WQ0006245_More Information (Received)_20200512

Sta-Lime Processing and Distribution Program Narrative
Sludge is pumped into a 1.5-million-gallon digester as Waste Activated Sludge.
The digested sludge is then pumped into the dewatering process onto a three -
belt, 3-meter press. The dewatered sludge is conveyed into a live bottom hopper
via a progressing cavity pump at the end of the belt press, and from there the
sludge is conveyed to a pug mill to be blended with Lime Kiln Dust. From this
point in the process on, the material is considered Sta-Lime.
The Sta-Lime is discharged from the pug mill onto a covered conveyor belt that
carries the Sta-Lime to covered pulse bins, where the Sta-Lime is held until the pH
and temperature requirements are met. From the pulse bins the Sta-Lime is
moved to a 170' by 70' covered storage pad, where it can be loaded by City
employees onto customers trucks / trailers.
There are two smaller live bottom hoppers that can receive dewatered sludge
from Third Creek WWTP for processing into Sta-Lime as well, should the need
ever arise. Sludge is no longer dewatered at the Water plant, so the City Water
plant will not be considered a Residual Source for Sta-Lime. Sludge from 3rd Creek
has never been used to make Sta-Lime but will be listed as a Residual Source
should the need arise to use it to make Sta-Lime in the future.
Should Sludge from 3rd Creek WWTP ever be used to make Sta-Lime, the sludge
will be dewatered at 3rd Creek WWTP by a 3-belt press and then transported to
4th Creek WWTP via City owned dump truck. That sludge would be discharged
into the smaller live bottom hoppers and fed into the pug mill to be blended with
Lime Kiln Dust and follow the same process as listed above.
All stormwater runoff from the sludge holding area is directed to the headworks
of the WWTP.
There was a Capital expenditure project in 2015 that updated the Sta-Lime
making equipment and configuration from previous permit cycles, but the process
has remained relatively unchanged.

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two conies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
® For new or renewed permits, submit a separate certification for each source facility.
❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
® Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
❑ For each source facility, attach the following:
® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for
Residuals Land Application Permits".
® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
❑ For each source facility, attach the following:
® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1

RESIDUALS SOURCE FACILITY SUMMARY
Applicanf s name: City of Statesville
Status
Code °
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current n
Proposed
R
City of Statesville
Third Creek
Iredell
NCO020591
Not currently used
for Class A
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: City of Statesville
2. Facility permit holder is: U Federal, 0 State, 0 Local Government, or 0 Private.
Facility permit issued by: Div. of Water Resources, Div. of Environmental Health,
or Other (explain: M.
3. Facility contact person and title: Scott Austin 3rd Creek Supervisor
Complete mailing address: PO Box 1111
City: Statesville State: NC Zip: 28687-1111
Telephone number: [phone] E-mail address: [e-mail]
4. Facility physical address: 444 Third Creek Road
City: Statesville State: NC Zip: 28677M
Coordinates: Latitude: 35' 44' 28.2 "N Longitude: 80. 50' 20.3" W
Datum: I&- Level of accuracy: _
Method of measurement: _
5. Purpose of the facility:
n treatment of municipal wastewater, treatment of 100% domestic wastewater,
❑ treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: 40 % industrial and 60 % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: 6 MGD and facility average daily flow: Approximately 1 MGD
8. Average amount of residuals being generated at this facility 1500 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 3 meter, 3 belt press
Type and volume of residuals storage (i.e., outside of residuals treatment units): 265' x 145' pad at 4' Creek
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological ❑ Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 06-16 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes ® no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes jo no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Prism and Date of analysis: 8/07/19
Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: yes no. Flashpoint: = OF (> 140°F)
Passed reactivity test: ® yes ❑no. HCN: __I mg/kg (<250) & H2S: _ mg/kg (<500)
TCLP Parameter
Limit
(m917)
Result
(m917)
TCLP Parameter
Limit
(mgfi)
Result
(m917)
Arsenic
5.0
<0.10
Hexachlorobenzene
0.13
<0.020
Barium
100.0
<5
Hexachloro-1,3-Butadiene
0.5
<0.050
Benzene
0.5
<0.025
Hexachloroethane
3.0
<0.050
Cadmium
1.0
<0.025
Lead
5.0
<0.050
Carbon Tetrachloride
0.5
<0.025
Lindane (gamma-BHC)
0.4
<0.00050
Chlordane
0.03
<0.0025
Mercury
0.2
<0.010
Chlorobenzene
100.0
<5
Methoxychlor
10.0
<0.00050
Chloroform
6.0
<0.30
Methyl Ethyl Ketone
200.0
<10
Chromium
5.0
<0.25
Nitrobenzene
2.0
<0.050
m-Cresol
200.0
Pentachlorophenol
100.0
<0.25
o-Cresol
200.0
Pyridine
5.0
<0.25
p-Cresol
200.0
Selenium
1.0
<0.15
Cresol
200.0
Silver
5.0
<0.25
2,4-D
10.0
<0.2
Tetrachloroethylene
0.7
<0.035
1,4-Dichlorobenzene
7.5
<0.38
Toxaphene
0.5
<0.025
1,2-Dichloroethane
0.5
<0.025
Trichloroethylene
0.5
<0.025
1,1-Dichloroethylene
0.7
<0.035
2,4,5-Trichlorophenol
400.0
<0.25
2,4-Dinitrotoluene
0.13
<0.012
2,4,6-Trichlorophenol
2.0
<0.10
Endrin
0.02
<0.00050
2,4,5-TP (Silvex)
1.0
<0.2
Heptachlor and its Hydroxide
0.008
<0.00050
Vinyl Chloride
0.2
<0.010
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Prism and Date of analysis: 11/25/19
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
13
Cadmium
85
39
<0.75
Copper
4,300
1,500
54
Lead
840
300
9
Mercury
57
17
0.095
Molybdenum
75
n/a
24
Nickel
420
420
15
Selenium
100
100
27
Zinc
7,500
2,800
100
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: = and Date of analysis: =
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
W > 0 but < 25
30
200
210
19 > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 66.3 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Prism / WayPoint and Date of analysis: 11/25/19 4/27/20
Parameter
Result
(mg1kg)
Aluminum
16,000
Ammonia -Nitrogen
120
Calcium
2400
Magnesium
<1
Nitrate -Nitrite Nitrogen
9.3
pH (Standard Unit)
12.55
Phosphorus
4300
Potassium
4600
Sodium
1100
Total Kjeldahl Nitrogen
4000
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 1_0
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This
rate is a (check one): JJ default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: ii
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1") Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mglkg)
Surface
1233.3
1,932.463
Injection/Incorporation
1293.3
1,992.463
6. Other Pollutants Determination: S ecify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment.
Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
n Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: composting, " heat drying, 77 heat treatment,
thermophilic aerobic digestion, ❑ beta ray irradiation,
J0 gamma ray irradiation, or ® pasteurization.
b. For Land Application of Class B.
Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, I
air drying, ❑ anaerobic digestion,
El composting, or lime stabilization.
c. For Surface Disposal:
TJ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
J Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
J Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
J Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
EJ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T. 1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T. I 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T. 1107(a)(7)] - Drying of Stabilized Residuals.
E] Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals.
El Alternative 9 [15A NCAC 02T. 1107(a)(9)] - Injection.
E] Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
El Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
id Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit
General - This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
® For new or renewed permits, submit a separate certification for each source facility.
❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
® Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
❑ For each source facility, attach the following:
® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for
Residuals Land Application Permits".
® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
❑ For each source facility, attach the following:
® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: City of Statesville
Status
Code a
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current n
Proposed
R
City of Statesville
Sta-Lime Processing & Dist.
Iredell
WQ0006245
7,000
7,000
'Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (Le, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: City of Statesville
2. Facility permit holder is: p Federal, 0 State, 0 Local Government, or 0 Private.
Facility permit issued by: Div. of Water Resources, Div. of Environmental Health,
or Other (explain: M.
3. Facility contact person and title: Ken Galloway 4' Creek Supervisor
Complete mailing address: PO Box 1111
City: Statesville State: NC Zip: 28687-1111
Telephone number: 704 878-3438 E-mail address: [e-mail]
4. Facility physical address: 693 Bell Farm Road
City: Statesville State: NC Zip: 28687-1111-
Coordinates: Latitude: 350 46' W" Longitude: 800 47' 15"
Datum: _ Level of accuracy: _
Method of measurement: _
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: 40 % industrial and 60 % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: 6 MGD and facility average daily flow: 3_2 MGD
8. Average amount of residuals being generated at this facility 1500 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 3 meter, 3 belt press
Type and volume of residuals storage (i.e., outside of residuals treatment units): 265' x 145' pad
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102 (6) as:
Biological ❑ Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 06-16 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Prism and Date of analysis: 8/07/19
Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: yes no. Flashpoint: _ °F (> 140°F)
Passed reactivity test: Eyes Mno. HCN: _ mg/kg (<250) & H2S: _ mg/kg (<500)
TCLP Parameter
Limit
(Mg/7)
Result
(Mg/7)
TCLP Parameter
Limit
(Mg/7)
Result
NO)
Arsenic
5.0
<0.10
Hexachlorobenzene
0.13
<0.020
Barium
100.0
<5
Hexachloro-1,3-Butadiene
0.5
<0.050
Benzene
0.5
<0.025
Hexachloroethane
3.0
<0.050
Cadmium
1.0
<0.025
Lead
5.0
<0.050
Carbon Tetrachloride
0.5
<0.025
Lindane (gamma-BHC)
0.4
<0.00050
Chlordane
0.03
<0.0025
Mercury
0.2
<0.010
Chlorobenzene
100.0
<5
Methoxychlor
10.0
<0.00050
Chloroform
6.0
<0.30
Methyl Ethyl Ketone
200.0
<10
Chromium
5.0
<0.25
Nitrobenzene
2.0
<0.050
m-Cresol
200.0
Pentachlorophenol
100.0
<0.25
o-Cresol
200.0
Pyridine
5.0
<0.25
p-Cresol
200.0
Selenium
1.0
<0.15
Cresol
200.0
Silver
5.0
<0.25
2,4-D
10.0
<0.2
Tetrachloroethylene
0.7
<0.035
1,4-Dichlorobenzene
7.5
<0.38
Toxaphene
0.5
<0.025
1,2-Dichloroethane
0.5
<0.025
Trichloroethylene
0.5
<0.025
1, 1 -Dichloroethylene
0.7
<0.035
2,4,5-Trichlorophenol
400.0
<0.25
2,4-Dinitrotoluene
0.13
<0.012
2,4,6-Trichlorophenol
2.0
<0.10
Endrin
0.02
<0.00050
2,4,5-TP (Silvex)
1.0
<0.2
Heptachlor and its Hydroxide
0.008
<0.00050
Vinyl Chloride
0.2
<0.010
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Prism and Date of analysis: 11/25/19
Parameter
Ceiling
Concentration Limits
(C1assA & C1assB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
13
Cadmium
85
39
<0.75
Copper
4,300
1,500
54
Lead
840
300
9
Mercury
57
17
0.095
Molybdenum
75
n/a
7.4
Nickel
420
420
15
Selenium
100
100
27
Zinc
7,500
2,800
100
b. For Surface Disposal Unit (Iandfrll): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
> 0 but < 25
30
200
210
> 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 66.3 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Prism / WayPoint and Date of analysis: 11/25/19 / 4/27/20
Parameter
Result
(mglkg)
Aluminum
18000
Ammonia -Nitrogen
120
Calcium
2400
Magnesium
< 1
Nitrate -Nitrite Nitrogen
9.3
pH (Standard Unit)
12.55
Phosphorus
4300
Potassium
4600
Sodium
1100
Total Kjeldahl Nitrogen
4000
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 1_0
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This
rate is a (check one): JJ default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: ii
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (V) Year PAN
Five -Year
Maximum Adjusted PAN
(m91k9)
(mg/kg)
Surface
1233.3
1,932.463
Injection/Incorporation
1293.3
1,992.463
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For DistributiomEand Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
II Alternative 1 [15A NCAC 02T.1106 (b) (3) (A)] - Time/Temperature Compliance.
® Alternative 2 [15A NCAC 02T.1106(b) (3) (B)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T.1106(b) (3) (C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 [15A NCAC 02T.1106 (b) (3) (D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
FJ Alternative 5 [15A NCAC 02T.1106(b) (3) (E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: 7 composting, 0 heat drying, 77 heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
gamma ray irradiation, or ® pasteurization.
b. For Land Application of Class B.
71 Alternative 1 [15A NCAC 02T.1106(c) (1)] - Fecal Coliform Density Demonstration.
q Alternative 2 [15A NCAC 02T.1106(c) (2)] -Process to Significantly Reduce Pathogens (PSRP).
Specify one: aerobic digestion, air drying, n anaerobic digestion,
composting, i I lime stabilization.
c. For Surface Disposal,
9 Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II.7a. above.
J Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
J Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a) (2)].
J Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑
Alternative 1 [15A NCAC 02T.1107(a) (1)] -
38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
E]
Alternative 2 [15A NCAC 02T.1107(a) (2)] -
40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T.1107(a) (3)] -
30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T.1107(a) (4)] -
Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T.1107(a) (5)] -
14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T.1107(a) (6)] -Alkaline
Stabilization.
Alternative 7 [15A NCAC 02T.1107(a) (7)] -Drying
of Stabilized Residuals.
E]
Alternative 8 [15A NCAC 02T.1107(a) (8)] -Drying
of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T.1107(a) (9)] -Injection.
E]
Alternative 10 [15A NCAC 02T.1107(a) (10)]
-Incorporation.
Alternative for Surface Disposal Units Only
- Soil/Other Material Cover [15A NCAC 02T.1107(b) (2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
10.37
10,33
10.28
10.27
10.23
10.22
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
1/2/2019
12
1I2/19 8:41
1/2/18 8:54
SA
300
1.6
13.1
14.4
0.0
10A
1.0
vlliliters
(o Dry Solids
egrees Celsius
egrees Celsius
1.86 mg Oxygen/hr
0.39 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 1 0.5$ 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
10.87
10.83
10.8
10.75
10.71
10.68
10.65
10.61
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
1/3/2019
11.9
1/3/19 8:58
SA
1/3118 9:04
SA
iilliliters
io Dry Solids
egrees Celsius
egrees Celsius
0.0
11.1
1.0
2.15 mg Oxygen/hr
0.45 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.72 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
9.19
9.17
8.98
8.96
8.96
8.94
8.93
Slope. -
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate. -
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
1 /4/2019
15.5
1/4/19 10:14
SA
1/4/18 10:19
1.6
15.4
15
0.0
9.2
1.0
illiliters
P Dry Solids
agrees Celsius
wees Celsius
1.43 mg Oxygen/hr
0.30 mg Oxygen/g/hr
15 degrees Celsius
1,402551731
Temperature Corrected Specific Oxygen Uptake Rate; I =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
1 /7/2019
15.7
1/7/19 13:03
SA
1/7/18 13:09
SA
300
1.6
16
14.9
Dissolved Oxygen Level
8.77
8.76
8.74
M&D
8.62
0
8.61
8.59
8.57
8.56
8.53
i
8.5
8.49
a
8.46
8.44
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
8.8
1.0
1.35 mg Oxygen/hr
0.28 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: V titzac0.7mg Oxygenlg/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids;
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
1 /8/2019
10.4
1/8/19 8:23
SA
1/8/18 8:31
SA
300
1.6
10.9
12.6
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
11.7
1.0
1.75 mg Oxygen/hr
0.36 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 0.63 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
1/9/2019
14.8
1/9119 7:33
SA
119118 7:41
SA
300
1.6
14.9
15.1
Dissolved Oxygen Level
8.64
8.63
8.6
8.59
8.56
8.1
a
8.48
8.44
8.42
8A
8.37
8.35
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
8.6
0.7
1.32 mg Oxygen/hr
0.28 mg Oxygen/glhr
15 degrees Celsius
1.402551731
T.Temperature Corrected Specific Oxygen Uptake Rate: 0.39mg Oxygenlglhr
:r
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
m 11
9.83
9.08
9.78
9.75
9.73
9.72
9.7
9.68
9.63
9.6
9.57
9.55
9.51
9.48
9.47
9.45
Slope:
Intercept:
Correlation Coefficient:
Third Creek WWTP
WQ0016247
1/10/2019
10.8
1/10119 8:44
SA
1110118 8:50
300
1.6
10.9
11.3
0.0
9.7
0.3
Ililiters
Dry Solids
grees Celsius
frees Celsius
r
Oxygen Uptake Rate: 0.75 mg Oxygenlhr
Ambient Specific Oxygen Uptake Rate: 0.16 mg Oxygenlglhr
Average Temperature: 11 degrees Celsius
Temperature Correction Factor: 1.838459212
Temperature Corrected Specific Oxygen Uptake Rate: 0.29 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By;
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.91
6.88
6.85
6.82
6.79
6.74
6.71
6.7
6.68
6.67
6.65
6.63
6.61
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
W00016247
4/1/2019
16.1
4/1/19 10:28
iIIiliters
Dry Solids
agrees Celsius
:arees Celsius
0.0
6.9
1.0
1.25 mg Oxygen/hr
0.21 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: 0.27 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling DatelTime:
Sampled By:
Analysis DatelTime:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP16
milliliters
I Dry Solids
degrees Celsius
degrees Celsius
WQ00247
4/2/2019
15.3
412119 8:26
1
SA
4/2/19 8:33
SA
300
1.9
15.5
15.7
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.2
1.0
1.25 mg Oxygen/hr
0.22 mg Oxygenlg/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: 0.29 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.1
w
7.07
7.06
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
illiliters
% Dry Solids
egrees Celsius
feareesCelsius
W00016247
4/3/2019
17.1
4/3/19 13:04
SA
4/3/19 13:13
SA
300
1.9
17.2
16.8
0.0
7.1
1.0
1.25 mg Oxygen/hr
0.22 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.54
6.53
6.49
6.48
6.47
6.44
6.4
6.39
6.37
6.34
6.28
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
4/4/2019
15.3
4/4119 8:33
SA
414119 8:41
300
1.9
14.4
148
0.0
6.6
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
1.25 mg Oxygen/hr
0.22 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: 0.31 mg Oxygenlg/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.32
6.31
6.29
6.27
6.26
6.26
6.24
6.21
6.18
6.16
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
4/5/2019
17.4
4/5/19 8:32
SA
4/5/19 8:40
SA
300
1.9
17.2
17.1
0.0
6.4
1.0
1.09 mg Oxygen/hr
0.19 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate: 0.23 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number. -
Date:
Digester Temperature:
Sampling Date/Time.-
Sampled By:
Analysis Daterrime:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
5.09
5.06
5.04
CIYll
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
4/8/2019
18.8
SA
418/
SA
300
1.9
18.6
18.8
Aliliters
16 ❑r'y Solids
egrees Celsius
eqrees Celsius
0.0
5.1
1.0
1.84 mg Oxygen/hr
0.32 mg Oxygen/glhr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.34 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
W00016247
4/9/2019
18.6
419119 8:32
SA
419119 8:39
SA
300
1.9
18.9
19.3
Dissolved Oxygen Level
6.754
6.7
6.68
6.65
6.64
6.61
6.59
6.56
6.54
6.49
6.45
6.43
6.4
6.38
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
6.8
1.0
1.49 mg Oxygenlhr
0.26 mg Oxygenlglhr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.28jmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters —
% Dry Solids
degrees Celsius
degrees Celsius
WQ0019247
7/2/2019
21.3
7/2/19 10:26
SA
7/2/19 10:31
SA
300
1.9
20.8
20.8
Dissolved Oxygen Level
7.8
7.78
7.75
7.73
7.69
7.65
7.71
7.62
7,58
7.55
7.53
7.49
7.46
7.43
7.41
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.8
1.0
1.61 mg Oxygen/hr
0.28 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: ^ 0.27mg Oxygenlglhr
_.:_.
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
WQ0016247
Date:
7/3/2019
Digester Temperature:
21.6
Sampling Date/Time:
713119 7:38
Sampled By:
SA
Analysis Date/Time:
713119 7:45
Analyzed By:
SA
Sample Volume:
300
Total Solids:
1.9
Beginning Temperature:
21.4
End Temperature:
21.5
Dissolved Oxygen Level
7.36
7.33
7.27
e
7.24
7.2
7.17
7.15
7.14
7.11
7.06
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.3
1.0
ilfiliters
Dry Solids
agrees Celsius
:cirees Celsius
1.66 mg Oxygen/hr
0.29 mg Oxygenlglhr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.28 1mg Oxygenlglhr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By. -
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.65
6.61
6.56
6.51
6.49
6.43
6.41
6.39
6.37
6.34
6.33
6.28
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature. -
Temperature Correction Factor:
W00016247
7/5/2019
7/5/� 4
SA
7/5/19 7:41
SA
300
1.9
22.9
22.5
Pt ._
0.0
6.6
1.0
iliCers .
Dry Solids
Trees Celsius
frees Celsius
1.41 mg Oxygen/hr
0.25 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
:L7.L.7_� eta r.r --a
Temperature Corrected Specific Oxygen Uptake Rate: rMWIL- �mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0019247
7/8/2019
23.7
7/8/19 9:58
SA
7/8/19 10:07
SA
300
1.9
24.4
23.7
Dissolved Oxygen Level
5.91
5.87
5.81
5.78
5.76
5.71
5.66
5.62
5.53
5.46
5.41
5.38
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
5.9
1.0
2.24 mg Oxygen/hr
0.39 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:1 0.32 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
millitiCers
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
7/9/2019
23.6
7/9119 7:22
SA
719119 7:32
SA
300
'1.9
23.4
22,5
Dissolved Oxygen Level
6.31
6.28
6,25
6.22
6.2
6.16
6.12
6.1
6.06
6.02
5.95
5.93
0
5.92
5.9
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
6.3
1.0
1.78 mg Oxygen/hr
0.31 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Ratef= 0.27 g Oxygen/g/hr
Instructions.- Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
10
11
12
13
14
15
Facility Nam(
Biosolids Permit Numbe
Dat(
Digester Temperatur(
Sampling Date/Time
Sampled B)
Analysis Date/Timc
Analyzed BI
Sample VolumE
Total Solids
Beginning Temperature
End TemperaturE
Dissolved Oxygen Level
Third Creek WWTP
WQ0016247
7/10/2019
23.3
7110119 8:03
SA
7/10/19 8:10
SA
300
m
1.9
%
22.8
dE
22.6
de
Ililiters
Dry Solids
grees Celsius
grees Celsius
Slope:
0.0
Intercept:
6.5
Correlation Coefficient:
1.0
Oxygen Uptake Rate:
2.31 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate:
0.41 mg Oxygenlglhr
Average Temperature:
23 degrees Celsius
Temperature Correction Factor:
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: 0.35 mg Oxygenlglhr
Instructions: Enter Data in the Blue Boxes.
The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume. -
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.76
0
6.71
6.67
W-1
6.52
6.4
6.44
6.42
6.37
6.33
6.27
6.23
6.19
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate. -
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
7/11/2019
23.3
7/11/19 7:03
SA
7/11/19 7:09
SA
300
1.9
23.3
22.6
0.0
6.8
1.0
milliliters
Dry Solids
legrees Celsius
learees Celsius
2.36 mg Oxygen/hr
0.41 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: ` 0.36 Jmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.13
7.09
7.04
Slope:
Intercept:
Correlation Coefficient. -
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek VW
W00016247
10/1/2019
21.8
10/1/19 7:12
SA
10/1/19 7:22
1.8
21.9
0.0
7.5
1.0
nilliliters
Yo Dry Solids
iegrees Celsius
learees Celsius
1.93 mg Oxygen/hr
0.36 mg Oxygenlg/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate: L0.32 mg Oxygen/g/hr
Instructions.- Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Daterrime:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.84
7.79
7.74
7.7
7.67
T64
7.6
e
7.59
7.61
7.58
7.5
7.46
7.41
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
W00016247
10/2/2019
22
10/2/19 7:12
10/2/
SA
300
1.6
22
21.6
0.0
7.8
1.0
ii0iliters ,
o Dry Solids
egrees Celsius
egrees Celsius
1.55 mg Oxygen/hr
0.35 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate: LL mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
J .
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
W00017247
10/3/2019
21.7
10/3/19 8:39
SA
10/3/19 8:47
SA
300
1.5
21.6
21.2
Dissolved Oxygen Level
7.4
7,35
7.33
7.3
7.27
7.28
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.4
1.0
1.29 mg Oxygen/hr
029 mg Oxygen/g/hr
21 degrees Celsius
0,952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.27 Dmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis DatelTime:
Analyzed By:
Sample Volume. -
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.39
7.38
7.35
7.33
7.29
7.26
7.22
7.18
7.16
7.11
e�
7.07
7.02
6.97
®s
6.97
6.91
6.87
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
10/4/2019
21.3
SA
1014/19 7:31
1.5
21.3
0.0
7.4
1.0
illiliters
Dry Solids
agrees Celsius
agrees Celsius
2.16 mg Oxygenlhr
0.48 mg Oxygenlglhr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: r 0.46 mg Oxygenlglhr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosoiids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
f.
8
7.95
7.92
7.87
7.88
7.7
7.69
7.67
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate. -
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WO0016247
10/7/2019
19.2
10/7/19 7:34
SA
10/7/19 T43
SA
300
1.5
19.4
19.7 i
0.0
8.1
1.0
illiliters
Dry Solids
agrees Celsius
:green Celsius
1.82 mg Oxygen/hr
0.40 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: E 0.40 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time.-
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids;
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.21
e
8.17
0
8.16
8.11
8.1
8.06
8.04
8.02
8
7.97
7.94
7.9
7.82
7.79
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
W00016247
1...19.5 ...,
10/8/19 7:24
SA
10/81
SA
300
1.5
19.8
0.0
8.2
1.0
lilliliters - _....
16 Dry Solids
egrees Celsius
earees Celsius
1.57 mg Oxygenlhr
0.35 mg Oxygen/glhr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.35 mg Oxygenlglhr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milGsiite�._
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
10/9/2019
18.8
10/9/19 8:38
SA
10/9/19 8:46
SA
300
1.5
18.8
19.1
Dissolved Oxygen Level
7.56
7.53
7.51
7.47
7.43
7.37
7.39
7.34
7.28
7.22
7.19
7.15
7.12
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature!
Temperature Correction Factor:
0.0
7.6
1.0
1.87 mg Oxygen/hr
0.42 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.45 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature. -
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen level
9.57
9.68
14* 4
9.5
9.5
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
7
1/2312019
11.1
1 /23/19 10:52 AM
1/23/19 10:57 AM
BJ
300
1.47
11.4
11.7
0.0
9.7
0.5
illiliters
� Dry Solids
?grees Celsius
:arees Celsius
0.63 mg Oxygenlhr
0.14 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 0.24 1mg Oxygenlglhr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name. Fo
Biosolids Permit Number.
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
4
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
24/2019
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
12.8
19 1:12 PM
LC
19 1:17 PM
BJ
300
1.37
12.7
13.2
0.0
9.3
0.8
1.39 mg Oxygenlhr
0.34 mg Oxygenlglhr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.54 mg Oxygenlglhr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling DatelTime:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
m !I
0
9.44
1
9.47
2
9.48
3
9.48
4
9.43
5
9.4
6
9.3
7
9.51
8
9.46
9
9.4
10
9.32
11
9.23
12
9.22
13
9.17
14
9.1
15
9.07
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
(Fourth Creek WWTPI
1/25/2019
10.7
1/25/19 1:01 PM
LC
1125119 1:08 PM
BJ
300
1.39
11.1
0.0
9.5
0.9
illiliters
Dry Solids
:grees Celsius
:grees Celsius
1.56 mg Oxygen/hr
0.37 mg Oxygenlglhr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 0.64 1mg Oxygenlglhr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
[minutes]
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Fourth Creek WW'
Biosolids Permit Number:
Date:
1 /28/2019
Digester Temperature:
15.7
Sampling Date/Time:
1/28119 1:58 PM
Sampled By:
KG
Analysis Date/Time:
1/28/19 Z02 PM
Analyzed By:
BJ
Sample Volume:
300
Total Solids:1
1.37
Beginning Temperature: 16
End Temperature: 15.5
Dissolved Oxygen Level
me 11
7.77
7.66
7.61
7.58
7.54
7.43
7.72
7.79
7.79
7.76
7.69
7.55
7.59
7.61
7.61
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.7
0.0
Milliliters
6 Dry Solids
egrees Celsius
earees Celsius
0.05 mg Oxygen/hr
0.01 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: 0.02 Jmg Oxygen/glhr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/0
0
6.59
1
6.51
2
6.43
3
6.3
4
6.28
5
6.24
6
6.08
7
5.99
8
5.95
9
5.84
10
5.78
11
5.72
12
5.67
13
5.56
14
5.53
15
5.49
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
(Fourth Creek VWIlTPI
1/29/2019
20.2
1/29/19 1:00 PM
KG
1/29/19 1:13 PM
BJ
300
1.56
20.2
0.1
6.6
1.0
illiliters
Dry Solids
agrees Celsius
!grees Celsius
4.54 mg Oxygen/hr
0.97 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 1 0.97 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature. -
End Temperature:
Dissolved Oxygen Level
7.04
6.99
6.98
7.01
6.95
6.94
6.93
6.87
�s
6.8
6.74
6.73
6.7
6.66
6.63
6.58
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
(Fourth Creek WWTPI
1/30/2019
17.7
1/30/19 1:01 PM
LC
1130/19 1:12 PM
BJ
300
1.41
17.3
16.9
0.0
7.1
1.0
Ililiters
Dry Solids
grees Celsius
grees Celsius
2.04 mg Oxygen/hr
0.48 mg Oxygenlglhr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate: 0.59 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
1/31/2019
11.9
1/31/19 1:00 PM
RG
1/31/19 1:09 PM
BJ
300
1.36
12.3
12.4
Dissolved Oxygen Level
Mpg
9.91
9.88
9.82
9.77
9,689
9.66
9.65
9.6
9.47
9.38
9,37
9.32
Slope:
Intercept:
Correlation Coefficient. -
Oxygen Uptake Rate. -
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
V
t
2.49 mg Oxygen/hr
0.61 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 1.05 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
3.71
3.46
2.56
2.4
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
(Fourth Creek WWTP!
1 5/20/2019 1
5/20/19 8:06 AM
BD
5/20/19 8:09 AM
300
1.26
22.3
22.7
0.1
3.6
1.0
iilliliters
c Dry Solids
egrees Celsius
eorees Celsius
5.01 mg Oxygen/hr
1.32 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: 1.14 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By. -
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
m /1
2.88
2,68
2.53
2.38
2.62
2.9
2.88
2.77
2.67
2.57
2.43
2.37
2.34
2.27
2.2
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
4
22
KG
5/22119 2:56 PM
KG
300 milliliters
1.23 % Dry Solids
22 degrees Celsius
22.5 dearees Celsius
0.0
2.8
0.7
1.95 mg Oxygen/hr
0.53 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate: 1 0.48 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids;
Beginning Temperature
End Temperature.
Time Dissolved Oxygen Level
(minutes) m /I
0
3.85
1
3.6
2
3.41
3
3.25
4
3.09
5
2.91
6
2,76
7
2.57
8
2.37
9
2.18
10
2.29
11
2.56
12
2.52
13
2.37
14
2.2
15
2.01
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
r5/23
/23/2019
23.3
/19 2:22 PM
KG
119 2:24 PM
KG
300
1.2
23.3
24.1
0.1
3.5
0.9
Ililiters
Dry Solids
grees Celsius
grees Celsius
6.40 mg Oxygen/hr
1.78 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 1.46 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling DatelTime:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
2.97
2.83
2.97
2.96
2.83
2.63
2.51
2.32
2.13
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
(Fourth Creek WWTPI
1 5/24/2019 1
5/24/19 7:20 AM
BD
5/24/19 7:27 AM
BD
300
1.29
21.9
22.3
0.1
3.8
1.0
iilliliters
16 Dry Solids
egrees Celsius
eorees Celsius
6.30 mg Oxygen/hr
1.63 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate: 1.48 1mg Oxygen/glhr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourth Creek V1
Biosolids Permit Number:
Date: 1 5/28/2017
Digester Temperature:
Sampling Date/Time.-
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
m /I
0
5.56
1
5.47
2
5.38
3
5.27
4
5.18
5
5.1
6
5.02
7
4.29
8
4.86
9
4.78
10
7.4
11
4.65
12
4.6
13
4.55
14
4.5
15
4.46
Slope:
Intercept:
Correlation Coefficient. -
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
5/28/19 10:50AM
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
BD
5/28/19 12:00 AM
BD
300
1.02
26.3
25.8
0.1
5.5
0.3
3.23 mg Oxygenlhr
1.06 mg Oxygen/glhr
26 degrees Celsius
0.746215397
Temperature Corrected Specific Oxygen Uptake Rate: 0.79 mg Oxygenlglhr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek VVWTP11
5/29/2019
22.7
5/29/19 7:38 AM
BD
5/29/19 7:43 AM
BD
300
1.32
22.7
23.1
0.1
6.0
0.9
Ililiters
Dry Solids
grees Celsius
grees Celsius
5.70 mg Oxygen/hr
1.44 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: 1 1.24 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling DatelTime:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
5.61
5.45
5.32
5.22
5.04
4.95
4.88
4.8
4.74
4.58
4.49
4.38
4.35
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
IFourth Creek WWTPI
5/30/2019
22.2
5/30/19 7:34 AM
5/30/19 7:39 AM 11
BD
1.2
22.2
22.6
0.1
5.5
1.0
illiliters
Dry Solids
;green Celsius
wees Celsius
4.90 mg Oxygenlhr
1.36 mg Oxygenlglhr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate: 1.23 mg Oxygenlglhr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
7/12/2019
24
7/12/19 8:57 AM
BD
7/12/19 9:01 AM
BD
300
1.3
24
24
Dissolved Oxygen Level
6.9
5.73
5.75.77
5.58
5.5
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
5.9
1.0
4.13 mg Oxygen/hr
1.06 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 0.87 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:1
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
7/15/2019
23.7
7/15/19 7:30 AM
BD
7115/19 7:35 AM
BD
300
1.4
23.7
24
Dissolved Oxygen Level
6.35
6.35
6.3
6.25
6.15
6.11
6.05
6
5.96
5.92
5.9
5.87
5.84
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
6.4
1.0
2.37 mg Oxygen/hr
0.56 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:l 0.46 Dmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
MU
5.52
5.19
5.19
5.1
5.06
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature. -
Temperature Correction Factor:
Fourth Creek WWTP
7/16/2019
25.4
7/16/19 1:15 PM
KG
7/16/19 1:20PM
BD
300
1.3
25.4
25.2
0.0
5.4
1.0
lliliters
Dry Solids
grees Celsius
grees Celsius
1.44 mg Oxygen/hr
0.37 mg Oxygen/g/hr
25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: 0.29 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time.-
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.02
76 8
6.43
6.39
6.25
6.16
6.03
5.96
5.88
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
(Fourth Creek WWTPI
7/17/2019
23
7/17/19 7:28 AM
BD
7/17/19 7:32 AM
BD
300
1.32
23
23.4
0.1
6.8
1.0
lilllllters
(a Dry Solids
egrees Celsius
egrees Celsius
4.98 mg Oxygen/hr
1.26 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: 1 1.09 m7mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis DatelTime:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
7/18/2019
23.8
7/18119 7:31 AM
BD
7/18/19 7:36 AM
BD
300
1.3
23.8
23.7
Dissolved Oxygen Level
6.58
6.32
6.3
6.24
6.17
6.09
6.04
6.02
6
5.95
5.9
5.86
5.92
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
6.5
1.0
3.06 mg Oxygen/hr
0.79 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 0.65 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
m 11
7.48
7.2
7.11
7.03
6.96
6.92
6.89
6.87
6.85
6.86
6.83
6.76
6.71
6.69
6,64
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
(Fourth Creek WWTP+
7/19/2019
23.7
7/19/19 7:36 AM
BD
7/19/19 7:40 AM
BD
300
1.3
23.7
23.5
0.0
7.2
0.9
illiliters
Dry Solids
!green Celsius
wees Celsius
2.39 mg Oxygen/hr
0.61 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 0.50 mg Oxygenlg/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:,
End Temperature:)
Dissolved Oxygen Level
7.54
7.25
e
7.23
0
7.27
7.27
7.22
7.06
7.02
-
6.97
-
6.96
6.87
6.82
-
6.79
-
6.75
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
(Fourth Creek WWTPI
7/20/2019
24.1
7/20/19 7:37 AM
BD
7/20/19 7:42 AM
300
0
1.2
24.1
0.0
7.4
1.0
illiliters
Dry Solids
agrees Celsius
rgrees Celsius
2.82 mg Oxygen/hr
0.78 mg Oxygenlglhr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 0.64 mg Oxygenlg/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date. -
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.2
8.1
8.03
7.98
7.94
7.9
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
10/1/2019
23
10/1 /19 9:32 AM
BD
10/1/19 9:36 AM
BD
300
1.4
23
23.4
0.0
8.1
1.0
Aliliters
eo Dry Solids
egrees Celsius
egrees Celsius
2.84 mg Oxygen/hr
0.68 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: 0.58 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
10/2/2019
22.7
10/2/19 7:39 AM
BD
10/2/19 7:44 AM
BD
300
1.4
22.7
22.7
Dissolved Oxygen Level
8.14
E-1I:I
7.97
7,93
7.88
s
7.84
7.81
s
7.77
7.73
7.69
7.61
7.57
7.53
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate. -
Average Temperature:
Temperature Correction Factor:
0.0
8.1
1.0
2.44 mg Oxygen/hr
0.58 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rake: 0.50 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name: Fourth Creek WWT
Biosolids Permit Number:
Date: 10/3/2019
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.07
8.03
7.95
7.92
s
7.89
7.84
7.8
7.76
7.71
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
22.2
10/3/19 7:28 AM
BD
10/3/19 7:31 AM
BD
300
1.49
22.2 i
0.0
8.3
1.0
Ililiters
Dry Solids
grees Celsius
Qrees Celsius
2.51 mg Oxygen/hr
0.56 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate: 1 0.51 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume. -
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.65
8.6
8.52
8.48
8.4
8.36
8.32
8.28
8.24
8.17
8.12
8.07
a
8.03
Slope:
Intercept:
Correlation Coefficient. -
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
mi
%
de
10/4/2019
21.5
1014119 7:24 AM
BD
1014/19 7:28 AM
BD
300
Ide
1.5
21.5
21.7
0.0
8.6
1.0
Ililiters
Dry Solids
grees Celsius
grees Celsius
2.43 mg Oxygenlhr
0.54 mg Oxygenlglhr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate: 0.49 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature. -
Sampling Date/Time:
Sampled By. -
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
(Fourth Creek WWTP1
1 /5/2019
21
10/5119 8:25 AM
BD
10/5/ 19 8:2 9 AM
BD
1.48
21
21
0.0
8.7
0.8
illiliters
Dry Solids
:green Celsius
:arees Celsius
2.22 mg Oxygen/hr
0.50 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 1 0.48 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
mittiiiters
% Dry Solids
degrees Celsius
degrees Celsius
10/7/2019
18.8
10/7/19 7:34 AM
BD
1017/19 7:38 AM
BD
300
1.7
18.8
19
Dissolved Oxygen Level
9.25
9.23
9.19
9.18
9.24
9.17
9.16
9.14
9.12
9.1
9.08
9.06
�t
8.93
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
9.3
1.0
1.22 mg Oxygen/hr
0.24 mg Oxygenlg/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: .. 0.26 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
10/8/2019
19.8
10/8/19 7:31 AM
BD
1018119 7:34 AM
BD
340
1.4
19.8
19.8
Dissolved Oxygen Level
fmalli
9.05
9.04
9.04
9.03
9.02
9
8.98
8.94
8.92
8.91
8.89
8.87
8.85
8.81
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature. -
Temperature Correction Factor:
0.0
9.1
1.0
1.01 mg Oxygen/hr
0.24 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.24 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

■
Way point
ANALYTICAL
City of Statesville, NC
Ken Galloway
P.O. Box 1111
Statesville, NC 28687
INC Certification No. 402
INC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: StaLime (Quarterly Parameters)
Lab Submittal Date: 04/27/2020
Work Order: 0040304
Case Narrative
5/4/20 15:32
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
Terri W. Cole
Project Manager
Data Qualifiers Key Reference:
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 7

0 (2)
Waypoint
ANALYTICAL
Sample Receipt Summary
05/04/2020
Work Order: 0040304
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
Sta-Lime
0040304-01
Solid
04/27/20 14:15
04/27/20 15:45
3rd Creek Sludge
0040304-02
Solid
04/27/20 14:15
04/27/20 15:45
4th Creek Sludge
0040304-03
Solid
04/27/20 14:15
04/27/20 15:45
Samples were received in good condition at 3.0 degrees C unless otherwise noted
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 2 of 7

■
Way point
ANALYTICAL
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
05/04/2020
Project: StaLime (Quarterly Client Sample ID: Sta-Lime
Parameters) Sample ID: 0040304-01
Work Order: 0040304
Sample Matrix: Solid Time Collected: 04/27/20 14:15
Time Submitted: 04/27/20 15:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 89.9 % by 0.100 0.100 1 *SM2540 G 5/1/20 9:43 EDV POD0467
Weight
Total Metals
Aluminum 13000
Molybdenum 2.5
mg/kg dry 140 30 5 *6010D 4/29/20 10:37 JAB POD0431
mg/kg dry 1.1 0.13 1 *6010D 4/29/20 9:26 JAB POD0431
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 7

■
Way po�nt
ANALYTICAL
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Quarterly
Parameters)
Sample Matrix: Solid
Laboratory Report
05/04/2020
Client Sample ID: 3rd Creek Sludge
Sample ID: 0040304-02
Work Order: 0040304
Time Collected: 04/27/20 14:15
Time Submitted: 04/27/20 15:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
23.7
% by
0.100
0.100
1
*SM2540 G
5/1/20 9:43
EDV
POD0467
Weight
Total Metals
Aluminum
16000
mg/kg dry
1100
230
10
*6010D
4/29/20 10:15
JAB
POD0431
Molybdenum
24
mg/kg dry
4.2
0.51
1
*6010D
4/29/20 9:51
JAB
POD0431
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 4 of 7

■
Way po�nt
ANALYTICAL
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Quarterly
Parameters)
Sample Matrix: Solid
Laboratory Report
05/04/2020
Client Sample ID: 4th Creek Sludge
Sample ID: 0040304-03
Work Order: 0040304
Time Collected: 04/27/20 14:15
Time Submitted: 04/27/20 15:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
22.1
% by
0.100
0.100
1
*SM2540 G
5/1/20 9:43
EDV
POD0467
Weight
Total Metals
Aluminum
18000
mg/kg dry
1100
250
10
*6010D
4/29/20 10:23
JAB
POD0431
Molybdenum
7.4
mg/kg dry
4.5
0.54
1
*6010D
4/29/20 9:59
JAB
POD0431
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 5 of 7

Way po ■ 0 nt
ANALYTICAL
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch POD0431 - 3050B
Project: StaLime (Quarterly Parameters)
Level II QC Report
5/4/20
Work Order: 0040304
Time Submitted: 4/27/2020 3:45:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (POD0431-BLK1)
Prepared: 04/28/20 Analyzed: 04/29/20
Aluminum
BRL
25
mg/kg wet
Molybdenum
BRL
1.0
mg/kg wet
LCS (POD0431-BS1)
Prepared: 04/28/20 Analyzed: 04/29/20
Aluminum
1260
25
mg/kg wet
1250 101 80-120
Molybdenum
12.9
1.0
mg/kg wet
12.50 103 80-120
Matrix Spike (POD0431-MS1)
Source: 0040304-01
Prepared: 04/28/20 Analyzed: 04/29/20
Aluminum
2.78E10
28
mg/kg dry
1390 12800 NR 75-125 MC
Molybdenum
14.9
1.1
mg/kg dry
13.90 2.47 90 75-125
Matrix Spike Dup (POD0431-MSD1)
Source: 0040304-01
Prepared: 04/28/20 Analyzed: 04/29/20
Aluminum
2.78E10
28
mg/kg dry
1390 12800 NR 75-125 0 20 MC
Molybdenum
14.9
1.1
mg/kg dry
13.90 2.47 90 75-125 0.1 20
Post Spike (POD0431 -PS1)
Source:0040304-01
Prepared: 04/28/20 Analyzed: 04/29/20
Aluminum
493
mg/L
50.00 460 66 75-125 MC
Molybdenum
0.527
mg/L
0.5000 0.0888 88 75-125
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch
Initial
Final
Date/Time
0040304-01 POD0467
30 g
30 g
04/30/20 11:22
0040304-02 POD0467
30 g
30 g
04/30/20 11:22
0040304-03 POD0467
30 g
30 g
04/30/20 11:22
Prep Method: 3050B
Lab Number Batch
Initial
Final
Date/Time
0040304-01
POD0431
2
g 50
mL
04/28/20
7:57
0040304-01
POD0431
2
g 50
mL
04/28/20
7:57
0040304-02
POD0431
2
g 50
mL
04/28/20
7:57
0040304-02
POD0431
2
g 50
mL
04/28/20
7:57
0040304-03
POD0431
2
g 50
mL
04/28/20
7:57
0040304-03
POD0431
2
g 50
mL
04/28/20
7:57
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 6of7

PRIS {� A I FullService Analytical &
CHAIN OF CUSTODY RECORD]
' V' Environmental Solutions PAGE OF QUOTE # TO ENSURE PROPER BILLING:
LABORATORIES, INC.
449 Springbrook Road • Charlotte, NC 28217 Project Name:
Phone [phone] Fax: [phone] Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
La � � [��(+11c�St,�. He
ATTACH any project specific reporting (QC LEVEL 1 II III IV)
Client Company Name: crTy provisions and/or QC Requirements
Report To/Contact Name: KEN CAIIaW.sy _ Invoice To:
Reporting Address:
Address:
YES NO N
Samples INTACT upon arrival? _
Received ON WET ICE? _.
PROPER PRESERVATIVES indicated? 0)
Received WITHIN HOLDING TIMES?
c�
CUSTODY SEALS INTACT? 0-
VOLATILES rec'd W/OUT HEADSPACE?
PROPER CONTAINERS used? _
TEMP: Therm I -5G-/ Observed: 2 CI *C / Corr: 3D °C
Phone: 7041 - F7 S- 34S8 Fax � (No):10V- Slf-ir6SS purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL_ .
Email Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD FL NC
%
!--
EDD Type: PDF Excel Other
"Working Days" ❑ 6-9 Dave ❑ Standard 10 days ❑ Rush Work Must Be
Pre -Approved
Site Location Name: FL.:t n4l Car-Ek Samples received after 14:00 will be processed next business day.
SC OTHER N/
Site Location Physical Address: G q3
O cAl 1FAZ,RJTurnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO�
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES_ NO
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
PRISM
CLIENT DATE
COLLECTED
(SOIL,
PRESERVA-
REMARKS
LAB
SAMPLE DESCRIPTION COLLECTED
MILITARY
WATER OR
'TYPE
NO.
SIZE
TIVES
ID NO.
HOURS
SLUDGE)
SEE BELOW
pp
C'REF4 Sits
i
GI
_3 n'.4
y rrj
l
w1h cr 1< S
'1'
Sampler's Signature G(1
Sampled By (Print Name) /fA 1�.� r Affiliation
Upon relinquishing, this Chain of Custody
is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to th rism Project Manager. There will be charges for any changes after analyses have been initialized. PRISM USE
ONLY
R inquished : (SI
Rs By: f5i naturr Date MilltarylHours Additional Comments:
� Site Arrival Time:
q - ed Ignntu
/ RedaiKd By: (Signature) ate Site Departure Time:
Relinquis y: (Signature
Field Tech Fee:
Received Far " Lettorstanas By Date
? , J
' 7 Mileage:
Methotl of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT H CUS EALS FOR TRANSPORTATION TO THE LABORATORY. COC G n pL
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORATORY. ��
❑ Fed Ex ❑ UPS ❑ Hand -delivered m Field Service ❑ Other
NU
JLILI
ILL OTHER:
❑NC❑SCf ❑NC ❑SC ❑I�C 0SfIC 0NC I❑SCATER: ❑NC El SC ❑NC❑SC ❑NC ❑SC ❑NCF❑SC El NC El SC
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
ORIGINAL

City Of Statesville Alkaline Stabilization Record Por
Process To Further -Reduce Pathogens (PFRP)
BIN # 1 setup Date: f- Q g- 1 Removal From Bin Date: 1-3i. 17
Date Time Pk >12.0 Far 72 Hrs. TEMP: >S2 Deg. C For 12 Hrs. Operator
In .
nlpH. 1s7,5q 1-Ae-19 i-Aq- 1q
Corrected pN:1 2, 73°& 30 t'°C�d7,`o5 r?c1�
a Final pH: �,5� 1-31-Iq --4,J
1 31-fy 10; 3�.� Corrected pH: f,.. `7,1 130 0 11 nm
Has 12 Dour Ternp Criteria Been Met? N
Has 7.2 Hour nw Criteria Been Met? CY N
BIN # a Setup Date: 1-. q_ 3 Removal From Bin Date: 2-1 14
Date Time pH >12.0 F or 72 Hrs: TEMP. >52 Deg. C For 12 Hrs. Operator
Initial pH: i� . t✓ 3 1- 2q,-1 �1 14 30 - 19
e
Corrected p13: 1,, . 93 7 5'0, 11. ; S-5160,1,60 �+���
1_ 1 i.1:rla�o Corrected ply: 1). F1
Has 12 Hour Temp Criteria Beery Met? OY N
Has 72 flour pH Criteria Been Met?
B!N # 7' Setup Date:. 1m 30 - 114 Rem' oval From Bin Date: 2 -
Date Time IaH>12.0For 72fIrs. TEMP. >52Deg.CForl2Hrs. Operator
1-3r3-1`1 1� ;3 Initial pH. 1,?.!0 �� 11 -7
1-3o41i-31- 1
Corrected pH: 1 d.7 q ` o C-) 1,z., 0,1 SG" (2 011,0 Ltd
11 Final pH. 12. `1 - -i A
d�, Corrected pH: .9s'C�
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? Y N
BIN ## 5
Setup Date: 1-31-11 Removal From lain Date; d -S- 1,3�
Dpa e ! lme
pH >12:0 FOr.72 I-Irs. TEMP. >52 Deg. C For 121-Irs.
Operator
Initial p1l: 1,2, d 9
1-31- 1 Se)
Corrected p1l: f.?,? 0� �' 11� �C� a 0 i
Rkto
Final p1l. i2, 5L7 1-q-r:l
Corrected pli: f ,l , (, q 93 :16) 0.115�
f Has 12 Hour Ternp Criteria Been Met? �Y) N f
Has 72 Hoour pal Criteria Been Met? �Y) N
BIN # 0/
ISetup Date:
Rei+moval,From Bin Date:
Date 'Time
pal >12.0 Fat' 72 fArs.
TEMP.'>.52 Deg. C For 12 Ilrs. `
Operator
I q 0 7: 3 0
initial pH: 1d,51
A-1-19 �T,f--1Q
`'D 1 Pr97 I�0 c `1. 311
R4 t,)
Corrected pH: ,1 .`ai
A
Final pN: 1 d ,' 5 )
I.RI,
LJ
Corrected pal: 1o7. _3 EEI
Has 12 HOUr Teii.-np Criteria Been Met? N
Has 72 Hopr pli Q'iteria Been Met? i) : N

.k v
City Of Statesville Alkaline Stabilization Record For,
• Process T-o Further'Reduce Pathogens (PFRP)
BIN## 7-V 6 setup Date: Z-IS - 1q Removal From Bin Elate: 2,1 r-I q
Date I Time pW >12.0 For 72 Hrs. TEMP. >s2 Deg. C For 22 Hrs. Operator .
Initial pH: f.1. 60 2-le-m 2-1a- t 9
10, k5tn corrected pH: J,T, `J �'U4 it 0 :a p �' 0j:gf RxL�1
Final pH: 12. 63 ,�-�- r •••ovc� -r�
2• I•iq !!- 3Ciny CorrectedpH: i� *J b`woiv 09;4 g er�.rxcc� 9,rp
f� W,
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hoifr pH Criteria Been Met. Y. N
BIN # J r', setup Date: lRemoval From Bin Date:
Date Time pH >12.0 FOr 72 Hrs.. TEMP. >52 Deg. C For 12 Hrs. I Operator
Initial pH: l,�,k �• t-' [� �q
,+�1 - ►p Jf:�® Corrected pH: /R.7 > a'IF 11; A
Final pH: i.,7. S7 i q
Correded pH: I�, q7 aPb j�j i.� I
Has 12 Hour. Temp Criteria Been Met?
Has 72 •Hnur-pH Criter'la Been Met? N
13IN SCS Setup Date: 446 lRernoval Ftom Bin pate:,f-.1S-1�
Date Time pH , 110 For 72 Ws. TEMP. >52 Deg.CFnrll Firs. Operator
lnitial pH: 7.4► t'S
d l // 0? Corrected pH: 10, P S' 10'W 07,U 6 ID S' LP 67--15 W,
Final pH: l01.iq A. AS. i
l -Ag l l � r e [� CorrectedpH: 19. 71 fly, & d w'' 5 � @�r
Has 12 Dour Te— nip CriteriaBeen Met? N
Has 72 HOUr pH Criteria Been Meth l
BIN## q e e setup Date: Removal From Biro date;
pate I `rime pW >i2;0 rpr.72 Hrs. TEMP. >52 Deg. C r-or12 Firs. Operator
1"WaiPH: 0, 5 Ir- I-1r} •x�• r
2-,tl f ' lCorrectedp": 12.?f. go`Lv 04:4o 1060oltia rA(A)
Final pH: to?. �19 P--ll -
Corrected pH: 14, g'-
Has 12 Flour Temp Criteria Been Met? N
Has 72 Flour pFl Criteria Been Met? N
Bllil ## P 4' �2 Setup Date: 2- 2 A- 17 Rem' oval From Bin Date:
ij*te- "Time 'pA- >-"-1"2.0- •For 72 "-,r$. 7'EnAP.I>�z peg. C rot V Hrs-. Dperatdr
initial pH: 1.7.57 Z•-n- N
Corrected pH: 1,2. 7 -7 1,00 76 07-,°O + j
Final pH:
i PM CorrectedpH: L2 .` 3
Has 1.2 Hal,ll° Temp Criteria Been Meth Y N
Has 72 H©urplA. criteria Been Met? 4�Y l`4

'City Of Statesville Alkaline Stabilization Record For.
Process To Further -Reduce Pathogens (PFRP)
BIN # / ' Setup Date: 5- gy I q Removal .rrom Bin late: 13• l q
Date Time pH >12.0 For 72 Hrs. TEMP: >52 Deg. CFor 12 Hrs. Operator .
initial pH: 1 .' G. V- W- t Q S- Q- 1 Q.
CorrectedpH:ll. 04 10,UA ��� OT,Y7 q0e �dW
Final pH: 14, F $
in 1 ' rq f w 5o A lCorrected pH: 10. '>' S, 900
Ha's 12 H®ur Temp Criteria Been Met? N
Has 72 HoLlr PH Criteria Been MetILYj
?Y N
$IN #l' .3 e5. Setup Date: 5-, qe I q lRem.oval From Bin Date: S7-1
-11
®ate
Time po >22.0 For 72 Hrs-. TEMP. >52 Deg. C Fnr 1t Hrs.
Operator
initial pli: R.Ar`fi
lj�+f A�Corrected pH: M, E 11 A goo d�: Y0 ��1 �
Rlw
Final pH: 14, e'V
CorreetedpH: 0. I?V l�s:��� ���
K4W
Has 12 Hour Temp Criteria 8eeh Met? Y;. N
1413S 72,Hour.pH Criteria Been Viet? Y N
$IN It l e t jSetupDa.e.,.S­j,0c,.fj Removal From Bin Date: t, j'i:.1 q
Date
T1t 10 1 l 2;0 for 72 Hrs. TEMP. >52 Deg. c Tor 12 Hrs.
Operator
.y�va
Initial pH: jib, l:.1a- €••$ice Y
kla A Corrected pH: #:#.�� iI: iiy� €��� ��:�3a �f a
k4W
Wi �'
Final pH: 14, Y4
Correcteti_pNc:, !ll Ala 1i�
Has 12 Hour Temp Criteria Been Meth N
Has 72 HoUrpH Criteria Been Met? N
BIN # je, ' ISotup Date: il. # I
lRernoval From Bin Date, i 6. f
Date
Tlme pH >12:0 For.72 Wrs.
TEMP. >52 Reg. CFor 12 Hrs.
Operator
initial pH: ,
_V:-q— 14
e j a M
Corrected pH: If. `14
18:jtA 46"'
j3wY q6
Pl w
Final PH: 1-,J, '
I b Y.s Corrected pH: fui_. 94
t-1
Has 12 Hour Temp Criteria Been Met? �X) N
Has 72 Hour pH Criteria Been Met? .l) N
SIN •f# 36,
Setup Date: 6.jq,Iq
Reinoval.From Bin Date: Sj741
bite
Time
H >12.0 Fos %2 H'rs' .
fEf41P. >52 Deg. C For 12 Hrs. `
Operator
�1�1�6`
fi.h+z 1ti
Initial pH: I . �®
a - lijd e
ilA 90®
3 . 15_ f
CorrectedpH:tlt7"f.
Final pH: 1_7, Y (.
S - j 6 - 14.1
-1 I3 90 o
Corrected pH:
leas U F0UrTem'p Cr.i.teria Been Pvget? T N
Has 72Hourp",.Criteria Been Met?

City Of Statesville Alkaline Stabilization Record For.
Process To Further -Reduce Pathogens (PFRP)
BIN # '7 4 ? Setup Date: S• /s" - I q Removal From Bin Date:
Date Time pH > Z.fl For 72 Hrs. TEMP: >52 Deg. C For 12 Hrs, Operator .
Initial pH: 1?, 5r7 3 _ 16- R .
2b P Corrected pH: 1.2,747 lr.3o1� �0° 07:15 goo
-Ao-19 0q.1-ti
Has 12 Hour Temp Criteria Been Met? W N
Has 72 Hour pH Criteria Been Met.? N
BIN # 10 Setup bate: S e 16-19 Removal From Bin Date: 9;-Aq- 14
Date Time pb >12.0 For 72 Hrs. TEMP. >52 Deg, C For 1Z Hrs, Operator.
InitialpH:
'�iLa t
11 Corrected p11: lr�. °� D4��-�
sills 166
Final pH: #.43
ad -!
b �� Fi I;urrecietf PH: f
log
Has 12 Hour Ternp Criteria been Met?
* N
Has 72-Hour.pH Criteria Beer Meta
• N
BIN # 3
letup'Date: 37-1`1-; Rempva1 Vrorn Bin bate: 6:_.Ae - !�`
Date
Time pH;?12..0 For 72 Hrs. TEMP. >52Deg.0For 1.2Hrs.
operator
initial pH:1i. j'�'s4-1
9-11r.PI
1DA Corrected pH: }�.t�� ��:1� ��4�
i�il�F3 ���
�i•� w
Final pH: 0. Y S
4-jC)-(q1DqAk I Corrected. pH:RLvv
Has 12 Hour Temp Criteria Been Mat? N
Has 72 HOUr pH Criteria Been Met? TY) -N
8114 It v '
Setup Date: : t) f Removal From Bits bate,
Date
Time
pH >110 For.72 Mrs. 'TEMP. >52 Deg. C For 12 Hrs.
operator
�t
1
Initial pH:
Corrected pH: if V.J.
; ` �
1
Final pH: fs?,(i 9
Corrected p'H: Ia. (1
Has 12 Hour Temp Criteria Been Met? ' Y
Has 72 Hour 'PH Criteria Bben Met? I) N
BIN #
Setup Date:
Removal .From Bin Date:
®�t0
Time
721 ir5.
TtMP.'>' 2Deg. C Foy 12? Hrs. "
631ierator
Initial pH:
.Corrected pH:
Final pH:
Corrected pH:
Has 12 F10-r.lr6 Temp Criteria Been Met? Y
Has 72 Fiopr.pH Criteria Been Met? Y

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # j j� Setup Date: 11 1rt- l q Removal From Bin Date: j j- x� a i Q
Date Time pH >12.0 For 72 Firs. TEMP. >52 V12p.eatotor
Initial pH: 1+2.5ft-fq-��
if-I?-!�! 1i:3� Corrected pH. l-7,6�j 110" 6e�ct3
Pinal pH: 1% ,qd
�",i Corrected pH: j: , eo Has 12 Hour Temp Criteria Been MeHas 72 Hoer pH Criteria Beery Met
BIN it 3 4! Setup Date: !t-00 - [q lRemoval From Gin Date:
Date I Time pH >12.0 For 72 III-S. TEMP. >52 Deg. C For 12 Hrs. Operator
Initial pH: IEr<rf`�lda d it-P1-l�
lire``-0�t rl� s Corrected PH: 11.11 D `!t�
Final pt�: ¢, , q5
rf-t�i� jf`cs� Corrected PH:Ix4.
Has 12 Hoerr Ternp Criteria Beery Met? Y N
Has 72 Hour pH Criteria Been Me4
6IN ## 7 4' Setup Date: -iir- 0I� I q Removal FE-Ohl Bin Date: tr: a'11q
Date Time pH >12.0 rur 72 Hrs. TEMP. >52 Deg. CFor 12 Hrs. Operator
Initial PH: 1 , e�=fir- �� OL-m-tj
Corrected pH: fa. i F f • 5: eT 11 60: l0
Is-s,s' d 1r ;t Corrected pH: 0-4-�T tv €1
Has 12 Herr Temp Criteria Beeh MUt? N
Has 72 HOUr pH Criteria Been Met? .Y , N
BIBS f€ Setup Date: I Removal From Bin Date,
Date Time I pH>12.0For 72IMPS. TENT. >52 Deg, C For 12 Hrs. Operator
initial pH:
Corrected pH:
Final pil:
Corrected pH:
K—FIS 12 I` OUr Ternp Criteria Been Met.? Y N
Has 72 HOUr pl=l Criteria Been Met? y N
t31I�i ## Setup Date: Removal From Bin Date:
DateI -i-inle pH >12.0 For 72 l-IrS. TEMP. >52 Deg. C For 12 Ears. Operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:
Flas 12 Hour Temp Criteria Been Met? y N
Has 72 HOLU' pH Criteria Been Met? Y N
W

P RIS M Full -Service Analytical &
Environmental Solutions
R
City of Statesville, NC
Ken Galloway
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: Sludge (Hazardous Testing)
Lab Submittal Date: 08/07/2019
Prism Work Order: 9080093
Case Narrative
8/21 /19 13:44
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Herbicide analysis was subcontracted to AES. Reactivity analysis was subcontracted to GCAL.
Laboratory reports are attached.
Prism Summary of Detections does not include subcontracted data.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
)� 4 a_.
?-n--
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
A Negative, Pass
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 30

Sample Receipt Summary
r
Full -Service Analytical &
PRISM
Environmental Solutions
08/21/2019
Sao awroaie�, ma
Prism Work Order: 9080093
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled Date/Time Received
4th Creek Sludge
9080093-01
Solid
08/07/19 9:55 08/07/19 16:00
3rd Creek Sludge
9080093-02
Solid
08/07/19 9:45 08/07/19 16:00
Sta-Lime
9080093-03
Solid
08/07/19 9:30 08/07/19 16:00
Samples were received in good condition at 5.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 30

P R I S M Full -Service Analytical &
Laboratory Report
Environmental Solutions 08/21/2019
:� u�AroftiEaiHc
City of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID: 4th Creek Sludge
Attn: Ken Galloway Prism Sample ID: 9080093-01
P.O. Box 1111 Prism Work Order: 9080093
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/07/19 09:55
Time Submitted: 08/07/19 16:00
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
14.7
% by
0.100
0.100 1
*SM2540 G
8/16/19 8:30
EDV
P9H0264
Weight
Corrosivity-pH
5.4
pH Units
1
*9045D
8/9/19 13:40
BMS
P9H0161
Ignitability
BRLA
mm/sec
0.10
1
*1030
8/9/19 8:25
BMS
P9H0143
Temperature
22
pH Units
1
*9045D
8/9/19 13:40
BMS
P9H0161
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311 ZHE
8/13/19 7:30
TBL
P9H0174
TCLP Extraction
Complete
N/A
1
*1311
8/13/19 7:50
MMR
P9H0185
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000034
1
*7470A
8/15/19 14:09
MMR
P9H0261
Arsenic
BRL
mg/L
0.10
0.030
1
*6010D
8/13/19 17:06
JAB
PgH0203
Barium
BRL
mg/L
5.0
0.010
1
*6010D
8/13/19 17:06
JAB
PgH0203
Cadmium
BRL
mg/L
0.025
0.0020
1
*6010D
8/13/19 17:06
JAB
PgH0203
Chromium
BRL
mg/L
0.25
0.015
1
*6010D
8/13/19 17:06
JAB
PgH0203
Lead
BRL
mg/L
0.050
0.020
1
*6010D
8/13/19 17:06
JAB
PgH0203
Selenium
BRL
mg/L
0.15
0.063
1
*6010D
8/13/19 17:06
JAB
P9H0203
Silver
BRL
mg/L
0.25
0.0045
1
*6010D
8/13/19 17:06
JAB
P9H0203
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00090
1
*8081 B
8/14/19 16:49
ZRC
PgH0227
Dieldrin
BRL
mg/L
0.00050
0.000068
1
*8081 B
8/14/19 16:49
ZRC
P9H0227
Endrin
BRL
mg/L
0.00050
0.000068
1
*8081 B
8/14/19 16:49
ZRC
P9H0227
gamma-BHC
BRL
mg/L
0.00050
0.000030
1
*8081B
8/14/19 16:49
ZRC
PgH0227
Heptachlor
BRL
mg/L
0.00050
0.000065
1
*8081 B
8/14/19 16:49
ZRC
PgH0227
Heptachlor Epoxide
BRL
mg/L
0.00050
0.00011
1
*8081 B
8/14/19 16:49
ZRC
PgH0227
Methoxychlor
BRL
mg/L
0.00050
0.000090
1
*8081 B
8/14/19 16:49
ZRC
PgH0227
Toxaphene
BRL
mg/L
0.025
0.0018
1
*8081 B
8/14/19 16:49
ZRC
PgH0227
TCLP Semivolatile Organic Compounds by GUMS
Surrogate
Decachlorobiphenyl
Tetrachloro-m-xylene
Recovery
82 %
92 %
Control Limits
13-186
40-134
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0036
1
*8270E
8/13/19 18:07
JMV
P9H0193
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0045
1
*8270E
8/13/19 18:07
JMV
P9H0193
2,4-Dinitrotoluene
BRL
mg/L
0.012
0.0042
1
*8270E
8/13/19 18:07
JMV
P9H0193
2-Methylphenol
BRL
mg/L
0.050
0.0024
1
*8270E
8/13/19 18:07
JMV
P9H0193
3/4-Methyl phenol
BRL
mg/L
0.050
0.0025
1
*8270E
8/13/19 18:07
JMV
P9H0193
Hexachlorobenzene
BRL
mg/L
0.020
0.0039
1
*8270E
8/13/19 18:07
JMV
P9H0193
Hexachlorobutadiene
BRL
mg/L
0.050
0.0045
1
*8270E
8/13/19 18:07
JMV
P9H0193
Hexachloroethane
BRL
mg/L
0.050
0.0037
1
*8270E
8/13/19 18:07
JMV
P9H0193
Nitrobenzene
BRL
mg/L
0.050
0.0038
1
*8270E
8/13/19 18:07
JMV
P9H0193
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 3 of 30

PRISM Full -Service Analytical
Environmental Solutions
• Li160RATORI ' _
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
08/21/2019
Project: Sludge (Hazardous Testing) Client Sample ID: 4th Creek Sludge
Prism Sample ID: 9080093-01
Prism Work Order: 9080093
Sample Matrix: Solid Time Collected: 08/07/19 09:55
Time Submitted: 08/07/19 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Pentachlorophenol BRL mg/L 0.25 0.011 1 *8270E 8/13/19 18:07 JMV P9H0193
Pyridine BRL mg/L 0.25 0.0016 1 *8270E 8/13/19 18:07 JMV P9H0193
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
91 %
43-140
2-Fluorobiphenyl
97 %
44-119
2-Fluorophenol
65 %
19-119
Nitrobenzene-d5
90 %
44-120
Phenol-d5
42 %
11-52
Terphenyl-d14
98 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
mg/L
0.035 0.0035
1
*8260D
8/13/19 19:18
KDM
P9H0197
1,2-Dichloroethane
BRL
mg/L
0.025 0.0041
1
*8260D
8/13/19 19:18
KDM
P9H0197
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.0042
1
*8260D
8/13/19 19:18
KDM
P9H0197
Benzene
BRL
mg/L
0.025 0.0034
1
*8260D
8/13/19 19:18
KDM
P9H0197
Carbon Tetrachloride
BRL
mg/L
0.025 0.0055
1
*8260D
8/13/19 19:18
KDM
P9H0197
Chlorobenzene
BRL
mg/L
5.0 0.0034
1
*8260D
8/13/19 19:18
KDM
P9H0197
Chloroform
BRL
mg/L
0.30 0.0048
1
*8260D
8/13/19 19:18
KDM
P9H0197
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/L
10 0.0078
1
*8260D
8/13/19 19:18
KDM
P9H0197
Tetrachloroethylene
BRL
mg/L
0.035 0.0031
1
*8260D
8/13/19 19:18
KDM
P9H0197
Trichloroethylene
BRL
mg/L
0.025 0.0046
1
*8260D
8/13/19 19:18
KDM
P9H0197
Vinyl chloride
BRL
mg/L
0.010 0.0041
1
*8260D
8/13/19 19:18
KDM
P9H0197
Surrogate
Recovery Control Limits
4-Bromofluorobenzene 103 % 80-124
Dibromofluoromethane 107 % 75-129
Toluene-d8 94 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 30

PRISM Full -Service Analytical
Environmental Solutions
• Li160RATORI ' _
Laboratory Report
08/21/2019
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Sludge (Hazardous Testing)
Sample Matrix: Solid
Client Sample ID: 3rd Creek Sludge
Prism Sample ID: 9080093-02
Prism Work Order: 9080093
Time Collected: 08/07/19 09:45
Time Submitted: 08/07/19 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
18.6
% by 0.100
0.100 1
*SM2540 G
8/16/19 8:30
EDV
P9H0264
Weight
Corrosivity-pH
4.4
pH Units
1
*9045D
8/9/19 13:40
BMS
P9H0161
Ignitability
BRLA
mm/sec 0.10
1
*1030
8/9/19 8:25
BMS
P9H0143
Temperature
22
pH Units
1
*9045D
8/9/19 13:40
BMS
P9H0161
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311 ZHE
8/13/19 7:30
TBL
P9H0174
TCLP Extraction
Complete
N/A
1
*1311
8/13/19 7:50
MMR
P9H0185
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000034
1
*7470A
8/15/19 13:57
MMR
PgH0261
Arsenic
BRL
mg/L
0.10
0.030
1
*6010D
8/13/19 17:13
JAB
PgH0203
Barium
BRL
mg/L
5.0
0.010
1
*6010D
8/13/19 17:13
JAB
PgH0203
Cadmium
BRL
mg/L
0.025
0.0020
1
*6010D
8/13/19 17:13
JAB
PgH0203
Chromium
BRL
mg/L
0.25
0.015
1
*6010D
8/13/19 17:13
JAB
PgH0203
Lead
BRL
mg/L
0.050
0.020
1
*6010D
8/13/19 17:13
JAB
P9H0203
Selenium
BRL
mg/L
0.15
0.063
1
*6010D
8/13/19 17:13
JAB
P9H0203
Silver
BRL
mg/L
0.25
0.0045
1
*6010D
8/13/19 17:13
JAB
P9H0203
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00090
1
*8081 B
8/14/19 17:00
ZRC
PgH0227
Dieldrin
BRL
mg/L
0.00050
0.000068
1
*8081 B
8/14/19 17:00
ZRC
PgH0227
Endrin
BRL
mg/L
0.00050
0.000068
1
*8081 B
8/14/19 17:00
ZRC
PgH0227
gamma-BHC
BRL
mg/L
0.00050
0.000030
1
*8081B
8/14/19 17:00
ZRC
PgH0227
Heptachlor
BRL
mg/L
0.00050
0.000065
1
*8081 B
8/14/19 17:00
ZRC
PgH0227
Heptachlor Epoxide
BRL
mg/L
0.00050
0.00011
1
*8081 B
8/14/19 17:00
ZRC
PgH0227
Methoxychlor
BRL
mg/L
0.00050
0.000090
1
*8081 B
8/14/19 17:00
ZRC
P9H0227
Toxaphene
BRL
mg/L
0.025
0.0018
1
*8081 B
8/14/19 17:00
ZRC
P9H0227
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
82 %
13-186
Tetrachloro-m-xylene
83 %
40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0036
1
*8270E
8/13/19 18:30
JMV
P9H0193
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0045
1
*8270E
8/13/19 18:30
JMV
P9H0193
2,4-Dinitrotoluene
BRL
mg/L
0.012
0.0042
1
*8270E
8/13/19 18:30
JMV
P9H0193
2-Methylphenol
BRL
mg/L
0.050
0.0024
1
*8270E
8/13/19 18:30
JMV
P9H0193
3/4-Methyl phenol
BRL
mg/L
0.050
0.0025
1
*8270E
8/13/19 18:30
JMV
P9H0193
Hexachlorobenzene
BRL
mg/L
0.020
0.0039
1
*8270E
8/13/19 18:30
JMV
P9H0193
Hexachlorobutadiene
BRL
mg/L
0.050
0.0045
1
*8270E
8/13/19 18:30
JMV
P9H0193
Hexachloroethane
BRL
mg/L
0.050
0.0037
1
*8270E
8/13/19 18:30
JMV
P9H0193
Nitrobenzene
BRL
mg/L
0.050
0.0038
1
*8270E
8/13/19 18:30
JMV
P9H0193
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 30

PRISM Full -Service Analytical
Environmental Solutions
• Li160RATORI ' _
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
08/21/2019
Project: Sludge (Hazardous Testing) Client Sample ID: 3rd Creek Sludge
Prism Sample ID: 9080093-02
Prism Work Order: 9080093
Sample Matrix: Solid Time Collected: 08/07/19 09:45
Time Submitted: 08/07/19 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Pentachlorophenol BRL mg/L 0.25 0.011 1 *8270E 8/13/19 18:30 JMV P9H0193
Pyridine BRL mg/L 0.25 0.0016 1 *8270E 8/13/19 18:30 JMV P9H0193
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
106 %
43-140
2-Fluorobiphenyl
106 %
44-119
2-Fluorophenol
72 %
19-119
Nitrobenzene-d5
94 %
44-120
Phenol-d5
46 %
11-52
Terphenyl-d14
98 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
mg/L
0.035 0.0035
1
*8260D
8/13/19 19:52
KDM
P9H0197
1,2-Dichloroethane
BRL
mg/L
0.025 0.0041
1
*8260D
8/13/19 19:52
KDM
P9H0197
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.0042
1
*8260D
8/13/19 19:52
KDM
P9H0197
Benzene
BRL
mg/L
0.025 0.0034
1
*8260D
8/13/19 19:52
KDM
P9H0197
Carbon Tetrachloride
BRL
mg/L
0.025 0.0055
1
*8260D
8/13/19 19:52
KDM
P9H0197
Chlorobenzene
BRL
mg/L
5.0 0.0034
1
*8260D
8/13/19 19:52
KDM
P9H0197
Chloroform
BRL
mg/L
0.30 0.0048
1
*8260D
8/13/19 19:52
KDM
P9H0197
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/L
10 0.0078
1
*8260D
8/13/19 19:52
KDM
P9H0197
Tetrachloroethylene
BRL
mg/L
0.035 0.0031
1
*8260D
8/13/19 19:52
KDM
P9H0197
Trichloroethylene
BRL
mg/L
0.025 0.0046
1
*8260D
8/13/19 19:52
KDM
P9H0197
Vinyl chloride
BRL
mg/L
0.010 0.0041
1
*8260D
8/13/19 19:52
KDM
P9H0197
Surrogate
Recovery Control Limits
4-Bromofluorobenzene 104 % 80-124
Dibromofluoromethane 104 % 75-129
Toluene-d8 95 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 30

PRISM Full -Service Analytical
Environmental Solutions
• Li160RATORI ' _
Laboratory Report
08/21/2019
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Sludge (Hazardous Testing)
Sample Matrix: Solid
Client Sample ID: Sta-Lime
Prism Sample ID: 9080093-03
Prism Work Order: 9080093
Time Collected: 08/07/19 09:30
Time Submitted: 08/07/19 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
76.6
% by 0.100
0.100 1
*SM2540 G
8/16/19 8:30
EDV
P9H0264
Weight
Corrosivity-pH
12
pH Units
1
*9045D
8/9/19 13:40
BMS
P9H0161
Ignitability
BRLA
mm/sec 0.10
1
*1030
8/9/19 8:25
BMS
P9H0143
Temperature
22
pH Units
1
*9045D
8/9/19 13:40
BMS
P9H0161
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311 ZHE
8/13/19 7:30
TBL
P9H0174
TCLP Extraction
Complete
N/A
1
*1311
8/13/19 7:50
MMR
P9H0185
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000034
1
*7470A
8/15/19 14:12
MMR
PgH0261
Arsenic
BRL
mg/L
0.10
0.030
1
*6010D
8/13/19 17:21
JAB
PgH0203
Barium
BRL
mg/L
5.0
0.010
1
*6010D
8/13/19 17:21
JAB
PgH0203
Cadmium
BRL
mg/L
0.025
0.0020
1
*6010D
8/13/19 17:21
JAB
PgH0203
Chromium
BRL
mg/L
0.25
0.015
1
*6010D
8/13/19 17:21
JAB
PgH0203
Lead
BRL
mg/L
0.050
0.020
1
*6010D
8/13/19 17:21
JAB
P9H0203
Selenium
BRL
mg/L
0.15
0.063
1
*6010D
8/13/19 17:21
JAB
P9H0203
Silver
BRL
mg/L
0.25
0.0045
1
*6010D
8/13/19 17:21
JAB
P9H0203
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00090
1
*8081 B
8/14/19 17:12
ZRC
PgH0227
Dieldrin
BRL
mg/L
0.00050
0.000068
1
*8081 B
8/14/19 17:12
ZRC
PgH0227
Endrin
BRL
mg/L
0.00050
0.000068
1
*8081 B
8/14/19 17:12
ZRC
PgH0227
gamma-BHC
BRL
mg/L
0.00050
0.000030
1
*8081B
8/14/19 17:12
ZRC
PgH0227
Heptachlor
BRL
mg/L
0.00050
0.000065
1
*8081 B
8/14/19 17:12
ZRC
PgH0227
Heptachlor Epoxide
BRL
mg/L
0.00050
0.00011
1
*8081 B
8/14/19 17:12
ZRC
PgH0227
Methoxychlor
BRL
mg/L
0.00050
0.000090
1
*8081 B
8/14/19 17:12
ZRC
P9H0227
Toxaphene
BRL
mg/L
0.025
0.0018
1
*8081 B
8/14/19 17:12
ZRC
P9H0227
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
75 %
13-186
Tetrachloro-m-xylene
97 %
40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0036
1
*8270E
8/13/19 18:53
JMV
P9H0193
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0045
1
*8270E
8/13/19 18:53
JMV
P9H0193
2,4-Dinitrotoluene
BRL
mg/L
0.012
0.0042
1
*8270E
8/13/19 18:53
JMV
P9H0193
2-Methylphenol
BRL
mg/L
0.050
0.0024
1
*8270E
8/13/19 18:53
JMV
P9H0193
3/4-Methyl phenol
BRL
mg/L
0.050
0.0025
1
*8270E
8/13/19 18:53
JMV
P9H0193
Hexachlorobenzene
BRL
mg/L
0.020
0.0039
1
*8270E
8/13/19 18:53
JMV
P9H0193
Hexachlorobutadiene
BRL
mg/L
0.050
0.0045
1
*8270E
8/13/19 18:53
JMV
P9H0193
Hexachloroethane
BRL
mg/L
0.050
0.0037
1
*8270E
8/13/19 18:53
JMV
P9H0193
Nitrobenzene
BRL
mg/L
0.050
0.0038
1
*8270E
8/13/19 18:53
JMV
P9H0193
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 30

PRISM Full -Service Analytical
Environmental Solutions
• Li160RATORI ' _
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
08/21/2019
Project: Sludge (Hazardous Testing) Client Sample ID: Sta-Lime
Prism Sample ID: 9080093-03
Prism Work Order: 9080093
Sample Matrix: Solid Time Collected: 08/07/19 09:30
Time Submitted: 08/07/19 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Pentachlorophenol BRL mg/L 0.25 0.011 1 *8270E 8/13/19 18:53 JMV P9H0193
Pyridine BRL mg/L 0.25 0.0016 1 *8270E 8/13/19 18:53 JMV P9H0193
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
114 %
43-140
2-Fluorobiphenyl
104 %
44-119
2-Fluorophenol
73 %
19-119
Nitrobenzene-d5
92 %
44-120
Phenol-d5
46 %
11-52
Terphenyl-d14
95 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
mg/L
0.035 0.0035
1
*8260D
8/13/19 20:26
KDM
P9H0197
1,2-Dichloroethane
BRL
mg/L
0.025 0.0041
1
*8260D
8/13/19 20:26
KDM
P9H0197
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.0042
1
*8260D
8/13/19 20:26
KDM
P9H0197
Benzene
BRL
mg/L
0.025 0.0034
1
*8260D
8/13/19 20:26
KDM
P9H0197
Carbon Tetrachloride
BRL
mg/L
0.025 0.0055
1
*8260D
8/13/19 20:26
KDM
P9H0197
Chlorobenzene
BRL
mg/L
5.0 0.0034
1
*8260D
8/13/19 20:26
KDM
P9H0197
Chloroform
BRL
mg/L
0.30 0.0048
1
*8260D
8/13/19 20:26
KDM
P9H0197
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/L
10 0.0078
1
*8260D
8/13/19 20:26
KDM
P9H0197
Tetrachloroethylene
BRL
mg/L
0.035 0.0031
1
*8260D
8/13/19 20:26
KDM
P9H0197
Trichloroethylene
BRL
mg/L
0.025 0.0046
1
*8260D
8/13/19 20:26
KDM
P9H0197
Vinyl chloride
BRL
mg/L
0.010 0.0041
1
*8260D
8/13/19 20:26
KDM
P9H0197
Surrogate
Recovery Control Limits
4-Bromofluorobenzene 101 % 80-124
Dibromofluoromethane 88 % 75-129
Toluene-d8 96 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 30

Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P9H0264
30
g
30 g
08/15/19 15:05
9080093-02
P9H0264
30
g
30 g
08/15/19 15:05
9080093-03
P9H0264
30
g
30 g
08/15/19 15:05
Prep Method: 1311
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P9H0185
100
g
2000 mL
08/12/19 15:45
9080093-01
P9H0174
12.5
g
250 mL
08/12/19 13:40
9080093-02
P9H0174
12.5
g
250 mL
08/12/19 13:40
9080093-02
P9H0185
100
g
2000 mL
08/12/19 15:45
9080093-03
P9H0185
100
g
2000 mL
08/12/19 15:45
9080093-03
P9H0174
12.5
g
250 mL
08/12/19 13:40
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
PgH0203
10
mL
50 mL
08/13/19 10:43
9080093-02
PgH0203
10
mL
50 mL
08/13/19 10:43
9080093-03
PgH0203
10
mL
50 mL
08/13/19 10:43
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
PgH0261
20
mL
30 mL
08/15/19 10:30
9080093-02
PgH0261
20
mL
30 mL
08/15/19 10:30
9080093-03
PgH0261
20
mL
30 mL
08/15/19 10:30
Prep Method: 3510C GC
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
PgH0227
200
mL
10 mL
08/14/19 9:08
9080093-02
P9H0227
200
mL
10 mL
08/14/19 9:08
9080093-03
P9H0227
200
mL
10 mL
08/14/19 9:08
Prep Method: 3510C MS
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P9H0193
200
mL
1 mL
08/13/19 10:30
9080093-02
P9H0193
200
mL
1 mL
08/13/19 10:30
9080093-03
P9H0193
200
mL
1 mL
08/13/19 10:30
Prep Method: 5030B
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P9H0197
1
mL
10 mL
08/13/19 8:19
9080093-02
P9H0197
1
mL
10 mL
08/13/19 8:19
9080093-03
P9H0197
1
mL
10 mL
08/13/19 8:19
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 30

Subcontracted Analyses
The following analyses were subcontracted to Analytical Environmental Services, Inc.
Lab Number
Analysis
9080093-01 Herbicides TCLP (Sub)
9080093-02 Herbicides TCLP (Sub)
9080093-03 Herbicides TCLP (Sub)
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Lab Number
Analysis
9080093-01
Reactivity, Cyanide (Sub)
9080093-01
Reactivity, Sulfide (Sub)
9080093-02
Reactivity, Cyanide (Sub)
9080093-02
Reactivity, Sulfide (Sub)
9080093-03
Reactivity, Cyanide (Sub)
9080093-03
Reactivity, Sulfide (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 30

Full -Service Analytical &
I
CHAIN OF CUSTODY RECORD
LAB USE ONLY
t'PRISM
Environmental Solutions
PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING.
YES
Iv,
LABORATORIES INC
Samples INTACT upon arrival?
449 Springbrook Road - Charlotte, NC 28217
Phone [phone] - Fax: [phone]
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
Received ON WET ICE?
PROPER PRESERVATIVES indicated? L
Client Company Name: C-*4V a S4a 4 es
'Please ATTACH any project specific reporting (QC LEVEL I II III IV)
Received WITHIN HOLDING TIMES?
Report To/Contact Name: '1(dn Ca li}w
provisions and/or QC Requirements
CUSTODY SEALS INTACT?
,
Reporting Address:
Invoice To:
---
VOLATILES rec'd W/OUT HEADSPACE?
_—
Address:
PROPER CONTAINS S used?
TEMP: Therm ID:/ r' Observed: s ' � °C
Phone: 704-97 $- 3`!3V Fax es (No): 70'tf- $°i $- U55
Email Address:
purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
EDD Type: PDF Excel Other
Requested Due Date ❑ ❑ ❑ 1 Day 2 Days ❑ 3 Days 4 Days El Days
"Working
Certification: NELAC DoD FL
NC
Site Location Name: FCrur-4 h C rr n
Rush Work Must Be
Days" ❑ 6a9 Days CI Standard 1{l days ❑ Pre -Approved
Sc OTHER
Samples received after 14:00 will he processed next business day.
N/A
Site Location Physical Address: �
Tumarcund time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES NO
(SEE REVERSE FOR TERMS a CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, )NC. TO CLIENT)
Sample Iced Upon Collection: YES_ NO
CLIENT
TIME
DATE COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
ANALYSIS REQUESTED
f
PRISM
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
"TYPE
TIVES
REMARKS
LAB
HOURS
SLUDGE)
SEE BELOW
NO.
SIZE
J%f
ID NO.
8-749
09,65
G
`�'
�;
b
T(%__ L P
U I
3,91 CQFt k S i,
SfA-P
8- 7- Iq f O9%'V5
5- 7-19 I 0 9:
ICor osi. i —
G
rclF1 m
G- S e V [7
Sampler's Signature 0 Sampled By (Print Name)
Upon relinquishing, this Chain of Custody is your authorization for Prism to proc
submitted in writing to the Prism Project Manager. There will be charaes kn'A v
N
For
n f-Ugrocl< I Affiliation
sed with the analyses as requested above. Any changes must be
changes after analyses have been initialized.
%MFMA
rx-anrpmvn[• NOTE- ALL SAMPLE COOLERS SHOULD 8E TAPED SWUT WITH CUSTODY SEALS FOR SPORTATION TO 7HE TORY. t: Gmtlp Nc.
ZSAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT T BORATORY.
ElHand-deliveredEl Prism Field Service ❑ 01" J
wo E❑ SC ❑❑ NC ❑ SC ❑❑ INC ❑ SCAR ❑ NC I❑ SC I ❑ N ; ❑ SIC E. ❑NBC ❑ SC ❑ N ; ❑ SIC ❑ NC F❑ SC ❑ N OTHp SC
❑ I I❑ I❑
TAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments:
Site Arrival Time:
Site Departure Time:
Field Tech Fee:
Mileage:
ORIGINAI

1.1
ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
ATTENTION
RobbiJones
PROJECTID
9080093
LABORATORY REPORT NUMBER
219081317
DATE
08/16/2019
Primary Data Review By
Authorized Signature
PLEASE NOTE;
Secondary Data Review By
Ashley B. Amick
Project Manager, Access Analytical, Inc.
[e-mail]
- Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL),
7979 Innovation Park Dr., Baton Rouge, LA 70820.
- GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955,
NELAP certified laboratory # 01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be
directed to your local Access Analytical representative at 803.781.4243 or toll free at 888 315.4243
Lab Report#: 219081317
Page 12 of 30

4"" (SC,&L
Af
LELAP CERTIFICATE NUMBER: 01955
DOD -FLAP ACCREDITATION NUMBER: 74960
ANALYTICAL RESULTS
Deliver To
Robbi Jones
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
800-529-6364
1*.Mk
PJ LA
Testing
Ckib EIAP
PERFORMED BY
GCAL, LLC
7979 innovation Park Dr.
Baton Rouge, LA 70820
[phone]
Report Date 08/16/2019
GOAL Report 2190813q17
I III I II III II II III I II III
Project 9080093
Additional Recipients
NONE
;,CCRk-e
d
Lab Report#: 219081317 Page 2 of 12
Page 13 of 30

�q% ���� Report#: 219081317
Project ID: 9080093
Laboratory Endorsement
Report Date: 08/16/2019
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with GCAL's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or] Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
* Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis —when appended to Client Sample ID
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in
full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results
are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
— //?/ /,Z - �'�/ 2 � -
Authorized Signature
GCAL Report 219081317
Lab Report#: 219081317 Page 14 of 30

I GC&L
Report#: 219081317
Project ID: 9080093
Certifications
Report Date: 08/16/2019
Certification
Certification Number
DOD ELAP
74960
Alabama
01955
Arkansas
88-0655
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
Washington
C929
USDA Soil Permit
P330-16-00234
Lab Report#: 219081317 Page 4 of
Page 15 of 30

�1% Report#: 219081317
GCAL
Project ID: 9080093
Case Narrative
Client: Access Analytical Report: 219081317
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
Report Date: 08/16/2019
Lab Report#: 219081317
Page 16 of 30

GCAL Report#: 219081317
Project ID: 9080093
Sample Summary
Report Date: 08/16/2019
GCAL ID
Client ID
Matrix
. Collect Date/Time
Receive Date/Time
21908131701
4th Creek Sludge
Solid
08/07/2019 09:55
08/13/2019 10:20
21908131702
3rd Creek Sludge
Solid
08/07/2019 09:45
08/13/2019 10:20
21908131703
Sta-Lime
Solid
08/07/2019 09:30
08/13/2019 10:20
Lab Report#: 219081317
Page 17 of 30

0'04 GCA& Report#: 219081317
ProjectID: 9080093
Summary of Compounds Detected
No analytes were detected for analyses performed by GCAL.
Report Date: 08/16/2019
Lab Report#: 219081317
Page 18 of 30

Q� GCAL
4th Creek Sludge
EPA 9012B
Report#: 219081317
Project ID: 9080093
Sample Results
Collect Date 08/07/2019 09:55
Receive Date 08/13/2019 10:20
Report Date: 08/16/2019
GCAL ID 21908131701
Matrix Solid
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch `
08/16/2019 08:00 665475 EPA 7.3.3.2 (1997) 1 08/16/2019 14:48 MOS 665678 Ej
CAS#
57-12-5R
EPA 9034
Parameter
Reactivity Cyanide
Result DL LOQ Units
248U 248 248 mg/kg
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
08/16/2019 08:00 665476 EPA 7.3.4.2 (1997) 1 08/16/2019 13:16 RYC 665676
CAS# Parameter
18496-25-8R Reactivity Sulfide
F3rd Creek Sludge
EPA 9012B
Result
DL
LOQ
Units
248U
248
248
mg/kg
Collect Date 08/07/2019 09:45 GCAL ID 21908131702
Receive Date 08/13/2019 10:20 Matrix Solid
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
08/16/2019 08:00 665475 EPA 7.3.3.2 (1997) 1 08/16/2019 14:50 MOS 665678
CAS#
57-12-5R
EPA 9034
Parameter
Reactivity Cyanide
Result DL LOQ Units
250U 250 250 mg/kg
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
08/16/2019 08:00 665476 EPA 7.3.4 2 (1997) 1 08/16/2019 13:16 RYC 665676
CAS# Parameter
18496-25-8R Reactivity Sulfide
Result DL LOQ Units
250U 250 250 mg/kg
Lab Report#: 219081317
Page 8 of 12
Page 19 of 30

Report#: 219081317
Project ID: 9080093
Sample Results
Report Date: 08/16/2019
Sta-Lime Collect Date 08/07/2019 09:30 GCAL ID 21908131703
Receive Date 08/13/2019 10:20 Matrix Solid
EPA 9012B
Prep Date
Prep Batch Prep Method
Dilution Analysis Date
By Analytical Batch
08/16/2019 08:00
665475 EPA 7.3.3.2 (1997)
1 08/16/2019 14:53
MOS 665678
CAS#
Parameter
Result
DL LOQ Units
57-12-5R
Reactivity Cyanide
248U
248 248 mg/kg
GDA 00'ZA
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
08/16/2019 08:00 665476 EPA 7.3.4.2 (1997) 1 08/16/2019 13:16 RYC 665676
CAS# Parameter
18496-25-8R Reactivity Sulfide
Result DL LOQ Units
248U 248 248 mg/kg
Lab Report#:219081317
Page 20 of 30

(SCAL
Report#: 219081317
Project ID: 9080093
General Chemistry QC Summary
Report Date: 08/16/2019
Analytical Batch Client ID
MB665476
LCS665476
665676 GCALID
1952122
1952123
Prep Batch Sample Type
MB
LCS
665476 Prep Date
08/16/2019 08:00
08/16/2019 08:00
Prep Method Analysis Date
08/16/2019 13:16
08/16/2019 13:16
EPA 7.3.4.2 (1997) Matrix
Solid
Solid
EPA 9034
Units
mg/kg
Spike Result
I
%R
I
I Control
Result
DL
Added
Limits%R
Reactivity Sulfide 18496-25-8R
250U
250
10001 1026
103
47 - 135
Analytical Batch Client ID
MB665475
LCS665475
665678 GCALID
1952119
1952120
Prep Batch Sample Type
MB
LCS
665475 Prep Date
08/16/2019 08:00
08/16/2019 08:00
Prep Method Analysis Date
08/16/2019 14:39
08/16/2019 14:41
EPA 7.3.3.2 1997 Matrix
Solid
Solid
EPA 9012B
Units mg/kg
Spike
Result
%R
Control
Result DL
Added
Limits°/uR
Reactivity Cyanide 57-12-5R
NDI 250
250
29.41
12
1 1 - 25
Lab Report#: 219081317 Page 10 of 12
Page 21 of 30

I—
tn
o-
M
m
co
coo
Client ID: 4565 - Access Analytical
1
SDG: 219081317
PM' DLH
al &
1 £null At mentalnalyti
5�. 1. k A
SUBCONTRACT ORDER
Prism
Ccrtfe,;lticet 1 . C
Laboratories, Inc.
I'S=tCF
Oil
9080093 N/.-t
NFAr f "r; I,•+t10R.%T0rY
R EM. VSNV Li ++, 7RY_ .
Pljsni Labtnatm ies, lnc.
Gulf Coast Analytical Labs, ➢:c.
P. O. Bux 240543
10781 Course_v Btvd
Charlouc, NC 23224-0543
Balon Rougc, LA 70516
Phonc: SOO-529-6364
Phonc :[phone]
Fax: [phone]
Fax: [phone]
Project T4mngct: Robbi A. ]ones
Analysis Due
Expires
Comments
Labm(a/torry IDl�
C
Sample ID: 9080093-01 Solid
Sampled: 09/07/1909:55
Reactivity, Sulfide (Sub)
03/14lI9 09:55
Reactivity, Cyanide (Sub)
OS12U19 09:55
t-rlrcdmr Sgjt 4T? -
i —
r GnCtr
Sample ID: 9030093-02 Solid
SatnpleJ: 08/07119 09:45
d
Reactivity. Suirrde (SW-
OS/14i19 09:45
11cactivityi Cyanide (Sub)
08n [A9 09:45
Cnnluiavr Supph-Fed.,
Sdmpk ICI: 9080093-03
Solid
Sampled: 08/0M9 09:30
OSll4i19 09:30
R-eti:•ity, Sulfide (Sub)
Rcactivi[y, Cyanide (Sub)
OM ]l19 09:30
Cr rlminrlJ.S:rp;llicdr
Released By /
Data
^ • • •'eca R; l'
44
't
1celcnscd Il+
Ytit
Recei'J RI �� l J D,r,c
Rc!cased lly
Dim
i cccn:d 0: Date
Re!eued Py
Dane
Rccrr. ml 13v De.
Paae 1 of 1
Page 22 of 30

4� GCAL
SAMPLE RECEIVING CHECKLIST
IIII II III III II
III I
I II II
* 2 1 9 0 8 1
3 1
7
CHECKLIST
YES
NO
SAMPLE DELIVERY GROUP
I
219081317
Client PM DLH
Transport Method f
Samples received with proper thermal preservation?
❑v
❑
4565 - Access Analytical
F®DC
Radioactivity is <1600 cpm? If no, record cpm value in notes section.
COC relinquished and complete (including samplelDs, collect times, and sampler)?
Q
0
❑
❑
Profile Number
Received ®jr
80251
Savage, Tiffany R
All containers received in good condition and within hold time?
All sample labels and containers received match the chain of custody?
0
0
❑
❑
Line Item(s)
Receive Date(s)
2 - Solid
08/13/19
Preservative added to any containers?
❑
0
If received, was headspace for VOC water containers < 6mm?
0
❑
Samples collected in containers provided by GCAL?
❑
COOLERS
DISCREPANCIES
LAB PRESERVATIONS
Airbill Thermometer ID: E34
Temp °C
None
None
T/59-6349-3542
0.2
NOTES
Fbvision 1.6
Page 1 of 1
Lab Report#: 219081317 Page 12 of 12

Acass
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
ATTENTION
Robbi A. Jones
PROJECT ID
9080093
LABORATORY REPORT NUMBER
190801
DATE
August 19, 2019
Primary Data Review By Secondary Data Review By
�' Ashley Amick
Chris Pafford
Project Manager, Access Analytical
Project Manager, AES [e-mail]
PLEASE NOTE:
Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, INletals, PCNI Asbestos,
Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal)
Direct Examination.
Local support services for this project are provided by Access Analytical; Inc. Access Analytical is a
representative ofAES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll tee at 883.315.4243
Page 24 of 30

rL q-P n 9 I (2. Eo< �C-6
R 1 S n %p EService Analytical 8
I v � Environmental Solutions
_. IASOWUNE$IVC
SUBCONTRACT ORDER
CcrtilicaIlru_ 'CELAC I'1SACE_
Prism
Laboratories, Inc.
N >� SC_ Other
9080093
N/A
SF.s NC: LARORATORY:
11WEIF11yG L Tj() iATDRY:
Prism Laboratories, Inc.
Analytical Lnvironmental Services, hle,
P. 0. Box 240543
30SO Presidential Parkway
Charlotte, NC 28224-0543
Atlanta, GA 30340
Phonc: 800-529-6364
Phonc :[phone]
Fax: [phone]
Fax: NA
Projcc(Munager. Rabbi A. Jones
V
Analvsis
Due
Expires
Laboratory ID Comments
Sample ID: 9080093-01
Solid
Sampled: 09/07/19 09:55
Ilclbicidca TCLP (Sub)
031,4119 09:55
l_•nll/nine•I',c
T
fI�a{JI�J�
Sample ID: 9080093-02
Solid
Sampled: 08/07/19 09:45
�i
llerbicidec TCLP (Sub)
0811M) 9 09:45
Conmbmrr.5i,ppl ed:
p••
Sample ID: 9080093-03
Solid
Sampled: 08107/I9 09:39
HCibicidcs TCLP (Sub)
03/ 4/19 0 9:3 0
Cmm�iuertc suppli.•d:
20
t'k L--f-
Re�ez,:d B�•
Rcic scd By
Rc c:.::d R,
8 -I % ./.:) a 6,1�_
Unte Rcc._'\od 3v
Date Rcecived By }i i�S
Darc Fs),
C,..:c Rcceircct F. v
Date
Page 1 of '
Pag Page 25 of 30

Analytical Environmental Services, Inc
Date: 19-Aug-19
Client:
Prism Laboratories
Client Sample ID:
4th Creek Sludge
Lab Order
190801
Tag Number:
9080093-01
Project Name:
9080093
Collection Date:
8/7/2019 9:55:00 AM
Lab ID:
190801-001A
Matrix:
Solid
Analyses Result Qual MDL Reporting Units BatchID DF Date Analyzed Analyst
Limit
HERBICIDES, TCLP SW1311/8151A
2,4,5-TP (Silvex) BRL
2,4-D BRL
Surr: DCAA 69 1
Qualifiers: ' Va l ue exceeds maximum cofnaminanl l eel
BRL Not Defected u NIDL
H Holding lanes for preparation or analNsfs exceeded
N Anah9c not NELAC cendied
D Anah to detected in the associated method blank
(SW3510C)
0.030 020 mg/L 283568 1 08/16/201914:32 HB
0.051 0.20 mg/L 283568 1 08/16/201914:32 HB
0 49.4-120 %REC 283568 1 08/16/201914:32 HB
E Estimated %slue above quantitation range
S Spike Recovery outside limns due to mafnx
> Greater than Result salue
J Estimated salue detected bclo\v Reporting Lunn
< Less than Result %clue
Page Page 26 of 30

Analytical Environmental Services, Inc
Date: 19-Aug-19
Client:
Prism Laboratories
Client Sample ID:
3rd Creek SLUDGE
Lab Order
190801
Tag Number:
9080093-02
Project Name:
9080093
Collection Date:
W12019 9:45:00 AM
Lab ID:
1908C31-002A
Matrix:
Solid
Analyses Result Reporting
y Qual MDL Limit Units BatchID DF Date Analyzed Analyst
HERBICIDES, TCLP SW1311/8151A
2,4,5-TP (Silvex) BRL
2,4-D BRL
Surr: DCAA 65.6
Qualifiers: ' Value exceeds maximum contaminant level
BRL Not Detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
(SW3510C)
0.030 0.20 mg/L 283568 1 08/16/201914:53 HB
0.051 0.20 mp/L 283568 1 08/16/201914:53 HB
0 49.4-120 %REC 283568 1 08/16/201914:53 HB
E Estimated value above quantization range
S Spike Recovery outside limits due to matrix
> Greater than Result value
J Estimated value detected below Reporting Limit
< Less dean Result value
Page 27 of 30

Analytical Environmental Services, Inc
Date: 19-Aug-19
Client:
Prism Laboratories
Client Sample ID:
Sta-Lime
Lab Order
190801
Tag Number:
9080093-03
Project Name:
9080093
Collection Date:
8n12019 9:30:00 AM
Lab ID:
1908C31-003A
Matrix:
Solid
Analyses
Result
Qual MDL
ReportingUnits
Limit
BatchID
DF Date Analyzed
Analyst
HERBICIDES, TCLP SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex)
BRL
0.030
0.20
mg/L 283568
1 08/16/2019 15:14
HB
2,4-D
BRL
0.051
0.20
mg/L 283568
1 08/16/2019 15:14
HB
Surr: DCAA
662
0
49.4-120
%REC 283568
1 08/16/2019 15:14
HB
Qualifiers: ' Value exceeds maximum contaminant level E Estimated value above quantitation range
BRL Not Detected at MDL S Spike Recovery outside limits due to matrix
H Holding times for preparation or analysis exceeded > Greater than Result value
N Ana lyre not NELAC certified J Estimated value detected below Reponmg Limit
B Analvte detected in the associated method blank < Less than Result value
Pag Page 28 of 30

Clear Save as
A NA LYCI CA f.
r`.N1T HDI� i1iF ti'I',1L
AF.S St:z VICTIS. rtit. SAMPLE/COOLER RECEIPT CHECKLIST
1. Client Name: ACCE?SS Analytical, Inc. AES Work Order Number: 190801
2. Carrier: FedEx E ups ❑ usps ❑ Client ❑ Courier❑ Othei
Yes No N/A Details Comments
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
Shipping container/cooler received in good condition?
.•
10damaged
❑ leaking ❑ other❑
Custody seals present on shipping container?
i
Custody seals intact on shipping container?
•
Temperature blanks present?
■
Cooler temperature(s) within limits of 0-690 [See item 13 and 14 for
temperature recordings.]
©
Cooling initiated for recently collected samples / ice
present ❑
Chain of Custody (COC) present?
■
Chain of Custody signed, dated, and timed when relinquished and received?
•
Sampler name and/or signature on COC?
Were all samples received within holding time?
I
TAT marked on the COC?
If no TAT indicated, proceeded with standard TAT per Terms & Conditions. ■
13. Cooler 1 Temperature 0.7 °C Cooler 2 Temperature
14. Cooler 5 Temperature °C Cooler 6 Temperature
15 Comments.-
16.
17,
18.
19.
20.
21.
22.
23.
24
25.
26.
°C Cooler 3 Temperature °C Cooler 4 Temperature °C
°C Cooler 7 Temperature °C Cooler 8 Temperature °C
I certify that I have completed sections 1-15 (dated initials).
Yes No N/A Details Comments
Were sample containers intact upon receipt?
•
Custody seals present on sample containers?
Custody seals intact on sample containers?
0•
Do sample container labels match the COC?
G)
®
®
incomplete info ❑ illegible ❑
no label ❑ other ❑
Are analyses requested indicated on the COC?
■
Were all of the samples listed on the COC received?
(D
0
®
samples received but not listed on COC
samples listed on COC not received
Was the sample collection date/time noted?
•
Did we receive sufficient sample volume for indicated analyses?
•
Were samples received in appropriate containers?
■
Were VOA samples received without headspace (< 1/4" bubble)?
•
Were trip blanks submitted?
o
•
Ilisted on COC ❑ not listed on CDC ❑
27. Comments,
This section only applies to samples where pH can be I certify that I have completed sections 16-27 (dated initials).
checked at Sample Receipt. Yes No N/A Details Comments
28_
29,
CO
30,
CD
Note: Certain analyses require chemical reservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH.
N Y 9 P Y P P P
co I certify that I have completed sections 28-30 (dated initials).
O
W Checklist 6.9.17 Rev 2 Locked
O
EW 8/13/19
needing chemical preservation been checked? *
•s
meet preservation guidelines?
ffHavecontainers
djusted at Sample Receipt?
•
EW 8/13/19
Page 6 of 7

Analytical Environmental Services, Inc
Client: Prism Laboratories
Project Namc: 9080093
NVorkorder: 190801
Date: 19-Aug-19
ANALYTICAL QC SUMMARY REPORT
BatchlD: 283568
Sample ID: N[13-283568
Client ID:
Units: mg/L
Prep Date: 08/15/2019
Run No: 405118
SampleType: MBLK
TestCode: IIERBICIDES,TCLP SW1311/8151A
BatchlD: 283568
Analysis Date: 08/16/2019
SegNo: 9101944
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qua]
2.4,5-TP (Silvex) BRL 0.20
2.4-D BRL 0.20
Surr: DCAA 0.3375 0 0.5000 67.5 49.4 120
Sample ID: LCS-283568
Client ID:
Units: mg/L
Prep Date: 08/15/2019
Run No: 405118
SampleType: LCS
TestCode: HERBICIDES,TCLP SW1311/8151A
BatchlD:283568
Analysis Date: 08/16/2019
SegNo: 9101945
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2.4,5-TP (Silvex)
0.3451
0.20
0.5000
69.0
49
120
2.4-D
0.3658
0.20
0.5000
73.2
50.9
120
Surr: DCAA
0.3548
0
0.5000
71.0
49.4
120
Sample ID: 190801-003AMS
Client ID:
Sta-Lime
Units: mg/L
Prep Date: 08/15/2019
Run No: 405118
SampleType: NIS
TestCode:
HERBICIDES, TCLP SW1311/8151A
BatchID: 283568
Analysis Date: 08/16/2019
Seq No: 9101950
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex)
0.3637
0.20
0.5000
72.7
48.2
120
2,4-D
0.3913
0.20
0.5000
78.3
45
130
Surr: DCAA
0.3670
0
0.5000
73.4
49.4
120
n
(Q Quailrtcrs: > Gramcr than Result salue
CD
W BRL Bclmv reporling limn
O .I Esumated salue detected below Reporting Luau
O
�+ Rpl Lim Reporting Lnnn
W
O
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 7 of 7

NC Certification No.402 Case Narrative
P RIS M Full -Service Analytical & NC Drinking Water Cert No. 37735 12/5/19 11:46
Environmental Solutions SC Certification No. 99012
R
City of Statesville, NC
Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: StaLime
Lab Submittal Date: 11/25/2019
Prism Work Order: 9110421
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR =[Na]/SQRT {([Ca]+[Mg])/2}
SAR = [ 180/23 ] / SQRT { ( [2400/20] + [0.047/12.2]) / 2 }
SAR = 1.0
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) +
Nitrate —Nitrite
PAN = 0.3 * (4000 — 120) + 0.5 * (120) + 9.3
PAN = 1200 mg/kg
Equation uses Mineralization Rate (MR) for Aerobically Digested
Solids (0.3)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 1 of 17

Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
��vvu:
Terri W. Cole
Project Manager
Data Qualifiers Key Reference:
' ('0 66a,"
Reviewed By Terri W. Cole
Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
M Matrix spike outside of the control limits.
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 17

Full -Service Analytical &
PRISM
r Sao Environmental Solutions
awroaie�, ma
Sample Receipt Summary
12/05/2019
Prism Work Order: 9110421
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled Date/Time Received
StaLime (and Fecal 1)
9110421-01
Solid
11/25/19 11:45 11/25/19 12:40
2
9110421-02
Solid
11/25/19 11:45 11/25/19 12:40
3
9110421-03
Solid
11/25/19 11:45 11/25/19 12:40
4
9110421-04
Solid
11/25/19 11:45 11/25/19 12:40
5
9110421-05
Solid
11/25/19 11:45 11/25/19 12:40
6
9110421-06
Solid
11/25/19 11:45 11/25/19 12:40
7
9110421-07
Solid
11/25/19 11:45 11/25/19 12:40
Samples were received in good condition at 2.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 17

P R I S M Full -Service Analytical &
Laboratory Report
Environmental Solutions 12/05/2019
:� u�AroftiEaiHc
City of Statesville, NC Project: StaLime Client Sample ID: StaLime (and Fecal 1)
Attn: Ken Galloway Prism Sample ID: 9110421-01
P.O. Box 1111 Prism Work Order: 9110421
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Plant Available Nitrogen
1200
mg/kg dry
120
63
1
*Calculation
12/4/19 9:05
CLB
[CALC]
% Solids
66.3
% by
0.100
0.100
1
*SM2540 G
11/27/19 9:08
EDV
P9K0490
Weight
Ammonia as N
120
mg/kg dry
15
3.7
1
*SM4500-NH3 C
11/27/19 14:00
BMS
P9K0504
Nitrate/Nitrite as N
9.3
mg/kg dry
7.5
2.1
1
*SM4500-NO3 F
12/2/19 10:32
CLB
P91-0009
Phosphorus -Total
4300
mg/kg dry
150
46
20
*SM4500-P F
12/3/19 12:15
CLB
P91-0031
Total Kjeldahl Nitrogen
4000
mg/kg dry
380
200
1
*351.2
12/4/19 9:05
CLB
P91-0041
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
11/25/19 14:30
BMS
P91<0483
Total Metals
Mercury
0.095
mg/kg dry
0.075
0.026
1
*747113
11/27/19 10:34
MMR
P9K0493
SAR Soil Preparation
Complete
g
1
*2-78-054
11/27/19 13:30
EDV
P91<0491
SAR Percent Moisture
51.5
% by
0.100
0.100
1
*2-78-054
12/2/19 8:10
EDV
P9K0510
Weight
Arsenic
13
mg/kg dry
1.5
0.20
1
*6010D
12/2/19 20:13
JAB
P9K0494
Sodium Absorption Ratio
1.0
[blank]
0.30
0.016
1
*2-78-054
12/3/19 8:50
JAB
P9K0508
Cadmium
BRL
mg/kg dry
0.75
0.051
1
*6010D
12/2/19 20:13
JAB
P91<0494
Calcium, SAR
2400
mg/L
200
2.0
200
*6010D
12/3/19 8:50
JAB
P9K0508
Copper
54
mg/kg dry
3.8
0.51
1
*6010D
12/2/19 20:13
JAB
P9K0494
Lead
9.0
mg/kg dry
1.5
0.25
1
*6010D
12/2/19 20:13
JAB
P9K0494
Magnesium, SAR
BRL
mg/L
1.0
0.086
10
*6010D
12/3/19 8:50
JAB
P91<0508
Nickel
15
mg/kg dry
1.5
0.45
1
*6010D
12/2/19 20:13
JAB
P9K0494
Potassium
4600
mg/kg dry
150
16
1
*6010D
12/2/19 20:13
JAB
P9K0494
Selenium
27
mg/kg dry
1.5
0.41
1
*6010D
12/2/19 20:13
JAB
P9K0494
Sodium
1100
mg/kg dry
150
20
1
*6010D
12/2/19 20:13
JAB
P9K0494
Sodium, SAR
180 B
mg/L
5.0
0.18
10
*6010D
12/3/19 8:50
JAB
P9K0508
Zinc
100
mg/kg dry
15
2.1
1
*6010D
12/2/19 20:13
JAB
P9K0494
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 4 of 17

Laboratory Report
Full -Service Analytical &
P R I S M Environmental Solutions
-0-ORIES ING
12/05/2019
City of Statesville, NC
Project: StaLime
Client Sample ID: 2
Attn: Ken Galloway
Prism Sample ID: 9110421-02
P.O. Box 1111
Prism Work Order: 9110421
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
% Solids 65.3
% by
0.100
0.100 1 "SM2540 G 11/27/19 9:08 EDV P9K0490
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 `SM9221 E 11/25/19 14:30 BMS P91<0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 17

Laboratory Report
Full -Service Analytical &
P R I S M Environmental Solutions
-0-ORIES ING
12/05/2019
City of Statesville, NC
Project: StaLime
Client Sample ID: 3
Attn: Ken Galloway
Prism Sample ID: 9110421-03
P.O. Box 1111
Prism Work Order: 9110421
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
% Solids 63.9
% by
0.100
0.100 1 "SM2540 G 11/27/19 9:08 EDV P9K0490
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 `SM9221 E 11/25/19 14:30 BMS P91<0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 17

Laboratory Report
Full -Service Analytical &
P R I S M Environmental Solutions
-0-ORIES ING
12/05/2019
City of Statesville, NC
Project: StaLime
Client Sample ID: 4
Attn: Ken Galloway
Prism Sample ID: 9110421-04
P.O. Box 1111
Prism Work Order: 9110421
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
% Solids 65.1
% by
0.100
0.100 1 "SM2540 G 11/27/19 9:08 EDV P9K0490
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 `SM9221 E 11/25/19 14:30 BMS P91<0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 17

Laboratory Report
Full -Service Analytical &
P R I S M Environmental Solutions
-0-ORIES ING
12/05/2019
City of Statesville, NC
Project: StaLime
Client Sample ID: 5
Attn: Ken Galloway
Prism Sample ID: 9110421-05
P.O. Box 1111
Prism Work Order: 9110421
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
% Solids 66.4
% by
0.100
0.100 1 "SM2540 G 11/27/19 9:08 EDV P9K0490
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 `SM9221 E 11/25/19 14:30 BMS P91<0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 17

Laboratory Report
Full -Service Analytical &
P R I S M Environmental Solutions
-0-ORIES ING
12/05/2019
City of Statesville, NC
Project: StaLime
Client Sample ID: 6
Attn: Ken Galloway
Prism Sample ID: 9110421-06
P.O. Box 1111
Prism Work Order: 9110421
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
% Solids 64.0
% by
0.100
0.100 1 "SM2540 G 11/27/19 9:08 EDV P9K0490
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 `SM9221 E 11/25/19 14:30 BMS P91<0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 17

Laboratory Report
Full -Service Analytical &
P R I S M Environmental Solutions
-0-ORIES ING
12/05/2019
City of Statesville, NC
Project: StaLime
Client Sample ID: 7
Attn: Ken Galloway
Prism Sample ID: 9110421-07
P.O. Box 1111
Prism Work Order: 9110421
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
% Solids 67.2
% by
0.100
0.100 1 "SM2540 G 11/27/19 9:08 EDV P9K0490
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 `SM9221 E 11/25/19 14:30 BMS P91<0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 17

P R I S M Full -Service Analytical
Environmental Solutions
Level II QC Report
12/5/19
City of Statesville, NC Project: StaLime Prism Work Order: 9110421
Attn: Ken Galloway Time Submitted: 11/25/2019 12:40:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9K0491 - SAR 2-78-054
Blank (P9KO491-BLK1)
Prepared: 11/26/19 Analyzed: 11/27/19
SAR Soil Preparation
Complete g
Batch P9KO493 - 7471 B
Blank (P9KO493-BLK1)
Prepared &Analyzed: 11/27/19
Mercury
BRL 0.050 mg/kg wet
LCS (P9KO493-BS1)
Prepared &Analyzed: 11/27/19
Mercury
0.421 0.050 mg/kg wet 0.4167 101 80-120
Batch P9KO494 - 3050B
Blank (P9KO494-BLK1)
Prepared: 11/27/19 Analyzed:
12/02/19
Arsenic
BRL
1.0
mg/kg wet
Cadmium
BRL
0.50
mg/kg wet
Copper
BRL
2.5
mg/kg wet
Lead
BRL
1.0
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
100
mg/kg wet
Selenium
BRL
1.0
mg/kg wet
Sodium
BRL
100
mg/kg wet
Zinc
BRL
10
mg/kg wet
LCS (P9KO494-BS1)
Prepared: 11/27/19 Analyzed:
12/02/19
Arsenic
12.8
1.0
mg/kg wet
12.50 103
80-120
Cadmium
12.8
0.50
mg/kg wet
12.50 103
80-120
Copper
13.8
2.5
mg/kg wet
12.50 110
80-120
Lead
13.0
1.0
mg/kg wet
12.50 104
80-120
Nickel
13.1
1.0
mg/kg wet
12.50 105
80-120
Potassium
1200
100
mg/kg wet
1250 96
80-120
Selenium
12.2
1.0
mg/kg wet
12.50 98
80-120
Sodium
1210
100
mg/kg wet
1250 97
80-120
Zinc
12.7
10
mg/kg wet
12.50 102
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 17

PRI S M Fullironm n AnalyticalsEnvironmental Solutions�-W
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime
Level II QC Report
12/5/19
Prism Work Order: 9110421
Time Submitted: 11/25/2019 12:40:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9K0508 - 301 OA
Blank (P9KO508-BLK1) Prepared: 11/27/19 Analyzed: 12/03/19
Calcium, SAR BRL 1.0 mg/L
Magnesium, SAR BRL 0.10 mg/L
Sodium, SAR 1.73 0.50 mg/L BH
Batch P9KO510 - NO PREP
Duplicate (P9K0510-DUP1) Source: 9110421-01 Prepared: 11/27/19 Analyzed: 12/02/19
SAR Percent Moisture 51.0 0.100 % by Weight 51.5 1 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 17

Full-S
PRISM Environmental
elutial s
Environmental Solutions
LA6DAATOAIEy ING
Level II QC Report
12/5/19
City of Statesville, NC Project: StaLime Prism Work Order: 9110421
Attn: Ken Galloway Time Submitted: 11/25/2019 12:40:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9K0490 - NO PREP
Duplicate (P9KO490-DUP2)
Source: 9110421-01
Prepared: 11/26/19 Analyzed: 11/27/19
% Solids
Batch P9KO504 - SM4500-NH3 B
66.5 0.100 % by Weight 66.3
0.2 20
Blank (P9KO504-BLK1)
Prepared &Analyzed: 11/27/19
Ammonia as N
LCS (P9KO504-BS1)
BRL 10 mg/kg wet
Prepared &Analyzed: 11/27/19
Ammonia as N
Matrix Spike (P9KO504-MS1)
454 10 mg/kg wet
Source: 9110421-01
500.0 91
Prepared &Analyzed: 11/27/19
80-120
Ammonia as N
Matrix Spike Dup (P9KO504-MSD1)
791 14 mg/kg dry
Source: 9110421-01
724.7 121 92
Prepared &Analyzed: 11/27/19
80-120
Ammonia as N
Batch P91L0009 - NO PREP
816 14 mg/kg dry
724.7 121 96
80-120 3 200
Blank (P9L0009-BLK1)
Prepared &Analyzed: 12/02/19
Nitrate/Nitrite as N
LCS (P9L0009-BS1)
BRL 5.0 mg/kg wet
Prepared &Analyzed: 12/02/19
Nitrate/Nitrite as N
Matrix Spike (P9L0009-MS1)
47.7 5.0 mg/kg wet
Source: 9110421-01
50.00 95
Prepared &Analyzed: 12/02/19
80-120
Nitrate/Nitrite as N
89.8 7.5 mg/kg dry
75.37 9.35 107
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 17

Full-S
PRISM Environmental
elutial s
Environmental Solutions
LA6DAATOAIEy ING
Level II QC Report
12/5/19
City of Statesville, NC Project: StaLime Prism Work Order: 9110421
Attn: Ken Galloway Time Submitted: 11/25/2019 12:40:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9L0009 - NO PREP
Matrix Spike Dup (P9L0009-MSD1)
Source: 9110421-01
Prepared &Analyzed: 12/02/19
Nitrate/Nitrite as N
Batch P9L0031 - SM4500-PB5
89.2 7.5 mg/kg dry
75.37 9.35 106 80-120 0.8 20
Blank (P9L0031-BLK1)
Prepared &Analyzed: 12/03/19
Phosphorus -Total
LCS (P9L0031-BS1)
BRL 5.0 mg/kg wet
Prepared &Analyzed: 12/03/19
Phosphorus -Total
Matrix Spike (P9L0031-MS1)
97.6 5.0 mg/kg wet
Source: 9110421-01
100.0 98 90-110
Prepared &Analyzed: 12/03/19
Phosphorus -Total
Matrix Spike Dup (P9L0031-MSD1)
4790 150 mg/kg dry
Source: 9110421-01
150.7 4250 353 80-120 MC
Prepared &Analyzed: 12/03/19
Phosphorus -Total
Batch P9L0041 - 351.2
4920 150 mg/kg dry
150.7 4250 445 80-120 3 20 MC
Blank (P90041-BLK1)
Prepared: 12/03/19 Analyzed: 12/04/19
Total Kjeldahl Nitrogen
LCS (P9L0041-BS1)
BRL 25 mg/kg wet
Prepared: 12/03/19 Analyzed: 12/04/19
Total Kjeldahl Nitrogen
Matrix Spike (P9L0041-MS1)
123 25 mg/kg wet
Source: 9110421-01
125.0 99 90-110
Prepared: 12/03/19 Analyzed: 12/04/19
Total Kjeldahl Nitrogen
6750 750 mg/kg dry
1884 3960 148 90-110 M
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 17

PRI S M Fullironm n AnalyticalsEnvironmental Solutions�-W
City of Statesville, NC Project: StaLime
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
12/5/19
Prism Work Order: 9110421
Time Submitted: 11/25/2019 12:40:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9L0041 - 351.2
Matrix Spike Dup (P9L0041-MSD1) Source: 9110421-01 Prepared: 12/03/19 Analyzed: 12/04/19
Total Kjeldahl Nitrogen 6490 750 mg/kg dry 1884 3960 134 90-110 4 20 M
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 15 of 17

Full-S
PRISM Environmental
elutial s
Environmental Solutions
LA6DAATOAIEy ING
City of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Batch PgK0483 - NO PREP
Project: StaLime
Level II QC Report
12/5/19
Prism Work Order: 9110421
Time Submitted: 11/25/2019 12:40:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P9KO483-BLK1)
Prepared &Analyzed: 11/25/19
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction
Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
9110421-01
P91_0041
0.05 g
25 mL
12/03/19 10:15
Prep Method: SM4500-NH3 B
Lab Number
Batch
Initial
Final
Date/Time
9110421-01
P91<0504
1.01 g
50 mL
11/27/19 8:55
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Date/Time
9110421-01
P91_0031
1 g
50 mL
12/03/19 6:15
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
9110421-01
P9K0508
50
mL
50 mL
11/27/19 13:30
9110421-01
P9K0508
50
mL
50 mL
11/27/19 13:30
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
9110421-01
P91<0494
2
g
50 mL
11/27/19 8:05
Prep Method: 7471 B
Lab Number
Batch
Initial
Final
Date/Time
9110421-01
PgK0493
0.6
g
50 mL
11/27/19 8:14
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
9110421-01 P9K0491 250 g 250 g 11/26/19 13:30
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