples are taken from the end of the pipe 006 at the bank of the river.
The composite sampler at Pipe 001 is time composite at 200 mL every 30 minutes.
The chain -of -custody reports were accurate and in good order.
Mr. Howell continues to perform in an excellent manner. The compliance evaluation inspection is considered
satisfactory. If you have any questions please contact George Smith at [phone].
Sincerely,
W. Corey Basinger
Regional Supervisor
cc: WSRO Files

United States Environmental Protection Agency
Form Approved.
E PA Washington, D.C. 20460
OMB No. 2040-0057
Approval expires 8-31-98
Section A: National Data System Coding (i.e., PCS)
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type
1 INI 2 15I 31 NC0000019 111 121 13/05/31 117 18I C I 19! S I 20I I
J !J
Remarks
211IIIIIIIIIIIIIIIIIIIIIII111111111111111111111116
Inspection Work Days Facility Self -Monitoring Evaluation Rating B1 QA — — ---- - --- Reserved---- -- ---- -
67 I 169 70131 71 LI 72 I N I 73 L_U 74 751 I I I I I Li
Section B: Facility Data
Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include
Entry Time/Date
Permit Effective Date
POTW name and NPDES permit Number)
10:15 AM 13/06/31
12/01/01
United Chemi-Con
Exit Time/Date
Permit Expiration Date
185 McNeil Rd
Lansing NC 28643
10:50 AM 13/05/31
16/03/31
Name(s) of Onsite Representative(s)/Titles(s)/Phone and Fax Number(s)
Other Facility Data
///
Gale Dean Howell/ORC/336-384-6917/
Name, Address of Responsible Official/Title/Phone and Fax Number
Contacted
Gale D Howell,185 McNeil Rd Lansing NC 28643//336-384-6917/ No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit Flow Measurement Operations & Maintenance 0 Records/Reports
Self -Monitoring Program Facility Site Review Effluent/Receiving Waters
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date
George S Smith WSRO WQ//336-771-5000/
Signature of Management Q A Reviewer Agency/Office/Phone and Fax Numbers Date
EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete.
Page # 1

NPDES
yr/mo/day
31 NC0000019 I11 121 13/05/31 I17
Inspection Type
18I '
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
Page # 2

Permit: NC0000019
Inspection Date: 05/31/2013
Owner - Facility: United Chemi-Con
Inspection Type: Compliance Evaluation
Operations & Maintenance
Yes
No
NA
NE
Is the plant generally clean with acceptable housekeeping?
■
n
n
Q
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable Solids, pH, DO, Sludge ■
Q
❑
❑
Judge, and other that are applicable?
Comment:
Permit
Yes
No
NA
NE
(If the present permit expires in 6 months or less). Has the permittee submitted a new application?
Q
❑
■
0
Is the facility as described in the permit?
■
# Are there any special conditions for the permit?
❑
■
❑
Q
Is access to the plant site restricted to the general public?
■
D
❑
0
Is the inspector granted access to all areas for inspection?
■
0
0
0
Comment: Pipe 001 has no treatment and is calibrated for flow.
Pipe 006 is domestic flow and is instantaneous.
Record Keeping
Yes
No
NA
NE
Are records kept and maintained as required by the permit?
■
❑
n
11
Is all required information readily available, complete and current?
■
Q
Are all records maintained for 3 years (lab. reg. required 5 years)?
■
❑
❑
0
Are analytical results consistent with data reported on DMRs?
■
D
❑
El
Is the chain -of -custody complete?
■
El
C1
El
Dates, times and location of sampling
■
Name of individual performing the sampling
■
Results of analysis and calibration
■
Dates of analysis
■
Name of person performing analyses
■
Transported COCs
■
Are DMRs complete: do they include all permit parameters?
■
❑
Q
Q
Has the facility submitted its annual compliance report to users and DWQ?
0
❑
■
0
(If the facility is = or > 5 MGD permitted flow) Do they operate 24/7 with a certified operator on each shift?
❑
❑
■
0
Is the ORC visitation log available and current?
■
❑
❑
O
Is the ORC certified at grade equal to or higher than the facility classification?
■
0
Q
n
Is the backup operator certified at one grade less or greater than the facility classification?
■
Q
11
0
Page # 3

Permit: NC0000019
Inspection Date: 05/31/2013
Owner - Facility: United Chemi-Con
Inspection Type: Compliance Evaluation
Record Keeping
Is a copy of the current NPDES permit available on site?
Facility has copy of previous year's Annual Report on file for review?
Comment:
Flow Measurement - Effluent
# Is flow meter used for reporting?
Is flow meter calibrated annually?
Is the flow meter operational?
(if units are separated) Does the chart recorder match the flow meter?
Comment:
'IN
■❑❑❑
❑❑■❑
Yes No NA NE
Page # 4

Cover Sheet from
Staff Member to
Regional Supervisor
DMR Review Record
Facility: un+ i� C�i�a; - ��� PermitfPipe No.: A,0000012 Month/Year t dre4 2013
Monthly Average Violations
Parameter Permit Limit DMR Value % Over Limit
weekly/Daily Violations
Date Parameter Permit Limitll'v�e DMR Value % Over Limit
Monitoring Frequency Violations
Date Parameter Permit Frequ encv Values Reported # of Violations
:3-3/ TTD PIPE DO _ IXURr'itry ___1 F� b do 13 0 "t R
Other Violations
Completed by: --
Date:
Regional Water Quality
Date:
Supervisor Signoff:l �D �- �
D k- J

AZ -
WV ►A
NCDENR
North Carolina Department of Environment and
Division of Water Quality
Beverly Eaves Perdue Charles Wakild, P.E.
Governor Director
December 31, 2012
CERTIFIED MAIL
RETURN RECEIPT REQUESTED: 7007 1490 0004 5533 7148
Mr. Gale D. Howell
United Chemi-Con Inc.
185 McNeil Rd.
Lansing, NC 28643
Natural Resources
Subject: NOTICE OF VIOLATION: NR NOV-2012-MV-0132
Effluent Toxicity Testing
NPDES Permit No. NC0000019
United Chemi-Con WWTP
Ashe County
Dear Mr. Howell:
rv.,—uept. of ENR
JAN 0 4 2013
Winston-Salem
Regional Office
Dee Freeman
Secretary
This is to inform you that the Environmental Sciences Section has not received your quarterly toxicity self -
monitoring report form for the month of October 2012. This is in violation of Title 15A of the North Carolina
Administrative Code, Chapter 2, Subchapter 213, Section .0506 (a)(1)(A) which states that "monthly monitoring
reports shall be filed no later than 30 days after the end of the reporting period for which the report was made."
Please remember that reporting of toxicity self -monitoring data is a dual requirement. Toxicity test results must be entered
on your Discharge Monitoring Report and the Toxicity Reporting Form (AT Report Form). The AT report form must be
submitted to: DWQ/ESS, 1621 Mail Service Center, Raleigh NC 27699-1621 within the required time frame.
Your NPDES permit requires you to submit an Aquatic Toxicity Self -Monitoring Form to this office during a month in which
toxicity testing is required, regardless of whether a discharge occurs from the facility. Please ensure that AT test forms
labeled "No Flow" are sent to this office during months when no discharge occurs and the facility is required to perform
toxicity testing.
Additional reporting and/or monitoring violations within a twelve (12) month period subiects the facility to the
enforcement authority of the Division.
Environmental Sciences Section
1621 Mail Service Center, Raleigh, North Carolina 27699-1621
Location: 4401 Reedy Creek Road, Raleigh, North Carolina 27607
Phone: [phone] FAX: [phone] Customer Service: 1-877-623-6748
Internet: hftp://h2o.enr,state.nc.uslesb/
NorthCarolina
Naturld'y
An Equal Opportunity 1 Affirmative Action Employer

Attached to this Notice, you will find a summary of important toxicity monitoring and reporting requirements. Please read
this summary. If you have any questions concerning this Notice, please contact Mr. John Giorgino with the Aquatic
Toxicology Unit at [phone].
Sincerely,
() � dro r
Cindy Moore
Supervisor, Aquatic Toxicology Unit
cc: Corey Basinger- Winston-Salem Regional Office
Jenifer Carter- Winston-Salem Regional Office
Aquatic Toxicology Unit
Central Files
Environmental Sciences Section
1621 Mail Service Center, Raleigh, North Carolina 27699-1621
Location: 4401 Reedy Creek Road, Ralegh, North Carolina 27607
Phone: [phone] \ FAX: [phone] \ Customer Service: 1-877.623-6748
Internet: http:l/h2o.enr.state.nc.us/esbl
NorthCarolina
Naturally
An Equal Opportunity \ Affirmative Action Employer

WHOLE EFFLUENT TOXICITY MONITORING AND REPORTING INFORMATION
➢ The following items are provided in an effort to assist you with identifying critical and sometimes overlooked toxicity testing and reporting
information. Please take time to review this information. The items below do not address or include all the toxicity testing and reporting
reauirements contained in your NPDES permit. If you should have any questions about your toxicity testing requirement, please contact Mr.
John Giorgino with the Aquatic Toxicology Unit at [phone] or another Unit representative at the same number.
➢ The permittee is responsible for ensuring that toxicity testing is conducted according to the permit requirement and that toxicity report forms are
appropriately filed.
➢ The reporting of whole effluent toxicity testing data is a dual requirement. All toxicity test results must be entered (with the appropriate
parameter code) on your monthly Discharge Monitoring Report which is submitted to:
North Carolina Division of Water Quality
Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
IN ADDITION
Toxicity test data (original "AT" form) must be submitted to the following address:
North Carolina Division of Water Quality
Environmental Sciences Section
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
➢ Toxicity test results shall be filed with the Environmental Sciences Section no later than 30 days after the end of the reporting period
(eg, January test result is due by the end of February).
➢ Toxicity test condition language contained in your NPDES permit may require use of multiple concentration toxicity testing upon failure of any
single quarterly toxicity test. If the initial pass/fail test fails or if the chronic value is lower than the permit limit, then at least two multiple
concentration toxicity tests (one per month) will be conducted over the following two months. As many analyses as can be completed will be
accepted. If your NPDES permit does not require use of multiple concentration toxicity testing upon failure of any single quarterly test, you
may choose to conduct either single concentration toxicity testing or multiple concentration toxicity testing per the Division's WET enforcement
initiatives effective July 1, 1999. Follow-up multiple concentration toxicity testing will influence the Division's enforcement response.
➢ Toxicity testing months are specified by the NPDES Permit, except for NPDES Permits which contain episodic toxicity monitoring
requirements (eg, if the testing months specified in your NPDES permit are March, June, September, and December, then toxicity testing must
be conducted during these months).
➢ If your NPDES Permit specifies episodic monitoring and your facility does not have a discharge from January 1-June 30, then you must provide
written notification to the Environmental Sciences Section by June-30-that-adischarge_did not -occur during the first six months of the calendar
year.
➢ If you receive notification from your contract laboratory that a test was invalidated, you should immediately notify the Environmental Sciences
Section at [phone] and provide written documentation indicating why the test was invalidated and the date when follow-up testing will
occur.
➢ If your facility is required to conduct toxicity testing during a month in which no discharge occurs, you should complete the information block
located at the top of the AT form indicating the facility name, permit number, pipe number, county and the month/year of the subject report.
You should also write "No Flow" on the AT form, sign the form and submit following normal procedures.
➢ The Aquatic Toxicity Test forms shall be signed by the facility's Operator in Responsible Charge (ORC) except for facilities which have not
received a facility classification. In these cases, a duly authorized facility representative must sign the AT form. The AT form must also be
signed by the performing lab supervisor.
➢ To determine if your AT test forms were received on time by the Division of Water Quality, you may consider submitting your toxicity test
results certified mail, return receipt requested to the Environmental Sciences Section.
Environmental Sciences Section
1621 Mail Service Center, Raleigh, North Carolina 27699-1621
Location: 4401 Reedy Creek Road, Raleigh, North Carolina 27607
Phone: [phone] FAX: [phone] Customer Service:1-877-623-6748
Internet httpJ/h2o.enr.state.nc.us/esb/
NorthCarohna
Nakiii4
An Equal Opportunity 1 Affirmative Action Employer

Environmental Sciences Section
1621 Mail Service Center, Raleigh, North Carolina 27699-1621
Location: 4401 Reedy Creek Road, Raleigh, North Carolina 27607
Phone: [phone] FAX: [phone] Customer Service: 1-877-623-6748
Internet: http://h2o.enr.state.nc.ustesb/
NorthCarolina
Naturally
An Equal Opportunity 1 Affirmative Action Employer

Pr
Beverly Eaves Perdue
Governor
Mr. Butch Howell
United Chemi-Con
185 McNeil Road
Lansing, NC 28643
AILTrKywr
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Charles Wakild, P. E.
Director
November 27, 2012
Subject: NOTICE OF DEFICIENCY
United Chemi-Con WWTP, Pipe 001
NPDES Permit # NC0000019
Ashe County
Dear Mr. Howell:
Dee Freeman
Secretary
A review of the August 2012 Discharge Monitoring Report (DMR) revealed a monitoring violation of the
following parameter(s) at Outfall 001:
Parameter
Date
Permit Frequency
Values Reported
# of Violations
Flow
Aug 16
Continuous
30
1
Remedial actions should be taken to correct the cause(s) of this violation. The violations described above
should be abated immediately and properly resolved.
If you have any questions or require any additional information, please contact George Smith at (336) 771-
4968, [e-mail], or myself at [phone], [e-mail].
Sincerely,
W. Corey Basinger
Surface Water Protection Section
cc: WSRO File Copy
North Carolina Division of Water Quality, Winston-Salem Regional Office
Location: 585 Waughtown St. Winston-Salem, North Carolina 27107
Phone: [phone] FAX: [phone]
Internet: www.ncwaterquality.org
An Equal Opportunity 1 Affirmative Action Employer
NorthCarolina
Natmallty

Pr
Cover Sheet from
Staff Member to
Regional Supervisor
DNIR Review Record
Facility: ! z ,leni - p
�� � G�j� Permit/Pipe No.: _/LG�DOGY�l�' Month/Year �N � /),
OCR/
Monthly Average Violations
Parameter Permit Limit DMR Value % Over Limit
Weekly/DaiIy Violations
Date Parameter Permit Limit/Type DMR Value % Over Limit
Monitoring Frequency Violations
Date Parameter Permit Frequency Values Reported # of Violations
%( go /
Other Violations
Completed by: Date: A/ , v sT
Regional Water Quality V
Supervisor Signoff: Date:
1 l ,-�
a� �V0D

Cover Sheet from
Staff Member to
Regional Supervisor
DMR Review Record
Facility: Lfntt;, �.M; - �n Permit/Pipe No.: >JC 0 D000 l9 Monavyear _Dec _a0 I '),
Monthly Average Violations
Parameter Permit Limit DMR Value % Over Limit
weekly/Daily Violations
Date Parameter Permit Limit�i'vDe DMR Value % Over Limit
Monitoring Frequency Violations
Date Parameter Permit Frequencv Values Reported # of No
11-�31 T772 Pwe-,201 C�dar�Nly• Su�rnrt2cL No Lliol'tT�n
C
3l 7-7-0y
rt /vim. (����iVc� t'{✓ Pe✓vn
Other Violations
n ,)
0 1".J
Completed by: G! �_— Date: 3 - IS' t 3 3 b +3
Regional Water Quality � �� Za ( 3
Supervisor SiQnoff: Date:

Cover Sheet from
Staff Member to
Regional Supervisor
DNIR Review Record
Facility: `-IrticPermit/Pipe No.: N60000ol Y Month/Year Tune �a/a.
Monthly Average Violations
Parameter Permit Limit DMR Value % Over Limit
Weekly/Daily Violations
Date Parameter Permit Lirf i vDe DMR Value % Over Limit
Monitoring Frequency Violations
Date Parameter Permit Frequency Values Reported # of Violations
I:Y
C l36 I-T-0 cl,trne 00/ _____L_ Sk� �rtCt� ►✓
r►?�Y D to 2
C13t, 7-1-0 ��Km✓ �r�r DD �7 0 n8Z' P1rM;r— t^clvirt�
No V,Wf c'/6IJ
Other Violations
Ski I"? U/M,S
Completed by: C•.� �i/ Date: _ 9 -io - poi
Regional Water Quality
Supervisor SiQnoff: ate: fO
J V V �Q?T
Ar• c4t�
t /it //)-

NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Charles Wakild, P. E.
Governor Director
Yoshi Narita, Vice President of Operations
United Chemi-Con, Inc.
185 McNeil Road
Lansing, NC 28643
Subject:
Dear Mr. Narita:
Notice of Violation
United Chemi-Con
NPDES No. NC0000019
Ashe County
June 27, 2012
Dee Freeman
Secretary
Review of the self -monitoring report for the month of March 2012 revealed the following violation(s):
Monitoring Violation(s)
Parameter Pipe Date Permit Freq. Values Reported # of Violations
Chronic Toxicity 001 3/31
Quarterly 0
Temp. 001 3/3
Weekly 0
Flow 006 3/3
Weekly 0
Temp. 006 3/3
Weekly 0
Remedial actions, if not already implemented, should be taken to correct the above noncompliance
problem(s). Please be aware that violations of your NPDES permit could subject you to enforcement action
by this Division with the possible assessment of civil penalties of up to $25,000 per day per violation. Should
you have any questions, please contact me at [phone].
Sincerely,
W. Corey Basinger
Regional Supervisor
cc: WSRO Files
North Carolina Division of Water Quality, Winston-Salem Regional Office
Location: 585 Waughtown St. Winston-Salem, North Carolina 27107
Phone: [phone] FAX: [phone]
Internet: www.ncwaterquality.org
An Equal Opportunity 1 Affirmative Action Employer
Nne
orthCarolina
Naturally

Pr
001
Cover Sheet from
Staff Member to
Regional Supervisor
DNIR Review Record
Facility: Permit/Pipe No.: _NC 600001 � MonthNear Oa-r 0/a,
Monthly Average Violations
Parameter Permit Limit DMR Value
Weekly/Daily Violations
Date Parameter Permit Limit/7vpe DMR Value
Monitoring, Frequency Violations
% Over Limit
% Over Limit
Date Parameter Permit Frequency Values Reported # of Violations .
�-91 TT(7 _ O rrfor rc2 �n b OMt
3 -3l Chey.,e TX O
3-03
0 0 6
_3—O
Flow
wec-k ly
0
O06
3-03
T e-r7P
0 i
Completed by: CA2� Date: G /:Z7 /;-0/ a,
,U
Regional Water Quality II
Supervisor Signoff: .�YV� Date:

Ashe
NC0000019
Monitoring Violation
Frequency
Violation
2012 3
Frequency
Violation
2012 3
Frequency
Violation
20123
Frequency
Violation
2012'. 3.
Frequency
Violation
2012i 3i'.
Frequency
Violation
2012 3':
Frequency
Violation
2012 3
Frequency
Violation
2012 3
001
001
001
001
006
006
006
006
United Chemi-Con
treatment plant
03-03-2012
Weekly
Day
Organic, Total Toxic
Milligrams
(TTO)
03-31-2012
Quarterly
per Liter
P/F STATRE 7Day Chr
Pass=O,
Ceriodaphnia
03-31-2012
Quarterly
Fail=1
Temperature, Water
-
Degrees
Deg. Centigrade
103-03-2012
Weekly
Centigrade
_........ _
Flow, in conduit or thm
10
Gallons per
treatment plant
03-03-2012
Weekly
Day
Organics, Total Toxic
Milligrams
(TTO)
03-31-2012
Quarterly
per Liter
P/F STATRE 7Day Chr
Pass=O,
'Ceriodaphnia
03-31-2012
Quarterly
Fail=1
Temperature, Water
:
Degrees
Deg. Centigrade
'03-03-2012
(Weekly
Centigrade
�rrnS
Bi�'IS
PIS
vi t'1$
ea-13
/e� viOl' -10A ItOt' t^ (�lrtS,
�rw�

Or
Beverly Eaves Perdue
Governor
Mr. Butch Howell
United Chemi-Con
185 McNeil Road
Lansing, NC 28643
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Charles Wakild, P. E.
Director
June 11, 2012
SUBJECT: Compliance Evaluation Inspection (CEI)
United Chemi-Con WWTP
NPDES Permit # NC0000019
Ashe County
Dear Mr. Howell:
Dee Freeman
Secretary
On June 6, 2012 George Smith performed a Compliance Evaluation Inspection. Mr. Gale D. Howell, ORC,
Grade IV, was present for the inspection. The inspection is comprised of an overall evaluation in order to
document compliance and noncompliance of. facilities equipment, capability to meet effluent limits, and
NPDES permit terms & conditions.
Permit
Your NPDES permit became effective on January 1, 2012 and expires on March 31, 2016. This permit is
currently effective until the new permit is issued.
The permit identifies the following discharge pipes:
(001) Non -contact cooling water, A/C condensate, boiler blow -down, de -ionizer backwash, assembled product
wash water & process wastewater.
(003) A/C condensate.
(006) Domestic wastewater.
(007) Recycled non -contact cooling water, and filtered surface water during maintenance periods only.
Records & Reports
Mr. Howell maintains a log. Mr. Howell documents phone conversations, calibrations, process control, and all
are done in an excellent manner.
Facility Site Review
The effluent from the Imhoff tank was clear with no visible solids.
North Carolina Division of Water Quality, Winston-Salem Regional Office
Location: 585 Waughtown St. Winston-Salem, North Carolina 27107
Phone: [phone] FAX: [phone]
Internet www.ncwaterquality.org
An Equal Opportunity 1 Affirmative Action Employer
NorthCarolina
Naturally

CEI
June 11, 2012
Page 2 of 3
11
The sandfilters were raked and appeared to be clean and in good condition. There was no evidence of ponding
on the surface of the sandfilters.
The dosing lines and concrete pads are intact.
Flow Measurement
The instantaneous flow at Outfall 006 is obtained by measuring the height of the water in a 1-inch parshall
flume then converting it to flow (MGD).
The Stevens, Model 6 1 R flow meter at Outfall 001 was calibrated by B.W. Allen on March 23, 2012.
Laboratory
Mr. Howell performs pH and Temperature; and these tests are recorded on the daily monitoring report.
A field certification for pH and Temperature was issued to Mr. Butch Howell for United Chemi-Con (lab
#5099). All remaining tests are performed by TriTest (Certified Lab #103).
Calibration for pH is performed using Fisher standards of pH 4, 7, 10.
The temperature is recorded against a NIST traceable thermometer.
Effluent/Receiving Waters
The effluent from Pipe 006 to the North Fork New River, Class C HQW waters of the State was clear, no color,
no solids, or no odor.
The effluent from pipes 001, 003, 006, and 007 do not impact the North Fork New River. The manhole with the
parshall flume for Pipe 006 was cleaned. It contained mud and algae which may have affected the sample
integrity.
Effluent pipes 003 and 007 were not discharging.
Operations & Maintenance
Mr. Butch Howell, Grade IV is the current ORC. The back-up operator is Mr. Allan Miller is in training.
The facility (pipe 006) with the Imhoff tank is considered a Class II facility.
The facility was well maintained by the staff, and they are considered to perform their jobs in an outstanding
manner. The sandbed is well maintained. The Imhoff tank appears to be well operated & maintained.

FJCEl
une 11, 2012
Page 3 of 3
Process control tests of pH, ammonia, alkalinity, oil & grease are performed on the influent and Imhoff tank.
Process control tests appear to be successfully used in measuring plant performance.
Self -Monitoring Program
A review of the monthly self -monitoring reports from April 2011 through February 2012 did not show any limit
violations. However, the following monitoring violations did occur:
Copper
12/31/2011
Pipe 001
Quarterly
Zinc
12/31/2011
Pipe 001
Quarterly
pH
4/30/2011
Pipe 001
2x Month
Temp.
4/9/2011
Pipe 001
Weekly
Temp.
4/16/2011
Pipe 001
Weekly
Temp.
4/23/2011
Pipe 001
Weekly
Temp.
4/30/2011
Pipe 001
Weekly
Grab samples are taken from the end of the pipe 006 at the bank of the river.
The composite sampler at Pipe 001 is time composite at 200 mL every 30 minutes.
The chain -of -custody reports were accurate and in good order.
Mr. Howell continues to perform in an outstanding manner. The compliance evaluation inspection is considered
excellent. If you have any questions please contact George Smith at [phone].
Sincerely,
W. Corey Basinger
Regional Supervisor
cc: WSRO Files

F "r
United States Environmental Protection Agency
Form Approved.
EPA Washington, D.C. 20460
OMB No. 2040-0057
Approval expires 8-31-98
Section A: National Data System Coding (i.e., PCS)
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type
1 INI 2 15 I 31 NC0000019 111 121 12/06/06 117 181 Cl 19I S I 201 I
Remarks
211111111111111111111111111111111111111111 1111 1 11 6
Inspection Work Days Facility Self -Monitoring Evaluation Rating 61 QA —-------------- ---------- Reserved ----------- ----------
67 I 169 70151 71 I DI 721 N I 73 W 74 751 I I I I I Li
Section B: Facility Data
Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include
Entry Time/Date
Permit Effective Date
POTW name and NPDES permit Number)
United Chemi-Con
09:15 AM 12/06/06
12/01/01
Exit Time/Date
Permit Expiration Date
185 McNeil Rd
Lansing NC 28643
11:15 AM 12/06/06
16/03/31
Name(s) of Onsite Representative(s)/Titles(s)/Phone and Fax Number(s)
Other Facility Data
///
Gale Dean Howell/ORC/336-384-6917/
Name, Address of Responsible Official/Title/Phone and Fax Number
Contacted
Gale D Howell,185 McNeil Rd Lansing NC 28643//336-384-6917/
No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit 0 Flow Measurement Operations & Maintenance N Records/Reports
Self -Monitoring Program Facility Site Review Effluent/Receiving Waters
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date
George S Smith WSRO WQ//336-771-5000/
�jZ 0 O
Signature of Management Q A Reviewer Agency/Office/Phone and Fax Numbers Date
EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete.
Page # 1

NPDES yr/mo/day Inspection Type
1
s l NC0000019 1„ 12 1 12/06/06 1 17 , 8 LC
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
Page # 2

Permit: NC0000019
Inspection Date: 06/06/2012
Owner - Facility: United Chemi-Con
Inspection Type: Compliance Evaluation
Operations & Maintenance Yes No NA NE
Is the plant generally clean with acceptable housekeeping? ■ n n n
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable Solids, pH, DO, Sludge ■ n n n
Judge, and other that are applicable?
Comment:
Permit
Yes
No
NA
NO
(If the present permit expires in 6 months or less). Has the permittee submitted a new application?
n
n
■
n
Is the facility as described in the permit?
■
n
n
n
# Are there any special conditions for the permit?
■
n
n
n
Is access to the plant site restricted to the general public?
■
n
n
n
Is the inspector granted access to all areas for inspection?
■
n
n
n
Comment: Acute toxicity episodic conditions
Record Keeping
Yes
No
NA
NE
Are records kept and maintained as required by the permit?
■
n
n
n
Is all required information readily available, complete and current?
■
n
❑
n
Are all records maintained for 3 years (lab. reg. required 5 years)?
■
n
n
n
Are analytical results consistent with data reported on DMRs?
■
n
n
n
Is the chain -of -custody complete?
■
n
n
n
Dates, times and location of sampling
■
Name of individual performing the sampling
■
Results of analysis and calibration
■
Dates of analysis
■
Name of person performing analyses
■
Transported COCs
■
Are DMRs complete: do they include all permit parameters?
■
n
n
n
Has the facility submitted its annual compliance report to users and DWQ?
n
n
■
n
(If the facility is = or > 5 MGD permitted flow) Do they operate 24/7 with a certified operator on each shift?
n
n
■
n
Is the ORC visitation log available and current?
■
Cl
n
n
Is the ORC certified at grade equal to or higher than the facility classification?
■
n
n
n
Is the backup operator certified at one grade less or greater than the facility classification?
■
Cl
n
n
Is a copy of the current NPDES permit available on site?
■
n
n
n
Page # 3

Permit: NC0000019
Inspection Date: 06/06/2012
Owner - Facility: United Chemi-Con
Inspection Type: Compliance Evaluation
Record Keeping
Facility has copy of previous year's Annual Report on file for review?
Comment:
Effluent Pipe
Is right of way to the outfall properly maintained?
Are the receiving water free of foam other than trace amounts and other debris?
If effluent (diffuser pipes are required) are they operating properly?
Comment:
Flow Measurement - Effluent
# Is flow meter used for reporting?
Is flow meter calibrated annually?
Is the flow meter operational?
(If units are separated) Does the chart recorder match the flow meter?
Comment:
Sand Filters (Low rate)
(If pumps are used) Is an audible and visible alarm Present and operational?
Is the distribution box level and watertight?
Is sand filter free of ponding?
Is the sand filter effluent re -circulated at a valid ratio?
# Is the sand filter surface free of algae or excessive vegetation?
# Is the sand filter effluent re -circulated at a valid ratio? (Approximately 3 to 1)
Comment:
C
Yes No NA NE
nn■n
Yes No NA NE
■nnn
■nnn
nn■n
Yes No NA NE
Page # 4

4
Fr NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Charles Wakild, P. E.
Governor Director
March 14, 2012
Yoshi Narita, Vice President of Operations
United Chemi-Con, Inc.
185 McNeil Road
Lansing, NC 28643
Subject: Notice of Violation
United Chemi-Con
NPDES No. NC0000019
Ashe County
Dear Mr. Narita:
Dee Freeman
Secretary
Review of the self -monitoring report for the month of December 2011 revealed the following violation(s):
Monitoring Violation(s)
Parameter
Pipe
Date
Permit Freq.
Values Reported
# of Violations
Copper
001
12/31
Quarterly
0
1
Zinc
001
12/31
Quarterly
0
1
Remedial actions, if not already implemented, should be taken to correct the above noncompliance
problem(s). Please be aware that violations of your NPDES permit could subject you to enforcement action
by this Division with the possible assessment of civil penalties of up to $25,000 per day per violation. Should
you have any questions, please contact me at [phone].
Sincerely,
W. Corey Basinger
Regional Supervisor
cc: WSRO Files
North Carolina Division of Water Quality, Winston-Salem Regional Office
Location: 585 Waughtown St. Winston-Salem, North Carolina 27107
Phone: [phone] FAX: [phone]
Internet: www.ncwaterquality.org
An Equal Opportunity 1 Affirmative Action Employer
Nne
orthCarolina
Nahma!!Y

Cover Sheet from
Staff Member to
Regional Supervisor
DMR Review Record
Facility: JIM-e G Chem; -Ccn Permit/Pipe No.: 1VC 0000D I q Month/Year
Monthly Average Violations
Parameter Permit Limit DMR Value % Over Limit
Date Parameter
Weekly/Daily Violations
Permit Limitjype DMR Value % Over Limit
Monitoring Frequency Violations
Date Parameter Permit Freauencv Values Reported
I 13i GOPPt1' Quirt--ly O
I a 131 Z��►G o
Q 13/ TTO . ri
# of Violations
C (no I1!4; T)
O Su �,. �tr{� A1011,
Other Violations I
FA-.- CIZC jool<J r-or N1crCc1S tn2 �t 51►2
kry-T- 'co S�mP�t
Completed by: �i- Date:
Regional Water Quality
Supervisor SiQnoff: Date:
rk�
%Zacui. 1 y, a o�z
+t rJ k
/air'IS

FV
Beverly Eaves Perdue
Governor
Mr. Butch Howell
United Chemi-Con
185 McNeil Road
Lansing, NC 28643
ALA
WDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Charles Wakild, P. E.
Director
January 4, 2012
Subject: NOTICE OF DEFICIENCY
United Chemi-Con WWTP, Pipe 001
NPDES Permit # NC0000019
Ashe County
Dear Mr. Howell:
Dee Freeman
Secretary
A review of the September 2012 Discharge Monitoring Report (DMR) revealed a monitoring violation of the
following parameter(s) at Outfall 001:
Parameter
Date
Permit Frequency
Values Reported
# of Violations
Flow
Sept.18
Continuous
28
1
Flow
Sept.19
Continuous
28
1
Remedial actions should be taken to correct the cause(s) of this violation. The violations described above
should be abated immediately and properly resolved.
If you have any questions or require any additional information, please contact George Smith at (336) 771-
4968, [e-mail], or myself at [phone], [e-mail].
Sincerely,
W. Corey Basinger
Surface Water Protection Section
cc: WSRO File Copy
North Carolina Division of Water Quality, Winston-Salem Regional Office
Location: 585 Waughtown St. Winston-Salem, North Carolina 27107
Phone: [phone] FAX: [phone]
Internet: www.ncwaterquality.org
An Equal Opportunity 1 Affirmative Action Employer
Nne
orthCarolina
NaturallY

Cover Sheet from
Staff Member to
Regional Supervisor
DMR Review Record
Facility: 1A
PermitTipe No.: M 000001 y Month/Year �Ol k
Monthly Average Violations
Parameter Permit Limit DMR Value
Date Parameter
Weekly/Daily Violations
Permit Lin- li'vpe DMR Value
Monitoring Frequency Violations
% Over Limit
% Over Limit
Date Parameter Perrrit Frequency Values Reported # of Violations
C I }—/,4- ( 6 '-1nuout'
l ` —+
Other Violations
Completed by:
� Date: 1.3
Regional Water Quality <�U✓� Date: Supervisor SiQnoff:
pjms gy1i3
,A16
9'P7 f tr TT °

Frr
Cover Sheet frorn
Staff Member to
Regional Supervisor
MIR Review Record
Facility: Permit/Pipe No.: ,NG00060/9 Month/Year20//
Parameter
Date Parameter
Date
'i 13y
Monthly Average Violations
Permit Limit DMR Value % Over Limit
Weekly/Daily Violations
Permit Limit/TvDe D\R Value 7o Over Limit
Monitoring Frequency Violations
Parameter Permit Frequencv Values Reported # of Violations
7-7-0
7-T (2 (t�OG� A,'r, T- V'e� t I �t d M 0yi i 1,
% (607 /VoZ QrmS
Other Violations
Completed by:Date:
Regional Water Quality 7A l Z
Supervisor Signoff: Date:
l3cr�S

PV
WE
J4/
RPr
r.�
a©l/
TTO (,SAP 30)
2011)
T'r v 31,
2 011)
TTo �J"'«n 301
)o 1/ )
rtTO (MAP, 311
)0/1)
4pr Dig � TT0
TI 4-OVY 0111Qs
T7'U s

Pr
Cover Sheet from
Staff Member to
Regional Supervisor
DNIR Review Record
Facility:y1111a &,ni^Can Permit/Pipe No.: N(-f 00001 `( Monih/Year Twit 20/
Monthly Average Violations
Parameter Permit Limit DMR Value % Over Limit
Weekly/Daily Violations
Date Parameter Permit Llrrtit/Tvpe DMR Value % Over Limit
Monitoring Frequency Violations
Permit Freauencv Values Reported # of Violations
Date Parameter PerAeez VIL A
Ov,l I CR�_ 14Pri'1 0 m R
d 130 7'r� S`ZtrltnL v4lLtr �y
00�,
007 �
Other Violations
JVot' P�gv�rt� N0 V1,014 toA
Iliart� N() VI01,trion
Completed by: Date: 10 b e I t
Regional Water Quality Date: � �� �"
Supers°isor Sianoff: �""`'
Ulm S
tv�

Beverly Eaves Perdue
Governor
44 Y-A
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Coleen H. Sullins
Director
July 22, 2011
Yoshi Narita
Vice President of Operations
United Chemi-Con, Inc.
185 McNeil Road
Lansing, NC 28643
Subject: Notice of Violation
United Chemi-Con
NPDES No. NC0000019
Ashe County
Dear Mr. Narita:
Dee Freeman
Secretary
Review of the self -monitoring report for the month of April 2011 revealed the following violation(s):
Monitoring Violation(s)
Parameter Pipe Date Permit Frea. Values Reported # of Violations
pH
001
4/30
2x / month
0 2
Temp.
001
4/9
Weekly
0 4
Temp.
001
4/16
Weekly
0 4
Temp.
001
4/23
Weekly
0 4
Temp.
001
4/30
Weekly
0 4
Remedial actions, if not already implemented, should be taken to correct the above noncompliance
problem(s). Please be aware that violations of your NPDES permit could subject you to enforcement action
by this Division with the possible assessment of civil penalties of up to $25,000 per day per violation. Should
you have any questions, please contact me at [phone].
Sincerely,
W. Corey Basinger
Regional Supervisor
cc: WSRO Files
North Carolina Division of Water Quality, Winston-Salem Regional Office
Location: 585 Waughtown St. Winston-Salem, North Carolina 27107
Phone: [phone] FAX: [phone] Customer Service:1-877-623-6748
Internet: www.ncwaterquality.org
An Equal Opportunity 1 Affirmative Action Employer
NorthCarohna
NaturallrY

Cover Sheet from
Staff Member to
Regional Supervisor
DMR Review Record
Facility: Ull frej CI, [M: (.on Permit/Pipe No.: VC 600001 y Month/Year Liz Zv r /
Monthly Avera;e Violations
Parameter Permit Limit DMR Value % Over Limit
Weekly/Daily Violations
Date Parameter Permit Lbm avDe DMR Value % Over Limit
Monitorin- Frequency Violations
Date Parameter �� Pen-ni Frequency Values Reported # of Violations
130 -P-H 001 _ ZX_ Mons{_ b 2-_ �I�M�T)
y lit Tan
i /11 TcrnP
H
1.3 Tzn0
y /30 'T,,l
Other Violations
I
O
PIr<S b0� o
007 wile nee vt1(Z70i1S hor I',)13/►"IS
Completed by: c Date: 7 lz /
Regional Water Quality c 21 JJ4, -10o
Supervisor Sienoff: Date:
gin S
7�,tT�/i

Ashe
NC0000019 United Chenni-Con, Inc.
Monitorina Violation
Standard
Frequency
Units, i.e.,
Violation
2011
4
001
pH
04-30-2011
2 X month
Ph
Frequency
Temperature, Water
Degrees
Violation
2011
4
001
Deg. Centigrade
04-09-2011
Weekly
Centigrade
Frequency
Temperature, Water
Degrees
Violation
2011
4
001
Deg. Centigrade
04-16-2011
Weekly
Centigrade
Frequency
Temperature, Water
Degrees
Violation
2011
4
001
Deg. Centigrade
04-23-2011
Weekly
Centigrade
Frequency
Temperature, Water
Degrees
Violation
2011
4
001
Deg, Centigrade
04-30-2011
Weekly
Centigrade
Standard
Frequency
Units, i.e.,
Violation
2011
4
006
pH
04-30-2011
2 X month
Ph
Frequency
Temperature, Water
Degrees
Violation
2011
4
006
Deg, Centigrade
04-09-2011
Weekly
Centigrade
Frequency
Temperature, Water
Degrees
Violation
2011
4
006
Deg. Centigrade
04-16-2011
Weekly
Centigrade
Frequency
Temperature, Water
Degrees
Violation
2011
4
006
Deg. Centigrade
04-23-2011
Weekly
Centigrade
Frequency
Temperature, Water
Degrees
Violation
2011
4
006
Deg, Centigrade
04-30-2011
Weekly
Centigrade
Standard
Frequency
Units, i.e.,
Violation
2011
4
007
pH
04-30-2011
2 X month
Ph
Frequency
Temperature, Water
Degrees
Violation
2011
4
007
Deg. Centigrade
04-09-2011
Weekly
Centigrade
Frequency
Temperature, Water
Degrees
Violation
2011
4
007
Deg, Centigrade
04-16-2011
Weekly
Centigrade
Frequency
Temperature, Water
Degrees
Violation
2011
4
007
Deg. Centigrade
04-23-2011
Weekly
Centigrade
Frequency
Temperature, Water
Degrees
Violation
2011
4
007
Deg. Centigrade
04-30-2011
Weekly
Centigrade
00 (1o t Stow (✓1 a l m's
J h�ic tY�G I)OT vlvltvlo✓1 S.

RECEIVED
N.C. DeDt. of ENF
JUN 17 2011
Winston-Salem
185 McNeil Road. Lansing, NC 28643-8300 • Phone [phone] • Fax 336,384.6928 • http:l/www chemi-roo i°''aI ``
UNITED CHEMI-CON, INC.
June 14, 2011
W. Corey Basinger
North Carolina Department of Environment and Natural Resources
Division of Water Quality
585 Waughtown Street
Winston-Salem, NC 27107
Dear Ms. Basinger:
Please reference your letter dated June 7, 2011 regarding the compliance evaluation inspection
conducted at this facility on June 2, 2011. Specifically, your concern regarding the "... stream of
foam..." being discharged from Outfall 001 during Mr. George Smith's inspection.
As per Mr. Smith's request, an immediate investigation was conducted to determine the
excessive foam mentioned above. This investigation was inconclusive, but revealed the probable
source of the foam to be from the cleaning of air conditioning coils on the roof of our facility.
As the coils were being cleaned, the detergent was washed into the rainwater collection system
and carried to Outfall 001, causing the excessive foaming.
The material being used was Hydro Balance Non -Acid Hydro-Kleen Concentrate, and was being
used in accordance with instructions on the container.
Should more action be required, please feel free to contact me.
4�_
G.D. Butch Howell
Environmental/Safety Manager

PV
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins
Governor Director
June 20, 2011
Yoshi Narita
Vice President of Operations
United Chemi-Con, Inc.
185 McNeil Road
Lansing, NC 28643
Subject: Notice of Violation
United Chemi-Con
NPDES No. NC0000019
Ashe County
Dear Mr. Narita:
Dee Freeman
Secretary
Review of the self -monitoring report for the month of March 2011 revealed the following violation(s):
Monitorine Violation(s)
Parameter Pipe Date Permit Freg. Values Reported # of Violations
Copper 001 3/31 Quarterly 0
Temp. 001 3/5 Weekly 0
Temp. 006 3/5 Quarterly 0
Remedial actions, if not already implemented, should be taken to correct the above noncompliance
problem(s). Please be aware that violations of your NPDES permit could subject you to enforcement action
by this Division with the possible assessment of civil penalties of up to $25,000 per day per violation. Should
you have any questions, please contact me at [phone].
Sincerely,
J&All�&044y—
W. Corey Basinger
Interim Regional Supervisor
cc: WSRO Files
North Carolina Division of Water Quality, Winston-Salem Regional Office
Location: 585 Waughtown St. Winston-Salem, North Carolina 27107
Phone: [phone] FAX: [phone] Customer Service:1-877-623-6748
Internet: www,ncwaterquality.org
NorthCarolina
Aaturally
An Equal Opportunity 1 Affirmative Action Employer

Cover Sheet from
Staff Member to
Regional Supervisor
DMR Review Record
Facility:
Cl� ' C Permit/Pipe No.: AlC000Dol� Month/Year
�n�r� �,- oh
Monthly Avera-e Violations
Parameter Permit Limit DMR Value % Over Limit
Weekly/Daily Violations
Date
Parameter Permit Limit/Tvpe DMR Value
% Over Limit
Monitoring- Frequency Violations
Date
Parameter Permit Frequencv Values Reported
# of Violations �vv
3 -3 i
G'o i°P<r p, c.00 Q�ar�e,-ly _Ov
a
3- S'
I -_A p (PP{ Wee-kI
O
�
3 -S
T—M P l PIP. C>ed
QthipViolations ,� FsYo^ QtMs C'Q(cvlc�r
h�.e,.
,�„ _ ► �,., (PcPorT<� oh ��& OmQ 1 TrU
✓<rorZ sv6�i�E<cl/
_
Pi D - TTD CELLFlow - tio Flow r<✓ofl-i
�IPti DD' — C 1 TV poi ✓{ v�iti in Pzr,n%t Flow L- T-<#nP low✓'cYo��<�
l 9 nerti
Completed by: Vim' `-�'"�„/`�, Date: G /t 3 12 ot/
Regional Water Quality n Date: 3 �f
Supervisor Signoff: t S
ctxd if

V
Mickey, Mike
From: Smith, George
Sent: Tuesday, June 14, 2011 3:31 PM
To: Mickey, Mike
Subject: FW: United ChemiCon
Mike,
Why is this new format showing a violation for TTO and Copper? Charles says BIMS does not show it for outfalls 006 and
007.
George Smith
New email: [e-mail]
NC DENR Winston-Salem Regional Office
Division of Water Quality, Water Quality Section
585 Waughtown Street
Winston-Salem, NC 27107
Voice: [phone]
FAX: [phone]
E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be
disclosed to third parties.
From: Weaver, Charles
Sent: Tuesday, June 14, 2011 9:55 AM
To: Smith, George
Subject: RE: United ChemiCon
George — the recent TTO and Copper violations are for outfall 001, not 006 or 007.
I checked BIMS just now — neither 006 nor 007 ask for TTO or Copper.
CHW
From: Smith, George
Sent: Tuesday, June 14, 2011 7:20 AM
To: Weaver, Charles
Subject: United ChemiCon
Charles,

United ChemiCon NC0000019 in Ashe county has some monitoring violations in the March DMR that are permit related
and need to be fixed:
Pipe 006; Copper and TTO are not required. BIMS sees this as a permit violation
Pipe 007; Copper and TTO are not required. RIMS sees this as a permit violation
Thanks for your help in this matter.
George
Ps Of course, you could give me your password and I can use the Maintain Button as many times as I want?
George Smith
New email: [e-mail]
NC DENR Winston-Salem Regional Office
Division of Water Quality, Water Quality Section
585 Waughtown Street
Winston-Salem, NC 27107
Voice: [phone]
FAX: [phone]
E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be
disclosed to third parties.

Ashe
NC00OOO19
Monitoring Violation
United Chemi-Con, Inc.
Frequency
Milligrams
Violation
2011
3
001
Copper, Total (as Cu)
03-31-2011
Quarterly
per Liter
Million
Frequency
Flow, in conduit or thru
Gallons per
Violation
2011
3
001
treatment plant
03-05-2011
Weekly
Day
Frequency
Organics, Total Toxic
Milligrams
Violation
2011
3
001
(TTO)
03-31-2011
Quarterly
per Liter
Frequency
Temperature, Water
Degrees
Violation
2011
3
001
Deg. Centigrade
03-05-2011
Weekly
Centigrade
Frequency
�—
Milligrams
Violation
2011
3
006
Copper, Total (as Cu)
03-31-2011
Quarterly
per Liter
Million
Frequency
Flow, in conduit or thru
Gallons per
Violation
2011
3
006
treatment plant
03-05-2011
Weekly
Day
Frequency
Organics, Total Toxic
Milligrams
Violation
2011
3
006
(TTO)
03-31-2011
Quarterly
per Liter
Frequency
Temperature, Water
Degrees
Violation
2011
3
006
Deg. Centigrade
03-05-2011
Weekly
Centigrade
Frequency
Milligrams
Violation
2011
3
007
Copper, Total (as Cu)
03-31-2011
Quarterly
per Liter
Million
Frequency
Flow, in conduit or thru
Gallons per
Violation
2011
3
007
treatment plant
03-05-2011
Weekly
Day
Frequency
Organics, Total Toxic
Milligrams
Violation
2011
3
007
(TTO)
03-31-2011
Quarterly
per Liter
Frequency
Temperature, Water
Degrees
Violation
2011
3
007
Deg. Centigrade
03-05-2011
Weekly
Centigrade
ioftarooC�)
I►a� n�`��►
Na
via*C-M
kD i►lolation
viol" rlo",
V10I t tro>•G!J
�D Fle tv
/ro r 101v
/Vo (`tuw'

Beverly Eaves Perdue
Governor
Mr. Butch Howell
United Chemi-Con
185 McNeil Road
Lansing, NC 28643
LPKWA
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Coleen H. Sullins
Director
SUBJECT:
Dear Mr. Howell:
June 7, 2011
Compliance Evaluation Inspection (CEI)
United Chemi-Con WWTP
NPDES Permit # NC0000019
Ashe County
Dee Freeman
Secretary
On June 2, 2011 George Smith performed a Compliance Evaluation Inspection. Mr. Gale D. Howell, ORC,
Grade IV, was present for the inspection. Mr. Allan Miller is currently training as a Back-up operator. The
inspection is comprised of an overall evaluation in order to document compliance and noncompliance of:
facilities equipment, capability to meet effluent limits, and NPDES permit terms & conditions.
Permit
Your NPDES permit became effective on January 1, 2007 and expires on March 31, 2011. This permit is
currently effective until the new permit is issued.
The permit identifies the following discharge pipes:
(001) Non -contact cooling water, A/C condensate, boiler blow -down, de -ionizer backwash, assembled product
wash water & process wastewater.
(003) A/C condensate.
(006) Domestic wastewater.
(007) Recycled non -contact cooling water, and filtered surface water during maintenance periods only.
Records & Reports
Mr. Howell maintains a log. Mr. Howell documents phone conversations, calibrations, process control, and all
are done in an excellent manner.
Facility Site Review
The effluent from the Imhoff tank was clear with no visible solids.
North Carolina Division of Water Quality, Winston-Salem Regional Office
Location: 585 Waughtown St. Winston-Salem, North Carolina 27107
Phone: [phone] FAX: [phone] Customer Service:1-877.623-6748
Internet www.ncwaterqual4.org
An Equal Opportunity 1 Affirmative Action Employer
One
NorthCarolina
Naturally

CEI
June 7, 2011
Page 2 of 3
The sandfilters were raked and appeared to be clean and in good condition. There was no evidence of ponding
on the surface of the sandfilters.
The dosing lines and concrete pads are intact.
Flow Measurement
The instantaneous flow at Outfall 006 is obtained by measuring the height of the water in a 1-inch parshall
flume then converting it to flow (MGD).
The Stevens, Model 61R flow meter at Outfall 001 was calibrated by B.W. Allen on March 23, 2011.
Laboratory
Mr. Howell performs pH and Temperature; and these tests are recorded on the daily monitoring report.
A field certification for pH and Temperature was issued to Mr. Butch Howell for United Chemi-Con (lab
#5099). All remaining tests are performed by TriTest (Certified Lab #103).
Calibration for pH is performed using Fisher standards of pH 4, 7, 10.
The temperature is recorded against a NIST traceable thermometer.
Effluent/Receiving Waters
The effluent from Pipe 001 to the North Fork New River, Class C + waters of the State showed a continuous
stream of foam entering the river and then dissipated. There are no obvious impacts. The permit requires that no
visible foam should be discharged other than trace amounts.
The effluent from Pipe 006 to the North Fork New River, Class C + waters of the State was clear, no color, no
solids, or no odor.
The effluent from pipes 001, 003, 006, and 007 do not impact the North Fork New River.
Effluent pipes 003 and 007 were not discharging.
Operations & Maintenance
Mr. Butch Howell, Grade IV is the current ORC. The back-up operator is Mr. Allan Miller is in training.
The facility (pipe 006) with the Imhoff tank is considered a Class II facility.

CEI
June 7, 2011
Page 3 of 3
The facility was well maintained by the staff, and they are considered to perform their jobs in an outstanding
manner. The sandbed is well maintained. The Imhoff tank appears to be well operated & maintained.
Process control tests of pH, ammonia, alkalinity, oil & grease are performed on the influent and Imhoff tank.
Process control tests appear to be successfully used in measuring plant performance.
Self -Monitoring Pro ram
A review of the monthly self -monitoring reports from April 2010 through February 2011 did not show any limit
violations.
Please note that monitoring must be performed according to the permit except for weekends and State holidays.
(please see attached memo)
Grab samples are taken from the end of the pipe 006 at the bank of the river.
The composite sampler at Pipe 001 is time composite at 200 mL every 30 minutes.
The chain -of -custody reports were accurate and in good order.
Action Item(s)
During the previous report it was noted that process wastewater was hauled away from the site. During the
inspection of Outfall 001 a continuous stream of foam was discharged to the river and then dissipated. There are
no obvious impacts to the river. Your permit does allow the discharge of assembled product wash water and
process wastewater. Please investigateprocess water that is discharged from Outfal1001, and the pollutants
that are present and provide a resort to this office. Please respond to this office, in writing, in ten (10) days of
receipt of this letter.
Mr. Howell continues to perform in an outstanding manner. The compliance evaluation inspection is considered
excellent. If you have any questions please contact George Smith at [phone].
Sincerely,
W. Corey Basinger
Regional Supervisor
cc: WSRO Files

rr_
United States Environmental Protection Agency
Form Approved.
EPA Washington, D.C. 20460
OMB No. 2040-0057
Water Compliance Inspection Report
Approval expires 8-31-98
Section A: National Data System Coding (i.e., PCS)
Transaction Code NPDES ydmo/day Inspection Type Inspector Fac Type
1 INI 2 I5! 31 NC0000019 11 121 11/06/02 117 18)r' 191SI 201 I
J L!
Remarks
21I111IIIIIIIIIIIIIIIII11111111111111111111111lU1
Inspection Work Days Facility Self -Monitoring Evaluation Rating B1 CIA ---------Reserved-------
67 I 169 70141 711 DI 72 i N i 73 W 74 751 I I I I I I 180
�--
Section B: Facility Data
Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include
Entry Time/Date
Permit Effective Date
POTW name and NPDES permit Number)
United Chemi-Con, Inc.
10.16 AM 11/06/02
07/01/01
Exit Time/Date
Permit Expiration Date
185 McNeil Rd
Lansing NC 28643
11.10 AM 11/06/02
11/03/31
Name(s) of Onsite Representative(s)lTitles(s)/Phone and Fax Number(s)
Other Facility Data
Gale Dean Howell/ORC/336-384-6917/
Name, Address of Responsible Official[Title/Phone and Fax Number
Contacted
Gale D Howell,185 McNeil Rd Lansing NC 28643//336-384-6917/ No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit Flow Measurement Operations & Maintenance Records/Reports
Self -Monitoring Program Facility Site Review Effluent/Receiving Waters Laboratory
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date
George S Smith WSRO WQ//336-771-5000/
Signature of Management Q A Reviewer Agency/Office/Phone and Fax Numbers Date
A!;OOLPL - i ti/cn- GL QUO Jt/W ?-r/l
EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete.
Page # 1

NPDES yr/mo/day Inspection Type 1
3I 11 12I 11/06/02 117 181 ^I
NC0000019 I
Section D: Summary of 1Finding/Comments (Attach additional) sJheets of narrative and checklists as necessary)
Page # 2

Permit: NC0000019 Owner - Facility: United Chemi-Con, Inc.
Inspection Date: 06/02/2011 Inspection Type: Compliance Evaluation
Operations & Maintenance Yes No NA NE
Is the plant generally clean with acceptable housekeeping? ■ ❑ ❑ ❑
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable Solids, pH, DO, Sludge ■ (_1 ❑ ❑
Judge, and other that are applicable?
Comment: Alkalinity at imhoff tank.
Permit
Yes No
NA
NE
(If the present permit expires in 6 months or less). Has the permittee submitted a new application?
■ ❑
n
❑
Is the facility as described in the permit?
■ ❑
❑
❑
# Are there any special conditions for the permit?
❑ ■
❑
❑
Is access to the plant site restricted to the general public?
■ ❑
❑
❑
Is the inspector granted access to all areas for inspection?
■ ❑
❑
❑
Comment:
Record Keeping
Yes
No
NA
NE
Are records kept and maintained as required by the permit?
■
❑
❑
❑
Is all required information readily available, complete and current?
■
❑
❑
❑
Are all records maintained for 3 years (lab. reg. required 5 years)?
■
❑
❑
❑
Are analytical results consistent with data reported on DMRs?
■
Cl
❑
❑
Is the chain -of -custody complete?
■
❑
❑
❑
Dates, times and location of sampling
■
Name of individual performing the sampling
■
Results of analysis and calibration
■
Dates of analysis
■
Name of person performing analyses
■
Transported COCs
■
Are DMRs complete: do they include all permit parameters?
■
❑
❑
❑
Has the facility submitted its annual compliance report to users and DWQ?
❑
❑
■
❑
(If the facility is = or > 5 MGD permitted flow) Do they operate 24/7 with a certified operator on each shift?
❑
❑
■
Cl
Is the ORC visitation log available and current?
■
❑
❑
❑
Is the ORC certified at grade equal to or higher than the facility classification?
■
❑
❑
❑
Is the backup operator certified at one grade less or greater than the facility classification?
❑
■
❑
❑
Is a copy of the current NPDES permit available on site?
■
❑
❑
❑
Page # 3

Permit: NC0000019 Owner - Facility: United Chemi-Con, Inc.
Inspection Date: 06/02/2011 Inspection Type: Compliance Evaluation
Record Keeping Yes No NA NE
Facility has copy of previous year's Annual Report on file for review? ❑ ❑ 0 0
Comment: Allan Miller is training for back-up
Sand Filters (Low rate)
(if pumps are used) Is an audible and visible alarm Present and operational?
Is the distribution box level and watertight?
Is sand filter free of ponding?
Is the sand filter effluent re -circulated at a valid ratio?
# Is the sand filter surface free of algae or excessive vegetation?
# Is the sand filter effluent re -circulated at a valid ratio? (Approximately 3 to 1)
Comment:
Page # 4

NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins
Governor Director
March 14, 2011
Yoshi Narita
Vice President of Operations
United Chemi-Con Inc.
185 McNeil Road
Lansing, NC 28643
Subject: Notice of Violation
United Chemi-Con
NPDES No. NC0000019 — Outfall 001
Ashe County
Dear Mr. Narita:
Dee Freeman
Secretary
Review of the self -monitoring report for the month of December 2010 revealed the following violation(s):
Monitoring Violation(s)
Parameter
Date
Permit Freq.
Values Reported
# of Violations
Total Toxic Organics'
12/31
Quarterly
0
1
1. In lieu of monitoring for Total Toxic Organics, the permittee may submit the following statement: "Based on my
inquiry of the person or persons directly responsible for managing compliance with the permit limitation for
total toxic organics, I certify that, to the best of my knowledge and belief, no dumping of concentrated toxic
organics into the wastewater has occurred since the filing of the last discharge report."
Remedial actions, if not already implemented, should be taken to correct the above noncompliance
problem(s). Please be aware that violations of your NPDES permit could subject you to enforcement action
by this Division with the possible assessment of civil penalties of up to $25,000 per day per violation. Should
you have any questions, please contact me at [phone].
Sincerely,
W. Corey Basinger
Interim Regional Supervisor
cc: WSRO Files
North Carolina Division of Water Quality, Winston-Salem Regional Office
Location: 585 Waughtown St. Winston-Salem, North Carolina 27107
Phone: [phone] FAX: [phone] Customer Service: 1-877-623-6748
Internet: www.ncwaterquality.org
An Equal Opportunity 1 Affirmative Action Employer
NorthCarolina
Naturally

Cover Sheet from
Staff Member to
Regional Supervisor
DMR Review Record
Facility: Onice the '- eon PermitlPipe No.: NP.©Dbpol y Month/Year c a010
�c ool
Monthly Average Violations
Parameter Permit Limit DMR Value % Over Limit
Weekly/Daily Violations
Date Parameter Permit LirnitlI'vpe DMR Value % Over Limit
Monitoring Frequency Violations
Date Parameter Permit Frequencv Values Reported # of Violations
Q-31 Tbzul
Other) Violations
/v © � ,� .� f m� n GS take ✓I -
Completed by: -�� a`'� Date: 3 - 1D - 1
Regional Water Quality �> Date:
Supervisor SiQnoff:
j6-V

�74 �XO� RECEIVED
N.C. ^-
�"�—' ocr a LA"
z zoo
W Win-
NCDENR
North Carolina Department of Environment and Natural Resources R giona, :r
Division of Water Quality -
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
October 5, 2010
YOSHI NARITA
VICE PRESIDENT OF OPERATIONS
UNITED CHEMI-CON INC
185 MCNEIL ROAD
LANSING NC 28643
Subject: Receipt of permit renewal application
NPDES Permit NC0000019
United Chemi-Con, Inc.
Ashe County
Dear Mr. Narita:
The NPDES Unit received your permit renewal application on October 4, 2010. A member of the NPDES
Unit will review your application. They will contact you if additional information is required to complete your
permit renewal. You should expect to receive a draft permit approximately 30-45 days before your existing permit
expires.
If you have any additional questions concerning renewal of the subject permit, please contact Jeff Poupart at
[phone].
Sincerely,
Dina Sprinkle
Point Source Branch
cc: CENTRAL FILES
Winston-Salem Regional Office/Surface Water Protection
NPDES Unit
1617 Mail Service Center, Rale�h, North Carolina 27699-1617
Location: 512 N. Salisbury St. Raleigh, North Carolina 27604
Phone: [phone] \ FAX: [phone] i Customer Service:1-877-623-6748
Internet: www.ncwaterquality.org
One
NorthCarolna
An Equal Opportunity 1 Affirmative Action Employer

NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial
Minor industrial, manufacturing and commercial facilities.
Mail the complete application to:
N. C. Department of Environment and Natural Resources
Division of Water Quality / NPDES Unit
1617 Mail Service Center, Raleigh, NC 27699-1617
NPDES Permit Number INCO000019
Please print or type.
1. Contact Information:
Owner Name Yoshi Narita
Facility Name United Chemi-Con, Inc
Mailing Address 185 McNeil Rd
City Lansing
State / Zip Code NC 28643
Telephone Number 336-384-2551
Fax Number 336-384-6930
e-mail Address [e-mail]
2. Location of facility producing discharge:
Check here if same as above xxx❑
RD
�IJJ�Ijj D
Street Address or State Road same
O C T 42010
LeN
City
R
State / Zip Code
.-AT
POINT SOURCE BRANCH
County
3. Operator Information:
Name of the firm, consultant or other entity that operates the facility. (Note that this is not referring to the
Operator in Responsible Charge or ORC)
Name
Mailing Address
City
State / Zip Code
Telephone Number
Fax Number
4. Ownership Status:
Federal ❑ State ❑ Private xx❑ Public ❑
Page 1 of 5 C-MI 10/08

NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial
Minor industrial, manufacturing and commercial facilities.
5. Standard Industrial Classification (SIC) code(s): 3675
6. Number of employees:325
7. Describe the treatment system List all installed waste treatment components with capacities,
describe the processes that generate wastewaters. If the space provided is not sufficient attach a
separate sheet of paper with the system description.
-noncontact cooling water, A/C condensate, boiler blow down, deionizer backwash,
assembled product wash water and process wastewater from outfall 001; A/C condensate
from outfall 003; domestic wastewater from outfall 006; non -contact cooling water and
filtered surface water (during maintenance periods only) from outfall 007
8. Is facility covered under federal effluent limitation guidelines? No xx❑ Yes ❑
If yes, specify the category?
9. Principal product(s) produced: aluminum electrolytic capacitors
Principal raw material(s) consumed: aluminum foil, ethylene glycol
Briefly describe the manufacturing process(es):
master aluminum foil rolls are slit into widths consistant with various design specs, then rolled
into coil with seperator paper between anode and cathode aluminum sheets. the coiled units are then
impregnated with propriety electrolyte(s) consisting of either a ethylene glycol base or a
gammabutrolactone base. the units are then assembled into an an aluminum can with a phenolic
cover assembly.
Page 2 of 5 C-MI 10/08

NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial
Minor industrial, manufacturing and commercial facilities.
10. Amount of principal product produced or raw material consumed
ir.,-t cnarifir• mmmrntc rnncumed and/or units of production over the last three nears)
Product Produced or Raw Material
Consumed
AVERAGE
Product Produced or Raw Material
Consumed
PEAK
per Day
60569 capacitors
77703 capacitors
per Month
1211383 capacitors
1554066 capacitors
per Year
14536600 capacitors
18648800 capacitors
11. Frequency of discharge: Continuous ❑
If intermittent:
Days per week discharge occurs: 6
Intermittent xx❑
Duration: 24/ hrs/ day
12. Types of wastewater discharged to surface waters only
Discharge
Flow
GALLONS PER DAY
Sanitary - monthly average
400
Utility water, etc. - monthly average
1000
Process water - monthly average
127,000
Stormwater - monthly average
6993
Other - monthly average
Explain:
0
Monthly Average
total discharge (all types)
135,000
13. Number of separate discharge points: 4 Outfall Identification number(s)
001,003,006,007_
14. Name of receiving stream(s) (Provide a map shouring the exact location of each outfall, including
latitude and longituderNorth Fork of New River
latitude/longitude 36.2847 81.3019
Page 3 of 5 C-MI 10/08

NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial
Minor industrial, manufacturing and commercial facilities.
15. Effluent Data [for new or proposed discharges]
Provide data for the parameters listed. Temperature and pH shall be grab samples, for all other parameters 24-hour
composite sampling shall be used. If more than one analysis is reported, report daily maximum and monthly average.
If only one analysis is reported, report as daily maximum.
NOTE: Permittees requesting renewal should complete the table ONLY for the parameters
currentli/ menitorPd_ A1'1Mm.7r47o tha V%. + _2 ..e.,r..� _r e0s7.. -4 .4-4-
Parameter
Daily
Maximum
Monthly
Average
Units of
Measurement
Biochemical Oxygen Demand (BOD5)
21.2
0.59
mg/1
Chemical Oxygen Demand (COD)
Total Organic Carbon
Total Suspended Solids
21.0
3.5
mg/1
Ammonia as N
Temperature (Summer)
34.31
31.62
degrees centigrade
Temperature (Winter)
29.44
27.52
degrees centigrade
pH
8.8
7.96
standard units
Fecal Coliform (If sanitary waste is
present)
Total Residual Chlorine (if chlorine is
used)
16. List all permits, construction approvals and/or applications (check all that apply and provide permit
numbers or check none if not applicable). -
Type Permit Number Type Permit Number
Hazardous Waste (RCRA) NCD336771500 NESHAPS (CAA)
UIC (SDWA) none
NPDES NC0000019
PSD (CAA) none
Non -attainment program (CAA) none
none
Ocean Dumping (MPRSA) none
Dredge or fill (Section 404 or CWA) none
Other
none
17. List any chemicals that may be discharged (Please list and explain source and potential
amounts.)
ethylene glycol - formulation component
gammabutralactone - formulation component
Page 4 of 5 C-MI 10/08

NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial
Minor industrial, manufacturing and commercial facilities.
18. Is this facility located on Indian country? (check one)
Yes ❑ No xx ❑
19. Applicant Certification
I certify that I am familiar with the information contained in the application and that to the
best of my knowledge and belief such information is true, complete, and accurate.
Yoshi Narita Vice President of Operations
Printed name of Person Signing Title
of Applicant
Date
North Carolina General Statute 143-215.6 (b)(2) provides that: Any person who knowingly makes any false
statement representation, or certification in any application, record, report, plan, or other document files or
required to be maintained under Article 21 or regulations of the Environmental Management Commission
implementing that Article, or who falsifies, tampers with, or knowingly renders inaccurate any recording or
monitoring device or method required to be operated or maintained under Article 21 or regulations of the
Environmental Management Commission implementing that Article, shall be guilty of a misdemeanor punishable
by a fine not to exceed $25,000, or by imprisonment not to exceed six months, or by both. (18 U.S.C. Section
1001 provides a punishment by a fine of not more than $25,000 or imprisonment not more than 5 years, or both,
for a similar offense.)
Page 5 of 5 C-MI 10108

0
0 Page 1 of 4
T .NEST
Laboratory Report
Lab Location R' Lab Location 'C' Lab Location 'W
NCMNV Cert.#: 067 NC/DW Cert.#: 37731 NC/WW Cert.#: 103 NC/DW Cert.#: 37733 NC/WW Cert.#: 075 NC/DW Cert.#: 37721
6701 Conference Dr, Raleigh, NC 27607 6300 Ramada Dr, Suite C2, Clemmons, NC 27012 6624 Gordon Rd, Unit G, Wilmington, NC 28411
Ph: [phone] Fax: [phone] Ph: [phone] Fax: [phone] Ph: [phone] Fax: [phone]
Project No.: Report Date: 9/27/2010
Project ID: OUTFALL #001; PPA Date Received: 9/14/2010
-- Prepared for --
Butch Howell
UNITED CHEMI-CON
185 MCNEIL RD.
LANSING, NC 28643
Work Order* 1009-00882
Cust. Code: 800205
Cust. P.O.#:
No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition
001 OUTFALL #001 9/14/2010 8:00 WW Composite 4 +/- 2 deg C
Test Performed Method Results Lab Loc DaieyZed Time Qualifier
Ammonia
SM 4500 NH3 F
0.1 mg/L as N
C
9/21/10
9:30
Total Phosphorus
SM 4500 P E
0.03 mg/L
C
9124110
9:00
Total Kjeldahl Nitrogen
EPA 351.2
<0.25 mg/L
R
9/22/10
13:15
Nitrate -Nitrite
EPA 353.2
0.38 mg/L as N
R
9121/10
10:57
Total Nitrogen Calculation
CALCULATION
0.38 mg/L
R
9122/10
13:16
Total Dissolved Solids
SM 2540C
38 mg/L
C
9116110
9:00
Antimony
EPA 200.8
<0.003 mg/L
R
9117110
14:48
Arsenic
EPA 200.8
<0.005 mg/L
R
9117/10
14:48
Beryllium
EPA 200.8
<0.002 mg/L
R
9/17/10
14:48
Cadmium
EPA 200.8
<0.005 mg/L
R
9/17110
14:48
Chromium
EPA 200.8
<0.010 mg/L
R
9/17110
14:48
Copper
EPA 200.8
0.010 mg/L
R
9/17/10
14:48
EPA 200.8
<0.005 mg/L
R
9117/10
14:48
Nickel
EPA 200.8
<0.010 mg/L
R
9117/10
14:48
Selenium
EPA 200.8
<0.002 mg/L
R
9/17/10
14:48
Silver
EPA 200.8
<0.010 mg/L
R
9/17/10
14:48
Thallium
EPA 200.8
<0.001 mg/L
R
9/17/10
14:48
Zinc
EPA 200.8
<0.010 mg/L
R
9/17/10
14:48
TOTAL HARDNESS (WW)
R
0:00
Calcium
EPA 200.8
10.3 mg/L
R
9122110
10:42
Magnesium
EPA 200.8
1.96 mg/L
R
9/22/10
10:42
Total Hardness Calculation
CALC.
33.8 mg/L
R
9/22/10
10:42
No. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition
002 OUTFALL #001 9/14/2010 8:00 WW Grab 4 +/- 2 deg C
-- -- /final zed -
Test Performed Method Results Lab Loc atey Time Qualifier
Oil & Grease
EPA 1664A <5.0 mg/L
R
9/20/10
12:00
Cyanide
WC10-204-00-14 <0.005 mg/L
R
9/17/10
11:20
Phenols
EPA 420.4 11.0 ug/L
R
9/17/10
8:47
VOCs by 624
EPA 624
R
9/16/10
8:05

Telephone: [phone]
Fax: [phone]
No. Sample ID
002 OUTFALL #001
0
0
UGsOUTEST
6701 Conference Drive
Raleigh, NC 27607
Telephone: [phone]
Fax: [phone]
Laboratory Report
Work Order #: 1009-00882
Page 2 of 4
NC/WW Cert. #: 067
NC/DW Cert. #: 37731
11
Date Sampled Time Sampled Matrix Sample Type Condition
9/14/2010 8:00 WW Grab 4 +/- 2 deg C
finl --,
Test Performed Method Results Lab Loc---- Daaed te Time Qualifier
Benzene
EPA 624
<5 ug/L
R
9/16/10
8:05
Acrolein
EPA 624
<50 ug/L
R
9116/10
8:05
Acrylonitrile
EPA 624
<50 ug/L
R
9/16110
8:05
Bromodichloromethane
EPA 624
<5 ug/L
R
9/16/10
8:05
Bromoform
EPA 624
<5 ug/L
R
9/16110
8:05
Bromomethane
EPA 624
<10 ug/L
R
9/16/10
8:05
Dibromomethane
EPA 624
<2 ug/L
R
9/16/10
8:05
Carbon tetrachloride
EPA 624
<5 ug/L
R
9/16/10
8:05
Chlorobenzene
EPA 624
<5 ug/L
R
9/16/10
8:05
Chloroethane
EPA 624
<5 ug/L
R
9/16/10
8:05
2-Chloroethylvinyl ether
EPA 624
<10 ug/L
R
9116/10
8:05
Chloroform
EPA 624
<5 ug/L
R
9116/10
8:05
Chloromethane
EPA 624
<5 ug/L
R
9/16/10
8:05
Dibromochloromethane
EPA 624
<5 ug/L
R
9/16/10
8:05
1,2-Dichlorobenzene
EPA 624
<5 ug/L
R
9/16110
8:05
1,3-Dichlorobenzene
EPA 624
<5 ug/L
R
9/16/10
8:05
1,4-Dichlorobenzene
EPA 624
<5 ug/L
R
9/16/10
8:05
1,1-Dichloroethane
EPA 624
<5 ug/L
R
9/16/10
8:05
1,2-Dichloroethane
EPA 624
<5 ug/L
R
9/16/10
8:05
1,1-Dichloroethene
EPA 624
<5 ug/L
R
9116/10
8:05
trans-1,2-Dichloroethene
EPA 624
<5 ug/L
R
9/16/19
8.06
1,2-Dichloropropane
EPA 624
<5 ug/L
R
9/16/10
8:05
cis-1,3-Dichloropropene
EPA 624
<5 ug/L
R
9/16/10
8:05
trans-1,3-Dichloropropene
EPA 624
<5 ug/L
R
9/16110
8:05
Ethylbenzene
EPA 624
<5 ug/L
R
9/16/10
8:05
Methylene chloride
EPA 624
<5 ug/L
R
9/16110
8:05
1,1,2,2-Tetrachloroethane
EPA 624
<5 ug/L
R
9/16/10
8:05
Tetrachloroethene
EPA 624
<5 ug/L
R
9/16110
8:05
Toluene
EPA 624
<5 ug/L
R
9/16/10
8:05
1,1,1-Trichloroethane
EPA 624
<10 ug/L
R
9/16/10
8:05
1,1,2-Trichloroethane
EPA 624
<5 ug/L
R
9/16/10
8:05
Trichloroethene
EPA 624
<5 ug/L
R
9/16/10
8:05
Trichlorofluoromethane
EPA 624
<5 ug/L
R
9/16/10
8:05
Vinyl chloride
EPA 624
<5 ug/L
R
9/16/10
8:05
cis-1,2-Dichloroethene
EPA 624
<5 ug/L
R
9/16110
8,05
SVOCs (A&B/N) by 625
EPA 625
R
9/21/10
14:00
Acenaphthene
EPA 625
<10 ug/L
R
9/21/10
14:00
Acenaphthylene
EPA 625
<10 ug/L
R
9/21110
14:00
Anthracene
EPA 625
<10 ug/L
R
9/21/10
14:00
Benzidine
EPA 625
<50 ug/L
R
9/21110
14:00
Benzo(a)anthracene
EPA 625
<10 ug/L
R
9121/10
14:00

0
0
7R TEST
6701 Conference Drive Page 3 of 4
Raleigh, NC 27607
Telephone: [phone]
Telephone: [phone] Fax: [phone] NC/WW Cert. #: 067
Fax: [phone] NC/DW Cert. #: 37731
Laboratory
Report
Work Order #: 1009-00882
No. Sample ID
Date Sampled
Time Sampled Matrix
Sample Type
Condition
002 OUTFALL #001
9/14/2010
8:00 WW
Grab
4 +/- 2 deg C
— nal zed ----
Test Performed
Method
Results
Lab Loc
atey
Time Qualifier
Benzo(b)fluoranthene
EPA 625
<10 ug/L
R
9121/10
14:00
Benzo(k)fluoranthene
EPA 625
<10 ug/L
R
9/21110
14:00
Benzo(a)pyrene
EPA 625
<10 ug/L
R
9/21110
14:00
Benzo(g,h,i)perylene
EPA 625
<10 ug/L
R
9/21110
14:00
Benzyl butyl phthalate
EPA 625
<10 ug/L
R
9121/10
14:00
Bis(2-chloroethyl)ether
EPA 625
<10 ug/L
R
9/21/10
14:00
Bis(2-chloroethoxy)methane
EPA 625
<10 ug/L
R
9/21/10
14:00
Bis(2-chloroisopropyl)ether
EPA 625
<10 ug/L
R
9/21/10
14:00
Bis(2-ethylhexyl)phthalate
EPA 625
<10 ug/L
R
9121/10
14:00
4-Bromophenyl phenyl ether
EPA 625
<10 ug/L
R
9/21110
14:00
2-Chloronaphthalene
EPA 625
<10 ug/L
R
9/21/10
14:00
4-Chioro3-methylphenol
EPA 625
<10 ug/L
R
9121/10
14:00
2-Chlorophenol
EPA 625
<10 ug/L
R
9/21/10
14:00
4-Chlorophenyl phenyl ether
EPA 625
<10 ug/L
R
9/21110
14:00
Chrysene
EPA 625
<10 ug/L
R
9/21/10
14:00
Dibenzo(a,h)anthracene
EPA 625
<10 ug/L
R
9/21110
14:00
Di-n-butyl phthalate
EPA 625
<10 ug/L
R
9121/10
14:00
3,3'-Dichlorobenzidine
EPA 625
<20 ug/L
R
9121/10
14:00
1,2-Dichlorobenzene
EPA 625
<10 ug/L
R
9/21/10
14:00
1,3-Dichlorobenzene
EPA 625
<10 ug/L
R
9/21/10
14:00
1,4-Dichlorobenzene
EPA 625
<10 ug/L
R
9/21/10
14:00
2,4-Dichiorophenol
EPA 625
<10 ug/L
R
9/21/10
14:00
Diethyl phthalate
EPA 625
<10 ug/L
R
9/21110
14:00
2,4-Dimethylphenoi
EPA 625
<10 ug/L
R
9/21110
14:00
Dimethyl phthalate
EPA 625
<10 ug/L
R
9/21110
14:00
2,4-Dinitrophenol
EPA 625
<50 ug/L
R
9/21/10
14:00
2,4-Dinitrotoluene
EPA 625
<10 ug/L
R
9/21/10
14:00
2,6-Dinitrotoluene
EPA 625
<10 ug/L
R
9/21/10
14:00
Di-n-octyl phthalate
EPA 625
<10 ug/L
R
9121110
14:00
Fluoranthene
EPA 625
<10 ug/L
R
9/21/10
14:00
Fluorene
EPA 625
<10 ug/L
R
9/21/10
14:00
Hexachlorobenzene
EPA 625
<10 ug/L
R
9121/10
14:00
Hexachlorobutadiene
EPA 625
<10 ug/L
R
9/21110
14:00
Hexachlorocyciopentadiene
EPA 625
<10 ug/L
R
9/21/10
14:00
Hexachloroethane
EPA 625
<10 ug/L
R
9/21/10
14:00
Indeno(1,2,3-c,d)pyrene
EPA 625
<10 ug/L
R
9/21/10
14:00
Isophorone
EPA 625
<10 ug/L
R
9121/10
14:00
2-Methyl4,6-dinitrophenol
EPA 625
<50 ug/L
R
9121/10
14:00
Naphthalene
EPA 625
<10 ug/L
R
9/21/10
14:00
Nitrobenzene
EPA 625
<10 ug/L
R
9/21/10
14:00
2-Nitrophenol
EPA 625
<10 ug/L
R
9/21/10
14:00

Telephone: [phone]
Fax: [phone]
0
0
-m TE ST
6701 Conference Drive
Raleigh, NC 27607
Telephone: [phone]
Fax: [phone]
Page 4 of 4
NCMW Cert #: 067
NC/DW CerL #: 37731
11
Laboratory
Report
Work Order#: 1009-00882
No. Sample ID
Date Sampled
Time Sampled
Matrix
Sample Type
Condition
002 OUTFALL #001
9/14/2010
8:00
WW
Grab
4 +/- 2 deg C
Test Performed
Method
Results
— nal zed —
Lab Loc atey Time Qualifier
4-Nitrophenol
EPA 625
<10 ug/L
R 9/21/10
14:00
N-Nitrosodi-n-propylamine
EPA 625
<20 ug/L
R 9/21/10
14:00
Pentachlorophenol
EPA 625
<30 ug/L
R 9121/10
14:00
Phenanthrene
EPA 625
<10 ug/L
R 9/21/10
14:00
Phenol
EPA 625
<10 ug/L
R 9/21/10
14:00
Pyrene
EPA 625
<10 ug/L
R 9/21/10
14:00
1,2,4-Trichlorobenzene
EPA 625
<20 ug/L
R 9/21/10
14:00
2,4,6-Trichlorophenol
EPA 625
<10 ug/L
R 9121110
14:00
N-Nitrosodimethylamine
EPA 625
<10 ug/L
R 9/21/10
14:00
N-Nitrosodiphenylamine
EPA 625
<20 ug/L
R 9121/10
14:00
1,2-Diphenylhydrazine
EPA 625
<10 ug/L
R 9/21/10
14:00
No. Sample ID
Date Sampled
Time Sampled
Matrix
Sample Type
Condition
003 OUTFALL #001
9/14/2010
8:00
WW
Grab
4 +/- 2 deg C
Test Performed
Method
Results
— Panal zed
Lab Loc atey
Time Qualifier
Low Level Mercury
EPA 1631
2.08 ng/L
R 9/20110
6.31
No. Sample ID
Date Sampled
Time Sampled
Matrix
Sample Type
Condition
004 BLANK
9/14/2010
8:00
WW
Grab
4 +/- 2 deg C
Test Performed
Method
Results
Lab Loc Dates
Time Qualifier
Low Level Mercury
EPA 1631
<1.0 ng/L
R 9120110
6:31
Reviewed by:
for Tritest, Inc.

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NC00000019 United Chemi-Con Facility
'j,"M
�-,itude: 3535'70" Sub -Basin: 05-07-02
Location
Lonitgude: 800
52'21
Ouad #: B 12NE[Warrensville
Stream Class: C+ Receiving Stream: NoUnited Chenti-Con Manufacturing, Inc.
North Fork New River NC0000019
No F United Chetni-Con

sl6

pr
Beverly Eaves Perdue
Governor
Mr. Butch Howell
United Chemi-Con
185 McNeil Road
Lansing, NC 28643
ALIV-5WA
__
Affl�
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Coleen H. Sullins
Director
SUBJECT:
Dear Mr. Howell:
April 29, 2010
Compliance Evaluation Inspection
United Chemi-Con WWTP
NPDES Permit # NC0000019
Ashe County
Dee Freeman
Secretary
On April 16, 2010 George Smith performed a Compliance Evaluation Inspection. Mr. Gale D. Howell, ORC,
Grade IV, was present for the inspection. Mr. Gale Wyatt is the Grade I Back-up operator. The inspection is
comprised of an overall evaluation in order to document compliance and noncompliance of: facilities
equipment, capability to meet effluent limits, and NPDES permit terms & conditions.
Permit
Your NPDES permit became effective on January 1, 2007 and expires on March 31, 2011.
The permit identifies the following discharge pipes:
(001) Non -contact cooling water, A/C condensate, boiler blow -down, de -ionizer backwash, assembled product
wash water & process wastewater. Process wastewater is not discharged, it is hauled away.
(003) A/C condensate.
(006) Domestic wastewater.
(007) Recycled non -contact cooling water, and filtered surface water during maintenance periods only.
Records & Reports
Mr. Howell maintains a log. Mr. Howell documents phone conversations, calibrations, process control, and all
are done in an excellent manner.
Facility Site Review
The effluent from the Imhoff tank was clear with no visible solids.
North Carolina Division of Water Quality, Winston-Salem Regional Office
Location: 585 Waughtown St, Winston-Salem, North Carolina 27107
Phone: [phone] FAX: [phone] Customer Service: 1-877-623-6748
Internet: www.ncwaterquai4.org
An Equal Opportunity 1 Affirmative Action Employer
Nne
orthCarohna
naturally

Mr. Howell
April 29, 2010
Page 2 of 3
11
The sandfilters were raked and appeared to be clean and in good condition. There was no evidence of ponding
on the surface of the sandfilters.
The dosing lines were discharging onto the concrete pads. They worked good.
Flow Measurement
The instantaneous flow at Outfall 006 is obtained by measuring the height of the water in a 1-inch parshall
flume then converting it to flow (MGD).
The Stevens, Model 6 1 R flow meter at Outfall 001 was calibrated by B.W. Allen on March 23 2010.
Laboratory
Mr. Howell performs pH and Temperature; and these tests are recorded on the daily monitoring report.
A field certification for pH and Temperature was issued to Mr. Butch Howell for United Chemi-Con (lab
#5099). All remaining tests are performed by Tritest (Certified Lab #103).
Calibration for pH is performed using Fisher standards of pH 4, 7, 10.
The temperature is recorded against a NIST traceable thermometer.
Effluent/Receivine Waters
The effluent from Pipes 001 and 006 to the North Fork New River, Class C + waters of the State was clear, no
color, no solids, or no odor.
The effluent from pipes 001, 003, 006, and 007 do not impact the North Fork New River.
Effluent pipes 003 and 007 were not discharging.
Operations & Maintenance
Mr. Butch Howell, Grade IV is the current ORC. The back-up operator is Mr. Gale Wyatt, Grade I.
The facility (pipe 006) with the Imhoff tank is considered a Class II facility.
The facility was well maintained by the staff, and they are considered to perform their jobs in an outstanding
manner. The sandbed is well maintained. The Imhoff tank appears to be well operated & maintained.
Process control tests of pH, ammonia, alkalinity, oil & grease are performed on the influent and Imhoff tank.
Process control tests appear to be successfully used in measuring plant performance.

FX4r. Howell
April 29, 2010
Page 3 of 3
Self -Monitoring Program
A review of the monthly self -monitoring reports from March 2009 through December 2009 did not show any
monitoring or limit violations.
Grab samples are taken from the end of the pipe 006 at the bank of the river.
The composite sampler at Pipe 001 is time composite at 200 mL every 30 minutes.
The chain -of -custody reports were accurate and in good order.
Mr. Gale Wyatt performs the plant Operations & Maintenance in an outstanding manner. Mr. Howell continues
to perform in an outstanding manner. The compliance evaluation inspection is considered excellent. If you have
any questions please contact George Smith at [phone].
Sincerely,
Steve W. Tedder
Regional Supervisor
cc: WSRO Files

United States Environmental Protection Agency
Form Approved.
EPA Washington, D.C. 20460
OMB No. 2040-0057
Water Compliance Inspection Report
Approval expires 8-31-98
Section A: National Data System Coding (i.e., PCS)
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type
1 I NI 2 151 31 NC0000019 111 121 10/04/19 117 181 CI 191SI 201 I
Remarks
21111111111111111111111111111111111111111111111116
Inspection Work Days Facility Self -Monitoring Evaluation Rating 131 QA --------- ----------------- Reserved ------- —--------- ---
67) 169 701 51 711 DI 721 NJ 73I 174 751 I I I I I I 180
�II —I
Section B: Facility Data
Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include
Entry Time/Date
Permit Effective Date
POTW name and NPDES permit Number)
United Chemi-Con, Inc.
11:05 AM 10/04/19
07/01/01
Exit Time/Date
Permit Expiration Date
185 McNeil Rd
Lansing NC 28643
12:05 PM 10/04/19
11/03/31
Name(s) of Onsite Representative(s)/Titles(s)/Phone and Fax Number(s)
Other Facility Data
Gale Dean Howell/ORC/336-384-6917/
Name, Address of Responsible Official/Title/Phone and Fax Number
Gale D Howe11,185 McNeil Rd Lansing NC 28693//336-384-6917/ Contacted
No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit N Flow Measurement Operations & Maintenance 0 Records/Reports
Self -Monitoring Program N Facility Site Review Effluent/Receiving Waters
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date
George S Smith WSRO WQ//336-771-5000/ oaU to
Signature of Management Q A Reviewer Agency/Office/Phone and Fax Numbers Date
Z'F4�L Zil o
r I r a/ 6W w, / V oill 4-
-EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete.
Page # 1

NPDES yr/mo/day Inspection Type
3I NC0000019 I11 12, 10/04/19 117 18I�I
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
All discharge outfalls are in compliance.
Page # 2

pr
Permit: NC0000019
Inspection Date: 04/19/2010
Owner - Facility: United Chemi-Con, Inc.
Inspection Type: Compliance Evaluation
Operations & Maintenance Yes No NA NE
Is the plant generally clean with acceptable housekeeping? ■ ❑ ❑ ❑
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable Solids, pH, DO, Sludge ■ n ❑ n
Judge, and other that are applicable?
Comment:
(If the present permit expires in 6 months or less). Has the permittee submitted a new application?
n
n
■
n
Is the facility as described in the permit?
■
n
n
n
# Are there any special conditions for the permit?
n
■
n
n
Is access to the plant site restricted to the general public?
■
n
n
n
Is the inspector granted access to all areas for inspection?
■
n
n
n
Comment:
Flow Measurement - Effluent
Yes
No
NA
NE
# Is flow meter used for reporting?
■
n
❑
❑
Is flow meter calibrated annually?
0.0
n
n
Is the flow meter operational?
■
n
n
n
(If units are separated) Does the chart recorder match the flow meter?
n
n
n
■
Comment:
Record Keeping
Yes
No
NA
NE
Are records kept and maintained as required by the permit?
■
n
n
n
Is all required information readily available, complete and current?
■
n
n
n
Are all records maintained for 3 years (lab. reg. required 5 years)?
■
n
n
n
Are analytical results consistent with data reported on DMRs?
■
n
n
n
Is the chain -of -custody complete?
■
n
n
n
Dates, times and location of sampling
■
Name of individual performing the sampling
■
Results of analysis and calibration
■
Dates of analysis IN
Name of person performing analyses ■
Transported COCs ■
Are DMRs complete: do they include all permit parameters? ■ n n n
Page # 3

Permit: NC0000019
Inspection Date: 04/19/2010
owner - Facility: United Chemi-Con, Inc.
Inspection Type: Compliance Evaluation
Record Keeping
Has the facility submitted its annual compliance report to users and DWQ?
(if the facility is = or > 5 MGD permitted flow) Do they operate 24/7 with a certified operator on each shift?
Is the ORC visitation log available and current?
Is the ORC certified at grade equal to or higher than the facility classification?
Is the backup operator certified at one grade less or greater than the facility classification?
Is a copy of the current NPDES permit available on site?
Facility has copy of previous year's Annual Report on file for review?
Comment:
Sand Filters (Low rate)
(If pumps are used) Is an audible and visible alarm Present and operational?
Is the distribution box level and watertight?
Is sand filter free of ponding?
Is the sand filter effluent re -circulated at a valid ratio?
# Is the sand filter surface free of algae or excessive vegetation?
# Is the sand filter effluent re -circulated at a valid ratio? (Approximately 3 to 1)
Comment:
Yes No NA NE
nn■o
■nnn
■nnn
nn■n
■nnn
nn■o
Page # 4

185 McNeil Road, Lansing, NC 28643-8300 • Phone [phone] • Fax [phone] • http://www.chemi-con.com
UNRED
CHEMI•CON
UNITED CHEMI—CON, INCfzp!ofEENR s_
April 23, 2010 APR 2 g 2010
W,. ;ton -Salem
Regional Office
Point Source Branch
Surface Water Protection Section
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
SUBJECT: Delegation of Signature Authority
UNITED CHEMI-CON
NPDES No. NC 0000019
To Whom It May Concern:
By notice of this letter, I hereby delegate signatory authority to each of the following
individuals for all permit applications, discharge monitoring reports, and other information
relating to the operations at United Chemi-Con as required by all applicable federal, state, and
local environmental agencies specifically with the requirements for signatory authority as
specifled in 15A NCAC 2B.0506.
Name Title
Yoshi Narita Vice -President General Manager
Steve Katz Plant Manager
John Kolbow Controller
Gale D. Howell Environmental/Safety Manager
If you have any questions regarding this letter, please feel free to contact me at [phone].
Sincerely,
'Yoshi Narita
Vice -President General Manager
sr
cc: Winston-Salem Regional Office

Beverly Eaves Perdue
Governor
5099
Mr. Gale D. "Butch" Howell
UNITED CHEMI-CON
185 McNeil Rd.
Lansing, NC 28643-
�X j
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Coleen H. Sullins
Director
December 23, 2009
SUBJECT: Wastewater/Groundwater Laboratory Certification Renewal
FIELD PARAMETERS ONLY
Dear Mr. Howell:
Dee Freeman
Secretary
j RECEIVED
II ]eoL of ENR
i
DEC 3 0 2009
L MnstonSalern
Regional Office
The Department of Environment and Natural Resources, in accordance with the provisions of NC GS 143-215-
.3 (a) (10), 15 NCAC 2H .0800, is pleased to renew certification for your laboratory to perform specified
environmental analyses required by EMC monitoring and reporting regulations 15 NCAC 213 .0500, 2H .0900 and
2L .0100, .0200, .0300, and 2N .0100 through .0800.
Enclosed for your use is a certificate describing the requirements and limits of your certification. Please review
this certificate to insure that your laboratory is certified for all parameters required to properly meet your
certification needs.
Please contact us at 919-733-3908 if you have questions or need additional information.
Sincerely,
Pat Donnelly
Certification Branch Manager
Laboratory Section
Enclosure
cc:
Ramon Cook
Dana Satterwhite
Winston - Salem Regional Office
DENR DWQ Laboratory Section NC Wastewater/Groundwater Laboratory Certification Branch
1623 Mail Service Center, Raleigh, North Carolina 27699-1623
Location: 4405 Reedy Creek Road. Raleigh, North Carolina 27607-6445
Phone: [phone] FAX: [phone]
Internet: www.dwglab.org
Nne
orthCarolina
Nahmallty
An Equal Opportunity \AffrmativeAction Employer Customer Service:1-877-623-6748 www.ncwaterquality.org

STATE OF NORTH CAROLINA DEPARTMENT OF THE
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
LABORATORY CERTIFICATION PROGRAM
In accordance with the provisions ofN.C.G.S. 143-215.3 (a) (1), 143-215.3 (a)(10) and NCAC 2H.0800:
2010
UNITED CHEMI-CON
Is hereby certified to perform environmental analysis as listed on Attachment I and report monitoring data to DWQ for
compliance with NPDES effluent, surface water, groundwater, and pretreatment regulations.
By reference 15A NCAC 2H .0800 is made a part of this certificate.
This certificate does not guarantee validity of data generated, but indicates the methodology, equipment, quality control procedures,
records, and proficiency of the laboratory have been examined and found to be acceptable.
This certificate shall be valid until December 31, 2010
Certificate N 5099
Pat Donnelly

Address:
) CHEMI-CON
185 McNeil Rd.
Lansing, NC 28643-
Attachment I
North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Certificate Number: 5099
Effective Date: 01 /01 /2010
Expiration Date: 12/31/2010
Date of Last Amendment:
The above named laboratory, having duly met the requirements of 15A NCAC 21-1.0800, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
INORGANICS
pH
Std Method 4500 H B
TEMPERATURE
Std Method 2550B
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are
subject to civil penalties and/or decertification for infractions as set forth in 15A NCAC 21-1.0807.

PF
Beverly Eaves Perdue
Governor
Mr. Butch Howell
United Chemi-Con
185 McNeil Road
Lansing, NC 28643
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Coleen H. Sullins
Director
May 27, 2009
SUBJECT: Compliance Evaluation Inspection
United Chemi-Con WWTP
NPDES Permit # NC0000019
Ashe County
Dear Mr. Howell:
Dee Freeman
Secretary
On May 20, 2009 George Smith performed a Compliance Evaluation Inspection. Mr. Gale D. Howell, ORC,
Grade IV, was present for the inspection. Mr. Gale Wyatt is the Grade I Back-up operator. The inspection is
comprised of an overall evaluation in order to document compliance and noncompliance of- facilities
equipment, capability to meet effluent limits, and NPDES permit terms & conditions.
Permit
Your NPDES permit became effective on January 1, 2007 and expires on March 31, 2011.
The permit identifies the following discharge pipes:
(001) Non -contact cooling water, A/C condensate, boiler blow -down, de -ionizer backwash, assembled product
wash water & process wastewater. Process wastewater is not discharged, it is hauled away.
(003) A/C condensate.
(006) Domestic wastewater.
(007) Recycled non -contact cooling water, and filtered surface water during maintenance periods only.
Records & Reports
Mr. Howell maintains a log. Mr. Howell documents phone conversations, calibrations, process control, and all
are done in an excellent manner.
Facility Site Review
The effluent from the Imhoff tank was clear with no visible solids.
North Carolina Division of Water Quality, Winston-Salem Regional Office
Location: 585 Waughtown St. Winston-Salem, North Carolina 27107
Phone: [phone] FAX: [phone] Customer Service:1-877.623.6748
Internet www.ncwaterquality.org
An Equal Opportunity 1 Affirmative Action Employer
One
NorthCarolina
Na&ra!!rf

Mr. Howell
May 27, 2009
Page 2 of 3
11
The sandfilters were raked and appeared to be clean and in good condition. There was no evidence of ponding
on the surface of the sandfilters.
The dosing lines appear to be functioning properly.
Flow Measurement
The instantaneous flow at Outfall 006 is obtained by measuring the height of the water in a 1-inch parshall
flume then converting it to flow (MGD).
The Stevens, Model 6 1 R flow meter at Outfall 001 was calibrated by B.W. Allen on March 11, 2009.
Laboratory
Mr. Howell performs pH and Temperature; and these tests are recorded on the daily monitoring report.
A field certification for pH and Temperature was issued to Mr. Butch Howell for United Chemi-Con (lab
#5099). All remaining tests are performed by Tritest (Certified Lab #103).
Calibration for pH is performed using Fisher standards of pH 4, 7, 10.
The temperature is recorded against a NIST traceable thermometer.
Effluent/Receiving Waters
The effluent from Pipes 001 and 006 to the North Fork New River, Class C + waters of the State was clear, no
color, no solids, or no odor.
The effluent from pipes 001, 003, 006, and 007 do not impact the North Fork New River.
Effluent pipes 003 and 007 were not discharging.
Operations & Maintenance
Mr. Butch Howell, Grade IV is the current ORC. The back-up operator is Mr. Gale Wyatt, Grade I.
The facility (pipe 006) with the Imhoff tank is considered a Class II facility.
The facility was well maintained by the staff, and they are considered to perform their jobs in an outstanding
manner. The sandbed is well maintained. The Imhoff tank appears to be well operated & maintained.
Process control tests of pH, ammonia, alkalinity, oil & grease are performed on the influent and Imhoff tank.
Process control tests appear to be successfully used in measuring plant performance.

rMrHowell
May 27, 2009
Page 3 of 3
Self -Monitoring Program
A review of the monthly self -monitoring reports from April 2008 through February 2009 did not show any
monitoring or limit violations.
Grab samples are taken from the end of the pipe 006 at the bank of the river.
The composite sampler at Pipe 001 is time composite at 200 mL every 30 minutes.
The chain -of -custody reports were accurate and in good order.
Mr. Gale Wyatt performs the plant Operations & Maintenance in an outstanding manner. Mr. Howell continues
to perform in an outstanding manner. The compliance evaluation inspection is considered excellent. If you have
any questions please contact George Smith at [phone].
Sincerely,
oo
Steve W. Tedder
Regional Supervisor
cc: WSRO Files

United States Environmental Protection Agency
FormApproved.
EP ^ Washington, D.C. 20460
j-�
OMB
OMB No. 2040-0057
Water Compliance Inspection Report
Approval expires 8-31-98
Section A: National Data System Coding (i.e., PCS)
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type
1 I NI 2 15I 31 NC0000019 111 121 09/05/20 117 181CI 191SI 201 I
l-
Remarks
211 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I -J 6
Inspection Work Days Facility Self -Monitoring Evaluation Rating B1 QA --------------Reserved-----------
67I 169 701 5 i 711 DI 721 j 73I I 174 751 I I I I I Li 80
W
Section B: Facility Data
Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include
Entry Time/Date
Permit Effective Date
POTW name and NPDES permit Number)
10:55 AM 09/05/20
07/01/01
United Chemi-Con, Inc.
Exit Time/Date
Permit Expiration Date
185 McNeil Rd
Lansing NC 28643
12.05 PM 09/05/20
11/03/31
Name(s) of Onsite Representative(s)/Titles(s)/Phone and Fax Number(s)
Other Facility Data
Gale Dean Howell/ORC/336-384-6917/
Name, Address of Responsible Officialfritle/Phone and Fax Number
Contacted
Gale D Howell,185 McNeil Rd Lansing NC 28643//336-384-6917/ No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit Flow Measurement Operations & Maintenance Records/Reports
Self -Monitoring Program Facility Site Review Effluent/Receiving Waters
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date
George S Smith WSRO WQ//336-771-5000/ /
Signature of Maillilgement Q A Re ' wer Agency/Office/Phone and Fax Numbers Date
f " .,J"T — 0 f
EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete.
Page # 1

NPDES
yr/mo/day
31 NC0000019 1
11 121 09/05/20 I1'
Inspection Type
181
LJ
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
Page # 2

Permit: NC0000019
Inspection Date: 05/20/2009
Owner - Facility: United Chemi-Con, Inc.
Inspection Type: Compliance Evaluation
Operations & Maintenance Yes No NA NE
Is the plant generally clean with acceptable housekeeping? ■ n n n
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable Solids, pH, DO, Sludge ■ ❑ n n
Judge, and other that are applicable?
Comment:
Permit Yes No NA NE
(If the present permit expires in 6 months or less). Has the permittee submitted a new application?
n n
■
n
Is the facility as described in the permit?
■ n
n
n
# Are there any special conditions for the permit?
❑ ■
❑
❑
Is access to the plant site restricted to the general public?
■ n
n
n
Is the inspector granted access to all areas for inspection?
■ n
n
n
Comment:
Record Keeping
Yes
No
NA NE
Are records kept and maintained as required by the permit?
■
n
n
n
Is all required information readily available, complete and. current?
■
❑
n
n
Are all records maintained for 3 years (lab. reg. required 5 years)?
■
n
n
n
Are analytical results consistent with data reported on DMRs?
■
n
❑
n
Is the chain -of -custody complete?
■
n
n
Dates, times and location of sampling
■
Name of individual performing the sampling
■
Results of analysis and calibration
■
Dates of analysis
■
Name of person performing analyses
■
Transported COCs
■
Are DMRs complete: do they include all permit parameters?
■
❑
n
Has the facility submitted its annual compliance report to users and DWQ?
n
n
■
(If the facility is = or > 5 MGD permitted flow) Do they operate 24/7 with a certified operator on each shift?
n
n
■
n
Is the ORC visitation log available and current?
■
n
n
n
Is the ORC certified at grade equal to or higher than the facility classification?
■
n
n
n
Is the backup operator certified at one grade less or greater than the facility classification?
■
n
n
n
Is a copy of the current NPDES permit available on site?
■
n
n
n
Page # 3

Permit: NC0000019
Inspection Date: 05/20/2009
Record Keeping
Facility has copy of previous year's Annual Report on file for review?
Comment:
Flow Measurement - Effluent
# Is flow meter used for reporting?
Is flow meter calibrated annually?
Is the flow meter operational?
Owner - Facility: United Chemi-Con, Inc.
Inspection Type: Compliance Evaluation
(If units are separated) Does the chart recorder match the flow meter?
Comment:
Sand Filters (Low rate)
(If pumps are used) Is an audible and visible alarm Present and operational?
Is the distribution box level and watertight?
Is sand filter free of ponding?
Is the sand filter effluent re -circulated at a valid ratio?
# Is the sand filter surface free of algae or excessive vegetation?
# Is the sand filter effluent re -circulated at a valid ratio? (Approximately 3 to 1)
Comment:
Yes No NA NE
00■O
Yes No NA NE
■O00
0000
MOOD
O000
Yes No NA NE
00■0
■000
■D00
OD■0
■000
00■0
Page # 4

—I
December 19, 2008
5099
Mr. Gale D. "Butch" Howell
UNITED CHEMI-CON
185 McNeil Rd.
Lansing, NC 28643-
�r
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
SUBJECT: Wastewater/Groundwater Laboratory Certification Renewal
FIELD PARAMETERS ONLY
Dear: Mr. Howell
Coleen H. Sullins, Director
Division of Water Quality
RECEIVED
N.C. Deot. of ENR
JAN 0 g 2009
Winston-Salem
Regional Office
The Department of Environment and Natural Resources, in accordance with the provisions of NC GS 143-215-.3
(a) (10), 15 NCAC 2H .0800, is pleased to renew certification for your laboratory to perform specified
environmental analyses required by EMC monitoring and reporting regulations 15 NCAC 2B .0500, 2H .0900 and
2L .0100, .0200, .0300, and 2N .0100 through .0800.
Enclosed for your use is a certificate describing the requirements and limits of your certification. Please review
this certificate to insure that your laboratory is certified for all parameters required to properly meet your
certification needs.
Please contact us at 919-733-3908 if you have questions or need additional information.
Sincerely,
10
Pat Donnelly
Certification Branch Manager
Laboratory Section
Enclosure
cc: Ramon L. Cook /
Dana Satterwhite
Winston-Salem Regional Office
NoZhCarolina
Naturally
Laboratory Section 1623 Mail Service Center; Raleigh, NC 27699-1623 Phone [phone]
Location: 4405 Reedy Creek Road; Raleigh, NC 27607 FAX [phone]
Intemet: www.dwglab.org/Customer Service1-877-623-6748
An Equal Opportunity/Affirmative Action Employer— 50% Recycled/10% Post Consumer Paper

Certificate No. 5099
STATE OF NORTH CAROLINA DEPARTMENT OF THE
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
LABORATORY CERTIFICATION PROGRAM
In accordance with the provisions of N.C.G.S. 143-215.3 (a) (1), 143-215.3 (a)(10) and NCAC 2H.0800:
Field Parameter Only
UNITED CHEMI-CON
Is hereby certified to perform environmental analysis as listed on Attachment I and report monitoring data to DWQ for
compliance with NPDES effluent, surface water, groundwater, and pretreatment regulations.
By reference 15A NCAC 2H .0800 is made a part of this certificate.
This certificate does not guarantee validity of data generated, but indicates the methodology, equipment, quality control procedures,
records, and proficiency of the laboratory have been examined and found to be acceptable.
This certificate shall be valid until December 31, 2009
Pat Donnelly

1NITED CHEMI-CON
85 McNeil Rd.
Lansing, NC 28643-
Attachment
North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
FIELD PARAMETERS ONLY
Certificate Number:
Effective Date:
Expiration Date:
Date of Last Amendment:
5099
01/01/2009
12/31/2009
The above named laboratory, having duly met the requirements of 15A NCAC 21-1.0800, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
INORGANICS
pH
Std Method 4500 H B
TEMPERATURE
Std Method 2550B
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are
subject to civil penalties and/or decertification for infractions as set forth in 15A NCAC 2H.0807.

O�O� W AT �99G
r
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Coleen H. Sullins, Director
Division of Water Quality
June 2, 2008
Mr. Butch Howell
United Chemi-Con
185 McNeil Road
Lansing, NC 28643
SUBJECT: Compliance Evaluation Inspection
United Chemi-Con WWTP
NPDES Permit # NC0000019
Ashe County
Dear Mr. Howell:
A Compliance Evaluation Inspection was performed by George Smith and Sue White on May 28,
2008. Mr. Gale D. Howell, ORC, Grade IV, was present for the inspection. Mr. Gale Wyatt is the
Grade I Back-up operator. Theinspection was comprised of an overall evaluation in order to
document compliance and noncompliance of. facilities equipment, capability to meet effluent limits,
and NPDES permit terms & conditions.
The attached inspection form evaluates nine (9) areas as noted in Section C of the attached
EPA inspection report, and the observations and comments during the inspection are
addressed below:
Parm it
Your NPDES permit became effective on January 1, 2007 and expires on March 31, 2011.
The permit identifies the following discharge pipes:
(001) Non -contact cooling water, A/C condensate, boiler blow -down, de -ionizer backwash,
assembled product wash water & process wastewater. Process wastewater is not discharged,
it is hauled away.
(003) A/C condensate.
(006) Domestic wastewater.
(007) Recycled non -contact cooling water, and filtered surface water during maintenance periods
only.
Records & Reports
Mr. Howell maintains a log. Mr. Howell documents phone conversations, calibrations, process
control, and all are done in an excellent manner. one
NgnhCarolina
atma!!y
North Carolina Division of Water Quality 585 Waughtown Street Phone [phone] Customer Service
Winston-Salem Regional Office Winston-Salem, NC 27107 Fax [phone]
Internet: www.ncwateMuality.org
An Equal Opportunity/Affirmative Action Employer— 50% Recycled/10% Post Consumer Paper

rMr. Howell
June 2, 2008
Page 2 of 3
Facility Site Review
The effluent from the Imhoff tank was clear with no visible solids.
The sandfilters were raked and appeared to be clean and in good condition. There was no evidence of
ponding on the surface of the sandfilters.
The dosing lines appear to be functioning properly.
Flow Measurement
The instantaneous flow at Outfall 006 is measured with a 1-inch parshall flume by measuring the
head and converting it to flow (MGD).
The Stevens, Model 61 R flow meter at Outfall 001 was calibrated by B.W. Allen on March 14, 2008.
Laboratory
Mr. Howell performs pH and Temperature; and these tests are recorded on the daily monitoring
report.
A field certification for pH and Temperature was issued to Mr. Butch Howell for United Chemi-Con
(lab #5099). All remaining tests are performed by Tritest (Lab #103), which is a certified lab.
The pH calibration is performed using a two -point calibration method (pH 4 & 10), and a mid -range
check (pH 7). The calibrations were documented.
The temperature is recorded against a NIST traceable thermometer.
Effluent/Receiving Waters
The effluent from Pipes 001 and 006 to the North Fork New River, Class C + waters of the State was
clear, no color, no solids, or no odor.
The effluent from pipes 001, 003, 006, and 007 did not appear to impact the North Fork New River.
In fact, pipes 003 and 007 were not discharging.
Operations & Maintenance
Mr. Butch Howell, Grade IV is the current ORC. The back-up operator is Mr. Gale Wyatt, Grade I.
The facility (pipe 006) with the Imhoff tank is considered a Class II facility.

rmr.Howell
June 2, 2008
Page 3 of 3
The facility was well maintained by the staff, and they are considered to perform their jobs in an
outstanding manner. The equipment appeared to be in good operating order. The Imhoff tank appears
to be well operated & maintained.
Process control tests of pH, ammonia, alkalinity, oil & grease are performed on the influent and
Imhoff tank. Process control tests appear to be successfully used in measuring plant performance.
Self -Monitoring Program
A review of the monthly self -monitoring reports from April 2007 through March 2008 did not show
any monitoring or limit violations.
Data verification was performed on March 2008 data. The lab data and the monitoring report data
were identical.
The grab samples, if required, are taken from the end of the pipe at all outfalls.
The composite sampler at Pipe 001 is time composite at 200 mL every 30 minutes.
The chain -of -custody reports were accurate and in good order.
Sludge Disposal
Sludge is removed from the plant by Cox Septic Service.
Mr. Howell continues to perform his job in an outstanding manner. Mr. Gale Wyatt performs the
plant Operations & Maintenance in an outstanding manner. The compliance evaluation inspection is
considered excellent. If you have any questions please contact George Smith at [phone].
Sincerely,
Steve W. Tedder
Regional Supervisor
cc: SWP Central Files
WSRO Files

United States Environmental Protection Agency
Form Approved.
EPA Washington, D.C. 20460
OMB No. 2040-0057
Water Compliance Inspection Report
Approval expires8-31-98
Section A: National Data System Coding (i.e., PCS)
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type
1 I NI 2 151 31 N00000019 111 121 08/05/28 117 181 CI 191SI 201 I
Remarks
211111111111111111 111111111111 I II I III I IIII 11111116
Inspection Work Days Facility Self -Monitoring Evaluation Rating B1 QA -------------------------- Reserved ----- ----------------
67 I 169 701 51 711 NJ . 721 NJ 73I 174 751 I I I I I Li 80
wI
Section B: Facility Data
Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include
Entry Time/Date
Permit Effective Date
POTW name and NPDES permit Number)
10:55 AM 08/05/28
07/01/01
United Chemi-Con, Inc.
Exit Time/Date
Permit Expiration Date
185 McNeil Rd
Lansing NC 28643
11:30 AM 08/05/28
11/03/31
Name(s) of Onsite Representative(s)/Titles(s)/Phone and Fax Number(s)
Other Facility Data
Gale Dean Howell/ORC/336-384-6917/
Name, Address of Responsible Official/Title/Phone and Fax Number
Contacted
Gale D Howel1,185 McNeil Rd Lansing NC 28643//336-384-6917/ No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit Flow Measurement Operations & Maintenance Records/Reports
Self -Monitoring Program Facility Site Review Effluent/Receiving Waters Laboratory
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date
George S Smith WSRO WQ//336-771-5000/ ` - a -0
10 1-0
'(� W
Signature of Manage ent Q A Review Agency/Office/Phone and Fax Numbers Date
6&'11 <olll<— Y
EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete.
Page # 1

NPDES yr/mo/day Inspection Type
3I NC0000019 I11 121 08/05/28 117 18ICI
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
Facility is compliant with the permit.
Page # 2

Permit: NC0000019
Inspection Date: 05/28/2008
Owner - Facility: United Chemi-Con, Inc.
Inspection Type: Compliance Evaluation
Operations & Maintenance Yes No NA NE
Is the plant generally clean with acceptable housekeeping? ■ n n n
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable Solids, pH, DO, Sludge ■ n n n
Judge, and other that are applicable?
Comment:
Permit
Yes
No
NA
NE
(If the present permit expires in 6 months or less). Has the permittee submitted a new application?
n
n
■
❑
Is the facility as described in the permit?
■
❑
❑
n
# Are there any special conditions for the permit?
n
■
n
n
Is access to the plant site restricted to the general public?
■
n
n
n
Is the inspector granted access to all areas for inspection?
■
n
n
n
Comment:
Record Keeping
Yes
No
NA
NE
Are records kept and maintained as required by the permit?
■
n
n
n
Is all required information readily available, complete and current?
■
n
n
n
Are all records maintained for 3 years (lab. reg. required 5 years)?
■
In
In
n
Are analytical results consistent with data reported on DMRs?
■
n
n
n
Is the chain -of -custody complete?
■
❑
❑
❑
Dates, times and location of sampling
■
Name of individual performing the sampling
■
Results of analysis and calibration
■
Dates of analysis
■
Name of person performing analyses
■
Transported COCs
■
Are DMRs complete: do they include all permit parameters?
■
n
n
n
Has the facility submitted its annual compliance report to users and DWQ?
n
n
■
n
(If the facility is = or > 5 MGD permitted flow) Do they operate 24/7 with a certified operator on each shift?
❑
❑
■
❑
Is the ORC visitation log available and current?
■
n
n
In
Is the ORC certified at grade equal to or higher than the facility classification?
■
n
n
n
Is the backup operator certified at one grade less or greater than the facility classification?
■
n
n
n
Is a copy of the current NPDES permit available on site?
■
n
n
n
Page # 3

Permit: NC0000019 Owner - Facility: United Chemi-Con, Inc.
Inspection Date: 05/28/2008 Inspection Type: Compliance Evaluation
Record Keeping
Facility has copy of previous year's Annual Report on file for review?
Comment:
Flow Measurement - Effluent
# Is flow meter used for reporting?
Is flow meter calibrated annually?
Is the flow meter operational?
(If units are separated) Does the chart recorder match the flow meter?
Comment:
Sand Filters (Low rate)
(If pumps are used) Is an audible and visible alarm Present and operational?
Is the distribution box level and watertight?
Is sand filter free of ponding?
Is the sand filter effluent re -circulated at a valid ratio?
# Is the sand filter surface free of algae or excessive vegetation?
# Is the sand filter effluent re -circulated at a valid ratio? (Approximately 3 to 1)
Comment:
Yes No NA NE
nn■n
■nnn
■nnn
nn■o
■nnn
nn■o
Page # 4

O�O� W A T �9Q0
o <
June 11, 2007
Mr. Butch Howell
United Chemi-Con
185 McNeil Road
Lansing, NC 28643
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
SUBJECT: Compliance Evaluation Inspection
United Chemi-Con WWTP
NPDES Permit # NC0000019
Ashe County
Dear Mr. Howell:
Coleen Sullins. Director
Division of Water Quality
A Compliance Evaluation Inspection was performed by George Smith and Sue White on May 10,
2007. Mr. Gale D. Howell, ORC, Grade IV, was present for the inspection. Mr. Gale Wyatt is the
Grade I Back-up operator. The inspection was comprised of an overall evaluation in order to
document compliance and noncompliance of: facilities equipment, capability to meet effluent limits,
and NPDES permit terms & conditions.
The attached inspection form evaluates nine (9) areas as noted in Section C of the attached
EPA inspection report, and the observations and comments during the inspection are
addressed below:
Permit
Your NPDES permit became effective on January 1, 2007 and expires on March 31, 2011.
The permit identifies the following discharge pipes:
(001) Non -contact cooling water, A/C condensate, boiler blowdown, de -ionizer backwash,
assembled product wash water & process wastewater. Process wastewater is not discharged,
it is hauled away.
(003) A/C condensate.
(006) Domestic wastewater.
(007) Recycled non -contact cooling water, and filtered surface water during maintenance periods
only.
Records & Reports
Mr. Howell maintains a log. Mr. Howell documents phone conversations, calibrations, process
control, and all are done in an excellent manner. NOne Carolina
Ntura!!y
North Carolina Division of Water Quality 585 Waughtown Street Phone [phone] Customer Service
Winston-Salem Regional Office Winston-Salem, NC 27107 Fax [phone]
Internet: www.newateMuality.org
An Equal Opportunity/Affirmative Action Employer— 50% Recycled/10% Post Consumer Paper

Mr. Howell
June 11, 2007
Page 2 of 3
Facilily Site Review
The effluent from the Imhoff tank was clear with no visible solids.
The sandfilters were raked and appeared to be clean and in good condition. There was no evidence of
ponding on the surface of the sandfilters.
The dosing lines appear to be functioning properly.
Flow Measurement
The instantaneous flow at Outfall 006 is measured with a 1-inch parshall flume by measuring the
head and converting it to flow (MGD).
The Stevens, Model 61 R flow meter at Outfall 001 was calibrated by B.W. Allen on March 14, 2007.
The instantaneous flow from the chart read 0.002 MGD at the time of the inspection.
Laboratory
Mr. Howell performs pH and Temperature; and these tests are recorded on the daily monitoring
report.
A field certification for pH and Temperature was issued to Mr. Butch Howell for United Chemi-Con
(lab #5099). All remaining tests are performed by Tritest (Lab #103), which is,a certified lab.
The pH calibration is performed using a two -point calibration method (pH 4 & 10), and a mid -range
check (pH 7). The calibrations were documented.
The temperature is recorded against a NIST traceable thermometer.
Effluent/Receiving Waters
The effluent from Pipes 001 and 006 to the North Fork New River, Class C + waters of the State was
clear, no color, no solids, or no odor.
The effluent from pipes 001, 003, 006, and 007 did not appear to impact the North Fork New River.
In fact, pipes 003 and 007 were not discharging.
Operations & Maintenance
Mr. Butch Howell, Grade IV is the current ORC. The back-up operator is Mr. Gale Wyatt, Grade I.
The facility (pipe 006) with the Imhoff tank is considered a Class II facility.

JMr. Howell
June 11, 2007
Page 3 of 3
The facility was well maintained by the staff, and they are considered to perform their jobs in an
outstanding manner. The equipment appeared to be in good operating order. The Imhoff tank showed
vigorous degassing at the sidewalls, which indicate that the system is well operated & maintained.
Process control tests of pH, ammonia, alkalinity, oil & grease are performed on the influent and
Imhoff tank. Process control tests appear to be successfully used in measuring plant performance.
Self -Monitoring Program
A review of the monthly self -monitoring reports from April 2006 through March 2007 did not show
any monitoring or limit violations.
Data verification was performed on November 2006 data. The lab data and the monitoring report
data were identical.
The grab samples, if required, are taken from the end of the pipe at all outfalls.
The composite sampler at Pipe 001 is time composite at 200 mL every 30 minutes.
The chain -of -custody reports were accurate and in good order.
Sludge Disposal
Sludge is removed from the plant by Cox Septic Service.
Mr. Howell continues to perform his job in an outstanding manner. Mr. Gale Wyatt performs the
plant Operations & Maintenance in an outstanding manner. The compliance evaluation inspection is
considered excellent. If you have any questions please contact George Smith at [phone].
Sincerely,
Steve W. Tedder
Regional Supervisor
cc: SWP Central Files
OWSRO Files

United States Environmental Protection Agency
Form Approved.
EPA Washington, D.C. 20460
OMB No. 2040-0057
Water Compliance Inspection Report
Approval expires8-31-98
Section A: National Data System Coding (i.e., PCS)
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type
1 I NI 2 151 31 NC0000019 111 121 07/05/10 117 181 CI 191 SI 201 1
Remarks
21IIII II IIIIIIIIII IIIIIIII IIIIIIIIIIII IIIIIIII III6
Inspection Work Days Facility Self -Monitoring Evaluation Rating B1 QA --------------------------- Reserved ----------------------
67I 169 70 15 I 711 DI 721 N I 73 W 74 751 I I I I I 1-1 80
Section B: Facility Data
Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include
Entry Time/Date
Permit Effective Date
POTW name and NPDES permit Number)
10:06 AM 07/05/10
07/01/01
United Chemi-Con, Inc.
Exit Time/Date
Permit Expiration Date
185 McNeil Rd
Lansing NC 28643
12:10 PM 07/05/10
11/03/31
Name(s) of Onsite Representative (s)/Titles(s)/Phone and Fax Number(s)
Other Facility Data
Gale Dean Howell/ORC/336-384-6917/
Name, Address of Responsible Official/Title/Phone and Fax Number
Contacted
Gale D Howell,185 McNeil Rd Lansing NC 28643//336-384-6917/ No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit Flow Measurement Operations & Maintenance Records/Reports
Self -Monitoring Program Sludge Handling Disposal Facility Site Review Effluent/Receiving Waters
Laboratory
Section D: Summary of Finding/Comments Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date
George S Smith WSRO WQ//336-771-5000/
Signature of Man ement Q A Revi Agency/Office/Phone and Fax Numbers Date
EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete.
Page # 1

NPDES yr/mo/day Inspection Type
JF3I NC0000019 I11 12I 07/05/10 I17 18ICI
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
Page # 2

Permit: NC0000019
Inspection Date: 05/10/2007
Owner - Facility: United Chemi-Con, Inc.
Inspection Type: Compliance Evaluation
Operations & Maintenance
Yes
No
NA
NE
Is the plant generally clean with acceptable housekeeping?
■
❑
❑
n
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable Solids, pH, DO, Sludge
■
n
n
n
Judge, and other that are applicable?
Comment:
Permit
Yes
No
NA
NE
(If the present permit expires in 6 months or less). Has the permittee submitted a new application?
n
n
■
n
Is the facility as described in the permit?
■
n
n
n
# Are there any special conditions for the permit?
n
■
n
n
Is access to the plant site restricted to the general public?
■
n
n
n
Is the inspector granted access to all areas for inspection?
■
n
n
n
Comment:
Record Keeping
Yes
No
NA
NE
Are records kept and maintained as required by the permit?
■
❑
❑
n
Is all required information readily available, complete and current?
■
n
n
n
Are all records maintained for 3 years (lab. reg. required 5 years)?
■
❑
n
Are analytical results consistent with data reported on DMRs?
■
n
n
n
Is the chain -of -custody complete?
■
n
n
n
Dates, times and location of sampling
■
Name of individual performing the sampling
■
Results of analysis and calibration
■
Dates of analysis
■
Name of person performing analyses
n
Transported COCs
■
Are DMRs complete: do they include all permit parameters?
■
n
❑
❑
Has the facility submitted its annual compliance report to users and DWQ?
n
n
■
n
(If the facility is = or > 5 MGD permitted flow) Do they operate 24/7 with a certified operator on each shift?
n
n
■
n
Is the ORC visitation log available and current?
■
n
n
n
Is the ORC certified at grade equal to or higher than the facility classification?
■
n
n
n
Is the backup operator certified at one grade less or greater than the facility classification?
■
n
n
n
Is a copy of the current NPDES permit available on site?
■
n
n
n
Page # 3

Permit: NC0000019 Owner - Facility: United Chemi-Con, Inc.
Inspection Date: 05/10/2007 Inspection Type: Compliance Evaluation
Record Keeping
Yes
No
NA
NE
Facility has copy of previous year's Annual Report on file for review?
n
n
■
n
Comment:
Flow Measurement - Effluent
Yes
No
NA
NE
# Is flow meter used for reporting?
■
n
n
n
Is flow meter calibrated annually?
■
n
n
n
Is the flow meter operational?
■
n
n
n
(If units are separated) Does the chart recorder match the flow meter?
■
n
n
n
Comment:
Disinfection -Tablet
Yes
No
NA
NE
Are tablet chlorinators operational?
n
n
■
n
Are the tablets the proper size and type?
n
n
■
n
Number of tubes in use?
Is the level of chlorine residual acceptable?
n
n
■
n
Is the contact chamber free of growth, or sludge buildup?
❑
n
■
n
Is there chlorine residual prior to de -chlorination?
n
n
■
n
Comment:
Sand Filters (Low rate)
Yes
No
NA
NE
(If pumps are used) Is an audible and visible alarm Present and operational?
❑
n
■
❑
Is the distribution box level and watertight?
■
n
n
n
Is sand filter free of ponding?
■
n
n
n
Is the sand filter effluent re -circulated at a valid ratio?
n
n
■
n
# Is the sand filter surface free of algae or excessive vegetation?
■
n
n
n
# Is the sand filter effluent re -circulated at a valid ratio? (Approximately 3 to 1)
n
n
■
n
Comment:
Page # 4

Mr. Hiroshi Ohashi
United Cheni-Con Manufacturing
185 McNeil Road
Lansing, North Carolina 28643
Dear Mr. Ohashi:
Michael F. Easley, Governor
State of North Carolina
William G. Ross, Jr., Secretary
Department of Environment and Natural Resources
Alan W. Klimek, P.E., Director
Division of Water Quality
September 13, 2006
SEP 14 20
Wins±on•S;;
Regional Ofrce
Subject: Draft NPDES Permit
Permit NC0000019
United Chemi-Con WWTP
Ashe County
Enclosed with this letter is a copy of the draft permit for your facility. Please review the draft very
carefully to ensure thorough understanding of the conditions and requirements it contains.
This draft has the following significant changes from your current permit:
• Quarterly monitoring for aluminum and butyrolactone has been removed from your permit due
to a lack of reasonable potential for levels of these pollutants to cause an exceedance of applicable
water quality standards.
• A total residual chlorine (TRC) limit has been added to this permit. The limit will take effect 18
months after the effective date of the final permit. See the attached TRC policy memo for details.
I have also enclosed application Form 1. Please fill out and return this brief addendum to your
application so that we have current contact information for your facility.
Please submit any comments to me no later than thirty days following your receipt of the draft.
Comments should be sent to the address listed at the bottom of this page. If no adverse comments are
received from the public or from you, this permit will likely be issued in two months.
If you have any questions or comments concerning this draft permit, please contact me at [phone] x
551 or via email at [e-mail].
Sincerely,
LeToya Fields
Western NPDES Program
cc: Winston-Salem Regional Office, Surface Water Protection
NPDES Unit
Aquatic Toxicology Unit
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] FAX [phone] NorthCarolina
512 N. Salisbury Street, Raleigh, North Carolina 27604 On the Internet at http://www.ncwaterquality.org ,%VlTfllCll��f
An Equal Opportunity/Affirmative Action Employer

C)F VV ATFR Michael F. Easley
Governor
p7 William G. Ross, Jr., Secretary
r NCDENR North Carolina Department of Environment and Natural Resources
p < Alan W. Klimek, P.E., Director
Division of Water Quality
June 19, 2003
TO: NPDES Unit Staff �/�
FROM: David A. Goodrich Vc'(
NPDES Unlit Supervisor
SUBJECT: Total Residual Chlorine Policy for NPDES permits
Every three years the State is required by the Clean Water Act to review its surface water quality standards and
classifications, determine if changes arc needed and to make any necessary changes. This review process is referred to
as the "triennial review." Public hearings were held to solicit comments for the 2000-2003 Triennial Review of surface
cater quality standards during the summer of 2002. The Hearing Officer's recommendations were presented before
the state's Environmental Management Commission on October 10, 2002.
The Hearing Officer's recommended changes included modifications to the existing standards for Arsenic, Cyanide,
Methylene Blue Active Substances (MBAS) and Total Residual Chlorine (TRC). The Hearing Officer also
recommended the addition of a standard for Methyl Tert-Butyl Ether (MTBE).
All of the Hearing Officer's proposed changes were adopted with the exception of NME. The changes took effect
on April 1, 2003. This memo documents the changes to the NPDES permitting policy for TRC limits.
Total Residual Chlorine (TRC)
Previously, TRC had an Action Level Standard, except in designated Trout waters. The Triennial Review changes
modified the TRC Action Level Standard to an Aquatic Life Standard of 17 µg/L The Aquatic Life Standard will
remain for designated Trout waters.
Aquatic Life Standard — 17 µg/L (freshwater only)
Trout Waters — 17 µg/L
Revised TRC Policy
➢ TRC limits will be assigned to permit renewals and all new permits issued after April 1, 2003.
➢ Facilities that do not use chlorine will not receive a TRC limit; however, the presence of a chlorine back-up
system to augment UV or other disinfection requires a TRC Emit.
➢ Facilities discharging to streams with a 7Q10 <0.05 cfs (zero -flow streams) will receive a limit of 17 µg/L.
➢ Limits will be capped at 28 µg/L to protect against acute impacts.
It is likely that many facilities will need to add dechlorination (or use another means of disinfection) to comply with
the new TRC standard. Therefore, a compliance schedule of 18 months from the effective date of the permit may
be added to any TRC limit added during the current permit renewal. This time period is allowed in order for the
facility to budget and design/construct the dechlorination and/or alternative disinfection system(s). The NPDES
Unit has promulgated minimum design criteria in order to expedite permitting of dechlorination equipment.
cc: Coleen Sullins
Regional Office Supervisors (Dechlorination guidance attached)
— - Shannon Langley

EPA FORM 3510-1 (8-90) CONTINUED ON REVERSE

EPA FORM 3510-1 (8-90)

Permit NC0000019
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
United Chemi-Con Manufacturing, Incorporated
is hereby authorized to discharge wastewater from a facility located at the
end of NCSR 1659
south of Lansing
Ashe County
to receiving waters designated as North Fork New River in the New River Basin in
accordance with effluent limitations, monitoring requirements, and other conditions set forth
in Parts I, II, III and IV hereof.
This permit shall become effective.
This permit and authorization, to discharge shall expire at midnight on March 31, 2011.
Signed this day.
DRAFT
Alan W. Klimek, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

SUPPLEMENT TO PERMIT COVER SHEET
"q4 Permit NC000001
All previous NPDES Permits issued to this facility, whether for operation or discharge are hereby revoked. As of this permit
issuance, any previously issued permit bearing this number is no longer effective. Therefore, the exclusive authority to
operate and discharge from this facility arises under the permit conditions, requirements, terms, and provisions included
herein.
United Chemi-Con Manufacturing, Incorporated is hereby authorized to:
1. Continue to discharge the following:
o Non -contact cooling water, A/C condensate, boiler blowdown, deionizer
backwash, assembled product wash water and process wastewater from outfall
001;
o A/C condensate from outfall 003;
o Domestic wastewater from outfall 006;
o Non -contact cooling water and filtered surface water (during maintenance
periods only) from outfall 007;
From a facility located at United Chemi-Con Manufacturing at the end of NCSR 1659,
south of Lansing, Ashe County, and
2. Discharge from said treatment works at the location specified on the attached map
into the North Fork New River which is classified C+ waters in the New River Basin.

"'N
Permit NC0000019
A. (1.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
During the period beginning on the effective date of this permit and lasting until expiration, the Permittee is
authorized to discharge from outfall 001: non -contact cooling water, boiler blowdown, deionization
regeneration water, A/C condensate, and process wastewater. Such discharges shall be limited and monitored
by the Permittee as specified below:
EFFLUENT �
LIIVITT5
MOIVITQRING REQUIREMENTS
...�
+IARACTERI'STICS
f
Mdith1y
iall
asu
Merement
Samle
Sample Local ion:
h..:. .. .....
Avra e
Maximum;,
_..
:',,Frequency.
,
Flow
0.2 MGD
Continuous
Recording
Influent or Effluent
Temperature2
Weekly
Grab
Effluent, Upstream and
Downstream
pH3
2/Month
Grab
Effluent
Total Suspended Solids
Monthly
Composite
Effluent
Oil and Grease
26.0 mg/L
52.0 mg/L
Monthly
Grab
Effluent
BOD5
Monthly
Composite
Effluent
Total Residual Chlorine¢
28 Pg/L
Monthly
Grab
Effluent
Total Toxic Organics5
Quarterly
Grab
Effluent
Total Zinc
Quarterly
Composite
Effluent
Total Copper
Quarterly
Composite
Effluent
Chronic Toxicity6
Quarterly
Composite
Effluent
Footnotes:
1. Sample Locations: Upstream = Upstream at least 100 feet; Downstream = Downstream at least 300 feet.
2. The temperature of the effluent shall not cause an increase in the temperature of the receiving stream of
more than 2.8°C and in no case cause the ambient water temperature in the receiving stream to exceed 29°C.
3. The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units.
4. Limit and monitoring requirement apply only if chlorine is added to the cooling water or any other
wastewater contributor. Limit will take effect 18 months after the effective date of the final permit.
5. In lieu of monitoring for Total Toxic Organics, the permittee may submit the following statement: 'Based on
my inquiry of the person or persons directly responsible for managing compliance with the permit
limitation for total toxic organics, I certify that, to the best of my knowledge and belief, no dumping of
concentrated toxic organics into the wastewater has occurred since the filing of the last discharge report."
6. Chronic Toxicity (Ceriodaphnia) Quarterly, NOEC limit Q 0.75% See A.(5).
There shall be no discharge of floating solids or visible foam in other than trace amounts.

PPPPPPP'
Permit NC0000019
A. (2.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
During the period beginning on the effective date of this permit and lasting until expiration, the Permittee is
authorized to discharge from outfall 003: A/C condensate. Such discharges shall be limited and monitored by
the Permittee as specified below:
EFFLUENT
LIMITS
MONITORING REQUIREMENTS
GLIAR CTER TICS
e
Monthly
Daily
Measurement
SampleType
Sample Lorahoni.:
..
AVera a . :.Max
M'
F i uene N�
p
Flow
Not limited
Monthly
Instantaneous
Influent or Effluent
Temperature2
Monthly
Grab
Effluent, Upstream
and Downstream
Total Residual Chlorine3
28 pg/L
Monthly
Grab
Effluent
pH4
2/Month
Grab
Effluent
Footnotes:
1. Sample Locations: Upstream = Upstream at least 100 feet; Downstream = Downstream at least 300 feet.
2. The temperature of the effluent shall not cause an increase in the temperature of the receiving stream of
more than 2.8°C and in no case cause the ambient water temperature in the receiving stream to exceed 29°C.
3. Limit and monitoring requirement apply only if chlorine is added to the cooling water or any other
wastewater contributor. Limit takes effect 18 months after the effective date of the final permit.
4. The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units.
There shall be no discharge of floating solids or visible foam in other than trace amounts.
There shall be no chromium, zinc or copper added to the treatment system except as a pre -approved
additive to biocidal compounds (See A.(6.)).
A. (3.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
During the period beginning on the effective date of this permit and lasting until expiration, the Permittee is --- -
authorized to discharge from outfall 006: domestic wastewater. Such discharges shall be limited and monitored
by the Permittee as specified below:
EFFLUENT :
LIMITS.
-
MONITORING
REQUIREMENTS
CHARAC7'ERISTIS ..
1Vlonthly
Daily _'
Measurement
Sample.Type
Sample Location
Avers e.
Maximum;,!
Frei uenc"
Flow
0.018 MGD
Weekly
Instantaneous
went or
Effluent
BODs, 200C
30.0 mg/L
45.0 mg/L
2/Month
Grab
Effluent
Total Suspended Residue
30.0 mg/L
45.0 mg/L
2/Month
Grab
Effluent
Temperature
Weekly
Grab
Effluent
NH3 as N
Monthly
Grab
Effluent
PH'
2/Month
Grab
Effluent
Footnotes:
1. The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units.
See Part A(7.), Disinfection Condition.
There shall be no discharge of floating solids or visible foam in other than trace amounts.

qq
Permit NC0000019
A. (4.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
During the period beginning on the effective date of this permit and lasting until expiration, the Permittee is
authorized to discharge from outfall 007: recycled non -contact cooling water and filtered surface water. Such
discharges shall be limited and monitored by the Permittee as specified below:
EFFLUENT
LIMITS -`"
MONITORING REQUIREMENTS
CHARACTERISTICS
Mon#h1y
Daily
Measurement
Sample Type
Sample Locationx "
Aveza a
imuni
Fre uen
Flow
Not limited
Monthly
Instantaneous
Influent or Effluent
Temperature2
Monthly
Grab
Effluent, Upstream
and Downstream
Total Residual Chlorine3
28 pg/L
Monthly
Grab
Effluent
Settleable Solids
Monthly
Grab
Effluent
pH4
2/Month
Grab
Effluent
Footnotes:
1. Sample Locations: Upstream = Upstream at least 100 feet; Downstream = Downstream at least 300 feet.
2. The temperature of the effluent shall not cause an increase in the temperature of the receiving stream of more than
2.80C and in no case cause the ambient water temperature in the receiving stream to exceed 290C.
3. Limit and monitoring requirement applies only if chlorine is added to the cooling water or any other wastewater
contributor. Limit takes effect 18 months after the effective date of the final permit.
4. The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units.
Monitoring shall be performed only if discharge occurs.
There shall be no discharge of floating solids or visible foam in other than trace amounts.
There shall be no chromium, zinc or copper added to the treatment system except as apre-approved
additive to biocidal compounds (See A.K)).

Permit NC0000019
CHRONIC TOXICITY PERMIT LIMIT (QRTRLY)
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to
Ceriodaphnia dubia at an effluent concentration of 0.75%%
The permit holder shall perform at a minimum, quarterly monitoring using test procedures outlined in the
"North Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or subsequent
versions or "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998)
or subsequent versions. The tests will be performed during the months of January, April, July and October.
Effluent sampling for this testing shall be performed at the NPDES permitted final effluent discharge below all
treatment processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV below the permit
limit, then multiple -concentration testing shall be performed at a minimum, in each of the two following months
as described in "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February
1998) or subsequent versions.
The chronic value for multiple concentration tests will be determined using the geometric mean of the highest
concentration having no detectable impairment of reproduction or survival and the lowest concentration that
does have a detectable impairment of reproduction or survival. The definition of "detectable impairment,"
collection methods, exposure regimes, and further statistical methods are specified in the "North Carolina Phase
II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the months in which tests were performed, using the parameter code TGP3B for
the pass/fail results and THP3B for the Chronic Value. Additionally, DWQ Form AT-3 (original) is to be sent to
the following address:
Attention: North Carolina Division of Water Quality
Environmental Sciences Section
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
_ Completed Aquatic Toxicity Test -Forms shall be filed with the Environmental Sciences Section no later than 30__
days after the end of the reporting period for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all
concentration/response data, and be certified 6y laboratory supervisor and ORC or approved designate
signature. Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is
employed for disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required,
the permittee will complete the information located at the top of the aquatic toxicity (AT) test form indicating
the facility name, permit number, pipe number, county, and the month/year of the report with the notation of
"No Flow" in the comment area of the form. The report shall be submitted to the Environmental Sciences
Section at the address cited above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be
required during the following month.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of
Water Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to
include alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism
survival, minimum control organism reproduction, and appropriate environmental controls, shall constitute an
invalid test and will require immediate follow-up testing to be completed no later than the last day of the month
following the month of the initial monitoring.

Permit NC000001
A.K) BIOCIDE CONDITION
The permittee shall not use any biocides except those approved in conjunction with the permit
application. The permittee shall notify the Director in writing not later than ninety (90) days prior to instituting
use of any additional biocide used in cooling systems which may be toxic to aquatic life other than those
previously reported to the Division of Water Quality. Such notification shall include completion of Biocide
Worksheet Form 101 and a map locating the discharge point and receiving stream.
A.M) DISINFECTION CONDITION
In the event that violations of the fecal coliform requirements of the North Carolina water quality standards
occur as a result of this discharge, disinfection will immediately be required and the permit amended to
establish a coliform effluent limitation.

ppppwpr, -
NCDENR/DWQ
FACT SHEET FOR NPDES PERMIT DEVELOPMENT
United Chemi-Con Manufacturing
NC0000019
Al.) Facility Name`_
United Ch_emi-Con
(2.) Permitted Flow MGD):
0.218
_
(6.) County:
Ashe
(3.) Facility Class:
I
(7.) Regional Office:
Winston-Salem
(4.) Pretreatment Program:
N/A
(8.) USGS To o Quad:
B12NE
(5.) Permit Status:
_
Existin /renewal
(9.) USGS Quad Name:
Warrensville
(1.) Receiving Stream:
North Fork New
(7.) Drainage Area (mi2):
142
River
(2.) Sub -basin:
05-07-02
(8.) Summer 7Q10 (cfs):
41
(3.) Stream Assessment Unit:
10-2-(12)
(9.) Winter 7Q10 (cfs):
56
(4.) Stream Classification:
C+
(10.) 30Q2 (cfs):
79
(5.) 303(d) Status:
_
Not listed
(11.) Average Flow (cfs):
240
(6.) 305(b) Status:
1
1 (12.) IWC %:
0.75
I. Proposed Changes Incorporated into Permit Renewal
• Remove aluminum and butyrolactone monitoring.
• Add TRC limit with compliance schedule.
II. Summary
United Chemi-Con is a manufacturer of aluminum electrolytic capacitators, an industrial
function not specified in the 40 CFR. Four outfalls discharge wastewater from the site.
o Outfall 001 regularly discharges a combined flow of non -contact cooling water, A/C
condensate, boiler blowdown, deionizer backwash, and stormwater. The facility also has
the ability to discharge assembled -product washwater and process wastewater, however
according to the 11/2005 staff report, the facility hauls away all process wastewater.
o Outfall 003 discharges A/C condensate intermittently.
o Outfall 006 discharges domestic wastewater on a fairly regular basis. A kitchen, which
has grease traps, also discharges into this system.
o Outfall 007 discharges non -contact cooling water and filtered surface water once a year
during maintenance. Sludge is hauled off -site.
III. Compliance Summary
DMR Data Review
DMRs were reviewed for the period of January 2003 through June 2006. Summaries of monthly
average DMR data for outfalls 001 and 006 are included in Tables 1 and 2, respectively. During
this time there was no recorded discharge from outfalls 003 and 007.

NPDES Permit Fact Sheet - 08/31 /06
Page 2
Table 1: Monthly Average DMR Data Summary For Outfall 001
United Chemi Conqqq
Mfg
' NC0000019
Flow
emp
TRC
Bp!?,
pH
TSS
O&�G
0
l (de Cl . ..
... -
im ` )
: ;{s.u.)
fm.� :..1
(
Avg
0.06
31.66
6.05
5.56
6.53
2.36
3.65
Max
0.10
40.00
13.40
48.00
7.15
7.00
13.40
Min
0.0004
22.25
0.00
0.00
6.14
0.00
0.00
Table 2: Monthly Average DMR Data Summary For Outfall 006
Flpw
Temp
NH3
BOD:
pH;
TSS'.
�-
u
i1 G��.."
4( CJ:..
lair }._-:
- frn ` L) .
(s.u.) m
(in ,� )
Avg
0.0009
15.1232
2.8500
5.0172
6.4573
3.3810
Max
0.0220
39.0000
40.5000
23.5000
6.8260
12.0000
Min
0.0000
3.7500
0.0000
0.0000
6.2100
0.0000
Instream Data Review
Instream temperature data was reviewed for May 2004- June 2006. There was no difference
between values reported at upstream and downstream sites.
RPA Analysis
RPAs were performed for copper, zinc, aluminum, and butrolactone. Aluminum monitoring will
be removed due to the lack of reasonable potential for the levels present to cause an exceedance
of EPA criteria (there are no NC standards for Al). Butrolactone monitoring will also be removed
since no detections were noted during the entire review period. Quarterly monitoring for copper
and zinc will remain. Reported levels were higher than the acute criteria, however monitoring
will not be increased since the facility consistently passes its WET tests.
WET Test Results
United Chemic Con has a chronic whole effluent toxicity (WET) testing requirement at 0.75%
effluent concentration. The facility has passed 18/18 tests administered since January 2002.
Correspondence File Review/Compliance History
There were no limit violations during the reviev .)eriod. Staff reports note that the facility is well
operated and maintained.
IV. Pro]2osed Schedule for Permit Issuance
Draft Permit to Public Notice: September 13, 2006
Permit Scheduled to Issue: November 13, 2006
V. State Contact Information
If you have any questions on any of the above information or on the attached permit, please
contact Toya Fields at [phone], extension 551.
Copies of the following are attached to provide further information on the permit development:

NPDES Permit Fact Sheet - 08/31/06
Page 3
Draft permit
RPA Summary including copper and zinc limit calculation
NPDES Recommendation by:
Signature Date
Regional Office Comments:
Regional Recommendation by:
Signature Date
Regional Supervisor:
Signature Date
United Chemi Con Mfg
NC0000019

REASONABLE POTENTIAL ANALYSIS
United Chem! -Con
NC0000019
Time Period 0
Ow (MGD) 0.2
701OS (c1s) 41
701OW (ds) 56
3002 (ds) 79
Avg. Stream Flow, OA (c1s) 240
Reeving Stream North Fork New River
WWTP Class IV
IWC (%) 0 7010S 0.7504
0 701OW 0.5505
0 3002 0.3909
Q OA 0.129
Stream Class C+
Outfall 001
Ow = 0.2 MGD
STANDARDS"
PARAMETER
TYPE
CRITERIA (2)
POL
Units
REASONABLE POTENTIALRESULTS
RECOMMENDED ACTION
(1)
NCWQS/ HFAY/
s tinHIMt LProd Qr Abwdk Cw
'
Chrome Acub
-
Acute: 7
Max preWcted>acute allowable
Copper
NC
7 AL 7.3
ug/L
8 7 126.0
_
Action level parameter.' AetairIORT_RLYmoMoring _
Note: n<12
_ _ _
Chronic: 933
Limited data set
Acute: 67
Max predicted > acute:eibwabie
Zinc
NC
50.0 AL 67
uglL
8 5 1708.6
Action level parameter: Retain ORTRLY monitoring
Note: n<12
Chronic: 6,663—
Limiled date set
Acute: WA
Aluminum
NC
87
ug/L
8 5 4108.8
Note: n<12
...................................
Chronic: 11,593
----------
Max predcted > acute aMewabie (EPA criteria)
Limited data set
Remove monitoring
Acute: WA
Butryolaetone
6 4 727.3
_ _ _ _ _
_ _ _ — — — — — — — ---
Note: n<12
Chronic::rtor 0 T
Remove monitoring_—
Limited dote set
Acute: WA
0 0
WA
— — — — — — — — — — — — —
_ _ _
Chronic::rtor 0 Type.—
—
Acute: WA
0 0
WA
— — — — _ — _ — —
_ _ ......
C...hroniErtor 0 Type.
_— _ _ —_— —
Acute: WA
0 0
WA
_ _ _ _
Chronic::rror 0 Type "—------- — — — ----- --- — --
Acute: WA
0 0
WA
— — — —
•
Chronic: Ertor 0 Type.'—
— — — — - - — — --
Acute: WA
Chronic: :rtor 0 Type.;
-- — — --- --- — ----- — — — —
Acute: WA
0 0
WA
Chronic::rror 0Type.
Acute: WA
0 0
WA
..........
Chronic::rror ._Type
_—_— —_—_— — — — — — — — —_— —
Acute: WA
0 0
WA
_ _
Chronic::rror 0 Type
;.._— — — ——_—_—_—_—_—_— — —_— 7—
Acute: WA
0 0
WA
............
..Chronic::rror 0 Type'
................... — — ---
Acute: WA
0 0
WA
-------------- — — --- ------
_ ____
Chronic:..
hr... 0 Type
:rrorAcute:
—
WA
0 0
WA
_ _ _ _
Chronic: Type.-------------------------------- Error 0
Legend: " Freshwater Discharge
C = Carcinogenic
NC = Non -carcinogenic
A = Aesthetic
00019rpa.x1s, rpa
6/31/2006

pppppp� -
REASONABLE POTENTIAL ANALYSIS
Copper
Zinc
Date Data BDL_112DL
Results
Date Data
BDL=1/2DL
Results
1
Jul-20 ': 19.0 19.0
Std Dev.
14.5308
1 '
10
5.0
Std Dev.
68.0688
2
Jan 2006, 8.0 8.0
Mean
25.0000
2 >
10
5.0
Mean
50.7500
3
Oc4-2005 25"-6' 25.0
C.V.
0.5812
3
10'
5.0
C.V.
1.3413
4
Sep-200S 33.0: 33.0
n
8
4 `i
11
11.0
n
8
5
Sep-200'4 39.0' 39.0
5
89
189.0
6
'4r--2004, 39.0' 39.0
MultFactor=
3.2300
6
70'
70.0
Mull Factor =
9.0400
,
7
. Mar=2004 '• 2.0: 1.0
Max. Value
39.0 ug/L
7
110
110.0
Max. Value
189.0 ug/L
8
Jun-2005=� 36.0 36.0
Max. Pred Cw
126.0 ug/L
8
- ' 11
11.0
Max. Pred Cw
1708.6 ug/L
9
9 1
10
10
11.
11
12
12
13 ,.
13
14 .
-
14
15
15
16
16
17
17
18
18 ,
19
19
20
20
00019rpa.xls, data
1 8/31/2006

REASONABLE POTENTIAL ANALYSIS
3
4
Aluminum
Butryolactone
Date Data
BDL=1/2DL
Results
Date Data
BDL=1/2DL
Results
1
17
, 17.0
Std Dev.
188.4506
1 Apr-2006
50 25.0
Std Dev.
10.2062
2
63-
63.0
Mean
146.2500
2
Mean
4.1667
3
10
5.0
C.V.
1.2886
3
0 0.0
C.V.
2.4495
4
0
0.0
n
8
4
n
6
5
500
" 250.0
5
00.0
6 ,
.' 350-
350.0
Mult Factor =
8.5600
6
0 0.0
Mult Factor =
29.0900
7
486
480.0
Max. Value
480.0 ug/L
7
0 0.0
Max. Value
25.0 0
8
10
5.0
Max. Pred Cw
4108.8 ug/L
8
0 0.0
Max. Pred Cw
727.3 0
9
9
10
10
11
11
12
12
13
13
14
14
15
15
16
16
17
17 ,
18
18
19
19
20
20
00019rpa.)ds, data
-2- 8/31/2006

Whole Effluent Toxicity Testing Self -Monitoring Summary August 15, 2006
FACILITY REQUIREMENT
YEAR JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG_
SEP
OCT
NO_ V
DEC_
UNC-Chapel HID Power Plant 24hr ac monit epic fthd
Fthd24Ac
2002 H
H
H
H
H
—
H
H
H
H
H
H
NC0025305/001 Begin:9/1/2001 Frequency: 5OWD/A
NonCornp:
2003 H
H
H
H
H
H
—
H
H
H
H
H
County: Orange Region: RRO Subbain: CPF06
2004 H
H
H
H
H
H
H
H
H
H
H
H
PF: 0.048 Special
2006 H
H
H
H
H
H
H
11
H
H
H
H
7Q10: 0.0 IWC(°/a) 100 Order:
2006 H
H
H
H
H
H
UniB-Kinston LLC CHR LIM: 1.9%
Ceti7dPF
2002 Late
Pass
—
Paw
—
—
NR
Paw
—
Pau
—
—
NC0003760/001 Begin:4/12003 Frequency: Q Jan Apr Jul Oct
+ NonComp:SINGLE
2003 Paw
—
—
Pau
—
—
Pan
—
—
Pau
—
—
County. Lenoir Region: WARO Subbain: NEU05
2004 Pau
—
—
Pau
—
—
Pass
—
—
Pau
—
—
PF: 3.6 Special
2005 Pau
—
—
Pass
—
—
Pus
—
—
Pass
—
—
7QIO: 283.1 IWC(%) 1.9 order:
2006 Pau
—
—
Pau
—
—
Unimin Corp -Min Operations (001) chr lim: WK
Ceri7dPF
2002 —
late
Pau
—
Pus
—
—
Pau
—
—
Pau
—
NC0000361/001 Begin:g/1/2004 Frequency:Q Feb May Aug Nov
+ NonComp:Single
2003 —
Pass
—
—
Pass
—
—
Pass
—
—
Pau
—
County: Avery Region: ARO Subbasin: FRB06
2004 —
Pas
—
—
late
Pass
—
Pass
—
—
Pau
—
PF: 2.16 Special
2005 —
Pus
—
—
Pass
—
—
Pass
—
—
Pau
—
7Q10: 30 IWC(*/.) 10 Order:
2006 —
Pas
—
—
Pass
—
Unim)n Corp. chr lim: I 1 %
Ceri7dPF
4 2002 Pass
—
—
Pass
—
—
Pass
—
—
Fag
>44
>44
NC00001751001 Begin:8/1/2004 Frequency.Q Jan Apr Jul Oct
+ NonComp:Single
2003 Pau
—
—
Fag
<5.5
e5.5,6.6,>44
Pass
—
—
Pau
—
—
County: Mitchell Region: ARO Subbain: FRB06
2DO4 Pau
—
—
Pass
—
—
Pau
—
—
Pau
—
—
PF: 3.61 Special
ZOOS pon,Pan
—
—
Pau
—
—
Pau
—
—
Pau
—
—
7QI0: 45.0 IWC(%) I I Order:
2006 Pun
—
—
Pau
—
—
Unlmin Corp. Red Hill Plant chr lim: 1.2%
Ceri7dPF
2002 Paw
—
—
Pau
—
—
Pau
—
—
Pass
—
—
NCO085839/001 Begin:5/1/2004 Frequency:Q Jan Apr Jul Oct
+ NonCcmp:Single
20D3 Pass
—
—
Pau
—
—
Pass
—
—
Pau
—
—
County: Mitchell Region: ARO Subbain: FRB06
2004 Fag
>4.8
>4.8
Pau
—
—
Pas
—
—
Pass
—
—
PF: 0.682 Special
2DD5 pan
—
—
Pass
—
—
Pau
—
—
pan
—
—
7Q10: 90.7 IWC(%) 1.2 Order:
2006 Pass
—
—
Pau
—
—
Pus
Unimin Corp. -Crystal Operation chr lim: 1.3%
Ceri7dPF
2002 N
—
—
N
—
—
N
—
—
N
—
—
NCO084620/001 Begin:5/1/2004 Frequency:Q Jan Apr Jul Oct
+ NonComp:Single
20D3 N
—
—
N
—
—
N
—
—
N
—
—
County: Mitchell Region: ARO Subbain: FRB06
20D4 N
—
—
N
—
—
H
—
—
H
—
—
PF: 0.36 Specul
2005 H
—
—
H
—
—
H
—
—
H
—
—
7Q10: 41 IWC(%) 1.3 Order:
2DD6 H
—
—
H
—
—
Union County -Six Mile Creek chr lim: 90%
Ceri7dPF
2002 —
H
—
—
H
—
—
H
—
—
H
—
NCO066559/001 Begin: 12/1/1996 Frequency: QP/F + Feb May Aug Nov
NonComp:Single
20D3 —
H
—
—
H
—
—
H
—
—
H
—
County: Union Region: MRO Subbain: CTB38
2D04 —
H
—
—
H
—
—
H
—
—
—
—
PF: 1.0 Speei.1
2DD5 —
H
—
—
H
—
—
H
—
—
H
—
7Q10: 0.0 IWC(e/.) 100 Order
2006 —
H
—
—
H
—
Union County -Twelve Mile Creek W WTP chr lim: 90%
Ceri7dPF
2002 —
Fag
67.1
>1DD
Pus
—
—
Pau
—
—
Pau
—
NCO085359/001 Begin: 11/12005 Frequency:Q Feb May Aug Nov
+ NonComp:Single
2003 —
Pus
—
—
Pass
—
—
Pass
—
—
Pass
—
Coun[y Union Region: MRO Subbain: CTB38
2D04 —
Pass>1Do(p)
—
—
Pus,92.5(P) —
—
Pass,97.5(P) —
—
Psss,>100(P) —
PF: 2.5 Special
2OD5 —
Pus
—
—
Post
—
—
Pan
—
—
Pan
—
7QI0: 0.0 IWC(%) 100 Order:
2006 —
Pas
—
—
Pus
—
United Chemi-Coo chr lim: 0.75%
Ceri7dPF
2002 Pon
—
—
Pau
—
—
Pau
—
—
Pau
—
—
NC0000019/001 Begin:4/12001 Frequency: Q Jan Apr Jul Oct
+ NonComp:Single
2DD3 Pan
—
—
Pan
—
—
Pan
—
—
paps
—
—
County: Ashe Region: WSRO Subbmin:NEW02
2DD4 Pass
—
—
Pass
—
—
Pass
—
—
Pap
—
—
PF: 0.2 5peei.1
2005 Pau
—
—
Pus
—
—
Pau
—
— -
Pass
—
—
7Q10:41.0 IWC(%)0.75 Order:
2006 Pna
—
—
Pass
—
—
Unocal Corp-Rhom and Ham Facility chr lim: 90%
Ceri7dPF
2002 Fag
>10D
>100
Pan
—
—
Pass
—
—
Pau
—
—
NCO085057/001 Begin:12112005 Frequency. Q Jan Apr Jul Oct
+ NonComp:Single
2003 Pan
—
—
Pan
—
—
Pau
—
—
pass
—
—
County: Mecklenburg Region: MRO Subbain: CTB34
2004 NRIH
—
—
H
—
—
H
—
—
H
—
—
PF: 0.0432 Special
2005 H
—
—
NRIH
—
—
H
-_
-
H
—
—
7Q10: 0.0 IWC(%) 100 Order:
200E H
—
—
NRIH
—
—
USMC Camp Lejeune Hadnot Pt W WTP 001 chr lim: 5%
Mysd7dPF
2002 Pass
—
—
Pan
—
—
pass
—
—
Pass
—
—
NCO063029/001 Begin:1/12003 Frequency:Q + Jan Apr Jul Oct
NonComp:Single
2003 Pau
—
—
Pau
—
—
Pau
—
--
.Page
—
—
County: Onalow Region: WIRO Subbain: WOKO:
20D4 Late
Pus
—
Pau
—
—
Pau
—
—
Pau
—
—
PF: 8.0 Speei.l
2005 pan
—
—
Pan
—
—
Pass
—
—
Pan
—
—
7Q10: TIDAL IWC(%)NA Order:
20D8 Pan
—
—
Pan
—
—
Y Pre 2002 Data Available
LEGEND:
PERM — Permit Requirement LET = Administrative Letter -Target Frequency = Monitoring frequency: Q- Quarterly; M- Monthly; BM- Bimonthly; SA- Semiannually; A- Annually; OWD- Only when discharging; D. Discontinued monitoring requirement
Begin = First month required 7Q I O = Receiving stream low Bow criterion (e(s) += quarterly monitoring increases to monthly upon failure or NR Months that testing mat occur -ex. Jan, Apr, Jul, Oct NonComp = Current Compliance Requirement
PF = Permitted glow (MGD) IWC*/. = Instream waste concentration P/F = Pass(Fail test AC = Acute CHR = Chronic
Data Notation: f - Fathead Minnow; a - Ceriodaphnia sp.; my - Mysid shrimp; ChV - Chronic value; P - Mortality of stated percentage at highest concentration; at - Performed by DWQ Aquatic Tox Unit; bt - Bad test
Reporting Notation: --- = Data not required; NR - Not reported Facility Activity Status: I - Inactive, N -Newly Issued(To construct); H -Active but not discharging; t-More data available for month in question; = ORC signature needed
44

NEW RIVER BASIN
Name of Stream Subbasin Stream Index Number Map Number Class
Little Windfall Branch
NEW02
10-2-21-5
Al2SE5
C;Tr:+
Long Branch
NEW01
10-1-36-1
B13NE1
B;Tr:+
Long Branch
NEW02
10-2-21-8-3
B12NE3
C:+
Long Branch
NEW02
10-2-27-4-3
A13SW5
C:+
Long Hope Creek
NEW02
10-2-13-3
B12SW3
C;Tr:+
Long Shoals Creek
NEW02
10-2-25
B13NW2
C;Tr:+
Lost Branch
NEW02
10-2-27-2
Al2SE6
C;Tr:+
Maine Branch
NEW02
10-2-3
B12SW2
C;Tr:+
Maple Branch
NEW01
10-1-37-3-1
B14NW4
B;Tr:+
Matney Branch
NEW01
10-1-3-6
C12NW6
WS-IV;Tr:+
Meadow Creek
NEW01
10-1-17
B12SEB
C:+
Meadow Fork
NEW01
10-1-37-2
B14NW7
B;Tr:+
Meat Camp Creek
NEW01
10-1-10
B12SW5
C;Tr:+
Middle Fork Little Horse Creek
NEW02
10-2-21-8-1
Al2SW9
C;Tr:+
Middle Fork South Fork New River
NEW01
10-1-2-(6)
C12NW9
WS-IV;Tr:+
Middle Fork South Fork New River
NEW01
10-1-2-(14)
C12NW6
WS-IV:+
Middle Fork South Fork New River
NEW01
10-1-2-(15)
C12NW6
WS-IV;CA:+
Middle Fork South Fork New River (Chetola Lake)
NEW01
10-1-2-(1)
C12NWB
WS-IV:+
Mill Creek
NEW02
10-2-17
B12NE1
C;Tr:+
Mill Creek (Grassy Creek)
NEW01
10-1-18
B12SE5
C;Tr:+
Millpond Branch
NEW02
10-2-28
B13NW3
C:+
Mine Branch
NEW02
10-2-2
B12SW2
C;Tr:+
Moccasin Creek
NEW03
10-9-11
A14SE5
C
Monkey Branch
NEW02
10-2-9-1
B12NW5
C;Tr:+
Moore Branch
NEW01
10-1-2-9
C12NW9
WS-IV;Tr:+
Moretz Branch
NEW01
10-1-9-3
B12SW7
WS-II;Tr,HQW
Mud Creek (Mud Fork)
NEW02
10-2-21-4
Al2SE2
C;HQW
Mutton Creek (Rocky Knob Creek)
NEW01
10-1-6
C12NE4
C;Tr:+
Naked Creek
NEW01
10-1-32
B13NW4
C:+
Nathans Creek
NEW01
10-1-36
B13NW3
B;Tr:+
NEW RIVER (North Carolina Portion)
NEW01
10
A14SW5
C;ORW
NEW RIVER (North Carolina Portion)
NEW02
10
A14SW5
C;ORW
NEW RIVER (North Carolina Portion)
NEW03
10
A14SW5
C;ORW
No Head Branch
NEW03
10-9-5-1
B14NW6
C;Tr
Norris Branch
NEW01
10-1-9-7-(2)
C12NW2
C;Tr:+
Norris Branch, including the raw water holding
NEW01
10-1-9-7-(1)
C12NW2
WS-II;Tr,HQW,CA
reservoir below normal reservoir elevation
Norris Fork
NEW01
10-1-10-2
B12SWS
C;Tr:+
North Fork New River
NEW02
10-2-(1)
B12SW2
C;Tr:+
North Fork New River
NEW01
10-2-(12)
B12NE4
C:+
North Fork New River
NEW02
10-2-(12)
B12NE4
C:+
Obids Creek
NEW01
10-1-27-(1)
B13SW3
C;Tr:+
Obids Creek
NEW01
10-1-27-(2)
B13SW6
WS-IV;Tr:+
Old Field Branch (Grass Branch)
NEW02
10-2-21-9
Al2SE9
C;Tr:+
Old Field Creek
NEW01
10-1-22-(0.3)
B12SE3
C;Tr:+
Old Field Creek
NEW01
10-1-22-(0.7)
B12SE6
C;Tr,ORW
Old Field Creek
NEW02
10-2-26
A13SW8
C:+
Ore Knob Branch
NEW01
10-1-35-3
B13NEB
B;Tr:+
Payne Branch
NEW01
10-1-2-13
C12NW6
WS-IV;Tr:+
Peak Creek
NEW01
10-1-35-(l)
B13SE3
C;Tr:+
Peak Creek
NEW01
10-1-35-(2)
B13SE3
B;Tr:+
Penley Branch
NEW01
10-1-2-4
C12NW8
WS-IV:+
Perkins Branch
NEW01
10-1-5-1
C12NW3
C:+
Pine Branch
NEW01
10-1-13-1
C12NE2
C:+
Page 3 of 5

NC DENR - DIVISON OF WATER QUALITY
.0307 NEW RIVER BASIN
2B .0300
Classification
Name of Stream
Description
Class
Date
Index No.
North Fork New River
From Three
Top
Creek to New
C:+
02/01/93
10-2-(12)
River
Three Top Creek
From source
to
North Fork
C;Tr:+
02/01/93
10-2-13
New River
Big Branch
From source
to
Three Top
C;Tr:+
02/01/93
10-2-13-1
Creek
Ben Bolen Creek
From source
to
Three Top
C;Tr:+
02/01/93
10-2-13-2
Creek
Long Hope Creek
From source
to
Three Top
C;Tr:+
02/01/93
10-2-13-3
Creek
Big Laurel Creek
From source
to
North Fork
C;Tr:+
02/01/93
10-2-14
New River
Dixon Creek
From source
to
Big Laurel
C;Tr:+
02/01/93
10-2-14-1
Creek
Kilby Creek
From source
to
Big Laurel
C;Tr:+
02/01/93
10-2-14-2
Creek
Woodard Branch
From source
to
Big Laurel
C;Tr:+
02/01/93
10-2-14-3
Creek
Cut Laurel Creek
From source
to
Big Laurel
C;Tr:+
02/01/93
10-2-14-4
Creek
Swift Branch
From source
to
Big Laurel
C;Tr:+
02/01/93
10-2-14-5
Creek
Soup Bean Branch
From source
to
Big Laurel
C;Tr:+
02/01/93
10-2-14-6
Creek
Roaring Fork (Roaring Fork
From source
to
Big Laurel
C;Tr:+
02/01/93
10-2-14-7
Creek)
Creek
East Fork Roaring Fork
From source
to
Roaring Fork
C;Tr:+
02/01/93
10-2-14-7-1
Big Branch
From source
to
Big Laurel
C;Tr:+
02/01/93
10-2-14-8
Creek
Little Laurel Creek'
From source
to
Big Laurel
C:+
02/01/93
10-2-14-9
Creek
Rich Hill Creek
From source
to
North Fork
C;Tr:+
02/01/93
10-2-15
New River
Copeland Creek
From source
to
North Fork
C;Tr:+
02/01/93
10-2-16
New River
Mill Creek
From source
to
North Fork
C;Tr:+
02/01/93
10-2-17
New River
Sugar Tree Branch (Sugar
From source
to
North Fork
C;Tr:+
02/01/93
10-2-18
Branch)
New River
Stagg Creek
From source
to
North Fork
C;Tr:+
02/01/93
10-2-19
New River
Buffalo Creek
From source
to
North Fork
C;Tr:+
02/01/93
10-2-20
New River
Little Buffalo Creek
From source
to
Buffalo Creek
C;Tr:+
02/01/93
10-2-20-1
0

MONITORING REPORT(MR) VIOLATIONS for: Report Date: 08/29/06 Page: 1 of 3
PERMIT: NC0000019
FACILITY: United Chemi-Con Manufacturing Inc - United Chemi-Con COUNTY: Ashe
REGION: Winston-Salem
Manufacturing
Monitoring Violation
MONITORING OUTFALL
VIOLATION
UNIT OF CALCULATED
REPORT
/ PPI
LOCATION
PARAMETER
DATE
FREQUENCY
MEASURE LIMIT VALUE
VIOLATION TYPE
VIOLATION ACTION
09 - 2005
001
Effluent
Aluminum, Total (as Al)
09/30/05
Quarterly
mg/I
Frequency Violation
None
05 - 2005
001
Effluent
Chlorine, Total Residual
05/31/05
Monthly
mg/I
Frequency Violation
None
06 - 2005
001
Effluent
Chlorine, Total Residual
06/30/05
Monthly
mg/I
Frequency Violation
None
07 - 2005
001
Effluent
Chlorine, Total Residual
07/31/05
Monthly
mg/I
Frequency Violation
None
08 - 2005
001
Effluent
Chlorine, Total Residual
08/31/05
Monthly
mg/I
Frequency Violation
None
09 - 2005
001
Effluent
Chlorine, Total Residual
09/30/05
Monthly
mg/I
Frequency Violation
None
10 - 2005
001
Effluent
Chlorine, Total Residual
10/31/05
Monthly
mg/I
Frequency Violation
None
11 - 2005
001
Effluent
Chlorine, Total Residual
11/30/05
Monthly
mg/I
Frequency Violation
None
12 - 2005
001
Effluent
Chlorine, Total Residual
12/31/05
Monthly
mg/I
Frequency Violation
None
01 - 2006
001
Effluent
Chlorine, Total Residual
01/31/06
Monthly
mg/I
Frequency Violation
None
02 - 2006
001
Effluent
Chlorine, Total Residual
02/28/06
Monthly
mg/I
Frequency Violation
None
03 - 2006
001
Effluent
Chlorine, Total Residual
03/31/06
Monthly
mg/I
Frequency Violation
None
04 - 2006
001
Effluent
Chlorine, Total Residual
04/30/06
Monthly
mg/I
Frequency Violation
None
05 - 2006
001
Effluent
Chlorine, Total Residual
05/31/06
Monthly
mg/I
Frequency Violation
None
06 - 2006
001
Effluent
Chlorine, Total Residual
06/30/06
Monthly
mg/I
Frequency Violation
None '
04 - 2006
001
Effluent
Flow, in conduit or thru treatment
04/30/06
Continuous
mgd
Frequency Violation
None
plant
•
06 - 2005
001
Effluent
LC50 STAT 48hr ACU D. PULEX
06/30/05
Quarterly
percent
Frequency Violation
None

MONITORING REPORT(MR) VIOLATIONS for:
Report Date: 08/29/06 Page: 2 of 3
PERMIT: NC0000019 FACILITY: United Chemi-Con Manufacturing Inc - United Chem! -Con COUNTY: Ashe REGION: Winston-Salem
Manufacturing
It
Monitoring Violation
MONITORING
OUTFALL
VIOLATION
UNIT OF CALCULATED
REPORT
/ PPI
LOCATION
PARAMETER
DATE
FREQUENCY
MEASURE LIMIT VALUE
VIOLATION TYPE
VIOLATION ACTION
09 - 2005
001
Effluent
LC50 STAT 48hr ACU D. PULEX
09/30/05
Quarterly
percent
Frequency Violation
None
12 - 2005
001
Effluent
LC50 STAT 48hr ACU D. PULEX
12/31/05
Quarterly
percent
Frequency Violation
None
03 - 2006
001
Effluent
LC50 STAT 48hr ACU D. PULEX
03/31/06
Quarterly
percent
Frequency Violation
None
06 - 2005
001
Effluent
Organics, Total Toxic (TTO)
06/30/05
Quarterly
mg/1
Frequency Violation
None
09 - 2005
001
Effluent
Organics, Total Toxic (TTO)
09/30/05
Quarterly
mg/1
Frequency Violation
None
12 - 2005
001
Effluent
Organics, Total Toxic (TTO)
12/31/05
Quarterly
mg/1
Frequency Violation
None
03 - 2006
001
Effluent
Organics, Total Toxic (TTO)
03/31/06
Quarterly
mg/I
Frequency Violation
None
06 - 2005
001
Effluent
Silver, Total (as Ag)
06/30/05
Quarterly
mg/I
Frequency Violation
None
12 - 2005
001
Effluent
Silver, Total (as Ag)
12/31/05
Quarterly
mg/1
Frequency Violation
None
03 - 2006
001
Effluent
Silver, Total (as Ag)
03/31/06
Quarterly
mg/I
Frequency Violation
None
06 - 2006
001
Effluent
Silver, Total (as Ag)
06/30/06
Quarterly
mg/I
Frequency Violation
None
04 - 2006
001
Effluent
Temperature, Water Deg.
04/29/06
Weekly
deg c
Frequency Violation
None
Centigrade
06 - 2006
001
Effluent
Temperature, Water Deg.
06/03/06
Weekly
deg c
Frequency Violation
None
Centigrade
04 - 2006
006
Effluent
Flow, in conduit or thru treatment
04/29/06
Weekly
mgd
Frequency Violation
None
plant
06 - 2006
006
Effluent
Flow, in conduit or thru treatment
06/03/06
Weekly
mgd
Frequency Violation
None
plant
04 - 2006
006
Effluent
Temperature, Water Deg.
04/29/06
Weekly
deg c
Frequency Violation
None
Centigrade

MONITORING REPORT(MR) VIOLATIONS for: Report Date: 08/29/06 Page: 3 of 3
PERMIT: NC0000019 FACILITY: United Chemi-Con Manufacturing Inc - United Chemi-Con COUNTY: Ashe REGION: Winston-Salem
Manufacturing
Monitoring Violation
MONITORING OUTFALL
VIOLATION
UNIT OF
CALCULATED
REPORT / PPI
LOCATION
PARAMETER
DATE
FREQUENCY
MEASURE
LIMIT VALUE
VIOLATION TYPE
VIOLATION ACTION
06 - 2006 006
Effluent
Temperature, Water Deg.
06/03/06
Weekly
deg c
Frequency Violation
None
Centigrade
06 - 2006 006
Effluent
Temperature, Water Deg.
06/10/06
Weekly
deg c
Frequency Violation
None
Centigrade
06 - 2006 006
Effluent
Temperature, Water Deg.
06/17/06
Weekly
deg c
Frequency Violation
None
Centigrade
06 - 2006 006
Effluent
Temperature, Water Deg.
06/24/06
Weekly
deg c
Frequency Violation
None
Centigrade
06 - 2006 006
Effluent
pH
06/30/06
2 X month
su
Frequency Violation
None
Reporting Violation
MONITORING OUTFALL
VIOLATION
UNIT OF
CALCULATED
REPORT / PPI
LOCATION
PARAMETER
DATE
FREQUENCY
MEASURE
LIMIT VALUE
VIOLATION TYPE
VIOLATION ACTION
06 - 2006 001
Effluent
Aluminum, Total (as AI)
06/30/06
Quarterly
mg/I
Parameter Missing
None
06 - 2006 001
Effluent
LC50 STAT 48hr ACU D. PULEX
06/30/06
Quarterly
percent
Parameter Missing
None
06 - 2006 001
Effluent
Organics, Total Toxic (TTO)
06/30/06
Quarterly
mg/I
Parameter Missing
None
06 - 2006 001
Effluent
P/F STATRE 7Day Chr
06/30/06
Quarterly
pass/fail
Parameter Missing
None
Cenodaphma
06 - 2006 001 Upstream Temperature, Water Deg. 06/30/06 Weekly deg c Parameter Missing None
Centigrade
06 - 2006 001 Effluent Zinc, Total (as Zn) 06/30/06 Quarterly mg/I Parameter Missing None

O�o� W A T 4z'9PG
IF_co r
� _i
o -c
Mr. Butch Howell
United Chemi-Con
185 McNeil Road
Lansing, NC 28643
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
SUBJECT: Compliance Evaluation Inspection
United Chemi-Con WWTP
NPDES Permit # NC0000019
Ashe County
Dear Mr. Howell:
Alan W. Klimek, P.E. Director
Division of Water Quality
June 15, 2006
A Compliance Evaluation Inspection was performed by George Smith on June 8, 2006. Mr. Gale D.
Howell, ORC, Grade IV, was present for the inspection. Mr. Everett Adams back-up operator, Grade
I, was not present. The inspection was comprised of an overall evaluation in order to document
compliance and noncompliance of: facilities equipment, capability to meet effluent limits, and
NPDES permit terms & conditions.
The attached inspection form evaluates nine (9) areas as noted in Section C of the attached
EPA inspection report, and the observations and comments during the inspection are
addressed below:
Permit
Your NPDES permit became effective on April 1, 2001 and expires on March 31, 2006. The permit
renewal application was sent to the NPDES Unit. The new permit was not yet issued.
The permit identifies the following discharge pipes:
(001) Non -contact cooling water, A/C condensate, boiler blowdown, de -ionizer backwash,
assembled product wash water & process wastewater. Process wastewater is not discharged,
it is hauled away.
(003) A/C condensate.
(006) Domestic wastewater.
(007) Recycled non -contact cooling water, and filtered surface water during maintenance periods
only.
Records & Reports
Mr. Howell maintains a log. Mr. Howell documents phone conversations, calibrations, process
control, and all are done in an excellent manner. y to«y
North Carolina Division of Water Quality 585 Waughtown Street Phone [phone] Customer Service
Winston-Salem Regional Office Winston-Salem, NC 27107 Fax [phone]
Internet: www.ncwaterauality.om
An Equal Opportunity/Affirmative Action Employer— 50% Recycled110% Post Consumer Paper �p

Mr. Howell
June 15, 2006
Page 2 of 3
Facility Site Review
The effluent from the Imhoff tank was clear with no visible solids.
The sandfilters were raked and appeared to be clean and in good condition. There was no evidence of
ponding on the surface of the sandfilters.
The dosing lines appear to be functioning properly.
Flow Measurement
The instantaneous flow at Outfall 006 is measured with a 1-inch parshall flume by measuring the
head and converting it to flow (MGD). There was a thin film of mud noticed all over the flume since
it is sometime submerged when the river is high. This was noticed during the previous inspection.
The Stevens, Model 6 1 R flow meter at Outfall 001 was calibrated by B.W. Allen on April 6, 2006.
The instantaneous flow from the chart read 0.10 MGD at the time of the inspection.
Laboratory
Mr. Howell performs pH and Temperature; and these tests are recorded on the daily monitoring
report.
A field certification for pH and Temperature was issued to Mr. Butch Howell for United Chemi-Con
(lab #5099). All remaining tests are performed by Tritest (Lab 4103), which is a certified lab.
The pH calibration is performed using a two -point calibration method (pH 4 & 10), and a mid -range
check (pH 7). The calibrations were documented.
The temperature is recorded against a NIST traceable thermometer.
Effluent/Receiving Waters
The effluent from Pipes 001 and 006 to the North Fork New River, Class C + waters of the State was
clear, no color, no solids, or no odor.
The effluent from pipes 001, 003, 006, and 007 did not appear to impact the North Fork New River.
In fact, pipes 003 and 007 were not discharging.
Operations & Maintenance
Mr. Butch Howell, Grade IV is the current ORC. The back-up operator is Mr. Everett Adams, Grade
I. The facility (pipe 006) with the Imhoff tank is considered a Class II facility.

Mr. Howell
June 15, 2006
Page 3 of 3
The facility was well maintained by the staff, and they are considered to perform their jobs in an
outstanding manner. The equipment appeared to be in good operating order. The Imhoff tank showed
vigorous degassing at the sidewalls, which indicate that the system is well operated & maintained.
Process control tests of pH, ammonia, alkalinity, oil & grease are performed on the influent and
Imhoff tank. Process control tests appear to be successfully used in measuring plant performance.
The operator adds 50 pounds of Soda Ash approximately once a month to keep the alkalinity at a
good level.
Self -Monitoring Program
A review of the monthly self -monitoring reports from April 2005 through March 2006 did not show
any monitoring or limit violations.
The grab samples, if required, are taken from the end of the pipe at all outfalls.
The composite sampler at Pipe 001 is time composite at 200 mL every 30 minutes.
The chain -of -custody reports were accurate and in good order.
Sludge Disposal
Sludge is removed from the plant by Cox Septic Service.
The sludge drying beds are never used.
Mr. Howell continues to perform his job in an outstanding manner. The compliance evaluation
inspection is considered excellent. If you have any questions please contact George Smith at (336)
771-5000.
Sincerely,
Steve W. Tedder
Regional Supervisor
cc: SWP Central Files
WSRO Files

I�
United States Environmental Protection Agency
Form Approved.
EPA Washington, D.C. 20460
OMB No. 2040-0057
8-31-98
Water Compliance inspection Report
Approval expires
Section A: National Data System Coding (i.e., PCS)
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type
18I 19( gl 20IJ
1 UN 2 (5( 31 NC0000019 111 121 06/06/08 117 C
J
�.!
Remarks
1 1 1 1 1 1 1 16
211 I I I I I I I I I I I I I I I I I I I Ill 1 1 1 1 1 1 1 1 1 11 1 1 1 1 1
Inspection Work Days Facility Self -Monitoring Evaluation Rating 131 OA-------------------------Reserved------------------
70U 71(D( 72L 73� 74 751 I ( I I I I I 80
67 169 ��--
''��
Section B: Facility Data
Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include
Entry Time/Date
Permit Effective Date
POTW name and NPDES permit Number)
09:45 AM 06/06/08
05/05/01
United Chemi-Con Manufacturing
Exit Time/Date
Permit Expiration Date
185 McNeil Rd
Lansing NC 28643
11:30 AM 06/06/08
06/03/31
Name(s) of Onsite Representative(s)rritles(s)/Phone and Fax Number(s)
Other Facility Data
Gale Dean Howell/ORC/336-384-6917/
Name, Address of Responsible Official/Title/Phone and Fax Number
Contacted
Hiroshi Ohashi,185 McNeil Rd Lansing NC 28643/VP of No
Operations/336-384-2551/3363846928
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit N Flow Measurement E Operations & Maintenance Records/Reports
Self -Monitoring Program 0 Sludge Handling Disposal 0 Facility Site Review Effluent/Receiving Waters
Laboratory
Section D: Summary of Finding/Comments Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date
George S Smit�h� WSRO WQ//336-771-5000/ `, Is -DE,
�'�`'r' �' t:�vwt.✓V
Signature of Mana ment Q A R_evie Agency/Office/Phone and Fax Numbers Date
"A G—is-o�
EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete.
Page # 1

1
NPDES yr/mo/day Inspection Type
3) NC0000019 I11 121
06/06/08 117 18U _i
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
Page # 2

I
Permit: NC0000019 Owner- Facility: United Chemi-Con Manufacturing
pection Date: 06/08/2006 Inspection Type: Complianc-- Evaluation
Yes No NA NE
Operations & Maintenance
■ ❑ ❑ ❑
Is the plant generally clean with acceptable housekeeping?
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable Solids, pH, DO, Sludge
■ ❑ ❑ ❑
Judge, and other that are applicable?
Comment:
Yes No NA NE
Permit
(If the present permit expires in 6 months or less). Has the permittee submitted anew application?
■ 000
■ ❑ ❑ ❑
Is the facility as described in the permit?
# Are there any special conditions for the permit?
Is access to the plant site restricted.to the general public?
■ ❑ ❑ ❑
Is the inspector granted access to all areas for inspection?
Comment:
Yes No NA NE
Record Keeping
■ ❑ ❑ ❑
Are records kept and maintained as required by the permit?
■ ❑ ❑ ❑
Is all required information readily available, complete and current?
Are all records maintained for 3 years (lab. reg. required 5 years)?
Are analytical results consistent with data reported on DMRs?
Is the chain -of -custody complete?
■
Dates, times and location of sampling
■
Name of individual performing the sampling
■
Results of analysis and calibration
■
Dates of analysis
■
Name of person performing analyses
■
Transported COCs
Are DMRs complete: do they include all permit parameters?
Has the facility submitted its annual compliance report to users and DWQ?
(If the facility is = or > 5 MGD permitted flow) Do they operate 24/7 with a certified operator on each shift?
❑ ❑ ■ ❑
Is the ORC visitation log available and current?
Is the ORC certified at grade equal to or higher than the facility classification?
Is the backup operator certified at one grade less or greater than the facility classification?
■ ❑ ❑ Cl
■ ❑ ❑ ❑
Is a copy of the current NPDES permit available on site?
Page # 3

Permit: NC0000019 Owner - Facility: United Chemi-Con Manufacturing
Inspection Date: 06/08.12006 Inspection Type: Compliance Evaluation
Yes No NA
NE
Record Keeping
Facility has copy of previous year's Annual Report on file for review?
Comment:
Yes No NA
NE
Sand Filters (Low rate)
(If pumps are used) Is an audible and visible alarm Present and operational?
■ Q Q
❑
Is the distribution box level and watertight?
■ ❑ ❑
❑
Is sand filter free of ponding?
❑ ❑ ■
❑
Is the sand filter effluent re -circulated at a valid ratio?
# Is the sand filter surface free of algae or excessive vegetation?
■ ❑ ❑
❑
# Is the sand filter effluent re -circulated at a valid ratio? (Approximately 3 to 1)
QQ■❑
Comment:
Yes No NA
NE
Effluent Sampling
❑ ■ ❑
❑
Is composite sampling flow proportional?
Is sample collected below all treatment units?
■ ❑ ❑
❑
Is proper volume collected?
■ ❑ ❑
❑
Is the tubing clean?
Is proper temperature set for sample storage (kept at 1.0 to 4.4 degrees Celsius)?
■ ❑ ❑
❑
Is the facility sampling performed as required by the permit (frequency, sampling type representative)? ■ ❑ ❑
Comment: Time composite is acceptable for this sample.
Yes No NA NE
Upstream / Downstream Sailing
Is the facility sampling performed as required by the permit (frequency, sampling type, and sampling location)? ■ Q Q ❑
Comment:
Page # 4

Lz 0 U
o o --
R .Of- D o 7
C;,IL ���

i Carolina
rtment of Environment and Natural Resources
'Pollution Control System Operator Certification Commission
Michael F. Easley, Governor
William G. Ross Jr., Secretary
Coleen H. Sullins, Chairman
CERTIFIED MAEL
RETURN RECEIPT REQUESTED
Mr. Thomas W. Efford
United Chemi-Con
185 McNeil Road
Lansing, NC 28643
W.W, V J
61
NCDENR
N 0August 17, 2001
AUG 3 0 2001
Re
gional office
System: United Chemi-Con Wastewater Treatment System
Classification: Grade 1 Physical Chemical System
Subject: Designation of ORC and Backup ORC for Physical / Chemical
Permit: NC0000019
Dear Mr. Efford:
The Water Pollution Control System Operators Certification Commission adopted Rule 15A
NCAC 8G .0306, Classification of Physical / Chemical Systems, effective April 1, 1999. In
order to insure the proper operation and maintenance of these systems, this Rule requires that
all systems permitted for a physical / chemical process to treat wastewater be classified as
physical / chemical systems.
If the subject physical / chemical system consists of systems designed for (1) the remediation
of contaminated groundwater, or (2) that utilizes a primarily physical process to treat
wastewaters, (with the exception of reverse osmosis, electrodialysis, and utrafiltration
systems), then that system shall be classified as a Grade I Physical / Chemical Water Pollution
Control System. Rule 15A NCAC 8G .0306(a)
If the subject physical / chemical system consists of systems that utilizes a primarily chemical
process to treat wastewaters (including those systems whose treatment processes are
augmented physical processes), they shall be classified as a Grade H Physical / Chemical
Water Pollution Control System. Reverse osmosis, electrodialysis, and utrafiltration systems
shall also be classified as Grade H Physical / Chemical Water Pollution Control System. Rule
15A NCAC 8G .0306(b)
If the water pollution control system that has, as part of its treatment process, biological water
pollution control system that may be classified under Rule .0302, then that system shall be
subject to additional classification as a biological water pollution control system. Rule 15A
NCAC 8G .0306(c)
Any water pollution control system subject to classification under Rule .0302 of this Section,
utilizing a physical / chemical process to enhance an activated sludge or fixed growth process,
shall not be subject to additional classification. Rule 15A NCAC 8G .0306(d)
1618 Mail Service Center, Raleigh, North Carolina 27699-1618
Phone: 919 — 733-0026 \ FAX: 919 — 733-1338
AN EQUAL OPPORTUNITY \ AFFLRMATIVE ACTION EMPLOYER - 50% RECYCLED / 10% POST CONSUMER PAPER

IV
The Water Pollution Control System Operators Certification Commission hereby classifies
your system as a Grade 1 Physical Chemical System. This classification is based on
information submitted in your application for a NPDES permit and/or based on the
information you provided in the physical chemical classification survey that you completed
during the months of April -May 2001.
As required by Rule 15A NCAC 8G .0202(2) and the subject permit, a certified Operator in
Responsible Charge (ORC) and back-up operator of the appropriate type must be
designated for each classified system. Your system requires an ORC and back-up
operator who hold valid phvsical / chemical operator certificates Please complete and
return the enclosed designation form to this office by December 31, 2003. Failure to
designate a properly certified ORC and back-up operator is a violation of the permit issued
for this system.
In accordance with Rule 15A NCAC 8G .0406(b), individuals presently working at physical /
chemical water pollution control systems holding a valid Grade I, II, III, or IV wastewater
treatment plant operator certification, may apply for a conditional operators physical /
chemical certificate without examination. He or she may do so if, he or she has one year
experience and has successfully completed a training school sponsored or co -sponsored by the
Commission for Grade I or Grade 2 Physical / Chemical Water Pollution Control System
Operators. This conditional certification allows the bearer to act as the ORC or Backup
ORC of that System only. This conditional certification must be renewed annually per
section .0700 of the rules. The Rules for this certification as well as others is found on the
DWQ/Technical Assistance and Certification Unit web page (http://h20.enr.state.nc.us/tacuf).
Plans are now being made to conduct the first physical chemical school in January 15-18.
2002 at the McKimmon Center in Raleigh. This school is co -sponsored by AWWA/WEA
and the NC Water Pollution Control System Operators Certification Commission. As soon as
arrangements for the school are finalized you will receive more information.
If we can be of assistance or you have any questions concerning this requirement, please call
James Pugh at 919-733-0026, ext. 341 or e-mail: [e-mail].
Enclosures
cc: WSRO
Central Files
TAC Facility Files
Sincerely,
Tony Arnold, Supervisor
Technical Assistance and Certification Unit