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Home My WebLink AboutWQ0004967_Monitoring - 03-2020_20200430 (2)GW-59A COMPLIANCE REPORT FORM,:', Permit # W Q Q0o 14%7 (Submit one each monitoring period with GW-59forms.) I Enter date monitoring results were due. ( ) Will this monitoring report (GIN-59 and GW-59A) YES NO be submitted after the established due date? x 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question f or 2 is "YES; list in the space provided below.the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YE NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is 'NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurr ce (for the / st two ears). NEON MWL)f M(slMJA�tMW, P44 MN MWZ MvI31N4U91tAw'i PAW Ce MwZiM►�3frIwSM�J� 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES C.Nw If the answer is "YES'; a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO" monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES" describe those actions in the space provided below. If the answer to question 7 is "NO'; contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/orpena/ties. g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. Signature of Permittee (in huthorized Agent) Date GW-59A 12/8/2003 SUBMIT FORM ON YELLOW PAPER ONLY DWATER QUALITY MONITORING: ANCE REPORT FORM Name: AIIJuice Realtl Name (if different): _ Crldmc, 352 Jet Street LLC County Henderson act Person: Barry Sester/Plant Manager Telephone#: 82"94-7736 Location/Site Name: MW-2 No. of wells to be sampled: 7 .L ID NUMBER (from Permit): MW-2 Date sample collected: 3-16-20 Depth: _ft. Well Diameter: 2 in. In to Water Level e254e: 14.89 ft. below measuring point Screened Interval: ft. to ft. wring Point is ft. above land surface Relative M.P. Elevation: ft. Tie of water pumped/bailed before sampling: - gallons )ate sample analyzed: a-1a-20m3-m-20 Laboratory Name: Pace IARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.040 mg/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO.) as N 00620 <0.040 mg/L Coliform: MF Total 315N /100mL Phosphorus: Total as P 00665 <0.050 mg/L (Note: Use MPN madied for highly Wrbid samples) Orthophosphate 70507 mg/L Dissolved Solids:Total 70300 227 mg/L AI -Aluminum 01105 mg/L pH (Lab) 00403 units Be - Barium omo7 ug/L TOC green mg/L Ca - Calcium 00916 mg/L Chloride 00940 32.3 mg/L Cd- Cadmium o1oz7 ug/L Arsenic 01002 ug/L Chromium: Total o1034 ug/L Grease and Oils oms2 mg/L Cu - Copper 01042 mg/L Phenol 32730 ug/L Fe - Iron 01045 7570 ug/L Sulfate rows mg/L Hg - Mercury 71900 ug/L Specific Conductance 00095 µMhos K - Potassium oo937 mg/L Total Ammonia 00610 28.5 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitmgan: NH.as N; Ammonia Nitrogen, Total) Mn- Manganese o1o5510200 ug/L TKN as N oo625 mg/L Ni - Nickel 01067 ug/L rui metrteuianon aystems Vnty tNRacn "D KepoRS): mrluent total VL)L.s: Robert Barr/Authorized Agent Permittee (or Authonzed Agent) Name and Title - Please print or type GW-59 Rev. 8/2013 :RMIT Number: Expiration Date: 3-21-22 In -Discharge UIC IDES Other WQr004967 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑' Spray Field 0 Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: pH 00400: 6.5 units Temp. og01o: 9.7 °C Spec. Cond. 000et µMhos Odor oroes: Slight Appearance Clear Certification No. 40 Pb - Lead 01051 ug/L Zn - Zinc oio92 mg/L Other (Specify Compounds and Concentration Units): NA Sodium 81500 ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? 0 - Yes (1) ® No (0) VOC 78732 method # method # method # method # Effluent Total VOCs: mg/L VOC Z- 4S DRY time of u SUBMIT FORM ON YELLOW PAPER ONLY :R QUALITY MONITORING: REPORT FORM ITY INFORMATION Please Pnat Cleary or Type Name: AlUuice Realty, LLC Name (if different): Address: 352 Jet Street ;o;yt act Person: Barry Sester/Plant Location/Site Name: MW-3 L ID NUMBER (from Permit): MW_3 ts=_'; Depth: _ft. h to Water Level 82646: 15.54 ft. below measuring point 6unng Point is ft. above land surface me of water pumped/bailed before sampling: Dies for metals were collected unfiltered: ❑ YES I County Henderson Telephone#: 828-694-7736 No. of wells to be sampled: 7 :RMIT Number: Expiration Date: 3-21-m in -Discharge UIC 'DES Other W00004967 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon m Remediation: Infiltration Gallery '❑ Spray Field CO Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample collected: 3-17-20 FIELD ANALYSES: WAS DRY Well Diameter: in. pH oo400: 5.9 units Temp. 000lo: 15.5 oC at time of µMhos sampling, Screened Interval:_ft. to _ft. Spec. Cond. 00094: check Relative M.P. Elevation: ft. Odor 00085: Slight here: Appearance Brown tint/Solids ate sample analyzed: a17-2003-21-20 Laboratory Name: Pace I RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 <0.040 mg/L Coliform: MF Fecal 31616 -4.0 /100mL Nitrate (NO.) as N 00620 0.17 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P oo665 0.09 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Dissolved Solids:Total 70300 127 mg/L At -Aluminum o11o5 mg/L pH (Lab) 00403 units Be - Barium 01007 ug/L TOC oo680 mg/L Ca - Calcium 00916 mg/L Chloride oosao 14.4 mg/L Cd - Cadmium 01027 ug/L Arsenic oloo2 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L Phenol 32730 ug/L Fe -Iron 0104514200 uglL Sulfate oo946 mg/L Hg - Mercury 71900 uglL Specific Conductance 00095 µMhos K - Potassium oo937 mg/L Total Ammonia ooslo 1.0 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn-Manganese o1o55863 ug/L TKN as N 00625 mg/L Ni - Nickel 01067 ua/L Robert Barr/Authorized Agent Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 8/2013 Certification No. 40 Pb - Lead 01051 ug/L Zn - Zinc 01092mg/L Other (Specify Compounds and Concentration Units) NA Sodium 23800 ug/L ORGANICS: (by GC, GO/MS, HPLC) (Specify test and method M ATTACH LAB REPORT.) Lab Report Attached? ED Yes (1) ® No (0) VOC 78732 method # method # method # method # FEW SUBMIT FORM ON YELLOW PAPER ONLY :R QUALITY MONITORING: REPORT FORM Name: AlUuice Realty, LLC Name (if different): Address: 1352 Jet Street Hendersonville NC 28792 County Henderson act Person: Barry Sester/Plant Manager Telephone#: 826E94-7736 Location/Site Name: No. of wells to be sampled: 7 .LID NUMBER (from Permit): MW-5 Depth: 80 ft. h to Water Level 82546: 49.99 ft. below measuring point guring Point is 2 ft. above land surface me of water pumped/bailed before sampling: - gallons Iles for metals were collected unfiltered: ❑ YES rl NO Date sample collected: 3-17-20 Well Diameter: 2 in. Screened Interval: 60 ft. Relative M.P. Elevation: 2185 sample analyzed: a17-20 to ago-2u Laboratory Name: Pace Analytical to 80 tL ft. RKAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD oo335 mg/L Nitrite (NO2) as N o0615 <0.040 mg/L Colifonn: MF Fecal 31616 <1.0 /100mL Nitrate (NO.) as N 00620 0.26 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.050 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Dissolved Solids:Total 70300 30.0 mg/L Al -Aluminum o1105 mg/L pH (Lab) 00403 _ units Be - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride oos4o 3.9 mg/L Cd - Cadmium 01027 ug/L Arsenic otom ug/L Chromium: Total olom ug/L Grease and Oils ooss2 ni - Cu - Copper 01042 mg/L Phenol 32730 ug/L Fe - Iron o1045 448 ug/L Sulfate oog45 mg/L Hg - Mercury 71900 ug/L Specific Conductance gross µMhos K - Potassium 00937 mg/L Total Ammonia 00610 <0.10 mg/L Mg - Magnesium 009N mg/L (PmnaniaNitmgeq NH,s N: Ammonia Nrogeq Total) Mn- Manganese 0105515-7 ug/L TKN as N 00625 mg/L Ni - Nickel o1o67 ug/L ror Kememation Systems Vnly (Attach Lab KepOr[e): Influent Total Robert Ban/Authorized Agent Permittee (or Authonzed Agent) Name and Title - Please print or type GW-59 Rev. 8/2013 :RMIT Number: Expiration Date: a31-m In -Discharge UIC 'DES Other W00004967 PE OF PERMITTED OPERATION BEING MONITORED 11 Lagoon m Remediation: Infiltration Gallery ❑ Spray Field ® Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: pH oo400: 6.5 units Spec. Cond. 000s4: Odor 00035: None Appearance Clear Pb - Lead 01051 Zn - Zinc 01092 WAS DRY at time of Temp o0010: 16.1 °C sampling, µMhos 1,lh� Certification No. 40 ug/L Other (Specify Compounds and Concentration Units): NA Sodium < 5000ug/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method A ATTACH LAB REPORT.) Lab Report Attached? ❑7 Yes (1) ❑ No (0) VOC 78732 , method # method # method # method # mg/L Effluent Total VOCs: VOC 0 SUBMIT FORM ON YELLOW PAPER ONLY ;R QUALITY MONITORING: REPORT FORM Name: AIIJuice Realty, LLC Name (if different): Address: 352 Jet Street County Henderson act Person: Barry Sester/Plant Manager Telephone#: 828-694-7736 Location/Site Name: MW-7 No. of wells to be sampled: 7 :RMIT Number: Expiration Date: 3-21-22 m-Discharge UIC DDES Other W00004967 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field 0 Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump 13 Other: L ID NUMBER (from Permit): MW-7 Date sample collected: 3-16-20 FIELD ANALYSES: Depth: _ft. Well Diameter, —in. pH 00400: 4.8 units Temp. 000to: 11.1 °C h to Water Level 62546: 20.91 ft. below measuring point Screened Interval: _ft. to ft. Spec. Cond. 00094: µMhos curing Point is ft. above land surface Relative M.P. Elevation: ft. Odor 000ss: None ne of water pumpedibailed before sampling: gallons Appearance Clear Dles for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO ate sample analyzed: 3-16-20 to 3-26-20 Laboratory Name: Pace 11RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (1102)as N 00615 <0.040 mg/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NOa). as N 0062o 2.6 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.050 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Dissolved Solids:Total 703M 46.0 mg/L At -Aluminum o1105 mg/L pH (Lab) 00403 units Be - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 11.4 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L Phenol 32730 ug/L Fe - Iron 01045 <50.0 uglL Sulfate rows mg/L Hg - Mercury 71900 ug/L Specific Conductance 00095 µMhos K - Potassium oo937 mg/L Total Ammonia oo610 <0.10 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nibageq NH,,as N;Ammnnia Nitroge, Toleg Mn- Manganese olo55 438 ug/L TKN as N 00625 mg/L Ni - Nickel o1o67 ug/L hor Kemealanon systems unly IA=cn Lan Robert Barr/Authorized Agent Pennirtee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 812013 Influent total Certification No. 40 Pb - Lead o1o51 ug/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): NA Sodium 8430 ua/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? El Yes (1) 0 No (0) VOC 78732 , method # method # method # method # mg/L Effluent Total VOCs: VOC W AS DRY time of here: SUBMIT FORM ON YELLOW PAPER ONLY :R QUALITY MONITORING: REPORT FORM Name: AIIJuice Realty, LLC Name (if different): Address: 352 Jet Street County Henderson act Person: Barry Sester/Plant Manager Telephone#: 828-694-7736 Location/Site Name: MW-8 No. of wells to be sampled: 7 L ID NUMBER (from Permit): MW-8 Depth: _ft. In to Water Level 82546: 20.73 ft. below measuring point curing Point is ft. above land surface ne of water pumped/bailed before sampling: gallons -RMIT Number: Expiration Date: se1-2z m-Discharge UIC IDES Other WQ0004967 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon m Remedialion: Infiltration Gallery 0 Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample collected: 3-16-20 FIELD ANALYSES: Well Diameter: — in. pH 00400: 5.6 units Temp. otto10: 12.3 oC Screened Interval:_ft. to _ft. Spec. Cond. oo0s4: µMhos Relative M.P. Elevation: ft. Odor 00085: None Appearance Clear and field acidified: ❑ YES ❑ NO ate sample analyzed: s'&-20to 3-262o Laboratory Name: Pace UFUI METERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 <0.040 mg/L Coliform: MF Feral 31616 <1.0 /100mL Nitrate (NO,) as N oo62o 1.7 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.050 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 705m mgJL Dissolved Solids:Total 70300 115 mg/L At -Aluminum ol1o5 mg/L pH (Lab) o04o3 units Be - Barium olo07 ug/L TOC oo68o mg/L Ca - Calcium 00916 mg/L Chloride ooeao 19.7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olom ug/L Grease and Oils oc552 mg/L Cu - Copper olo42 mg/L Phenol 32730 ug/L Fe - Iron o1o4s <50.0 ug/L Sulfate oosa5 mgJL Hg - Mercury 71900 ug/L Specific Conductance 000gs µMhos K - Potassium oogs7 mgJL Total Ammonia 00610 '0.10 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitragen; NH3as N; Ammonia Nitrogen. Totap 2740 Mn - Manganese rilluglL TKN as N 00625 mg/L Ni - Nickel oio67 ug/L Robert Barr/Authorized Agent Pemlittee (of Authorized Agent) Name and Title - Please print or type GW-59 Rev. 8/2013 Certification No. 40 Pb - Lead 01051 ug/L Zn-Zinc olo92 mq/L Other (Specify Compounds and Concentration Units): NA Sodium 35400 uq/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑+ Yes (1) ® No (0) VOC 78732 , method # method # method # method # DRY e of n SUBMIT FORM ON YELLOW PAPER ONLY DWATER QUALITY MONITORING: IANCE REPORT FORM Name: AIIJuice Realty, LLC Name (if different): Address: -352 Jet Street County Henderson act Person: Barry Sester/Plant Manager Telephone#: 828-694-7736 Location/Site Name: MW-9 No. of wells to be sampled: 7 L ID NUMBER (from Permit): MW-9 Depth: _ft. h to Water Level 62546: 36.75 ft. below measuring point wring Point is ft. above land surface ne of water pumpedthailed before sampling: :RMIT Number: Expiration Date: a21-zz ,n-Discharge UIC IDES Other W00004967 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon m Remediation: Infiltration Gallery ❑ Spray Field ® Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample collected: 3-17-20 FIELD ANALYSES: Well Diameter: _in, pH 00400: 5.7 units Temp. 000lo: 13.2 eC Screened interval:_ft. to _ft. Spec. Cord. 00094: µMhos Relative M.P. Elevation: ft. Odor 00085: None Appearance Clear )ate sample analyzed: 117-20 b 3-26-2o Laboratory Name: Pace rARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO,) as N 00615 <0.040 mg/L Coliform: MF Feral 31616 <1.0 /100mL Nitrate (NO,) as N 00620 021 mg/L Coliform: MF Total 31504 /100ni Phosphorus: Total as P 00665 <0.050 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Dissolved Solids:Total 7030025.0 mg/L AI -Aluminum 01105 mg/L pH (Lab) aD403 units Be - Barium 01007 ug/L TOC oc680 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 1.6 mg/L Cd - Cadmium 01027 ug/L Arsenic oloo2 ug/L Chromium: Total 01034 ug/L Grease and Oils oo552 mg/L Cu - Copper 01042 mg/L Phenol 32730 ug/L Fe - Iron 01045 147 ug/L Sulfate 00945 ni Hg - Mercury 71goo ug/L Specific Conductance 000ss µMhos K - Potassium 00937 mg/L Total Ammonia 00610 <0.10 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitragen: NH,as N;Ammonia Nimagen, Total) Mn- Manganese 01 o5557.1 ug/L TKN as N 00625 ni Ni - Nickel 01067 ug/L ror RemewanOn 0yslents Vrly (Anacn L20 KePOM): Influent total VUGs: Robert Barr/Authorized Agent Permiftee (or Authorized Agent) Name and Tft e - Please pnnt retype GW-59 Rev. 812013 Certification No. 40 Pb - Lead 01051 _ ug/L Zn - Zinc 01092 mq/L Other (Specify Compounds and Concentration Units) NA Sodium 5100 ug/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑7 Yes (1) ❑ No (0) VOC 78732 method # method # method # method # Effluent Total VOCs: VOID 4S DRY time of SUBMIT FORM ON YELLOW PAPER ONLY iR QUALITY MONITORING: REPORT FORM Name: AIIJuice Realty, LLC Name (if different): Address: 352 Jet Street act Person: Barry Sester/Plant Manager Location/Site Name: MW-10 L ID NUMBER (from Permit): MW-10 Depth: _ft. h to Water Level 62546: 21.18 ft. below measuring point luring Point is ft. above land surface ne of water pumped/bailed before sampling: tiles for metals were collected unfiltered: ❑ YES I County Henderson Telephone#: 82M94-7736 No. of wells to be sampled: 7 Number: Expiration Date: )DES Other WQ0004967 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon m Remediation: infiltration Gallery I] Spray Field ® Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample collected: 3-16-20 FIELD ANALYSES: Well Diameter:_ in. pH oo400: 4.6 units Temp.coolo: 10.5 °C Screened Interval: ft. to _ft. Spec. Cond. room µMhos Relative M.P. Elevation: ft. Odor 000m None gallons Appearance Clear NO and field acidified: ❑ YES ❑ NO ate sample analyzed: 3-16-20 to a.2e-20 Laboratory Name: Pace 11RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.040 mg/L Coliform: MF Fecal 31616 <7.0 /100mL Nitrate (NO3) as N o062o 4.0 mg/L ColiformrMF Total 31504 /100mL Phosphorus: Total as P 00665 <0.050 mg/L (Note: Use MPN methed for highly turbid samples) Orthophosphate 70507 mg/L Dissolved Solids:Total 70300 92.0 mg/L Al -Aluminum ono, mg/L pH (Lab) 00403 units Be - Barium 01007 ug/L TOC oosao mg/L Ca - Calcium oa916 mg/L Chloride oosao 37.3 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L Phenol 3273o ug/L Fe - Iron 01045 69.1 ug/L Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Specific Conductance 00095 µMhos K - Potassium m937 mg/L Total Ammonia radio <0.10 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NN,as N; Ammonia Nitrogen. Total Mn- Manganese oloss 52.9 ug/L TKN as N 00625 mg/L Ni - Nickel olo67 ug/L For Remediation Systems Only (Attach Lab Reports): Robert Barr/Authorized Agent Permitte , (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 812013 Influent Total VOCs: Certification No. 40 Pb - Lead 01051 ug/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): NA Sodium 25100 uq/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑+ Yes (1) ® No (0) VOC 73732 , method # method # method # method # Effluent Total VOCs: VOC Removal AS DRY time of here: ,�a�eAnalj6cal' www.paesls8s.dem March 26, 2020 Mr. Robert Barr RPB Systems Inc. P.O. Box 1325 Asheville, NC 28802 RE: Project: ALL JUICE MW 3-16-2020 Pace Project No.: 92469665 Dear Mr. Barr: Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on March 16, 2020. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, 4-- Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 25 _del I �ac"Analidkale www.pecelabs.cam March 26, 2020 Mr. Robert Barr RPB Systems Inc. P.O. Box 1325 Asheville, NC 28802 RE: Project: ALL JUICE MW 3-17-2020 Pace Project No.: 92469871 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7178 Dear Mr. Barr: Enclosed are the analytical results for sample(s) received by the laboratory on March 17, 2020. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, 4-- Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 25 ceAnalytical e www.pecelabesem ANALYTICAL RESULTS Pace Analytical services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: . ALL JUICE MW 3-16-2020 - - Pace Project No.: 92469665 Sample: MW-2 Lab ID: 92469666001 Collected: 03/16/20 10:45 Received: 03/16/2016:10 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual Monitoring Well Data Analytical Method: Collected By Mark 1 03/16/20 10:45 Swann Collected Date 3116120 1 03/16/20 10:45 Collected Time 10:45 1 03/16/20 10:45 pH 6.5 Sid. Units 1 03/16/20 10:45 Temperature 9.7 deg C 1 03/16/20 10:45 Static Water Level 14.89 feet 1 03/16/20 10:45 Specific Conductance 664 umhos/cm 1 03/16/20 10:45 Oxidation Potential 42.30.48 mV 1 03/16/20 10:45 Turbidity 1.64 NTU 1 0311612010:45 Odor Slight 1 03/16/20 10:45 Odor Appearance Clear 1 03/16/20 10:45 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Iron 7570 ug/L 50.0 1 03/18/20 01:31 03/20/20 20:35 7439-89-6 Manganese - 10200 ug/L 25.0 5 03/18/20 01:31 03/21/20 14:34 7439-96-5 Sodium 81500 ug/L 5000 1 03/18/20 01:31 03/20/20 20:35 7440-23-5 2540C Total Dissolved Solids Analytical Method: SM 254OC-2011 Total Dissolved Solids 227 mg/L 25.0 1 03/18/20 15:46 MBIO 9222D Fecal Coliform AVL Analytical Method: SM 922213-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms ND CFU/100 mL 1.0 1 03/16/20 17:39 03/17/20 17:24 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Nitrogen, Ammonia 28.5 mg/L 0.30 3 03126/2011:38 7664-41-7 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, Nitrate NO mg/L 0.040 1 03/17/20 16:26 14797-55-8 Nitrogen, Nitrite NO mg/L 0.040 1 03/17/2016:26 14797-65-0 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus NO mg/L 0.050 1 03/18/20 15:22 03/18/20 20:34 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 32.3 mg/L 1.0 1 03/17/2011:48 16887-00-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/26/2020 05:49 PM - without the written consent of Pace Analytical Services, I.I.C. Page 4 of 25 �acehlaljdicalo wwepscelehs.rarn ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: ALL JUICE MW3-17-2020 - Pace Project No.: 92469871 Sample: MW-3 Lab ID: 92469871001 Collected: 03/1712015:05 Received: 03/1712016:10 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual Monitoring Well Data Analytical Method: Collected By Mark 1 03/17/20 15:05 Swann Collected Date 3117/20 - 1 03/17/20 15:05 Collected Time 15:05 1 03/17/20 15:05 pH 5.9 Std. Units 1 03/17/20 15:05 Temperature 15.5 deg C 1 03/17/20 16:05 Static Water Level 15.54 feet 1 03/17/20 15:05 Specific Conductance 234 umhos/cm 1 03/17/20 15:05 Oxidation Potential 75.8 my 1 03/17/20 15:05 Oxygen, Dissolved 0.18 mg/L 1 03/17/20 15:05 7782-44-7 Turbidity 15.37 NTU 1 03117/2016:05 Odor Slight 1 03/17/20 15:05 Odor Appearance Brown Tint 1 03/17/20 15:05 / Solids 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.41994 Iron 14200 ug/L 50.0 1 03120/2001:46 03121/2016:47 7439-89-6 Manganese 863 ug/L 5.0 1 03/20/2001:46 03121/2016:47 7439-96-5 Sodium 23800 ug/L 5000 1 03/20/20 01:46 03/21/20 16:47 7440-23-5 2640C Total Dissolved Solids Analytical Method: SM 254OC-2011. Total Dissolved Solids 127 mg/L 25.0 1 03/18/20 15:46 MBIO 9222D Fecal Coliform AVL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms NO CFU/100 mL 4.0 4 03/17/20 18:04 03/18/20 17:08 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Nitrogen, Ammonia 1.0 mg/L 0.10 1 03126/2013:14 7664-41-7 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, Nitrate 0.17 mg/L 0.040 1 03118/2013:12 14797-55-8 Nitrogen, Nitrite NO mg/L 0.040 1 0311812013:12 14797-65-0 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus 0.090 mg/L 0.050 1 03/1812015:22 03/18/2020:38 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 14.4 mg/L 1.0 1 03118/2018:27 16887-00-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 03/26/2020 06:00 PM without the written consent of Pace Analytical Services, U.C. Page 4 of 25 42XAnalytieal e w .pacfhnsxaro ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: ALL JUICE MW3-17-2020 Pace Project No.: 92469871 Sample: MW-5 Lab ID: 92469871002 Collected: 03/17/20 14:05 Received: 03/17/2016:10- Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Collected By Mark 1 03/17/20 14:05 Swann Collected Dale - 3117120 1 03/17/20 14:05 Collected Time 14:05 1 03/17/20 14:05 pH 6.5 Std. Units 1 0311712014:05 Temperature 16.1 deg C 1 03/17/20 14:05 Static Water Level 49.99 feet 1 03/17/20 14:05 Specific Conductance 123 umhos/cm 1 03/17/20 14:05 Oxidation Potential 130.3 my 1 03/17/20 14:05 Oxygen, Dissolved 5.36 mg/L 1 03/17/20 14:05 7782-44-7 Turbidity 9.52 NTU 1 03/1712014:05 Odor No Odor 1 03/1712014:05 Appearance Clear 1 03/17/20 14:05 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Iron 446 ug/L 50.0 1 03/20/2001:46 03121/2016:50 7439-89-6 Manganese 16.7 ug/L 5.0 1 03120/2001:46 03121/2016:50 7439-96-5 Sodium ND ug/L 5000 1 03/20/2001:46 03/21/2016:50 7440-23-5 2640C Total Dissolved Solids Analytical Method: SM 254OC-2011 Total Dissolved Solids 30.0 mg/L 25.0 1 03/18/20 15:46 MB10 9222D Fecal Coliform AVL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms - NO CFU/100 mL 1.0 1 03/17/20 18:04 03/18/20 17:08 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Nitrogen, Ammonia NO mg/L 0.10 1 03126/2013:16 7664-41-7 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, Nitrate 0.26 mg/L 0.040 1 03/18/20 13:11 14797-55-8 Nitrogen, Nitrite NO mg/L 0.040 1 03/18/20 13:11 14797-65-0 366.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus NO mg/L 0.050 1 03118/2015:22 0311812020:39 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 3.9 mg/L 1.0 1 - 0311812018:27 16887-00-6 Date: 03/26/2020 06:00 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. D6 Page 5 of 25 aceAna116ca1e wanopecalebacae ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: ALL JUICE MW 3-16-2020 Pace Project No.: 92469665 Sample: MW-7 Lab ID: 92469665002 Collected: 03/16/20 12:00 Received:. 03/1612016:10 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual Monitoring Well Data Analytical Method: Collected By Mark 1 03/16/20 12:00 Swann Collected Date 3116120 1 03/16/20 12:00 Collected Time 12:00 1 03/16/20 12:00 pH 4.8 Sid. Units 1 0311612012:00 Temperature 11.1 deg C 1 03/16/20 12:00 Static Water Level 20.91 feet 1 03/16/20 12:00 Specific Conductance 76 umhos/cm 1 03/16/20 12:00 Oxidation Potential 131.3 my 1 03/16/20 12:00 Oxygen, Dissolved - 4.44 mg/L 1 03/16/20 12:00 7782-44-7 Turbidity 1.3 NTU 1 03/16/20 12:00 Odor No Odor 1 03/16/20 12:00 Appearance Clear 1 03/16/20 12:00 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Iron NO ug/L 50.0 1 03/19/2001:06 03120/2017:42 7439-89-6 Manganese 438 ug/L 5.0 1 03/19/20 01:06 03/20/20 17:42 7439-96-5 Sodium 8430 ug/L 5000 1 03/19/2001:06 03/21/2014:22 7440-23-5 2640C Total Dissolved Solids Analytical Method: SM 254OC-2011 Total Dissolved Solids 46.0 mg/L 25.0 1 03/18/20 15:46 MBIO 9222D Fecal Coliform AVL Analytical Method: SM9222D-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms ND CFU/100 mL 1.0 1 03/16/20 17:39 03/17/20 17:24 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Nitrogen, Ammonia NO mg/L 0.10 1 03/26/20 11:02 7664-41-7 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, Nitrate 2.6 mg/L 0.040 1 03/17/20 16:29 14797-55-8 Nitrogen, Nitrite ND mg/L 0.040 1 03/17/20 16:29 14797-66-0 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus ND mg/L 0.050 1 03/18/2015:22 0311812020:36 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 11.4 mg/L 1.0 1 03/17/2011:49 16887-00-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/26/2020 05:49 PM without the written consent of Pace Analytical Services, U.C. Page 5 of 26 1.41111, �aceAnaljftala www.pacalrbsxars ANALYTICAL RESULTS Project: ALL JUICE MW3.16-2020 Pace Project No.: 92469665 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: MW-6 Lab ID: 92469665003 Collected: 03/16/20 14:35 Received: 03/16/20 16:10 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method: Collected By Mark 1 03/16/20 14:35 Swann Collected Date 3116120 1 03/16/20 14:35 Collected Time 14:35 1 03/16/20 14:35 pH 5.6 Std. Units 1 03/16/20 14:35 Temperature 12.3 deg C 1 03/16/20 14:35 Static Water Level 20.73 feet 1 03/16/20 14:35 Specific Conductance 184 umhos/cm 1 03/16/20 14:35 Oxidation Potential 153.4 my 1 03/16/20 14:35 Oxygen, Dissolved 0.27 mg/L 1 03/16/20 14:35 7782-44-7 Turbidity 3.04 NTU 1 - 03/16/20 14:35 Odor No Odor 1 03/16/20 14:35 Appearance - Clear 1 0311612014:35 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method:. EPA 200.7 Rev 4.4 1994 Iron NO ug/L 50.0 1 03/19/20 01:06 03/20/20 17:45 7439-89-6 Manganese 2740 ug/L 5.0 1 03/19/20 01:06 03/20/20 17:45 7439-96-5 Sodium 36400 ug/L 5000 1 03/19/20 01:06 03/21/20 14:25 7440-23-5 2540C Total Dissolved Solids Analytical Method: SM 254OC-2011 Total Dissolved Solids 115 mg/L 25.0 1 03/18/20 15:46 MBIO 9222D Fecal Collform AVL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms NO CFU/100 mL 1.0 1 03/16/20 17:39 03/17/20 17:24 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Nitrogen, Ammonia ND mg/L 0.10 1 03/26/20 11:06 7664-41-7 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, Nitrate - 1.7 mg/L 0.040 1 03/17/20 16:32 14797-55-8 Nitrogen, Nitrite NO mg/L 0.040 1 03/17/20 16:32 14797-65-0 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus NO mg/L 0.050 1 03/18/2015:22 03/18/2020:37 7723-14-0 4600 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 19.7 mg/L 1.0 1 03/1712011:50 16887-00-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/26/2020 05:49 PM without the written consent of Pace Analytical Services, L-C. Page 6 of 25 "AnalXical %fW.pscelebs.cea Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: ALL JUICE MW 3-17-2020 Pace Project No.: 92469871 Sample: MW-9 Lab ID: 92469871003 Collected: 03/17/20 12:10 .Received: 03/1712016:10 Matrix: Water Parameters Results Units I Report Limit DF Prepared Analyzed CAS No. Monitoring Well Data Analytical Method: Collected By Mark 1 03/17/20 12:10 Swann Collected Date 3117120 - 1 03/17/20 12:10 Collected Time 12:10 1 03/17/20 12:10 pH 5.7 Std. Units 1 03/17/20 12:10 Temperature 13.2 deg C 1 03/17/20 12:10 Static Water Level 36.75 feet 1 03/17/20 12:10 Specific Conductance 44 umhos/cm 1 03/17/2012:10 Oxidation Potential 123.3 my 1 03/17/20 12:10 Oxygen, Dissolved 6.78 mg/L 1 03/17/20 12:10 7782-44-7 Turbidity 9.52 NTU 1 03/17/20 12:10 Odor No Odor 1 03/17/20 12:10 Appearance Clear 1 03/17/20 12:10 200.7 MET ICP - Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Iron 147 ug/L 50.0 1 03/20/20 01:46 03/21/20 16:53 7439-89-6 Manganese. 57.1 ug/L 5.0 1 03120/2001:46 03/21/2016:53 7439-96-5 Sodium 5100 ug/L 5000 1 03/20/20 01:46 03121/2016:53 7440-23-5 2640C Total Dissolved Solids Analytical Method: SM 254OC-2011 Total Dissolved Solids 25.0 mg/L 25.0 1 03/18/20 15:46 MBIO 9222D Fecal Coliform AVL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms ND CFU/100 mL 1.0 1 03/17/20 17:24 03/18/20 17:08 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Nitrogen, Ammonia ND mg/L 0.10 1 03/26/2013:17 7664-41-7 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, Nitrate 0.21 mg/L 0.040 1 03/18/20 13:09 14797-55-8 Nitrogen, Nitrite ND mg/L 0.040 1 03/18/20 13:09 14797-65-0 366.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus NO mg/L 0.050 1 03/18/2015:22 0311812020:40 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 1.6 mg/L 1.0 1 03/18/2018:28 16887-00-6 Qual REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 03/26/2020 06:00 PM without the written consent of Pace Analytical Services, L-C. Page 6 of 25 ceAnalytical s wvraincelaba.00111 ANALYTICAL RESULTS Pau Analytical services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 'Project: ALL JUICE MW3-16-2020 - - - Pace Project No.: 92469666 Sample: MW-10 Lab ID: 92469665004 Collected: 03116120 13:10 Received: 03/16/20 16:10 Matrix: Water Parameters Monitoring Well Data Collected By Collected Date Collected Time pH Temperature Static Water Level Specific Conductance Oxidation Potential Oxygen, Dissolved Turbidity Odor Appearance 200.7 MET ICP Iron Manganese Sodium 2540C Total Dissolved Solids Total Dissolved Solids MBIO 9222D Fecal Coliform AVL Fecal Coliforms 350.1 Ammonia Nitrogen, Ammonia 353.2 Nitrogen, N021NO3 unpres Nitrogen, Nitrate Nitrogen, Nitrite 365.1 Phosphorus, Total Phosphorus 4500 Chloride Chloride Date: 03/26/2020 05:49 PM Results Units Report Limit DF Prepared Analyzed CAS No. Oual Analytical Method: Mark Swann 3116120 13:10 4.6 Std. Units 10.5 deg C 21.18 feel 174 umhos/cm 162.1 my 5.65 mg/L 3.17 NTU No Odor Clear 1 03/16/20 13:10 03116120 13:10 03116120 13:10 03/16/20 13:10 03/16/20 13:10 03/16/20 13:10 03116/20 13:10 03/16/20 13:10 03/16/20 13:10 7782-44-7 03/16/20 13:10 03/16/20 13:10 03/16/20 13:10 Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 69.1 ug/L 50.0 1 03/19/20 01:06 03/20/20 17:48 7439-89-6 52.9 ug/L 5.0 1 03/19/20 01:06 03/20/20 17:48 7439-96-5 25100 ug/L 5000 1 03/19/20 01:06 03/21/20 14:31 7440-23-5 Analytical Method: SM 254OC-2011 92.0 mg/L 25.0 1 0311812015:46 Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 NO CFU/100 mL 1.0 1 03/16/20 17:39 03/17/20 17:24 Analytical Method: EPA 350.1 Rev 2.0 1993 ND mg/L 0.10 1 0312612011:08 7664-41-7 Analytical Method: EPA 353.2 Rev 2.0 1993 4.0 mg/L 0.040 1 03/1712016:30 14797-55-8 NO mg/L 0.040 1 03/17/20 16:30 14797-65-0 Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 NO mg/L 0.050 1 03/18/2015:22 03/18/2020:38 7723-14-0 Analytical Method: SM 4500-CI-E-2011 37.3 mg/L 1.0 1 03/1712011:60 16887-00-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L-C. Page 7 of 25 Document Name. Document Revised: February 7, 2018 b- Sample Condition Upon Receipt(SCUR Page Iof 2 aGeAnalYtiCat Document No.; issuing Authority; F-CAR•CS•031 Rev.06. Pace Carolinas Quality Office Laboratory receiving sa les: Asheville) Eden Greenwood,❑ Nuntersville[] Raleigh[] MechanicsvilleE] Client Name: .. WO# ich1 py t Project $ (924698 Courier: []Fe Ex E]UPS ❑USPS QCRent 1111111111111111111111 [] Commercial ace pother; 824868 1 Custody Seal Present? Dyes -No Seals intact? (]Yes "J!iNo Contents; pate/Initiais Person Examining Packing Material: ❑Bubble Wrap. QBubbie Bags Jaflona other Biological Tissue Fro n? Thermometer; A�y—I^ []Yes QNp /A. R Gun ID: yl `r I � ' TYDe oface: Wet ORlue []None Cooler 7emp(`C): _��Correct(on Factors-Add/Subtract. (°C) Temp should be above freezing to..6°C Cooler Temp Corrected(°C): _I . sr - OSainpies outoftemp criteria. Samples on ice;: cooling;process has begun USDA Regulated Soil ( N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, ::-_i..n��u.... i..il-n 0,... nRifn171 IYPS nNo `Yes LjNo. �n.,.... .._.._.._.- . — CommentsJDigcrepancy: Chain of Custody Present? es. []No N/A 1. ,_.. Samples Arrived within. Hold Time? Yes No N(A 2, Short Hold Time Ana lysis(472 hr.)? es No QN/A. 3• Rush Turn Around Time Requested? Dyes QNJA 4. Sufficient Volume? s. No N/A 5. Correct Containers. Used? -Pace Containers Used? Yes Yes QNo QN. QN/A N/A 6. Containers Intact? E3es [IN. Q N/A 7. Dissolved analysis: Samples Field.Fittered? oyss [:]No FN/A. 8, Sample: Labels Match COC? -Includes Date/Time/W/Analysis. Matrix:.. Headspace in VOA Vials(>"mm)? Trig Blank Present? Tri' Blank Custody Seals Present? es: r Byes QYes ❑Yes. QNo 1 No o. No ❑NIA WA CIN/A A 9. 10, 11. '. COMMENTS/SAMPLE DISCREPANCY Field Data Required? E]Yes'JTNo Person contacted: Date/Time:. Project: Manager SCURF Review: ./ Project Manager SRF Review, Date::,[f x Date: It 2 Ar' Page 16 of 25 Document Name: Document Revlsed: February 7,2018 t�CCAflaIyhG$I Sample Condition Upon Receipt(SCUR) Pace 1 of 2 - Document No.: Issuing Authority: F-CAR-CS-033•Rev06 Pace: Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions' VOA, Coliform, TOC, Oliand Grease,. DRO/8015(water) OOC, LLHg **Bottom half of box is to list number of bottle Project WO# : 92469871 Fiji: CD3 Due Date: 03/27/200 CLIENT: 93-RPB uEt m m o m �E $ �� J E N �- E as ZE m J E al a m 1 E in n a 9 -Q v a L ¢ E En n ¢ `u E ¢ J E O iiQ. Q pzj'> E A l- T `t E Ory as Q Z a $ .A E rJ x Q J E 4l ° as °> j 'm -.M R J E " 2 J E O h y E N m -1 E per¢^ G 2 J. E N XZZ C D. E. g 1 2 3 t 4 5 s - 7 s 9 10 11 1? pH Adjustment Log for Preserved Samples Sample to Type orPreservadve " pH upon receipt Date preservation adjusted Time presentation adjusted Amount of Preservative. :added Lot If note: wnenevercnereIsaOlscrepancyanecting North Carpnria compliance samples, aCOPY -0t tmstnin will aetentto Me NouhCarollna DEHNR Certification office(i.e. Out of hold, Incorrect presentative, out of temp, Incorrect containers. -- - Page 17 Of 25 N N O CHAIN -OF -CUSTODY / Analytical Request Document .-� The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be WMPleted OWUMttly_ rn m a Se.OonA Secliun aSS C