WQ0012346_Residual Annual Report 2019_20200303

fIFr,f
MAR I
DWR
O FOR"TION
CLASS "A" WASTEWATER RESIVC,"tA, *_01DWR
ANNUAL APPLICATION [JAR _ 3 2020
REPORT YEAR 2019 Non -Discharge
UNITED STATES
MARINE CORPS BASE
CAMP LEJEUNE, N. C.
PERMIT NO. WQ0012346

2019
ANNUAL REPORT ON
DISTRIBUTION OF CLASS "A"
WASTEWATER RESIDUALS
MARINE CORPS BASE
CAMP LEJEUNE
PERMIT NO. WQ0012346

2019 ANNUAL REPORT ON
DISTRIBUTION OF CLASS A
WASTEWATER RESIDUALS
MARINE CORPS BASE, CAMP LEJEUNE
PERMIT NO. WQ0012346
• Cover Letter..................................................................... SECTION 1
• Class A Annual Distribution and Marketing/Surface Disposal SECTION 2
Certification and Summary Form (Form DMSDF)........................
• Annual Residuals Sampling Summary Forms SECTION 3
(Forms RSSF & RSSF-B)......................................................
• Residuals Analysis Lab Sheets ................................................ SECTION 4
• TCLP Lab Sheets............................................................... SECTION 5
• Annual Pathogen & Vector Attraction Reduction Forms SECTION 6
(Form PVRF 503)............................................................
• Pathogen & Vector Attraction Reduction Lab Sheets/Records........... SECTION 7

.n
h6a ;

SECTION 1
Cover Letter

�p1T Op
tf� SrArCS of
UNITED STATES MARINE CORPS
MARINE CORPS INSTALLATIONS EAST —MARINE CORPS BASE
PSC BOX 20005
CAMP LEJEUNE NC 28542-0005
5090.20.1
G-F/EMD
FEB 2 6 2020
Mr. Nathaniel Thornburg
North Carolina Department of
Environmental Quality
Division of Water Resources
Non -Discharge Permitting Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Dear Mr. Thornburg:
In accordance with requirements of 40 CFR Part 503, the enclosure
forwards Marine Corps Base Camp Lejeune's (MCB CAMLEJ) Class "A"
Wastewater Residuals Annual Application Report for the Year 2019.
The following explanation is provided per instruction in the Class
"A" Annual Distribution and Marketing/Surface Disposal Certification
and Summary Form (DMSDF) and the Annual Pathogen and Vector Attraction
Reduction Form (PVRF 503 Rules).
For your awareness, our CROM tank was out of service for the
majority of the year. Bench scale samples were not collected during
the first three quarters of 2019 while it was out of service.
Operators have since been instructed that bench scale samples must be
collected even when the CROM tank is out of service. ATAD Sludge
Solids Analyses, which also estimate percent solids removal, were
however performed during this time. Treated solids were stored on -
site to the maximum extent possible. Due to limited storage capacity,
some solids were land applied, and some were belt -pressed and used as
soil conditioner for daily cover at the Base landfill. Fecal analyses
and time and temperature requirements were met prior to this land
application. NCDEQ was notified of the CROM tank maintenance and use
of residuals at the Base landfill accordingly.
You may direct any questions to Mr. Travis Voorhees, Environmental
Quality Branch, Environmental Management Division, at [phone].
Sincerely,
AC rxtn,�
t hn R. Townson
Director, Environmental Management
by direction
of the commanding general
Enclosure: MCB CAMLEJ's Class "A" Wastewater Residuals Annual
Application Report Year 2019 (3 copies)

SECTION 2
Class A Distribution & Marketing/Surface
Disposal Certification &Summary Form
(Form DMSDF)

Reporting Period 2019
CLASS A ANNUAL DISTRIBUTION AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT M: WQW12346 FACILITY NAME: Camp Lejeune AWWTP
PHONE M: [phone] COUNTY: Onskrw OPERATOR:
FACILITY TYPE (please check one): Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C):
Distribution and Marketing (complete Parts A, 6, Cl
Was the facility in operation during the past calendar year? Yes QQ No ❑ -cif No skip parts A, e,C and certify form below
Part A
Part B
Month
Source(s) (include NPDES
M if applicable)
V
ume (dry tons
Recipient Information
en men
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended uses)
January
Camp Lejeune AWWTP NCW63029
34.4
February
Camp Lejeune AWWTP NC0063fl29
7.7
March
Camp Lejeune AWWTP NC0063029
27.2
April
Camp Lejeune AWWTP N00063029
81.7
May
Camp Lejeune AWWTP NC0063029
57.3
June
Camp Lejeune AWWTP NCDO63029
11.6
July
Camp Lejeune AWWTP NC0063029
2.3
August
Camp Lejeune AWWTP NCDG63029
23.9
September
Camp Lejeune AWWTP NCDD63029
28.5
October
Camp Lejeune AWWTP NCO063029
39.8
November
Camp Lejeune AWWTP NCDO63029
10.8
December
Camp Lejeune AWWTP NCDo63029
2LB
Total from FORM DM5L1F (sup)
0.0
Totals Annual (dry tons):
354.6
Amendment(s) used:1 8uiking Agent(s) used:
if more space Is required,Mich additionaln ormat on sheets supp of Nu r of Form DMSDF (Supp)
nor t t..
Facility was compliant during the past calendar year with all conditions of land application permit �_) Yes
(Including but not limited to Items 1-3 below) issued by the Division of Water Quality: No - > H No, explain in Narrative
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laborator results are attached.
2. All operation and maintenance requirements were compiled with or, In the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information Is, to the best of my knowledge and beWef, true, accurate and complete. I am aware that there are significant penalties for
submitting false inf Ion, Including the possibility of fines and imprisonment for knowing viol
5 n ure of Permittee D e SJ ure of Pre '• Date
Herent from Permittee)
•'Preparer Is defined In 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) DENR FORM DMSOF (12/2006)

LoadDate
LoadTime VehiclelD
Sludge
8/29/2019
11:13
16.50
8/30/2019
11:16
13.92
9/3/2019
11:18
14.29
9/4/2019
11:19
25.86
9/10/2019
11:20
15.31
9/11/2019
11:20
13.78
9/12/2019
11:21
15.28
9/13/2019
11:22
15.07
9/17/2019
11:22
14.22
9/18/2019
11:23
29.82
9/19/2019
11:23
15.87
9/20/2019
11:24
15.72
9/23/2019
11:25
15.55
9/24/2019
11:25
14.35
9/25/2019
11:26
14.83
9/26/2019
11:27
15.99
9/27/2019
11:27
15.99
9/30/2019
11:28
15.12
10/1/2019
11:28
34.12
10/2/2019
11:29
16.20
10/3/2019
11:30
14.06
10/11/2019
11:31
15.63
10/21/2019
11:31
16.13
10/22/2019
11:32
34.77
10/23/2019
12:11
33.50
10/24/2019
12:14
15.37
10/25/2019
12:35
33.25
10/28/2019
12:36
16.28
10/29/2019
12:37
33.51
Wednesday, February 5, 2020 Page -I of 2

'_oadDate
LoadTime VehiclelD
Sludge
0/30/2019
12:37
15.87
_1/5/2019
12:39
12.38
11/5/2019
12:40
12.38
11/6/2019
12:39
34.7_
11/7/2019
12:40
33.15
11/8/2019
12:40
34.57
11/12/2019
12:41
35.88
11/13/2019
12:42
33.61
11/14/2019
12:43
18.07
11/18/2019
12:43
33.22
11/19/2019
12:45
34.13
11/20/2019
12:45
35.03
12/3/2019
12:46
36.47
12/4/2019
12:47
36.15
12/5/2019
12:47
34.65
12/6/2019
12:50
17.13
12/9/2019
12:48
34.93
12/9/2019
12:49
35.91
12/11/2019
12:51
35.33
12/12/2019
12:51
33.98
12/16/2019
12:52
16.19
12/17/2019
12:52
16.31
12/18/2019
12:53
16.61
12/19/2019
12:53
16.87
12/20/2019
12:54
16.25
12/30/2019
12:54
16.48
12/31/2019
12:55
16.27
Total Sludge
1,272.86 Tons
Wednesday, February 5, 2020 Page 2 of 2

BIODYNAMIC VOLATILITY ENHANCEMENT LOG
WT-310CS SWEET CANE SYRUP
(SUGAR WATER)
Date sweet cane syrup added Train 1 Reactor A ! Igallons
Train 1 Reactor B
Igallons
Thursday, January 17, 2019 Train 2 Reactor A 137 gallons
jTrain 2 Reactor B 137
Igallons
Train 3 Reactor A gallons
�Train 3 Reactor B
gallons
jTrain 4 Reactor A all
!Train 4 Reactor B
jgal s
Date sweet cane syrup added ITrain 1 Reactor A
gallons
rain 1 Reactor B :
allons
Thursday, January 17, 2019 rain 2 Reactor A 137.5
gallons
rain 2 Reactor B 137.5
i Ilons
—
(Train 3 Reactor A
-
gallons
- -- _
Tr is n 3 Reactor B �—
j allons
rain 4 Reactor A--!----
;gallons j
;Train 4 Reactor B
;gallons
Date sweet cane syrup added (Train 1 Reactor A
137 gallons I
ITrain 1 Reactor B
Igallons
Tuesday, February a rY 19, 2019 Train 2 Reactor A
gallons
rain 2 Reactor B
137 gallons
rain 3 Reactor A
gallons
Train 3 Reactor B
!gallons i
Train 4 Reactor A
gallons
Train 4 Reactor B
gallons
Date sweet cane syrup added rain 1 Reactor A 137.5 (gallons
rain 1 Reactor B
137.5 gallons
--
Tuesday, February 19, 2019 rain 2 Reactor A gallons
rain 2 Reactor B
melons J
Traln 3 Reactor A allons
rain 3 Reactor B
allons
Train 4 Reactor A gallons
Train 4 Reactor B
_
igallons
Date sweet cane syrup added Train 1 Reactor A !gallons
Train 1 Reactor B
gallons
Tuesday, July 30, 2019 — -lTrain 2 Reactor A gallons
rain 2 Reactor B 275
gallons
Train 3 Reactor A gallons
[Train 3 Reactor B
--
gallons
rain 4 Reactor A gallons
rain 4 Reactor B
gallons
Date sweet cane syrup added !Train 1 Reactor A gallons
rain 1 Reactor B !
allons
Tuesday, - 201
July 30, Z019 Train 2 Reactor A gallons
g
Train 2 Reactor B
550 allons
g
-_ _ _
rain 3 Reactor A gallons
rain 3 Reactor B
--
_jillons
rain 4 Reactor A gallons
ITrain 4 Reactor B
— ! allons
Date sweet cane syrup added ITrain 1 Reactor A 275
Igallons Train 1 Reactor B _
gallons
Thursday, August 1, 2019 Train 2 Reactor A
_gallons Train 2 Reactor B
gallons
!Train 3 Reactor A
;gallons Train 3 Reactor B !
gallons
_
(Train 4 Reactor A
gallons Train 4 Reactor B
gall no s
Wednesday, February 5, 2020 Page 1 of 2

BIODYNAMIC VOLATILITY ENHANCEMENT LOG
WT-310CS SWEET CANE SYRUP
(SUGAR WATER)
sweet cane syrup added Train 1 Reactor A 275 'gallons Train 1 Reactor B ! ;gallons
Ada, August 1, 2019 i Y _8 _ ]Train 2 Reactor A gallons Train 2 Reactor B .Igallons
!Train 3 Reactor A gallons Train 3 Reactor B Igallons
JTrain 4 Reactor A gallons Train 4 Reactor B ! 'gallons
sweet cane syrup added (Train 1 Reactor A
;gallons
tesday, August 7, 2019Train 2 Reactor A 275gallons
!Train 3 Reactor A
Igallons
Train 4 Reactor A
Igallons
(Train 1 Reactor B
igallons
_
�rain 2 Reactor B
gallons
Train 3 Reactor B
Igallons
JTrain 4 Reactor B
Igallons
ate sweet cane syrup added ,Train 1 Reactor A
gallons
rain 1 Reactor B
gallons
onda ,November 18, 2019 - Tram 2 Reactor A
X__ � 137
gallons
` Train 2 Reactor B
137 gallons
Ifrain 3 Reactor A
gallons
�rain 3 Reactor B
gallons
Tram 4 Reactor A !,--
gallons
Train 4 Reactor B
-„
'gall I s
Date sweet cane syrup addedJTrain 1 Reactor A
Igallons Train 1 Reactor B
gallons
Wednesday, December 4, 2019 JTrain 2 Reactor A
137 gallons Train 2 Reactor B
137 gallons
,Train 3 Reactor A
igallons !Train 3 Reactor B
gallons
:Train 4 Reactor A
gall Ions ;Train 4 Reactor B
1 gallons
Wednesday, February 5, 2020 Page 2 of 2

SECTION 3
Annual Residuals Sampling Summary Forms
(Forms RSSF & RSSF-B)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please not that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - 8
WQ Permit Number: WQW12346
Facility Name: Camp Lejeune A1IVWTP
Residual Source WQ H
or NPOE5 #: NCO063029
WWTP Name: Camp Lejeune AWWTP
Residual Analysis Data
Laboratory: 1) EMD, ELS
2) Environmental Chemists
3)
4)
5)
Parameter
(rng/kg)
Ceiling Conc.
Limit(mg/kg)
Sample or Composite Date
2/23/2029
4/9/2019
7/9/2019
10/22/2029
Percent Solids %
NA
3.39
3.2
3.04
3.41
Arsenic
75
28.3
12
11.6
14.7
Cadmium
85
< is
< 10.8
< 9.9
< 5.63
Copper
4,300
322
338
305
349
Chromium
NA
30.1
22.7
20.5
28.7
Lead
840
< 15
16.6
17.3
17.4
Mercury
57
< 0.649
< 0.563
< 0.724
< 0.499
Molybdenum
75
< 15
< 10.8
< 9.9
8.39
Nickel
420
24
18.2
17.2
19.7
Selenium
100
< 15
< 10.8
< 9.9
< 5.63
Zinc
7,500
1300
1440
1470
1500
Total Phosphorus
NA
SS900
2010
49800
40900
TKN
NA
85400
60200
45800
52000
Ammonia -Nitrogen
NA
28800
26200
27000
25000
Nitrate and Nitrite
NA
6.72
223
238
Z4.2
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel
properly gathered and evaluated the information submitte m awar that there are significant penalties for submitting false information, including the possibility of fines
and imprisonment for knowing violations." ,'1
Charles Jo
Signature of Preparers J�jr
•Preparer is defined in 40 CFR Part 5t�3and 15A NCAC 2T .1102 (26)
2/20/2020
Date
DEM FORM SSF (1212006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please not that your permit may contain additional parameters to be analyzed. The parameters can be reported In FORM RSSF - 8
WQ Permit Number: WQ0012346
Facility Name: Camp Lejeune AWWTP
Residual Source WQ #
or NPDES #: NCO063029
WWTP Name: Camp Lejeune AWWTP
Residual Analvsis Data
Laboratory: 1) EMD, ELS
2)Environmental Chemists
3)
4)
5)
Parameter
(mg/kg)
Ceiling Conc.
Limit{mg/kg)
Sample or Composite Date
1/23/2029
4/9/2019
7/9/2019
20/22/2019
SAR
NA
2.84
0.63
3.17
0.94
Aluminum
NA
71200
48500
54400
72000
Calcium
NA
56500
49300
99500
S5800
Magnesium
NA
3540
4880
4930
3810
Sodium
NA
2580
3090
3780
4600
pH
NA
7.55
8.73
8.85
7.61
Plant Available
Nitrogen
NA
31300
235001
19400
20600
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel
properly gathered and evaluated the i cgtation submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines
and imprisonment for kgow v ations,
Date
defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DEM FORM SSF (12/2006)

SECTION 4
Residuals Analysis Lab Sheets

0

r
... .......li
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Alberta Y. Okamoto
Environmental Chemists, Inc®
6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab e 910.392.4424 Fax
710 8owsertawn Road Manteo NC 27954 a 252.473.5702 7 3 02 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e. 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Feb 18, 2019
Customer PO #:
Customer ID: 12060026
Report #: 2019-01306
Project ID: Camp Lejeune MCB
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-03346 Site: CROM Tank 1/23/2019 7:14 AM Solid/Sludge Acosta Julius
Test Method Results Date Analyzed
PAN 30% Mineralization rate used. Calculation 31300 mg/kg 02/15/2019
SAR
Calculation
2.84
02/11 /2019
Nitrate Nitrogen (talc)
Nitrite Nitrogen
EPA353.2
29.9mg/kg
01/29/2019
Nitrate Nitrogen
Subtraction Method
<0.59mg/kg
02/15/2019
Sludge Residuals
Aluminum
EPA 200.7
71200mg/kg
02/01/2019
Arsenic
EPA200.7
18.3mg/kg
01/30/2019
Cadmium
EPA 200.7
<15.0mg1kg
01/28/2019
Calcium
EPA 200.7
56500 mg/kg
02/02/2019
Chromium
EPA200.7
30.1 mg/kg
01/28/2019
Copper
EPA 200.7
322mg/kg
01/28/2019
Lead
EPA 200,7
<15.0 mg/kg
01/28/2019
Magnesium
EPA 200.7
3540 mg/kg
02/02/2019
Molybdenum
EPA 200.7
<15.0 mg/kg
01/30/2019
Nickel
EPA 200.7
24.0mg/kg
01/28/2019
Potassium
EPA 200 7
4010 mg/kg
02/02/2019
Selenium
EPA 200.7
<15.0mg/kg
01/28/2019
Sodium
EPA 2007
2580 mg/kg
02/02/2019
Zinc
EPA 200.7
1300 mg/kg
01/28/2019
Total Kjeldahl Nitrogen (TKN)
EPA351.2
85400mg/kg
02/05/2019
Nitrate+Nitrite-Nitrogen
EPA353.2
6.72mg/kg
02/13/2019
Total Solids (%)
SM 2540 B
3.39 %
01/24/2019
pH
SM 4500 H B
7.55 units
02/04/2019
Ammonia Nitrogen
SM 4500 NH3 C
28800 mg/kg
02/14/2019
Report #:: 2019-01306 Page 1 of 2

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
USMC Camp Lejeune Date of Report: Feb 18, 2019
G-F/EMD/ECB -12 Post Lane Customer PO #:
Camp Lejeune NC 28547 Customer ID: 12060026
Attention: Alberta Y. Okamoto Report #: 2019-01306
Project ID: Camp Lejeune MCB
Total Phosphorus sM 4500 P F 55900 mg/kg 02/06/2019
Mercury sw6467471B <0.649mg/kg 01/26/2019
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: -�GA�} , v-)
Report #:: 2019-01306 Page 2 of 2

ENVIRONMENTAL CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 26405
OFFICE: 910392-0223 FAX [phone]
[e-mail]
CLIENT: Commanding General
PROJECT NAME: Camp Lejeune MCB
REPORT NO:
ADDRESS: G-F/EMD/EQB/Environmental Lab
CONTACTNAME: Alberta Y. Okamoto
PO NO:
12 Post Lane
REPORTTO: Lauren Acosta
PHONFJFAX: 910-451-0020 (fax) 910-451-7195
Camp Le'eune NC 28547
COPY TO:
albena Okamoto@usmc MI. mben a Iv J r0usmc mil,
email: laarenaaosta usmcmli
Sampled By: ,4 cn S r.L _ t ,,—L SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
m
E F
a
m
E` o`
o
r,
_
o
a
0
s
m s
g°
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
i
o
d
s
o
°�
o
;
a
s
€
¢
i`
CROM TANK
t 7
v ' `
SLUDGE
C
P)
3'f
X
Aluminum, Arsenic, Cadmium, Chromium,
Copper, Lead, Magnesium, Molybdenum,
i G ,
P
Nickel, Potassium, Sodium, Selenium, Zinc,
Mercury, Sludge, Nitrite, Nitrate,
G
G
C
P
Nitrate -Nitrite, TKN, Total Solids/Soils &
Sludge, Ammonia, Total Phosphorus,
G
G
C
P
Calcium, SAR, PAN
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Daterrome
Received By:
Date/Time
0��2
2.
��.0 ��
(. 3 v bra 3
-----
, z , . (� 12 3.
Temperature when Received: v Accepted:
Delivered By:A,; ")L a- I,!; ,,s T.L Received

Marine Corps Installations East - Marine Carps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
12 Post Lane, Camp Lejeune, NC 28547
Client: FC Wastewater Date of Report: Feb 20, 2019
Date Collected: Jan 23, 2019 Report No.: 01232019
Date Received: Jan 23, 2019 Lab ID: 227
Sample: Quarterly Sludge
Analyte
Results
Units
pate
Tech
Method
Analyzed
t Solids
3.25
t
1/25/19
DES
SM 2540 G
PH
7.56
SU
1/23/19
DRS
SM 4500 H•B
FFecal
Coliforms
34.6
MPN/gram
1/23/19
DES
SM 9221 C E
Certified By:
LAUREN D. ACOSTA

Chain of Custody Record
CLIENT: Commanding General
G-F/EMD/EQB/Environmental Laboratory
12 Post Lane
Camp Lejeune, NC 28547
Attn: Alberta Y. Okamoto
(910) 451 - 0020
Collected by:
J
Signature:
Date Collected:
1 • Z3 . t Ci
Time Collected:
0"71'3
Location of sample:
Truck Loading Station
Comp/Grab:
Grab
Number of Containers:
2
Analyses Requested:
% Solids, pH '
Report all results as mglkg dry wt.
Was sample dechlorinated?
We
Preservation:
Ice
Regulatory Sample:
1
Yes
Comments:
-1 • S(rr
Relinquished by:
Date
Time
Received by:
Date
Time
Art 06 1-74
1. 23.19
b91S
P:�ftT
'b . S.k u t_s (At
p
w

CAMP LEJEUNE WWTP
pH READINGS FOR QUARTERLY SLUDGE SAMPLING
COLLECTED BY: RECEIVED BY:
DATE COLLECTED: 1 2 s (q DATE RECEIVED: Z 7a I GI
TIME COLLECTED: O i 3 TIME RECEIVED: 0 "1 i s
ANALYZED BY:
---� _
TIME:
DATE:
METHOD:
4500H+ B - 2011
TIME
TIME
VOLUME
TEMP
PH
SAMPLE
COLLECTED
ANALYZED
(mLs)
(°C)
(SU)
CALIBRATION
'
BUFFER 4.00
60
CALIBRATION
BUFFER 10.00
60
CHECK BUFFER 7.00
0-1 ��
-1 Z. C,
60
IRWIN MR,
CROM TANK
100
((.p . S
-"7 SCU
CROM TANK DUP
�k
100
CHECK BUFFER 7.00
60
Nn'r frNAL-1-46a
U- 2.2.0, 11
FORM UPDATED: JANUARY 2019 CHECKED BY:

DIF',

Environmental Chemists, Inc.
envirochem j6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax
L IF 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
sM; 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infar environmentalchemists.com
USMC Camp Lejeune
Date of Report: Apr 29, 2019
G-F/EMD/ECB -12 Post Lane
Customer PO #:
Camp Lejeune NC 28547
Customer ID: 12060026
Attention: Alberta Y. Okamoto
Report #: 2019-05840
Project ID: T2B
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-14679 Site: T26
4/9/2019 7:45 AM Solid/Sludge Williams
Test
Method
Results
Date Analyzed
PAN
calcination
23500 mg/kg
04/29/2019
Used 30%Mineralization Rate.
SAR
calculation
0.630
04/29/2019
Nitrate Nitrogen (calc)
Nitrite Nitrogen
EPA 353.2
129 mg/kg
04/24/2019
Nitrate Nitrogen
Subtraction Method
84.4 mg/kg
04/29/2019
Sludge Residuals
Aluminum
EPA 200.7
48500 mg/kg
04/15/2019
Arsenic
EPA 200.7
12.0 mg/kg
04/15/2019
Cadmium
EPA 200.7
<10.8mg/kg
04/15/2019
Calcium
EPA 2001
49300 mg/kg
04/15/2019
Chromium
EPA 200 7
22.7 mg/kg
04/15/2019
Copper
EPA 200.7
338 mg/kg
04/15/2019
Lead
EPA 2003
16.6 mg/kg
04/15/2019
Magnesium
EPA 2007
4880 mg/kg
04/15/2019
Molybdenum
EPA 2007
<10.8mg/kg
04/15/2019
Nickel
EPA 200.7
18.2 mg/kg
04/15/2019
Potassium
EPA 200.7
6410mg/kg
04/16/2019
Selenium
EPA 200.7
<10.8 mg/kg
04/15/2019
Sodium
EPA 200.7
3090 mg/kg
04/16/2019
Zinc
EPA 2001
1440 mg/kg
04/15/2019
Nitrate+Nitrite-Nitrogen
EPA 353.2
213 mg/kg
04/24/2019
Total Solids (%)
SM 2540 B
3.20 %
04/11 /2019
pH
SM4500 H B
8.73 units
04/15/2019
Ammonia Nitrogen
SM4500 NH3 C
26200 mg/kg
04/16/2019
Total Kjeldahl Nitrogen (TKN)
SM 4500 org B
60200 mg/kg
04/15/2019

F-77701 - _71
i 1i
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Alberta Y. Okamoto
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(T-environmen talchemists.com
Date of Report: Apr 29, 2019
Customer PO #:
Customer ID: 12060026
Report #: 2019-05840
Project ID: T213
Total Phosphorus SM 4500 P F 2010 mg/kg 04/26/2019
Mercury Sw8467471B <0.563mg/kg 04/12/2019
Comment: Results reported on a dry weight basis.
Reviewed by:

• ENVIRONMENTAL CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
CLIENT: Commandina General
PROJECT NAME: Camp Lejeune MCB
REPORT NO:
ADDRESS: G-F/EMD/EQB/Environmental Laboratory
CONTACT NAME: Alberta Y. Okamoto
PO NO:
12 Post Lane
REPORT TO: Patricia H. Raper....
PHONE/FAX: [phone] (fax) 910-451-7195
Camp Lejeune NC 28547
COPY TO:
patricia raperCEDusmc. milalbenaokamoto@usmc. mil.
email: rcbert a lowder@usmcmil lauren acosta usmc mil
Sampled Bv: _ W 1 L-r-1 A ^nS SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
~
Y
ci a
v
x
g z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
=
v
o
=
o
_
o
W
o
-IT
SLUDGE
C
P
X
kluminum, Arsenic, Cadmiu
G
G
C
P
,
agnesium, Molybdenum,
G
G
C
P
ickel, Potassium, Sodium,
�elenium, Zinc,
G
G
C
P
ercury Sludge, Nitrite,
G—T
G
C
P
KN, Total Solids/Soils &
G
G
G
P
hosphorus, Calcium, SAR
G
G
C
P
PAO
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Timq
Received By:
Date/Time
2.
r
1i mot`
16 i r 0-7
Temperature when Received: �,�_ Accepted: Reji�d` ! J Resample Requested: 41
Delivered By: Received By: �Date: �"C� 'i�l Time: c
Comments: -I- ___ __ TURNAROUND: _ __ _ __

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
12 Post Lane, Camp Lejeune, NC 28547
Client:
Date Collected:
Date Received:
Sample:
FC Wastewater
Apr 9, 2019
Apr 9, 2019
Quarterly Sludge
Date of Report: Apr 30, 2019
Report No.: 04092019 T2B
Lab ID: 227
Analyte
Results
Units
Date
Method
Analyzed By
Analyzed
Solids
3.35
4/12/19
SM 2540 G
ELS
PH
8.16
SU
4/9/19
SM 4500 H•B
ELS
Fecal
Coliforms
1.82
MPN/gram
4/9/19
SM 9221 C E
ELS
Nitrate
Nitrogen
See Attached
Envirochem
Sludge
Residuals
See Attached
Envirochem
Cert' ' d By:
UREN D. ACOSTA

Chain of Custody Record
CLIENT: Commanding General
G-F/EMD/EQB/Environmental Laboratory
12 Post Lane
Camp Lejeune, NC 28547
Attn: Alberta Y. Okamoto
(910) 451 - 0020
Collected by:
Lu�ttt//Af
Signature:
/
t ' c{r, fir, ! �r
Date Collected:
�/ i• !Q
Time Collected:
07,1S
Location of sample:
OWN
Comp/Grab:
Grab
Number of Containers:
2
Analyses Requested:
% Solids, pH
Report all results as mg /k dry W.
Was sample dechlorinated9
n/a
Preservation:
Ice
Regulatory Sample:_
Yes
Field
Comments:
Relinquished by:
Date
Time
Received by-.
Date
Time
� Cam" �--•-
`� - `�' • `1
l�7

CAMP LEJEUNE WWTP
pH READINGS FOR QUARTERLY SLUDGE SAMPLING
COLLECTED
DATE COLLECTED: - TIME: 0 "7 BY:
DATE: TIME: n2.
ANALYZED BY: METHOD: 4500H+ B - 2 01r 2n l l
N 4. IS -II
SAMPLE
TIME
COLLECTED
TIME
ANALYZED
VOLUME
mLs
TEMP
pH (SU)
RECOVERY
BUFFER 4.00
60
BUFFER 10.00
60
.G
CHECK BUFFER 7.00
60
% CJ
0 "7 S&
100
L48, 9I
Cr
-7 S `?
100
i-t 9 S
C --
CHECK BUFFER 7.00
60
FORM UPDATED: SEPTEMBER 2012 CHECKED BY:

sii
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab + 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab jFax
255-A Wilmington Highwav, Jacksonville, NC 28540 • 410.347.5843 Lab/Fax
info( environmentalchemists.com
USMC Camp Lejeune
Date of Report: Aug 02, 2019
G-F/EMD/ECB -12 Post Lane
Customer PO #:
Camp Lejeune NC 28547
Customer ID: 12060026
Attention: Alberta Y. Okamoto
Report #: 2019-11072
Project ID: Camp Lejeune MCB
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-28461 Site: Sludge
7/9/2019 7:35 AM Solid/Sludge Richard Williams
Test
Method
Results Date Analyzed
PAN Used 30% Mineralization Rate.
Calculation
19400 mg/kg
07/30/2019
SAR
Calculation
3.17
07/30/2019
Nitrate Nitrogen (calc)
Nitrite Nitrogen
EPA 353.2
215 mg/kg
07/12/2019
Analyzed outside of hold time.
Nitrate Nitrogen
Subtraction Method
23.1 mg/kg
07/25/2019
Sludge Residuals
Aluminum
EPA 200.7
54400 mg/kg
07/26/2019
Arsenic
EPA 200.7
11.6 mg/kg
07/24/2019
Cadmium
EPA200.7
<9.90 mg/kg
07/24/2019
Calcium
EPA 200.7
99500 mg/kg
07/25/2019
Chromium
EPA200.7
20.5 mg/kg
07/24/2019
Copper
EPA 200.7
305 mg/kg
07/24/2019
Lead
EPA 200 7
17.3 mg/kg
07/24/2019
Magnesium
EPA 200.7
4930 mg/kg
07/24/2019
Molybdenum
EPA 200 7
<9.90 mg/kg
07/24/2019
Nickel
EPA 200.7
17.2 mg/kg
07/24/2019
Potassium
EPA 200 7
6410 mg/kg
07/24/2019
Selenium
EPA 200.7
<9.90 mg/kg
07/24/2019
Sodium
EPA 200.7
3780 mg/kg
07/26/2019
Zinc
EPA 200.7
1470 mg/kg
07/24/2019
Nitrate+Nitrite-Nitrogen
EPA 353.2
238 mg/kg
07/23/2019
Total Solids (%)
SM 2540 B
3.04 %
07/10/2019
pH
SM 4500 H B
8.85 units
08101 /2019
Ammonia Nitrogen
SM 4500 NH3 C
27000 mg/kg
07/09/2019
Total Kjeldahl Nitrogen (TKN)
SM 4500 Org B
45800 mg/kg
07/13/2019

rge "n:':v ir o e h e m
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Alberta Y. Okamoto
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington 1-(ighway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
info(iecmvi ronmentalchem ists.com
Date of Report: Aug 02, 2019
Customer PO #:
Customer ID: 12060026
Report #: 2019-11072
Project ID: Camp Lejeune MCB
Total Phosphorus SM 4500 P F 49800 mg/kg 07/30/2019
Mercury SW84674718 <0.724mg/kg 07/11/2019
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: K' Cp0_ 13116J(Z

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
rrn I Pr-TI0N AND CHAIN OF CUSTODY
OVUG rvinurnui vvay vnnnrnywn, 11 . 4va
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
CLIENT:
PROJECT NAME: Camn Leieune MCB
REPORT NO:
ADDRESS: G-F/EMD/EQB/Environ mental Laboratory
CONTACT NAME: Alberta
PO NO:
12 Pnst Lane
REPORT TO: Lauren Acosta
PHONE/FAX: [phone] fax[phone]
COPY TO:
email: [e-mail], lauren.acosta@usm
a n A Wir C- r (,,AMPI F TYPE I = Influent E = Effluent W = Well. ST = Stream, SO = Soil, SL = Sludge, Other:
aaur FIVU v i-r
Sample Identification
Collection
a
E a
~
)
m p
ao
c
a _
c U
`o
° a
"
v
o W
m
g z
PRESERVATION
AN REQUESTED
Date
Time
Tern p
z
z
0
0
0
g
°
7 9 /y
CJ73
LUD
E C
P
X'�
X
luminum, Arsenic, Cadmi
G
G
C
P
agnesium, Molybdenum,
G
G
C
P
NicKei, Potassium, o iu
elenium, Zinc,
G
G
C
p
4ercury Sludge, Nitrite,
Fitrate.-
G
G
C
P
FKN, Total Solids/Soils
G
G
C
P
'
Phosphorus, Calcium, SAR
G
G
C
P
PAN
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
. (CPAW u l^
c)7
Refri erator
1 `i I I i V 7 S'"
2.
Refrigerator
-1 � R (9 l c45
`x� �
a Cc
Temperature when Received: Accepted:
Delivered By: Received By:
Comments:
Kesample Requested:
_Date: Time: %5 _
TURNAROUND:
� C7 ��

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
12 Post Lane, Camp Lejeune, NC 28547
Client
Date Collected:
Date Received:
Sample:
FC Wastewater
Jul 9, 2019
Jul 9, 2019
Quarterly Sludge
Date of Report
Report No.:
Lab ID:
Aug 8, 2019
07092019 T2B
227
Analyte
Results
Units
Date
Method
Analyzed By
Analyzed
o Solids
3.98
%
7/9/19
SM 2540 G
ELS
pH
SU
SM 4500 H' B
Fecal
Coliforms
< 4.5
MPN/gram
7/9/19
SM 9221 C E
ELS
Nitrate
Nitrogen
See Attached
Envirochem
Sludge
Residuals
See Attached
Envirochem
* pH not analyzed
Certified By:
XURENID. ACOSTA

Environmental Chemists, Inc.
6602 IVindmill Way, Wilmington, NC 28405 • 910.392.0223 Lab * 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 279.54 • 252.473.5702 Lab/Fax
"F� 255-A Wilmington Highwav, Jacksonville, NC 28540 • 910.347.5943 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(a environmentalchenusts.com
USMC Camp Lejeune Date of Report: Nov 27, 2019
G-F/EMD/ECB -12 Post Lane Customer PO #:
Camp Lejeune NC 28547 Customer ID: 12060026
Attention: Alberta Y. Okamoto Report #: 2019-11887
Project ID: Camp Lejeune MCB
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
19-45610 Site: TIB 10/22/2019 Solid/Sludge Williams
Test Method Results Date Analyzed
PAN Used 30%Mineralization Rate. Calculation 20600 mg/kg 11/27/2019
SAR
Calculation
0.940
11 /2712019
Aluminum
EPA 2007
72000mg/kg
11/01/2019
Arsenic
EPA 200 7
14.7 mg/kg
10/28/2019
Cadmium
EPA 200.7
<5.63 mg/kg
10/28/2019
Calcium
EPA 200.7
55800 mg/kg
1012812019
Chromium
EPA 2007
28.7 mg/kg
10/28/2019
Copper
EPA 2007
349 mg/kg
10/28/2019
Lead
EPA 2007
17.4 mg/kg
10/28/2019
Magnesium
EPA 200.7
3810 mg/kg
10/30/2019
Molybdenum
EPA 200.7
8.39mg/kg
10/28/2019
Nickel
EPA 200.7
19.7 mg/kg
10/28/2019
Potassium
EPA 2007
4430 mg/kg
10/30/2019
Selenium
EPA 200.7
<5.63mg/kg
10/2812019
Sodium
EPA 200.7
4600 mg/kg
10/30/2019
Zinc
EPA 200.7
1500 mg/kg
10/28/2019
Total Solids (%)
SM 2540 B
3.41 %
11/27/2019
Ammonia Nitrogen
SM 4500 NH3 C
25000 mg/kg
11/04/2019
Total Kjeldahl Nitrogen (TKN)
SM 4500 Org B
52000 mg/kg
11/18/2019
Total Phosphorus
SM 4500 P F
40900 mg/kg
10/30/2019
Mercury
Sw6467471B
<0.499mg/kg
10/26/2019
Nitrate Nitrogen (calc)
Nitrite Nitrogen
EPA 353.2
15.4 mg/kq
10/24/2019
Nitrate+Nitrite-Nitrogen
EPA 353.2
24.2 mg/kg
10/24/2019
Nitrate Nitrogen
Subtraction Method
8.80 mg/kg
11/27/2019

envixoche m
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Alberta Y. Okamoto
Environmental Chemists, Inc.
6602 Windmill Way: V, lmington, NC 28-405 • 910.392.0,713 Lab • 910.392.4424 Fax
710 Bowsertown Road, klanteo, NC 27954 • 252.473.5702 Lab/Fax
255-AWilmingtcm Higliw. iv, Jacksonville, NC 28540 • 910.347S8=43 Lab /Fax
Comment: Results reported on a dry weight basis.
Reviewed by: —lLZ& JQa Q,A,
in ti���renvironmentaichemists.cam
Date of Report: Nov 27, 2019
Customer PO #:
Customer ID: 12060026
Report #: 2019-17887
Project ID: Camp Lejeune MCB

ENVIRONMENTAL CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION a 94 NCDHHS: DLS CERTIFICATION a 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NO 28405
OFFICE: 910-392-0223 FAX [phone]
I nfo@envi ronmentalchem ists.com
CLIENT: Gopgral
PROJECT NAME: Camp I-eiPune
REPORT NO: {
ADDRESS: G-F/EMD/EQB/Environmental Laboratory
CONTACT NAME: Alberta
PO NO:
12 Post
REPORT TO: Lauren Acosta
PHONE/FAX: [phone] (fax) -7
COPY TO:
email: alhena Okamoto@usmc mil, lauren.acosta@usmc n
Sampled By: iviby&in SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
E
N~
m
E `o
E
U
-
3 0
U 6
d
3
V
o W
m f
5 Z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
z
2
p^
-
2
x_o
~
O
LUD
E
p
I
{
luminum, Arsenic, Cadmiu
G��I
C
P
I
agnesium, Molybdenum,
G
G
C
P
e o assium, Sodium,
3elenium, Zinc,
G
G
C
P
4ercury Sludge, Nitrite,
G
G
a
doo
C
pe
G
P
G
TKN, Total Solids/Soils &
hosphorus, Calcium, SAR,
CAM
PAN
4--
'
C
P
1
G
G
---
C
P
G
G
C
P
I -
G
G
Transfer
Relinquished By:
Dateff
Received By:
Date/Time
1.
c eu s
0-zz--ly 3 0
Refrigerator
-z r ,a /075-a
2.
Refrigerator
/U• f Q�(�
temperature when Received: _Accepted: ✓' i Rojected: i Resample Requested:
Delivered By:_____ Received By:%,( �: _ ui Date: I l9 Time:
Comments:__ ___ _ _ ___ TURNAROUND:

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
12 Post Lane, Camp Lejeune, NC 28547
Client
Date Collected:
Date Received:
Sample
FC Wastewater
Oct 22, 2019
Oct 22, 2019
Quarterly Sludge
Date of Report
Report No.:
Lab ID:
Dec 2, 2019
10222019_TlB
227
Analyte
Results
Units
Date
Method
Analyzed By
Analyzed
% Solids
5.38
0
10/22/19
SM 2540 G
ELS
pH
7.61
SU
10/22/2019
SM 4500 H*B
ELS
Fecal
< 3.35
MPN/gram
10/22/19
SM 9221 C E
ELS
Coliforms
Nitrate
See Attached
Envirochem
Nitrogen
Sludge
See Attached
Envirochem
Residuals
Certi "ed By:
L PUREND.ACOSTA

Chain of Custody Record
CLIENT: Commanding General
G-t=/EMD/EW/Environmental Laboratory
12 Post Lane
Camp Lejeune, NC 28547
Attn: Alberta Y. Okamoto
(910) 451 - 0020
Collected by:
WI5
Signature -
f
Date Collected:
r e -1.2-- r q
Time Collected:
u 950
Location of sample:
Truck Loading Station
Com Grab:
Grab
Number of Containers:
2
Analyses Requested:
% Solids, pH '
Report all results as m dry wt.
Was sample dechlorinated?
n/a
Preservation:
Ice
Regulatory Sample:1
Yes
Relinquished by:
Date
Time
Received by:
Date
Time
tvIc.Unrw1
rd- z2 -lF
9
68OS

CAMP LEJEUNE WWTP
pH READINGS FOR QUARTERLY SLUDGE SAMPLING
COLLECTED
DATE COLLECTED: (0- 7- 2- -I j TIME: 0 756 BY: CrJiul Arm P
DATE:
ANALYZED BY:
ID_22 ?-0
METHOD:
TIME: 030(�-
4500H+ B - 2000
SAMPLE
TIME
COLLECTED
TIME
ANALYZED
VOLUME
mLs
TEMP
pH (SU)
RECOVERY
BUFFER 4.00
"
60.
BUFFER 10.00
60
700
CHEC RYFFER 7.00
60
( 0 -Ott
0145D
100
37.1
7 U�
t
DUP
O D 01
100
3P-�
CHECK BUFFER 7.00
<` :
0°j(?°v
60
�' I
FORM UPDATED: SEPTEMBER 2012 CHECKED BY:

SECTION 5
TCLP Analysis Lab Sheets

rx
enywochem
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Alberta Y. Okamoto
Lab ID Sample ID:
19-03348 Site: CROM Tank
Test
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
Method
[e-mail]
Revised Report:
Feb 10, 2020
Original Report Date: March 01, 2019
Report #:
2019-01308
Customer ID:
12060026
Project ID:
Crom Tank
Collect Date/Time Matrix Sampled by
1/23/2019 7:15 AM Solid/Sludge Acosta Julius
Results Date Analyzed
pH
SM 4500 H B
7.54 units
02/04/2019
Chlordane (TCLP)
SW 846 Method 8081B/3510
<0.02 mg/L
02/12/2019
Endrin (TCLP)
SW 846 Method 80818/3510
<0.0005 mg/L
02/12/2019
Heptachlor (TCLP)
SW 846 Method 80818/3510
<0.0005 mg/L
02/12/2019
Heptachlor epoxide (TCLP)
SW 846 Method 80818/3510
<0.0005 mg/L
02/12/2019
Lindane (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
02/12/2019
Methoxychlor (TCLP)
SW 846 Method 8081 B/3510
<0.0005 mg/L
02/12/2019
Toxaphene (TCLP)
SW 846 Method 8081B/3510
<0.05 mg/L
02/12/2019
Trichloroethylene (TCLP)
SW 846 method 826OB15030B
<0.01 mg/L
02/11/2019
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/07/2019
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/07/2019
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/07/2019
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/07/2019
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/07/2019
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/07/2019
Hexachlorobenzene (TCLP)
SW 846 method 827013510
<0.050 mg/L
02/07/2019
Hexachloroethane (TCLP)
SW 846 method 827013510
<0.050 mg/L
02/07/2019
m + p-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/07/2019
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/07/2019
o-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/07/2019
Pentachlorophenol (TCLP)
SW 846 method 8270/3610
<0.250 mg/L
02/07/2019
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/07/2019
2,4,5-TP (TCLP)
SW846 Method 8151A
<0.0003 mg/L
02/13/2019
2,4-D (TCLP)
SW846 Method 8151A
<0.0003 mg/L
02/13/2019
1, 1 -Dich loroethylene (TCLP)
Sws46 Method 8260/5030
<0.01 mg/L
02/11/2019
1,2-Dichloroethane (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
02/11/2019
Report #: 2019-01308
Page 1 of 2

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ` 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
USMC Camp Lejeune Revised Report: Feb 10, 2020
G-F/EMD/ECB -12 Post Lane Original Report Date: March 01, 2019
Camp Lejeune NC 28547 Report #: 2019-01308
Attention: Alberta Y. Okamoto Customer ID: 12060026
Project ID: Crom Tank
Benzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
02/11/2019
Carbon Tetrachloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
02/11/2019
Chlorobenzene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
02/11/2019
Chloroform (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
02/11/2019
Methyl ethyl ketone (TCLP)
SW846 Method 8260/5030
<0.05 mg/L
02/11/2019
Tetrachloroethylene (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
02/11/2019
Vinyl Chloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
02/11/2019
RCI
Cyanide
EPA 335.4
<0.05 mg/kg
02/05/2019
Sulfide
SM 4500 S o
5.08 mg/kg
02/13/2019
Ignitability
SW 846 method 1010
>180 °F
02/15/2019
TCLP Metals
Arsenic
EPA 200.7
<1.Omg/L
02/09/2019
Barium
EPA 200.7
<1.O mg/L
02/09/2019
Cadmium
EPA 200.7
<1.O mg/L
02/09/2019
Chromium
EPA 200.7
<1.0 mg/L
02/09/2019
Lead
EPA 2007
<1.0 mg/L
02/09/2019
Selenium
EPA 200.7
<1.O mg/L
02/09/2019
Silver
EPA 200.7
<1.0 mg/L
02/09/2019
Mercury
EPA 245.1
<0.0002 mg/L
02/07/2019
Comment:
Revised to add trichloroet ylene.
Reviewed by:
Report #:: 2019-01308 Page 2 of 2

ENVIRONMENTAL CHEMISTS, INC OFFICE 910-392-0223IFiAX910-3 2r4424
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environrnentalchemis;ts"com
Anilvliral R Consultina Chemists
COLLECTION AND CHAIN OF Gus I UUY
CLIENT: Commandina General
PROJECT NAME: Camp Lejeune MCB REPORT NO: -
ADDRESS: G-F/EMD/EQB/Environmental Lab CONTACT NAME: Alberta Y. Okamoto PO NO:
12 Post Lane REPORT TO: Lauren Acosta PHONEIFAX: 910-451-0020 (fax) 910-451-7195
air,WIR MaMOUVOI s mil, MOW a luwderqusm mil,
Camp Lejeune NC 28547 COPY TO: email: lauran acosta usmc and
Sampled By: (I
Sample Identification
v I I
Collection
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PRESERVATION
.. - .• ••, • __. __.
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ANALYSIS REQUESTED
Date
Time
Temp
=
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=
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S
a
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CROM TANK
SC
C
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TCLP - Volatile, Semi -volatile,
Pesticides Herbicides RCRA 63 metals
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Reactivity, Corrosivity, Ignitabilily
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G
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Relinquished By: Date rime Received By: DateTlme
Transfer --
1. ILoS ttl f
fL=
2. n Resamole Requested:
Temperature wnen meceiveu: �,... r. ..•
Delivered By: Received
Comments:
:.' ` Time: 1 i�
T RNA OUND:

:enviroehem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910,392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info@environ mentalchemists.com
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Alberta Y. Okamoto
�n
r cam+`
T L
Lp*'-)o Pl
Date of Report: Mar 21, 2019
Customer PO #:
Customer ID: 12060026
Report #: 2019-03181
Project ID: Camp Lejeune MCB
Lab ID Sample ID:
Collect Daterrime Matrix Sampled by
19-08051 Site: Sludge W/Polymer
2/25/2019
2:30 PM Solid/Sludge Alberta Okamoto
Test
Method
Results
Date Analyzed
Chlordane (TCLP)
SW 846 Method 8081B/3510
<0.02 mg/L
03/06/2019
Endrin (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
03/06/2019
Heptachlor (TCLP)
SW 846 Method 80818/3510
<0.0005 mg/L
03/06/2019
Heptachlor epoxide (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
03/06/2019
Lindane (TCLP)
SW 846 Method 8081B/3510
<0.0005 mg/L
03/06/2019
Methoxychlor (TCLP)
SW 846 Method 80818/3510
<0.0005 mg/L
03/06/2019
Toxaphene (TCLP)
SW 846 Method 8081B/3510
<0.05 mg/L
03/06/2019
1,4-Dichlorobenzene (TCLP)
SW 848 method 8270/3510
<0.050 mg/L
03/07/2019
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
2,4-Dinitrotoluene (TCLP)
SW 646 method 8270/3510
<0.050 mg/L
03/07/2019
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
Hexachlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
m + p-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
o-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
03/07/2019
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
03/07/2019
2,4,5-TP (TCLP)
SW846 Method 8151A
<0.003 mg/L
03/06/2019
2,4-D (TCLP)
SW846 Method 8151A
<0.003 mg/L
03/06/2019
1,1-Dichloroethylene(TCLP)
SW846 Method 8260/5030
<0.01mg/L
03/12/2019
1,2-Dichloroethane (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
03/12/2019
Benzene (TCLP)
SW848 Method 8260/5030
<0.01 mg/L
03/12/2019
Carbon Tetrachloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
03/12/2019

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
USMC Camp Lejeune
Date of Report: Mar 21, 2019
G-F/EMD/ECB -12 Post Lane
Customer PO #:
Camp Lejeune NC 28547
Customer ID: 12060026
Attention: Alberta Y. Okamoto
Report #: 2019-03181
Project ID: Camp Lejeune MCB
Chlorobenzene (TCLP)
SW846 Method 826015030
<0.01 mg/L
03/12/2019
Chloroform (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
03/12/2019
Methyl ethyl ketone (TCLP)
SW846 Method 8260/5030
<0.05 mg/L
03/12/2019
Tetrachloroethylene (TCLP)
SW846 Method 8280/5030
<0.01 mg/L
03/12/2019
Trichloroethylene (TCLP)
SW846 Method 8280/5030
<0.01 mg/L
03/12/2019
Vinyl Chloride (TCLP)
SW846 Method 8260/5030
<0.01 mg/L
03/12/2019
RCI
Cyanide
EPA 335.4
<0.05 mg/kg
03/06/2019
Sulfide
SM 4500 S D
2.26 mg/kg
03/06/2019
Ignitability
SW 846 method 1010
>210 °F
03/04/2019
pH
SW 845 Method 9045D
6.98 units
03/14/2019
TCLP Metals
Arsenic
EPA 200.7
<1.0 mg/L
03/08/2019
Barium
EPA 200.7
<1.0 mg/L
03/08/2019
Cadmium
EPA 200.7
<1.0 mg/L
03/08/2019
Chromium
EPA 200.7
<1.0 mg/L
03/08/2019
Lead
EPA 200.7
<1.0 mg/L
03/08/2019
Selenium
EPA 200.7
<1.0mg/L
03/08/2019
Silver
EPA 200.7
<1.0 mg/L
03/08/2019
Mercury
EPA 245.1
<0.0002 mg/L
03/10/2019
Comment:
Reviewed by:,

ENVIRONMENTAL CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910392-0223 FAX [phone]
Info@environm entalchemists.com
CLIENT: Commandeng General
PROJECT NAME: Camp Lejeune MCB
REPORT NO:
ADDRESS: ICE/EMD/EQB/Environmental Lab
CONTACT NAME: Alberta Y. Okamoto
PO NO:
12 Post Lane
REPORT TO: Patricia H. Raper
PHONE/FAX: [phone] (fax) 910-451-7195
Camp Lejeune NC 28547 1
COPY TO:
email: patriaa raperausmc mil,albena okamotoQuamc mil,
Sampled Bv: Alberta Y. Okamoto SAMPLE TYPE: I = Influent. E = Effluent, W = Well. ST = Stream, SO = Soil, SL = Sludge, Other.
Sample Identification
Collection
A
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`o 'ono`'
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a
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PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp`�
°'
_
_
$
_
o
o
Sludge w/Polymer
2/25/201
1430
so
C
P
1
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Lsticides,Herbicide
G
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CRA (8 metals)
G
G
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Reactivity, Corrosivity,
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Ray,
As per our conversation:
G
G
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with/Polymer" and (2) 1/2 gallons marke
"Sludge". If you have any questions, ple
G
G
C
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Thanks,
G
G
C
P
Alberta
G
G
Transfer
Relin uis d By:
DatelTime
Receiv9d W
Da me
1,
,t
2/25/2019 1430
Re rigerator
02/25/2019 1435
2.
Refrigerator f j;577
M 053o
�-�,. g 3
Delivered By: Received
rime: i ( L

SECTION 6
Annual Pathogen & Vector Attraction
Reduction Forms
(Form PVRF 503)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Camp Lejeune AWWTP WQ Permit Number: WQ0012346
WWTP Name: Camp Lejeune AWWTP NPDES Number: WQ0063029
Monitoring Period: From 1/l/2019 To 3/31/2019
Pathogen Reduction (40 CFR 503,32) - Please indicate level achieved and alternative performed:
Class A: Ahernative 1 ® Alternative 2 Alternative 3
Alternative 4 Alternative 5 1 Altemative 6
j If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost I Heat Drying Heat Treatment Thermophilic 0
beta Ray Gamma Ray
Pasteurization
Class B:1 Alternative 1 Alternative 2
If applicable to alternative performed (Class B only) indicate "Process to Further Reduce Pathogens":
I Line Stabilization
Air Drying
Composting
Aerobic Digestion
I Anaerobic Digestion
j If applicable to alternative performed (Class A or Class B only) complete the following monitoring data:
Allowable Level in
Pathogen
Density
Number of
lFrequency
I Sample 1 Analytical
Parameter
Sludge
Excee-
of Analysis
Type I Technique
Minimum
Geo. Mean
Maximum
Units
dences
2x10 to the MP 4
( I
6th power per
Fecal Coliform
gram of total CFU
solids
1000 mpn per 4 grams
of total solid (dry weight)
0.04
1.82
37.40
MPN/g
0 Weekly
Grab
SM9221E
Salmonella bacteria 3 MPN per 4 grams total
(in lieu of fecal solid (dry weight)
coliform
Vector Attraction Reduction (40 CFR 503.33) - Please indicate potion performed:
Alt. i (VS reduction)
It. 2 (40-day bench)
Alt. 3 (30-day bench) Alt. 4 (Spec. 02 uptake
Alt. 5 (14-pay Aerobic)
Alt. 6 (Alk. Stabilization)
I Alt. 7 (Drying - Stable) l Alt. 8 (Drying - Unstable)
Alt. 9 (injection)
Alt. 10 (Incorporation)
Nctor attraction reduction alternatives were performed �y]
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction
reduction requirement in 40 CFR 503.33 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction
reduction requirement in 40 CFR 503.33 have not been met." (please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector
attraction reduction requirements have been met. I am aware that there are significant penalties for false certification
including fine and imprisonment."
Preparer Name and Witle{type or p 'fit) Land Applier Name and Title (if applicable)(type or print)
Y Z-Z0_Zt�
Signatur -of Preparer Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Camp Lejeune AWWTP WQ Permit Number: WQ0012346
WWTP Name: Camp Lejeune AWWTP
Monitoring Period: From 4/1/2019
To 6/30/2019
NPDES Number: WQ0063029
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 DD
Alternative 2 Alternative 3
Alternative 4
Alternative 5 Alternative 6
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying
Heat Treatment
Thermophilic 9
l Beta Ray
Gamma Ray
Pasteurization
Class B:
Alternative 1
Alternative 2
If applicable to alternative performed (Class B only_) indicate "Process to Further Reduce Pathogens":
Lime Stabilization Air Drying �� Composting
�Aerobic Digestion
Anaerobic Digestion
�
If applicable to alternative performed (Class A or Class B only) complete the following monitoring data:
Parameter
Allowable Level in
Sludge
Pathogen Density
Number of
Excee-
dences
Frequency Sample
of Analysis Type
Analytical
Technique
Minimum
Geo. Mean
Maximum
Units
I
I
'Fecal Coliform
2x10tothe IMPN
6th power er
gram oft tat CFU
solids
I
(,
((
1
1000 mpn per 4 grams
of total solid (dry weight)
0.51
1.41
i
j 5.10
MPN/g
0
Weekly
Grab + SM9221E
I
Salmonella bacteria
(in lieu oof rm cal
'3 MPN per 4 grams total
solid (dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt. 1 (VS reduction)
Alt. 2 (40-day bench)
Alt. 3 (30-day bench)
Alt. 4 (Spec. 02 uptake
Alt. 5 (14-Day Aerobic}
Alt. fi (Alk. Stabilization)
Alt. 7 (Drying - Stable)
Alt. S (Drying - Unstable)
Alt. 9 (injection)
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction
reduction requirement in 40 CFR 503.33 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction
reduction requirement in 40 CFR 503.33 have not been met." (please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector
attraction reduction requirements have been met. I am aware that there are significant penalties for false certification
including fine and imprisonment."
Preparer Name and it (type or print) Land Applier Name and Title (if applicable)(type or print)
Z7,�MZ [-,
Signat of epare Date Signature of Land Applier (if applicable) Date
*Prep r is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Camp Lejeune AWWTP WQ Permit Number: WQ0012346
WWTP Name: Camp Lejeune AWWTP
Monitoring Period: From 7/1/2019
To 9/30/2019
NPDES Number: WQ0063029
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1
Alternative 2
Alternative 3
Alternative 4
Alternative 5
Alternative 6
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying
Heat Treatment
Thermophilic O
Beta Ray
Gamma Ray
Pasteurization
Class B:
Alternative 1
Alternative 2
If applicable to alternative performed (Class B only) indicate "Process to Further Reduce Pathogens":
Lime Stabilization Air Drying
Composting Aerobic Digestion
k Anaerobic Digestion
If applicable to alternative performed (Class A or Class B only) complete the following monitoring data:
Parameter
Allowable Level in
Sludge
Pathogen Density
Number of
Excee-
dences
Frequency I sample ; Analytical
of Analysis Type Technique
Minimum
Geo. Mean Maximum
Units
Fecal Coliform
2x10tothe
6th power per
gram of total
solids
MPN
I "-
l
CFU
1000 mpn per 4 grams
of total solid (dry weight)
0.30
2.80
i 20.66
MPN/g
0
Weekly Grab SM9221E
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams total
solid (dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt. 1 (VS reduction)
Alt. 2 (40-day bench) Alt. 3 (30-day bench)
I Alt. 4 (Spec. 02 uptake �..._�
Alt. 5 (14-Day Aerobic)
Alt. 6 (Alk. Stabilization) Alt. 7 (Drying - Stable)
Alt. 8 (Drying - Unstable)
Alt. 9 (Injection)
Alt. 10 (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
011 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction
reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction
reduction requirement in 40 CFR 503.33 have not been met." (please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector
attraction reduction requirements have been met. I am aware that there are significant penalties for false certification
including fine and imprisonment."
cj,9 7
Preparer Name a d Ti (type or print)
Signatu o
Land Applier Name and Title (if applicable)(type or print)
�Zv Zu
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Camp Lejeune AWWTP WQ Permit Number: WQ0012346
WWTP Name: Camp Lejeune AWWTP NPDES Number: WQ0063029
Monitoring Period: From 10/1/2019 To 12/31/2019
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ®
Alternative 2
Alternative 3
Alternative 4 Alternative 5 Alternative 6
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying
Heat Treatment
Thermophilic
Beta Ray
Gamma Ray
Pasteurization
i
Class B:
Alternative 1
Alternative 2
If applicable to alternative performed (Class B only) indicate "Process to Further Reduce Pathogens":
Lime Stabilization
Air Drying
Composting
Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B only) complete the following monitoring data:
Parameter
_
Allowable Level in
Sludge
Pathogen Density
Numberof
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Technique
Minimum
Geo. Mean
Maximum
. Units
Fecal Coliform
WO to the
6th power per
cram of total
solids
MPN
CFU
j
10 mpn per 4 grams
'of total solid (dry weight)
3.11
4.69
7.25
MPN/g
0
Weekly
Grab
i SM9221E
Salmonella bacteria 3 MPN per 4 grams total
(in lieu of fecal coliform) solid (dry weight)
I
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt. 1(VS reduction) Alt. 2 (40-day bench)
Alt. 3 (30-day bench) ®
Alt. 4 (Spec. 02 uptake
Alt. 5 (14-Day Aerobic) Alt. 6 (Alk. Stabilization)
Alt. 7 (Drying - Stable)
Alt. 8 (Drying - Unstable)
Alt. 9 (Injection) Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
© "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction
reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction
reduction requirement in 40 CFR 503.33 have not been met." (please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector
attraction reduction requirements have been met. I am aware that there are significant penalties for false certification
including fine and imprisonment."
--
Preparer Na an itle (type or print) Land Applier Name and Title (if applicable)(type or print)
e Z ZJ
Sign re rer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

SECTION 7
Pathogen & Vector Attraction Reduction
Lab Sheets/Records

Train 1 Feed
Train 1A
Train 1B
Date
Volume T Solids V Solids
Temp T Solids V Solids Fetal Coliform
Temp T Solids V Solids Fecal Coliform Comments
(gal) % %
Deg{ % % (MPN/g)
Deg C % % (MPN/g)
1/1/2019
0
41.3
40.6
1/1/2019
0
41.3
40.6
1/2/2019
0
41.2
40.4
1/2/2019
0
41.2
40.4
1/2/2019
0
41.3
40.4
1/3/2019
0
40.3
1/4/2019
0
37.3
1/5/2019
0
34.3
1/6/2019
0
32.7
1/7/2019
0
31.1
1/8/2019
0
1/9/2019
0
1/10/2019
0
1/11/2019
0
1/11/2019
0
1/12/2019
0
1/13/2019
0
1/14/2019
0
1/15/2019
0
Wednesday, February 5, 2020 Page 1 of 5

Train 1 Feed
Train 1A
Train 1B
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp T Solids V Solids Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
Deg C % % (MPN/g)
1/16/2019
40,000
1/17/2019
40,000
19.3
14.5
1/18/2019
20.2
22.1
1/19/2019
0
21.7
25.2
1/20/2019
0
23.7
28.5
1/21/2019
0
24.8
30.8
1/22/2019
0
26.3
32.8
1/23/2019
0
31.2
35.5
1/24/2019
0
34.2
39.8
1/25/2019
0
1/26/2019
0
1/27/2019
0
1/28/2019
0
1/29/2019
0
1/30/2019
0
1/31/2019
0
2/1/2019
0
2/2/2019
0
2/3/2019
0
2/4/2019
120,000
2/5/2019
0
17.4
17.6
Comments
Wednesday, February 5, 2020 Page 2 of 5

Train 1 Feed
Train 1A
Train 1B
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp T Solids V Solids Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
Deg C % % (MPN/g)
2/6/2019
0
19.3
20.8
2/7/2019
0
21.5
24.0
2/8/2019
0
23.8
26.9
2/9/2019
0
25.7
29.0
2/10/2019
0
27.2
30.5
2/11/2019
0
28.7
32.4
2/12/2019
0
30.0
34.3
2/13/2019
0
31.7
36.3
2/14/2019
0
32.9
37.9
2/15/2019
0
34.6
39.9
2/16/2019
0
36.1
41.7
2/17/2019
0
37.0
42.4
2/18/2019
0
38.8
42.8
2/19/2019
0
40.4
42.8
2/20/2019
0
42.0
43.9
2/21/2019
0
42.8
44.1
2/22/2019
0
43.1
43.9
2/23/2019
0
42.7
42.7
2/24/2019
0
42.8
42.0
2/25/2019
0
42.7
41.3
2/26/2019
0
43.6
41.7
Comments
Wednesday, February 5, 2020 Page 3 of 5

Train 1 Feed
Train 1A
Date
Volun,re T Solids V Solids
Temp T Solids V Solids Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
2/27/2019
0
43.3
2/28/2019
0
3/1/2019
0
39.8
3/2/2019
0
3/3/2019
0
3/4/2019
0
3/5/2019
60,000
24.0
3/6/2019
0
23.3
3/7/2019
60,000
24.7
3/8/2019
0
24.4
3/9/2019
0
24.5
3/10/2019
0
25.6
3/11/2019
0
28.3
3/12/2019
0
31.3
3/13/2019
0
38.3
3/14/2019
0
45.2
3/15/2019
0
47.7
3/16/2019
0
53.0
3/17/2019
0
58.1
3/18/2019
0
58.2 0.49
3/19/2019
0
57.3
Train 1B
Temp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g)
41.4
40.8
37.7
34.8
33.3
32.1
28.0
27.8
31.5
35.1
39.7
45.0
48.1
50.4
45.7
52.7
58.9
52.7
Comments
Wednesday, February 5, 2020 Page 4 of 5

Train 1 Feed
Train 1A
Train 1B
Date
Volume
T Solids V Solids
Temp
T Solids V Solids
Fecal Coliform
Temp
T Solids V Solids
Fecal Coliform Comments
(gal)
% %
Deg C
% %
(MPN/g)
Deg C
% %
(MPN/g)
3/20/2019
0
56.1
43.1
3/21/2019
0
54.3
51.0
3/22/2019
0
53.7
49.3
3/23/2019
0
48.4
49.3
3/24/2019
0
50.2
49.3
3/25/2019
0
51.9
49.3
3/26/2019
0
57.0
47.9
3/27/2019
0
47.2
51.1
3/28/2019
0
54.3
54.4
3/29/2019
0
56.9
57.0
3/30/2019
0
55.3
56.1
3/31/2019
0
53.0
53.1
No. of Entries
93
0 0
69
0 0
1
65
0 0
0
Total
320,000
Min
0
17
0
15
Geom. Mean
58,603
0 0
36
0 0
0
38
0 0
0
Max
120,000
58
0
59
Wednesday, February 5, 2020 Page 5 of 5

ATAD TRAIN 2 QUARTERLY SUMMARY
AL,
Aw�'
Train 2 Feed
Train 2A
Train 2B
Date
Volume T Solids V Solids
Temp
T Solids V Solids Fecal Coliform
Temp
T Solids V Solids Fecal Coliform
(gal) % %
Deg C
% % (MPN/g)
Deg C
% % (MPN/g)
1/1/2019
0
48.6
57.1
1/1/2019
18,000
48.6
57.1
1/2/2019
18,000
51.6
56.3
1/2/2019
18,000
51.6
56.3
1/3/2019
0
45.2
14.80
54.7
1/4/2019
18,000
46.2
57.7
1/5/2019
0
44.9
53.9
1/6/2019
0
46.0
53.7
1/7/2019
18,000
46.9
53.2
1/8/2019
0
44.6
0.37
51.2
1/9/2019
18,000
46.3
51.2
1/10/2019
0
45.1
51.9
1/11/2019
18,000
43.0
50.5
1/11/2019
18,000
43.0
50.5
1/12/2019
0
44.5
50.5
1/13/2019
0
46.3
51.2
1/14/2019
18,000
44.4
50.3
1/15/2019
0
45.8
37.40
50.2
1/16/2019
0
47.9
50.3
Comments
Wednesday, February 5, 2020 Page 1 of 5

Train 2 Feed
Train 2A
Train 2B
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp T Solids V Solids Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
Deg C % % (MPN/g)
1/17/2019
18,000
44.7
49.9
1/18/2019
0
48.5
52.3
1/19/2019
0
51.5
53.8
1/20/2019
0
51.8
54.0
1/21/2019
0
50.4
53.0
1/22/2019
0
49.5
51.6
1/23/2019
3.3 34.60
1/23/2019
18,000
44.9 34.60
50.3
1/24/2019
0
44.5
48.8
1/25/2019
18,000
42.0
48.2
1/26/2019
0
44.5
47.4
1/27/2019
0
43.2
47.5
1/28/2019
0
44.3
47.1
1/29/2019
0
42.8
47.1
1/30/2019
0
42.6
46.7
1/31/2019
0
41.7
46.1
2/1/2019
0
40.8
45.7
2/2/2019
0
40.4
45.4
2/3/2019
0
40.1
45.2
2/4/2019
0
40.2
44.8
2/5/2019
0
39.1
44.2
Comments
Wednesday, February 5, 2020 Page 2 of 5

Train 2 Feed
Train 2A
Train 2B
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp T Solids V Solids Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
Deg C % % (MPN/g)
2/6/2019
0
39.0
43.8
2/7/2019
0
38.8
43.6
2/8/2019
0
38.6
43.7
2/9/2019
0
37.8
43.6
2/10/2019
0
36.6
42.7
2/11/2019
0
36.0
42.3
2/12/2019
0
35.5
41.9
2/13/2019
0
41.8
2/14/2019
0
2/15/2019
60,000
20.6
2/16/2019
0
22.4
2/17/2019
0
24.8
2/18/2019
60,000
23.5
27.5
2/19/2019
0
27.8
32.9
2/20/2019
0
29.5
38.2
2/21/2019
0
33.6
44.4
2/22/2019
0
40.5
48•9
2/23/2019
0
47.5
52.8
2/24/2019
0
52.6
58.5
2/25/2019
0
56.7
60.5
2/26/2019
3.6 4.76
Comments
Wednesday, February 5, 2020 Page 3 of 5

Train 2 Feed
Train 2A
Train 2B
Date
Volume T Solids V Solids
Temp
T Solids V Solids Fecal Coliformn
Temp
T Solids V Solids
Fecal Coliform
(gal) % %
Deg C
% % (MPN/g)
Deg C
% %
(MPN/g)
2/26/2019
0
57.4
4.76
60.8
2/27/2019
0
56.8
60.4
2/28/2019
0
59.6
3/1/2019
0
54.8
58.3
3/2/2019
0
53.4
57.0
3/3/2019
0
51.9
55.6
3/4/2019
0
50.6
54.3
3/5/2019
48.8
0.60
52.8
3/5/2019
3.3
0.60
3/6/2019
0
47.1
3/7/2019
0
45.9
3/8/2019
0
45.1
3/9/2019
0
45.1
3/10/2019
0
44.4
3/11/2019
60,000
44.0
3/12/2019
3.4
0.19
3/12/2019
0
37.7
0.19
42.2
3/13/2019
0
43.1
50.3
3/14/2019
0
48.8
52.3
3/15/2019
0
51.2
54.2
3/16/2019
0
53.6
54.6
Comments
Wednesday, February 5, 2020 Page 4 of 5

Train 2 Feed
Train 2A
Train 2B
Date
Volume
T Solids V Solids
Temp
T Solids V Solids
Fecal Coliform
Temp
T Solids
V Solids
Fecal Coliform Comments
(gal)
% %
Deg C
% %
(MPN/g)
Deg C
%
%
(MPN/g)
3/17/2019
0
53.1
54.6
3/18/2019
0
51.5
1.84
54.0
3/18/2019
3.3
1.84
3/19/2019
0
43.9
3/20/2019
18,000
43.9
3/21/2019
0
45.2
3/22/2019
60,000
45.5
51.3
3/23/2019
0
S4.9
51.5
3/24/2019
0
55.0
57.1
3/25/2019
0
61.4
61.1
3/26/2019
3.4
3.86
3/26/2019
0
63.0
3.86
63.0
3/27/2019
0
60.8
62.0
3/28/2019
0
56.5
60.9
3/29/2019
0
56.0
61.3
3/30/2019
0
55.4
60.5
3/31/2019
0
55.5
52.0
No. of Entries
92
0 0
90
0 0
9
80
6
0
6
Total
474,000
Min
0
21
0
28
3
0
Geom. Mean
23,895
0 0
45
0 0
3
51
3
0
2
Max
60,000
63
37
63
4
35
Wednesday, February 5, 2020 Page 5 of 5

ATAD TRAIN 3 QUARTERLY SUMMARY
Train 3 Feed
Train 3A
Train 3B
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp T Solids V Solids Fecal Coliform
(gal) °% %
Deg C % % (MPN/g)
Deg C % % (MPN/g)
1/1/2019
0
43.0
46.5
1/1/2019
0
43.0
46.5
1/1/2019
0
43.0
46.5
1/2/2019
0
47.1
48.2
1/2/2019
0
47.1
48.2
1/3/2019
0
49.1
48.9
1/4/2019
0
48.9
48.7
1/5/2019
0
48.2
47.3
1/6/2019
0
46.2
48.4
1/7/2019
0
44.6
47.8
1/8/2019
0
43.9
47.0
1/9/2019
0
43.2
46.1
1/10/2019
0
41.3
44.0
1/11/2019
0
40.1
42.6
1/11/2019
0
40.1
42.6
1/12/2019
0
38.9
41.4
1/13/2019
0
38.3
40.7
1/14/2019
0
37.2
39.7
1/15/2019
0
36.0
38.6
ea
Comments
Wednesday, February 5, 2020 Page 1 of 5

Train 3 Feed
Train 3A Train 38
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform Temp T Solids V Solids Fecal Coliform
(gal) % %
Deg C % % (MPN/g) Deg C % % (MPN/g)
1/16/2019
0
34.5
1/17/2019
0
33.1
1/18/2019
0
31.8
1/19/2019
0
30.7
1/20/2019
0
30.0
1/21/2019
0
28.7
1/22/2019
0
27.3
1/23/2019
0
1/24/2019
0
1/25/2019
0
1/26/2019
0
1/27/2019
0
1/28/2019
0
1/29/2019
0
1/30/2019
0
1/31/2019
0
2/1/2019
0
2/2/2019
0
2/3/2019
0
2/4/2019
0
2/5/2019
0
Comments
Wednesday, February 5, 2020 Page 2 of 5

Train 3 Feed
Train 3A
Train 3B
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp T Solids V Solids Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
Deg C % % (MPN/g)
2/6/2019
0
2/7/2019
0
2/8/2019
0
2/9/2019
0
2/10/2019
60,000
2/11/2019
0
18.2
2/12/2019
0
18.8
2/13/2019
60,000
20.2
2/14/2019
0
21.5
22.8
2/15/2019
0
54.6
26.9
2/16/2019
0
31.7
31.3
2/17/2019
0
37.7
36.6
2/18/2019
0
42.8
42.9
2/19/2019
0
46.9
47.9
2/20/2019
0
51.0
51.9
2/21/2019
0
53.1
54.7
2/22/2019
0
55.8
55.2
2/23/2019
0
54.2
54.5
2/24/2019
0
52.5
52.4
2/25/2019
0
50.2 0.15
49.8
2/25/2019
3.1 0.15
Comments
Wednesday, February 5, 2020 Page 3 of 5

Train 3 Feed
Train 3A
Train 3B
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp T Solids V Solids Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
Deg C % % (MPN/g)
2/26/2019
0
47.0
50.2
2/27/2019
0
2/28/2019
0
3/1/2019
60,000
31.1
3/2/2019
0
3/3/2019
0
3/4/2019
60,000
31.3
31.3
3/5/2019
0
30.0
33.3
3/6/2019
0
30.8
34.2
3/7/2019
0
32.7
35.3
3/8/2019
0
34.9
36.9
3/9/2019
0
35.2
36.8
3/10/2019
0
38.7
38.7
3/11/2019
0
43.3
41.1
3/12/2019
0
45.9
42.8
3/12/2019
3.9 1000.00
3/13/2019
0
48.3
44.2
3/14/2019
0
49.6
45.0
3/15/2019
0
45.5
50.0
3/16/2019
0
36.9
41.3
3/17/2019
0
53.0
54.0
Comments
Wednesday, February 5, 2020 Page 4 of 5

Train 3 Feed
Train 3A
Train 3B
Date
Volume
T Solids V Solids
Temp
T Solids V Solids
Fecal Coliform
Temp
T Solids
V Solids
Fecal Coliform Comments
(gal)
% %
Deg C
% %
(MPN/g)
Deg C
%
%
(MPN/g)
3/18/2019
0
49.3
1.06
45.3
3/18/2019
3.8
1.06
3/19/2019
0
49.1
50.3
3/20/2019
0
42.5
44.0
3/21/2019
0
46.7
48.3
3/22/2019
0
48.7
3/23/2019
0
49.9
3/24/2019
0
41.1
41.9
3/25/2019
0
47.9
42.9
3/26/2019
0
47.1
41.9
3/27/2019
0
39.4
3/28/2019
0
42.4
37.7
3/29/2019
60,000
47.1
38.4
3/30/2019
0
42.5
3/31/2019
0
43.1
No. of Entries
94
0 0
69
0 0
2
57
3
0
3
Total
300,000
Min
0
18
0
23
3
0
Geom. Mean
60,000
0 0
40
0 0
0
43
4
0
5
Max
60,000
56
1
55
4
1,000
Wednesday, February 5, 2020 Page 5 of 5

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
L- 9C
99e
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
p 7c D
CJiL7
tav°t
S C
3b
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
5M 2540 8 E 2011 �J
e 7 a C I n I c I c I r_
I
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
o
T
TOTAL
SOLIDS
0
�'
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
-A]
C- A
C- DI
ffUX 100
[Gfl X 100
Z
'ia 3 v
1� -�722--
o
S O°
10 . ► (�
o_ o
2f3
Sf. d
MK 4�sOV-
13 W 2P-/
1 0 - t v
V •
13 �
oC'
0- (13
0 • v 01-
-3• -f be
A 3
DUP.
�q
�C'1
(53
(-•oo
o. t-74
0ENC•o��-
I
%D=
BENCHSCALE
��. 3 l 71
I ,{�?-
t . `C D
•S�o
Q
CJ -��}
U v
O . I�jQ
0. 01 ?—
�i • (p D
5�j. ��
AVG MSCALEW
BENCHSCALE DUP
- D3 �
D
(fib
V �Q . n t
�� . v {
D t)
QC
OC TRUE VALUE: I I QC REPORTED: —�
% Duplicate = Difference in 2 values x 100 % Recovery = Resufts oqtajned x 100
Average of 2 values Known value
FORM UPDATED: DECEMBER 2017
QC RANGE: I—�—�
CHECKED BY U*
COPY MADE. W

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
I /30
O-70-7
LA t t<
SM 9221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO. W012345
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Enclosure
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB, OF
MPN INDEX
SAMPLE
POSITIVES
VALUE
MPN ! mL'
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
O-fLo
O
0
-T V—•-
15
15
Y /5
15
15
15
''" /5
15
S—O
A %0
f1
L4,0
DUP
15
15
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
dBSS
DATE OUT: , V1
TIME OUT:
TEMP: _ -C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
l 419
C]
D85�
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
vos
4
DS A-1 BROTH
p'Sf�'
A
MPN 1 mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN / GRAM2
% TOTAL SOLIDS
MPN/GRAM' = MPN 1 mL
CHECKED BY
COPY MADE
% Total Solids
(expressed as a decimal)
FORM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
/dIq
C `7C
SM 9221C E-2006 1
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: ,
TIME RECEIVED:
RECEIVED BY: �1✓J
PERMIT NO. WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Enclosure 1
SAMPLE
LOCATION
3 HRS AT 35 + 0.50C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN ! mL'
10 mL
1�mL
0.10 mL
0.{010 mL
10 mL
1 mL
0.10 mL
0.01100 mL
C�bi1n
0/5
/5
O /5
v 10/5
I 15
15 /5
/5
/5
_ � /�
l _Z V
0• I OlLJ
DUP
L-) 151
/ 5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HU KJ A I 35
�t.s.r�
Oct f
3c7 'C
0.50C IN INCUBATOR l/
DATE OUT: f f y
TIME OUT:
TEMP: 3S ' C-) 'C
21 + 2 HOURS AT 44.5 + 0.2'C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
V
MPN / ml- = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN ! GRAMI
% TOTAL SOLIDS
MPN/GRAMZ = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY w
COPY MADE
FORM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
11S I Ci
� -7
SM 9221C E-2006 I
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: l (i
TIME RECEIVED: o e)o j
RECEIVED BY:C�
PERMIT NO. I WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
( - 1 C_. l �I
6026
"Nas
Enclosure
SAMPLE
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44,5 + 0.21C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN I mL'
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
czot `
/5
0 15
C) l5
0 l5
0 l5
15
l5
Q /5
0-1 j-D
O 'CA
jL
0,09 '"�
DUP
O t5
0 /5
DATE 1N:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0,5'C IN INCUBATOR
1-t5-jq
o 0
�3� . v •C
DATE OUT: ` ' L S ' � `
TIME OUT: ` � L 0
TEMP: 3� 'C
21 + 2 H�'OURSAT 44.5 + 0.2°C IN WATER BATH
t
-, J 1 19
1 DATE OUT: 1. L,(o
i 4 TIME OUT:
• 'C TEMP: -7-1 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
d J
N
DS A-1 BROTH
pbs
Itj�
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN/GRAM 2
% TOTAL SOLIDS
MPNIGRAM' = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY (
COPY MADE
FORM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: �_; 19
TIME RECEIVED:,
RECEIVED BY:�'
PERMIT NO. �- WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
koCC)
ti-S
Enclosure (1)
SAMPLE
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT ".5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN ! m!'
LOCATION
110 mL
1 mL
0.110
0.010 mL
mL
1 mL
0.10 mL
0.010 mL
GIzo,v
f
L./ /5
0 /5
jmL
v 15
� /5
(100
"-' 15
� /5
O /5
O /5
DUp I—o
/5
J5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
lD zq
3S - D -C
DATE OUT: � - �- l `
TIME OUT: 132 `1
TEMP: 3 S . 0 •C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
MPN / mC = MPN Index Value
Largest Sample Volume
(from comb. of positives)
MPNIGRAM'
% TOTAL SOLIDS
MPN/GRAM' = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY,
COPY MADE
FORM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
10 4 �t
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: 2 .2 S . I I
TIME RECEIVED:
RECEIVED BY:
PERMIT NO. F WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
2-2s .I-(
2_ VS
tA-
Enclosure (1)
SAMPLE
3 HRS AT 35 + 0.5'C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
COMB, OF
POSITIVES
MPN INDEX
VALUE
MPN ! mL'
LOCATION
10 mL
1
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
-T36
O i5
rmL
5
5
v 5
4 :5
� 15
� 15
� /5
1
DUP
V
5
D 5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5'C IN INCUBATOR
DATE OUT: 2 Z- S-- ! l
TIME OUT: }G 1w
TEMP: •C
21 + 2 HOURS AT 44.5 + 0.2'C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
D
--
FORM UPDATED OCTOBER 2018
�2 .2& 11
��'22 }
•C
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN/GRAM
% TOTAL SOLIDS
l�
MPN/GRAM` = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY: V
COPY MADE

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
,2Q - 6;2C9 - f q
SM 9221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: Z 2-6- k9
TIME RECEIVED:
RECEIVED BY:
PERMIT NO. WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Enclosure (1)
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
MPN INDEX
SAMPLE
POSITIVES
VALUE
MPN 1 mL'
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL_,,A
1 mL
0.10 mL
0.010 mL
/5
/5
C_. 15
-- /5
X7 /5
/5
Ld /5
9• /5
b-11- I
1�.2��
DUP
15
l5
DATE IN
TIME IN
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
1�
35.v 'C
DATE OUT:
TIME OUT:
TEMP. S °C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
" 2 LD � �� DATE OUT: ;2 -7 I
`\ TIME OUT: 0 ? i)
'C TEMP: L f• � 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb. of positives)
MPN i GRAM2
% TOTAL SOLIDS
MPN/GRAM' = MPN / mL
CHECKED BY
COPY MADE
% Total Solids
(expressed as a decimal)
LA -
FORM UPUA'iEO OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: 3 �j Vt9
TIME RECEIVED: 0�.�-C,
RECEIVED BY:
PERMIT NO. �— WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Enclosure (1)
3 s 2-co 19
SAMPLE
LOCATION
3 HRS AT 35 + 0.5'C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN / mL'
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
15
15
15
0 15
15
P5
15
15
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 "UUKa A I Ja
•C
0.5°C IN INCUBATOR q
DATE OUT: 3 5 i
TIME OUT: 3O
TEMP: S v 'C
21 + 2 HOURS AT 44.5 + 0.2'C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
-3r 1-e, k9
1 l i 1C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
qD5
Nr -
DS A-1 BROTH
1?01
P e-L
MPN 1 GRnnAM2
U
% TOTAL SOLIDS
MPN I mL' = MPN Index Value MPN/GRAM'
Largest Sample Volume
(from comb of positives)
CHECKED BY
COPY MADE
MPN r mL
Total Solids
(expressed as a decimal)
FORM k1PDATED: OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
0'5-iL-i7
l5
W
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
;. 12 (ci
©9 ZO
SO L)Js l v e- ,
W012346
DATE ANALYZED:
TIME ANALYZED
ANALYZED BY:
3 I� 19
1o(S'
Enclosure (1)
SAMPLE
LOCATION
3 HRS AT 35 + 0.5'C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN / mL'
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
r v
`-' IS
`-r 15
15
CD 15
/5
/5
/5
3 15
5-5 "3
1
y
3,«
C
DUP
/5
O /5
3 HOURS AT 35+ 0.5°C IN INCUBATOR G�
DATE IN: t2 k 9 DATE OUT: t 2,
TIME IN: O� TIME OUT:
TEMP: 3 C1 TEMP:L 3 'C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE IN: �' 12 ' t DATE OUT: 3, j 3 . 19
TIME IN: l 3- TIME OUT: b t
TEMP: T 'ClTEMP: 4 '� 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
U�
DSA-1 BROTH
"M UPDATED OCTOBER 2018
MPN/GRAM'
7
% TOTAL SOLIDS
;•I I
MPN t mL' = MPN Index Value MPN/GRAM =
Largest Sample Volume
(from comb of positives)
MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY: w
COPY MADE.

DATE COLLECTED: --1 J.--
TIME COLLECTED: f `%
COLLECTED BY: 1�
METHOD: SM 9221C ESM E-20066
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
3 (2 • 201C1
09�2-0
WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY
WA ;
SO-15�ltfcr
Enclosure (1)
SAMPLE
LOCATION
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 41.5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN ! mL'
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
O /5
15
15
11
IS
15
15
5
5
15
/r
40.41a
DUP 1/51
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN: 4 DATE OUT: t '
TIME IN:TIME OUT: �f'f
TEMP: 3C °C TEMP: "Cl
21 + 2 HOURS AT 44.5 + 0.21C IN WATER BATH !!
DATE IN: trZ • DATE OUT: ✓ ' I I
TIME IN: TIME OUT:
TEMP: rT - •C TEMP: L•C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
MPN/GRAM2
G
D� D �S�•�t y^
% TOTAL SOLIDS
-4' 34
MPN / mL' = MPN Index Value MPNIGRAM' = MPN / mL
Largest Sample Volume % Total Solids
(from comb of positives) (expressed as a decimal)
CHECKED BY
COPY MADE
F -)RM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD: SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: '3.7 Z , , q
TIME RECEIVED: 0(1 �-v
RECEIVED BY: S�( I
PERMIT NO. W412346
DATE ANALYZED:
TIME ANALYZED
ANALYZED BY
Enclosure (1)
1 3. a- 19 1
3 HRS AT 35 + 0.5'C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
COMB. OF
MPN INDEX
SAMPLE
POSITIVES
VALUE
MPN 1 mL'
LOCATION
10 mL
I mL
0.10 mL
0.010 nil-
10 mL
1 mL
0.10 mL
0.010 mL
15
T / 5
15
15
/ 5
15
13 15
Q
DUP
/ 5
15
3 HOURS
AT 35 + 0.5"C IN INCUBATOR
cf
DATE IN: 2¢ i t DATE OUT: -3, 1 2 i
TIME IN: ' ` TIME OUT:
TEMP: 3 'C TEMP: 'C
211 + 2 HOURS AT 44.5 + 0.2'C IN WATER BATH I �j
DATE IN: ?' (2 �� DATE OUT:
TIME IN: 134 TIME OUT: f V
f ,
TEMP: ' � -C TEMP: -C
CONTROLS:
SITIVE
NEGATIVE
BLANK
SS A-1 BROTH
0 �
�Y->,
DS A-1 BROTH
-46\
FORM UPDATED OCTOBER 2018
r�
MPN I mL' = MPN Index Value
Largest Sample Volume
(from comb of posdrves)
MPN/GRAM
,'Clo
TOTAL SOLIDS
?%.3Lp
MPN/GRAM' = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE
13

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
3-18.17
o q ds
tN;IIrA►�-:
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: 3 _ it lq
TIME RECEIVED:
RECEIVED BY: S
PERMIT NO. W012346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
-3
Enclosure (1)
SAMPLE
3 HRS AT 35 + 0.5'C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN ! mLi
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
T 4
V /5
15
G, 15
15
V 15
15
D 15
15
0 ID
0 3�
DUP
15
151
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE OUT: 3' Ill? ' IR
TIME OUT: I Z L4 S
TEMP: 3 S - C 'C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
3 •1 S . }i DATE OUT: 3
1 Zy S TIME OUT: 0 g Z S
L M - 4' -ClTEMP: 14 Lq 1 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
1
t
/,
N
DS A-1 BROTH
MPN ' mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN ! GRAM'
} C)
% TOTAL SOLIDS
MPNIGRAM2 - MPN T mL
CHECKED BY
COPY MADE
% Total Solids
(expressed as a decimal)
FORM UPDATED: OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
3-!g�l9
a qo s
1N., 11,
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: 3 . 1?. 11
TIME RECEIVED: D 1 D
RECEIVED BY: C—S
PERMIT NO. WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
3.IIf ,11
D 12,0
A E-s
Enclosure (1)
SAMPLE
3 HRS AT 35 + O.S'C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN / mL'
LOCATION
10 mL
1 mL
0.10CnmL
0.0110 mL
10 mL
1 mL
0.10 mL
0.010 mL
T2g
15
0 /5
T /5
i' 15
15
/5
O r5
O
_3_0
0
p 5t„
`Y
0 `E
I
DUP
15
15
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5'C IN INCUBATOR
3. ►s t�
a � L4
3S.o -C
DATE OUT: 3 ` } g ' 1
ck—
TIME OUT: 1 Z S
TEMP: 3S - b •C
, 10
21 + 2 HOURS AT 44.5 + 0.2'C IN WATER BATH c�
3. 1 S - !9 DATE OUT: 3 ' 11 11
1 2-14 $ TIME OUT: b j 2 s
qL4. Ip 'C TEMP: L4- -C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
P
rI
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN/GRAM'
% TOTAL SOLIDS
'f.-�-(y
MPN/GRAM' = MPN / mL
CHECKED BY
COPY MADE
% Total Solids
(expressed as a decimal)
FORM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
0
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: -3 - , 5 t - I
TIME RECEIVED: Oct (0
RECEIVED BY: bps
PERMIT NO. WQ12346
DATE ANALYZED
TIME ANALYZED:
ANALYZED BY:
-3-tom t, �
09 20
Enclosure (1)
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2-C IN INCUBATOR
COMB. OF
MPN INDEX
SAMPLE
POSITIVES
VALUE
MPN / mL'
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
1 IS
(D r5
15
D 15
15
15
1 I5
l5
15
0-1-D
0.(g
0.Q
D
�
D
DUP
15
d5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5'C IN INCUBATOR
� \S 1a
DATE OUT: 'J l 3 ' ,
TIME OUT: 12 S
TEMP: 3S`_ V 'C
i + 0.2'C IN WATER BATH
DATE OUT: J - I
TIME OUT: 092.5
TEMP: `i q - -7 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
P
r%
N
DS A-1 BROTH
N
MPNImL'=
N
MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN I GRAM'
o, q I
% TOTAL SOLIDS
`-0
MPN/GRAM' = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE
FORM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
SM 4221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Enclosure (1)
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0,2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN 1 mL
SAMPLE
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
ZB
O /5
0 /5
"'" f5
/5
0/5
5
;5
r5
1 j
DUP
0 /5
1
O /5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE OUT: ' 2- C,, 1
TIME OUT: t� OC.3
TEMP: 3S L) •C
?i + 2 Hc]t1RS AT 44.5 + 0.2°C IN WATER BATH
DATE OUT: �
TIME OUT: (Y)
TEMP: •C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
f 10-
DS A-1 BROTH
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN/GRAM'
�-069
% TOTAL SOLIDS
MPN/GRAM' = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE
U'
FORM UPDATED OCTOBER 2018

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
3
I
4
t
++[
l - + •
�,�
TIME IN OVEN: 0��_
OVEN TEMP: p + • t -C
BALANCE CK:
METHOD: SM 2540 8 E - 2011
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
C�G3o
1 o�4-S
t off. S -G.
`tcm
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
w I"(.a�S
�S
20 --
Q�+ 6150 °C
1 L - T� 1 to
N
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
%
TOTAL
SOLIDS
%
VOLATILE
SOLIDS
°I -
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
IS - A
C - A
C - DJ
[F/El X 100
G/F X 100
�5. op
0,
0.
-2(s'
r36
`
ID - to o
6V
6�•510�
5. (50
0.
0 •
go
+1 • 130
91 a�-
b
15
15. od
01
0 • [TI
s?_
V, 04-
Ct V,
�cl
0- 1133
0,o96
t,;Cp
i3. v
AVG: f C�
DUPAom -rama-
0' t 03
0.061
3 b LP
s
%D= a
BENCHSCALE
?j,
�t
t ��
j�
?J
S.Ob
C�•I�
C7 �S
,,�.C�
y�.
BENCHS E
AVG .�j�j
BENCHSCALE DUP
b, b
lq • b 3
• L
5; U O10,(03
0 • (�, S
, • 0 &
53
J�
V
QC
QC TRUE VALUE:
% Duplicate = Difference 1112 values x 100
Average of 2 values /
FORM UPDATED: DECEMBER 2017
QC REPORTED: I —�I
% Recovery - Results obtained x 100
Known value
QC RANGE: I
CHECKED BY: Ulk
COPY MADE: Ue

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
1 S f
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
I • l u J %
l / a 1
OE33D
i C� • S °C
-' 'I v�
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
METHOD: �SM 2640 B_E - 2011
e I R C D E F G
0SOD
O "7 OU
to-2
t vim• °C
Q� .S� gp
(tD
SSD PC
X
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
OF
DISH+ASH
SALE
WE GHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(9)
(g)
(g)
(g)
(4)
(g)-
(g)
- A
C -
C - DJ
FIE X 100
G/>= X 100
3
�� 3tiq�
��. �r
��•��3
3q��
t),00
0 -rl :
o 100
3 Sg
655
eL 0.6S5(
`i t • 0 4
9(• �)-1
&. (
s. o0
0 [�
o off'(
3
S
. °'1
Fe
o - � 30
o
4 l�
010m
t 1�-
O. o e
3. sv
AVG s�
DUP: C,Qc�+m
0
7 0
3. 32-
3. i��3°�
S- oo
0 mi
0
%D= t
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE:
% Duplicate - Difference In 2 values x 100
Average of 2 values
QC REPORTED: L 771
% Recovery = Results obtained x 100
Known value
QC RANGE:
CHECKED BYy_
FORM UPDATED: DECEMBER 2017 COPY MADE

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS'
DATE COLLECTED:
DATE RECEIVED: l q
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
O,0-2,U
l S -C
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
in700
Q-0J
� � 30
q �'•� eC
t�l Ci1 1
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
SM 2640 B E - 2011 -71 U
4 I A I C I f} I F I F I G
rJ
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
�
TOTAL
SOLIDS
VOLATILE
TILE
SOLIDS
%
RECOVERY
{g)
(g)
(g)
(9)
(g)
(g)
Igo
- A
C - A
C - DJ
FIE X 100
[G/Fl X 100
,rzQ
��.3�-3�
�� ��
�� So t
7� �b
:�* 0o
0.1,10
0.
S
o
F
�3 Z923
'1
'i3•SZ(�0
1� I'll
Svo
p ;
p .lS
(QE3
(0S--00
; i'l
�A
s . o0
0 - I+F?
AVG
DUP:
%D=
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: QC REPORTED:
% Dupitcate = Difference In 2 values x 100 % Recovery = Resulls gbtained x 100
Average of 2 values Known value
QC RANGE. I�
CHECKED BY V`
FORM UPDATED DECEMBER 2017 COPY MADE.

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYST { t
DATE COLLECTED: i/ L I `I TIME COLLECTED:
DATE RECEIVED: 1 2� l TIME RECEIVED:
DATE ANALYZED: i TIME STARTED:
ri1:L I:[e]y/:121A
OVEN TEMP:
BALANCE CK:
METHOD:
D loS- TIME OUT OVEN:
(� LM°C OVEN TEMP:
I q l . c G A Iq D BALANCE CK:
SM 2540 B E - 2011
COLLECTED BY:
C
RECEIVED BY:
ANALYST:
��\\
TIME IN FURNACE:
FURNACE TEMP:
15 0 °C
BALANCE CK:
�l j q it O
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
a/,
TOTAL
SOLlDS
%
VOLATILE IDS SE
SOLLID
%
RECOVERY
(g)
(g)
(g)
(g)
{g)
(9)
(9)
A
C - A
(C - Oj
[F/Q X 100
[Gfl X 100
00
o. Zoe
a l `�
�{ • !
(� 3
- 2-38(�.p35�
1. ��
. 20'
l
s oo
o. L15
0, oq
3�4
e
.3
f:-e':L-J
96.31
1-40
-U[q
GAj4
�.00
14
.or
N-0m ul�v_
?3.tavt?` -'1�
-. 0
�� ��
�,.
s.On
0,1103
0 01'5t
3.
�fL ��
AVG 3
DUP: O M
U
l
Zl.
3 Z I
?' l Q
S 00
0, I b�
(i u� t�
9-
�
%D= I
BENCHSCALE
BFNCHSCA:E
AVG
BENCHSCALE DUP
%D=
QC
OC TRUE VALUE:
% Duplicate = pifierence In 2 values x 100
Average of 2 values
QC REPORTED:
% Recovery = Results obtained x 100
Known value
QC RANGE:
CHECKED BY: Vr
FORM UPDATED- DECEMBER 2017 COPY MADE-

"I4`'tlie Co �t���.,
CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS 6_4W°r & 3 -
DATE COLLECTED: ' Z ( T
DATE RECEIVED: r1 Z ` G
DATE ANALYZED: ! 2 ( 1 I
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
opt 0 S
104-A ^C
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
c,;7o0
0
°C
q0t �b
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
SM 2640 B E - 2t311
o I r I n I c I G I C,
U
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
°%
TOTAL
SOLIDS
%
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(9)
(9)
(9)
(g)
(9)
B- A
C- A
C- DI
F/E X 100
[Gfl X 100
7-11a
12-
0. �o(P
0
. 00
o . E1
0.09 3
5.40
53
AVG
DUP:
%0=
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D=
4C
QC TRUE VALUE: QC REPORTED:
1/6 Duplicate - Difference In 2 values x 100 % Recovery = Resufts obtained x 100
Average of 2 values Known value
QC RANGE: I t
CHECKED BY
FORM UPDATED: DECEMBER 2017 COPY MADE.

O ut ir,ctt i s Loc z-4a d , ,l N)crx5,
CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS R-rh -
(• -3t.II
DATE COLLECTED: I ' 2 R - 1
DATE RECEIVED: 1 �G
DATE ANALYZED: t
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
L7
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
r,✓iL C-1 4,-
�S
IDE:75
Sp^S U °C
J
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
TOTAL
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(9)
(9)
(9)
(9)
(9)
(9)
(9)
- A
C - A
(C - DJ
[F/EJ X 100
G/F X 100
rzb
9G-M4
T 39
OG-' O
s c,0
0 (1
2.100
3 SO
6s.O3
00
0 13
0 070
U O3
t�1 tt�
AVG
DUP:
%D=
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE:
% Duplicate = Difference In 2 values x 100
Average of 2 values
QC REPORTED:
% Recovery = Results obtained x 100
Known value
QC RANGE: I� - I
CHECKED BY: Or
FORM UPDATED: DECEMBER 2017 COPY MADE

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
ll`
4� f l fA
t I
°C
CSC
` t ��v
SM 2W B E - i
0 Z 30
01 OLU
�� os
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
U
SAMPLE
LOCATION
r`
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOUDS
WEIGHT
X
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(g)
(9)
(9)
(g)
(9)
(9)
(g)
A
C- A
C- DJ
[F/Fj X 100
[G/F7 X 100
5 0o
0 09 S
3 4(0
S
AVG r 1
DUP:
�r� 3 00
1
'�1 ��
G J'
1 V
s �v
o ��
0 C'q
S4
%D= l
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: I i QC REPORTED: I I
% Duplicate = Difference In 2 values x 100 % Recovery = Results obtsimed x 100
Average of 2 values Known value
QC RANGE: �— J
CHECKED BY
VIC-
FORM UPDATED: DECEMBER 2017 COPY MADE.

CAMP LEJEUNE WWTP — ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
Z— - y
TIME COLLECTED:
DATE RECEIVED:
7--'! — �g
TIME RECEIVED:
DATE ANALYZED:
� '��
TIME STARTED:
TIME IN OVEN:
y d
TIME OUT OVEN:
OVEN TEMP:
Q3 • C) °C
OVEN TEMP:
BALANCE CK:
I OO • 0
BALANCE CK:
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
METHOD: SM 2W B_E - 2011
r n C c C
E; SD I
l©o OkQ
SAMPLE
LOCATION
^
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
TOTAL
%DISH+ASH
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(g)
(9)
(g)
tg?
(g)
- A
C - A
C - DJ
[F/E7 X 100
[Gfl X 100
7'
a3S
91 tO
.2'��
25o
Oc,�
(? Z .
0. g
4.181
Co3. 5
Tzg
z�a
CP
-7 4 1O
.0
3.52_.
57 38
F-d-IF-
TS'• SY1Z
Fb .
`t 5.-1q
5•C,
3ca2_
s Wp
'- • 2
Co
AVG
DUP: F11.1P�73
Zq y3
. 31
J13. S3
`7 3,37 G,
5
O .Z� t`l
. "l In
G-5 3
%D= O .$
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE:
% Duplicate = Difference In 2 values x 100
Average of 2 values
FORM UPDATED' DECEMBER 2017
QC REPORTED: L- 7_771
% Recovery = Results obtained x 1 Do
Known value
QC RANGE:
CHECKED BY: v
COPY MADE:

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
2' 7 "+
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
2 ?^L
- 21-1-1
O
°C
I Lr) C' `j
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
METHOD: SM 2540 B_E - 2011
w I o I l' I r% I C ICI (
0 -7 u ,7
1b tD
VIIIA C�
o" .$ °c
`1 .::lq
SAMPLE
LOCATIOSOLIDS(g)
WT OF DISH
WT OF
DISH+WET
50QS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
�
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(g)
(g)
fig?
(g)
JB-A
C- A
C- Dj
FIE X 100
G/F X 100
ZS
y :3225
-19. 3
.yg9q
5.o35a
9
, Q q
. ` V-1
53.LID
r-6
La-ASch
9 2,.
t6D
2.3t '?
3
. W05
5.05%3
0 .-Z l I&S
/1 1139102
AVG 4. O
DUP. F E e. ,o
D.2
a
.2:A
. U
%D=
BENCHSCALE
SENCHSCALE
Avc
BENCHSCALE DUP
�D=
C}C
QC TRUE VALUE:
% Duplicate = Difference In 2 values x 100
Average of 2 values
QC REPORTED:
% Recovery = Results obtained x 100
Known value
QC RANGE:
CHECKED BY: LIK
FORM UPDATED' DECEMBER 2017 COPY MADE:

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:©U5.
BALANCE CK:
METHOD:
O `J`! t
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
�- 1
�t 5 lot
01036 CA
S� °C
Cl� • -t��
SM 2540 B E • 2011
C� o -
U+i c�v
wsco
(OS °C
u
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
.rs.t
°C
qq qqs--
0
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
°A
TOTAL
SOLIDS
VOLATILE
ATILE
SOLIDS
%
RECOVERY
(9)
(9)
(9)
(9)
(9)
(9)
(9)
B - A
C - A
C - DJ
[FU X 1
[Gfl X 100
r ItS
�`_
�i.3
�•
S�
0•livq
Dv°�i
-T Z 6
0
8 .2-
Oa t
5 Uo
t0
0.0-1
<�'
3
�
�
:5.Uo
tr.
AVG
DUP:'���
�r{•�
'��
�,j•.1
`�
G 00
O,,l.,el
0 fJckv
. ��%
�}
63. /4
%p= b
BENCHSCALE
SENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: F - QC REPORTED:
°% Duplicate - Difference In 2 values x 100 % Recovery = Resuhs obtained x 100
Average of 2 values Known value
QC RANGE: I I
CHECKED BY'
Vr-
FORM UPDATED' DECEMBER 2017 COPY MADE

w to ( -Skt, --1 d� �d f �- . ►�t
CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS o�P cut kc4ld-YA
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED: A - Is, t r
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
o 7 20
1 os(v
(O's °C
-S,19'T
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
NIT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
HT
WEIGHT
VOLATILE
SOLIDS
WEIGHT
TOTAL
SOLIDS
VOLATILE
A TILE
SOLIDS
%
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
8- A
C- A
(C - DI
FIE X 100
G/F X 100
--113
f 5
�D S3
1
.b��5
5.��
0, 2c1�3
0 ►� o
�Lv
5�.G
r 3 a
3
(go
13
00'
n (�
S 00
p ill
0.►�5�"
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AVG
DUP:
%D=
BENCHSCALE
9ENCHSCALE
Avc
BENCHSCALE DUP
%D=
C}C
QC TRUE VALUE:
% Duplicate - Difference In 2 values x 100
Average of 2 values
QC REPORTED: I - I
% Recovery = Resuhs obtained x 100
Known value
QC RANGE:
CHECKED BY w
FORM UPDATED' DECEMBER 2017 COPY MADE.

DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
v ? v q
093c')
0$3 0 �
l OSo
10 LA Z °C
99
"1g93
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
w
lZ"S
'C
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
T OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(g)
(g)
(g)
(9)
(g)
A
C - A
jC - Dj
FIE X 100
[GIF] X 100
-
6 ZFO
�9, 7l
7Li. M1
79 1 Co (
5. 2f>
0.200 1
p . tizo
3 3 L.,
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5. Li zz
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3
3.
S.o�SZ
o.
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DUP:
�. 3 u3
g3. yd
. -'-ZZLp
It>.43 %
5.0
Q.27.-73
U. I -19'
H-S
b 2
%D= �
BENCHSCALE
13ENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: I�
% Duplicate - Difference In 2 values x 100
Average of 2 values
QC REPORTED: I
% Recovery = Resume obtained x 100
Known value
QC RANGE: I
CHECKED BY' Uk
FORM UPDATED: DECEMBER 2017 COPY MADE:

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
Li / `I
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
;2- - 9/ -/
o! ",�2/ -! `i
O °C
l6 o
SM 2S40 B E - 2011
03 co
0830
Co,530
53-c�
( Dy Z °C
9n
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE: 123
FURNACE TEMP: °C
BALANCE CK: loo_ QU
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
OF
DISH ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(9)
(9)
(9)
(9)
(9)
(9)
(9)
A
C- A
C- DJ
IF/E7 X 100
[Gfl X 100
--_ p
5
D S
S.`lyoo
-7S, (.210
5, 'SS
0 3)
o . t 33
03
SS-C9;
Z
9
R 1. o z
i ts:og
�(� .uy z
s.
o. t 7
3�
S9 2g
Q
7g3z36,
7939
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3
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AVM z
DUP: %-3 Q
3.2�27
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t-tZZZ
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0.
o. S
Z U to
(92.30
%D= c) . 3
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: I
% Duplicate - Difference in 2 values x 100
Average of 2 values
QC REPORTED:
% Recovery = Results obtained x 1 DO
Known value
QC RANGE:
CHECKED BY. L<
FORM UPDATED DECEMBER 2017 COPY MADE:

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
,�- '� S ` 19
TIME COLLECTED.
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
2-- 2 S . 1 9
-,PL - 19
[-:a-- CD c7
'-A °C
I G . C)
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
METHOD: SM 2540 B_E - 2011
e I R I C I n I F I F I G
t
tG
S � °C
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRYLI
SODS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
%TOTAL
SOLIDS
VOLAA TILE
SOLIDS
%
RECOVERY
(g)
(9)
(g)
Igl
(9)
(g)
(g)
B- A
C- A
C- DI[FIE]
X 100
G/F X 100
v3S$
1. kc)
5,L9, kg L)
y
S .any
o
6 ct ois
3. S
S6 RI
AVG 3,
DUP: 'T 3 a
2.31(a�
33
Z y u
? 2.38 Sa
U �3Z
0 5 I
bBS�-
3. t
5C9 -�
%D= 3
BENCHSCALE
9ENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: I ! I
% Duplicate = Difference In 2 values x 100
Average of 2 values
QC REPORTED:
% Recovery = Results_ obtained x 100
Known value
QC RANGE:
CHECKED BY
LA -
FORM UPDATED: DECEMBER 2017 COPY MADE

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
X- —�, (p ` I
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
S^ QJ
p j
°C
i Q 0 -
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
METHOD: SM 2540 B E - 2011
A I B I C D E F G
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
%A
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(9)
(g)
(g)
(g)
Igl
- A
C -A]
C - Df
[F)Fj X 100
IGIN X 100
95 $
gS.9p
6
(,.l 7S
o
o-t
21�y
� .
3
-- z•zk-i9
AVG-
DUP:
3. -3 z
3S
33
73, LD
10, a5
BENCHSCALE
BENCHSCALE
Avg
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE:
°% Dupficale = Difference in 2 values x 100
Average of 2 values
QC REPORTED: I I
% Recovery = Rgsuft§obtained x 100
Known value
QC RANGE:
CHECKED BY: Ur_
FORM UPDATED: DECEMBER 2017 COPY MADE.

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED: �" '2—/
DATE ANALYZED: ) . ,-?-7 - f c
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
COLLECTED BY:
RECEIVED BY:
ANALYST,
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
� 1
Q 3 O
C
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
%
TOTAL
SOLIDS
VOLATILE
SOLIDS
°!°
RECOVERY
(9)
(g)
(9)
(g)
(g)
(9)
(g)
-A
C - A
(C - DJ
FIE X 100
IG/F7 X 100
AVG
DUP: l Z
g(a3
! I . y 0
S(,
5 9.5
%D= 2�-
BENCHSCALE
6ENCkSCALE
AVc
BENCHSCALE DUP
%D=
QC
'
QC TRUE VALUE: I I QC REPORTED:
% Uupiicate - DifferenCe to 2 vg_lueS x 100 % Recovery = Results obtained x 100
Average of 2 values Known value
QC RANGE:
CHECKED BY:
FORM UPDATED DECEMBER 2017 COPY MADE.

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:_
OVEN TEMP:
BALANCE CK:
METHOD:
-� �� �!
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
O "v� `� 9
c�$ r/ /
°C
OCR . a
ES M 2640 B_E - 2011
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
I-, cc r,I—
�4 O
°C
G
O
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
°
TOTAL
SOLIDS
A
VOLATILE
SOLIDS
%
RECOVERY
(g)
(9)
(9)
(g)
(g)
(g)
(g)
- A
C - A
C - Dj
F/E X 100
G/F X 100
0
2$tS
3
3.8S
7
o�1L
'
S`y . s
raC
? q 323--
33
3
O.
.3 2
.2.0r,v
3 Z
kcXj
AVG �• 9
DUP: �� t_7
c t� I
S5 •Cs`1 W
�� �D �o
�G. L
C�
d.Li3G
(�.Z��I�Q
3 is3
%D- O
BENCHSCALE
BENCHSCALE
wG
BENCHSCALE DUP
%D=
QC
I
j
QC TRUE VALUE: F—
°% Duplicate = Difference in 2 values x 100
Average of 2 values
QC REPORTED:
% Recovery = Results obti!ined x 100
Known value
QC RANGE:
CHECKED BY w
FORM UPDATED DECEMBER 2017 COPY MADE.

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: U 3 -O s — l cj
DATE RECEIVED: 'I- I
DATE ANALYZED: -77 1' t61
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
023->
0��(�
aa�
t °C
tl.ql�Od
«A
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
456b°C
aj,l-I
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
QISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
��
TOTAL
SOUDS
TILE
VOLATILE
SOLIDS
%,
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
A
C- A
C- DJ
IFIE7 X 100
GIF] X 100
r
T Z
0. O3UD
3
V(�.�v7D
�a
o.at��
a
AVG Z
DUP: '� t'�
1�
+4 1514.40
1 a-
6 0 a
u i ��
u 3 (p (a
� %�
r �},
'/ / ��
%D= V
BENCHSCALE
SENCHSCALE
Avc
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: I
% Duplicate = Difference In 2 values x 100
Average of 2 values
FORM UPDATED DECEMBER 2017
QC REPORTED: I I
% Recovery = Rpsuhs obtained x 100
Known value
QC RANGE: I iI
CHECKED BY LA —
COPY
MADE.

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: ` -7—/? TIME COLLECTED:
DATE RECEIVED: 212 TIME RECEIVED:
DATE ANALYZED: r l I TIME STARTED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
0e)1 w'
°C
l `� O
SM 2640 B E .2011
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
pro
°C
u
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
°� TOTAL
SOLIDS
VOLATILE
TILE
SOLIDS
%
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
B- A
C- A
C- DI
IF/Ej X 100
[GIF] X 100
T
o 1 o4
ubat/51
ib( m10
o 7u6
o j"7OQ
4.i
U?V;
1?.D
�7•;7615
�i 00
0 ? 12 0
1 l 1
AVG , J
DUP: r�l
��
d ��
I'7. t��y
I t( 1
LJ"�V
I V
O• �U
%D=
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: I�
% Duplicate - Difference in_2 values x 100
Average of 2 values
FORM UPDATED DECEMBER 2017
QC REPORTED:
% Recovery = Results obtilined x IGO
Known value
QC RANGE: I I
CHECKED BY
COPY MADE

U
CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
J ~ -A- — I S
TIME COLLECTED:
DATE RECEIVED:
3 lS ��
TIME RECEIVED:
DATE ANALYZED:
15. tr
TIME STARTED:
Oct 30
TIME IN OVEN:
TIME OUT OVEN:
OVEN TEMP:
( C °C
OVEN TEMP:
Gp
- C19
BALANCE CK:
t l l
BALANCE CK:
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
10
METHOD: SM 2540 B E • 2011
A I B I C D I E I F I G
De-/ ky
�a-rs
'C
iJ
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
°
TOTAL
SOLIDS
k °
VOLATILE
SOLIDS
%
RECOVERY
(9)
(9)
(9)
(9)
(9)
(9)
(g)
B-A[C-Al
C-DJ
FIE X 100
[GIF] X 100
2
13 -L94
3.4 �3
13.3
5 oo
0, its$
0.094
7L
513-. �
T
g�. g
� 50E38.44-65
5-00
0-icl
0.
I
3.q
OLP
3 a buP
r
. 135
s' L> C)
0 t �i 5�'
D t 04
D
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AVG.3 I
DUP:
%D=
BENCHSCALE
SENCHSCA:E
Avc
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: QC REPORTED:
% Duplicate = Difference in 2 values x 100 % Recovery = Results obtained x 100
Average of 2 values Known value
FORM UPDATED: DECEMBER 2017
QC RANGE:
CHECKED BY. LA -
COPY MADE:

v
CAMP LEJEUNE VWUTP - ATAD SLUDGE SOLIDS ANALYSIS V,-1 5Vu4fi `'�ltc` "''�` e Qr
31z . tq • DES
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
- I y
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
3 IS ��j
3 ' +�
(:)9 0
� 01+ °C
p�
t-L t%
SM 2W B - 2011
677E
Q-1oo
oC\t�"
Hso
L 01i °C
IT Cl
u
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
lei
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
TOTAL
SOLIDS
VOLATILE
TILE
SOLIDS
%
RECOVERY
t91
(g)
(g)
(g)
(g)
(9)
(g}
A
C- A]
[F/Ej X 100
[G/?:7 X 100
.00
p,t66
3- a-
5S 33
T26
8�. t
`�(
�(o.
�1a.1�
5.00
o. kW4
0. I0
V
T36
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1�-�3
.S` 6
-1AAM
c-D
0
0, (-),l
4 4
5T +
F-I—s
��
q-0
V
14• 14
S.ov
0•'�5cl
0.O
c8
AVG
DUP:
%D-
BENCHSCALE
BENCMSCAL£
AVG
BENCHSCALE DUP
%Om
QC
QC TRUE VALUE: I i QC REPORTED: 1 ` 71
% Duplicate = Difference in 2 values x 100 % Recovery = Results obtained x 100
Average of 2 values Known value
FORM UPDATED: DECEMBER 2017
QC RANGE:
CHECKED BY.
COPY MADE

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: 3 • S . } TIME COLLECTED: D O S COLLECTED BY:
DATE RECEIVED: 3 19 ) `i TIME RECEIVED: 0 l d RECEIVED BY:
DATE ANALYZED: 4 Ct l C) TIME STARTED: 0 vC ANALYST:
TIME IN OVEN: o� ZZ- TIME OUT OVEN: l -0' TIME IN FURNACE:
OVEN TEMP: ' �v °C OVEN TEMP: �D`f - (_0°C FURNACE TEMP:
BALANCE CK: oft qci Cl 9 BALANCE CK: CIql t BALANCE CK:
METHOD: SM 2540 B_E - 2011 PERMIT NO. W40012346
n I R CI n E F G
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
/°
TOTAL
SOLIDS
/°
VOLATILE
SOLIDS
%
RECOVERY
(9)
(9)
(9)
(9)
(9)
(9)
(9)
_
B - A
C -A]
(C - of[FIE]
X 100
G/F X 100
oo
o, o
0 t t2-
4.0
5 co
D. l6 3
D CW�,
• 2,(v
c 3�
�� 0.
� • �
1�. �
i ,�{
S . va
o . [
o- 09(v
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50
AVG
DUP: 1' iE>
iS.�34°
D_5
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��� (��
s. L)b
o 1c3(3
O. u 95
Co
53
%D=
BENCHSCALE
er;NcliscALE
AVG
BENCHSCALE DUP
I J
%D=
QC
QC TRUE VALUE:
% Duplicate = Difference in 2 values x 100
Average of 2 values
QC REPORTED: 1 71
% Recovery = Results obtained x 100
Known value
QC RANGE:
CHECKED BY l
FORM UPDATED: OCTOBER 2018 COPY MADE.

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
3 - a/ - 17
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
_
3 9-IS ,
D s
C) t3
(GO3 l o °C
G
�- 1 -l�
SM 2540 B E - 2011
05 aC)
o`-[ L)v
050
l 0 1 a--
\ �3 �p °C
�WJ
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
�S
°C
Rq9
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
D1SH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
�T
TOTAL
SOLIDS
VOLAA TILE
SOLIDS
%
RECOVERY
(9)
(g)
(9)
(9)
(9)
(g)
(9)
A
C- A
(C - D)
JFIE7 X 100
[GIF] X
i- E E ►�
J., t, a33
Tb
00
0 - a51;�
0.161
t Q)
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5 . L�)o
0. 200
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50. GD
is
I?-. 3p(0
-I-, 3 �-
5 OD
0 . *�-o Co
0 10 00
+. (2-
5,3- �
3 ►
WILP
14-. -AVA
5 c)o
0. t-19
e . 001
3• 5-0
49 ,1
AVG: 3. S `'�
DUP:
�J•2
�� �ej
�3-
�. v�
C7 l t30
0. OiOJ�
3. 4 O
BENCHSCALE
9ENCHSCALE
AVG
BENCHSCALE DUP
96D=
QC
QC TRUE VALUE: I i
°% Duplicate - Difference in 2 values x 100
Average of 2 values
QC REPORTED:
°% Recovery - Resufts obtained x 100
Known value
QC RANGE:
CHECKED BY: 1/"
FORM UPDATED: DECEMBER 2017 COPY MADE'

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: 3- 26- lot
DATE DECEIVED:
DATE ANALYZED: 1
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
C)9')-5
gia.9qc1
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
072-0
O-10C�
boa oe,
t t 5L6
1 C 4. SS °C
4tOL •q q'Al t
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
SM 2540 - 2011 U
e R I C n F F G
W LtA-h
,Q!Es
bl::: s 1
(D-00
�J S U 'C
199
U
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
VVT OF
DISH+DRY
SOLIDS
OF
DISH ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(9)
(g)
(9)
(9)
(9)
I9r
B- A
C- A
C- DJ
tF)Ej X 100
G/F X 100
�D
13-111b
?3. q
0• 16'1
0. t00
�,-70
Sa.
;`i
3l0
13 31
s ov
0 ' t10
0.09a'
+D
a-
14,U
1q G3
1410D
1+1M
5. c-,,v
0. tll -
0. 0a2'
� 50
5;,5-7
r
23108
11-3L
I S49
2
-5--DO
0•P50
0-t(Pl
4 tfD
o.w
AVG 133
DUP:'(^2
i� �2l
��-3?'
'��•`i oo
12.4DDT
s vv
O,�Ce�i
O.
%D=
BENCHSCALE
aENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: I` 7�:]
% Duplicate = Difference in 2 values x 100
Average of 2 values
QC REPORTED:
% Recovery = Results obtained x 100
Known value
QC RANGE: F- I
CHECKED BY LA
FORM UPDATED DECEMBER 2017 COPY MADE

V6� warR•i- Wl+h +iL Co I(ec
CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS CGrc- pf 3.1&. ICJ • DES
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED.
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
"- 2$ " ( IF
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
3 Z� ( C�
J 1 5
Oct a5
10 . S °C
Ci9 C� t
SM 2640 B - 2011
ME
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
1P 00
5 sD °C
`,C • IRS
IJ
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
OF
DI Hr+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
8 - A
C - A
[C - DJ
F/E X 100
G/F X 100
Ti
Nv, (b�
0. IlD
0 - LD
3. dD
1
S L3
1�535
60.54
ID31-o
O.ltcg
0.0%-�
(O
ST`?
8� -2Oy3�
I1.04
.f3 -
W,,�
s o0
0 160
0.0`13
-4,,v
5 -b7
•%gyp
J/
��.3�-
SSl 1
s . v(D
0 - )-;�7
0 ' t 5
- S
b. q Lo
AVG.
DUP-.
%D=
BENCHSCALE
HENC•1SCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: F 7:1 OC REPORTED:
% Duplicate = 0192rence in 2 values x 100 % Recovery - Results oblained x 100
Average of 2 values Known value
QC RANGE:
CHECKED BY: W
FORM UPDATED' DECEMBER 2017 COPY MADE:

1 � � , r. ��

Train l Feed
Train 1A
Train 1B
Date
Volume T5o|ids V3o|ids
Temp TSo|ids VSo|ids Feca|[oUhorm
Temp TSo|ids VSo|ids Feca|[oUform
(gal) Y6 Y6
Deg Y6 % (MPN/g)
Deg Y6 % (K8PN/g)
4/1/2019
50.2
51.6
4/2/2019
46.6
46.6
4/3/2019
43.7
45.7
4/4/2019
41.9
46.3
4/5/2019
13'500
33.5
417
4/6/2019
40.6
42J
4/7/2019
47.0
46.6
4/8/2019
50.9
50.6
4/9/2019
53.4
52.9
4/10/2019
SSJ
SlS
4/11/2019
547
52.0
4/12/2019
46.7
48.9
4/13/2019
39.3
41.4
4/14/2019
38.1
39.1
4/15/2019
120'000
34.4
34.4
4/16/2010
29.7
32.8
4/17/2019
33.8
3SJ
4/18/I019
38.0
39.4
4/19/2019
43.4
441
^
Comments
Wednesday, February 5'2U2O Page1ufJ

Train 1 Feed
Train 1A
Train 1B
Date Volume T Solids V Solids
Temp
T Solids V Solids
Fecal Coliform
Temp
T Solids V Solids
Fecal Coliform Comments
(gal) % %
Deg C
% %
(MPN/g)
Deg C
% %
(MPN/g)
4/20/2019
50.1
50.4
4/21/2019
60.2
59.5
4/22/2019
66.9
64.4
4/23/2019
67.1
66.2
4/24/2019
66.0
65.1
4/25/2019 45,000
57.2
60.1
4/26/2019
60.7
60.7
4/27/2019
62.7
60.2
4/28/2019
62.1
60.5
4/29/2019 18,000
60.4
58.6
4/30/2019 23,500
48.1
53.7
No. of Entries 5 0 0
30
0 0
0
30
0 0
0
Total 220,000
Min 13,500
30
33
Geom. Mean 31,464 0 0
48
0 0
0
49
0 0
0
Max' 120,000
67
66
Wednesday, February 5, 2020 Page 2 of 2

Train 2 Feed
Train 2A
Train 26
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp
T Solids V Solids
Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
Deg C
% %
(MPN/g)
4/1/2019
50.2
4/2/2019
46.6
4/2/2019
3.2
0.60
4/3/2019
43.7
4/4/2019
41.9
4/5/2019
45,000
33.5
4/6/2019
40.4
4/7/2019
48.1
4/8/2019
53.0
4/9/2019
55.5
4/9/2019
3.4
1.82
4/9/2019
3.4
1.82
4/10/2019
4/11/2019
4/12/2019
120,000
32.3
44.4
4/13/2019
35.1
40.9
4/14/2019
40.5
44.3
4/15/2019
47.0
49.7
4/16/2019
55.5
58.3
Comments
Wednesday, February 5, 2020 Page 1 of 3

Date
4/17/2019
4/18/2019
4/19/2019
4/20/2019
4/21/2019
4/22/2019
4/22/2019
4/23/2019
4/24/2019
4/25/2019
4/26/2019
4/27/2019
4/28/2019
4/29/2019
4/30/2019
5/7/2019
5/14/2019
6/11/2019
6/18/2019
6/20/2019
6/25/2019
Train 2 Feed
Train 2A
Train 2B
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp
T Solids V Solids
Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
Deg C
% %
(MPN/g)
62.2
65.1
63.9
66.5
9,000
53.6
65.1
57.1
68.1
66.1
70.7
3.6
0.51
60,000
67.6
69.1
66.8
68.8
61.4
54.6
51.1
58.0
50.7
59.1
52.4
59.1
54.9
59.6
55.7
52.7
3.7
0.53
3.7
4.86
3.6
1.02
4.2
4.30
4.0
9.32
3.5
5.10
Comments
Wednesday, February 5, 2020 Page 2 of 3

Train 2 Feed
Date Volume T Solids V Solids
(gal) % %
Train 2A
Temp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g)
Train 2B
Temp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g)
No. of Entries
4 0 0
27
0 0
0 18
10 0
10
Total
234,000
Min
9,000
32
41
3
1
Geom. Mean
41,323 0 0
50 0 0
0 58
4 0
2
Max
120,000
68
71
4
9
Comments
Wednesday, February 5, 2020 Page 3 of 3

ATAD TRAIN 3 QUARTERLY SUMMARY
Train 3 Feed
Train 3A
Train 3B
Date Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp T Solids V Solids Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
Deg C % % (MPN/g)
4/1/2019
49.1
43.5
4/2/2019
48.0
43.4
4/3/2019
47.1
42.7
4/4/2019
47.7
42.7
4/5/2019
45.6
41.3
4/6/2019
46.6
41.3
4/7/2019
46.3
41.0
4/8/2019
45.6
40.8
4/9/2019
45.6
40.6
4/10/2019
44.8
40.2
4/11/2019
44.4
40.1
4/12/2019
44.1
39.5
4/13/2019
43.2
38.9
4/14/2019
41.6
39.1
4/15/2019
40.7
39.1
4/16/2019
40.3
38.3
4/17/2019
4/18/2019
4/19/2019 54,000 29.3
Comments
Wednesday, February 5, 2020 Page 1 of 2

Train 3 Feed
Train 3A
Train 38
Date
Volume
T Solids V Solids
Temp
T Solids V Solids
Fecal Coliform
Temp
T Solids V Solids
fecal Coliform
(gal)
% %
Deg C
% %
(MPN/g)
Deg C
% %
(MPN/g)
4/20/2019
28.3
4/21/2019
29.5
4/22/2019
60,000
29.0
28.8
4/23/2019
28.8
4/24/2019
30.0
31.7
4/25/2019
4/26/2019
4/27/2019
34.2
35.9
4/28/2019
4/29/2019
4/30/2019
23,500
52.1
50.5
5/2/2019
4.4
1.71
6/4/2019
3.4
5.40
No. of Entries
3
0 0
24
0 0
0
20
2 0
2
Tota I
137,500
Min'
23,500
28
29
3
2
Geom. Mean
42,384
0 0
40
0 0
0
40
4 0
3
Max
60,000
52
51
4
5
Comment,,
Wednesday, February 5, 2020 Wage 2 of 2

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
1-1-- Z -- 101
© 7�
w A-1 V-.s,V
SM 9221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO. I W012346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
C4 Z - t lz�
jU22
Enclosure (1
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT ".5 + 0.21C IN INCUBATOR
COMB. OF
MPN INDEX
SAMPLE
POSITIVES
VALUE
MPN / mL'
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
mL
0.10 mL
0.010 mL
0 15
0 l5
15
v 15
O 15
(1
15
15
l5
--�-
0 0
0
(�
`-""
DUP
15
151
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
0.5°C IN INCUBATOR
DATE OUT:
TIME OUT:
TEMP: ?j 5 J -C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
104 irk
'+T- S -Cl
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
MPN / mL' = MPN index Value
Largest Sample Volume
(from comb of positives)
MPN / GRAM2
% TOTAL SOLIDS
MPN/GRAM' = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE
FORM UPDATED OCTOBER 2018

DATE COLLECTED: q 8 q 1
TIME COLLECTED: 0 -7{$
COLLECTED BY: W� S1
METHOD: SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: l R g ) q
TIME RECEIVED: D 17 D
RECEIVED BY: w
PERMIT NO. WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Enclosure (1;
SAMPLE
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN ! mL'
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
Aln)g1rf,
D 15
15
15
15
/5
13 15
"D 15
0 15
-:7
DUP
/5
15
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35+0.5°C IN INCUBATOR
1135
1q4.9 •C
DATE OUT: S 1
TIME OUT: 2j
TEMP: 3 S o •C
i + 0.2'C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
4.9,tli
fj�{ D
f`T • ( •C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROT14
DSA-1BROTH
eos
Nl'
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN ! GRAM'
1.�D
% TOTAL SOLIDS
I.gS
9
MPN/GRAM2 = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY:
COPY MADE:
FORM UPDATED: OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
5M 9221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: C l C'
TIME RECEIVED: 000
RECEIVED BY: ! �S tk/el-
PERMIT NO. WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
4•`i- (Cl
Enclosure (1;
SAMPLE
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN I rnL'
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
J
15
5
5
5
' 5
1 5
d l 5
(/ 15
1 --z^
D o�f p
DUP
l5
cc)15
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
�. q" t 19
l o -3S
3S 0 -Cl
DATE OUT: + • ct . ( 9
TIME OUT: k :J-3S-
TEMP: -35 , d -C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
N
-�L-�
`J -C
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPNIGRAMZ
% TOTAL SOLIDS
MPN/GRAMZ = MPN / mL
% Total Solids
(expressed as a dearnal)
CHECKED BY
LA -
COPY MADE
FORM UPDATED OCTOBER 2018

DATE COLLECTED: V 11k _ ( '—
TIME COLLECTED: o f 3
COLLECTED BY: 1 k e
METHOD: SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: i1 la
TIME RECEIVED:
RECEIVED BY:S
PERMIT NO. WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:��j
Enclosure (1)
SAMPLE
LOCATION
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN ! mL'
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 rnL
[
O 15
0 5
O F5
"` 5
(5
G 15
O 15
O
i5
0-0-0
G D-t,5
.O1bo
DUP
� i5
5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS Al 3b + U,
�. as 1
36- o
5°C IN INCUBATOR
rci
DATE OUT:
TIME OUT:
TEMP:
+. aa. l9
l2
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
4-z3, iR
to0o
4zF- 4 •C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
C k,�
MPN ! ml- = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN/GRAM'
0.5
% TOTAL SOLIDS
MPN/GRAM' - MPN , mL
% Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE
I.ORM UPDATED OCIOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
w1 Lars
r SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: + ;z6 , ( a
TIME RECEIVED: 0e4'
RECEIVED BY: )�Ies
PERMIT NO. W012346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
. 25. 1 "I
o 1� coo
Enclosure (1)
SAMPLE
LOCATION
3 HRS AT 35 + 0 5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN t mL
10 mL
1 mL
0.10 mL
0.010 mL
1f 0 mL
1 mL
0.10 mL
0.010 mL
Q 15
15
O 15
/5
15
15
, l5
O 15
!�
0. Ji
DUP
V /5
O /5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 MUUKJ A 1 J,
419
1 O`At0
�5• D •c
0.5"C IN INCUBATOR
DATE OUT:
TIME OUT:
TEMP:
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
.4.2-(-,. t9
�°I o2s
•C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
MPN / ml-' = MPN Index Value
Largest Sample Volume
(IFOFn comb of positives)
MPNIGRAMZ
% TOTAL SOLIDS
�. t0)
MPNIGRAM2 = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE
I ORM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
L -36-n
v -7
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: �� [ci
TIME RECEIVED: b`"(rQ
RECEIVED BY: I'FS
PERMIT NO. WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Enclosure (1)
'+-:�;o- 19
3 HR5 AT 35 + 0 S°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB, OF
MPN INDEX
MPN / mL'
SAMPLE
POSITIVES
VALUE
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
Tt6
0 15
O 15
15
5
O 15
15
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
HCIIJRS AT 35 + 0.5'C IN INCUBATOR
-3c)- k
MOO
l OO
DATE OUT:
TIME OUT:
TEMP:
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
Pcz
C-
i
.0
c °C
MPN 1 mL - MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN I GRAMZ
% TOTAL SOLIDS
ot17
MPN/GRAM'- MPN J mL
% Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE
FORM UPDATED OC70817R 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
0-6
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO. I WQ12346
DATE ANALYZED
TIME ANALYZED:
ANALYZED BY:
,5- 2. I-\
o e -{-S-
Enclosure (1)
SAMPLE
LOCATION
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN / mL'
10 mL
1 mL
0.10 mL
0.010 mL
1{0�}mL
1 mL
O.iO mL
0.010 mL
15
0 15
0 15
CD5
`' 15
r5
15
C �5
DUP
r5
1
1 r5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
5. 19
p1�0
3'S-C7 .0
DATE OUT:
TIME OUT: l o�-
TEMP: 35 ' °C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
MPN mL MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN 1 GRAMZ
% TOTAL SOLIDS
MPNIGRAM- - MPN r mL
% Total Solids
(expressed as a decrmat)
CHECKED BY
COPY MADE
\'3
I OHM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
o5 -co -1
o -? l c�
1►� 4 wY
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: S. -7. 11
TIME RECEIVED: 0-7 3 7]
RECEIVED BY:
PERMIT NO. WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
5--7- 1`,
D-IL!`)
LA-
Enclosure (1)
SAMPLE
3 HRS AT 35 + 0 5`C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2-C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN / mL=
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 imL
0.10 mL
0.010 mL
t5
D 15
5
;5
15
5
a5
0:�-0
DUP
01511
r5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
-C
DATE OUT:
TIME OUT:
TEMP:
S -1- 1 1
35_0 -C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
5 .1 - 11 DATE OUT: S 911
I to a-- TIME OUT: b`1 Lt 3
-I q' -1 ^C TEMP: -f Lf . S •C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
f
`.,�
J _
DS A-1 BROTH
f
d
I-ORM UPDATED OCTOBER 201E
MPN, ml- = MPN Index Value
Largest Sample Volume
(frorn comb of positives)
MPN I GRAM2
0,53
% TOTAL SOLIDS
J .74
MPNIGRAM- MPN r mL
% Total Solids
(expressed as a decimal)
CHECKED BY
U
COPY MADE

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD.
5-N-19
01 Zr)
f.4f
SM 9221C E-2006
MCS CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED: 0
RECEIVED BY:
PERMIT NO. W012346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
0797
Enclosure (1
SAMPLE
LOCATION
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN J mL'
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
I �iD
0 15
;5
d ;5
0 5
5
15
0 15
O 15
-p- D
�Q-lS03
CD.Igb?3
DUP
�D 1151
D ; 5
1
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
I HnI IRR AT 35 + 0.5°C IN INCUBATOR
5. ►y
0519
3S _ f •�
DATE OUT:
TIME OUT:
TEMP:
�120
3s j °c
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
5"
0 `I Lq a
L,11 6' I
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
N
DS A-1 BROTH
pi
MPN I mL' = MPN Index Value
Largest Sample Volume
(frorneomb of positives)
MPN 1 GRAMZ
% TOTAL SOLIDS
-
( 1
MPNIGRAM` = MPN I mL
% Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE
I'ORM UPDA1*E0 OCTOBCR 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
2�
SM 9221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: q I q
TIME RECEIVED: 08 3S
RECEIVED BY:
PERMIT NO. W012346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Enclosure (1
SAMPLE
LOCATION
3 HRS AT 35 + 0.5'C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN I mL'
10 mL
1 mL
0.10 mL
0.010 mL
10 rnL
1 mL
0.10 mL
D.OiO mL
15
o.-(D-o
'-d .L$C)3
<0 .1 g o 3
►�
apiaA
DUP
5
+5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5'C IN INCUBATOR
DATE OUT: t1 4 11
TIME OUT: 1 Z- D
TEMP: 3 S O 'C
0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
C0 - s- �g
O S-
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
�1
N
DS A-1 BROTH
MPN I mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPNIGRAM2
LS,
TOTAL SOLIDS
3.35
MPNIGRAM' = MPN I mL
% Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE
FORM UPDA110 OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
06-1 �- 0
7.3 0
QV
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: , I _ + I
TIME RECEIVED: 17 3 S
RECEIVED BY:
PERMIT NO. W012346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
(,o l 1-19
vqu,�-
tD. Q S
Enclosure (i'
SAMPLE
3 HRS AT 35 + 0.50C IN INCUBATOR
21+2 HRS AT 44.5 + 0,2•C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN I mL'
LOCATION
1l!0��mL
1 mL
0.10 mL
0,010 mL
10 mL
1 mL
0.10 mL
0.,001�0 mL
V /5
v /5
V r�
5
D 5
2- t5
U 5
(/ '5
DUP
v l5
C 15
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5'C IN INCUBATOR
{0—N�-\q
3 S. 0 -Cl
DATE OUT:
TIME OUT:
TEMP:
35.0 •C
21 + 2 HOURS AT 44.5 + 0.2"C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
N
N
DS A-1 BROTH
YJ
•C
MPN / mL MPN Index Value
Largest Sample Volume
(from comb of positives)
MPNtGRAMZ
% TOTAL SOLIDS
MPN/GRAM` -- MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE
DORM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
-/ F-f
D7S0
WA-1 Kw
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO. W012346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
& 19 1 `�
V-7S-i
L,'t- .ix-s'
Enclosure (1
SAMPLE
3 HRS AT 35 + 0.5'C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN ! mL'
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
2 2—
/5
/5
/5
LJ /5
v /5
/5
D 115
15,l^o-
V
1� V Zy't1
th 4-vil, �
DUP
0 /5
O 151
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
6-1B8 11
oS�s
•C
DATE OUT: Ls? - lF " I
TIME OUT: i 2
TEMP: 3 S 6 'C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
y - k%-\a) DATE OUT:
1lZ 1 TIME OUT: ozz
S -C1 TEMP: H q . J -C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
MPN / mL1 = MPN Index Value
Largest Sample Volume
(from comb of positives)
MP,,NJJ 1 GRAM'
'1 • 3t3
to V zy•i't
% TOTAL SOLIDS
f \ 1
MPN/GRAM' = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE
w
FORM UPDATED. OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
0�-ao—aoJ�
o -7 J S-
�U10
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED -
TIME RECEIVED:
RECEIVED BY: 2S
PERMIT NO. WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
(0`-�)
D2S
Enclosure (
SAMPLE
LOCATION
3 HRS AT 35 + 0 5"C IN INCUBATOR
21+2 HRS AT 44.6 + 0.2'C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN 1 mL'
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
-ra6
O /5
0 /5
/5
/5
D /5
f5
15
G 15
r� Z-cD
V �
3.-7
0,Z—T
DUP
150-
1
�/ j� / 5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
- Zo- (9
DATE OUT: 2-0. i 1
TIME OUT: 1 40�
TEMP: 3s 'C
91 + 2 HOURS AT 44.5 + 0.1°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
P
N
Q
DS A-1 BROTH
v-1 q
•C
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN/GRAM'
% TOTAL SOLIDS
MPN/GRAM = MPN / mL
CHECKED BY
COPY MADE
% Total Solids
(expressed as a decurnal)
U
FORM UPDATED OC IOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
oG -a s ao q
o'7 35
SM 9221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY: (,y,Ei
PERMIT NO. W012346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
�. zs.
� -7
Enclosure (
SAMPLE
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN / mL'
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
7
/5
/5
l5
l5
a fD
DUP
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
a nuuna H I Ja
d'b1D3
3 S. -c
0.5°C IN INCUBATOR
DATE OUT: a
TIME OUT: 1 a 3
TEMP: "C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
,DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
1j�
pf
DS A-1 BROTH
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN / GRAM2
% TOTAL SOLIDS
3.5 3
MPN/GRAM' = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE -
FORM UPDATED' OCTOBER 2018

DATE COLLECTED:
DATE RECEIVED: `'• - t
DATE ANALYZED: �•
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
i
A I B I C I D I E I F I G
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CI(:
m
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
%
TOTAL
SOLIDS
%
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(9)
(g)
(g)
(g)
(g)
- A
Ic - A
(C - DJ
F/E X 100
t2E X 100
5,0o
0. HD
o. to
3. 30
6r3. t U
L DO
'90•311
It -
6.
®. Nga-
-5.
13.
3.4
9�U3
0 . t'l i
. ��
US. 0
AVG. I
DUP: f%-ev
-NP-
.1
5 . 0
15�3
®. ®e)
yy
BENCHSCALE
BENCHSCALE
BENCHSCALE
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE; I i QC REPORTED:
% Duplicate = Difference In 2 values x 100 % Recovery = Resub obtained ' x 100
Average of 2 values Known value
QC RANGE:
CHECKED BY: W
FORM UPDATED: DECEMBER 2017 COPY MADE.

DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CIS:
METHOD:
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
1
U
�' l
®�`� �
t °C
etq • gclq
Sift 2W B_ 2011
LIU
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK: -
A 1 a 1 r_ 1 n I P I G I G
u
LOCATJOCATION
1PlT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
Wf OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
o�
TOTAL
SOLIDS
A
VOLA
SOLIDSTILE
%
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
-
IC - A
C - DJ
FIE X 100
fGIFI X 100
oo
09
.il
.D31
-5
u• ISO
0.05
3, i is
5, I Lp
AVG,
DUP:
%D=
BENCHSCALE
BENCHSCALE
AVQ
BENCHSCALE DUP
%D=
!aC
QC TRUE VALUE: F
% Duplicate - Difference In 2 values x 100
Average of 2 values
FORM UPDATED' DECEMBER 2017
QC REPORTED: QC RANGE:
% Recovery = Results obtained x 100
Known value ���L �• v0� t tt�- I7
Vn Woc1�s1� W i n
5� S
CHECKED BY;
COPY MADE.

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS, ANALYSIS
DATE COLLECTED: �{. t3. I`I TIME COLLECTED: 0-7L15' COLLECTED BY:
DATE RECEIVED: L1, Q. )61 TIME RECEIVED: 091D0 RECEIVED BY:
DATE ANALYZED: � % - m TIME STARTED: 0 $ O ANALYST:
TIME IN OVEN: 08 4 (p TIME OUT OVEN: 10 N (p TIME IN FURNACE:
OVEN TEMP: I 0 Li. L{ °C OVEN TEMP: I 0 °C FURNACE TEMP:
BALANCE CK: DO • O g BALANCE CK: a g BALANCE CK:
METHOD: SM 2540 B_E - 2011 PERMIT NO. WQ0012346
A B C D E F G
Wi r! �Mary,.s
Ua'
5SD °C
qR-999Y g
WT OF
WT OF
WT OF
SAMPLE
TOTAL
VOLATILE
WT OF DISH
DISH+WET
DISH+DRY
DISH+ASH
WEIGHT
SOLIDS
SOLIDS
TOTAL
VOLATILE
%
SAMPLE
SOLIDS
SOLIDS
WEIGHT
WEIGHT
SOLIDS
SOLIDS
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
LOCATION
-
_
-• _-
:±-
- AC
- A
(C - DJ
[FIE] X i00
G/F X 1 00
-73 a 5o
3 0
-7y Ll I -T
311
S- 00
0. 09 a tv
0.1) 4 � (
S Sqj.7
-
AVG:
DuP: f�tY�p �rr�
Z .�9
�$ .30
�3. 3811
7& 3403
S pO
0.01 L(
0.1)468
%D= v' 5 .
BENCHSCALE
BENCHSCALE
AVG:
BENCHSCALE DUP
%D=�
ri;... Vi
QC
QC TRUE VALUE:
% Duplicate = Difference in 2 values x 100
Average of 2 values
QC REPORTED:
% Recovery = Results obtained x 100
Known value
QC RANGE:
CHECKED BY:
FORM UPDATED: OCTOBER 2016 COPY MADE:

DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CI(:
C "v (—
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
- J' -4 +
4• I l
°C
R94
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
METHOD: SM 2640 B_E - 2011
A B C D E F G
0 V
0-1 cX3
toil
(0 1. °C
W
SSC� °c
9�t . C'M 9
LWJ
WT OF DISH
WT OF
DISH+WET
WT OF
DISH+DRY
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
®
TOTWEIGHT TOTAL
T
A
VOLATILE
%
SAMPLE
LOCATION
SOLIDS
SOLIDS
SOLIDS
SOLIDS
RECOVERY
(g)
(g)
(9)
(9)
(9)
(9)
(g)
B - A
C-A
C - DJ
F X100
fGIF1 X100
•5, L-)o
o.
0• oqt
v.
53
0q3
3. :�
55•10
--
i�
1R-0
1�.1�
10�1
s.00
D- 61
0 . b5i-�.
14
1153-so
AVG: 3.3
DUPum OD 56 Q-
7 i�
i3.1'i3
3 D3
5 .o
0 . t (.p
o . o �3
3.3 Cv
5S 3
%D=
BENCHSCALE
AVG
BENCHSCALE
BENCHSCALE DUP
%D=
I
QC
-:J
QC TRUE VALUE:
% Duplicate = Difference in 2 values x 100
Average of 2 values
QC REPORTED:
% Recovery = Resufts obtained x 100
Known value
QC RANGE: I
CHECKED BY:
COPY MADE. _
FORM UPDATED: DECEMBER 2017

i4Ci/1 rloit : ur�t •�---zL � � �...-.._ t _.... _ . .
-i1^� W vrK5b�a L-� w i.A 4lax.
CAMP LEJEUNE WWTP - ATA® SLUDGE SOLIDS ANALYSIS vF 4, q 19 .
-�45
DATE COLLECTED:
DATE )RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
W `I 1 —1 j
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
+ tj
+(Z..
` 2-• el
®� "
1 '� . °C
�1. Ct
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
METHOD: SM 2640 B E - 201
A I B I C D E F G
01 Clyj
0-g1'�-
t0ao
i D3 - C-P
okI
°C
RA
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+VWET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
a� TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
-,4
C - A
C - DJ
/1= X 100
[GVFI X 100'
53-51
3 tS
A3)-S0
-IS-3,3
14-4,01
s, co
o 16', -
0.0
4Lo
D • l
t
AVG
DUP:
%D=
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE:
°% Duplicate = Difference in 2 values x 100
Average of 2 values
QC REPORTED:
°% Recovery = 8e8Ul1S obtained x 100
Known value
QC RANGE:
CHECKED BY
FORM UPDATED: DECEMBER 2017 COPY MADE.

CAMP
LEJEUNE r'P a. t SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
- 2,,3 - 17
I➢UIE COLLECTED:
DATE RECEIVED:
4 • 2- G • x c1
TIME RECEIVED:
DATE ANALYZED;
42 Cv •
TIME STARTED:
TIME IN OVEN:
I v
TIME OUT OVEN:
OVEN TEMP:
°C
OVEN TEMP:
BALANCE CK,L
1. qat Iq S Ck
BALANCE CK:
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
METHOD: 5M 2640 B_E - h1l
B `7 7
d9f5
a�3v
t� (31
t o4 - 1 4C
t� . a1915
SAMPLE r
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
VIIT OF
DISH+DRY
SOLIDS
WT OF
DI +ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(9)
(g)
(g)
(9)
(g)
(g)
(9)
B- A
C- A
F1EJX100
EE X 100
s. o
0 •:2-+u
-0 .
4.1 a-
( 5• 9S-
FQ,
6B. 6116
IS US-
a a
96,1546
5-0
0. 251
0. 1'l0
5. 11j-
. lC
3. .,
s o
a -1
0. opt
(p
55• ©Cp
AVG
DUP: -t-�-t3
-t� lQ3
��.$OS1
• 10$
�. o
o.n. 3
0.010
3.s(0
55 DCv
AD= D
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
�D=
QC
QC TRUE VALUE:
% Duplicate - Difference in 2 values x 100
Average of 2 values
FORM UPDATED: DECEMBER 2017
QC REPORTED:
% Recovery = Results obtained x 100
Known value
QC RANGE: -
CHECKED BY' V
COPY MADE.

DAMP LEJEUNE UWVTP '- ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
.�Z S —
TIME COLLECTED.
DATE RECEIVED:
Q
4.2c., I t
TIME RECEIVED:
DATE ANALYZED:
4. Z c. - k
TIME STARTED:
TIME IN OVEN:
3
TIME OUT OVEN:
OVEN TEMP:
( °C
OVEN TEMP:
BALANCE CK:
BALANCE CK:
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
METHOD: SM 2640 BE - 2011
e I a I C I n 1 F P G
�J
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
`SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
®�'
TOTAL
SOLIDS
%
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(g)
(9)
(g)
(g)
(g)
B- A
C- A
C- DI
[FIE X 100
G/F X 100
T►g
a.3��
'i't. 3�-
I)-. So9S
�Ao3(n
s. a
o - 01
D. IOLP
3:-74-
.b3
0. 24o
o t
4. D
� S� D
©�-11
0 . Sg
s
AVG:
DUP:
1-'5tDD
10-7
%D=
BENCHSCALE
BENCHSCALE
AW
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: f
% Duplicate = Difference In 2 values x 106
Average of 2 values
FORM UPDATED: DECEMBER 2017
QC REPORTED:
% Recovery = .Resulls obtained x 100
Known value
QC RANGE:
CHECKED BY:
COPY MADE:

DATE COLLECTED: 'i -3 J- t t
DATE RECEIVED: 5 3 {
DATE ANALYZED: �� {
TIME IN OVEN: Oct 00
OVEN TEMP: t b+ - 0 ®C
BALANCE CK: tcl - L 1915
METHOD: SlUI 2Sd0 B E - 2011
ANALYSIS
BY:
TIME COLLECTED:
L)
COLLECTED
TIME RECEIVED:
v 1 i]o
RECEIVED BY:
TIME STARTED:
� o8 2S
ANALYST:
TIME OUT OVEN:
i \ ®c>
TIME IN FURNACE:
OVEN TEMP:
O 'C
FURNACE TEMP:
BALANCE CK:
R��
BALANCE CK:
{- r
WW E. Sam
@anW E. 5m�
D
550 eC
i qq
u
SAMPLE
q
ITT OF DISH
o
WT OF
DISH+WET
IdsrT OF
DISH+DRY
�ii' A
DISH+ASH
WEIGHT
t JE1GHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
®T
TOTAL
VOLATILE
A
%
RECOVERY
LOCATION
SOURS
SOLIDS
SOLIDS
SOLIDS
(g)
(g)
(9)
(g)
(g)
(g)
(9)
- A
C - A
(C - 01
FIE X 100
G/F X 100
i t a �
�`� t��
�9 3
"l�. 02�3
14' 11S1�
5
o - La(o
D - I 03-
pi
09�t�5�3
�t3-c�S
3
2- a
o. �-31
o- [51
4
AVG:
DUP: -T l t?�
�. 3�?8
'l'1 3
'1�.5 ���
'1? �i�
s -
u ���
o I l v
3.
%D= t
SENCMSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D
QC
QC TRUE VALUE: QC REPORTED:
% Duplicate - Difference In 2 v lues x 100 % Recovery = Results obtained x 100
Average of 2 values Known value
QC RANGE: I !
CHECKED BY: _ IK
FORM UPDATED: DECEMBER 2017 COPY MADE:

DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED: S 3 lai
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
4otW
t o C7 °C
SM2640B E-2011
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
13ALANCE CK:
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
( V, "—
Daw E• gmosglvef
Wei E. 5a i sgiber
1?-oo
550 C
9-
SAMPLEPLI;
LOCATION
WT OF DISH
bVT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
�T
TOTAL
SOLIDS
A
VOLATILE.
SOLIDS
%
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
LB- A
C-�j}A/,{�
(C -
F/E XX 100
G/F X 100
P�
/7 5
t
+r� ' I
' ^
1p+J]
�, S
-L?,. 3
I, • ab
o ' I i t
3. q2-
51� • �3
-r 3 6
13. E-aU
�6. 30
13,515i
5.0
0. 219
0 - t30
4.30
51- -Z�
Er,
25-�
�'�
tS`�bp��
�S�la
s
d•glgt.P
0.
0-ct I
AVG: E
DUP: �3 g
?
7
�� j
"
�"; t(�
C '� l t
5 p
D a ��
r^�
D • �V
�'��
q
S� ' t
°/.D= l
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: QC REPORTED:
% Duplicate = Ottference fn 2 values x 100 % Recovery = Results obtained x 100
Average of 2 values Known value
QC RANGE: I
CHECKED BY: LA
FORM UPDATED: OECEMBER 2017 COPY MADE'

CAMP LEJEUNE WWTP - ATA® SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
0-7- 1,
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
Je� ' l`
" ^ '� - 1 `�
f`'i I
°C
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
METHOD: SM 2540 B_E - 2011
A B C" D E F G
09z)o
°C
SAIIAPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHTWEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
WEIGHT
%A
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(9)
(9)
(9)
(9)
d9)
JB -A
C - A
C-DJ
tffg x100
j2E x100
t l�
qS8
G1 co
3310
`gC�.a3g3
5,0�42c�
53.-IC)
i z6 CCrc<<qLi.,3L2U
-79 33
sl
-7q.Lit23
c.co D
v. %
09$
3.La3.3a
a
3.c�r7
,cEZ
o3�0
©
2
,1238
5. 03255
D 2 N y 3
. I s-d o
q. C6- Z
AVG:
DUP: 28
(n2s'S
-79,
S.o0J
D. kc�00
U.lo3S
3.�?�
Sy.
%D= 3
BENCHSCALE
BENCHSCALE
Avc
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE:
% Duplicate = Difference in 2 values x 100
Average of 2 values
QC REPORTED:
% Recovery = Resufts obtained x 100
Known value
QC RANGE:
CHECKED BY: W
FORM UPDATED' DECEMBER 2017 COPY MADE:

CAMP LEJEUNE WWrP - ATAD SLUDGE SOLIDS ANALYSIS
5'�r
DATE COLLECTED:
(R
TIME COLLECTED.
DATE RECEIVED:
S . l 3, l
TIME RECEIVED,
DATE ANALYZED:
(3 ��
TIME STARTED:
�
TIME OUT OVEN:
TIME IN OVEN:
OVEN TEMP:
i0 °C
OVEN TEMP:
BALANCE CK:
too . 0O
BALANCE CK:
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
METHOD: SM 2640 B E - 2E:1
., I r% I IaI t;
(r} �10 0
0 —i COC)
C��OU
°C
lOC)-� 2
V
SAMPLE
LOCATION
n
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+A SH
SAMPLE
WEIGHT
TOTAL
TOTAL
WEIGHT
VOLATILE
SOLIDS
WEIGHT
®/°
TOTAL
SOLIDS
°�
VOLATILE
SOLIDS
%
RECOVERY
(9)
(9)
(9)
(9)
(8)
(9)
(9)
- A
C - A
jC - D]
EU1.XL100
_[GIFI X 100
s. o
o TAS
o . t o
ee, 11L
S. o
OJ6 t
0.C)(�a-
3 a�
5�•
-rs�
5p,039a'
9).0+
36-93
6(.1�3
S o
b. [
o•t(D
5G.10
-Rip
ee.GG 0
`�'
5 C-)
0-)-[
AVG
DUP: `�tC�
is �
7�t 3
b
1� "1t7S�
S- a
l �l
o. t v
3 S
5�1 0
BENCHSCALE
BENCHSCALE
Avc
BENCHSCALE DUP
CIC
QC TRUE VALUE:
% Duplicate = Difference in 2 values x 100
Average of 2 values
FORM UPDATED: DECEMBER 2017
QC REPORTED:
% Recovery = Resutts obtained x 100
Known value
QC RANGE:
CHECKED BY:
COPY MADE.

DATE COLLECTED: 5-1{ - !
DATE RECEIVED: I
DATE ANALYZED: )I -_-
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
O83a
°C
SM 26401 - 2011
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
a7�5
p`Z 3D
0 °C
I R
:J
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
H
WT OF DISH
sa
WT OF
DISH+WET
WT OF
DISH+DRY
T OF
DISH+ASH
EIGHTMPLE
WEIGHT
W
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
T
TOTAL
��°
VOLATILE
SAMPLE
SOLIDS
SOLIDS
WEIGHT
WEIGHT
SOLIDS
SOLIDS
RECOVERY
(g)
(g)
(g)
(9)
(g)
(g)
(g)
LOCATION
B - A
C - A
fC -Dj
TFIQ X 100
fGIFI X 100
TI$
�i`f.3a.�3
-71-31
"i` .Sa37
-74 5-1
S.Do
o.l9lq
0-ItiBa
3.g5-
55 .
Z
80-s�
-(S7.1a3s
-�s.(�ay9
5.0'D
0.119s4
0.og8(D
3.`ll
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-7,30
1a_E�x
a.39(�3
Soo
b, a o I 1
0.123
AVG, ! A
DUP: o
a a
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE:
°% Duplicate = Difference In 2 values x 100
Average of 2 values
QC REPORTED:
% Recovery = Results obtained x 100
Known value
QC RANGE: L I
CHECKED BY:
ft-
FORM UPDATED: DECEMBER 2017 COPY MADE.

CAMP LEJEUNE WWrP - AiAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: U — / C(
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
0,jz z
°c
SM 25An B E 2091
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OMEN TEMP:
BALANCE CK:
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
SAMPLE
LOCATION
i 1T OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
SOLIDS
VOLATILE
SOLIDS
WEIGHT
°k
TOTAL
SOLIDS
°,6
VOLATILE
SOLIDS
°
/e
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
B- A
C- A
C- DJ
F/E X 100
GIF X 100
T
35
�3 .tl
8. S�?�
$. `t3�?
3
.
5191,0
. lt��Q2aQ
9
�.
�7 Bl
"T , ?2Lo
S.oLjol
0. 6%-7
qZ-5
.oZ
q 1 • ^?
b ,%'
. -m
�S . 0L,
-a-
9
S • Lo
AVG
DUP:
U • ocoo
I
�CQ • `�
J'3 z--
5.0%95o
. 2Fs 92-
0 (x
S -LoS
6 .88S
%D= 1
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: �y
% Duplicate - Difference in 2 values x 100
Average of 2 values
FORM UPDATED: DECEMBER 2017
OC DEPORTED:
% Recovery = Results g¢igfned x 1 DO
Known value
QC RANGE:
CHECKED BY.
tffi—
COPY MADE:

DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED;
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
06-Or! `f49O% 9
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
L
b • i - I I I
� - S " l`�
$
Q
3 ) °C
Q .
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
METHOD: SM 25a g E - 2011
A I B I C D E F G
08 33
DD
1c�3z.
�U 3 °C
SAMPLE
LOCATION
WT OF DISH
WT Of
DISH+WET
SOUDS
WT OF
DISK+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
TOTAL
SOLDDS
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
- AlC
- A
C - DJ
FIE X 100
[GIF] X 100
T (
2.32
3'. oC
-72 . 93
S 1 Uq
tj.?c--9)
0 TZ
3 . Lij
5 4,0-2-
z-
0J2
Li D
38 . W�r
5.CCo
2
r-CciA
See-
C-C,
AVG S• 4�
DUP: �2-~
S.
O.
85.4Syc)
�t
IS S
%D= 1
BENCHSCALE
BENCHSCALE
Avc
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: I
°h Duplicate = Difference In 2 values x 100
Average of 2 values
FORM UPDATED: DECEMBER 2017
QC REPORTED:
% Recovery = Resufts obtained x 100
Known value
QC RANGE: I�
CHECKED BY LW
COPY MADE.

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: tp - i TIME COLLECTED: D 3 S COLLECTED BY:
DATE RECEIVED: TIME RECEIVED: `� O D RECEIVED BY:
DATE ANALYZED: TIME STARTED: 09 DD J ANALYST:
TIME IN OVEN: O q D -1 TIME OUT OVEN: 11 0-7 TIME IN FURNACE:
OVEN TEMP: I D 3 • S °C OVEN TEMP: I C 3 - °C FURNACE TEMP:
BALANCE CK: OD . '6 91 BALANCE CK: 9 R - y9 q `t g BALANCE CK:
METHOD: SM 2540 B_E - 2011 PERMIT NO. WQ0012346
A B C D E F G
WT OF
'WT OF
WT OF
SAMPLE
TOTAL
VOLATILE
°
/°
SAMPLE
WT OF DISH
DISH+WET
SOLIDS
DISH+DRY
SOLIDS
DISH+ASH
WEIGHT
SOLIDS
WEIGHT
SOLIDS
WEIGHT
TOTAL
TILE
VOLATILE
%
RECOVERY
LOCATION
SOLIDS
(9)
(9)
(9)
(g)
(g)
(g)
(g)
-A]
(C-AZ
[C-Dj
F/E] X 100
G X 100
7`3$ CFe
88,��
3
�8 gl
88.�3o`t
S.o 3
_ 4
777 �t i
AVG. 3, 3 5
DUP: T'
. �00
` C 33
36-5°��
Si�
`i
0,1641
0.08(,8
%D= 0.3
BENCHSCALE
BENCHSCALE
AVG:
BENCHSCALE DUP
%D=
_
QC
QC TRUE VALUE:
% Duplicate = Difference in 2 values x 100
Average of 2 values
FORM UPDATED: OCTOBER 2018
QC REPORTED:
% Recovery = Results obtained x 100
Known value
QC RANGE:
CHECKED BY.
COPY MADE:

DATE COLLECTED: Ot O G
DATE RECEIVED: (� '► - Lc�
DATE ANALYZED: "1c
TIME IN OVEN:
OVEN TEMP:
BALANCE CIS:
METHOD:
t 3, G °C
SM 2540 B E - 2011
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
0g00
O$z-o
U$�
1c) 33
G 3. mC
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CIS:
(, 6 e- r_4_iC
EaS
C)
TJ 'C
(oc-) U1
r.�
SAMPLE
LOCATION
VYf OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
�T OF
DISH}ASH
WEIGSAMPHT
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
®T
TOTAL
SOLIDS
A
V SOLIDS
SOLIDS
%
RECOVERY
RECOVERY
(g)
(g)
(g)
(g)
(g)
t91
(9)
- A
C - A
jC - DJ
[FIFJ X 100
[GITX i0O
/=era(
�3F2
�O. CQZ
7S.
7S,G,Z-?S
6751'i(
sltg
d. 16 Z3
H gS
-5
,3ZZ3
�7 Sz-
Z_scx��,
. f9'i
3.sS
53, U�
2
73.29;
Z�3.3og
S.ot.
<�
) ,09
3,S
� 3
7 '!zU
`q.-7q
.YQZ3
n23
o,vga
s2. o
AVG S . 0
DUP:2.3
f`?12
'7.3 S
"t 2 . �1 C9
^t 2 , . p� g
S v 30g
. ZS
D . `6
S�$
96D= 3
BENCHSCALE
9ENCHSCALE
AVG
BENCHSCALE DUP
%D=
t�C
QC TRUE VALUE: QC REPORTED: 7771
% Duplicate = Dif(grano in 2 values x 100 % Recovery - Results obtained x 100
Average of 2 values Known value
QC RANGE:
CHECKED BY: �f_
FORM UPDATED: DECEMBER 20W COPY MADE:

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: f I " o? 0 / S TIME COLLECTED: 0 �-3 0 COLLECTED BY:
DATE RECEIVED: tp • 0- I ck TIME RECEIVED: Q -7 `l S` RECEIVED BY:
DATE ANALYZED: Io -e S t ', TIME STARTED: 01 I ANALYST:
TIME IN OVEN: d t Z D TIME OUT OVEN: (1 20 TIME IN FURNACE:
OVEN TEMP: I o 3• 9 °C OVEN TEMP: I DN °C FURNACE TEMP:
BALANCE CK: 1 uD o g BALANCE CK: 1 D0 • o b o l g BALANCE CK:
METHOD: SM 2540 B E - 201T:1
PERMIT NO. F77W00012346
A I B I C I D I E I F G
WT OF
WT OF
TOTAL
VOLATILE
WT OF DISH
DISH+WET
DISH+DRY
WT OF
SAMPLE
SOLIDS
%
%SAMPLE
SOLIDS
SOLIDS
DISH+ASH
WEIGHT
WEIGHT
.SOLIDS
WEIGHT
TOTAL
VOLATILE
RECOVERY
LOCATION
SOLIDS
SOLIDS
(g)
(g)
(g)
(g)
(g)
(g)
B - A
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QC RANGE:
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FORM UPDATED' OCTOBER 2018 COPY MADE.

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: / % TIME COLLECTED: D % S() COLLECTED BY:
DATE RECEIVED: /I�g ^ i3` t 9 TIME RECEIVED: !!O �5' � RECEIVED BY:
DATE ANALYZED: l� ��3 l� V TIME STARTED: V-\ ANALYST:
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BALANCE CK: QCD , BALANCE CK: Ov 1 BALANCE CK:
METHOD: SM 2540 B_E - 2011 PERMIT NO. WQ0012346
n I R I G I D E I F G
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FORM UPDATED: OCTOBER 2018 COPY MADE:

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: - I - f c TIME COLLECTED: U 7 yS COLLECTED BY: W ev
DATE RECEIVED: f $ ! 1 TIME RECEIVED: Q RECEIVED BY:
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FORM UPDATED: OCTOBER 2018 COPY MADE

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: -,;? v 1 9 TIME COLLECTED: C) 7 30 COLLECTED BY:
DATE RECEIVED: /U" Z �" 1 `''1 TIME RECEIVED: <�O C, RECEIVED BY:
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METHOD: SM 2540 B_E - 2011 PERMIT NO. W00012346
A I B C I D E I F G
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LOCATION
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WT OF
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WEIGHT
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QC RANGE:
CHECKED BY
FORM UPDATED: OCTOBER 2018 COPY MADE.

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
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FORM UPDATED OCTOBER 2018 COPY MADE.

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: I -Z-7- t TIME COLLECTED: a 'Co0 COLLECTED BY:
DATE RECEIVED: 2-i TIME RECEIVED: Q CCD RECEIVED BY:
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FORM UPDATED: OCTOBER 2018 COPY MADE:

�������������������H0���&0�
��V���� TRAIN -� QUARTERLY SUMMARY
Train lFeed
Train1A
Train 113
Date
Volume TSoUds VSo|ids
Temp TSoUds VSo|ids Fecal[u|ih»rm
Temp TSn|ids VSo|ids
Feca|[o|ifonn
Comments
(gal) % %
Deg % % (MPN/g)
Deg % %
(MpN/g)
7/29/2019
16/000
75.0 7.90
76.0
tes1.should bedeleted
7/30/2019
test3.xhou|d be deleted
8/1/2019
20'700
42.0
45.2
8/2/2019
44.2
483
8/3/2019
42.3
457
8/4/2019
43.7
45.0
8/5/2019
45.4
45.7
8/6/2019
47.3
46.4
8/7/2019
18'000
48.8
48.4
8/8/2019
46,500
49.1
49.1
8/9/2019
48.9
48.9
8/10/2019
48.5
48.5
8/11/2019
47.8
47.8
8/13/I019
18,000
46.5
46.5
8/13/2019
18,800
507
46.3
8/15/2019
53.2
47.3
8/16/2010
53.3
46.8
8/17/I019
52.5
447
8/18/2019
18,000
51.8
43.8
Wednesday, February S' 2020
Page 1 of3

Train 1 Feed
Train 1A
Train 1B
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp
T Solids V Solids
Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
Deg C
% %
(MPN/g)
8/19/2019
18,000
50.7
43.2
8/20/2019
18,000
50.9
47.0
8/21/2019
50.7
49.0
8/22/2019
50.0
48.7
8/23/2019
18,000
50.8
47.6
8/24/2019
51.4
45.6
8/25/2019
50.5
44.0
8/26/2019
18,000
50.2
47.8
8/27/2019
5.9
6.94
8/27/2019
18,000
50.7
51.8
8/28/2019
9,000
51.0
49.6
8/29/2019
18,000
50.8
46.9
8/30/2019
27,000
50.1
51.5
8/31/2019
47.7
54.5
9/3/2019
5.3
1.06
9/10/2019
5.7
1.31
9/17/2019
4.7
3.83
9/24/2019
5.1
3.56
Comments
Wednesday, February 5, 2020 Page 2 of 3

Train 1 Feed
Date Volume T Solids V Solids
(gal) % %
Train 1A
Temp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g)
Train 1B
Ternp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g)
No. of Entries', 15 0 0 31 0 0 1 31 5 0 5
Tota 1 300,000
Min 9,000 42 8 43 5 1
Geom. Mean 18,894 0 0 50 0 0 8 48 5 0 3
Max46,500 75 8 76 6 7
Comments
Wednesday, February 5, 2020 Page 3 of 3

ATAD TRAIN 2 QUARTERLY SUMMARY
Train 2 Feed Train 2A Train 28
Date Volume T Solids V Solids Temp T Solids V Solids Fecal Coliform Temp T Solids V Solids Fecal Coliform
(gal) % % Deg C % % (MPN/g) Deg C % % (MPN/g)
7/2/2019 4.3 4.20
7/9/2019 4.0 4.51
7/29/2019
7/30/2019
18,000
69.0
8/1/2019
48.2
8/2/2019
20,700
42.1
8/3/2019
44.6
8/4/2019
47.9
8/5/2019
47.6
8/6/2019
45.4
8/7/2019
46.9
8/8/2019
27,000
45.5
8/9/2019
42.7
8/10/2019
51.9
8/11/2019
50.1
8/12/2019
18,000
56.5
8/12/2019
8/13/2019
60.2
8/14/2019
64.4
8.10
70.0
58.0
59.4
60.3
61.0
59.7
57.7
56.2
55.8
48.9
55.2
68.6
62.0
63.2
69.2
Comments
testl. should be deleted
test2.should be deleted
testl on 8/12/19
Wednesday, February 5, 2020 Page 1 of 4

Train 2 Feed
Train 2A
Train 2B
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp T Solids V Solids Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
Deg C % % (MPN/g)
8/15/2019
64.3
70.7
8/15/2019
64.3
6967.0
8/15/2019
64.3
69.7
8/16/2019
57.9
67.5
8/17/2019
54.7
64.7
8/18/2019
57.5
63.6
8/19/2019
18,000
48.4
65.5
8/20/2019
18,000
51.2
62.4
8/21/2019
18,000
50.8
60.3
8/22/2019
18,000
51.7
58.7
8/23/2019
53.1
62.1
8/24/2019
58.4
65.5
8/25/2019
59.2
66.5
8/26/2019
18,000
55.8
65.2
8/27/2019
57.7
63.8
8/28/2019
57.1
62.8
8/29/2019
49.6
58.0
8/30/2019
46.6
57.8
8/31/2019
53.4
59.1
9/1/2019
0
57.1
62.8
9/1/2019
57.1
62.8
Comments
Wednesday, February 5, 2020 Page 2 of 4

Train 2 Feed
Train 2A
Train 28
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Ternp T Solids V Solids Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
Deg C % % (MPN/g)
9/2/2019
57.7
63.8
9/3/2019
57.0
62.9
9/4/2019
18,000
49.3
60.7
9/5/2019
55.5
58.9
9/6/2019
57.6
58.9
9/6/2019
57.6
58.9
9/7/2019
57.9
60.1
9/8/2019
57.4
60.6
9/9/2019
18,000
58.1
58.9
9/10/2019
54.8
59.1
9/11/2019
18,000
54.0
57.5
9/12/2019
18,000
51.5
57.4
9/13/2019
13,500
46.0
46.0
9/14/2019
51.7
56.8
9/15/2019
49.0
59.9
9/16/2019
18,000
47.8
58.5
9/17/2019
18,000
52.7
57.9
9/18/2019
54.1
59.4
9/19/2019
52.4
59.0
9/20/2019
44.6
54.9
9/21/2019
53.0
57.1
Comments
Wednesday, February 5, 2020 Page 3 of 4

Train 2 Feed
Train 2A
Train 2B
Date
Volume
T Solids V Solids
Temp
T Solids V Solids
Fecal Coliform
Temp
T Solids V Solids
Fecal Coliform Comments
(gal)
% %
Deg C
% %
(MPN/g)
Deg C
%
%
(MPN/g)
9/22/2019
57.0
60.4
9/23/2019
18,000
51.6
60.3
9/24/2019
49.1
55.8
9/25/2019
22,500
45.2
54.3
9/26/2019
47.8
53.9
9/27/2019
53.2
58.3
9/28/2019
57.8
63.77
9/29/2019
60.0
66.3
9/30/2019
9,000
55.2
64.9
No. of Entries
20
0 0
66
0 0
2
65
2
0
2
Total
344,700
s
Min
0
42
8
46
4
4
Geom. Mean
17,800
0 0
53
0 0
23
65
4
0
4
Max
27,000
69
64
6,967
4
5
Wednesday, February 5, 2020 Page 4 of 4

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
-� -)- --11
0 7 o 2-
l� t v
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: --I — 2 --' 9
TIME RECEIVED: 9
RECEIVED BY: �S
PERMIT NO. �W0123466
Enclosure
DATE ANALYZED:
TIME ANALYZED: 019 -\Z
ANALYZED BY: r�
V
SAMPLE
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN ! mL'
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
l z�
15
f.. 15
15
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15
i` 15
�' l5
I5
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DUP
151
1
1
1 /5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
0.5°C IN INCUBATOR
DATE OUT:
TIME OUT:
TEMP:
�7-2-Ic)
(Sc,o
7Iy C) °C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE OUT: ` 19
TIME OUT: v I ti
TEMP: L q • �r 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
N—)
DS A-1 BROTH
01
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb. of positives)
MPN/GRAM 2
% TOTAL SOLIDS
2"�
MPN/GRAM2 = MPN / mL
Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE -
FORM UPDATED OCT08ER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
7— q -a,0 9
0G57
r4-,,b e �+
r SM 9221 C E-2008
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: - 9
TIME RECEIVED: O "T
RECEIVED BY:
PERMIT NO. WQ12346��
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Er1CI05ure (1
SAMPLE
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
r
MPN ! mL
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
77. 6
V /5
1 5
c 15
i. 5
O /5
O /5
� /5
a 15
Lj g
r�
DUP
O /5
d /5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
^7 J riuuml Al 03
( 1 I
o 8 LA
3s. a •c
c � T c nv�+r�� r� � �r►.
r -1Lf
y L? 5 -C
0.5°C IN INCUBATOR
DATE OUT:
TIME OUT: a 3
TEMP: 3s a- -C
f 0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
-t--
—"
DS A-1 BROTH
+
r
—
DS o0
Lj S Ic
MPN / mL` = MPN Index Value ,
Largest Sample Volume
(from comb. of positives)
MPN/GRAMT
% TOTAL SOLIDS
3 q�
MPN/GRAM2 = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY'.14
COPY MADE.
FORM UPDATED' OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
GvlL�,r if—n.a
SM 9221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: g
TIME RECEIVED: +7
RECEIVED BY:tV
PERMIT NO. WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Enclosure (1)
SAMPLE
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN ! mL1
LOCATION
10 mL
mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
o.t�(�$
U
5
'I
`-� i5
;5
O 5
5
S I5
/5
v 15
1_. 50
t } R Y . t'l
L j 5
DUP
! 5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
i 1
o 6co
35 . o •C
DATE OUT: LJ ` � 01
TIME OUT:
TEMP: 35 -C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
F-0 - IV, 1 41 1
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
P
I v�
DS A-1 BROTH
P
'C
�Y0 -
��tft 1.}'7. V1
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN/GRAM
�tr--�-i•- • I �
% TOTAL SOLIDS
4. 1
MPN/GRAM' = MPN I mL
% Total Solids
(expressed as a decimal)
CHECKED BY 0'
COPY MADE
FORM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
09 -IS-,? 611�
U-73D
P--� u (tee. r-
SM 9221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: 3 I
TIME RECEIVED: p cf
RECEIVED BY:
PERMIT NO. �^ WQi2346 -�
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
8•l3�tq
Enclosure (i
3 HRS AT 35 0- 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0,2"C IN INCUBATOR
COMB, OF
MPN INDEX
,
SAMPLE
POSITIVES
VALUE
MPN / mL
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
FCC,,
0
Q
Q
0
CD
15
15
15
15
15
15
e5
15
G`S C)
}��5
O
DUP
! 5
15
DATE IN.
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE OUT: �3 ' i 3 I q
TIME OUT: 1 �-
TEMP: �J�J 'C
21 + 2 HOURS AT 44.5 + 0.2'C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
QbS
'C
MPN ! GRAM7
20. 4 tP
g ! I' 11
% TOTAL SOLIDS
q g5
MPN 1 mL' = MPN Index Value MPNIGRAM'=
Largest Sample Volume
(from comb of positives)
1ti1PN i mL
i, Total Solids
(expressed as a decimal)
CHECKED BY (7
COPY MADE
FORM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
b' Z,g 417
e eo S._
,G✓/ L t- I I) -Yu
SM 4221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO. W012345
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Enclosure (1)
9,. -o
\O?o
Semis Ve-r—
SAMPLE
LOCATION
3 HRS AT 35 + 0,5-C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2-C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
(„ PA 6-
,
MPN / mL
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
l
O 15
/5
/5
/5
O /5
�}
`� 15
/5
15
1*1
o- C
�{
t
a 09
DUP
/"�
11 / 5
O 15
DATE IN:
TIME IN:
TEMP:
DATE IN
TIME IN
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE OUT: �� t
TIME OUT:
TEMP: J -C
5 + 0.2'C IN WATER BATH /
DATE OUT: v - -2— t -
TIME OUT: G 1-3
TEMP: { f -C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
If
31
DS A-1 BROTH
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPNIGRAM'
% TOTAL SOLIDS
MPN/GRAM' = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE
LA -
FORM UPDATED OCTOBER 2018

DATE COLLECTED.
TIME COLLECTED:
COLLECTED BY:
METHOD:
d8117 /�9
Ob'a0
1.� l r �r+•S
SM 9221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED: g S
RECEIVED BY- Imo.
PERMIT NO. WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Enclosure (1)
-A
og3S
SAMPLE
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN ! mL'
LOCATION
10mL
1 mL
0.10 mL
0.010 mL
1/0 mL
1 mL
0.10 mL
0.0110 mL
U 15
v 15
/5
ZFJ /5
I 15
5 5
"5
lJ 5
f�_ r,- 0
( j
o, t
DUP
/5
O 15
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
3 oC
DATE OUT:
TIME OUT:
TEMP:
21 + 2 HOURS AT 44.5 + 0.2"C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
Ili
rJ
DS A-1 BROTH
ri
j
-C
S- aB. 161
�a I�
W • S -C
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN ! GRAM2
% TOTAL SOLIDS
MPN/GRAM' = MPN / mL
Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE
FORM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD
023 �
SM 9221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: Gi
TIME RECEIVED:
RECEIVED BY:
PERMIT NO. WQ123 6
DATE ANALYZED
TIME ANALYZED:
ANALYZED BY:
q 3A
�QID0
Enclosure (1
SAMPLE
3 HRS AT 35 + 0.5'C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN I mL'
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
l5
5
5
5
0 5
_ /5
/5
/5
Q_—
b4 'i14t r
DUP
D 5
O.5
DATE IN
TIME IN:
TEMP:
DATE IN
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5"C IN INCUBATOR
DATE OUT: 7 3 ) 1
TIME OUT: SO
TEMP: 3 • S -C
21 + 2 HOURS AT 44.5 + 0.2'C IN WATER BATH
DATE OUT: `
TIME OUT: 10 0 s
TEMP: f �, 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
--
MPN / mL' = N Ind alue
Large amp me
((r comb of positives
MPN f GRAM2
1-%ty
%, TOTAL SOLIDS
s. _-2
MPN/GRAM = MPN / mL
% Total Solids
(expressed as a decimal)
CHECKED BY
COPY MADE
FORM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
SM 9221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
q 10. )q
0910
WQ12346
DATE ANALYZED:
TIME ANALYZED.
ANALYZED BY:
1.10.11
091v
V'C-
irPj-J/,„n_ r_
Enclosure (1
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0,2°C IN INCUBATOR
COMB. OF
MPN INDEX
i
SAMPLE
POSITIVES
VALUE
MPN / mL
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
V
0
0
O �/5
1,67
'Df `( S
f vv
/ 5
i 5
15
15
/ 5
15
V 15
0-1 (f
IA K.13 �4
0.
�
DUP
15
15
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE OUT: + 10' �� 1
TIME OUT: ! t
TEMP: 35- l 'Cl
21 + 2 HOURS AT 44.5 + 0.2'C IN WATER BATH q
Gj I l7 7`0 L� DATE OUT: Ct. U . � t
(I TIME OUT: 02Y,
L- l
44,57 -C TEMP: 44 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
?cs
MPN/GRAM
% TOTAL SOLIDS
s � (
MPN I mL` = MPN Index Value MPN/GRAM =
Largest Sample Volume
(from comb of positives)
CHECKED BY
COPY MADE
MPN/mL
% Total Solids
(expressed as a decimal)
FORM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD; I SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: 1 1-7 lq
TIME RECEIVED: to 0-1
RECEIVED BY:
LA -
PERMIT NO. WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Enclosure C
SAMPLE
LOCATION
3 HRS AT 35 + 0.5'C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN I mL'
1. 0�
1 ,..t
0.1) 1
a. 0 0 l
1 V. t_
0. t .,.1-
O.vI .. 1<
0 -oolm L-
0:0'10'A
tq.
Q 0
1 1 6
O /5
0 15
0 /5
"5
0 5
15
/5
15
DUP
O 115
D r5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5'C IN INCUBATOR
DATE OUT:
TIME OUT:
TEMP:
►7- 1 1
J !
3s 3 .0
21 + 2 HOURS AT 44.5 + 0.2'C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
0 S
DS A-1 BROTH
p S
(1 v
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN I GRAM'
<3. 3
% TOTAL SOLIDS
MPN/GRAM =
CHECKED BY
COPY MADE
MPN / mL
% Total Solids
(expressed as a decimal)
Fil
FORM UPDATLD OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD
C)
c'-
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED. . I
TIME RECEIVED: 8 j
RECEIVED BY:
PERMIT NO. WQ12346
DATE ANALYZED: f 1_! _'
TIME ANALYZED: t) g L
ANALYZED BY: L"k-
Enclosure,
3 HRS AT 35 + 0 5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
MPN INDEX
SAMPLE
POSITIVES
VALUE
MPN 1 mL'
k1 -L
0•l n.i
0 01 n.L
D o oI MI-
^��
0.f n.L
D. oi. c
0. oot #, 1-
LOCATION
I^
m
10 mL
Mpr, 4
i I
G �5
u 15
C) J5
_
t5
5
o 5
;5
0- 0- P
0
0
DUP
/5
15
DATE IN
TIME IN,
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
ay- Iq
35 D aC
DATE OUT:
TIME OUT: 10
TEMP: 36 • �- 'C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH—
DS A-1 BROTH
i=ORM UPDATED OCTOUER 2018
MPN ml- MPN Index Value
Largest Sample Volume
(from comb of positives)
MPN/GRAM2
-3 s�
% TOTAL SOLIDS
S.Db
MPN/GRAMMPN mL
Total Solids
(expressed as a decimal)
Cl-ICCKED BY v
COPY MADI_

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: 1- -2- L 9 TIME COLLECTED: ", COLLECTED BY:
DATE RECEIVED: -7` Z ^ 9 TIME RECEIVED: , 00 RECEIVED BY:
DATE ANALYZED: `j - 2'-'t(:)j TIME STARTED: 0 © v ANALYST:
TIME IN OVEN: Ices- TIME OUT OVEN: 12 2 ,�- TIME IN FURNACE:
OVEN TEMP: 1014.0 °C OVEN TEMP: j b3 - °C FURNACE TEMP:
BALANCE CK: 1 too . 00 BALANCE CK: � f Q)c1 BALANCE CK:
METHOD: SM 2540 B_E - 2011 PERMIT NO. W00012346
A I B C I D E I F G
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
%
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
B - A
C -A]
[C - DJ
F/E] X 100
(GIF] X 100
l I
72. 32
.1-7. s 0
'i Z S i t, S
z ��s�"
s. t 16
q3 I
Q, cal
3
4 -7. �
,VV6
Z9
Fz� s
SS 5 i3
q0
S. 15Q
1
.c39
Q
LA'z-3-7
AVG: 1. L.)
DUP: i
-73.
S- 3
-73 S\Z3
-73.42.©3
s.CH3
S-7
0 ,011W
0. 2..-
BENCHSCALE
BENCHSCALE
AVG:
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE:
% Duplicate = Difference in 2 values x 100
Average of 2 values
QC REPORTED:
% Recovery = Results obtained x 100
Known value
QC RANGE:
CHECKED BY: U<
FORM UPDATED: OCTOBER 2018 COPY MADE:

DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
PERMIT NO.
> 70 S
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
• . I
D -7,;?c)
U -? 3 I
5
1 3 3 3
j o -3 • °C
) CI-( . D °C
so t pv 9
�{ �{q g q�•��Q�i g
WQ0012346
SM 2540 B_E - 2011
A
B
C
D
E
F
G
I cP/
(x'
F L)�-- ::=
ILfOp
5 SD °C
WT OF
WT OF
WT OF
SAMPLE
TOTAL
VOLATILE
%
%
SAMPLE
WT OF DISH
DISH+WET
SOLIDS
DISH+DRY
SOLIDS
DISH+ASH
WEIGHT
SOLIDS
WEIGHT
SOLIDS
WEIGHT
TOTAL
VOLATILE
°
/a
RECOVERY
LOCATION
SOLIDS
SOLIDS
(9)
(9)
(g)
(9)
(9)
(9)
(9)
B -A]
Ci�- AljC
-
[FIE]X 100
— -.J
R ! 7 �j
V V,4bv3
4 Q (� ']
U 1 _1 "'+
(� �(}
r t 1
4 1,,
U `y l.i a��
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0, 1~'q i
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g(�"?s 3y
3 oG
o.► q 5
o vLlqLq
3 R8
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ail 3�
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8�.�{�io
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0.�o3
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88.�SIS
�(.�
•�`�II
g$.��}�
a.��
O.tli�
�,o��a—
y 0L
91 I�(
%D= o `�
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: I-
% Duplicate = Difference in 2 values x 100
Average of 2 values
FORM UPDATED OCTOBER 2018
QC REPORTED:
% Recovery = Results obtained x 100
Known value
,X N uJ kv NJ, Q C" dt Ss,•-pZ vT2 .
QC RANGE:
CHECKED BY
COPY MADE

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
-7' / ( — f 9
I.ff')-to(
1 / v
j °C
!
q�•q��}
t-t 1 9
�SM 2540 B_E - 2011
TIME COLLECTED
TIME RECEIVED:
TIME STARTED:
TIME OUT OVEN:
OVEN TEMP:
BALANCE CK:
PERMIT NO.
r n
U (3 3 ,)
D
°C
/�i-1//��
"
WQ0012346
c C
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
r,
n
WT OF DISH
WT OF
DISH+WET
WT OF
DISH+DRY
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
TOTAL
%
VOLATILE
%
SAMPLE
LOCATION
SOLIDS
SOLIDS
WEIGHT
WEIGHT
SOLIDS
SOLIDS
RECOVERY
(9)
(9)
(9)
(9)
(9)
(9)
(9)
B - A
C - A
(C -D]
FIE X 100
[Gfl X 100
7 I b
�,��
�� ��
1a 4��b�
l 41!
c:2-00
-ra �b
11�-L/
r �•c,4(
6�-00
O.9-000
o. Qt' �
.oO
1--e-e-
AVG: 1'
DUP: `C�
�.�,a�.�1�(n
%D= 0.5
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE DUP
%D=
QC N! Ib
OC TRUE VALUE: 1 lY I ) --�
% Duplicale = Difference in 2 values x 100
Average of 2 values
OC REPORTED:
% Recovery = Results obtained x 100
Known value
CIC RANGE:
CHECKED BY:
FORM UPDATED: OCTOBER 2018 COPY MADE.

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: -7 - (O `a G 1 cl TIME COLLECTED: 0 -7 tt-31 U COLLECTED BY:
DATE RECEIVED: I I �) TIME RECEIVED: 61 1 RECEIVED BY:
DATE ANALYZED: TIME STARTED: 8oc) ANALYST:
TIME IN OVEN: TIME OUT OVEN: 1 O S LD TIME IN FURNACE:
OVEN TEMP: ( °C OVEN TEMP: { t] 30 °C FURNACE TEMP:
BALANCE CK: i C7 U Q
BALANCE CK: 1gg9 g BALANCE CK:
METHOD: SM 2540 B_E - 2011 PERMIT NO. W00012346
nI r% c r r
DZIS
C/�
l 3C�
sgzn, °C
c� UU 9
SAMPLE
LOCATION
.,
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
B - A
C - A
(C-0)
[FIEJ X100
fGfl X 100
c -7
(A s
Fe
29t t
S 3 0a9
- F)3 s
I
5
�,b
t"s
AVG.
DUP. F cE l7
—12.3235r
-? S
z .5�
5
, 75-7
0, y q {
`i -3 3
'39 W
%D= v 3
BENCHSCALE
BENCHSCALE
AVG
BENCHSCALE OUP
%0=
QC
QC TRUE VALUE:
% Duplicate = Difference in 2 values x 100
Average of 2 values
QC REPORTED:
%Recovery= Results obtained x 100
Known value
QC RANGE: I _I
CHECKED BY
FORM UPDATED OCTOBER 2018 COPY MADE

CAMP LEJEUNE WWTP - AT& aLUDGE SOLIDS ANALYSIS
DATE COLLECTED: ( 0 4 l TIME COLLECTED: O, ZS COLLECTED BY:
DATE RECEIVED: TIME RECEIVED: Z�t RECEIVED BY:
DATE ANALYZED: �� \� �1`'� TIME STARTED: U Z ANALYST:
TIME IN OVEN: 8 3 S TIME OUT OVEN: L S TIME IN FURNACE:
OVEN TEMP. 3. °C OVEN TEMP: IO °C FURNACE TEMP:
BALANCE CK: g BALANCE CK: ��g BALANCE CK:
METHOD: 2540 B_E - 2011 PERMIT NO. W00012 446
SM
Enclosure I
SAMPLE
LOCATION
A
WT OF DISH
D
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
%
TOTAL
SOLIDS
VOLATILE
SOLIDS
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
[B - A]
[C - Al
(C - 01
(F/E/ X 100
G/F X 100
o -Zs
63 L)
c� ��
. L42S
-3 Ll 9?S
—3
5 .
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AVG ��•
DUP: ��
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BENCHSCALE
BENCHSCALE
B
AVG
BENCHSCALE DUP
%D=
QC
QC TRUE VALUE: F QC REPORTED:
% Duplicate = Difference in 2 values x 100 % Recovery = Results obtained x 100
Average of 2 values Known value
QC RANGE: I I
CHECKED By
FORM UPDATED: OCTOBER 2018 COPY MADE

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: 2-J _ TIME COLLECTED: ! ( U
DATE RECEIVED: —j 3 I TIME RECEIVED: 0 -71 S
DATE ANALYZED: TIME STARTED: D -1 517
TIME IN OVEN: D g 3 TIME OUT OVEN: C y 3
OVEN TEMP: l 0 t'I - 1 °C OVEN TEMP: ! o oq °C
BALANCE CK: 100 O g BALANCE CK: r 19 1 ��419
METHOD: SM 2540 B_E - 2011 PERMIT NO. L WQ0012346
COLLECTED BY:
RECEIVED BY:
ANALYST:
;z S
TIME IN FURNACE:
FURNACE TEMP:
5 S O °C
BALANCE CK:
DD . r^ 9
r_
q
WT OF DISH
o
WT OF
DISH+WET
v
WT OF
DISH+pRY
WT OF
DISH+ASH
SAMPLESOLIDS
WEIGHT
TOTAL
-
VOLATILE
SOLIDS
TOTAL
VOLATILE
°I°
SAMPLE
SOLIDS
SOLIDS
WEIGHT
WEIGHT
SOLIDS
SOLIDS
RECOVERY
(9)
(9)
(g)
(9)
(g)
�9)
�9)
LOCATION
B - AlC
- A
(C - DJ[FIE]
X 100
GIF] X 100
1-7 IQ5
`f Q.3-A5a
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QC TRUE VALUE:
% Duplicate = Difference in 2 values x 100
Average of 2 values
QC REPORTED: I j
% Recovery = Results obtained x 100
Known value
QC RANGE: I I
CHECKED BY: _!
FORM UPDATED OCTOBER 2018 COPY MADE:

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: Gig -' 06 — TIME COLLECTED: 7 Y S COLLECTED BY:
DATE RECEIVED: Q� ��. TIME RECEIVED: O`�4�' RECEIVED BY:
DATE ANALYZED: �' %� �TIME STARTED: {? -1 �' ANALYST:
TIME IN OVEN: 0q 5� TIME OUT OVEN: 1 TIME IN FURNACE:
OVEN TEMP: -2 °C OVEN TEMP: �O °C FURNACE TEMP:
� G
BALANCE CK. �. �t BALANCECK:BALANCECK:
METHOD: SM 2540 B_E - 2011 PERMIT NO. WQ0012346 1
A 1 B 1 C I D E I F I G
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
RECOVERY
(g)
(g)
(g)
(g)
(g)
(g)
(g)
8 - A
C - A
(C - DJ[FIE]
X 100
[GIF1 X 100
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QC TRUE VALUE: —�
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Average of 2 values
QC REPORTED:
% Recovery = Results obtained x 100
Known value
QC RANGE: I I
CHECKED BY. Vx
FORM UPDATED OCTOBER 2018 COPY MADE:

CAMP LEJEUNE WWTP - ATX . LUDGE SOLIDS ANALYSIS Enclosure t ,
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
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OVEN TEMP.
BALANCE CK:
PERMIT NO.
r. I n
To-
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W00012346
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ANALYST:
TIME IN FURNACE:
FURNACE TEMP:
BALANCE CK:
G
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
%
TOTAL
SOLIDS
°
VOLATILE
SOLIDS
%
RECOVERY
(9)
(9)
(9)
(g}
(g)
(9)
(9)
B - AJ
(C - Al(C
D]
(F/EJ X 100
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OC REPORTED: 1 —�-1
% Recovery - Results obla:ced x 100
Known value
QC RANGE:
CHECKED BY Ur
FORM UPDATED OCTOBER 2018 COPY MADE

CAMP LEJEUNE WWTP - ATA, jLUDGE SOLIDS ANALYSIS
DATE COLLECTED: O TIME COLLECTED: Q -7 02 L) COLLECTED BY:
DATE RECEIVED: $ . { S qlot TIME RECEIVED: O g +3 S RECEIVED BY:
DATE ANALYZED: . S S 1 t TIME STARTED: S 1 ANALYST:
TIME IN OVEN: 7 �L� TIME OUT OVEN: I a TIME IN FURNACE:
OVEN TEMP: S °C OVEN TEMP: Qb 3 q °C FURNACE TEMP:
BALANCE CK: 10 O . O BALANCE CK: -/ ! 9g BALANCE CK:
METHOD: SM 2540 B_E - 2011 PERMIT NO. W00012346
Enclosure ((,,
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WT OF
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WT OF
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WEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
°I°
TOTAL
°
VOLATILE
%
SAMPLE
SOLIDS
SOLIDS
WEIGHT
WEIGHT
SOLIDS
SOLIDS
RECOVERY
(g)
(9)
(g)
(9}
(g)
(g)
(9)
LOCATION
8 - A
(C - A
(C - D)
[FIE] X 100
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Average of 2 values Known value
QC RANGE: I I
CHECKED BY t/"
FORM UPDATED OCTOBER 2018 COPY MADE

CAMP LEJEUNE WWTP - ATA, -iLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP:
BALANCE CK:
METHOD:
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l ©40 9
WQ0012346
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WT OF DISH
WT OF
DISH+WET
WT OF
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WT OF
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WEIGHT
TOTAL
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VOLATILE
SOLIDS
°
/°
TOTAL
°
VOLATILE
%
SAMPLE
SOLIDS
SOLIDS
WEIGHT
WEIGHT
SOLIDS
SOLIDS
RECOVERY
LOCATION
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Average of 2 values
QC REPORTED:
% Recovery = Results obtained x 100
Known value
QC RANGE: I
CHECKED BY W
FORM UPDATED OCTOBER 2018 COPY MADE

CAMP LEJEUNE WWTP - ATA..,LUDGE SOLIDS ANALYSIS
DATE COLLECTED: Zo t TIME COLLECTED: b g os COLLECTED BY:
DATE RECEIVED: $ oZ(, `l TIME RECEIVED: 0 "7 It-0 RECEIVED BY:
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DATE ANALYZED: l� TIME STARTED: 'r` 9 t� f l � I o ANALYST:
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METHOD: SM 2540 B_E - 2011 PERMIT NO. W00012346
Enclosure I .
I
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A
B
C
D
E
F
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SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
VJ7 OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
%%
TOTAL
SOLIDS
F/E X foo
VOLATILE
SOLIDS
GiFJ x 1Qo
%
RECOVERY
(g)
(g)
(g)
(g)
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QC TRUE VALUE: QC REPORTED: QC RANGE:
% Duplicate = Difference in 2 values x 100 % Recovery = Results obtained x 100
Average of 2 values Known value CHECKED BY
COPY MADE
FORM UPDATED OCTOBER 2018

CAMP LEJEUNE WWTP - ATA, jLUDGE SOLIDS ANALYSIS
DATE COLLECTED: TIME COLLECTED: 7 J COLLECTED BY:
DATE RECEIVED: a(P I TIME RECEIVED: D-7 1 te RECEIVED BY:
DATE ANALYZED: C a (, • j °� TIME STARTED: 0 O ANALYST:
TIME IN OVEN: D 1 S TIME OUT OVEN: I oZ TIME IN FURNACE:
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BALANCE CK: I ob . v 9 BALANCE CK: IUD. Du c, 3 91 BALANCE CK:
METHOD: SM 2540 B_E - 2011 PERMIT NO. W00012346
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9
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WT OF DISH
C
WT OF
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WT OF
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DISH+ASH
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WEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
TOTAL
VOLATILE
SAMPLE
SOLIDS
SOLIDS
WEIGHT
WEIGHT
SOLIDS
SOLIDS
RECOVERY
(g)
(g)
(g)
(g)
(g)
LOCATION
[B . A]
(C - Al(C
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(FIE] X 100
G/FJ X 100
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QC TRUE VALUE: I OC REPORTED: I I
% Duplicate = Difference in 2 values x 100 % Recovery = Resuits obtained x 100
Average of 2 values Known value
FORM UPDATED OCTOBER 2018
QC RANGE: I
CHECKED BY
COPY MADE

CAMP LEJEUNE WWTP -ATA, jLUDGE SOLIDS ANALYSIS Enclosure(,
DATE COLLECTED: 7 t Y TIME COLLECTED: 0 `7 30
DATE RECEIVED: g - a� • l`� TIME RECEIVED: D g S$
-771 DATE ANALYZED: a7 • l TIME STARTED:
TIME IN OVEN: 0 3 TIME OUT OVEN. 3
OVEN TEMP: I 0 3 -1 °C OVEN TEMP: 103,6 °C
BALANCE CK: 100,0 9 BALANCE CK: D 0 0 9
METHOD: SM 2540 B_E - 2011 PERMIT NO. WQ0012346
-- r --.. _. .z
COLLECTED BY:
RECEIVED BY:
ANALYST:
TIME IN FURNACE:
I Ll S
FURNACE TEMP:
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BALANCE CK:
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WT OF DISH
WT OF
DISH+WET
WT OF
DISH+DRY
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
%
TOTAL
%
VOLATILE
°
�°
SAMPLE
SOLIDS
SOLIDS
WEIGHT
WEIGHT
SOLIDS
SOLIDS
RECOVERY
(9)
(9)
(9)
(9)
i9}
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LOCATION
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Average of 2 values
QC REPORTED: I 1
% Recovery = Results obtained x 100
Known value
QC RANGE:
CHECKED BY
FORM UPDATED OCTOBER 2018 COPY MADE

CAMP LEJEUNE WWTP - ATA, jLUDGE SOLIDS ANALYSIS
DATE COLLECTED: 29 TIME COLLECTED: D_7 3d COLLECTED BY:
DATE RECEIVED: - 3 I 1 TIME RECEIVED: fi B 3 RECEIVED BY:
DATE ANALYZED: 3 1 °� TIME STARTED: D g ,3 ( ANALYST:
TIME IN OVEN: TIME OUT OVEN: 113 TIME IN FURNACE:
OVEN TEMP: 3 fP °C OVEN TEMP: (9 °C FURNACE TEMP:
BALANCE CK: ( O D - a 91 BALANCE CK: 'T, `r q'T 7 g BALANCE CK:
METHOD: SM 2540 B_E - 2011 PERMIT NO. WQ00123Z
Enclosure (:,
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WT OF
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WEIGHT
TOTAL
SOLIDS
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SOLIDS
%
TOTAL
VOLATILE
%
SAMPLE
SOLIDS
SOLIDS
WEIGHT
WEIGHT
SOLIDS
SOLIDS
RECOVERY
t9)
(g)
(g)
(g)
(g)
(g)
(9)
LOCATION
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Average of 2 values
QC REPORTED:
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Known value
QC RANGE: L
CHECKED BY
COPY MADE
FORM UPDATEDOCTOBER 2018

CAMP LEJEUNE WWTP - ATA� SLUDGE SOLIDS ANALYSIS
I nclositto ("
DATE COLLECTED: C`E TIME COLLECTED: 2- COLLECTED BY:
DATE RECEIVED: 2j . 1 TIME RECEIVED: $3 ` RECEIVED BY:
p [
DATE ANALYZED: �- �, TIME STARTED: U o 3 � ANALYST:
TIME IN OVEN: V,3 TIME OUT OVEN: ^� 0 - TIME IN FURNACE:
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BALANCE CK: 1 UO . ID BALANCE CK: `�. qq c�
9 BALANCE CK: ! 1- 1 l 9
METHOD: SM 2540 B_E - 2011 PERMIT NO. wQ0012346
SAMPLE
LOCATION
l
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
°!°
TOTAL
SOLIDS
°!°
VOLATILE
SOLIDS
f°
RECOVERY
(g)
(g)
(g)
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(g)
(9)
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QC REPORTED:
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Known vaIut-
QC RANGE: C I
CI ICCKED RY V"
FORM UPDAJED OCT01.3ER 2018 COPY MADE

CAMP LEJEUNE WWTP - ATA.- SLUDGE SOLIDS ANALYSIS
DATE COLLECTED: 09 — Q 0 t TIME COLLECTED: O i k S COLLECTED BY:
DATE RECEIVED: t i ai 1q TIME RECEIVED: 0 -73-7 RECEIVED BY:
DATE ANALYZED: ) ) "� TIME STARTED: BHa ANALYST:
TIME IN OVEN: TIME OUT OVEN: 0 -7 0 0 TIME IN FURNACE:
OVEN TEMP: 0 3 -"�i °C OVEN TEMP: 10 3 • (o °C FURNACE TEMP:
BALANCE CK: 100.0 g BALANCE CK: j OD. 0000 91 BALANCE CK:
METHOD: SM 2540 B_E - 2011 PERMIT NO. WQ0012346
C
Enclosure (. .
A
WT OF DISH
o
WT OF
DISH+WET
WT OF
DISH+DRY
WT OF
DISH+ASH
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WEIGHT
TOTAL
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SOLIDS
TOTAL
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%
SAMPLE
SOLIDS
SOLIDS
WEIGHT
WEIGHT
SOLIDS
SOLIDS
RECOVERY
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LOCATION
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QC TRUE VALUE: F QC REPORTED: L
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Average of 2 values Known value
QC RANGE: 1 1
CHECKED BY W
FORM UPDATED' OCTOBER 2018 COPY MADE

�k SfAEEr ;I -
CAMP LEJEUNE WWTP - ATA.- SLUDGE SOLIDS ANALYSIS i nrluure
DATE COLLECTED: �q } D R TIME COLLECTED: 0 -7 Lf S
DATE RECEIVED: t la - 1 `� TIME RECEIVED: fl ^! 3 -J
DATE ANALYZED: l 3 1`� TIME STARTED: b 3 $
TIME IN OVEN: I O S8 TIME OUT OVEN: D S
OVEN TEMP: ! 0 3 °C OVEN TEMP: 1 O 3 S °C
BALANCE CK: ( Dv. D g BALANCE CK: ` 1? g9Rl g
METHOD: SM 2540 B_E - 2011 PERMIT NO. WQQ012345 =
oI r I rn I F 1 F
COLLECTED BY:
Ltr 1-G
RECEIVED BY:
ANALYST:
-�
TIME IN FURNACE:
50-6
FURNACE TEMP:
55D °C
BALANCE CK:
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SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
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SOLIDS
WEIGHT
°
TOTAL
SOLIDS
VOLATILE
SOLIDS
RECOVERY
(9)
(9)
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(9)
(9)
(9)
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(C - A)
(C - D]
[FIE) X" 100
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lo.
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AVG
DUP:
%D=
BENCHSCALE
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QC TRUE VALUE: QC REPORTED: 1-
% Duplicate = Difference in 2 values x 100 % Recovery = Results obtained x 100
Average of 2 values Known value
F e,d S0_k,ti e- YLLLrn6L1j-z 1 1 r°rrt Q.ta i`i 0.rnv C,S, S.
FORM UPDATED: OCT08ER 207Fi
QC RANGE: i
CHECKED BY V
COPY MADE

CAMP LEJEUNE WWTP - ATAD SLUDGE SOLIDS ANALYSIS
DATE COLLECTED:
DATE RECEIVED:
DATE ANALYZED:
TIME IN OVEN:
OVEN TEMP.
BALANCE CK:
"
TIME COLLECTED:
TIME RECEIVED:
TIME STARTED:
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BALANCE CK:
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FURNACE TEMP:
BALANCE CK:
METHOD: SM 2540 B_E - 2011
A B C D E F G
WT OF DISH
WT OF
DISH+WET
WT OF
DISH+DRY
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
VOLATILE
SOLIDS
°
/°
TOTAL
VOLATILE
%
SAMPLE
SOLIDS
SOLIDS
WEIGHT
WEIGHT
SOLIDS
SOLIDS
RECOVERY
(9)
(g)
(g)
(g)
(g)
(g)
(g)
LOCATION
B A
C - A
[C - DJ
[FIEJ X 100
[GIF] X 100
F-F.rA
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Average of 2 values
QC REPORTED: i�
% Recovery = Results obtained x 100
Known vatue
QC RANGE: I I
CHECKED BY L__
FORM UPDATED MARCH 2O18 COPY MADE

CAMP LEJEUNE WWTP - ATAL jLUDGE SOLIDS ANALYSIS I n(:losure
DATE COLLECTED: TIME COLLECTED: Q%/s COLLECTED BY: 40.lezK -r
DATE RECEIVED: i 1 TIME RECEIVED: $ I RECEIVED BY: (-
DATE ANALYZED: TIME STARTED: D 8 Ll 5- —� ANALYST:
TIME IN OVEN: `� D D TIME OUT OVEN: 0 -7o u �. i� IR TIME IN FURNACE:
OVEN TEMP: 3 °C OVEN TEMP: 1. v 3 • °C FURNACE TEMP: Sq� °C
BALANCE CK: 1 o v • g BALANCE CK: I DO . pv D o g BALANCE CK: ! $ 9
METHOD: SM 2540 B_E - 2011 PERMIT NO. —W00012346
r. (1
SAMPLE
LOCATION
A
WT OF DISH
o
WT OF
DISH+WET
SOLIDS
WT OF
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SOLIDS
WT OF
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SAMPLE
WEIGHT
TOTAL
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WEIGHT
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WEIGHT
%
TOTAL
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%
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soLlDs
°
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ly)
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(9)
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QC REPORTED: -
-
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Known value
QC RANGE: ! I
CHECKED BY w
FORM UPDA1 ED OCTOBI:k 2018 COPY MAI)E

CAMP LEJEUNE WWTP - ATA, -,LODGE SOLIDS ANALYSIS
DATE COLLECTED: ` (-? " TIME COLLECTED: U / LJS COLLECTED BY:
DATE RECEIVED: 9p a 3 I TIME RECEIVED: 1'� D0 RECEIVED BY:
DATE ANALYZED: 1 .7 l TIME STARTED: l`I a S ANALYST:
TIME IN OVEN: 31 TIME OUT OVEN: 1i S C� 1I) TIME IN FURNACE:
OVEN TEMP: p q q °C OVEN TEMP: (p q°C FURNACE TEMP:
BALANCE CK: ia0 D g BALANCE CK: K•�" f-t�r�`y BALANCE CK:
METHOD: SM 2540 B E - 2011 PERMIT NO. WQ0012346
I nclostxe ( .,
We-N'LV,
0-
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sw-v °C
- ! `7. � p 9
SAMPLE
LOCATION
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
%
TOTAL
SOLIDS
%
VOLATILE
SOLIDS
°
/°
RECOVERY
(g)
(g)
t91
(g)
(g)
(9)
[B - A]
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QC REPORTED;
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QC RANGE: f
Ct IECKED BY Vr
FORM UPDATED OCTOBER 20113 COPY MAUL

CAMP LEJEUNE WWTP -ATA, aLUDGE SOLIDS ANALYSIS I-nclosuteI.,
DATE COLLECTED: q- /Q- / 9 TIME COLLECTED: p73a COLLECTED BY:
DATE RECEIVED: Z 3 11 TIME RECEIVED: a 0+7 RECEIVED BY:
DATE ANALYZED: °� L3 1 TIME STARTED: I a� ANALYST: C
TIME IN OVEN: I`( 31 TIME OUT OVEN: 1 i 5 8 C ` - A9.19) TIME IN FURNACE: i 3 31
OVEN TEMP: ID q q C OVEN TEMP: 1 bq -1 q °C FURNACE TEMP: 59-a °C
BALANCE CK: 1 DO . 9 BALANCE CK: q�. �i� t g BALANCE CK: 1 9 T8 9
METHOD: SM 2540 B_E - 2011 PERMIT NO. WQ0012346
SAMPLE
LOCATION
n
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
WT OF
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
WEIGHT
VOLATILE
SOLIDS
WEIGHT
%
TOTAL
SOLIDS
%
VOLATILE
SOLIDS
u
/°
RECOVERY
(g)
(g�°
(g)
(9}
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Knovm value
QC RANGE: I I
CFIECKFD BY
f'ORM UPDAI LD OCtUf1CR 2018 COPY MADE

CAMP LEJEUNE WWTP - ATA- ,LUDGE SOLIDS ANALYSIS
DATE COLLECTED: -�� ( TIME COLLECTED: t_l7 � o COLLECTED BY:
DATE RECEIVED: - oZ - ( TIME RECEIVED: ( Zdv RECEIVED BY:
DATE ANALYZED: �- a _ I TIME STARTED: S C � ANALYST:
TIME IN OVEN: ! S D TIME OUT OVEN: Io `{ I i 2 0 `(-2 - n TIME IN FURNACE:
OVEN TEMP: ( (?q . i "C OVEN TEMP: 03 (°`! `! °c FURNACE TEMP.
BALANCE CK: J tit? • v g BALANCE CK: 9 (`� g BALANCE CK:
METHOD: SM 25Q0 B_E - 2011 PERMIT NO. W0001234G
I nc.loswe 1..
SAMPLE
LOCATION
^
WT OF DISH
WT OF
DISH+WET
SOLIDS
WT OF
DISH+DRY
SOLIDS
W7 OF
DISH+ASH
SAMPLE
WEIGHT
TOTAL
SOLIDS
WEIGHT
VOLATILE
SOLIDS
WEIGHT
%
TOTAL
SOLIDS
%
VOLATILE
SOLIDS
a /a
RECOVERY
(g)
t9`+
(g)
(g)
(g)
(g)
(g)
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IF/EJ X 100
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71
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BENCHSCALE DUP
°h b
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QC TRUE VALUE:
% Dvphcale = Diffewnce:n 2 values x 100
Average of 2 values
QC REPORTED:
`�� Recovery - Results obtained x 100
Known value
QC RANGE: I � I
CIJECK1:DBY V"
FORM UPDAI ED OC TOLIER 20111 C 013Y MADF.

ATAD TRAIL I QUARTERLY SUMMARY
r
Train 1 Feed Train lA Train 1B
Date Volume T Solids V Solids , Temp T Solids V Solids Fecal Coliform Temp T Solids V Solids Fecal Coliform
(gal) % % Deg C % % (MPN/g) Deg C % % (MPN/g)
10/8/2019
5.6
3.60
10/15/2019
5.8
3.11
10/22/2019
5.4
3.35
10/22/2019
5.4
3.35
10/29/2019
4.3
4.23
10/29/2019 4.9 59.8
4.3
46.6
4.23
11/1/2019 18,000
43.5
49.0
11/5/2019
3.5
5.20
11/5/2019
3.5
47.3
5.20
11/12/2019
2.8
7.26
11/12/2019 5.0 60.7
2.8
50.0
7.25
11/26/2019
4.3
45.1
4.22
11/26/2019
4.3
4.22
12/3/2019
3.1
5.73
12/3/2019
3.1
48.7
5.73
12/16/2019 72,000
35.0
37.1
12/17/2019 18,000
32.4
33.1
12/18/2019
25.2
26.5
12/19/2019
28.7
25.5
Comments
Wednesday, February 5, 2020 Page 1 of 3

Date
12/19/2019
12/20/2019
12/20/2019
12/21/2019
12/22/2019
12/23/2019
12/24/2019
12/25/2019
12/26/2019
12/26/2019
12/26/2019
12/26/2019
12/27/2019
12/28/2019
12/29/2019
12/30/2019
12/31/2019
12/31/2019
Train 1 Feed Train 1A Train 1B
Volume T Solids V Solids Temp T Solids V Solids Fecal Coliform Temp T Solids V Solids Fecal Coliform
(gal) % % Deg C % % (MPN/g) Deg C % % (MPN/g)
4.4 65.0 4.5 59.0
18,000
4.4 65.0
34.3
35.4
34.3
35.4
42.0
42.1
50.7
50.7
59.5
59.7
65.6
65.1
68.3
67.5
62.1
63.4
62.1
63.4
62.1
63.4
65.0
65.1
64.1
64.6
62.8
62.7
61.6
60.3
60.4 59.1
4.2 54.4
3.7 51.4
Comments
Wednesday, February 5, 2020 Page 2 of 3

Train 1 Feed
Date Volume T Solids V Solids
(gal) % %
Train 1A
Temp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g)
Train 1B
Temp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g)
No. of Entries
4
4
I 4 {
20 0 0 0
20
17
8
14
Total
126,000
Min
18,000
4
60
25
25
3
45
3
Geom. Mean
25,456
5
63
49 0 0 0
49
4
50
5
Max:
72,000
5
65
68
67
6
59
7
Comments
Wednesday, February 5, 2020 Page 3 of 3

Train 2 Feed
Train 2A
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
10/1/2019
32,400
39.6
10/2/2019
48.0
10/3/2019
9,000
52.9
10/5/2019
18,000
56.0
10/6/2019
59.7
10/7/2019
13,500
61.3
10/8/2019
57.1
10/9/2019
54.9
10/10/2019
44.8
10/11/2019
39.7
10/12/2019
39.4
10/13/2019
40.0
10/14/2019
40.0
10/15/2019
32,400
34.6
10/16/2019
38.4
10/17/2019
46.2
10/18/2019
54.0
10/19/2019
56.6
10/20/2019
57.4
Train 26
Temp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g)
53.5
51.3
58.7
58.8
63.1
62.6
62.0
60.1
49.7
48.2
46.8
45.6
44.3
44.0
51.1
56.8
58.2
54.7
60.1
Comments
Wednesday, February 5, 2020 Page 1 of 6

Train 2 Feed
Train 2A
Train 2B
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp
T Solids V Solids Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
Deg C
%
% (MPN/g)
10/21/2019
53.0
55.8
10/22/2019
54.0
57.9
10/23/2019
59.9
66.3
10/24/2019
18,000
55.8
64.2
10/25/2019
58.8
61.6
10/26/2019
59.2
63.3
10/27/2019
57.8
63.3
10/28/2019
18,000
47.0
55.5
10/29/2019
9,000
40.0
47.4
10/30/2019
42.3
46.2
10/31/2019
3.5 58.3
4.4
49.9
10/31/2019
18,000
43.1
46.9
11/1/2019
18,000
43.5
49.0
11/2/2019
46.2
56.6
11/3/2019
50.3
59.5
11/4/2019
18,000
46.5
58.4
11/5/2019
4.0
49.5
11/5/2019
53.1
62.1
11/6/2019
51.5
60.1
11/7/2019
48.0
48.1
11/7/2019
3.9
50.8
Comments
Wednesday, February 5, 2020 Page 2 of 6

Train 2 Feed
Train 2A
Train 2B
Date
Volume T Solids V Solids
Temp T Solids V Solids Fecal Coliform
Temp
T Solids V Solids Fecal Coliform
(gal) % %
Deg C % % (MPN/g)
Deg C
% % (MPN/g)
11/7/2019
48.0
48.1
11/8/2019
18,000
39.0
50.0
11/9/2019
38.0
52.4
11/10/2019
38.5
50.4
11/11/2019
39.2
55.6
11/12/2019
18,000
36.1
40.5
11/13/2019
18,000
33.4
40.2
11/14/2019
33.3
39.3
11/15/2019
36.1
38.4
11/16/2019
40.6
37.5
11/17/2019
45.5
36.8
11/18/2019
48.4
39.3
11/19/2019
51.7
50.3
11/20/2019
55.8
60.3
11/21/2019
4.9 60.9
4.2 49.2
11/21/2019
27,000
49.3
58.6
11/22/2019
51.9
62.2
11/23/2019
55.8
65.4
11/24/2019
52.4
63.5
11/25/2019
52.1
62.9
11/25/2019
18,000
52.4
63.5
Comments
Wednesday, February 5, 2020 Page 3 of 6

Date
11/26/2019
11/26/2019
11/27/2019
11/28/2019
11/29/2019
11/30/2019
12/1/2019
12/2/2019
12/3/2019
12/3/2019
12/4/2019
12/5/2019
12/5/2019
12/6/2019
12/7/2019
12/8/2019
12/9/2019
12/10/2019
12/11/2019
12/12/2019
12/13/2019
Train 2 Feed Train 2A Train 2B
Volume T Solids V Solids Temp T Solids V Solids Fecal Coliform Temp T Solids V Solids Fecal Coliform
(gal) % % Deg C % % (MPN/g) Deg C % % (MPN/g)
3.5 50.2
57.4
63.0
57.6
60.8
57.6
60.8
56.5
59.5
54.3
57.5
52.1
55.6
45.0
52.4
44.0
52.0
49.2
56.1
56.6
58.0
44.2
50.2
42.7
46.4
49.6
55.1
54.4
58.9
13,500 52.2
58.6
54.2
58.6
60.0
62.0
61.2
63.7
3.7 51.9
3.9 52.0
Comments
Wednesday, February 5, 2020 Page 4 of 6

Train 2 Feed Train 2A
Train 2B
Date
Volume T Solids V Solids Temp T Solids V Solids Fecal Coliform
Temp
T Solids V Solids
Fecal Coliform
(gal) % % Deg C % % (MPN/g)
Deg C
%
%
(MPN/g)
12/14/2019
60.3
63.2
12/15/2019
58.2
62.2
12/16/2019
57.2
59.0
12/17/2019
55.8
56.9
12/17/2019
3.5
52.7
5.08
12/18/2019
55.3
56.1
12/19/2019
53.9
54.9
12/20/2019
52.7
53.1
12/21/2019
51.5
51.4
12/22/2019
50.1
49.7
12/23/2019
48.9
48.0
12/24/2019
47.5
46.7
12/25/2019
45.8
45.4
12/26/2019
4.8
48.8
3.30
12/26/2019
45.6
47.8
12/27/2019
46.6
50.8
12/28/2019
47.0
51.1
12/29/2019
45.5
49.7
12/30/2019
44.1
48.2
12/31/2019
44.1
48.2
12/31/2019
4.0
46.9
4.56
Comments
Wednesday, February 5, 2020 Page 5 of 6

Train 2 Feed
Date Volume T Solids V Solids
(gal) % %
Train 2A
Temp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g)
Train 2B
Temp T Solids V Solids Fecal Coliform
Deg C % % (MPN/g)
No. of Entries
17
i 2
� 2 �
93 0 0 0
93
10
10
3 ,
Total
316,800
Min
9,000
4
58
33
37
3
47
3
Geom. Mean
17,601
4
60
49 0 0 0
54
4
50
4
Max
32,400
5
61
61
66
5
53
5
Comments
Wednesday, February 5, 2020 Page 6 of 6

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
(a-g.7�t`t
b-7
GtJsl;aw,.S
M 9221C E-2aafi (Biosolids}
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
DATE ANALYZED: j o 8 11
TIME ANALYZED: O q ) S-
ANALYZED BY: 0t-
Enclosure (1)
SAMPLE
LOCATION
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX!
100 mL
1
0.1 mL
0.01 mL
0.001 mL
1 mL
0.1 mL
0.01 mL
0.001 mL
-��
rrm�L
V 15
O 15
CJ / 5
15
15
O 15
15
/ 5
DUP
15
V I5
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN: to.? . t DATE OUT: I 0 • $ . 11
TIME IN: [) g 3 q TIME OUT: ha 3 S
TEMP: 3q - S -C TEMP: 3 `f • -C
21 + 2 HOURS AT 44.5 + 0.2'C IN WATER BATH
D S .1 R _ DATE OUT: l O a. i c\
DATE IN:
TIME IN: 1 TIME OUT:
TEMP: - I, 'C TEMP: 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
?C�3
N
DS A-1 BROTH
FORM UPDATED: SEPTEMBER 2019
% TOTAL SOLIDS
MPN Fee. Col.tg =
MPN I GRAM'
� 1
10 x MPN Indexl100ml-
Lowest dilution x % dry solids
CHECKED BY:
COPY MADE:

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
A Cos T�'
M 9221C E-2006 (Biosollds
MCS CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
1 D//��r,,s- � ti
05 00
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Enclosure (1
SAMPLE
LOCATION
3 HRS AT 35 + 0.5'C IN INCUBATOR
21+2 HRS AT ".5 + 0.2°C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX/
100 mL
1 mL
0.1 mL
0.01 mL
0.001 mL
1 mL
0.1 mL
0.01 mL
0.001 mL
f 8
0 )5
15
" 15
}
" l5
O /5
15
15
15
0.0.D
DUP
" /5
/5
DATE IN:
TIME IN:
TEMP:
DATE IN
TIME IN:
TEMP:
3 muuKJ A I Ja +
0 'C
21 + 2 HOURS AT 4&
44.
-C
0.5°C IN INCUBATOR
DATE OUT: 10. (S .,;IV Iq
TIME OUT: `T3�
TEMP: ' C 'C
5 + 0.2°C IN WATER BATH
DATE OUT: to
TIME OUT:
TEMP: 'i `C T -C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
S
FORM UPDATED: SEPTEMBER 201U
% TOTAL SOLIDS
MPN Fec. Col./g =
MPN I GRAM=
tk ,o
3.I1
10 x MPN Index/100ml-
Lowest dilution x % dry solids
CHECKED BY: V
COPY MADE -

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
10 - 2- I 9
%s
tt,l. `}n15
M 9221C E-2006 (Blosollds)
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
l0. n 2a
D�oS
WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
(01
�or0
Enclosure (1)
SAMPLE
LOCATION
3 HRS AT 35 + 0.5'C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX/
100 mL
1 mL
0.1 mL
0.01 mL
0.001 mL
1 mL
0..11 mL
0.01 mL
0.001 mL
B
is
`�' 15
/5
0 15
O l5
v /5
G /5
� 15
D—
DUP
/51
/5
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN: " I DATE OUT: r
0.
TIME IN: 1 TIME OUT:
TEMP: 3 S 'C TEMP: 3 D 'C
DATE IN:
TIME IN:
TEMP:
21 + 2 HOURS AT 44.5
0. a,2- 901
1�
- S -C
+ 0.2°C IN WATER BATH
DATE OUT: I 0 " i
TIME OUT: 01 a�
TEMP: � + -t'J-C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
—
—
DS A-1 BROTH
--
`
FORM UPDATED: SEPTEMBER 2019
% TOTAL SOLIDS
MPN Fec. CoUg =
MPN IGRAM2
3, 35
10 x MPN Index/100mL
Lowest dilution x % dry solids
CHECKED BY:
COPY MADE'

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD.
10-2N--19
c73o
WIt, 4
M 9221C E-2006 (Biosollds
MCB CAMLEJ VWUTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
o1/tD
DATE ANALYZED:
TIME ANALYZED:
fTMWf7i 1U
Enclosure (1;
SAMPLE
LOCATION
3 HRS AT 35 + 0.5'C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX/
100 mL
1 mL
0.1 mL
0.01 mL
0.001 mL
1(�m}L
0.1 mL
0�.001 mL
0.000}1 mL
I>
Q /5
lJ /5
(15
15
" I5
0 15
{f5
/ f5
O 0-0
(%')
DUP
/51
/s
3 /HOURS� AT 35 + 0.5°C IN INCUBATOR
DATE IN: t 0.7" ,ro � G1 DATE OUT:
1ro
TIME IN: t b D J(TIME OUT:
TEMP: '/(� -D •C TEMP:. 'C
DATE IN:
TIME IN:
TEMP:
A I T L Nuuma A l 49.'
O,a'zt.a�tL`j
l�ioy
5 + 0.2°C IN WATER BATH
DATE OUT: O.
TIME OUT: (o��
TEMP: .7- 1 " 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
l�5
DS A-1 BROTH
S
(-/ v
FORM UPDATED: SEPTEMBER 2019
% TOTAL SOLIDS
4-�
MPN Fec. Col./g =
MPN / GRAM;
10 x MPN Index/100mL
Lowest dilution x % dry solids
CHECKED BY: V
COPY MADE:

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
!l / $ f
70
M 9221C E-2006(Biosolids)
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
3 HRS AT 35 + 0.5"C IN INCUBATOR
SAMPLE
LOCATION
1 mL
0.1mL
0.01 mL
0.001 mL
15
D 1.5
� 7
All
� s
DUP
s
(5.-�ko1°I
00oS
WQ1
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
21+2 HRS AT ".5 + 0.2°C IN INCUBATOR
1 mL 0.1 mL 0.01 mL 0.001 mL
t5 �� l
/5
3 HOURS AT 35 + 0.5°C IN INCUBATOR G}
DATE IN: 1i "7 • DATE OUT: "� 1
TIME IN: l TIME OUT:
TEMP: v 'C TEMP: "v 'C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH 4�
DATE IN: ( '!� '1 DATE OUT: 11
TIME IN:
17�?f(_Q TIME OUT: M 7-�
TEMP: t TEMP: L 44' -C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
0 5
DS A-1 BROTH
J 5
r � V
FORM UPDATEDSEPTEMBER 2019
% TOTAL SOLIDS
MPN Fec. Col./g =
Enclosure (1)
cX11 -6,
COMB. OF MPN INDE)U
POSITIVES 100 mL
MPNIGRAMZ
10 x MPN Index/100mL
Lowest dilution x % dry solids
CHECKED BY;
COPY MADE:

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
I].IA •11
0 g 1S
PAx6. y �C
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
o$� 5
WQ12346
DATE ANALYZED: 11, 1;:t- I I
TIME ANALYZED: b tb O
ANALYZED BY: 1.
SAMPLE
LOCATION
3 HRS AT 35 +0.5'C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2•C IN INCUBATOR
45 G Confidence Range
COMB. OF
POSITIVES
MPN INDEX/
100 mL
1 mL
0.1 mL
0.01 mL
0.001 mL
1 mL
0.1 mL
0.01 mL
0.001 mL
18
O 15
0 15
O l5
p 15
15
15
l5
15
DUP
0 15
D 15
D 15
15
IS1
15
I/ /5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS AT 35 + 0.5-C IN INCUBATOR
t • I • 11 DATE OUT:
D 3 Q TIME OUT: 3 a$
34.1 CI TEMP: 1.0
21 + 2 HQUKb Al A
11•la.•t't
13 3e
4 y S •C
4.5 + 0.2°C IN WATER BATH
DATE OUT: I t 13• i R
TIME OUT: 0 $ a�
TEMP: I Liq •C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
Do 95% confidence ranges overlap? YES NO
% TOTAL SOLIDS MPN 1 GRAM'
DS Broth Batch #:
M ECOO - C 11 5
Ex Date.
11.19 . 1 1
SS Broth Batch #
M c O I Q- 0 L Ll
Exp Date
II -
Bottle Batch #,
N
MPN Fec. Gol.lg - 10 x MPN Index/100mL
Lowest dilution x % dry solids
CHECKED BY Pv-
FORM UPDATED NOVEMBER 2019
COPY MADE.

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
/I Zt-/1l
Gp
7 SM 9221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
1I-7-b-I
ALT-
WQ12346
DATE ANALYZED: 4 1 2.6 - kq
TIME ANALYZED: oq 5 $
ANALYZED BY: A LT
SAMPLE
LOCATION
3 HRS AT 35 + 0.5'C IN INCUBATOR
21+2 HRS AT ".5 + 0.2'C IN INCUBATOR
95% Confidence Range
COMB. OF
POSITIVES
MPN INDEX/
100 mL
1 mL
0.1 mL
0.01 mL
0.001 mL
1 mL
0.1 mL
0.01 mL
0.001 mL
1
15
15
l5
0 l5
15
0 l5
0/5
0— O r�
p�
L `. 3
DUP
15
l5
/5
!A/
/5
/5
3 HOURS AT 35 + 0.5'C IN INCUBATOR
DATE IN: I I 'Z CS2 DATE OUT: -
TIME IN: q Z TIME OUT: 1 Z�
TEMP: 'C TEMP:
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE IN: I'2--(.Q 'I©1 DATE OUT: 1 -7 • 1
TIME IN: 1,51;, 7j C) TIME OUT:
TEMP: "1 "I 15 C TEMP: H Luo 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
'P
r.I
Q
DS A-1 BROTH
P
N
I V
Do 95% confidence ranges overlap? YES NO
% TOTAL SOLIDS MPN / GRAM'
OS Broth Batch #:
,;;lpi —0 (P7
Exp. Date:
17- I
SS Broth Batch #:
HO ( .-O (_p
Ex . Date:
CZ. 3 l�
Bottle Balch #:
FjO-FT —OD i
MPN Fec. Coi.)g =
10 x MPN Index/100ml-
Lowest dilution x % dry solids
CHECKED BY
FORM UPDATED NOVEMBER 2019
COPY MADE

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
/ 2 3 /9
j �Z
A �
SM 9221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED
TIME RECEIVED
RECEIVED BY:
PERMIT NO.
WC11
DATE ANALYZED
TIME ANALYZED:
ANALYZED BY:
12��-mac
D� 1�
SAMPLE
LOCATION
3 HRS AT 35 + 0.5'C 1N INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
95'k Confidence Range
COMB. OF
POSITIVES
MPN INDEX/
100 mL
1 mL
0.1 mL
0.01 mL
0.001 mL
1 mL
0.1 mL
0.01 mL
mL
1'('37
D 15
D 15
Q 15
0 15
0 15
D 15
O 15
j0.001
15
r
D "��
D 00
L I
DUP
1 D 151
0 151
D /51
0 15
D 151
D /5
C) /51
O 15
G. �'�
O-0D
i
may, 3 HOURS AT 35 + 0.5'C IN INCUBATOR
DATE IN: , � 0 DATE OUT: ?DM
1
TIME IN: V `'/ v TIME OUT: �� 0
TEMP: 12)15; ' i 'C TEMP: 3 D 'C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE IN: �' �' !� DATE OUT: a �'
TIME IN: TIME OUT: 1 0
TEMP: 'C TEMP: C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
��5
V�
DS A-1 BROTH
fl
Y� I
�r
V U
Do 95 k confidence ranges overlap? YES NO
% TOTAL SOLIDS
MPN I GRAM'
5'-1 �2
DS Broth Batch #
dtprj
Exp Date
SS Broth Batch #
l(��lin���
/
tYtr�rNTi� ' C�L�,
E.p Date
Bottle Batch #
�� 1� 00
MPN Fec Col /g =
10 x MPN Index1100mL
Lowest dilution x 'ta dry solids
CHECKED BY V
FORM UPDATED NOVEMBER 2019
COPY MADE

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
/2• /0•l9
07 Y
I SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL. ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
oD}S
2346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
SAMPLE
LOCATION
3 HRS AT 35 + 0.5•C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
95 Confidence Range
COMB. OF
POSITIVES
MPN INDEX!
100 mL
1 mL
0.1 mL
0.01 mL
0.001 mL
1 mL
0.1 mL
0.01 mL
0.0(0`11 mL
15
D 15
O 15
D 15
0 15
� 15
D 15
(j 15
O— 617
%�•ID ", O O
L �[
DUP
15
l5
l5
l5
15
/51
15
15
3 HOURS AT 35 + 0.5°C IN INCUBATOR GJ
DATE IN: �' L7 ; 'b L DATE OUT: • 1 - 1
a %
TIME IN: Q TIME OUT: ! �7
TEMP: '� N '- 'C TEMP: 1
17/ -v 'C
t 21 + 2 HOURS AT 44.5 + 0.2`C IN WATER BATH i 1
DATE IN: �r' 1V 1 DATE OUT:
TIME IN: t J TIME OUT:
TEMP: 'C TEMP: 44.
• V 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
0
DS A-1 BROTH
OS
V
`'% .11.«
Do 95% confidence ranges overlap?-aG6S-�-rf0 i�1�
% TOTAL SOLIDS
MPN / GRAM2
DS Broth Batch #:
I'tV (�
Exp. Date:
SS Broth Batch #:
(�
`'
Exp. Date:
a �'
Bottle Batch #:
MPN Fec. Col./g =
10 x MPN Index/100mL
Lowest dilution x % dry solids
CHECKED BY: Or
FORM UPDATED: NOVEMBER 2019
COPY MADE:

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
W
1-2
SM 9221C E-2005
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
WQ12346
DATE ANALYZED
�rl��t�_vr_�>lr�a•�
ANALYZED BY:
oq 17)
SAMPLE
LOCATION
3 HRS AT 35 + 0.5'C IN INCUBATOR
1 mL 0.1 mL 0.01 mL 0.001 mL
21+2 HRS AT 44.5 + 0.2•C IN INCUBATOR
1 mL 0.1 mL 0.01 mL 0.001 mL
95•�L Confidence Range
COMB. OF
POSITIVES
MPN INDEXI
100 mL
/5
v 15
/5
/5
/5
/5
15F:
r
O �'
O
C -
/5
�
15
/5
1.5
15
5
/5
} 3 HOURS AT 35 + 0.5'C IN INCUBATOR } ^y
DATE IN: 1� ' W`- 1 DATE OUT:
TIME IN: ?D 11 { TIME OUT:
TEMP: ,, 7r 'C TEMP: . / h �5 'C
21 + 2 HOURS AT 44.5+ 0.2°C IN WATER BATH
DATE IN: (� DATE OUT: 19 t
TIME IN: � TIME OUT: L O O O
Q
TEMP: `+ 'C TEMP: 4,+'+ 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
$S A-1 BROTH
r'y
S A-1 BROTH
D S
� t I✓ �
FOAM UPDATED NOVEMBER 2019
Do 95% confidence ranges overlap? YES O 0.�S•,0--e
% TOTAL SOLIDS MPN / GRAM'
e�-1� 5.o1b
DS Broth Batch #,
to vV tq — p
6c . Date
12.1-7 tj
SS Broth Batch #
VL l '"�D
Ex Date:
Bottle Batch #'
" (���'�
1/�-' t I ~00 ( t
MPN Fec. Col./g = 10 x MPN Index/100ml-
Lowest dilution x % dry solids
CHECKED BY 0—
COPY MADE.

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
SM 9221C E-2006�
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
l WQ12346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
SAMPLE
LOCATION
3 HRS AT 35 + 0.5'C IN INCUBATOR
21+2 HRS AT 44,5 + 0.2'C IN INCUBATOR
95°!° Confidence Range
COMB. OF
POSITIVES
MPN INDEX/
100 mL
1 mL
0.1 mL
0.01 mL
0.001 mL
1mL
0.1 mL
0.01 mL
0..00011 mL
�L
V 15
(D 15
" 15
"' 15
(�`-` 15
/5
/5
/5
�/J
/5
/5
15
/5
/5
/5
/5
l5
�3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN: DATE OUT:
TIME IN: f TIME OUT:
y, r
TEMP: 1�'� 'C TEMP: 'C
21 + 2 HOURS AT 44.5 + 0,2°C IN WATER BATH ++ p�
DATE IN: �� �/ qv t l DATE OUT: � - �D l 1
TIME IN: ko TIME OUT:
TEMP: 444 'C TEMP: 4 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
rJ
1DS A-1 BROTH
O Q',
nj
L�c
v
FORM UPDATED NOVEMBER 2019
Do 95!° confidence ranges overlap? YES NO��
% TOTAL SOLIDS
MPNIGRAM2
DS Broth Batch #
"U,1t
Exp Date
"9'0
SS Broth Batch #
I�
�,t r
try ry I t
Exp. Dated
Bottle Batch #,
' 00
MPN Fec. Cot.lg =
10 x MPN Index/100mL
Lowest dilution x % dry solids
CHECKED BY
vr-
COPY MADE

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
cv St d
SM 9221C E-2006
MCS CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
1;-- ,,� I.7'o lei 1
1 0191b; I
DATE ANALYZED: l 2' 3 1 '
TIME ANALYZED: Q 3t-115
ANALYZED BY: A
3 HRS AT 3S + 0.5'C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
COMB. OF
MPN INDEX/
SAMPLE
957. Confidence Range
POSITIVES
100 mL
LOCATION
1 mL 0.1 mL 0.01 mL 0.001 mL
1 mL 0.1 mL 0.01 mL 0.001 mL
0 15
0 l5
b
G
O' U-
15
l5
/5
15
/5
/5
G .O
15
r5
15
33 HOURS AT 35 + 0.5'C IN INCUBATOR
DATE IN: I Z t DATE OUT:
TIME IN: 005-7 TIME OUT:
TEMP: G'i 'CI TEMP: 5• •C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATER BATH
DATE IN: DATE OUT:
TIME IN: 1 5 Ql TIME OUT: 0 9 0 S
TEMP: LN . `-t 'C TEMP: LA q • �,. 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
fJ
i
N
DS A-1 BROTH
Do 95% confidence ranges overlap? YES NO 6
% TOTAL SOLIDS MPN ! GRAM
t
DS Broth Batch #'
K IF O I R - 072
Exp. Date
' 2 2-b
SS Broth Batch #:
h4C-,b — 01 `
Ex . Date
Bottle Batch #
`i" r D01
MPN Fec. Col./g = 10 x MPN Index1100mL-,-
Lowest dilution x % dry solids
CHECKED BY
FORM UPDATED NOVEMBER 2019
COPY MADE.
t7�

MCB CAMLEJ ELS - TOTAL SOLIDS
DATE TIME
COLLECTED BY: COLLECTED: Q 3 COLLECTED: DOJ { (�
ANALYST: r ANALYZED: Q �'b ANALYZED:
DRYING OVEN 1 JV
BALANCE CK (g} OveEnlght Hr1 Hr2 Hr3
TRUE VAL. OO. 0 TIME IN: 14g1b O b0b (j9-10�
READING (AE100) 19 l -1 )j TIME OUT: 0'j O o J lY ' ��
READING (BO202) - l 1 .q 21 TEMP: FO'�, D 'C to 4-0 •C 1 oi, 'C 10 ( 'C
SM 2540 G•2011
PERMIT NO. W00012346
MUFFLE
Hr4 FURNACE
'G 'C
SAMPLE ID
O�
DISH wT (g)
NO.
10
�1
`7 . t 0
/}�
"J6.400-
WET DISH vvT(g)
`lk.©
,,'q-1
I00- 1 1
1
SAMPLE WT(g)
n.00
2-q,00
d,c; . 00
OVERNIGHT WT (g)
tlt'-�" t�9(�
�}(1.1L� i (
1 91 t
1-HR WT (g)
v
��. �++�
(/l/��. L ��
/
. ��5 g111
a
a
2-HR WT (g)
/J�`
g t%�f
//�--
+U-'(�
!!hh
✓ • � 1 �3
y
WT DIFF (g)*
000
001
O , ()Odd
a
3-HR WT {g}
WT DIFF (g)'
00�
+HR WT (g)
WT DIFF (g)'
TSVVT(g)
i•o�
o
DISH+ASH WT (g)
V1(/•i//''S )
�V•b��
�" "Gr%
VSWT(g)
°
%VW.�{(�
J�'�b YID%
. V
DUP AVG: L} � 0 %DUP: L 2,
1/ OUP = Difference in 2 values a 100
Average o1 2 values
It > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
JUN 2019

MCB CAMLEJ ELS - TOTAL SOLIDS
COLLECTED BY: w&z�y ,
ANALYST: ��
BALANCE CK lo)
TRUE VAL. 1000 TIME IN:
READING (AE100) t l j q eI TIME OUT:
READING (1210202) - I - l 91
TEMP:
DATE TIME
COLLECTED: t 0-�- ��C COLLECTED: 07?-0
ANALYZED: 9V1c( ANALYZED: 1:3,00
SM 2540 G-2011
PERMIT NO. W00012346
MUFFLE
Hr4 FURNACE
'C
SAMPLE 10
D-5
5
71 0 RIP
DISH WT (g)
�if. �
�} (��},7j
UV. �7 1 V
-
I ) -,
WET DISH WT (g)
�.'yf 0
, � 77- -% (P
�9
( 1
SAMPLE WT(g)
'r� •V
?Ic�,•() 0
% �'J o D
OVERNIGHT WT (g)
'rL� •'
M-5-(o
3• (�
1-HR WT (g)
qq��-j
` I (
l
M • 7l51
jj ��'l
n
2-HR WT (g)
1 i• 1 •• 1 V-P
1// 1-5144
1
-j
WC OiFF (9}'
0 . o ©1
V • d 00
0 0 (
a
3-HR WT (g)
I �-, 1 Vl'
V 1
!i Q�
WT DIFF (g)*
0 . 0 00+
D ' � 001
0.0004
4 HR WT (g)
WT DIFF (g)'
TS WT (g)
Cl
0 • J t _ + V
i • i � A
%TS
0
4.D
c
DISH+ASH WT (g)
�j,,
t
W�
VS WT (8)
0.
o.
>
% VW
DUP AVG: L}•� D� °!° DUP: `, L�
' If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
% DUP = Difference in 2 values x 100
Average of 2 values VK
JUN 2019 r"rrVr� �V

MCB CAMLEJ ELS - TOTAL SOLIDS
COLLECTED BY: �ll�-Qjir
ANALYST:
BALANCE CUM
TRUE VAL. I clO TIME IN:
READING (AE100) gq,q-1 V � 2
TIME OUT:
READING (BD202) 4q 9,99
TEMP IN:
DATE TIME
COLLECTED: to • (0. 9-D i�l COLLECTED:
ANALYZED: (() • t 0, -,v) JCJ ANALYZED: I ��
SM 2540 G-2011
PERMIT NO. W00012346
MUFFLE
HR4 FURNACE
'C'� 'C
SAMPLE ID
q(A}�
DISH WT (g)
rr��-fQ-
WET DISH WT (g)
(JJ f -,
! (�
SAMPLE WT(g)
7(�,00
7 ; (J
OVERNIGHT WT (g)
/t L�l.
lV
iO� CA
1-HR WT (g)
-74.411W1
✓l (/•" 1
0
J
2-HR WT (g)
U)
Q
WT DIFF (g)*
(HR1 - HR2)
O n/��
V V
0,000
N
0
3-HR WT (g)
WT DIFF (g)'
(HR2 - HR3)
4-HR WT (g)
WT DIFF (g)'
(HR3 - HRAI)
TS WT (g)
/
% TS
tn o
DISH+ASH WT (g)14.
O�►��
N
VS WT (g)
ry
p. -/q
O .40 (�-7
o
% VS
�}(0.1(0
4 .0
' If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
DUP AVG:
'�- q 1
I
EEI
0 , 12 1
% DUP = Difference in 2 values x 100
Average of 2 values
OCT 2019
U<
CHECKED BY

MCB CAMLEJ ELS - TOTAL SOLIDS
DATE TIME
COLLECTED BY: �� f �` S S COLLECTED: �Q l S_ iv COLLECTED: 0730
ANALYST: ANALYZED: E1C2 j 5. n [� ANALYZED:
DRYING OVEN
BALANCE CK (q) Overn)ght HR11 HR2 HR3
TRUE VAL. i 00. TIME IN: 0 � 4 Lj R9
READING (AE100) 1 4 -qOl 16S TIME OUT: 0110 091s W-5D
READING (BD202) /� (,�` TEMP IN: �J, �. •C Q -C 'a �. •C •C
SM 2540 G-2011
PERMIT NO. WQ0012346
MUFFLE
HR4 EU,RNACE
•C t?:�D 'C
SAMPLE ID
�
_ - ( ((�j
I ( (�/
DISH WT(9)
tFe
blD e(ID (
I .q4j
(bb•u' 24
WET DISH WT (g)
i 1 1.40 0
((')7 (p c5
SAMPLE WT(g)
�� .Q0
Z-19-OD
OVERNIGHT WT (g)%�
1-HR WT (g)
�'jlV` ` �tty("(7�
10
0941
0
2-HR WT (9)
It,/�503
.✓ J 0
r V i
`7
11 0! 1
a
WT DIFF (g)•
(HRi-HR2)
0.000(3-
0 ODb�
0-000
0
3-HR WT (9)
WT DIFF (g)•
(HR2 - HR3)
4-HR WT (9)
WT DIFF (g)'
(HR3 - HR4)
TS WT (g)
1.40
1-4 40b
1 -44UI
o
DISH+ASHWT(9)
iYIY•-(il
v"%(p
NVS
WT (g)
J
°
i. Vs�-
DUP AVG: l ,'1 % DUP: p
% DUP = Difference In 2 values x 100
Average of 2 values
OCT 2019
If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
CHECKED

MCB CAMLEJ ELS - TOTAL SOLIDS
DATE TIME
COLLECTED BY: R (A ,� COLLECTED: 10 (7 -7-0 1 COLLECTED: Q Pj Zt7
ANALYST: ANALYZED: f Q_ (, i7J (q ANALYZED: 073e?
DRYING OVEN
BALANCE CK Iq) Overnight HR1 HR2 NRI
TRUE VAL. (Q Q, Q TIME IN: 1•Ca � �J()�j I' -; 0
READING (AE100) � TIME OUT: 4o ( /f b y 70
READING (SD202) (0 0 -0 (7 TEMP IN: l o • 4 -C•C f (} -C 'C
SM 2540 G-2011
PERMIT NO. W00012346
MUFFLE
HR4 FURNACE
ogo8
og a3
•C SSA •C
SAMPLE ID
DISH WT (g)
fb�•(j%�
'��%•((�%C�
WET DISH WT (g)
[ - (91
� � (1 `
SAMPLE WT(g)
00
" ; - t7 0
OVERNIGHT WT (9)
Cq
-1 4,(f
1-HR WT (9).
/j'
O f��j{G7
4. (pic''JCO
0
a
2-HR WT (g)
,inn
Wf DIFF (g)'
(j %
000-
D 00c/,
Q
(HR1 - HR2)
�/ -
l
F
0
3-HR WT (g)
WT DIFF (g)'
(HR2 HR3)
4-HR WT (g)
WT DIFF (g)'
(HR3 HR41)
TS WT (g)
I . 0
% TS
i. o (o
a
n
DISH+ASH WT (g)
D to . Jr ��
' j D I a'
0
VS WT (g)
J
O
%VS
DUP AVG: %OUP: If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
% DUP = Difference in 2 values x 100
Average 01`2 values
OCT 2019
CHECKED BY

MCB CAMLEJ ELS - TOTAL SOLIDS
DATE TIME
COLLECTED BY: �` I t i $ COLLECTED: (� 1 a (� COLLECTED: O -�
ANALYST: L51ANALYZED: (p a ) ANALYZED: ( a ll -�
DRYING OVEN
BALANCE CK (gl Overnight HR1 HR2 HST
TRUE VAL. ( O 0 , p TIME IN: 3 D 0 p "j D
READING (AE100) '� , 8$ TIME OUT: `Z f) (p p
READING (80202) 91 TEMP IN: p 3 7 'C (d 3 . D °C `C
SM 2540 G-2011
PERMIT NO. W00012346
MUFFLE
HR4
FURNACE
(a(S-
0-738
J 3!5
o7S3
(09_ Lf C
55-Z) 'C
SAMPLE ID
DISH WT (g)
S8. 36 0$
1 :) - 3 1-M
WET DISH WT (g)
t i 5. 13
9 7 3(
�a y
SAMPLE WT(g)
a S' j
a S. 6 "3
go
OVERNIGHT VVT (9)
(p5`�cj
I-3 w,F8
-7P 3185-
1-HR WT (g)
g i (a (e 5�
3 i."1 3
a
2-HR V T (g)
h
WT DIFF (g)"
jjyy /
Q —(
%� j �j
O
(� a j �} q
" _ t�
J
(HR1 - HR2)
li
�/ `' !
�/ • V
4
0
3-NR WT (9)
$-7
3 (Plq 3
3 7
WT DIFF (g)"
(HR2-HR3)
Q. Q i 3
q
D• O O i
4-HR WT (g)
�. (� g `(
-73 (,'l 7 o
-7 . 9 2-
WT DIFF (g)'
(HR3 - HR4)
p. D 0
D.
D0 p 2
TSWT(g)
j. 308t
1. �3-(%
%TS
y -7
in o
DISH+ASH WT (g)
$ B, 9 7
3,
ti
VS WT (g)
ip "1 �sS
D . (e
1
°
% Vs
C 3
DUP AVG: Cj , 3 $ °/. DUP: O ��
% DUP = Difference In 2 values x 100
Average of 2 values
If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
V
CHECKED BY
OCT 2019

MGB CAMLEJ ELS - TOTAL SOLIDS
COLLECTED BY:/��
ANALYST.
BALANCE CK ig)
TRUE VAL. 100 .0 TIME IN:
READING (AE100) 1 �� (� TIME OUT:
READING (BD202) too. oc) 21 TEMP IN:
DATE TIME
COLLECTED: C� 2� ;�o COLLECTED: (r->OQ
ANALYZED: 10 7v) W LOl ANALYZED: no<
Overnight HRi
DRYING OVEN
HR22
HH RI3�
Z�
10';� �2'
SM 2540 G-2011
PERMIT NO. W00012346
MUFFLE
HR4 FURNACE
l 45d
15�7
SAMPLE ID
a
c/�I Q�r
DISHWT(g)
� �j. l
�j,� 11
J�-`tq
r���
✓l,`.{�+i//'fS,�j�
% ,)rvj{
WET DISH WT (g)
1 d0 • k o
I 1 (-Cy,,-J
11 l [ /
1�
-fits l
SAMPLE WT(g)
0,5 A"c/"�G
��Dt�
{1
% p ✓��
OVERNIGHT WT (9)
(�,t!
na V
6-7.. t;
%
';I
7J%
1-HR WT (9)
l)
f'-�
(f�)t(p
��y
a
2-HRWT(9)
�"t�I - c5�r�t�riV
IV. 1 Tl!/
y
J
WTDIFF (9)•
(HR1 -HR2)
Q.C�
O.ob4'�
O.0001
0.00(
0
3-HR WT (9)
1 �f 7
V I j
V�.���
`�•'i �P '
WT DIFF (g)'
(HR2-HR3)
O�O
00�'
f
0.000
O,QOO
4-HR WT (g)
WT DIFF (9)'
(HR3-HR4)
TS WT (g)
00%�
i S
},r� r .
0 --/"tc,-
% TS
L
o
DISH+ASH WT (9)
ry0
1 V
�J (
H
VS WT(9)
�
% VS
DUP AVG: I. jA:� 7. DUP:
% DUP = Difference in 2 values x 100
Average of 2 values
If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
V
CHECKED BY
OCT 2a19

MCB CAMLEJ ELS - TOTAL SOLIDS
DATF TIME
COLLECTED BY: 4 t j W C7 COLLECTED: I �, �� COLLECTED: a� O D SM 2540 G-2011
!
ANALYST: ANALYZED: l • ?'D t ANALYZED: + y� D PERMIT NO. W00012346
DRYING OVEN MUFFLE
HR4 FURNACE
BALANCE CK La1 DVernIght HR1 HR2 HR3
TRUE VAL. 100.0 TIME IN: �at� �}-l�� 10I5-
READING (AE700) I I . - 1 (� TIME OUT: V1 i Vo
v
READING (50202) 0O 0 TEMP IN: 10�. 'C iQ rf. L� 'C +(�%I 'C 'C 'C t55DAc
SAMPLE ID
�3
DISH WT(9)
WET DISH WT(g)
SAMPLE WT(g)
OVERNIGHT WT (9)
�
1-HRWT(g)
-C1
� -lbq 1
����LrJ
T "`'��
0
2-HR WT (y)
q✓�dl
J
Q
(HR1-HR2)
H
3-HR WT (g)
WT DIFF (g)'
(HR2 - HR3)
4-HR VVT (g)
WT DIFF (g)'
(HR3-11134){
TS V1IT (9)
!
[ OU-7
^�
1 ocpc l _
TS
o
DISH+ASH WT (g)
7�•����/
IlU. /U�
��% �tY ✓Q
J
h
VS WT (9)
D r l� o
l i
O• l�j
o
%VS
q.io
,4
DUP AVG: >te
% DUP = Difference in 2 values x 100
Average of 2 values
• If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
VX
CHECKED BY
OCT 2019

MCB CAMLEJ ELS - TOTAL SOLIDS
DATE TIME
COLLECTED BY: A c
COLLECTED: / O COLLECTED: O SM 2540 G-2011
ANALYST: ANALYZED: �� dj� yp ANALYZED: V (}� PERMIT NO. W00012345
DRYING OVEN
BALANCE CK la1 dvernlght HR1 HR2 HR{3� HR4 FURNACE
TRUE VAL. oo. V TIME 1N:
READING (AE100) TIME OUT: �� �V ' /O 1000 1 �7n 1
99') V
READING (BD202} G1 TEMP IN: la`'� •C �� '� �V'/-lam 'c �. 'o C /- " •C
SAMPLE ID F 2 f e/����rLY1L�IC,S ' 'r1L�1JS�'4�►l{L�
DISH WT (g) �i 'n10� 0 6� "TU �' / (-P1'
WET DISH WT (g) 1�� l t70 G✓^`-//� l �' 2 I
SAMPLE WT(g) L.r17 1 p sty, • �r,�
OVERNIGHT WT (g) �� `�U1 f• 31� 16.0
`J V� (1,
1 HR T (g1 AA �, v' Jy �((�Jy b � (0
UV�1}
Ul
2-HR WT (g)
h WTDIFFR(g)' WV t 0.0 0 0 QD©
0 3-HRWT(g) '����r 1�l/ �7 ✓��1' ���(/
4-HR WT (g)
WT DIFF (g)'
(HR0 - HR4)
o DISH+ASH WT (g)
N VS WT (g) b •D 5 l a �j r'1 0.
DUP AVG: l .�% `% If > 0.5 mg (O.000S g) sample must be dried for an additional hour.
F
% DUP = Difference in 2 values x 100
Average of 2 values
CHECKED BYO
nrr gn,a

COLLECTED BY: w ALL ,t�
ANALYST: Ea
BALANCE CK Ial
TRUE VAL. 1000 TIME IN:
READING (AE100) � TIME OUT:
READING (BD202) Gflji ��� j TEMP IN:
MCB CAMLEJ ELS -TOTAL SOLIDS
DATE
COLLECTED: I j S/ I q
ANALYZED: �� (J. 0
TIME
COLLECTED: O t VS
ANALYZED:
SM 2540 G-2011
PERMIT NO. W00012346
MUFFLF
HR4 FURNACE
t oo�
ion
•C •c
SAMPLE ID
DISH WT (9)
WET DISH WT (9)rj
SAMPLEWT(9)
(� l
7�i�
OVERNIGHT WT (9)
�}f)•LJ•2
1-HR WT (9)
. �
1 . q 5
�t:�• l 1
0
. 41 I2
2-HRWT(9)
4J`J "T
N
WT DIFF (9)'
IiR2)
oi�t}
0002-
0. bo V�
Q
r
(HR1 -
0
3-HR WT (g)
WT DIFF (9)'
(HR2 - HR3)
4-HR WT (g)
WT DIFF (g)`
(HR3 HR4)
TS WT (g)
0•�q�t�1 i
0. �b(0�1�1
p �✓��t
o
DISH+ASHWT(9)
�/i
14•�-Dt
o
°% vs
OUP AVG: �J-q % DUP: 0-1 ` if > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
% OUP = Difference in 2 values x 100
Average of 2 values
nr r ?rn a
CHECKED BY U

MCB CAMLEJ ELS - TOTAL SOLIDS
DATE TIME
COLLECTED BY: t COLLECTED: -1 lR COLLECTED: 00
ANALYST: ANALYZED: 1_ t, i q ANALYZED: y
BALANCE CK (Q)
TRUE VAL. 1 DO • Q
READING (AE100) 1 . j q 83
READING (8D202) I Oh - n a
TIME IN: I I
TIME OUT: dJ SB
TEMP IN: I o Ll
HR1 HR2 HR3
04-.;1,1 Icy
b"Ix1 134s
t0q.0 104- 204.0 •c
SM 2540 G-2011
PERMIT NO. WQ0012346
MUFFLE
HR4 FURNACE
t of
141%e
.c -c
r
SAMPLE ID
-- s
Pei�c(n $Gµt(�Gr(tb
DISH WT (g)
$� U S 33
e:33
-7 3 , a 9 81
WET DISH WT (g)
1 t 5. 0 3
11►e . 3
`1 g. `� 3
SAMPLE WT(g)
.Z V. 39
Ll
OVERNIGHT WT (g)
%1 . � l i{7
'-7S- o 6 q q
`13 . Sb Ll3
1-HR WT (g)
$9. � 41;-0
IT. vie
-7 3.5G 3b
Ck
2HRWT(g)
$q. �I�
7S-O
3. 5(,;a -7
OIn
J
WT DIFF (g)•
(HR1•HR2)
O.oba3
e.oal�
goo
4
0
3-HR WT (g)
5-o(* 3
-7
WT DIFF (g)'
(HR2 - HR3)
0.0005
0. O Q
4-HR WT (g)
WT DIFF (g)•
(HR3, HR• )
TSWT(g)
1. o�JSLJ
%TS
S -1 q
o 3
.03
a
DISH+ASH WT (g)
$ t - i 4 L(ID
-7 Ll • 8 SI 1
"r S . L.1 3o a
.J
N
vswT(9)
p.S�"1i
p.Pt-
o.t324
J
°
%VS
so a;1.
S°•ti$
so-:1
DUP AVG: I _ 03 °I° DUP: ' if > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
% DUP = Difference in 2 values x 100
Average of 2 values
CHECKED BY L _
OC T 2019

COLLECTED BY:
ANALYST:
BALANCE CK fnl
TRUE VAL. 100. ,p TIME IN:
READING (A£100) 1 Q $ 3 TIME OUT:
READING (1313202) 100 rn ni TEMP IN:
MCB CAMLEJ ELS - TOTAL SOLIDS
DATE
COLLECTED:
ANALYZED: t 3 1 c>{
TIME
COLLECTED: D a (s SM 2540 G-2011
ANALYZED: ( PERMIT NO. W00012346
RYING OVEN MUFFL
HR2 HR3 AP
14 RNAC
4ta aI
az
rjU U .0 �� � 55-0 C
SAMPLE ID
F:"
b
DISH WT (g)
g� D� s
S , 5ya8
WET DISH WT (g)
lg7.
103 • 01
SAMPLE WT(g)S-S-
OVERNIGHT WT (g)
$-? . s i t, S
-7
g- -Sy�R
"Ib. So3 1
1-HRVVT(g)
3
2-HR WT (g)
g"l S
'7
O
Q
WT RIFF (g)'
(HR1 - I-IR2)
0
I-
0
3-HR WT (g)
WT DIFF (g)'
ulR2 HR3)
4-HR WT (g)
WT DIFF (g)'
(HR3 - HRAI)
TS WT (g)
%TS
-5 •t3
In
DISH+ASH WT (g)
8 Ll b
7 s. 2.1 If
J
N
VS WT (g)
0 .�#' ID a t
0L
°°iVS
1ao.�3
3
DUP AVG� 1 _ % DUP: ' If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
% DUP - Difference in 2 values x 100 a
Average of 2 values Sc L
CHECKED BY
OCT 2019

MCB CAMLEJ ELS - TOTAL SOLIDS
TIMF
UAic _ -�
COLLECTED: _ COLLECTED: ) J SM 2540 G-2011
COLLECTED BY: � `t � '�+�
PERMIT NO. W00012346
ANALYST: ANALYZED: , `� t ANALYZED: O
DRYING OVEN MUFFLE.
HR4 FURNAC
BALANCE CK (o) Overnight Hill HR2 HR3
TRUE VAL, t�� . TIME IN: !K
READING (AE10(l) f `�t� TIME OUT
READING (BD202) TEMP IN: t��• 'C �%J. C �0 'C
SAMPLE ID
DISH WT(9)
�� ��"'bLY•
[u "/
�� `r,lvj,
�Vy
WET DISH WT(9)
-[�LY�
tti•4l
���V %
I' %,�
SAMPLE WT(g)
j . {0" l(/�-
ry,
�y,7. � %
o J "0qI
p�L;
�¢,�qC`►r
OVERNIGHT WT (g)
-16- �p� I�
r�0
V'j7��/J,�
��?,I o (qp
��/
1-HR WT (9)
'j 1p� (zo
IU��
'U i9/%-i/�-
/. I 1
5
tn fa
2HRWT(g)
���•ll�iJ57
V t1l� 1
/• V t/�
Qt,
a
WTDIFFIV
00004
0 ioo<
0.000 (J
0•000
J
4
t-
(HR1 tip?)
0
3-HR WT (g)
WT DIFF (g)'
(HR2 HR3)
4-HR WT (g)
WT DIFF (g)'
(HR3 - HR41
TS WT (g)
TS
a
DISH+ASH WT (9)
(9•1 /-1
0.1 J\�?
VSWT(g)
A
>
%VS
t-I
tpO•V
�
D
FDUP AVG: 5 • t� %DUP: O .
If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
4 Ot1P Difference in2 values x 100
Average of 2 values
rx- T •us ra
CHECKED BY b

MCB CAMLEJ ELS - TOTAL SOLIDS
DATE TIME
COLLECTED BY: �S r COLLECTED: COLLECTED: c 7 t/O SM 2540 G-2011
ANALYST: ANALYZED: �� ANALYZED: D PERMIT NO. WQ0012346
DRYING OVEN MUFFLE
HR4 FURNACE
BALANCE CK {p) OVemlpht HR1 HR2 HR3
TRUE VAL. 0d ,O TIME IN: 1��' V�Y �� to (I
READING (AE100) TIME OUT: 01 ��/ �� o i O�{�
1
READING 100202) C� �.C/1 TEMP IN: 'C ,1)�, 4 •C 104-"O 'C •C C 'J (/ •C
SAMPLE ID
2..
r
PiGVtS(
�v-t}r�licrMQv O�
DISH WT(9)
�%.R
{�
OCY
1O.
WET DISH WT (g)
�%%
yDT%
i 1
`t -Qkl
SAMPLE WT(g)
f��6y
OVERNIGHT WT (g)
/�
14. 1(y-i//9��-
G � �1
(
(�Ir 3,
il(J,�7 /) l�
/ "
�a U 2Q0
i HRW7{9)
�Q�l�
y(Ul
((✓
SLY
(jU,o�4
2-HR WT (g)-1}}
O
to
WT DIFF (g)'
o Do�
o• 000 4
0 0o o
0-00 1
--J
(HR1 HR2)
V
Q
H
0
3-HR WT (g)
WT DIFF (g)'
(HR2 - HR])
4-HR WT (g)
WT DIFF (g)'
(HR9 - HR4)
TS WT (9)
Q�yU,
o
DISH+ASH WT (g)
�f l� V
Y/�. lX%�1
��.��
l? ,41
O
U)
VS WT Ig)
p.
o. "t rl
>
%VS
DUP AVG: `•U �� % DUP: o
• If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
% DUP = Difference in 2 values x 100
Average of 2 values
CHECKED BY
ru-T 9n i a

MCB CAMLEJ ELS - TOTAL SOLIDS
DATE TIME
COLLECTED BY: ��(7� j� COLLECTED: �a �t� COLLECTED: �� SM2540G-2011
ANALYST: ANALYZED: �a•� �101I ANALYZED: ILO PERMIT NO.W00012346
DRYING OVEN MUFFLE
F RN C
BALANCE CK IM Overnight HR HRR HR3 HR4
TRUE VAL. 0 • (� TIME IN: t �L{ rt"t J 1 0 p c) I? (;v 0�-7 try,
READING (AE100) , TIME OUT- �7,4`� o
READING (BD202) � � -OilTEMP IN: � (� � .� •C `OL , LP -C t o� , � 'C 10A - 0 'C c rj� -C
SAMPLE ID
�f�/�
TI �
DISH WT (g)
U�
rj ���v
(},'(j
l/ 1 ?7
-7 4.�% "/ V
WET DISH WT (9)
0..45y -
``.
lei - 1�J%�)}
SAMPLEWT(g)
��.�-1�i^
�' ����
�4-.61"1-I/-
OVERNIGHT WT (g)
L L}��'
�%L� �-
�� •, I ��
1-HR WT (g)
e�,�
0
2-HR WT (g)
�%. ���
VI�J. �'�/f"
✓ l `��I
J
in
WT DIFF
17•1?o,
0.0n10
v•ODl.,5
HR1-HR)
0
3-HRWT(9)
��."c�K
✓tY.i/��O
�`�•��
VYTDIFF
0 (990
0 00O�
0 000�-
(HR2 HR3)
3)
4-HR VVT (g)
WT DIFF (g)'
(HR3 HR4)�j
TS WT (g)
'� 1
•� �t
d •� (b 1
%TS
��j/
�% i
1�
�' `�
in
DISH -ASH WT (9)
-nnCy,
��"%•
In
>
L---
% VS
L_
DUP AVG: % DUP: 3
Difference in 2 values X 1 oG
DUP
Average of 2 values
If > O.s mg (0.0005 g) sample must be dried for an additional hour.
CHECKED BY
OCT 2019

MCB CAMLEJ ELS - TOTAL SOLIDS
THUG
COLLECTED BY: COLLECTED: COLLECTED: Oy D SM 2540 G•2011
Ctl f c.t I .�'r� S r� ' S.• 1 �f
ANALYST: ANALYZED: �'� - CI- l ANALYZED: PERMIT NO. W00012346
DRYING OVEN MUFFLE -
HR4 FURNACE
BALANCE CK OVrarnight HR1 HR2 HR3
TRUE VAL. 0 -'� TIME IN: i C� O 4 l A-O
READING (AE100) TIME OUT: 01 4 i l jo
READING ($13202) �. TEMP IN: �I_ 'C , �) °c 'c -c •c •c
SAMPLE ID
`
�
DISH WT (g)
/Ip
WET DISH WT (g)
SAMPLE WT(g)
�� -�✓I l
OVERNIGHT WT (g)
• lI/ taj
1-HR WT (g)
0
2-HR WT (g)
a
VVTDIFF (g)'
(IiRi - I IR2)
�•000�
0 000
Q
a—
Q
3-HR WT (g)
WT DIFF (g)'
pIR2 HR3)
4-HR WT (g)
WT DIFF (g)'
(HR3 - HR4)
TSWT(g)
`i!�
/l ,,
Q.CACY'�7
r---./.Ts
o
DISH+ASH WT (g)
U)
'� 66
rr^, rp_
U �LU/
VS WT (g)
-j
o
% VS
{
F
UP AVG: �J, % DUP:
% DUP = Difference In 2 values x 100
Average of 2 values
If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
CHECKED BY V
OCT 2019

COLLECTED BY: AGdS-�—
ANALYST:
BALANCE CK fW
TRUE VAL. 100.0
OD•O TIME IN:
READING (AE100) 1 100. p0)� TIME OUT:
q,
READING (BD202) .G`` j TEMP IN
MCB CAMLEJ ELS - TOTAL SOLIDS
DATE TIME
COLLECTED: ! COLLECTED: Q 7 IS
ANALYZED: (p, yp (� ANALYZED:
Qvernlaht HR1
IWko D oo
015 �000
10q, p p -c
HR2 HR3
011� 1171 0
II(5I
SM 2540 G-2011
PERMIT NO. W00012346
MYLF—L!i.
HR4 FURNACE
01 1 c)
U-77S"�
•c �1f�m •c
SAMPLE ID
- j• Z
Qf
'`
DISH WT (g)
�LZ�(
p�/i_
WET DISH WT (g)O,I�
SAMPLE WT(g)
�J T
rr __ jj�
I : �"l LY `f'
?L� , �� 19
OVERNIGHT WT (g)
�}�(�
, -q.(fl o 4
1-HR WT (g)��'��j�}�
�-�
(00
in2-HR
WT (g)
�1
C) •�JD
��V
in o
4
WT DIFF (g)'
(HRt-IIR2)
f,%•OD(/r1/'
/nt �,, ,QQp
V DDG�ry,
�}
0 0cl ?"�—
0
3-HR WT (g)
I(� r �(�
J 'l O
✓ ' ����
WT DIFF (g)'
(1(R2-1)113)
0,000 '
0 ooa
o. 000�
4-HR WT (g)
WT DIFF (g)'
(14143-IIR,I)
TSWT(gi
(� /�/�y�
(J, 11v./
/� /fir
�llF'
/�} (_
I /4k, l
%TS
%.�
!�. (14
v,
DISHtASH WT (g)
G�� 0
1�.j��,���Q�
YJ �0• v' ' V
�j . UL�
in
VSWT(g)
�'-l�`T�
�lJ�v-(�'^
�•CO�j�
r
a
%V5.Q�,
DUP AVG: r VJ�� % DUP: 0-9—
% DUP = Dilference in 2 values x 100
Average of 2 values
OCT 2010
If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
CIIECKED BY V

MCB CAMLEJ ELS - TOTAL SOLIDS
DATE TIME
COLLECTED BY: COLLECTED: COLLECTED: 071
v
ANALYST: ANALYZED: 12 la ANALYZED: t %j
DRYING OVEN
BALANCE CK (M OYefnlght HR1 HR2 HR3
TRUE VAL. ! Lo TIME IN: { "t v D'� / a��00
READING (AE100) G( j _qq j bc,7 TIME OUT 0100
READING (BU202) ` ' l -1,�� TEMP IN: .0 (0� b9 ^C � 0+0 'C 'C
SM 2540 G-2011
PERMIT NO. WQ0012346
MUFFLE
HR4 FURNACE
WI`7
(D�i�
'C 'C
SAMPLE ID
FF5,Q
z
DISH WT (9)
(� S
�{
}1
r2
w w
WET DISH WT (g)
l7%. j
"I -A?c
i � { 01
SAMPLE WT(g)
OVERNIGHT WT (g)
-a/�- {�a/ -,
UPI
1-HRWT(9)
(Ob
0
2-HRWT(9).�1r7�
I %•7�i%'
�IQ. "I�
J
WT DIFF (g)•
0.0 0 0 -? 7
0. 0 D 0 2,
Q
(HR1 • I1142}
0
3-HR WT (9)
WT DIFF (g)'
(I I42 - HR3)
4-HR WT (g)
WT DIFF (g)-
(I W3 - HR4)
TSWT(9)
��y
0•o j lO
/}
o
DISH+ASH WT (9)
cAV
i . j "1 " -�
6& 4 e"I
N
VSWT(g)
++?t
DUP AVG: !%•�� %DUP:
% DUP = Difference in 2 values x 100
Average of 2 values
If > D.5 mg (0.0005 g) sample must be dried for an additional hour.
CHECKED BY
nr.T an 1 r

MCB CAMLEJ ELS - TOTAL SOLIDS
. A ./1111 TIMP
Ur+i c
COLLECTED BY: i1 COLLECTED: i _ _ 1 f COLLECTED: h � - SM 2540 G-2011
V )t LI
ANALYST: ANALYZED: I 1 j Q t ANALYZED: t 9,7 PERMIT NO. W00012346
DRYING OVEN MUFFLE
HR4
nnF�UR(N'A�CE
BALANCE CK ln) Overninht HR1 HR2 HR3 V �-
TRUE VAL. I O�- TIME IN: `!� l l ! -1)2-0 V 1 J
READING (AE100) t� ��TIME OUT: Q> IO Z 01 /
REARING (80202) ( D O , Oo TEMP IN: l wl! 'C 6 • lJ �� C �C •C
SAMPLE ID
DISH WT (9)
7i{.(p'jj�p
Cj"I t0
WET DISH WT (9)
't,
q , U (0
�^ 0.6 U/
SAMPLEWT(4)
ERNIGHT WT (g)
^\U
'��j •���%
�/ . i (b
1-HR WT (g)
�J � O
f/ 112a A
q
W
2-HR T (9)
i l. Q I
(� • "-4 I
9
ch
0
WTDIFF (g)'
0 00p�}
{�•ODQ/
Q
(HRI -HR2)
I-
0
3-HR WT (g)
WT DIFF (g)'
p IR2 - HRJ)
4-HR WT (9)
WT DIFF (g)'
(HRJ - HR4)
TSWT(9)
°!o TS
o
DISH+ASH WT (9)
1�1+
N
VSWT(9)
,�},
D.4t/bf
o
%VS
��
�j� •z✓lU
DUP AVG, �%• �J _°!o DUP: ��
% DUP - Difference in 2 values x 100
Average of 2 values
If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
CHECKED 0Y W-
OCT 2019

MCB CAMLEJ ELS - TOTAL SOLIDS
nnTr- TIME
COLLECTED BY: COLLECTED: 7- / COLLECTED: ©17DO SM 2540 G-2011
ANALYST: ANALYZED: �a , .'j17 ( ANALYZED: D� PERMIT NO. W00012346
NfEl
DRYING OVEN MUFFLE
BALANCE CK (n} Qverninht HR1 HR2 HR3 HR4 fURNACI
TRUE VAL. `() (? ,D g TIME IN: ! t o c) 0 MOO
READING (AE100) D'!� .�"t �j TIME OUT: 01 (� O6
READING (e0202) G(,f TEMP IN: l O(� ri 'C 1 'C
(
SAMPLE ID
{ ICJ QV
DISH WT(9)
WET DISH WT(g)
SAMPLE WT(g)
,`�
o4
OVERNIGHT WT (g)
• "q i,
1
U-, . a., I,p(
M. tG
1-HR WT (g)
4
0
2-HR WT (g)
a
w
WT DIFF (g)"
-Q©�
O O00
J
(HR1-Hl22)
a
r
0
3-HR WT (g)
WT DIFF (g)'
(# 012 - 11143)
4-HR WT (g)
WT DIFF (g)'
(HR3. 1034)
TSWT(g)
1
a
DISHrASH WT (g)
V
N
VS VVT (g)
o
%VS
l"✓ "1.�
DUP AVG:
9L OUP = Ddference in 2 values x 100
Average of 2 values
• If > 0.5 mg (0.0005 g) sample must he dried for an additional hour.
CHECKED BYE
OCT 2019

MCB CAMLEJ ELS - TOTAL SOLIDS
TIMF
COLLECTED BY: COLLECTED: COLLECTED: SM 2540 G-2011
CASTS? � f`fi
PERMIT NO. WQ001234G
ANALYST: ANALYZED: i/) 7LO/fjp tcl ANALYZED: ��} �-
DRYING OVEN MUFFLE
HR4 FURNACE.
BALANCE CK Icy) Overninht HR1 HR2 HR3
TRUEVAL. p 0 TIME IN: �`�}� p��o �'fl'j P24�
READING (AF100) 1
1 1 t- I b TIME OUT: 01 J W 1010 I n
READING (sD202) TEMP IN: O 'C ��L� 'C'G 'C 'G 'C
SAMPLE 10
7-1/3
e�,j�(r
�a-97
DISH WT(g)
j
VL,04,a�lG'
��7•`�l 'lY
�� f�/,�`J
WET DISH WT (g)
I �O/`,}{
I C��'Cj
I I � -4 O
SAMPLE WT(g)
�" V 1�
�.
�� �-" 1
�S 0149
OVERNIGHT WT (9)
`" -O V O V
I (/ V"T{
z�}1,� ✓ 0 v
1 cy• 2 1`(
1-HR WT (g)
��
(U� ��V
V�. 1310
2-HR WT (g)
M. V 1
(D
I tl/ • lY J Q
U . Q
f((/bi-I�"�
-1 J' Z ( (
a
WT DIFF
o-000+
oov(�
6)-DaQ<
r
0
3-HR WT (9)
WT DIFF (g)'
(I II12 -1IR:J)
4-FIR WT (g)
WT DIFF (g)'
(HR3 • 1-1114)
TSWT(g)
�}7,,
��U/�
Mb
in
DISH+ASH WT (g)
� ICJ. � 66
� � • "l �i1
D (- a 11
-15' y�`jT 9-
w
VS WTig)
p.y ��
0. 1 t6l
0.'5
�.(i t Ip
>
°
°� �S
���(�
t��.�
�� v9-
QUP AVG: " � F/.-DupT-
b L -- I
- I
% DUP - Ddfelence in 2 values x t00
Average of 2 values
If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
CHECKEDBYY'
OC T 2019

MCB CAMLEJ ELS - TOTAL SOLIDS
MATE! TIME
COLLECTED BY: COLLECTED: 5 COLLECTED: ,, SM 2540 G-2011
5{�
—co
ANALYST: iX ANALYZED: pf1'�J' (. (� • Z-0 ANALYZED: 00 PERMIT NO. W00012346
DRYING OVEN MUFFLE:
FURNACE
BALANCE. CK In) Overnight HR1 HR2 HR3 HR4
TRUE VAL. �00-0 TIME IN: 13'3Q pq 1-1 101315 1 t W y
READING (AE100) TIME OUT: OQ po to (v 1 3s 1159
i
TEMP IN: `D�3 • p 'c (o-j •o �`= (D 3 • H .c •c •C G55 p •c
READING (a0202) t l t�
`
SAMPLE ID
— 2
DISH WT (g)
2L - ft•
32
��• l�
WET DISH WT (9)
i« .
- q- 61
�D^� • �-,'. k
SAMPLE V%T(g)
%5 •q�}
?� .t/�O
`' l
OVERNIGHT WT (g)
g� 3Sgt�
-TS . 3yy8
i-HR WT (g)
$'� , 9j3�J3
3( %�
cc 1 q3
2-HR WT (g)
-7. $33a
']5 . 3t 2
`Xp • (� t y o
J
D
WT DIFF IV
(ItR1-IiR2)
0.0003
o•oao3
0• o00 3
a
r-
0
3-HR wr (g)
WT DIFF (g)•
(1IR2 043)
4-HR WT (g)
WT DIFF (g)'
(HR] - ftR4)
TSWT(9)
ID.9 2 C6Le
0.9'B$5
►. t7(P93
%Ts
3,U5
3.95
3.95
o
DISH+ASH WT (g)
13G. K6 0
14. JS
la t. E
J
VS wr (g)
() , y`t`7
tl� y y I
0. 9�?03
>
% VS
1, 3� lev.
w
'-f?, a
DUP AVG: '.� , 9 rj °I• DUP: Q
'Y DUI' Difference in 2 values x 100
Average of 2 values
• If > 0.5 mg (0.0005 g) sample must be dried for an additional hour.
CHECKEDBYVc
oCT 2019

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 12/18/2019
Report No.: 2019-0005 Lab ID: 227
Sample ID:
T1B
Date
Collected:
12/10/2019
Collected By:
ACOSTA
Time
Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.65
%
12/10/2019
SM 2540 G
AYO
% Volatile Solids
44.64
%
12/11/2019
SM 2540 G
AYO
Fecal Coliforms
3.19
MPN/gram
12/10/2019
SM 9221 C E
AYO
Sample ID: T2B Date Collected: 12/10/2019
Collected By: ACOSTA Time Collected: 0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.79
%
12/10/2019
SM 2540 G
AYO
% Volatile Solids
53.06
%
12/11/2019
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID: FEED Date Collected: 12/12/2019
Collected By: WILLIAMS Time Collected: 0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.23
%
12/12/2019
SM 2540 G
AYO
% Volatile Solids
61.82
%
12/13/2019
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E

Sample ID: T2B Date Collected: 12/12/2019
Collected By: WILLIAMS Time Collected: 0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.57
o
12/12/2019
SM 2540 G
AYO
% Volatile Solids
52.79
%
12/13/2019
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Certified By:
L REN D. ACOSTA

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application Date of Report: 01/08/2020
Report No.: 2020-0001 Lab ID: 227
Sample ID:
T2B
Date
Collected:
12/17/2019
Collected By:
WILLIAMS
Time
Collected:
0855
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.54
%
12/17/2019
SM 2540 G
AYO
% Volatile Solids
52.67
%
12/17/2019
SM 2540 G
AYO
Fecal Coliforms
5.08
MPN/gram
12/17/2019
SM 9221 C E
AYO
Sample ID: T1B Date Collected: 12/19/2019
Collected By: ACOSTA Time Collected: 0900
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.45
%
12/23/2019
SM 2540 G
AYO
% Volatile Solids
58.95
%
12/23/2019
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID: FEED Date Collected: 12/26/2019
Collected By: ACOSTA Time Collected: 0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.42
%
12/26/2019
SM 2540 G
AYO
% Volatile Solids
64.99
%
12/26/2019
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E

Sample ID: T1B Date Collected: 12/26/2019
Collected By: ACOSTA Time Collected: 0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.15
%
12/26/2019
SM 2540 G
AYO
% Volatile Solids
54.36
%
12/26/2019
SM 2540 G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID: T2B Date Collected: 12/26/2019
Collected By: ACOSTA Time Collected: 0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.75
%
12/26/2019
SM 2540 G
AYO
% Volatile Solids
48.82
%
12/26/2019
SM 2540 G
AYO
Fecal Coliforms
3.80
MPN/gram
12/26/2019
SM 9221 C E
AYO
Sample ID: T1B Date Collected: 12/31/2019
Collected By: ACOSTA Time Collected: 0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.65
%
01/06/2020
SM 2540 G
ALT
% Volatile Solids
51.37
%
01/06/2020
SM 2540 G
ALT
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM 9221 C E
Sample ID: T2B Date Collected: 12/31/2019
Collected By: ACOSTA Time Collected: 0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.95
%
01/06/2020
SM 2540 G
ALT
% Volatile Solids
46.94
%
01/06/2019
SM 2540 G
ALT
Fecal Coliforms
4.56
MPN/gram
12/31/2019
SM 9221 C E
ALT
Certified By:
LIZREN D. ACOSTA

ATAD Benchscale Worksheet
C1= Crom Tank
concentration v/
V1= Unknown volume of
Crom Tank biosolids V1
C2 = Needed
concentration (2%) 2
V2 = Known final volume 24
Date
Do
Temp.-twe'c mg/L Initials
F
Set Up Date
10/25/201D
r ,
M
10/28/2019
T
10/29/2019
W
10/30/2019
V
TH
10/31/2019
;1 .
F
11/1/2019
I (j.(p
M
11/4/2019
T
11/5/2019
,
W
11/6/2019
TH
11/7/2019
1 Li - g
F :
11/8/2019
A L-i
M
11/11/2019
T
11/12/2019
W
11/13/2019
$ , LA-
TH
11/14/2019
F
11/15/2019
(� • o (f+r
M
11/18/2019
T
11/19/2019
la
W
11/20/2019
ta-,
TH
11/21/2019
7.0
F
11/22/2019'
M
11/2 2019
T
11/ /2019
) p
W
11/21/2019
1 S•�—
TH
11/26/2019
�j Q
F
11/21/2019
(9-.(7
C1V1= C2V2
)(V1) _ (2)(24)
)(V1) _ (2)(24)
V1 = (2)(24)
( )
V1 = L Crom Tank biosolids
24L - � L = �'� L Effluent
Initial DO should be at least 2 mg/L
Temperature should be maintained at 20°C
Daily Maintenance:
1. Measure and record temperature of the tank.
2. Turn off the mixer and aeration apparatus.
3. Scrape the sludge off the sides of the tank. Use
the paddle to scrape the bottom of the tank.
4. Add distilled water to the fill mark if necessary.
5. Restart mixer and aeration apparatus.
Sampling:
The procedure for sampling follows:
1. After doing "Daily Maintenance" and after a mixing
period of 30 minutes, use the ladle to collect a
representative sample and a duplicate sample.
Use care not to come in contact with the mixing
shaft.
day to collect sample
a

CAMP LEJEUNE BENCH SCALE ATAD VOLATILE SOLIDS REDUCTION ANALYSIS
START-UP
DATE
10/25/2019
A
B
C
D
E
F
G
H
I
J
SAMPLE
DATE
INHOUSE
ATAD
DIGESTION
WTOFDISH
(g)
WTOF
DISH+WET
SOLIDS (g)
SAMPLE
WEIGHT (g)
[B-A)
WTOF
DISH+DRY
SOLIDS (9)
TOTAL
SOLIDS
WEIGHT
(g)
[D-A)
%TOTAL
SOLIDS
[(EJC)X1001
WTOF
DISH+ASH
(9)
ASH
WEIGHT
(g)
1 (G-A]
VOLATILE
SOLIDS
WEIGHT
(g)
(E-H]
%VOLATILE
SOLIDS
((VE)X100]
WEEKLY
AVERAGE
%VOLATILE
SOLIDS
REDUCTION
TEMP
0'C
10/28/2019
I.H. ATAD
86.0412
111.73
25.69 1
86.4377
0.3965
1.54
86.2274
0.1862
0.2103
53.04
52.98
20.5
DUP 72.3278 1 97.41 1 25.08 1 72.7152 1 0.3874 1.54 1 72.5102 1 0.1824 1 0.205 1 52.92
10/31/2019
I.H. ATAD
1 75.5428
1 100.86
25.32
75.8768
0.3340
1.32
75.7034
0.1606
0.1734
51A2
51.87
2.09
21.5
DUP 86.0626 111.27 25.21 86.3968 0.3342 1.33 86.2236 0.161 0.1732 51.83
11/B/2019
I.H. ATAD
74.6336
116.83
42.20
75.0693
0.4357
1.03
74.8511
0.2175
0.2182
50.08
50.16
3.29
16.8
DUP 73.2989 98.93 25.63 73.5628 0.2639 1.03 73.4302 0.1313 0.1326 50.25
11115/2019
I.H. ATAD
1 88.6521
1 113.67
25.02
88.9232
0.2711
1.08
88.785
0.1329
0.1382
50.98
50,99
-1.64
13.3
DUP
1 75.5417
1 100.54
25.00
75.8137
0.2720
1.09
75.675
0.1333
0.1387
50.99
11/22/2019
I.H. ATAD
1 73.6108
1 98.63
1 25.02
1 73.8914
0.2806
1.12
73.7519
0.1411
0.1395
49.71
49.85
2.23
12.9
DUP 88.6545 113.65 25.00 88.9372 0.2827 1.13 88.7959 0.1414 0.1413 49.98
11/29/2019
I.H. ATAD
86,0629
111.06
25.00
86,3339
0.2710
1.08
86.2058
0.1429
0.1281
47.27
47.55
4.60
12
DUP 72.3292 97.32 24.99 72.6024 0.2732 1.09 72.4717 0.1425 0.1307 47.04
VOLATILE SOLIDS REDUCTION = INITIAL VS - FINAL VS X 100
INITIAL VS (VSR <15%)

L�p
LEJEUNE BENCH SCALE ATAD VOLATILE SOLIDS REDUCTION ANALY50 0 '!
4th Quarter 2019
A
B
c
D
E
F
G
H
1
J
SAMPLE
IN-HOUSE
WT OF DISH
WT OF
WT OF
TOTAL
%
WT OF
ASH
VOLATILE
%
WEEKLY
%
TEf p
DATE
ATAD
DISH+WET
SAMPLE
DISH+DRYS
SOLIDS
TOTAL
DISH+ASH.
WEIGHT
SOLIDS
VOLATILE
AVERAGE
VOLATILE
DeG C
DIGESTION
SOLIDS
WEIGHT
OLIDS
WEIGHT
SOLIDS
WEIGHT
SOLIDS
SOLIDS
(g)
(g)
(g)
(g)
(g)
(g)
[B-A]
(g)
[D-A]
[E/C]X100
(g)
[G-A]
[E-H]
[I/E]X100
10/28/2019
LH. ATAD
86.0412
111.73
25.69
0.3965
0.3965
1.54%
86.2274
0.1862
0.2103
53.04%
52.98
0.00%
20.5
DUP
72.3278
97.41
25.08
0.3874
0.3874
1.54%
75.5102
3.1824
-2.7950
-721.48%
10/31/2019
1.H. ATAD
75.5428
100.86
25.32
75.8768
0.3340
1.32%
75.7034
0.1606
0.1734
51.92%
51.87
2.90%
21.5
DUP
86.0626
111.27
25.21
86.3968
0.3342
1.33%
86.2236
0.1610
0.1732
51.83%
11/8/2019
1.H. ATAD
74.6336
116.83
42.20
75.0693
0.4357
1.03%
74.8511
0.2175
0.2182
50.08%
50.16
3.29%
16.8
DUP
73.2989
98.93
25.63
73.5628
0.2639
1.03%
73.4302
0.1313
0.1326
50.25%
11/15/2019
1.1-1. ATAD
88.6521
113.67
25.02
88.9232
0.2711
1.08%
88.7850
0.1329
0.1382
50.98%
50.99
-1.64%
13.3
DUP
75.5417
100.54
25.00
75.8137
0.2720
1.09%
75.6750
0.1333
0.1387
50.99%
11/22/2019
1.H. ATAD
73.6108
98.63
25.02
73.8914
0.2806
1.12%
73.7519
0.1411
0.1395
49.71%
49.85
2.23%
12.9
DUP
88.6545
113.65
25.00
88.9372
0.2827
1.13%
88.7959
0.1414
0.1413
49.98%
11/29/2019
1.H. ATAD
86.0629
111.06
25.00
86.3339
0.2710
1.08%
86.2058
0.1429
0.1281
47.27%
47.55
4.60%
12.0
DUP
72.3292
97.32
24.99
72.6024
0.2732
1.09%
72.4717
0.1425
0.1307
47.84%
Wednesday, February 5, 2020 Page 1 of 1