HomeMy WebLinkAboutNCS000599_Application (NC0089982)_20200504April 24, 2020
North Carolina Department of Environmental Quality
1612 MSC
Raleigh, NC 27699-1612
Attn: Ms. Suzanne McCoy
E: Suzanne. mccoy(cDncdenr.gov
Re: Industrial Wastewater Discharge Permit Application
Wilbara Sulfuric Acid Plant
4620 Highway 421 North
Wilmington, NC 28401
Dear Ms. McCoy:
Irerracon
RECEIVED
MAY 0 4 2020
DENR-LAND QUALITY
STORMWATER PERMITTING
On behalf of Wilbara, LLC/Southern States Chemical, Terracon Consultants, Inc. (Terracon) has
completed the enclosed Industrial NPDES Permit Application and supporting documentation for
the above -referenced facility. Preparation of this NPDES Individual permit application is
associated with the proposed addition of wash waters from facility tank cleaning and
maintenance activities to the facility's present discharge of non -contact cooling water, boiler
blowdown, and cooling tower blowdown through Outfall 001. The individual permit would
replace the facility's present NPDES General Permit NCG500000.
Should you have any questions please contact us at your earliest convenience at (704) 594 -
8912 or via email at neal.mcelveenCc)-terracon.com .
Sincerely,
Terracon Consultants, Inc.
McKhenzy A. Welch, CPESC
Staff Scientist
Attachments:
Exhibits: Exhibit 1: Topographic Map
Exhibit 2: Site Diagram
Appendix A: EPA Form 3510-1: General Information
EPA Form 3510-2C: Existing Manufacturing,
Operations
Appendix B: EAA
Appendix C: Laboratory Analytical Reports
M. Neal McElveen, PE
Principal/Environmental Manager
Commercial, Mining, and Silviculture
Terracon Consultants, Inc. 2701 Westport Road Charlotte, North Carolina 28208
P [704] 509 1777 F [704] 509 1888 terracon.com
EXHIBITS
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34 19' 16.476" N
77°.58' 27.800" W
,,EApproximate Site Boundary
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`• -. — / '—'-STATE GAML LAND
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law
v ` Vic• +�,$r1� ' -'-- ti C. Cape Fear River Basin
Ll
Feet ® Approximate Site Boundary Source: 2011 National Geographic Society/ESRI, i-cubed
seamless USGS quadrangles (Castle Hayne, NC); Site
0 1,000,000 4,000 Approximate Outfall Location Boundary approximated by Terracon.
PM: Project No. Topographic Vicinity Map EXHIBIT
NM 71197840 NO.
Drawn By: Scale:
KT 1:51,363 Irerracon Wilmington Plant NPDES Permitting
Checked By: Filename: 4620 Highway 421 North
MW Topo Wilmington, New Hanover County,
Approved By: Date: 2701 weslportRd ChaOotte, NC 2820 North Carolina
NM February 2020 Phone: (704) 509-1777 Fax: (704) 509-1777
Feet
1140- Tidal Flow
Source: 2011 National Geographic Society/ESRI, i-cubed
0 750
1,500
3,000
® Approximate Outfall 001 Location
seamless USGS quadrangles (Castle Hayne, NC); Site
Boundary approximated byTerracon.
PM:
Project No.
Site Diagram
EXHIBIT
NM
71197840
No.
Drawn By:
Scale:
KT
1:18,000
Irerracon
Checked By:
Filename:
Wilmington Plant NPDES Permitting
24620
MW
Site_Diagram
Highway
g y 421 North
Approved By:
Date:
2701 wealportRd Chadone,NC2820
Wilmington, North Carolina
NM
February 2020
Phona: (704) 509-1777 Fax: (704) 509-1777
m uu =1 ilk
EPA Identification Number
NPDES Permit Number
Facility Name
Form Approved 03/05/19
Form
U.S. Environmental Protection Agency
1
OA
Application for NPDES Permit to Discharge Wastewater
NPDES
GENERAL INFORMATION
SECTION
1. ACTIVITIES REQUIRING
AN NPDES PERMIT (40 CFR 122.21(f) and (0(1))
1.1 Applicants Not
Required to Submit Form 1
1.1.1
Is the facility a new or existing publicly owned
1.1.2
Is the facility a new or existing treatment works
treatment works?
treating domestic sewage?
If yes, STOP. Do NOT complete No
If yes, STOP. Do NOT No
Form 1. Complete Form 2A.
complete Form 1. Complete
Form 2S.
1.2
Applicants Required to Submit Form I
1.2.1
Is the facility a concentrated animal feeding
1.2.2
Is the facility an existing manufacturing,
E
operation or a concentrated aquatic animal
commercial, mining, or silvicultural facility that is
IL
production facility?
currently discharging process wastewater?
LU
F� Yes 4 Complete Form 1 No
F.,7] Yes 4 Complete Form F� No
r-
1.2.3
Is the facility a new manufacturing, commercial,
1.2.4
Is the facility a new or existing manufacturing,
mining, or silvicultural facility that has not yet
commercial, mining, or silvicultural facility that
commenced to discharge?
discharges only nonprocess wastewater?
Cr
Yes 4 Complete Form 1 F.71 No
E] Yes 4 Complete Form No
CD
1.2.5
Is the facility a new or existing facility whose
discharge is composed entirely of stormwater
associated with industrial activity or whose
discharge is composed of both stormwater and
Yes 4 Complete Form 1 No
and Form 2F
unless exempted by
SECTION
i NAME,
MAILING ADDRESS, AND LOCATION (40 CFR 122.21(0(2))
2.1
Facility Name
Wilbara Sulfuric Acid Plant
.2
2.2
EPA Identification Number
2.3
Facility Contact
--FTitle
U)
Name (first and last)
Phone number
Bradley Smock
Process Engineer
(910) 274-0047
Email address
6
2.4
Facility Mailing Address
W
Street or P.O. box
4620 Highway 421 North
City or town
State
ZIP code
Wilmington
North Carolina
28401
EPA Form 3510-1 (revised 3-19)
EPA Identification Number
NPDES Permit Number
Facility Name
Form Approved 03/05/19
NCR000151795
SW8 090331
Wilbara Sulfuric Acid Plant
OMB No. 2040-0004
"
2.5
Facility Location
a
Street, route number, or other specific identifier
Q 0
4620 Highway421 North
0
as
c
County name
County code (if known)
New Hanover
0
E _j
City or town
State ZIP code
z R
Wilmington
North Carolina 28401
SECTION1
NAICS CODES1
3.1
SIC Code(s)
Description (optional)
2819
Vf
d
.a
O
C.)
N
U
Z
3.2
NAICS Code(s)
Description (optional)
v
325180
tis
4.1
7NFF77prator
Southern States Chemical
0
4.2
Is the name you listed in Item 4.1 also the owner?
cc
R
c
0 Yes ❑ No
4.3
Operator Status
0
L
❑ Public —federal ❑ Public —state ❑ Other public (specify)
0
0 Private ❑ Other (specify)
1
4.4
Phone Number of Operator
4.5
Operator Address
O
Street or P.O. Box
cc
E
4620 Highway 421 North
_
City or town
State
ZIP code
0 0
2
Wilmington
North Carolina
28401
n
Email address of operator
0
SECTIO,
N 5. INDI1
5.1
Is the facility located on Indian Land?
j
❑ Yes No
EPA Form 3510-1 (revised 3-19) Page 2
r_.
EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCR000151795 SW8 090331 1 Wilbara Sulfuric Acid Plant OMB No.2040-0004
6.1 Existing Environmental Permits (check all that apply and print or type the corresponding permit number for each)
d �✓ NPDES (discharges to surface ❑ RCRA (hazardous wastes) ❑ UIC (underground injection of
c H water) fluids)
L y.1
U a ❑" PSD (air emissions) ❑ Nonattainment program (CAA) ❑ NESHAPs (CAA)
c 09904T02 Title V
'x I ElOcean dumping (MPRSA) ElDredge or fill (CWA Section 404) ❑ Other (specify)
w
7.1 Have you attached a topographic map containing all required information to this application? (See instructions for
specific requirements.)
Yes ❑ No ❑ CAFO—Not Applicable (See requirements in Form 26.)
8.1 Describe the nature of your business.
Industrial manufacturer of commercial -grade sulfuric acid.
a>
c
.y
m
�0
O
d
O
R
Z
9.1 Does your facility use cooling water?
ID Yes ❑ No + SKIP to Item 10.1.
9.2 Identify the source of cooling water. (Note that facilities that use a cooling water intake structure as described at
a, R 40 CFR 125, Subparts I and J may have additional application requirements at 40 CFR 122.21(r). Consult with your
cNPDES permitting authority to determine what specific information needs to be submitted and when.)
v Mc
Water Supply Well
10.1 Do you intend to request or renew one or more of the variances authorized at 40 CFR 122.21(m)? (Check all that
y apply. Consult with your NPDES permitting authority to determine what information needs to be submitted and
when.)
d ❑ Fundamentally different factors (CWA ❑ Water quality related effluent limitations (CWA Section
d Section 301(n)) 302(b)(2))
R ❑ Non -conventional pollutants (CWA Thermal discharges (CWA Section 316(a))
Section 301(c) and (g))
Not applicable
._ EPA Form 3510-1 (revised 3-19) Page 3
EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCR000151795 SW8 090331 Wilbara Sulfuric Acid Plant OMB No. 2040-0004
SECTION 11. CHECKLIST AND CERTIFICATION STATEMENT (40 CFR 122.22(a) and (d))
11.1 In Column 1 below, mark the sections of Form 1 that you have completed and are submitting with your application.
For each section, specify in Column 2 any attachments that you are enclosing to alert the permitting authority. Note
that not all applicants are required to provide attachments.
Column I
Column 2
El Section 1: Activities Requiring an NPDES Permit
F� w/ attachments
Z Section 2: Name, Mailing Address, and Location
F1 w/ attachments
F,71 Section 3: SIC Codes
EI w/ attachments
2 Section 4: Operator Information
El w/ attachments
D Section 5: Indian Land
El w/ attachments
n-1 Section 6: Existing Environmental Permits
Z w/ attachments
E
Section 7: Map
w/ topographic
w/ additional attachments
map
Section 8: Nature of Business
w/ attachments
cc
ft
P1 Section 9: Cooling Water Intake Structures
w/ attachments
El Section 10: Variance Requests
F� w/ attachments
Section 11: Checklist and Certification Statement
w/ attachments
11.2
Certification Statement
certify under penalty of law that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and complete. / am aware that there are significant penalties for submitting false information,
including the possibility of fine and imprisonment for knowing violations.
Name (print or type first and last name)
Official title
Operations Manager
Steven Suek
Signature
Date signed
04/01/2020
Click to go back to the beginning of Form
EPA Form 3510-1 (revised 3-19) Page 4
EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCR0001 51795 SW8 090331 Wilbara Sulfuric Acid Plant OMB No. 2040-0004
Form U.S. Environmental Protection Agency
2C Mor Application for NPDES Permit to Discharge Wastewater
NPDES EXISTING MANUFACTURING, COMMERCIAL, MINING, AND SILVICULTURE OPERATIONS
SECTION 1. OUTFALL LOCATION (40 CIFIR 122.21(g)(1))
1.1 Provide information on each of the facility's outfalls in the table below.
Ouffall
Number Receiving Water Name Latitude Longitude
0
Unnamed Cove on Invista 34' 18' 55.77" IN -77* 58' 26.76" W
Prop. to the Cape Fear Rivei
0
SECTION 2. LINE DRAWING (40 CIFIR 122.21(g)(2))
CD 2.1 Have you attached a line drawing to this application that shows the water flow through your facility with a water
balance? (See instructions for drawing requirements. See Exhibit 2C-1 at end of instructions for example.)
0 21 Yes F� No
SECTION 3. AVERAGE FLOWS AND TREATMENT (40 CFR 122,21(g)(3))
3.1 For each outfall identified under Item 1.1, provide average flow and treatment information. Add additional sheets if
necessary.
**Ouffall Number** I
Operations Contributing to Flow
Operation Average Flow
tank/equipment cleaning, maintenance /operational 0.00001425 mgd
E Cooling Tower, Boiler /Cooling Tower Blow Down 0.018225 mgd
M
existing permit mgd
mgd
.2
U- Treatment Units
0 Description Final Disposal of Solid or
Code from
(include size, flow rate through each treatment unit, Liquid Wastes Other Than
Table 2C-1
retention time, etc.) by Discharge
0.01824 mgd 2-K Other - Not Applicable
EPA Form 3510-2C (Revised 3-19) Page 1
EPA Identification Number
NPIDES Permit Number
Facility Name
Form Approved 03/05/19
NCR000151795
SW8 090331
Wilbara Sulfuric Acid Plant
OMB No. 2040-0004
3.1
"Outfall Number"
cont.
Operations Contributing to Flow
Operation Average Flow
mgd
mgd
mgd
mgd
Treatment
Description
Units
Code from Final Disposal of Solid or
(include size, flow rate through each treatment unit,
Table 2C-1 Liquid Wastes Other Than
retention time, etc.)
by Discharge
0
4)
E
"Outfall Number"
U)
Operations Contributing to Flow
0
Operation Average Flow
U.
0
mgd
mgd
mgd
mgd
'Treatment
Units
Description Code from Final Disposal of Solid or
(include size, flow rate through each treatment unit, Table 2C-1 Liquid Wastes Other Than
retention time, etc.) by ischarge
3.2
Are you applying for an NPDES permit to operate a privately owned treatment works?
E
El Yes [21 No 4 SKIP to Section 4.
n
3.3
Have you attached a list that identifies each user of the treatment works?
El Yes El No
EPA Form 3510-2C (Revised 3-19) Page 2
EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCR000151795� SW8 090331 Wilbara Sulfuric Acid Plant OMB No. 2040-0004
SECTION 4. INTERMITTENT FLOWS (40 CFR 122.21( )(4))
9
4.1 Except for storm runoff, leaks, or spills, are any discharges described in Sections 1 and 3 intermittent or seasonal?
El Yes 2] No 4 SKIP to Section 5.
4.2
Provide information
on intermittent or seasonal.flows for each applicable outfall.
Attach additional pages, if n cessary.
Outfall
Operation
Frequency
Flow
Rate
Average
Average
Long -Term
Maximum
Number
(list)
Duration
Days/Week
Months/Year
Average
Daily
days/week
monthslyear
mgd
mgd
days
days/week
months/year
mgd
mgd
days
LL
4)
days/week
months/year
mgd
mgd
days
3�
E
days/week
monthslyear
mgd
mgd
days
days/week
months/year
mgd
mgd
days
days/week
months/year
mgd
mgd
days
days/week
months/year
mgd
mgd
days
days/week
I months/year
I mgd I
mgd
I days
days/week months/year mgd mgd days
SECTION
5. PRODUCTION
(40 CFR 122.21(g)(5))
5.1
Do any effluent limitation guidelines (ELGs) promulgated by EPA under Section 304 of the CWA apply to your facility?
r-1 Yes E] No 4 SKIP to Section 6.
5.2
Provide the following information on applicable EI-Gs.
ELG Category
ELG Subcategory
Regulatory Citation
CL
CL
5.3
Are any of the applicable EI-Gs expressed in terms of production (or other measure of operation)?
Yes No 4 SKIP to Section 6.
C
.2
5.4
Provide an actual measure of daily production expressed in terms and units of applicable EI-Gs.
E
Outfall
Operation, Product, or Material
Quantity per Day
Unit of
Number
Measure
C9
IL
EPA Form 3510-2C (Revised 3-19) Page 3
EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCR000151795 SW8 090331 Wilbara Sulfuric Acid Plant OMB No.2040-0004
SECTION• •. , ,
6.1 Are you presently required by any federal, state, or local authority to meet an implementation schedule for constructing,
upgrading, or operating wastewater treatment equipment or practices or any other environmental programs that could
affect the discharges described in this application?
❑ Yes ❑ No 4 SKIP to Item 6.3.
N
6.2
Briefly identify each applicable project in the table below.
Affected
Final Compliance Dates
E
Brief Identification and Description of
Outfalls
Source(s) of
c
Project
(list outfall
Discharge
Required
Projected
CL
number
E
f/!
d
R
tM
O.
-T
6.3
Have you attached sheets describing any additional water pollution control programs (or other environmental projects
that may affect your discharges) that you now have underway or planned? (optional item)
❑ Yes ❑ No Not applicable
,SECTIONA•A
i
See the instructions to determine the pollutants and parameters you are required to monitor and, in turn, the tables you must
complete. Not all applicants need to complete each table.
Table A. Conventional and Non -Conventional Pollutants
7.1
Are you requesting a waiver from your NPDES permitting authority for one or more of the Table A pollutants for any of
your outfalls?
❑ Yes [21 No 4 SKIP to Item 7.3.
7.2
If yes, indicate the applicable outfalls below. Attach waiver request and other required information to the application.
Outfall Number Outfall Number Outfall Number
7.3
Have you completed monitoring for all Table A pollutants at each of your outfalls for which a waiver has not been
requested and attached the results to this application package?
El Yes ❑ No; a waiver has been requested from my NPDES
Rpermitting
authority for all pollutants at all outfalls.
Table B.
Toxic Metals, Cyanide, Total Phenols, and Organic Toxic Pollutants
7.4
Do any of the facility's processes that contribute wastewater fall into one or more of the primary industry categories
c
listed in Exhibit 2C-3? (See end of instructions for exhibit.)
R
❑ Yes ❑ No 4 SKIP to Item 7.8.
7.5
Have you checked "Testing Required" for all toxic metals, cyanide, and total phenols in Section 1 of Table B?
w
0 Yes ❑ No
7.6
List the applicable primary industry categories and check the boxes indicating the required GUMS fraction(s) identified
in Exhibit 2C-3.
Primary Industry Category
Required GCIMS Fraction(s)
Check applicable boxes.
Inorganic Chemical Manufacturing
EI Volatile [D Acid El Base/Neutral ❑ Pesticide
❑ Volatile ❑ Acid ❑ Base/Neutral ❑ Pesticide
❑ Volatile ❑ Acid ❑ Base/Neutral ❑ Pesticide
EPA Form 3510-2C (Revised 3-19) Page 4
EPA Identification Number
NPDES Permit Number
Facility Name
Form Approved 03/05/19
N CR000151795
SW8 090331
Wilbara Sulfuric Acid Plant
OMB No.2040-0004
7.7
Have you checked "Testing Required" for all required pollutants in Sections 2 through 5 of Table B for each of the
GC/MS fractions checked in Item 7.6?
S Yes ❑ No
7.8
Have you checked "Believed Present" or "Believed Absent" for all pollutants listed in Sections 1 through 5 of Table B
where testing is not required?
El Yes ❑ No
7.9
Have you provided (1) quantitative data for those Section 1, Table B, pollutants for which you have indicated testing is
required or (2) quantitative data or other required information for those Section 1, Table B, pollutants that you have
indicated are `Believed Present" in your discharge?
✓❑ Yes ❑ No
7.10
Does the applicant qualify for a small business exemption under the criteria specified in the instructions?
❑ Yes 4 Note that you qualify at the top of Table B, ❑ No
then SKIP to Item 7.12.
_
7.11
Have you provided (1) quantitative data for those Sections 2 through 5, Table B, pollutants for which you have
0
determined testing is required or (2) quantitative data or an explanation for those Sections 2 through 5, Table B,
pollutants you have indicated are "Believed Present" in your discharge?
H
0 Yes ❑ No
a;
Table C. Certain Conventional and Non -Conventional Pollutants
7.12
Have you indicated whether pollutants are "Believed Present" or "Believed Absent" for all pollutants listed on Table C
for all outfalls?
;�
Qr Yes ❑ No
cc
7.13
Have you completed Table C by providing (1) quantitative data for those pollutants that are limited either directly or
indirectly in an ELG and/or (2) quantitative data or an explanation for those pollutants for which you have indicated
"Believed Present"?
❑ Yes ❑ No
w
Table D.
Certain Hazardous Substances and Asbestos
7.14
Have you indicated whether pollutants are 'Believed Present" or "Believed Absent" for all pollutants listed in Table D for
all outfalls?
✓❑ Yes ❑ No
7.15
Have you completed Table D by (1) describing the reasons the applicable pollutants are expected to be discharged
and (2) by providing quantitative data, if available?
21 Yes ❑ No
Table E. 2,3,7,8-Tetrachlorodibenzo- -Dioxin 2,3,7,8-TCDD
7.16
Does the facility use or manufacture one or more of the 2,3,7,8-TCDD congeners listed in the instructions, or do you
know or have reason to believe that TCDD is or may be present in the effluent?
❑ Yes 4 Complete Table E. R No 4 SKIP to Section 8.
7.17
Have you completed Table E by reporting qualitative data for TCDD?
❑ Yes ❑ No
SECTIONOR
MANUFACTURED TOXICSi
8.1
Is any pollutant listed in Table B a substance or a component of a substance used or manufactured at your facility as
an intermediate or final product or byproduct?
w
❑ Yes 0 No -+ SKIP to Section 9.
H
8.2
List the pollutants below.
c �
1. 4. 7.
0
2. 5. 8.
N
3. 6. 9.
EPA Form 3510-2C (Revised 3-19) Page 5
EPA Identification Number
NPDES Permit Number
Facility Name Form Approved 03/05/19
�NCR000151795�
SW8 090331
Wilbara Sulfuric Acid Plant OMB No.2040-0004
SECTION9:..
,
9.1
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made
within the last three years on (1) any of your discharges or (2) on a receiving water in relation to your discharge?
y
❑ Yes ❑✓ No 4 SKIP to Section 10.
w
N
14)
9.2
Identify the tests and their
3urposes below.
Test(s)
Purpose of Test(s)
Submitted to NPDES
Date Submitted
x
Permittin Authority?
0
v
❑ Yes ❑ No
0
m
❑ Yes ❑ No
❑ Yes ❑ No
SECTION•
•. ,
10.1
Were any of the analyses reported in Section 7 performed by a contract laboratory or consulting firm?
❑ Yes ❑ No 4 SKIP to Section 11.
10.2
Provide information for each contract laboratory or consulting firm below.
Laboratory Number 1
Laboratory Number 2
Laboratory Number 3
Name of laboratory/firm
Element One
Environmental Chemists, Inc.
y
d
Laboratory address
6319-D Carolina Beach Road
6602 Windmill Way
R
=
Q
Wilmington, NC 28412
Wilmington, INC 28405
R
.r
c
Phone number
(910)793-0128
(910)392-0223
Pollutant(s) analyzed Metals, TSS, cyanide, TOC, organics and phenolics
COD, BOD, Ammonia
11.1
Has the NPDES permitting authority requested additional information?
c
❑ Yes 0 No 4 SKIP to Section 12.
11.2
List the information requested and attach it to this application.
E
w
_=
1. 4.
R
c
0
2. 5.
Q
3. 6.
EPA Form 3510-2C (Revised 3-19) Page 6
EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCR000151795 Wilbara Sulfuric Acid Plant OMB No. 2040-0004
SECTIONCERTIFICATION
12.1
In Column 1 below, mark the sections of Form 2C that you have completed and are submitting with your application.
For each section, specify in Column 2 any attachments that you are enclosing to alert the permitting authority. Note
that not all applicants are required to com lete all sections or provide attachments.
Column 1
Column 2
in/ Section 1: Outfall Location
✓❑ w/ attachments
R✓ Section 2: Line Drawing
✓❑ w/ line drawing ❑ w/ additional attachments
Section 3: Average Flows and
w/ list of each user of
w/ attachments ❑ privately owned treatment
Treatment
works
❑ Section 4: Intermittent Flows
❑ w/ attachments
❑ Section 5: Production
❑ w/ attachments
w/ optional additional
❑ Section 6: Improvements
❑ w/ attachments ❑ sheets describing any
additional pollution control
tans
❑ wl request for a waiver and El w/ explanation for identical
supporting information outfalls
w/ small business exemption
El❑ w/ other attachments
request
N
❑ Section 7: Effluent and Intake
❑ w/ Table A ❑ w/ Table B
Characteristics
❑ w/ Table C ❑ w/ Table D
d
wl Table E w/ analytical results as an
❑ ❑
attachment
RSection
8: Used or Manufactured
❑
❑ w/ attachments
w
N
Toxics
Y
Section 9: Biological Toxicity
❑
❑ w/ attachments
s
Tests
U
✓❑ Section 10: Contract Analyses
❑ w/ attachments
❑ Section 11: Additional Information
❑ w/ attachments
El Section 12: Checklist and
❑ wl attachments
Certification Statement
12.2
Certification Statement
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly
responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fine and imprisonment for knowing violations.
Name (print or type first and last name)
Official title
Steven Suek
Operations Manager
Signature
Date signed
04/01/2020
EPA Form 3510-2C (Revised 3-19) Page 7
This page intentionally left blank.
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Memorandum
TO: TERRACON PROJECT FILE 71197840 AND ATTACHMENT FOR
NPDES PERMIT APPLICATION
FROM: Neal McElveen; McKhenzy Welch
DATE: March 31, 2020
RE: Engineering Alternatives Analysis — Wilbara LLC NPDES Permit, 4620 Hwy 421 N,
Wilmington, North Carolina
Terracon was retained by Wilbara, LLC, who is owned by Southern States Chemical, to prepare
an Engineering Alternatives Analysis (EAA) for the Wilbara, LLC site located at 4620 Hwy 421 N
in Wilmington, North Carolina. The Wilbara facility consists of approximately 15 acres within the
Invista property bordered to the west by the Invista facility, to the north south and east by
undeveloped land with the Northeast Cape Fear River beyond and to the northeast. Exhibit 1
and 2 show the Wilbara facility and plant layout.
Preparation of this EAA has been complete in conjunction with a NPDES
application for the addition of proposed wash waters from facility tank cleaning and
maintenance activities. The facility presently operates under NPDES General Permit
NCG500000 for discharge of non -contact cooling water, boiler blowdown, and cooling tower
blowdown through Outfall 001. The proposed addition of the process waters (tank and
equipment cleaning, maintenance activities, and operational activities) requires the facility
obtain an individual NPDES Permit. This EAA is for a non —municipal application, process tank
wash downs, non -contact cooling water, boiler and cooling tower blowdown; therefore, the flow
projections are based on engineering design considerations rather than population projections.
A description of the proposed project follows. Projections for flow, evaluation of technical and
financial feasibility, and Local Government Review are provided in later sections.
STEP 1. Background and Project Description
Terracon has reviewed the potential restrictions identified in the EAA guidance document and
do not believe that the identified restrictions will pose an impediment to an NPDES discharge
from this location. The discharge is to an unnamed canal to the Northeast Cape Fear River and
the treated discharge will be well— aerated and is expected to contain significant concentrations
of oxygen —consuming waste. A description of the treatment process and contact information
Charlotte, NC
Irerracon
Memorandum
are summarized below.
A. Contact Information
Contact information for the applicant ,facility, and EAA preparer(Terracon) are as follows. The
facility is currently owned and occupied by Wilbara LLC who is owned by Southern States
Chemical. The Wilbara facility is a sulfuric acid manufacturing plant.
Applicant
Wilbara, LLC/Southern States Chemical
Attn: Steven Suek
4620 Hwy 421 N
Wilmington, North Carolina 28401
Phone: 910-762-5054
Fax: 910-762-1600
email: ssuek@sschemical.com
Facility
Wilbara, LLC
4620 Hwy 421 N
Wilmington, New Hanover County, North Carolina 28401
Phone: 910-762-5054
Fax: 910-762-1600
email: ssuek@sschemical.com
EAA Preparer
Terracon Consultants, Inc.
Attn: M. Neal McELveen, P.E.
2701 Westport Road
Charlotte, NC 28208
Phone:704-5948912
Fax:704-509-1888
Email:neal.mcelveen@terracon.com
B. Description of Proposed Project
The Wilbara facility presently utilizes a metal basin to collect non -contact cooling tower water,
boiler blowdown and cooling tower blow down. The dimensions of the basin and volume of the
basin are as follows:
Charlotte, NC
Irerracon
Memorandum
Dimensions:
30' X 40' X 4'
Surface Area:
1200 sq. feet
Volume:
4,800 cubic feet
Capacity —Water:
35,904 gallons
Description:
Non -Contact cooling tower water along with boiler and cooler tower blowdowns are presently
collected in the basin. Wilbara proposes to add process wash water associated with tank and
equipment cleaning, maintenance activities, and operational activities to this discharge stream.
The anticipated volume to be added, 3,700 gallons per year or approximately 14.25 gallons per
day (GPD -assumes 260 days per year), is minimal compared to the volume generated from
the non -contact cooling water and blowdown waters — 18,225 GPD (average). Discharge of the
tank/equipment/maintenance cleaning waters will be intermittent with some additions occurring
once every 2.5 (cleaning towers) and 6 years (tank cleanings).
The wastewater is continuously recirculated through a sprayer inside the basin to cool down the
wastewater. The wastewater is continuously sampled for pH content and adjusted accordingly
with sodium hydroxide and/or sulfuric acid to keep the wastewater pH levels between 6.00 and
9.00. Float switches determine the timing of wastewater release to activate the release pump for
discharge to Outfall 001. Information on the automatic pH controller is attached for your
reference. Typical chemicals used in the water for treatment include biocides, corrosion
inhibitors and sodium hydroxide (pH adjustment). Discharge occurs seven days per week and
the discharge is automated based on the level accumulated in the basin.
C. Summary of Process Information and Flow Estimates
As described above, the facility is presently permitted to discharge non -contact cooling water
along with boiler and cooling tower blowdown and discharges an average of 18,225 GPD.
These waters are collected in a steel basin where it is recirculated through a surface spray to
cool the water. The basin also has an automated pH controller for continuous pH sampling and
adjustments. The facility cleans and washes out sulfuric acid tanks ever 6 years and also cleans
equipment. The estimated volume to be added to the average discharge of 18,225 gallons per
day is approximately 14.25 GPD as discussed above. Pumping rates for discharge to outfall 001
are 75 gallons per minute (GPM) based on the facilities documented discharge monitoring
events.
Charlotte, NC
Irerracon
Memorandum
D. Low Flow Data for Receiving Stream
Low flow information for the receiving water(s) was obtained from the US Geological Society
(USGS)and the NCDEQ in Raleigh, North Carolina. Correspondence from the agencies is
provided in Attachment A. Generally, the discharge from the basin will be outfall 001 through
underground piping. From the point of discharge, underground piping runs northeast and
discharges to an unnamed canal that flows directly to the Northeast Cape Fear River.
As summarized in the USGS correspondence (copies of the correspondence are including in
the attachments), the USGS South Atlantic Water Science Center (Raleigh office) currently
refrains from providing (or updating previously determined) low -flow estimates for streams
known or suspected of being tidally affected. There are currently no techniques that allow for
quantifying the effects of tides on low flows.
Concerns that tides may possibly reduce low -flow discharges (that is, relative to low -flow
estimates for the same stream not tidally -affected) lead us to speculate that any such estimates
for these streams may be too high. Given the "back-n-forth" flow dynamics associated with tidal
effects, attempting to determine low -flow characteristics based on the assumption of uni-
directional flow characteristics is not meaningful.
Frequency Discharge
7Q10
Not Provided
30Q2
Not Provided
W7Q10
Not Provided
7Q2
Not Provided
STEP 2. Reasonable Projections for Flow
As discussed in the EAA Guidance Document ,non —municipal flow projections are based on
engineering design considerations and/or production projections rather than population
projections. Based on information available from the facility's present discharge of non -contact
cooling water, cooling tower blowdown and boiler blowdown the basin presently has an average
discharge of 18,225 GPD or 0.018225 MGD. With the addition of the tank and equipment
cleaning wash waters (14.25 GPD), the volume will increase to 18,239 GPD or 0.018239 MGD.
Charlotte, NC
Irerracon
Memorandum
STEP3. Evaluate Technologically Feasible Alternatives
As discussed in the EAA Guidance Document, discharges from the basin (non -domestic waste
water) are required to evaluate whether wastewater treatment plant(WWTP) connection , land
application, wastewater reuse, discharge to surface waters, and combinations of the above.
A. Connection to an Existing WWTP
Review of available sewer connection to the local treatment works is not presently available at
the facility; therefore, use of an existing WWTP is not feasible.
B. Land Application
The facility is located at 4620 Hwy 421 N, Wilmington, North Carolina. This location is in a rural
industrial area. The facility is located within the INVISTA property and has a current State
Stormwater Management System (Permit No. SW8 090331) that utilizes an infiltration basin for
stormwater. The basin designed was based on the site specific stormwater drainage areas. The
addition of the non -contact cooling water, boiler and cooling tower blowdown , and tank/process
equipment cleaning waters would exceed the design parameters of the infiltration system.
Based on the design and land constraints and the available land, this application is not feasible
at this time.
C. Wastewater Reuse
The reuse of the wash/cleaning waters, cooling waters and boiler blowdown is not feasible for
the sulfuric acid process due to impurities. Therefore, wastewater reuse is not technically
feasible.
D. Direct Discharge to Surface Waters
Surface water discharge has been determined to be the only technically and economically
feasible alternative for disposal of tank and equipment wash waters that are proposed to be
combined with the non -contact cooling water, and boiler cooling tower blow downs. Generally,
the discharge from the metal basin will be Outfall 001 through underground piping. From the
point of discharge, underground piping runs northeast and discharges to an unnamed canal that
flows directly to the Northeast Cape Fear River. Refer to Exhibit 1 for the location of the facility
in relation to the Northeast Cape Fear River. Exhibit 2 shows the location of Outfall 001 and the
coordinates for the discharge point.
Charlotte, NC
EXHIBITS
' S r � - � � S ', \� ter• ! L. .
W
---�"��
- r
.r+
n
1
�! - - _ =.r _1r •�' 34° 19' 16.476" N - -
f�' 77 ,58' 27.800" W
Approximate Site Boundary /
J. _ � � i Jam.-'y i �-/ y � - - •-�'-_-.,+i. .�
i
• � i
J f LA E SUrTON I r�,a f 5 �•� 4 � = _ _ - ZT'; rt..LJt ` f : c rn
GlWETKI
w_t f T•}+-•' ryt` i.
4 .,► ,
4-1
_ Cape Fear River Basin
Feet ® Approximate Site Boundary Source: 2011 National Geographic Society/ESRI, i-cubed
seamless USGS quadrangles (Castle Hayne, NC); Site
0 1,000,000 4,000 Approximate Outfall Location Boundary approximated byTerracon.
PM: Project No. Topographic Vicinity Map EXHIBIT
NM 71197840 NO.
Drawn By: Scale:
KT 1:51,363 1rerracon Wilmington Plant NPDES Permitting
Checked By: Filename: 4620 Highway 421 North
MW Topo Wilmington, New Hanover County,
Approved By: Date: 2701 Westport Rd Chadotte,NC2820 North Carolina
NM February 2020 Phone: (704) 509-1777 Fax: (704) 509-1777
Feet- Tidal Flow Source: 2011 National Geographic Society/ESRI, i-cubed
seamless USGS quadrangles (Castle Hayne, NC); Site
0 750 1,500 3,000 Approximate Outfall 001 Location Boundary approximated by Terracon.
PM: Project No.
NM 71197840
Drawn By: Scale:
KT 1:18,000
Checked By: Filename:
MW Site_Diagram
Approved By: Date:
NM February 2020
Irerracon
i Rd Charlotte, NC 28201
509-1777 Fax: (704)509-1777
Site Diagram EXHIBIT
NO.
Wilmington Plant NPDES Permitting 2
4620 Highway 421 North
Wilmington, North Carolina
s
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Table 3A
2012 PRESENT VALUE ESTIMATING TABLE
Project: Claire Manufacturing Facility, 2100 North Church St, Charlotte, NC
Note: prior to entering 2010 cost est into formulas in cells H7, F37 and F39 ou will need to delete the space prior to the " '.sign.
Projected Costs Over 20-yearPeriod
2012 Annual Operation and Maintenance Cost Estimate (enter 2012 cost estimate in column H formula)
$ 36,568
Inflation Factor =
2.09%
Discount Rate =
0.75%
Year
n
Inflated Annual
Inflated and Discounted
Cost
Annual Cost
2012
1
$37,332
$37,054
2013
2
$38,113
$37,547
2014
- 3
$38,909
$38,047
2015
4
$39,722
_
$38,553
--
2016
_ _ 5
$40,552
$39,065
2017
6
_ $41,400
$39,585
2018
_ 7
$42,265
$40,111
2019
8
__ $43,149
$40,645
2020
9
$44,050
$41,186
}
2021
10
$44,971
_
$41,733
2022
11
$45,911
$42,288
_ 2023
_ _ 12
$46,811
$42,851
2024
13
$47,850
$43,421
2025
14
$48,850
_
$43,998
- --
2026
_ 15
$49,871
$44,583
2027
16
$50,913
_
$45,176
2028
17
$51,978
$45,777
--
2029
18
$53,064
$46,386
2030
19
$54,173
_
$47,003
-
2031
20
$55,305
_
$47,628
Totals
$915,250
$842,639
_
_
(Current Value -not discounted)
jPresent Value -discounted
w
Basis for this
ears ayments
Current Value
Present Value
2012 Capital Cost Estimate (refer to accompanying table)
$14,720
$14,720
2012 Recurring Cost Estimate from above
$915,250
$842,639
_
2012 Lost Opportunit, Cost Estimate (enter 2012 cost estimate In column F formula
$0
$0
TOTAL
_
_
$929,970
$857,359
Page 1
ATTACHMENTS
McElveen, Neal
From:
Sent:
To:
Subject:
McKhenzy Welch, CPESC
Terracon Consultants, Inc
P 980-938-7436 1 M 704-430-3174
Welch, McKhenzy A
Thursday, February 20, 2020 10:50 AM
McElveen, Neal
FW: Tidally Influenced Waters
From: Albertin, Klaus P <klaus.albertin@ncdenr.gov>
Sent: Friday, January 31, 2020 3:08 PM
To: Welch, McKhenzy A <Mckhenzy.Welch@terracon.com>
Cc: Hill, David A <david.hill@ncdenr.gov>
Subject: Tidally Influenced Waters
Mckhenzy,
I would contact David Hill regarding your request since USGS has determined that the location of interest is tidally
influenced. His information is below and I've copied him on this e-mail.
David Hill
Environmental Specialist II
NC DEQ / Division of Water Resources / Water Quality Permitting
NPDES Complex Permitting, Wastewater Branch
919 707-3612 office
919 707 9000 main office
david.hill(cbncdenr.gov
Physical Address: 512 North Salisbury St.,Raleigh, NC, 27604
Mailing Address: 1617 Mail Service Center, Raleigh, NC, 27699-1617
Klaus Albertin, CFM
Water Supply Planning Engineer
Division of Water Resources
North Carolina Department of Environmental Quality
919 707 9035 office
919 733 3558 fax
klaus.albertin(cDncdenr.gov
512 N. Salisbury Street
1611 Mail Service Center
Raleigh, NC 27699
Email correspondence to and from this address is subject to the
(� North Carolina Public Records Law and may be disclosed to third parties.
McElveen, Neal
From: Welch, McKhenzy A
Sent: Thursday, February 20, 2020 10:50 AM
To: McElveen, Neal
Subject: FW: USGS response concerning... Re: Low Flow Request - Cape Fear River
McKhenzy Welch, CPESC
Terracon Consultants, Inc
P 980-938-7436 1 M 704-430-3174
From: Weaver, John C <jcweaver@usgs.gov>
Sent: Wednesday, January 29, 2020 10:57 AM
To: Welch, McKhenzy A <Mckhenzy.Welch@terracon.com>
Cc: Albertin, Klaus P <klaus.albertin@ncdenr.gov>; Weaver, John C <jcweaver@usgs.gov>
Subject: Fw: USGS response concerning... Re: Low Flow Request - Cape Fear River
Mckhenzy,
Just a quick note to say that I received your voice mail left yesterday.
I should be back in the office tomorrow (Thursday) and Friday, so will attempt to contact you on Thursday. If
you have some specific questions you want to give me an advance, that would be helpful.
Thanks,
JCWeaver
I Curtis Weaver, Hydrologist, PE Email: icweaver(dusgs.gov
USGS South Atlantic Water Science Center Online: httos;//www.usgs.gov/centers/sa-water
North Carolina - South Carolina - Georgia
3916 Sunset Ridge Road
Raleigh, NC 27607
Phone: (919) 571-4043 // Fax: (919) 571-4041
From: Weaver, John C <jcweaver@usgs.eov>
Sent: Monday, January 13, 2020 11:04 AM
To: Welch, McKhenzy A <Mckhenzv.Welch@terracon.com>
Cc: McElveen, Neal <Neal.Mcelveen@terracon.com>; Albertin, Klaus P <klaus.albertin@ncdenr.gov>; Grzyb, Julie
<iulie.grzyb@ncdenr.gov>; Weaver, John C <icweaver@usgs.gov>
Subject: USGS response concerning —Re: Low Flow Request - Cape Fear River
Mr. Welch,
In response to your inquiry about the low -flow characteristics for a location on the Cape Fear River or the
Northeast Cape Fear River in the vicinity of Wilmington in New Hanover County, the following information is
provided:
Visual inspection of the facility location using Google Earth places the point of interest east of Lake Sutton
between the Cape Fear River and Northeast Cape Fear River. Plotting the lat/long coordinates
(34-18-55.78"N, 77°58-26.76"W) provided via your January 10 email indicates a possible point of interest at
the headwaters of a small channel draining towards the Northeast Cape Fear River. Your email mentions
needing the low -flow statistics for the Cape Fear River.
Regardless of the location for the point of interest, both the Cape Fear River and Northeast Cape Fear River
are known to be tidally affected at near the facility location.
The USGS South Atlantic Water Science Center (Raleigh office) currently refrains from providing (or updating
previously determined) low -flow estimates for streams known or suspected of being tidally affected.
There are currently no techniques that allow for quantifying the effects of tides on low flows.
Concerns that tides may possibly reduce low -flow discharges (that is, relative to low -flow estimates for the
same stream not tidally -affected) lead us to speculate that any such estimates for these streams may be too
high. Given the "back-n-forth" flow dynamics associated with tidal effects, attempting to determine low -flow
characteristics based on the assumption of uni-directional flow characteristics is not meaningful.
You will need to contact the NCDEQ Division of Water Resources to obtain further guidance concerning any
efforts to obtain an NPDES permit for a location in a tidally -affected stream. Please note that I have cc:ed Mr.
Klaus Albertin with NCDEQ who a primary State contact for low -flow requests sent to USGS. I will defer you
to him concerning a member of the staff within the water -quality unit at NCDEQ who can provide you this
further guidance.
I regret this response does not provide the flow statistics you were seeking, but hope this information is
helpful in some manner or at least provides some direction to you in your efforts on this matter.
Thank you.
Curtis Weaver
J. Curtis Weaver, Hydrologist, PE Email: icweaverOusgs.gov
USGS South Atlantic Water Science Center Online: httvs://www.usgs.gov/centers/sa-water
North Carolina - South Carolina - Georgia
3916 Sunset Ridge Road
Raleigh, NC 27607
Phone: (919) 571-4043 // Fax: (919) 571-4041
From: Welch, McKhenzy A <Mckhenzy.Welch@terracon.com>
Sent: Friday, January 10, 2020 2:46 PM
To: Weaver, John C <icweaver@usgs.gov>
Cc: McElveen, Neal <Neal.Mcelveen@terracon.com>
Subject: [EXTERNAL] Low Flow Request - Cape Fear River
Mr. Weaver
We are preparing an Engineering Alternatives Analysis (EAA) for a site located at 460 US highway 421 North in
Wilmington, NC. An aerial photo of the site is pending once we receive the location of the current outfalls of the facility
but I have attached a topographic map for site location. We are required to submit summer 7Q10 and 30Q2 low flow
data for the Cape Fear River for the submittal. The latitude and longitude for the property off Google Earth is:
34°18'55.78"N
77°58'26.76"W
When I receive the approximate discharge area I will provide the data. Please let me know the cost and delivery options
for this data. Free to call myself or Neal McElveen with any questions or comments for additional information. Hope all
is well.
McKhenzy Welch, CPESC
Terracon Consultants, Inc
P 980-938-74361 M 704-430-3174
Terracon provides environmental, facilities, geotechnical, and materials consulting engineering services delivered with
responsiveness, resourcefulness, and reliability.
Private and confidential as detailed here (www.terracon.com/disclaimer). If you cannot access the hyperlink, please e-mail
sender.
Irerracon
March 31, 2020
Clerk of the City
102 N, 3rd Street
Wilmington, NC 28401
Re: Industrial Wastewater Discharge Permit Application — Local Government Review Form
Wilbara Sulfuric Acid Plant
4620 Highway 421 North
Wilmington, NC 28401
To Whom it Concerns::
On behalf of Wilbara, LLC/Southern States Chemical, Terracon Consultants, Inc. (Terracon) has
completed the enclosed Industrial NPDES Permit Application and supporting documentation for
the above -referenced facility.
As part of the permit application, the NCDEQ requires the City to complete the form following
this letter and return it to my attention via email. We appreciate you time and effort to complete
the form.
Should you have any questions please contact us at your earliest convenience at (704) 594 -
8912 or via email at neal.mcelveen(a)terracon.com .
Sincerely,
Terracon Consultants, Inc.
M. Neal McElveen, PE
Principal/Environmental Manager
Attachments:
Government Form
Exhibits: Exhibit 1: Topographic Map
Exhibit 2: Site Diagram
Appendix A: EPA Form 3510-1: General Information
EPA Form 3510-2C: Existing Manufacturing, Commercial, Mining, and Silviculture
Operations
Appendix B: EAA
Appendix C: Laboratory Analytical Reports
Terracon Consultants, Inc. 2701 Westport Road Charlotte, North Carolina 28208
P [704] 509 1777 F [704] 509 1888 terracon.conn
Attachment A. Local Government Review Form
■ General Statute Overview: North Carolina General Statute 143-215.1 (c)(6) allows input from local
governments in the issuance of NPDES Permits for non -municipal domestic wastewater treatment facilities.
Specifically, the EnviroiunenLal Management Commission (EMC) may not act on an application for a new non -
municipal domestic wastewater discharge facility until it has received a written statement from each city and county
government having jurisdiction over any part of the lands on which the proposed facility and its appurtenances are to
be located. The written statement shall document whether the city or county has a zoning or subdivision ordinance in
effect and (if such an ordinance is in effect) whether the proposed facility is consistent with the ordinance. The EMC
shall not approve a permit application for any facility which a city or county has determined to be inconsistent with
zoning or subdivision ordinances unless the approval of such application is determined to have statewide significance
and is in the best interest of the State.
■ Instructions to the Applicant: Prior to submitting an application for a NPDES Permit for a proposed facility,
the applicant shall request that both the nearby city and county government complete this form. The applicant must:
■ Submit a copy of the permit application (with a written request for this form to be completed) to the clerk of
the city and the county by certified mail, return receipt requested.
■ If either (or both) local government(s) fail(s) to mail the completed form, as evidenced by the postmark on the
r certified mail card(s), within 15 days after receiving and signing for the certified mail, the applicant may submit
the application to the NPDES Unit.
f.. As evidence to the Commission that the local government(s) failed to respond within 15 days, the applicant
j shall submit a copy of the certified mail card along with a notarized letter stating that the local government(s)
failed to respond within the 15-day period.
■ Instructions to the Local Government: The nearby city and/or county government which may have or has
jurisdiction over any part of the land on which the proposed facility or its appurtenances are to be located is required
to complete and return this form to the applicant within 15 days of receipt. The form must be signed and notarized.
h
Name of local government WILMINGTON
(City/County)
Does the city/county have jurisdiction over any part of the land on which the proposed facility and its appurtenances are
to be located? Yes [ ] No [ ] If no, please sign this form, have it notarized, and return it to the applicant.
Does the city/county have in effect a zoning or subdivision ordinance? Yes [ ] No [ ]
If there is a zoning or subdivision ordinance in effect, is the plan for the proposed facility consistent with the ordinance?
Yes[ ]
No[ ]
Date
State
County of
Signature
(City Manager/County Manager)
On this day of , , personally appeared before me, the said
name to me known and known to me to be the person
described in and who executed the foregoing document and he (or she) acknowledged that he (or she) executed the
same and being duly sworn by me, made oath that the statements in the foregoing document are true.
My Commission expires .(Signature of Notary Public
Irerracon
March 31, 2020
Clerk of the County
230 Government Center Drive
Suite 175
Wilmington, NC 28403
Re: Industrial Wastewater Discharge Permit Application — Local Government Review Form
Wilbara Sulfuric Acid Plant
4620 Highway 421 North
Wilmington, NC 28401
To Whom it Concerns::
On behalf of Wilbara, LLC/Southern States Chemical, Terracon Consultants, Inc. (Terracon) has
completed the enclosed Industrial NPDES Permit Application and supporting documentation for
the above -referenced facility.
As part of the permit application, the NCDEQ requires the County to complete the form following
this letter and return it to my attention via email. We appreciate you time and effort to complete
the form.
Should you have any questions please contact us at your earliest convenience at (704) 594 -
8912 or via email at neal.mceiveen(cDterracon.com .
Sincerely,
Terracon Consultants, Inc.
M. Neal McElveen, PE
Principal/Environmental Manager
Attachments:
Government Form
Exhibits: Exhibit 1: Topographic Map
Exhibit 2: Site Diagram
Appendix A: EPA Form 3510-1: General Information
EPA Form 3510-2C: Existing Manufacturing, Commercial, Mining, and Silviculture
Operations
Appendix B: EAA
Appendix C: Laboratory Analytical Reports
Terracon Consultants, Inc. 2701 Westport Road Charlotte, North Carolina 28208
P [704] 509 1777 F [704] 509 1888 terracon.com
(
[
[_ Attachment A. Local Government Review Form
■ General Statute Overview: North Carolina General Statute 143-215.1 (c)(6) allows input from local
governments in the issuance of NPDES Permits for non -municipal domestic wastewater treatment facilities.
" Specifically, the Environmental Management Commission (EMC) may not act on an application for a new non -
municipal domestic wastewater discharge facility until it has received a written statement from each city and county
government having jurisdiction over any part of the lands on which the proposed facility and its appurtenances are to
be located. The written statement shall document whether the city or county has a zoning or subdivision ordinance in
effect and (if such an ordinance is in effect) whether the proposed facility is consistent with the ordinance. The EMC
shall not approve a permit application for any facility which a city or county has determined to be inconsistent with
zoning or subdivision ordinances unless the approval of such application is determined to have statewide significance
and is in the best interest of the State.
■ Instructions to the Applicant: Prior to submitting an application for a NPDES Permit for a proposed facility,
the applicant shall request that both the nearby city and county government complete this form. The applicant must:
■ Submit a copy of the permit application (with a written request for this form to be completed) to the clerk of
the city and the county by certified mail, return receipt requested.
■ If either (or both) local government(s) fail(s) to mail the completed form, as evidenced by the postmark on the
certified mail card(s), within 15 days after receiving and signing for the certified mail, the applicant may submit
the application to the NPDES Unit.
■ As evidence to the Commission that the local government(s) failed to respond within 15 days, the applicant
shall submit a copy of the certified mail card along with a notarized letter stating that the local government(s)
failed to respond within the 15-day period.
■ Instructions to the Local Government: The nearby city and/or county government which may have or has
jurisdiction over any part of the land on which the proposed facility or its appurtenances are to be located is required
to complete and return this form to the applicant within 15 days of receipt. The form must be signed and notarized.
Name of local government NEW HANOVER
' (City/County)
! Does the city/county have jurisdiction over any part of the land on which the proposed facility and its appurtenances are
to be located? Yes [ ] No [ ] If no, please sign this form, have it notarized, and return it to the applicant.
Does the city/county have in effect a zoning or subdivision ordinance? Yes [ ] No [ ]
If there is a zoning or subdivision ordinance in effect, is the plan for the proposed facility consistent with the ordinance?
Yes [ ]
No [ ]
Signature
(City Manager/County Manager)
State of , County of
On this day of , , personally appeared before me, the said
name to me known and known to me to be the person
described in and who executed the foregoing document and he (or she) acknowledged that he (or she) executed the
same and being duly sworn by me, made oath that the statements in the foregoing document are true.
My Commission expires .(Signature of Notary
_
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McElveen, Neal
From: noreply shipping
Sent: Thursday, April 2, 2020 8:16 PM
To: McElveen, Neal
Subject: Shipment Notification
SendPro' Enterprise
Shipment Notification
FedEx Web Services
Shipped To:
Clerk of the County
230 Government Center Drive
Suite 175
Wilmington NC 28403
us
AttentionTo: Kym Crowell
Tracking Number 391579485798
Click the link below to view the tracking information.
http://track. carrier-tracki nq.com/track. acti on?carrierTvpe=Fed Ex&contentTvr)e=html&tracki na N um ber=391579485798
FedEx Web Services
Shipped To:
Clerk of the County
230 Government Center Drive
Suite 175
Wilmington NC 28403
us
AttentionTo: Kym Crowell
Tracking Number 391579912487
Click the link below to view the tracking information.
_http://track.ca rder-tracki nq.com/track. action?carrierTvpe=Fed Ex&contentTviDe=htm I &tracki naN um ber=391579912487
FedEx Web Services
Shipped To:
Clerk of the City
102 N. 3rd Street
Wilmington NC 28401
us
AttentionTo: City Clerk
Tracking Number 391580535311
Click the link below to view the tracking information.
htti)://track. carrier-tracki na. com/track. action?carrierTvpe=Fed Ex&contentTvpe=htm I&tracki ng N um ber=391580535311
1
pitneybovres
Generated by Pitney Bowes SendPro@) Enterprise
F�
Irerracon
March 31, 2020�"
Clerk of the City
>!C RpR2420
102 N, 3�d Street
�' �ff��..r✓Ep
Wilmington, NC 28401
r'' 47). z'
Re: Industrial Wastewater Discharge Permit Application — Local Government Review Form
Wilbara Sulfuric Acid Plant
4620 Highway 421 North
Wilmington, NC 28401
To Whom it Concerns::
On behalf of Wilbara, LLC/Southern States Chemical, Terracon Consultants, Inc. (Terracon) has
completed the enclosed Industrial NPDES Permit Application and supporting documentation for
the above -referenced facility.
As part of the permit application, the NCDEQ requires the City to complete the form following
this letter and return it to my attention via email. We appreciate you time and effort to complete
the form.
Should you have any questions please contact us at your earliest convenience at (704) 594 -
8912 or via email at neal.mcelveen(a)terracon.com .
Sincerely,
Terracon Consultants, Inc.
M. Neal McElveen, PE
Principal/Environmental Manager
Attachments:
Government Form
Exhibits: Exhibit 1: Topographic Map
Exhibit 2: Site Diagram
Appendix A: EPA Form 3510-1: General Information
EPA Form 3510-2C: Existing Manufacturing, Commercial, Mining, and Silviculture
Operations
Appendix B: EAA
Appendix C: Laboratory Analytical Reports
Terracon Consultants, Inc. 2701 Westport Road Charlotte, North Carolina 28208
P [704] 509 1777 F [704] 509 1888 terracon.com
m :j :J:a ilk
Gail Penny
Southern States Chemical
4620 US Highway 421 N
Wilmington, NC 28401
Element One Inc.
Wilmington,28412
Phone:910
Fax: 910 792-6853
ellab@eitab.com
FINAL REPORT OF ANALYSES
March 13, 2020
Client Project Name: TERRACON
Client Project Number
E1 Project Number e34438
Sample ID: Neutralized Acid
Sample Matrix W
Sample Type
Date Received
03/04/2020
Date Sampled 03/04/2020
Time Sampled
1415
Time Received
1535
Delivered by Courier
Sampler
Received by
LLB
E1 Sample #
34438
Parameter
Result Unit
Dilution
DL
Method
Date
Beryllium
< 0.01 mg/L
10
0.001
EPA 200.8
03/12/2020
Calcium
9.17 mg/L
10
0.05
EPA 200.8
03/12/2020
Chromium
< 0.01 mg/L
10
0.001
EPA 200.8
03/12/2020
Nickel
< 0.01 mg/L
10
0.001
EPA 200.8
03/1212020
Copper
0.022 mg/L
10
0.001
EPA 200.8
03/12/2020
Zinc
0.051 mg/L
10
0.001
EPA 200.8
03/12/2020
Arsenic
< 0.01 mg/L
10
0.001
EPA 200.8
03/12/2020
Selenium
0.012 mg/L
10
0.001
EPA 200.8
03/12/2020
Silver
< 0.01 mg/L
10
0.001
EPA 200.8
03/11/2020
Antimony
< 0.01 mg/L
10
0.001
EPA 200.8
03/12/2020
-- Thallium
< 0.01 mg/L
10
0.001
EPA 200.8
03/12/2020
Lead
< 0.01 mg/L
10
0.001
EPA 200.8
03/11/2020
Mercury
< 0.0001 mg/L
1
0.0001
EPA 245.1
Due to matrix interference, it was necessary to analyze sample for metals at a minimum 1 Ox dilution.
Ken Smith, Laboratory Director
34438 Southern States Report Compiled by ` L
NC Certifications: DW 37788 and DWQ DENR 604
Page 1 of 2
•
d #
Gail Penny - -
Southem States Chemical
4620 US Highway 421 N
Wilmington, NC 28401
Sample Matrix
Date Sampled 03/04/2020
Delivered by Courier
Parameter
Cyanide
Total Organic Carbon
COD
BOD
Ammonia-N
Total Suspended Solids
4;6L�n
Ken Smith, Laboratory birector
Element One Inc.
Wilmington,NC 28412
Phone: 910 r 1 8
a„
ellab@ellab.com
FINAL REPORT OF ANALYSES
March 13, 2020
Client Project Name: TERRACON
Client Project Number
E1 Project Number e34438
Sample ID: Neutralized Acid
Sample Type Date Received 03/04/2020
Time Sampled 1415 Time Received 1535
Sampler Received by LLB
E1 Sample # 34438
Result
Unit
Dilution
DL
Method
Date
< 0.005
mg/L
1
0.005
SM 4500CN C&E
03/09/2020
2.09
mg/L
1
1.0
SM 5310B
03/12/2020
< 10
mg/L
1
10
HACH 8000
03/06/2020
< 2
mg/L
2
SM 5210 B
03/04/2020
< 0.20
mg/L
1
0.20
SM 4500NH3 B&D
03/1012020
26.6
mg/L
1
2.5
SM 2540 D
03/05/2020
34438 Southern States Report Compiled by_P. D
NC Certifications: DW 37788 and DWQ DENR 604
Page 2of2
ra
46
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Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ® 910-392.0223 Lab a 910.3914424 Fax
710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 0 910,347.5843 Lab/Fax
Element One Date of Report: Mar 23, 2020
6319-D Carolina Beach Road
Customer PO #:
Wilmington NC 28412
Customer ID: 08100049
Attention: Paula Smith
Report #: 2020-03864
Project ID:
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-09382 Site: 34438
3/5/2020 10:30 AM Water Gail Penny
Test Method Results Date Analyzed
Inorganic Phenols
Comment:
Reviewed by:
EPA 420.1
<0.05 mq/L 03/19/qnqn
Report #: 2020-03864
F-
Analytical Environmental Services, Inc
Client: Environmental Chemists, Inc.
Project Name:
Lab ID: 2003D37-008
- :Analyses
Phenolics, Total Recoverable E420A
f Phenolics, Total Recoverable
i
t
:
t
I'
l
r._
Qualifiers: 13iue escecds maxtmmn contaminant level
RRL E4elorr reporting In.
H Holding nines for preparation or analysis exceeded
N Anaivte nut NE[. AC certifi,d
H Analyte detected "I the associated method blank
Greater than
�Result
rvaine
Result
i3RI.
Date: 20-Mar-20
Client Sample ID: 20-09382
Collection Date: 3/5/2020 10:30:00 AM
Matrix. Aqueobs
Reporting Dilution
Limit
Qua1 units SatchlD Date Analyzed Analyst
Factor
(E420.1)
0-05 mg/L 294069 1 03/19/202015:57 AT
E Estimated (value above quantttanon range)
S Spike Recovery outside limits due to matris
)Tarr See case narrative
r Ana(yzea in the lab which is a deviation from the method
Less than Result value
11 Estmated value detected below Reporang limit
Pape 10 of 14
(
f
Environmental Chemist, Inc., Wilmington, NC Lab #94
i_
Sample Receipt Checklist
Client: '{> P 2,
Date: Report Number:
5602 Windmill Way
Wilmington, NC 28405
910,392.0223
Receipt of sample:
ed UPS ❑ FedEx ❑
Other ❑
E
ES
BEii
1. Were custody seals present on the cooler?
Original
ES
temperature
upon
2. If custody seals were present, were they intact/unbroken?
receipt
_9C Corrected temperature upon receipt
How temperature taken: ❑ Temperature Blank
Against Bottles
IR Gun ID Thomas Traceable S/N 192511657
❑
YES
❑
NO
IR Gun Correction Factor °C: 0.0
3. If temperature of cooler exceeded 6°C,
YES
❑
NO
was Project Mgr.JQA notified?
4. Were proper custody procedures (relinquished/received)
YES
❑
NO
followed?
5. Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time listed on the COC?
POD
YES
YES
❑
❑
NO
8. Were tests to be performed listed on the COC?
PQ
YES
❑
NO
9. Did samples arrive in proper containers for each test?
NO
10. Did samples arrive in good condition for each test?
VYES
YES
❑
NO
11. Was adequate sample volume available?'
YES
❑
❑
NO
12. Were samples received within proper holding time for requested tests?
❑
NO
13. Were acid preserved samples received at a pH of <2?
YES
❑
NO
14, Were cyanide samples received at a pH >12?
❑
YES
❑
NO
15. Were sulfide samples received at a pH >9?
❑
❑
YES
YES
❑
❑
NO
16. Were NH3/TKNJPhenol received at a chlorine residual of <0.5 rn L?
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
* TOC/Voiatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet
Sample Preservation: ;Must be completed for any sample(s) incorrectly preserved or with headspace)
_ Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): HMSO, HNO3 HCI NaOH
Time of preservation: if more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Samples) Nere received with headspace
COMMENTS:
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����viro��me��W������i��s, Inc*
6602Windmill Way, Wilmington, N[284O5 ° 910.392.0223Lab ° 9l0.392/�24Faz
7l0Bm^esozwnRoad, Manu:,,NC27954 ° 252.473.5702La6/Fax
255-AWilmington Bj�bwo�]ud'monvJ]c'��CZ854V ° 9I0347.5843L^b/Fax
Element One
Date of Mar 23'2O2O
� S31Q-[}Carolina Beach Road
Customer pO#t
Wilmington NC 28412
Customer ID: 08100048
^ Attention: Ken Smith
Ropmrt#: 2020-03791
�
Project ID: 34438
Lab ID Sample ID:
ColYwotBmte/Tirme Matrix Sampled by
^20-00210 Sitm:34438
3/4/2020 2:15PM VVutmr Gail Penny
- Test
Method
Results Date Analyzed
1.1.1-Tr|Ch|uroethana
spA»:*
<0.5pg/L
03/06/2020
1.1.2.2-Tetronh|onoethane
cpAam
<&5pg/L
03/08/2020
' 1.1'2-Trioh}unoethene
spAzw
<0.5pg/L
03/08/2020
1.1-Dinh|oroethane
ep^m4
<0.5pg/L
03/06/2020
�1.1'D|oh!onoetheoe
en^«:w
<0.5Ag/L
03/06/2020
r1,2-Dich>orobenzene
Ee«uc*
«0.5pg/L
03/08C2020
/ 1.2,Dich|onoet ane
_
spAmw
<0.5pg/L
03/00/2020
1.2-Dioh|oropropone
en^ww
<0.5pg/L
03/06/2020
1.3-Dioh|orobenzene
sp»«m
<0.6pg/L
03/06/2820
_
1.4-Dioh|orobenzene
cp«sm
<0.5pQ/L
03/06/2020
- Acno\ein
epAmw
<1Opg/L
03/06/2020
- Acry|onihi{e
spAsw
<5pg/L
03/06/2028
Benzene
en^«u4
<0.5pO/L
03/06/2020
- Brornodioh|orornethane
cp^»e*
<0.5pg/L
03/08/2020
Bronnoforrn
EpA»m
<0.5pg/L
03/06/2020
_~ Bronnornethone
en^am
<0.5pg/L
03/06/2020
Carbon Tetrachloride
epAa»*
«0.5pg/L
03/08/2820
Ch|orobnnzene
sp^um
x0.5pg/L
03/06/2020
Chbroothana
sp«624
<0.5pg/L
03/08/2020
` Chloroform
epAee4
^8.5pg/L
03/00/2020
� Ch|oronnethene
sp^o2w
<0.5pg/L
03/06/2020
� cis-1.3-Dioh|oropnopene
spAa24
<0.5pg/L
03/06V2020
-� DibvornooNoronnethone
spAao4
<0.6ug/L
03/08/2020
Ethy|benzene
sp«62w
<0.5pg/L
03/06/2820
� &0+PXy)ene
En^«2w
«1.Opg/L
03/86/2020
Methylene chloride
sn^»u*
<0.5pg/L
03/06/2020
Report �. 20e0-03791 page Im4
Element One
Date of Report: Mar 23.202U
&' G310-DCarolina Beach Road
Customer PO#:
VVi|nninQtnn NC 28412
Customer ID: 08100048
� Attention: Ken Smith
Rmpmrt#: 2020-03781
�
Project ID: 34438
ortho-Xy|ene
cp«mw
<0.5pg/L
03/06/2020
^Tetraoh|oroethene
spA«c*
<0�5pg/L
03/06/2020
Toluene
sp^s2w
<U.bUg/L
03/06/2020
L Trans- 1.2'Dioh|unuetheno
spAe»4
<0.5pg/L
03/08/2020
_ trans- 1.3-Dich|oropn}pene
sP»o2w
<0.5pg/L
03/06/2020
' Trioh|oroethene
spAsc*
<0.5pg/L
03/06/2820
Thoh|oroOuovurnethane
sp«szw
<0�5pg/L
03/06/2020
| Vinyl chloride
[
spAeu*
<0.6pg/L
03/06C2020
2.4.6-Thoh|onopheno|
sp«eca
<5,10pg/L
03/05C2020
2.4-Dich|oropheno|
EPA 62e
x5AOVg/L
03/05/2020
^- 2.4-Oinnethy|pheno|
spAeua
<5.10pg/L
03/05/2020
2.4-Dinitropheno|
sp«eos
<25.5pg/L
03/05/2020
L 2-Ch|onopheno|
sp«suo
<5.10pg/L
03/05/2020
2-yWedhy|-4.8-dinibnphenol
F
epAsos
<25.5pg/L
03/05/2020
| 2-Nitropheno|
e*^62a
«25.5pg/L
03X05/2020
4-Ch|orm'3-nnethy|pheno|
spx«2s
<5.10pg/L
03/05/2020
-
� 4-Nbropheno|
spA*es
<25.5pg/L
03/05C2020
- Pentauh|oropheno|
cpAeos
<25.5pg/L
03/05/2020
phon0|
c*^mo
<5.10pQ/L
03/05C2020
- 1.2 Dipheny|hydnazine
epAnus
<5.10pg/L
03/05/2020
- 1.2.4-Trich|nrobenzene
ee^a»a
«5.10pg/L
03/05/3020
_ 1.2-Oich|orobenzene
ep»»xs
«5.10pg/L
03/05/2020
1.3-Dioh|onobenzene
sp««us
<5.10pg/L
03/05/2020
_ 1'4-Oich|onobenzene
s*^uu»
<5.10pg/L
03/05/2020
1-K4ethy|naphtho|ene
sp«oe«
<5.10pg/L
03/05/2020
2.4-Dinitnzbz|uene
sn^«ea
<510pg/L
03/05/2020
2.6-[)initroto|uene
sp«e«s
<5.10pQ/L
03/05/2020
? 2-Chiuronaphthai*ne
�'A:2:
<��1Opg/L
D3/O�/2O20
~� 2-Mathy|naphtha|ene
sp*ocs
<5.10pg/L
03/05/2028
3 3' Dich)orob�nzidinm
� .-
sp««»s
�
�1D2pg/L
03/05/2020
~ Report #:: e020-03u1
Page cof 4
Element One
Date wfReport: Mar 23.202O
&
8319-DCarolina Beach Road
Customer PO#:
Wilmington NC 28412
Customer ID: 88100049
«
0
Attention: � Ken Smith
Report#^ 2020'03791
`
-
Project ID: 34438
4-8romnphenylphenyl ether
spAmo
<5.10pg/L
03/85/2020
-
4-Ch|onophenylphenyl ether
epAaa
<5.10pg/L
03/05/2020
Aoenaphthene
spAe»»
«5.10pA/L
03/05/2020
L
Aoenaphthy|ene
epAau»
<5.10pg/L
03/06/2020
Anthracane
spA»c*
<5.10pg/L
03/05/2020
�
Benzidine
cpAau5
<10.2pg/L
03/05/2020
`
8enzo[e]pynene
sp«»cs
<5.10Ug/L
83/05/2020
�
Benzo(a)aOthracane
sm 625
<5.10pg/L
03/05/2020
Bonzo(b)MuonanMbene
spA625
<5.10pg/L
03/05/2020
Benzo(g.h.i)pery|ene
spAsus
<5.10pg/L
03/05/2020
�-
Benzo(k)Uuonuntheno
cpAoo5
<5.18pg/L
03/05/2020
Bio( oh|nromothy| )ethe,
sp»au:
<5.10pg/L
03/05/2020
�
Bie(2-Ch|nnoethoxy)methane
spA«zs
<5.10pg/L
03/05/2020
Bia(2-Ch|oroothy|)ather
En^ou»
<5.10pg/L
03/05/2020
�
-
Bia(2-Ch|orniaopropy|)ether
cpAaus
<5.10pg/L
03/05/2020
Bio(2'eth}4hexy|)phdha|ate
ep»am
<5.10pg/L
03/05/2020
�
Buty|benzy|phtha|aba
EPA «uo
<5.10pg/L
03/05/2020
�
Chrysene
Ep«ous
<5.10pQ/L
03/05/2820
Dibenzo(e,h)anthnacmng
spAoo«
<5.10pg/L
03/05/2020
^-
Diethy|phthe|ate
Ep^ous
<6.10pg/L
03/05/2020
Dimethy|phtha|aka
spAu2a
6.94pg/L
03/05/2020
Di-n-Bub/!Ahthe|ate
en^u2s
<5.10pg/L
03/05/2020
Di'n-Dcty|phthalate
spA»2s
<5.10pQ/L
03/05/2020
h
F|uonanthane
s'^«cs
<5.10Vg/L
03/05/2020
F|uorene
sn^«uu
<5.10pg/L
03/05/2020
U
�
Hexach|onobenzane
spA«us
<5.10pQ/L
03/05/2020
Hexach|orobutadigne
sp«mo
<5.10pg/L
03/05/2020
HexBohiorocydopenbsdiene
spwasn
<25.5pg/L
03/05/2020
~�
Haxach|oroethane
se««ea
<5.10pg/L
03/05/2020
yndeno(1.2.3-od)pyrene
ee«szs
<5.10pg/L
03/05/2020
��
Report #:: 20e0'037e1
Page nof 4
Report #:: 2020-03791 Page 4 of 4
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Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 2840S
910,392.0223
Sample Receipt Checklist
Client:,,
.
F
} Date: i? Report
Number:
Receipt of sample:
❑ YES ❑ NO
Delivered UPS ❑ Fedfx ❑ r ❑
❑ YES
❑
NO
N/A
N/A
dy seals present on the cooler?
1. We�Zio
Original temperature
upon
receipt 3
2. if G
QLseals were present, were they intact/unbroken?
.
How temperature taken: Corrected temperature upon receipt
❑ Temperature Blank
IR Gun ID:
Thomas Traceable S/N 192511657 Against Bottles
❑ YES
❑
NO
IR Gun Correction Factor'C: Q.0
3. If temperature of cooler
YES
YES
O
❑
NO
exceeded 6'C, was Project Mgr
4. Were proper custody ./CtA notified?
Procedures (relinquished/received) followed?
NO
S. Were sample 10's listed on the COL?
YES
S
O
❑
NO
6. Were saples ID's listed on sample containers?
mNO
E5
❑
NO
7. Were collection date and time listed on the COC?
YE5
❑
NO
8. Were tests to be performed listed on the COC?
Lq YES
NO
9. Did samples arrive in proper containers for each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
YES
❑
NO
11. Was adequate sample volume available?'
❑ YES
NO
12. Were samples received within proper holding time for requested tests?
13. Were acid preserved samples
❑ YES
❑ YES
❑
NO
received at a pH of <2?
14. Were cyanide samples received at a pH >12?
❑ YES
❑
❑
NO
SS. Were sulfide samples received at a pH >9?
❑ YES
❑
NO
NO
16. Were 11H3/TKN/Phenol received at a chlorine residual of <0.5 m/! ?
17, Were Sulfide/Cyanide
received at a chlorine residual of <O.S m/L?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
* Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrect) Samples) o -. ESQ( ,were received incorrect) y preserved or with headspace)
by adding (circle one): Hz a HNO3 HCI y Preserved and were adjusted accordingly
Time of preservation: � if NaOH
more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sam e r
notify the state lab if directed to analyzed by the customer. Who was notified, date and 3 Volatiles Sample(s) time:�� dC"LJ
Nere received with headspace
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