WQ0005763_Residual Annual Report 2019_20200319

TUCKASEIGEE WATER & SEWER AUTHORITY
SERVING JACKSON COUNTY
1246 West Main Street
Sylva, NC 28779
Phone: [phone] • Fax: [phone]
Feb 27 h, 2020
NCDENR
Division of Water Resources
Water Quality Permit Section
Non -Discharge Permitting Unit
1636 Mail Service Center
Raleigh NC 27699-1636
Attn: Non -Discharge Compliance Unit,
Enclosed are three copies of the Annual Residuals Report for the Tuckaseigee Water and Sewer
Authority Residuals Stabilization facility (permit #WQ0005763) for the period of January 1,
2019 - December 31, 2019
Should you have questions or comments or if I can provide you any additional information,
please don't hesitate to contact me.
Sincerely,
Stan Bryson
Wastewater Plant Operations Superintendent
Tuckaseigee Water & Sewer Authority
xc: Mr Daniel Manring
Executive Director
Tuckaseigee Water and Sewer Authority
This institution is an equal opportunity provider and employer.

2019
Annual Residuals Stabilization Report
for
The Tuckaseigee Water and Sewer Authority
Distribution of Class A Residuals Permit # WQ0005763
for the period of January 1, 2019-December 31, 2019
as required by
40 CFR, Part 503
Standards for the use or disposal of
Sewage sludge

ANNUAL SEWAGE SLUDGE REPORT
OF
TUCKASEIGEE WATER AND SEWER AUTHORITY
PLANT # 1-NPDES # NCO039578 (WQ0005763)
for the period of January 1, 2019-December 31, 2019
as required by
40 CFI;, PART 503
STANDARDS FOR THE USE OR DISPOSAL OF SEWAGE
SLUDGE

TABLE OF CONTENTS
(1) PERTINENT INFORMATION
(2) Land Application Certification Form (DENR Form ACF)
Residual Sampling Summary Form (DENR Form RSSF)
Class A Distribution and Marketing Summary (DENR Form DMSDF)
Pathogen and Vector Attraction Reduction form (DENR Form PVRF 503)
(3) 2019 Sludge Production Data
(a) 2019 Monthly Residual Sources and Volumes Summary
(b) 2019 Monthly Distribution and Marketing Summary
(c) TCLP Analysis
(d) Residuals Analysis
(e) Daily Dryer Record
(f) Annual Belt Press Record
0

Pertinent
Information
•

TWSA Plant #1
The Tuckaseigee Water and Sewer Authority Wastewater Treatment Plant #1 is rated as a 3.5
mgd facility. The facility also treats the sludge from three additional plants owned by the
authority -
Pertinent information includes:
Facility name: Tuckaseigee Water & Sewer Authority Plant # 1
NPDES # NC0039578
WQ 00005763
Correspondence address: 1246 West Main St
Sylva NC 28779
Physical address: 1871 North River Rd
Sylva NC 28779
Facility operator: Stan Bryson
Wastewater Plant Operations Superintendent
Email- [e-mail]
ph. 828-586-9318

Land Application Certification Form
(DENR Form ACF)
Residual Sampling Summary Form
(DENR Form RSSF)
Class A Distribution and Marketing
Summary
(DENR Form DMSDF)
Pathogen and Vector Attraction Reduction
(DENR Form PVRF 503)

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ 0005763 County: Jackson Year: 2019
Facility Name (as shown on permit): Tuckaseigee Water and Sewer Authority
Land Application Operator: Stan Bryson (lic # 13180) Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
N/A
Total number of fields utilized for land application during the year:
N/A
Total amount of dry tons applied during the year for all application sites:
53
Total number of acres utilizes for land application during the year:
N/A
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. R1 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Stan Bryson, WWTP Operations Supt.
Permittee Name and Title (type or print)
C&=� 65�4 �&
Signature of Permittee — -
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0005763
Facility Name: Tuckaseigee Water and Sewer Auth.
Residual Source WQ # or NCO039578
NPDES #:
WWTP Name: TWSA Plant #1
Residual Analvsic Data
Laboratory: 1) Pace Analytical
2) Environmental Testing Services
3)
4)
5)
Parameter
(mg/kg)
Conc.
Limit
m a
Sample or Composite Date
2/5
5/7
8/6
1115
12/16
12/16
Percent Solids (%)
NA
98.3
97
92.1
98.9
96
96
Arsenic
75
1.2
< 0.90
2.4
1.5
Cadmium
85
1
0.95
1.2
1.4
Copper
4,300
368
261
406
398
Chromium
NA
22.4
19.6
22.4
32
Lead
840
14.7
13.1
17.7
16.8
Mercury
57
0.81
0.55
1
1
Molybdenum
75
5.3
4.8
5.8
4.8
Nickel
420
13.8
15
17.8
20.5
Selenium
100
4.7
2.2
5.8
6
Zinc
7,500
944
599
813
1410
Total Phosphorus
NA
10200
12900
14100
8730
TKN
NA
49100
42800
47800
28700
Ammonia -Nitrogen
NA
1580
1390
2050
1180
Nitrate and Nitrite
NA
< 2.0
< 4.0
< 4.3
< 4.0
r or surrace aisposai raciaties the ceumg concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalt' s for sub m' 'ng false information, including the possibility of fines and imprisonment for knowing violations."
01
c54 -7
Signature of Preparer Dfite
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0005763 FACILITY NAME: Tuckaseigee Water and Sewer Auth.
PHONE: [phone] COUNTY: Jackson OPERATOR: Stan Bryson
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
Rl Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes Rl No ❑ —♦ If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources s ( include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
(TWSA Plant #1-NC0039578,
34.16
0
Bobby Collins
48
Hayfield
February
TWSA Plant #2-NC0020214,
38.12
0
Harlan Helmers
5
Hayfield
March
and
42.29
0
April
TWSA Plant #3-NC0063321)
40.83
0
May
* All residuals produced by these
6.56
0
June
three plants were combined. Total
0.22
48
July
residuals in was calculated by press
0
0
August
and dryer runs.
27.68
0
September
Total product out was obtained by
16.62
5
October
estimating weights on trucks.
33.54
0
November
50.14
0
December
40.23
0
Total from FORM DMSDF (sup)
Totals:
Annual (dry tons):
0
330.39 1
53
53
Amendment(s) used: 1 0 Bulking Agent(s) used: 0
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit Rl Yes
(including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No --► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee Date
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Signature of Preparer**
(if different from Permittee)
Date
N :( A 9! : 11 6

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Tuckaseigee Water and Sewer Auth. WQ Permit Number: WQ0005763
WWTP Name: TWSA Plant #1 NPDES Number: NCO039578
Monitoring Period: From 1/1/2019 To 12/31/2019
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 703]
Alternative 4 [3
Alternative 5 v❑
Alternative 6
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost ❑
Heat Drying 0
Heat Treatment ❑
Thermophilic ❑
Beta Ra❑
Y
a a
Gamin R Y
Pasteurization
Class B:
Alternative 1 ❑
Alternative 2 ❑
'>:-<<
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion
..............a.,;v
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
in
Pathogen Density
Number o
Excee-
den s
Frequency
of Analysis
y
SampleAnalytical
Type
Tech -
maue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
< 2
7
586
mpn/g
0
quarterly
grab
SM 9221
Salmonella bacteria
(in lieu of fecal
coliform)
3 WN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
I Alt. 4 (Spec. 02 uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
JAR. 8 (Drying - Unstable)
0
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector- attraction reduction requirements have been met. I 'am aware that there are
significant penalties for false certification including fine and imprisonment."
Stan Bryson, WWTP Operations Supt.
Preparer N e and Title(type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* 4D3t Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 503 (12/2006)

I
(3)
2019 Sludge Production
Data

2019 SLUDGE PRODUCTION DATA
-` TWSA PLANT # 1 (3.5 mgd plant capacity)
NPDES # NC0039578
Sludge dewatered on belt press .................... ..........:.:................................ 3,463,941 gallons
total tons...............................................330.39 tons
total metric tons............................................299.7 dry metric tons
The following residuals were included in the above totals.
TWSA PLANT # 2 (0.5 mgd plant capacity)
NPDES # NC0020214
Sludge Hauled to Plant # 1 digestor..............:.............................................. 330,700 gallons
totaltons.......................................................................... 26.31 tons
total metric tons.......................................................:....:.23.9 dry metric tons
TWSA PLANT #. 3 (0.2 mgd plant capacity)
NPDES # NC0063321
Sludge Hauled to Plant # 1 digestor........................................................ 97500 gallons
totaltons.........................................................................12.08 dry tons
total metric tons..............................................................11.0 dry metric tons
Total Calculated Sludge Production, 2019= 330.4 dry tons, (299.7 metric tons).
This number was calculated from the volume (gals) and the % total solids
_ dewatered on the belt press.
There was a total of 243.4 tons of dried residual landfilled in 2019. At an avg. % solids of 95.9
these residuals equaled 233.4 dry tons.
There was a total of 205.2 tons of wet residual landfilled in 2019. At an avg. % solids of 18.4
these residuals totaled 37.76 dry tons.
A total of 53 tons were. distributed to the public in 2019. At an avg % solids of 95.9 these
residuals totaled 50.8 dry tons
An estimated 25 tons were stored in the silo on Dec 31'% 2019. At an avg % solids of 95.9 thes
residuals totaled 23.98 dry tons
233.4+37.76+50.8+23.98 = 345.9 dry tons= 313.7 dry metric tons accounted for in 2019.
All sludge or residuals landfilled in 2019 were hauled by a private contractor to the:
R&B Landfill This landfill operated by: Waste Management Services
610 Frank, Bennet Rd 1001 Fannin St
Homer GA, 30547 Houston TX 77002

(a)
2019 Monthly Residual Sources
and Volume
Summary

2019
Appendix A
Part A
Residual Sources and Volume
Sludge Volume
Produced
Month Source (dry tons
January
TWSA Plant # 1 (NC0039578)
TWSA Plant # 2 (NC0020214)
TWSA Plant # 3 (NC0063321)
Monthly Total
32.67
1.49
0.00
34.16
February
TWSA Plant # 1 (NC0039578)
TWSA Plant # 2 (NC0020214)
TWSA Plant # 3 (NC0063321)
Monthly Total
36.7
1.42
0.00
38.12
March
TWSA Plant # 1 (NC0039578)
TWSA Plant # 2 (NC0020214)
TWSA Plant # 3 (NC0063321)
Monthly Total
40.03
2.26
0.00
42.29
April
TWSA Plant # 1 (NC0039578)
TWSA Plant # 2 (NC0020214)
TWSA Plant # 3 (NC0063321)
Monthly Total
35.96
1.75
3.12
40.83
May
TWSA Plant # 1 (NC0039578)
TWSA Plant # 2 (NC0020214)
TWSA Plant # 3 (NC0063321)
Monthly Total
4.73
1.83
0.00
6.56
June
TWSA Plant # 1 (NC0039578)
TWSA Plant # 2 (NC0020214)
TWSA Plant # 3 (NC0063321)
Monthly Total
0.22
1.80
3.03
5.05
Est. Total "sludge" produced by all sources for 2019= 330.4 dry tons
Part A
Residual Sources and Volume
Sludge Volume
Produced
Month Source (dry tons
July
TWSA Plant # 1 (NC0039578)
TWSA Plant # 2 (NC0020214)
TWSA Plant # 3 (NC0063321)
Monthly Total
0
2.80
0.00
2.80
August
TWSA Plant # 1 (NC0039578)
TWSA Plant # 2 (NC0020214)
TWSA Plant # 3 (NC0063321)
Monthly Total
26.27
1.41
0.00
27.68
September
TWSA Plant # 1 (NC0039578)
TWSA Plant # 2 (NC0020214)
TWSA Plant # 3 (NC0063321)
Monthly Total
12.36
1.54
2.72
_ 16.62
October
TWSA Plant # 1 (NC0039578)
TWSA Plant # 2 (NC0020214)
TWSA Plant # 3 (NC0063321)
Monthly Total
32.55
0.99
0.00
33.54
November
TWSA Plant # 1 (NC0039578)
TWSA Plant # 2 (NC0020214)
TWSA Plant # 3 (NC0063321)
Monthly Total
47.74
2.40
0.00'
50.14
December
TWSA Plant # 1 (NC0039578)
TWSA Plant # 2 (NC0020214)
TWSA Plant # 3 (NC0063321)
Monthly Total
39.47
0.76
0.00
40.23

(b)
2019 Monthly Distribution
and Marketing
Summary

J
Appendix A
TWSA PLANT # 1
ANNUAL DISTRIBUTION AND
MARKETING SUMMARY
2019
Part B
Recipient Information
Month Name & Date Est. Volume Intended Use Destination
Address I (wet tons)
January 0
February 0
March 0
April 0
May 0
June
Bobby Collins
6112
24
Hayfield
327 Cedar Ridge Rd.
Monthly
327 Cedar Ridge Rd.
6112
24
Franklin NC 28734
Total
Franklin NC 28734
Macon Co
48 Tons
ph: [phone]
July 0
August I I 1 0
September
Harlan Helmers
9/20
3
Hayfield
32 Pine Hill Lane
Monthly
32 Pine Hill Lane
9124
2
Sylva NC 28779
Total
Sylva NC 28779
Jackson Co.
5 Tons
Ph: [phone]
October I , I 1 0
November I I 1 0
December I I 1 0
Annual Total Tons Distributed to the public= 53.0 tons
= 48.1 metric tons

(C)
2019 TCLP
Analysis

r
aceAnalyticar
_. www.pacelabs:com
t August 20, 2019
Mr. Stan Bryson
Tuckaseigee Water & Sewer Co.
1246 West Main Street
Sylva, NC 28779
i
RE: Project: TWSA D. RESIDUAL TCLP 8-6-19
- Pace Project No.: 92440179
' AUG 2 9 2019
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Dear Mr. Bryson:
Enclosed are the analytical results for sample(s) received by the laboratory on August 06, 2019. The
results relate only to the samples included in this report. Results reported herein -conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
(r
1
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, ,LLC.
Page 1 of 18

Ar
aceAt7alyiical
/ www.pacelabs.com
1
Project: TWSA D. RESIDUAL TCLP 8-6-19
Pace Project No.: 92440179
Atlanta Certification IDs
110 Technology Parkway Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
Georgia DW Microbiology Certification M 812
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification M 12
CERTIFICATIONS
North Carolina Certification M 381
South Carolina Certification* 98011001
Virginia Certification M 460204
South Carolina Certification M 99006001
Flodda/NELAP Certification M E87627
Kentucky UST Certification M 84
Vrginia/VELAP Certification M 460221
Asheville Certification IDs.
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification M 40
Florida/NELAP Certification M E87648 South Carolina Certification M 99030001
Massachusetts Certification* M-NC030 MrginiaNELAP Certification M 460222
North Carolina Drinking Water Certification M 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 18

Pace Analytical Services, LLC
aceAn*ical
2225 Riverside Dr.
Asheville, NC 28804
www.pacelabs.com
[phone]
SAMPLE ANALYTE COUNT
Project: - TWSA D. RESIDUAL TCLP 8-6-19
Pace Project No.: 92440179
Analytes
Lab ID Sample ID
Method
Analysts
Reported Laboratory
92440179001 TWSA DRIED RESIDUAL
EPA 8081 B
SEM
9 PASI-C
EPA 8151A
MZP
3 PASI-GA
EPA 601OD.
DS
7 PASI-A
EPA 7470A
JMW1
1 PASI-A
EPA 8270D
PKS
18 PASI-C
EPA 8260E
GAW
14 PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 18

Pace Analytical Services, LLC
a2225 Riverside Dr.
ceAnalytical Asheville, NC 28804
www.pacelabs.com (828)2547176
ANALYTICAL RESULTS
Project: TWSA D. RESIDUAL TCLP 8-6-19
t
Pace Project No.: 92440179
Sample: TWSA DRIED RESIDUAL
Lab ID: 92440179001 Collected: 08/06/19 14:00 Received: 08/06/19 15:14 Matrix: Water
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
I
8081 TCLP Pesticides RVE
Analytical Method: EPA 8081 B Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 08/08/19 19:21 Initial'pH: 7.01; Final pH: 4
gamma-BHC (Lindane)
ND ug/L 0.50 1. 08/12/19 14:54 08/17/19 20:33 58-89-9 ' M1,R1
Chlordane (Technical)
ND ug/L 3.0 1 08112/19 14:54 08/17/19 20:33 57-74-9
Endrin
ND ug/L 0.50 1 08/12/1914:54 08/17/19 20:33 72-20-8 M1,R1
Heptachlor
ND ug/L 0.50 1 08/12/19 14:54 08/17/19 20:33 76-44-8 M1
Heptachlor epoxide
ND ug/L 0.50 1 08/12/19 14:54 08/17/19 20:33 1024-57-3 M1,R1
Methoxychlor
ND ug/L 1000 1 08/12/19 14:54 08/17/19 20:33 7243-5 M1
Toxaphene
ND ug/L 3.0 1 08/12/19 14:54 08/17/19 20:33 8001-35-2
Surrogates
Decachlorobiphenyl (S)
54 % 10-138 ' 1 08/12/1914:54 08/17/19 20:33 2051-24-3
Tetrachloro-m-xylene (S)
82 % 10-110 1 08/12/1914:54 09/17/19 20:33 877-09-8
815.1ACIAcid Herbicides TCLP
Analytical Method: EPA8151A Preparation Method: EPA8151A
Leachate. Method/Date: EPA 1311; 08/08/19 15:00 Initial pH: 6.44; Final pH: 5.08
F
2,4-D
ND mg/L 0.0050 1 08/09/19 07:45 08/09/1919:41 94-75-7
2,4,5-TP (Silvex)
ND mg/L 0.010 1 08/09/19 07:45 08/09/19 19:41 93-72-1
`
Surrogates
2,4-DCAA (S)
104 %. 10-155 1 08/09/19 07:45 08/09/19 19.41 19719-28-9
6010 MET ICP, TCLP
Analytical Method: EPA6010D Preparation Method: EPA3010A
Leachate Method/Date: EPA 1311; 08/15/19 21:14 Initial pH: 6.29; Final pH: 4.5
Arsenic
ND mg/L 0.050 1 08/17/19 16:32 08/18/19 22:23 7440-38-2
Barium
ND mg/L 0.25 1 08/17/19 16:32 08/18/19 22:23 7440-39-3
Cadmium
ND mg1L 0.0050 1 08/17/19 16:32 08/18/19 22:23 7440-43-9
Chromium
ND mg/L 0.050 1 08/17/19 16:32 08/18/19 22:23 7440-47-3
Lead
ND mg/L 0.025 1 08/17/19 16:32 08/18/19 22:23 7439-92-1
Selenium
ND mg/L 0.10 1 08/17/19 16:32 08/18/19 22:23 7782-49-2
Silver .
ND mg/L 0.025 1 08/17/19 16:32 08/18/19 22:23 7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA7470A Preparation Method: EPA7470A
Leachate Method/Date: EPA 1311; 08/15/19 21:14 Initial pH: 6.29; Final pH: 4.5
Mercury
ND mg/L 0.00020 1 08/19/19 08:26 08/19/19 13:23 7439-97-6
8270 MSSV TCLP Sep Funnel
Analytical Method: EPA8270D Preparation Method: EPA3510C
Leachate Method/Date: EPA 1311; 08/08/1919:21 Initial pH: 7.01; Final pH: 4
1,4-Dichlorobenzene
ND ug/L 50.0 1 08/12/19 18:41 08/13/19 15:37 106-46-7
2,4Dinitrotoluene
ND ug/L 50.0 1 08/12/19 18:41 08/13/19 15:37 121-14-2
Hexachloro-1,3-butadiene
ND ug/L 50.0 1 08/12/19 18:41 08/1311915:37 87-68-3
Hexachiorobenzene
ND ug/L 50.0 1 08/1211918:41 08/13/1915:37 118-74-1
Hexachloroethane
ND ug/L 50.0 1 08/12/1918:41 08/13/19 15:37 67-72-1
-
2-Methylphenol(o-Cresol)
ND ug/L 50.0 1 08/12/19 18:41 08/13/19 15:37 95-48-7
`
3&4Methylphenol(m&p Cresol)
163 ug/L 50.0 1 08/12/19 18:41 08/13/19 15:37 15831-10-4
Nitrobenzene
ND ug/L 50.0 1 08112/1918:41 08/1311915:37 98-95-3
i
Pentachlorophenol
ND ug/L 100 -1 08/12/19 18:41 08/1311915:37 87-86-5
Pyridine
ND ug/L 50.0 1 08/12/19 18:41 08/13/19 15:37 110-86-1
2,4,5-Trichlorophenot
ND ug/L 50.0 1- 08/12/19 18:41 08/13/19 15:37 95-95-4
REPORT OF LABORATORY ANALYSIS
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Date: 08/20/2019 02:50 PM
without the written consent of Pace Analytical Services, LLC. Page 4 of 18

(�IacioAnaOcal
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ANALYTICAL RESULTS
Project: TWSA D. RESIDUAL TCLP 8-6-19
Pace Project No.: 92440176
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: TWSA DRIED RESIDUAL Lab ID: 92440179001 Collected: 08/06/19 14:00 Received: 08/06/19 15:14 Matrix: Water
Parameters Results Units 'Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV TCLP Sep Funnel
2,4,6-Tdchlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tdbromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEIN
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
�. Tetrachloroethene .
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-& (S)
4-Bromofluorobenzene (S)
Date: 08/20/2019 02:50 PM
Analytical Method: EPA 8270D Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 08/08/19 19:21 Initial pH: 7.01; Final pH: 4
ND
ug/L
50.0
1 08/12/1918:41
08/1311915:37 88-06-2
14
%
12-102
1 08/12/1918:41
08113/1915:37 4165-60-0
17
%
13-107
1 08112/1918:41
08/13/1915:37 321-60-8
68
%
21-132
1 08/12/1918:41
08/13/1915:37 1718-51-0
13
- %
10-110
1 08/12/1918:41
08/13/1915:37 13127-88-3
12
%
10-110
1 0811 2/l 9 18:41
08/13/1915:37 367=12-4
60
%
27-108
1 08112/1918:41
08/13/1915:37 118-79-6
Analytical Method:
EPA 8260B
Leachate Method/Date: EPA 1311; 08/16/19 13:43
ND
ug/L
100
20
08118/1.917:38 71-43-2
426
ug/L
200
20
08/18/1917:38 78-93-3
ND
ug/L
100
20
08/18/1917:38 56-23-5
ND
ug/L
100
20
08/18/1917:38 108-90-7
ND
ug/L
100
20
08/18/1917:38 67-66-3
ND
ug/L
100
20
08/18/1917:38 106-46-7
ND
ug/L
100
20
08/18/1917:38 107-06-2
ND
ug/L
100
20
08/1811917:38 75-35-4
ND
ug/L
100
20
08/18/1917:38 127-18-4
ND
ug/L
100
20
08/18/1917:38 79-01-6
ND
ug/L
100
20
08/18/1917:38 75-01-4
108
%
70-130
20
08/18/1917:38 17060-07-0
104
%
70-130
20
08/18/1917:38 2037-26-5
101
%
70-130
20
08/18/1917:38 460-00-4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 5 of 18

aceAnalytcal
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Project: TWSA D. RESIDUAL TCLP 8-6-19
Pace Project No.: 92440179
QC Batch: 492969
QC Batch Method: EPA 7470A
Associated Lab Samples: 92440179001
METHOD BLANK: 2656141
Associated Lab Samples: 92440179001
Parameter Units
Mercury mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 7470A
Analysis Description: 7470 Mercury TCLP
Matrix: Water
Blank Reporting
Result Limit Analyzed
ND 0.00020 08/19/1913:19
Qualifiers
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 2657347
Spike . LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury mg/L 0.0025 0.0026 105 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2657348 2657349
MS MSD
92440179001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Mercury rng/L ND 0.0025 0.0025 0.0024 0.0025 96 100 75-125 4
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/20/2019 02:50 PM without the written consent of Pace Analytical Services, LLC.
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aceAnalytical
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QUALITY CONTROL DATA
Project: TWSA D. RESIDUAL TCLP 8-6-19
Pace Project No.: 92440179
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QC Batch: 492968
Analysis Method:
EPA 601 OD
QC Batch Method: -EPA 3010A
Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92440179001
METHOD BLANK: - 2656141
Matrix: Water
Associated Lab Samples: 92440179001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Arsenic
mg/L
ND
0.050
08/18/19 22:04
Barium
mg/L
ND
6.25
08/18/19 22:04
Cadmium
mg/L
ND
0.0050
08/18/19 22:04
Chromium
mg/L
ND
0.050
08/18/19 22:04
Lead
mg/L
ND
0.025
08/18/19 22:04
Selenium
mg/L.
ND
0.10
08/18/19 22:0'4
Silver
mg/L
ND
0.025
08/18/19 22:04
i LABORATORY CONTROL SAMPLE:
26573.44
Spike
LCS
LCS %
Rec
Parameter
Units
Cone.
Result
% Rec Limits Qualifiers
Arsenic
mg/L
2.5
2.5
99
80-120
i - Barium
mg/L
2.5
2.5
99
80-120
Cadmium
mg/L
2.5
2.4
98
80-120
Chromium
mg/L
2.5
2.5
99
80-120
Lead
mg/L
2.5
2.3
94
80-120
Selenium
mg/L
2.5
2.5
101
80-120
Silver
mg/L
1.2
1.3
100
80-120
MATRIX SPIKE R MATRIX SPIKE DUPLICATE: 2657345
2657346
MS
MSD
-
92440006001
Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result % Rec % Rec
Limits
RPD
Arsenic
mg/L
ND
2.5
2.5
2.5
2.5
98 100
75-125
2
Barium
mg/L
0.34
2.5
2.5
2.8
2.8
98 100
75-125
2
Cadmium
mg/L
ND
2.5
2.5
2.4
2.5
97 •100
75-125
2
Chromium
mg/L
ND
2.5
2.5
2.4
2.5
96 99
75-125
3
' Lead
mg/L
ND
2.5
2.5
2.3
2.4
92 94
75-125
2
Selenium
mg/L
ND
2.5
2.5
2.5
2.6
99 103
75-125
4
Silver
mg/L
ND
1.2
1.2
1.2
1.3 100 103
75-125
3
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 08/20/2019 02:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qua[
Page 7 of 18

aceAnalytical
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j
1
QUALITY CONTROL DATA
Project: TWSA D. RESIDUAL TCLP 8-6-19
Pace Project No.: 92440179
QC Batch: 493035
QC Batch Method: EPA 8260E
Associated Lab Samples: 92440179001
Analysis Method: EPA 8260B
Analysis Description: 8260 MSV TCLP
METHOD BLANK: 2655217 '
Matrix: Water
Associated Lab Samples: 92440179001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
1,1-Dichloroethene
ug/L
ND
5.0
08/18/1913:00
1,2-Dichloroethane
ug/L
ND
5.0
08/1811913:00
1,4-Dichlorobenzene
ug/L
ND
5.0
08/18/1913:00
2-Butanone (MEK)
ug/L
ND
10.0
08/18/1913:00
Benzene
ug/L.
ND
5.0
08/1811913:00
Carbon tetrachloride
ug/-L
ND
5.0
08/18/1913:00
'Chlorobenzene
ug/L
39.0
5.0
08/1811913:00
Chloroform
ug/L
ND
5.0
08/18/1913:00
Tetrachloroethene
ug/L
ND
5.0
08/18/1913:00
Trichloroethene
ug/L
ND
5.0
08/18/1913:00
Vinyl chloride
ug/L .
ND
5.0
08/18/19 13:00
1,2-Dichloroethane-d4 (S)
%
105
70-130
08/18/19 13:00
4-Bromofluorobenzene (S)
%
101
70-130
08/18/19 13:00
Toluene-d8 (S)
%
107
70-130
08/18/1913:00
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2657515
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1-Dichloroethene
ug/L
50
59.9
120
70-130
1,2-Dichloroethane
ug/L
50
50.2
100
76-130
1,4-Dichlorobenzene
ug/L
50
46.3
93
70-130
2-Butanone (MEK)
ug/L
100
115
115
64-135
Benzene
ug/L
50
52.0
104
70-130
Carbon tetrachloride
ug/L
50
50.8
102
70-130
Chlorobenzene
ug/L
50
47.5
95
70-130
Chloroform
ug/L
50
50.2
100
70-130
Tetrachloroethene
ug/L
50
52.8
106
69-130
Trichloroethene
ug/L
50
53.2
106
70-130
Vinyl chloride
ug/L
50
58.7
'117
70-131
1,2-Dichloroethane-d4 (S)
%
102
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
103
70-130
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28604
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2657516 2657517
MS MSD
92441516001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
1,1-Dichloroethene ug/L ND 400 400 499 490 125 122 70-154 2
Results presented on this page are in the units indicated by the "UnIts" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/20/2019 02:50 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 18

aceAnalyfical
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I
QUALITY CONTROL DATA
Project: TWSA D. RESIDUAL TCLP 8-6-19
Pace Project No.: 92440179
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2657516
2657517
MS
MSD
92441516001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc:
Result
Result
% Rec
%.Rec
Limits
RPD Qual
1,2-Dichloroethane
ug/L
ND
400
400
436
446
109
111
70-137
2
1,4-Dichlorobenzene
ug/L
ND
400
400
393
390
98
97
70-133
1
2-Butanone (MEK)
ug/L
ND
800
800
930
896
116
112
60-139
4
Benzene
ug/L
ND
400
400
479
468
120
117
70-151
2
Carbon tetrachloride
ug/L
ND
400
400
480
449
120
112
70-143
7
Chlorobenzene
ug/L
ND
400
400
430
433
107
108
70-138
1
Chloroform
ug/L
ND
400
400
476
443
119
11f
70-139
7
Tetrachloroethene
ug/L
ND
400
400
413
431
103
108
59-143
4'
Trichloroethene
ug/L
ND
400
400
494
472
123
118
70-147
4
Vinyl chloride
ug/L
ND
400
400
528
501
132
125
70-156
5
1,2-Dichloroethane-d4 (S)
%
102
98
70-130
4-Bromof borobenzene (S)
%
99
99
70-130
Toluene-d8 (S)
%
100 '
102
70-130
Results presented -on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
'REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/20/2019 02:50 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 18

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: TWSA D. RESIDUAL TCLP 8-6-19
Pace Project No.: 92440179
r
Y
QC Batch: 491739
Analysis Method: EPA 8081 B
QC Batch Method: EPA 3510C
Analysis Description: 8081 TCLP Pesticides RV
Associated Lab Samples: 92440179001
METHOD BLANK: 2649804 .
Matrix: Water
Associated Lab Samples: 92440179001
Blank
Reporting
r Parameter
Units
Result
Limit
Analyzed
Qualifiers
Chlordane (Technical)
ug/L
ND 3.0
08/17/19 21:24
Endrin
ug/L
ND 0.50
08/17/19 21:24
gamma-BHC (Lindane)
ug/L
ND 0.50
08/17/19 21:24
Heptachlor .
ug/L
ND 0.50
08/17/19 21:24
Heptachlor epoxide
ug/L
ND 0.50
08/17/19 21:24
Methoxychlor
ug/L
ND 1000
08/17/19 21.:24
Toxaphene-
ug/L
ND 3.0
08/17/19 21:24
Decachlorobiphenyl (S)
%
110 10-138
08/17/19 21:24
Tetrachloro-m-xylene (S)
%
117 10-110
08/17/19 21:24
S3
LABORATORY CONTROL SAMPLE: 2651845
Spike
LCS
LCS %
Rec
r- Parameter
Units
Conc.
Result
% Rec Limits
Qualifiers
\ Endrin •
ug/L
1.2
1.3
104
20-134
gamma-BHC (Lindane)
ug/L
1.2
1.4
112
20-118 -
Heptachlor
ug/L
1.2
1.2
95
20-142
Heptachlor epoxide
ug/L
1.2
1.1
92
22-133
Methoxychlor
ug/L
3.8
4.7J
125
44-150
Decachlorobiphenyl (S)
%
102
10-138
Tetrachloro-m-xylene (S)
%
102
10-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2651847
2651846
MS
MSD
92440179001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Endrin
ug/L
ND
1.2
1.2
1.8
4.7
141
372
21-133
90 M1,R1
gamma-BHC (Lindane)
ug/L
ND
1.2
1.2
1.7
2.7
138
214
24-119
44 M1,R1
Heptachlor
ug/L
ND
1.2
1.2
2.3
2.3
182
181
16-128
0 M1
Heptachlor epoxide
ug/L
ND
1.2
1.2
1.9
4.0
149
317
50-150
72 M1,R1
Methoxychlor
ug/L
ND
3.8
3.8
6.1
7.2J
160
192
50-150
M1
Decachlorobiphenyl (S)
%
98
241
10-138
SO
Tetrachloro-m-xylene (S)
%
69
162
10-110
SO
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 08/20/2019 02:50 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 10 of 18

Ar
`1-1-AaceAnalytical
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I
\'
QUALITY CONTROL DATA
Project: TWSAD. RESIDUAL TCLP 8-6-19
Pace Project No.: 92440179
QC Batch: 33299
Analysis Method: EPA8151A
QC Batch Method: EPA 8151A
Analysis Description: 8151 GCS TCLP Herbicides
Associated Lab Samples: 92440179001
METHOD BLANK: 149048
Matrix: Water
Associated Lab Samples; 92440179001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
2,4,5-TP (Silvex)
mg/L
ND 0.010
08/09/19 17:09
2,4-D
mg/L
ND 0.0050
08/09/19 17:09
2,4-DCAA (S)
%.
101 10-155
08/09/19 17:09
METHOD BLANK: 149550
Matrix: Water
Associated Lab Samples: 92440179001
Blank Reporting
Parameter
Units
Result Limit
_ Analyzed Qualifiers
2,4,5-TP (Silvex)
mg/L
ND 0.010
08/09/19 17:52
2,4-D
mg/L
ND 0.0050
08/0911917:52
2,4-DCAA (S)
%.
91 10-155
08/09/19 17:52
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 149714
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
2,4,5-TP (Silvex) mg/L 2 1.9 95 39-138
2,4-D mg/L 2 1.7 85 29-145
2,4-DCAA (S) %. 104 10-155
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
149715
149716
MS
MSD
2621570001 Spike
Spike MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc. Result
Result
% Rec
% Rec
Limits RPD Qual
2,4,5-TP (Silvex)
mg/L
ND 2
2 1.6
1.8
79
88
10-156 11
2,4-D
mg/L
ND 2
2 1.4
1.6
69
79
10-156 15
2,4-DCAA (S)
%.
84
94
10-155
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 08/20/2019 02:50 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 11 of 18

Pace Analytical Services, LLC
aceAi7alytical ®
2225 Riverside Dr.
r
/ www.pacelabs.com
l
Asheville, NC 28804
(828)2547176
QUALITY CONTROL DATA
Project: TWSA D. RESIDUAL TCLP 8-6-19
Pace Project No.: 9244017.9
QC Batch: 491821
Analysis Method:
EPA 8270D
QC Batch Method: EPA 3510C
Analysis Description:.
8270D TCLP MSSV
Associated Lab Samples: 92440179001
METHOD BLANK: 2649804
Matrix: Water
Associated Lab Samples: 92440179001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
1,4-Dichlorobenzene
ug/L
ND
50.0
08/13/1911:35
2,4,5-Trichlorophenol
ug/L
ND
50.0
08/13/1911:35
2,4,6-Trichlorophenol
ug/L
ND
50.0
08113/1911:35
f 2,4-Dinitrotoluene
ug/L
ND
50.0
08/13/1911:35
2-Methylphenol(o-Cresol)
ug/L
ND
50.0
08/13/1911:35.
3&4-Methylphenol(m&p Cresol)
ug/L
ND
50.0
08/13/19 11:35
Hexachloro-1;3-butadiene
ug/L
ND
50.0
08/13/1911:35
Hexachlorobenzene
ug/L
ND
50.0
08/13/1911:35
Hexachloroethane
ug/L
ND
50.0
08/13/1911:35
Nitrobenzene
ug/L
ND
50.0
08/13/1911:35
Pentachlorophenol
ug/L
ND
100
08/13/1911:35
Pyridine
ug/L
ND
50.0
08/13/1911:35'
2,4,6-Tribromophenol (S)
%
67
27-108
08/13/19 11:35
2-Fluorobiphenyl (S)
%
6B
13-107
08/13/19 11:35
2-Fluorophenol (S)
%
43
10-110
08/13/19 11:35
Nitrobenzene-d5 (S)
%
66
12-102
08/13/1911:35
Phenol-d6 (S)
%
28
10-110
08/13/1911:35
Terphenyl-04 (S)
%
86
21-132
08/13/1911:35
LABORATORY CONTROL SAMPLE:
2652364
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
500
299
60
10-110
2,4,5-Trichlorophenol
ug/L
500
323
65
39-108-
2,4,6-Trichlorophenol
ug/L
500
345
69
40-104
2,4-Dinitrotoluene
ug/L
500
376
75
42-109
2-Methylphenol(o-Cresol)
ug/L
500
336
67
31-110
3&4-Methylphenol(m&p•Cresol)
ug/L
500
302
60
30-110
Hexachloro-1,3-butadiene
ug/L
500
221
44
10-110
Hexachlorobenzene
ug/L
500
353
71
39-121
Hexachloroethane
ug/L
500
286
57
10-110
Nitrobenzene
ug/L
500
333
67
32-101
Pentachlorophenol
ug/L
1000
704
70
18-108
Pyridine
ug/L
500
207
41
10-110
2,4,6-Tribromophenol (S)
%
.74
27-108
2-Fluorobiphenyl (S)
%
73
13-107
2-Fluorophenol(S)
%
46
10-110
Nitrobenzene-d5 (S)
%
71
12-102
Phenol-d6 (S)
%
29
10-110
Terphenyl-04 (S)
%
87
21-132
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of.the result.
Date: 08/20/2019 02:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 18

Analytical®
www.pacelabs.com
`
QUALITY CONTROL DATA
Project: TWSA D. RESIDUAL TCLP 8-6-19
Pace Project No.: 92440179
-
MATRIX SPIKE SAMPLE:
2652366
_,•
92440276001
Spike
MS
MS
Parameter
Units
Result
Conc.
Result
% Rec
1,4-Dichlorobenzene
ug/L
ND
500
291
58
2,45-Trichlorophenol
ug/L
ND
500
310
62
2,4,6-Trichlorophenol
ug/L
ND
500
325
65
2,4-Dinitrotoluene
ug/L
ND
- 500
368
74
2-Methylphenol(o-Cresol)
ug/L
ND
500
290
58
3&4-Methylphenol(m&p Cresol)
ug/L
ND
500
283
57
Hexachloro-1,3-butadiene
ug/L
ND
500
202
40
Hexachlorobenzene
ug/L
ND
500
362
72
Hexachloroethane
ug/L
ND
500
274
55
Nitrobenzene
ug/L
ND
500
320
64
Pentachlorophenol
ug/L
ND
1000
676
68
Pyridine
ug/L
ND
500
175
35-
2,4,6-Tdbromophenol (S)
%
78
2-Fluorobiphenyl (S)
%
70
2-Fluorophenol (S)
%
47
Nitrobenzene-d5(S)
%
71
Phenol-d6 (S)
%
31
Terphenyl-dl4 (S)
%
90
SAMPLE DUPLICATE: 2652367
92440279001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,4-Dichlorobenzerie
ug/L
ND
ND
2,4,5-Trichlorophenol
ug/L
ND
ND
2,4,6-Trichlorophenol
ug/L
ND
ND
2,4-Dinitrotoluene
ug/L
ND
ND
2-Methylphenol(o-Cresol)
ug/L
ND
ND
3&4-Methylphenol(m&p Cresol)
ug/L
54.5
49.1.1
Hexachloro-1,3-butadiene
ug/L
ND
ND
Hexachlorobenzene
ug/L
ND
ND
Hexachloroethane
ug/L
ND
ND
Nitrobenzene
ug/L
ND
ND
Pentachlorophenol
ug/L
ND
ND
Pyridine
ug/L
ND
ND
2,4,6-Tribromophenol (S)
%
74
76
2-Fluorobiphenyl (S)
%
68
70
2-Fluorophenol (S)
%
41
43
Nitrobenzene-d5 (S)
%
71
75
Phenol-d6 (S)
%
27
28
Terphenyl-d14 (S)
%
82
88
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
% Rec
Limits Qualifiers
30-150
30-150
30-150
30-150
30-150
30-150
30-150
30-150
30-150
30-150
30-150
90-150
27-108
13-107
10-110
12-102
10-110
21-132
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/20/2019 02:50 PM without the written consent of Pace Analytical Services, I.I.C. Page 13 of 18

Pace Analytical Services, LLC
Q q,, ® 2225 Riverside Dr.
F aoMaOca! Asheville. NC 28804
*_ www.pacela6scam
[phone]
f '
QUALIFIERS
Project: TWSA D. RESIDUAL TCLP 8-6-19
ti Pace Project No.: 92440179
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL• -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
(e bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, uhrounded data are displayed and have been used to calculate %• recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
1
NC - Not Calculable.
SG - Silica Gel - Clean -Up
i U - Indicates the compound was analyzed for, but not detected.
/ Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
- A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
{ each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-GA Pace Analytical Services -Atlanta, GA
r�
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
REPORT OF LABORATORY ANALYSIS
This report shall -not be reproduced, except in full,
Date: 08/20/2019 02:50 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18

9-07
Pace Analytical Services, LLC
aceAnalgical ® 2225 Riverside Dr.
www.pacefabs.cour Asheville, NC 28804
` [phone]
CQUALITY CONTROL DATA CROSS REFERENCE TABLE A LE
Project: • TWSA D. RESIDUAL TCLP 8-6-19
Pace Project No.: 92440179
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92440179001
TWSA DRIED RESIDUAL
EPA 3510C
491739
EPA 8081B
491874
92440179001
TWSA DRIED RESIDUAL
EPA 8151A
33299
EPA 8151A
33339
92440179001
TWSA DRIED RESIDUAL
EPA 3010A
492968
EPA 6010D
492984
92440179001
TWSA DRIED RESIDUAL
EPA 7470A
492969
EPA 7470A
493101
92440179001
TWSA DRIED RESIDUAL
EPA 3510C
491821
EPA 8270D
491974
92440179001
7WSA DRIED RESIDUAL
EPA 8260E
493035
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/20/2019 02:50 PM without the written consent of Pace Analytical Services, I.I.C. Page 15 of 18

�' cleAild(ytICc l
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑i �� Eden[] Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicsville❑
M.N.Client.Name:
W® • 92440179
.. Project #:
i
Courier: [-]Fed Ex ❑UPS❑USPS []Client
❑ Commercial ❑Pace ❑Other:
92440179
Custody Seal Present? .❑Yes �36o Seals Intact? []Yes, / No
.
Date/initials Person Examining Contents:
Packing Material: ❑bubble Wrap ❑Bubble Bags []Atone ❑ Other
Biological Tissue Frozen?
Tfiermomete a r1.�; r
_!, -, lr:�`L Type of ice: ' 4Yet ❑Blue'
f ' I v
7R
[]Yes ONO❑N/A
❑Plane
Gun ID: �'
t
Cooler Temp ('C): 411 Correction Factor: Add/Subtract('C) ' i
r
Temp should be above freezing to VC
Cooler Temp Corrected ("C): `
[]Samples out of temp criteria. Samples on ice, cooling process
USDA Regulated:Soil ("N/A, water sample)
haf tegun
Did samples originate -in a quarantine zone within the United States: CA, NY, orSC.(check maps)?:
Ulds:inQles originate
._.nfrom a foreign sodree (internationally,
u.....,::4 O..ehn Rie.17 r-lVot 1 erINO
Comments/Discrepancy:
Chain.of Custody Present?
byes
[]No
❑NIA
A.
Samples'Aftived within Hold Time?
©Yes
ONO
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
Yes
❑No,
[]N/A
3.
Rush Turn Around Time Requested?
[]Yes
(TNo
[]N/A
4.
Sufficient Volume.?
©Yes
[]No
[IN/A.
S.
Correct Containers Used?
-Pace Containers- Used?
❑Yes
❑Yes
[]No
' No
❑N/A
❑N/A
6.
Containers. Intact?
Rlyes
[]No
❑N/A
7.
Dissolved analysis: Samples Field: Filtered?
❑Yes
ON
❑N/A
S.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
)]Yes
'
[]No
[]N/A
9.
Headspace in VOA Vials (>54mm)?
[]Yes
ONO
iN/A
lo.
Ti ip Blank Present?
Trip Blank Custody Seals Present?
'❑Yes
Des
❑No
ONO
N/A
N/A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes E1go
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Date:
Date:
Page 16 of 18

t
A
0
ou
C.
Item# .
BP4U-125'ntLPiastic Unpreserved (N/A). (CH .
BP3U-250 mL Plastic Unpreserved (N/A)
8P2U•500 rrrL Plastic Unpreserved (N/A)
BP1U-1 liter Plastic Unpreserved (N/A)
BP4S-125 ml Plastic 1-12504 (pH < 2) (Cl-)
BP3N-250 pal plastic HNO3 (ptl c 2)
BP4Z-125 mL Plastic ZN Acetate & NaOH�(>9)
BP4C-125. rnL Plastic NaOH (pli > 12).(CI-)
WGFU-Wide-mouthed Glass jar Unpreserved
AGiU-1 liter AmberUhpreseryed"(N/A)' (Cl:-)
Z
z
Z
Z
741—
AGiH-1 liter Amber'HCI (pH < 2)
AG31.1-250 mL Amber Unp[eserved (N/A) (CI-)
AG15-i liter -Amber H2SO4 (pH r,2)
zzzz
AG3S-250 ml Artlher. I.12SO4 (pH < 2)
AG3A(DG3A)-250.mL Amber NH4CI (N/A)(CI-)
D69H-40 mL VOA HCI (N/A) •
VG9T-40 mL VOA Na25203 (N/A)
VG7U-40 mt- VOA Unp (N/A)
'
•
oG9P-40 ml VOA H3PO4 (N/A)
VOAK'(6via1q per kit)-5035 kit (N/A)
V/GK (3 vials perkit)•VPPI/Gas kit (N/A)
5PST-125 mL Sterile Plastic (N/A —lab)
SP2T-250 mLSYerilePlastic (N/A —.lab)
BP3A-250 mL Plastic (NI.12)25U4 (93-9:7)
AGOU-100'mL Amber Unprese

a aceAnal. jcal"
CHAIWOF-CUSTODY I Analytical Request Document
The Chain-of-Cuslody is a'LEGAL DOCUMENT. All relevant fields must be completed accurately,
r Pago:
of
Section A Section B Section.0
�a f ra
4
taquirad Client Information: Rerjbired Project Information: Invoice Information:
',QQ,tpan : i Report To: Attention:
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To.,
Company Name:
REGULATORY AGENCY
V 1
Address:
F NPDESr GROUNDWATER i DRINKING WATER
I— UST I—' RCRA I— OTHER
'Smal, T :
Purchase Order No.:
prow Qupin
Reforenee:
-hone: Fax:
Project Name:
Pace Prolael,
Site Location
Maiia9ar:
STATE:
taquested Due DataiTAT:
Project Number
Paw Profla A.
Requested Analysis Filtered.(Y/N)
Section D -Matrix Codes
RaqutmdCnant Inftmmnrian M+aTliltt_LCORG
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°3-..
COLLECTED
Prosorv,afi
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Sample date- 802019
Sample IDs MUST UNIQUE Tissue TS
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Analysis Requested:
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DATE
TIME
DATE
TIME .
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aluminum (Aq Molybdenum (Mo) Total Nitrogen (N) .
Arsenic(Ar) % Total Solid s _ Total Phosphorous"(Pj
Cadmium (Cd) Nickel (Ni) Ammonia Nitrogen {NH3-N
Calcium (Ca) Potassium (K) Total Kjeldahl Nitrogen (TK
Chromium (Cr) Selenium (Se) 0 Corrosivity.
Copper (Cu) Sodium (Na) r Ignitability
1
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Lead (Pb) Zinc (Zn) Reactivity
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Magnesium (Mg) ph TCLP (Full:Scan)
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Mercury (Hg) a Fecal Coljform mpn/g -
g
Plant Available Nitrogen (PAN) Surface applied
s
11
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ADOmONAL COMMENTS
RELINQUISHED BY I AFFILIATION,' -
DATE
TIME
ACCEPTED 13Y I AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
SAMPLERNAME'ANIUSIGNATURE
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' 1

(d)
2019 Residuals
Analysis

t
aceAnalytical
wmpace/abacom
February 19, 2019
Mr. 'Stan Bryson
Tuckaseigee Water & Sewer Co.
1246 West Main Street
Sylva, NC 28779
RE: Project: Dried Residual 2/5/19
Pace Project No.: 92416464
Pace Analytical Services, LLC
2225 Riverside Dr..
Asheville, NC 28804
' [phone]
FES 2 8 2019
i.
Dear Mr. Bryson:
Enclosed are the analytical results for sample(s) received by the laboratory on February 05, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
64-- r--
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 24

�;=Analytkal
mnvpacelabs.com
Project: Dried Residual 2/5/19
Pace Project No.: 9241646.4
Pennsylvania Certification IDs
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601
ANAB DOD-ELAP Rad Accreditation M L2417
Alabama Certification M 41590
Arizona Certification M AZ0734
Arkansas Certification
California Certification M 04222CA
Colorado Certification M PA01547
Connecticut Certification M PH-0694
Delaware Certification
EPA Region 4 DW Red
Flodda/TNI Certification M E87683
Georgia Certification M C040
Guam Certification
Hawaii Certification
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification M 391
Kansas/TNI Certification M E-10358
Kentucky Certification M KY90133
KY WW Permit KY0098221
KY WW Permit KY0000221
Louisiana DHH/TNI Certification M LA180012
Louisiana DEQ/rNI Certification M 4086
Maine Certification M 2017020
Maryland Certification M 308
Massachusetts Certification M M-PA1457
Michigan/PADEP Certification M 9991
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification M E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification M 37712
CERTIFICATIONS
Missouri Certification M 235
Montana Certification M Cert0082
Nebraska Certification M NE-OS-29-14
Nevada Certification M PA014572018-1
New Hampshire/rNI Certification M 297617
New Jersey/TNI Certification M PA051
New Mexico Certification M PA01457 -
New YorklrNl Certification M 10888
North Carolina Certification M 42706
North Dakota Certification M R-190
Ohio EPA Red Approval: #41249
Oregon/TNI Certification M PA200002-010
Pennsylvania/TNI Certification M 65-00282
Puerto Rico Certification M PA01457
Rhode Island Certification M 65-00282
South Dakota Certification
Tennessee Certification M 02867
Texas/TNI Certification M T104704188-17-3
Utah/TNI Certification M PA014572017-9
USDA Soil Permit #: P330-17-00091
Vermont Dept. of Health: ID# VT-0282
Virgin Island/PADEP Certification
VirginiaNELAP Certification M 9526
Washington Certification #: C868
West Virginia DEP Certification M 143
West Virginia DHHR Certification #: 9964C
Wisconsin Approve List for Red
Wyoming Certification M 8TMS-L
South Carolina Certification M 99006001
Florida/NELAP Certification M E87627
Kentucky UST Certification M 84
Virginia/VELAP Certification M 460221
North Carolina Wastewater Certification M 40
South Carolina Certification M 99030001
VirginiaNELAP Certification M 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.L.C.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 24

ANALYTICAL RESULTS
Project: Dried Residual 2/5119
Pace Project No.: 92416464
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: TWSA DRIED RESIDUAL
Lab ID: 92416464001 Collected: 02/05/19 14:00
Received: 02/05/19 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation
Method: EPA 3050B
Aluminum
33700 mg/kg
55.3
10
02/11/19 09:37
02/13/1912:19
7429-90-5
Arsenic
1.2 mg/kg
0.55
1
02/11/19 09:37
02/11/19 23:26
7440-38-2
K Cadmium
1.0 mg/kg
0.055
1
02/11/19 09:37
02/11/19 23:26
7440-43-9
Calcium
10100 mg/kg
55.3
10
02/11/19 09:37
02/13/1912:19
7440-70-2
Chromium
22.4 mg/kg
0.28
1
02/11/19 09:37
02/11/19 23:26
7440-47-3
Copper
368 mg/kg
0.28
1
02/11/19 09:37
02/11/19 23:26
7440-50-8
Lead
14.7 mg/kg
0.28
1
02/11/19 09:37
02/11/19 23:26
7439-92-1
Magnesium
4090 mg/kg
5.5
1
02/11/19 09:37
02/11/19 23:26
7439-95-4
Molybdenum
5.3 mglkg
0.28
1
02/11/19 09:37
02/11/19 23:26
7439-98-7
Nickel
13.8 mg/kg
0.28
1
02/11/19 09:37
02/11/19 23:26
7440-02-0
Potassium
4080 mg/kg
277
1
02/11/19 09:37
02/11/19 23:26
7440-09-7
Selenium
4.7 mg/kg
0.55
1
02/11/19 09:37
02/11/19 23:26
7782-49-2
Sodium
541 mg/kg
277
1
02/11/19 09:37
02/11/19 23:26
7440-23-5
Zinc
9" mg/kg
5.5
10
02/11/19 09:37
02/13/19 12:19
7440-66-6
7471 Mercury
Analytical Method: EPA 7471B Preparation
Method: EPA 7471B
Mercury
0.81 mg/kg
0.038
10
02/06/1918:52
02107/1914:25
7439-97-6
2540G Total Percent Solids
Analytical Method: SM 2540G-2011
Total Solids
98.3 %
0.10
1
02/06/19 13:26
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
1.7 %
0.10
1
02/06/19 13:09
9045 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
6.0 Std. Units
0.10
1
02/18/19 11:26
H3
Plant Available Nitrogen
Analytical Method: SM 271 OB-2011
Plant Available Nitrogen
15000 mg/kg
0.12
1
02/12/19 13:40
N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
49100 mg/kg
40.0
1
02/12/1913:20
7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0
1993 Mod.
Nitrogen, Ammonia
1580 mg/kg
50.9
5
02/08/1912:27
02/09/1916:35
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
49100 mg/kg
3510
100
02/09/19 01:19
02/12/19 02:31
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.01993 Preparation Method: EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
ND mg/kg
2.0
1
02/09/19 04:09
02/09/19 05:23
Nitrogen, Nitrate
ND mg/kg
2.0
1
02/09/19 04:09
02/09/19 05:23
14797-55-8
Nitrogen,'Nitrite
ND mg/kg
1.0
1
02/09/19 04:09
02/09/19 05:23
14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/19/2019 04:39 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 24

aceAnalytical
www.pacdabs.com
ANALYTICAL RESULTS
Project: Dried Residual 2/5/19
Pace Project No.: 92416464
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: TWSA DRIED RESIDUAL Lab ID: 92416464001 Collected: 02/05/19 14:00 Received: 02/05/19 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. -
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.01993
Phosphorus 10200 mg/kg 170 200 02/07/1919:20 02107/1922:19 7723-14-0 M6,R1
Sample: TWSA DRIED RESIDUAL Lab ID: 92416464002 Collected: 02/05/19 14:00 Received: 02/05/19 15:00 Matrix: Solid
' Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No.
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010A
Flashpoint
>200.0 deg F 70.0 1 02/08/19 17:22
9045 pH Soil
Analytical Method: EPA9045D
pH at 25 Degrees C
6.1 Sid. Units 0.10 1 02/18/19 11:28
733C S Reactive Cyanide
Analytical Method: EPA9014 Preparation Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg 1.0 1 02/07/19 21:35 02/08/19 01:05
' 734S Reactive Sulfide
Analytical Method: SM 4500S2F-00 Preparation Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/kg 10 1 02/07/19 21:35 02/07/19 21:47
Date: 02/19/2019 04:39 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qual
H3
Page 5 of 24

www.pecelabs.com
QUALIFIERS
Project: Dried Residual 2/5/19
Pace Project No.: 92416464
DEFINITIONS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-PA Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
E Analyte concentration exceeded the calibration range. The reported result is estimated.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
Date: 02/19/2019 04:39 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 24

kkeAnalXical*
CHAIN -OF -CUSTODY / Analytical Request Document N
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. o
N
N
Page:
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Section A
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STATE.
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Total Nitrogen (N)
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Ammonia Nitrogen (N43-N)
3
Calcium (Ca) Potassium (K)
Total Kjeldahl'Nitrogen (TKI
4
Chromium (Cr) Selenium (Se) Corrosivity
Copper (Cu) Sodium (Na) Ignitability
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ADDITIONAL COMMENTS
RELINQUISHED. BY/
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DATE
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SAMPLER NAME•AND.SIGNATURE
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LAORATORi CS I NCO
For: Pace Analytical -Asheville
2225 Riverside Drive
Asheville, NC 28804
Attn: Chris Derouen
Report of Analysis
2/1212019
OlItIIIIII ANIiCYT''�M
s re NC N34 Z
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Site: Pace Analylical-Asheville Collection Date: 2/5/2019 14:00
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Parameter Method^ MResult ~Units _ Rep Limit Analyst Analysis Date/Time- {
Fecal Coliforrtt SR4 �3221 C E-2006 <2 mpnlg TS 2 E3J 216f2019 1000
rMA = not onalyze d
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P.O. BOX 473 106 Short Street Kernersville, North Carolina 27264 Tel: [phone] Fax: [phone] www.randalabs.com Page 1
Page 23 of 24

Chain of Custody
��acie
Workorder. 92416464 Workarder Name: Dried Residual 2/5/19
iiesuns
mequesieu
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Chris Derouen
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Pace Analytical Asheville P.O.
2225 Riverside Dr.
Asheville, NO 28804
Phone [phone]
Email: christapher.derouen@pacelabs-com
State of Sample Origin: -'Prbsbiv edContalner9V
0
LAB USE ONLY
x
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TWSA ORM13 RESIDUAL
PJ612019 14.00
92416464001
Solid
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Tuesday, February 05, 2019 3.18:58 PM FMT-ALL-C-002rov-00 24March2OO9 Page 1 of

t
r
�., SAR Calculations- 2/5/2019
SAR = Sodium (Na) Milli Equivalent
0.5 X (Calcium (Ca) Milli Equivalent+ Magnesium(Mg) Milli Equivalent)o.5
Na= 541 mg/kg/ Na Milli Equivalent(ME)= 541/23 equivalent wgt=23.5 ME
Ca=10100 mg/kg/Ca Milli Equivalent(ME)=10100/20 equivalent wgt= 505 ME
Mg= 4090 mg/kg/Mg Milli Equivalent(ME)= 4090/12 equivalent wgt= 340.8 ME
SAR= 23.5 Na Milli Equivalent
- 0.5 X (505 Ca Milli Equivalent + 340.8 Mg Milli Equivalent)0.5
23.5 Na Milli Eauivalent
(0.5 X 845.8) 0.5
= 23.5 Na Milli Equivalent
(422.9)0.5
= 23.5 Na Milli Equivalent
20.6

acoAnalytical
wmpace/abacom
February 19, 2019
Mr. Stan Bryson
Tuckaseigee Water & Sewer Co.
1246 West Main Street
Sylva, NC 28779
RE: Project: Dried Residual Fecal 2/12
Pace Project No.: 92417440
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Dear Mr. Bryson:
Enclosed are the analytical results for sample(s) received by the laboratory on February 12, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
6�— c
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 6

Parameter
Fecal Colifo
iLAWRATORiES INC.
For: Pace Analytical -Asheville
2225 Riverside Drive
Asheville, NC 28804
Attn: Chris .Derouen
Client Sample ID: TWSA Dried Residual Lab Sample 10: 62944-01
Site: Pace,Analy0cal-Asheville Collection Date: 2/12/2019 14:00
~ M Method �M Result Units Rep Limit Analyst Analysis Date/Tirne �) .
SM 9221 C E-2006 <2 mpn/g TS 2 fiJ 2/1312019- 1125
Report of Analysis
2/14/2019
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P.O. Box 473 108 Short Street Kernersville, North Carolina 27284
NA = not oralyted
Tel: [phone] Fax: [phone] " mvmrandalabs.com Page 1
Page 5 of 6

15, 21 - ...
lyfi'.-
CHAIN-OF-CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
ro
0
Page: of D
Section A ' Section BSection C
Required Client Information: a Required Project Information: Invoice Information:.�
Com�py: �epod_T ' Attention:
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Chain of Custody
(�5ace.Lnalyfic!f
wwwPGC"&C=
Workorder. 92417440 Workorder Name: Ned Residual Fecal 2/12 RAntafn RAntiantm Rw! q/qr%iqniQ
N.
Chris Derouen
Pace Analytic I al Asheville P.O. -o- Vr7o-s
2225 Riverside Dr.
Asheville, NC 28804
Phone [phone]
Email: [e-mail]
lot, sg,--.t SI
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LAB USE ONLY
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,juesday, February 12; 2019 3:56:64 PM FMT-Page I of I
R
0)

wmpacelabScem
M V 2 S 2019
May 22, 2019
Mr. Stan Bryson
Tuckaseigee Water & Sewer Co.
1246 West Main Street
Sylva, NC 28779
RE: Project: Dried Residual 517
Pace Project No.: 92428219
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Dear Mr. Bryson:
Enclosed are the analytical results for sample(s) received by the laboratory on May 07, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions corfcerning this report, please feel free to contact me.
Sincerely,
Gam —
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
C
..;,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in hill,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 24

� 1
( ;2
Pace Analytical Services, LLC
ace. maixical ®
2225 Riverside Dr.
(
Asheville, NC 28804
�
lwwx pacea6xcom
(828)2547176
1
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ANALYTICAL RESULTS
Project: Dried Residual W.
i
Pace Project No.: 92428219
Sample: TWSA DRIED RESIDUAL
Lab ID: 92428219001 Collected: 05/07/19
14:30
Received: 05/07/19 15:51 Matrix: Solid
Results reported on a ' dry weight" basis and are adjusted forpercent moisture, sample size and any dilutions. -
Parameters
Results Units Report limit
DF
Prepared Analyzed CAS No. Quai
6010 MET ICP
Analytical Method: EPA 60101) Preparation Method: EPA 3050E
Aluminum
26300 mg/kg 45.2
5
05/08/19 16:40 05/12/19 21:52 7429-90-5
- ,
Arsenic
ND mglkg 0.90
1
05/08/19 16:40 05/09/19 19:57 7440-38-2
Cadmium
0.95 mglkg 0.090
1
05108/1916:40 05/09/1919:57 7440-43-9
Calcium
7650 mglkg 9.0
1
05/08/19 16:40 05/09/1919:57 7440-70-2
Chromium
19.6 mglkg 0.45
1
05/08/19 16:40 05/09/1919:57 7440-47-3
Copper
261 mg/kg 0.45
1
05/08/19 16:40 05/09/1919:57 7440-50-8
Lead
13.1 mg/kg 0.45
1
05/08/19 16:40 05/09/1919:57 7439-92-1
_-.
Magnesium
3530 mglkg 9.0
1
05/08/19 16:40 05/09/1919:57 7439-95-4
Molybdenum
4.8 mglkg 0.45
1
05108/1916:40 05/09/1919:57 7439-98-7
Nickel
15.0 mglkg 0.45
1
05/08/19 16:40 05/09/1919:57 7440-02-0 .
Potassium
4630 mg/kg 452
1
05/08/1916:40 05109/1919:57 7440-09-7
Selenium
2.2 mg/kg 0.90
1
05108/1916:40 05/09/1919:57 7782-49-2
Sodium
516 mg/kg 452
1
05/08/19 16:40 05/09/1919:57 7440-23-5
Zinc
599 mglkg 0.90
1
05/08/19 16:40 05109/1919:57 7440-66-6 .
7471 Mercury
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Mercury
0.65 mglkg 0.036
10
05/08/1916:37 05/09/1911:12 7439-97-6
�-
254OG Total Percent Solids
Analytical Method: SM 254OG-2011
Total Solids
97.0 % 0.10
1
05/08/19 12:47
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
3.1 % 0.10
1
05/08/19 12:37
9046 pH Soil
Analytical Method: EPA 9D45D
pH at 25 Degrees C
6.1 Sid. Units 0.10
1
05/13/19 15:26 H1
Plant Available Nitrogen
Analytical Method: SM 271OB-2011
Plant Available Nitrogen
13100 mg/kg 0.12
1
05/1611915:10 N2
i�
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
42800 mg/kg 40.0
1
05/20/19 09:38 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Nitrogen, Ammonia
1390 mg/kg 50.6
5
05/09/19 10:31 05/09/19 18:50 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.01993
Nitrogen, Kjeldahl, Total
42800 mg/kg 10300
50
05/14/19 18:11 05/15/19 05:03 7727-37-9
l ;
353.2 Nitrogen, NO2IN03
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.01993 -
(�;
Nitrogen, NO2 plus NO3
ND mg/kg 4.0
1
05/08/19 00:51 05/08/19 02:18
Nitrogen, Nitrate
ND mg/kg 4.0
1
05/08/19 00:51 05/08/19 02:18 14797-55-8
Nitrogen, Nitrite
ND mglkg 4.0
1
05/08/19 00:51 05/08/19 02:18 14797-65-0
mil
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2019 10:34 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 24

anoAnalytical
www.pecolabs.com
�F
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804'
[phone]
Project: Dried Residual 5/7
} Pace Project No.: 92428219
Sample: TWSA DRIED RESIDUAL Lab ID: 92428219001 Collected: 05/0711914:30 Received: 05/0711915:51 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, -sample size and any dilutions.
l Parameters Results Units Report Limit DF Prepared " Analyzed CAS No. Qual
L 366.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.01993
Phosphorus 12900 mg/kg 496. 500 05/12/1913:43 05/1211916:12 7723-14-0
t ' Sample: TWSA DRIED RESIDUAL
Lab ID: 92428219002 Collected: 05/07/19 14:30 Received: 05/07/19 15:51 Matrix: Solid
Results reported on a ' dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010A.
Flashpoint
>200 deg F 70.0 1 05/19/19 12:35
9045 pH Soil
Analytical Method: EPA9045D
pH at 25 Degrees C
6.6 Sid. Units 0.10 1 05/13/19 15:30 H1
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg 1.0 1 05/13/19 18:13 05/13/1919:13
734S Reactive Sulfide
Analytical Method: SM 4500S2F-00 Preparation Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/kg 10 1 05/13/19 18:13 05/13/1918:18
r�
i
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/201910:34 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 24

.PaceAnalytical'
wwu-nualahc enm
CHAIN -OF -CUSTODY / Analytical Request Document N
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. o
N
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'SectionA 'Section B Section C Page.
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Required Client Information: Requlrad Project Information: Invoice Information:
Com any: Report To: Attention:
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Copy To:
Company Name:
REGULATORY AGENCY
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r NPDES r IGI20UND WATER r DRINKING WATER
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Purchase Order No.:
Paco Quota
Reference:
Phone:
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Project Name:
Paco Project
Site Location
Manager.
STATE:
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Project Number: '
P1C° Pto1eQ n:
Requested • Analysis Flitered (,YIN)
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'MATRIX
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' .Drinking Water DW
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Sample IOs MUST BE UNIQUE Tissue
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Analysis Requested:
Aluminum (AI) Molybdenum (Mo) Total Nitrogen (N)
`84.el L
1
Arsenic (Ar) ' % Total Solids Total Phosphorous (P)
Cadmium (Cd) Nickel (Ni) Ammonia Nitrogen (NH3-N)
2.
3
Calcium (Ca) Potassium (K) Total Kjeldahl Nitrogen (TKN)
4
Chromium (Cr) Selenium (Se) Corrosivity
5
Copper (Cu) Sodium (Na) Ignilability
s
Lead (Pb) Zinc (Zn) Reactivity
T
Magnesium (Mg) ph
a
Mercury (Hg) Fecal Coliform•mpnlg
Plant Available Nitrogen (PAN) Surface applied
s
10
11
12
ADDMONAL COMMENTS
RELINQUISHED BY (AFFILIATION
DATE
TIME'
ACCEPTED BY, AFFILIATION
DATE
TIME
SAMPLE'CONDITIONS
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SAMPLER NAME AND SIGNATURE
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KESEARCh & ANAIYACAI
Ubm- TORI'ES INCO
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Co
Pace Analytical -Asheville,
2225 Riverside Drive
Asheville, NC M04
Attn: Chris Derouen.
Report.of Analysis
VM1201*0
Clle6t* Sample it): TWSA Dried Residual Lab Sample ID: dOSMI
Site: Pace Analytical -Asheville Collection Date, 517J2019 1430
. Parameter Method. Result Units Rep. Limit Analvdit Anal4sIw.Dat41Tlme
:Fecal Goliform SPA 9221 G E-4006 -c2 mpnlg TS 2 Bi 51.8/2019 1310
P.O:. Box 473 106 Short Str.*eet Kernersville, North Carolina 2728.4
NA =-not onalyzed
Tel: .[phone] . 41 Fax: [phone] www.randalabs.com Page -I
Page 23 of 24

Chain of Custody
clMna"cal
Workorder: 9242821'.9 Workorder Name. Wed Residual.5/7 Results Requested BY: 5/21/2619
RepoitlInVOICd-TO
chiis E)er.ouen
Pace.AnalyWal Asheville P.o.
2225 Riverside fir.
Asheville, KC 28404
Phone [phone]
Email-'christopher.der,ouen0pacal6bs..00m
State of Sample -Origin:
I LU:
0
LAB,USE ONLY
M
1?!E!!
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TW54 DRIED RESIDUAL
SM/201914.30
92428219=
Solid
x
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on ice _YL)nr N
Sam les Intact 'Y or N
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T�hsday,,May 07.2019 5'49:20 PM FMT-AL.L-C-002rov.00 24March2009
Page 1 of 1
0

SAR Calculations- 5/7/2019
SAR = Sodium (Na) Milli Equivalent
0.5 X (Calcium (Ca) Milli Equivalent+ Magnesium(Mg) Milli Equivalent)o•5
Na= 516 mg/kg/ Na Milli Equivalent(ME)= 516/23 equivalent wgt= 22.4ME
Ca= 7650 mg/kg/Ca Milli Equivalent(ME)= 7650/20 equivalent wgt= 382.5 ME
Mg= 3530 mg/kg/Mg Milli Equivalent(ME)= 3530/12 equivalent wgt= 294.2ME
SAR= 22.4 Na Milli Equivalent
0.5 X (382.5 Ca Milli Equivalent + 294.2 Mg Milli Equivalent)o•5
= 22.4 Na Milli Equivalent
(0.5X676.7)0.5
22.4 Na Milli Equivalent
(338.4)0.5
= 24.7 Na Milli Equivalent
18.4
SAR= 1.3

Jr 140*211
lAaceAnalXical"
l www.pacelabs.com
it
AUG 2 9 2019
August 20, 2019
Mr. Stan Bryson
Tuckaseigee Water & Sewer Co.
1246 West Main Street
Sylva, NC 28779
RE: Project: TWSA Dried Residual 8-6-19,
Pace Project No.: 92440161
Pace Analytical Services, LLC
2226 Riverside Dr.
Asheville, NC 28804
[phone]
Dear Mr. Bryson:
Enclosed are the analytical results for sample(s) received by the laboratory on August 06, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
�ti--
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pagel of 24

Pace Analytical Services, LLC
® 2225 Riverside Dr.
aceAnalyiical Asheville, NC 28804
www.pacelabsmm [phone]
I� F
ANALYTICAL RESULTS
Project: TWSA Dried Residual 8-6-19
Pace Project No.: 92440161
-
Sample: TWSA DRIED RESIDUAL
Lab ID: 92440161001 Collected: 08/06/1914:00
Received: 08/06/1915:14 Matrix: Solid
Results reported on a dry weight' basis and are adjusted forpercent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No.
Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050E
Aluminum
36700 mglkg
44.5
5 .
08/15/19 00:10 08/17/19 14:25 7429-90-5
-_
Arsenic
2.4 mg/kg
0.89
1
08/15/19 00:10 08/17/19 02:14 7440-38-2
Cadmium
1.2 mg/kg
0.089
1
08/15/19 00:10 08/17/19 02:14 7440-43-9
Calcium
11600 mg/kg
44.5
5
08/15/19 00:10 08/17/19 14:25 7440-70-2
Chromium
22.4 mg/kg
0.45
1
08/15/19 00:10 08/17/19 02:14 7440-47-3
Copper
406 mglkg
0.45
1
08/15/19 00:10 08/17/19 02:14 7440-50-8
Lead
17.7 mg/kg
0.45
1
'08/15/19 00:10 08/17/19 02:14 7439-92-1
Magnesium
3650 mg/kg
8.9
1
06/15/19 00:10 08/17/19 02:14 7439-95-4
Molybdenum.
5.8 mg/kg
0.45
1
08/15/19 00:10 08/17/19 02:14 7439-98-7
Nickel
17.8 mg/kg
0.45
1
08/15/19 00:10 08/17/19 02:14 7440-02-0
Potassium
3990 mg/kg
445
1
08/15/19 00A 0 08/17/19 02:14 7440-09-7
Selenium
5.8 mg/kg
0.89
1
08/15/19 00:10 08/17/19 02:14 7782-49-2
BC
Sodium
557 mg/kg
445
1
08/15/19 00:10 08/17/19 02:14 7440-23-5
Zinc
813 mg/kg
0.89
1
08/15/19 00:10 08/17/19 02:14 7440-66-6
-
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Mercury
1.0 mg/kg
0.045
10
08/13/1914:48 08/15/1911:13 7439-97-6
254OG Total Percent Solids
Analytical Method: SM 254OG-2011
Total Solids
92.1 %
0.10
1
08/08/1916:12
r
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
7.9 %
0.10
1
08/08/19 15:59
9045 pH Soil
Analytical Method: EPA9045D
pH at 25 Degrees C
5.5 Sid. Units
0.10
1
08/19/19 15:08
D6,H3
Plant Available Nitrogen
Analytical Method: SM 271OB-2011
Plant Available Nitrogen
14800 mg/kg
0.12
1
08/19/19 13:50
N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
47800 mg/kg
40.0
1
08115/1911:56 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.01993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Nitrogen, Ammonia
2050 mg/kg
31.3
3
08/12/19 17:06 08/13/19 11:41 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.01993
-
Nitrogen, Kjeldahl, Total
47800 mg/kg
5170
100
08/14/19 17:29 08/15/19 05:16 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA353.2 Rev 2.01993 Preparation Method: EPA353.2 Rev 2.01993 .
Nitrogen, NO2 plus NO3
ND mg/kg
4.3
1
08/07/19 13:26 08/07/19 15:35
Nitrogen, Nitrate
ND mg/kg
4.3
1
08/07/19 13:26 08/07/19 15:35 14797-55-8
Nitrogen, Nitrite
ND mg/kg
4.3
1
08/07/19 13:26 08/07/1915:35 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/20/2019 05:09 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 24

aceAnalytica!
www.pacelabs.com
i
i 1
ANALYTICAL RESULTS
Project: - TWSA Dried Residual 8-6-19
Pace Project No.: 92440161
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: TWSA DRIED -RESIDUAL Lab ID: 92440161001 Collected: 08/06/1914:00 Received: 08/06/19 15:14 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
365.1 Phosphorus; Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method:EPA 365.1 Rev 2.0 1993-
Phosphorus 14100 mglkg 319 300 08/07/1914:40 08/07/19 21:28 7723-14-0 •
Sample: TWSA DRIED RESIDUAL
Lab ID: 92440161002 Collected: 08/06/19 14:00 Received: 08/06/19 15:14 Matrix: Solid
' N Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any di'lutions..
` Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
7.9 % 0.10 1 08/08/19 16:12
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010A
Flashpoint
>200 deg F 70.0 1 08/12/1916:31
9045 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
5.9 Sid. Units 0.10 1 08/19/19 15:10 H3
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg 1.1 . 1 08/12/1917:28 08/12/19 18:04
734S Reactive Sulfide
Analytical Method: SM 4500S2F-2011 Preparation Method: SW 846 7.3.4.2
Sulfide, Reactive
ND mg/kg 10.9 1 08/12/19 17:28 08/12/19 17:37
Date: 08/20/2019 05:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.I.C.
Page 5 of 24

V,
KESEARCh&ANA[Y.ACA[,
LAORATORIES INC,,
For: Face Analyticat-Ashevilld
2225 Riverside Drive'
Asheville, NC 288K
A#n: 0MIS berouen
Report of Analysis
8/-14/2019
011entSaffole ID: TW.SA.Dri.ed Residual' Lab Sample ID: 7016-01
Site:: Pad6 Ahalyftal-Asheiiille Collection bate:.. 8/W019 14:00
Parameter Method Units Rea Limit Analys.AnalVWs-Dat#ITlme
Fecal Coliform 'SM'922TC E-4006 <2 mWa TS2 8i 817/2019 12115.
AA =:nollanqlyzed
P.O. Box.473 106 Shott.Street Ketnersville. North Carolina 27284 Tel: [phone] Fax: 336=996-0326 www.randalabs.eorn Pace 1

SAR Calculations- 8/6/2019
SAR = Sodium (Na) Milli Equivalent
0.5 X (Calcium (Ca) Milli Equivalent+ Magnesium(Mg) Milli Equivalent)o.s
Na= 516 mg/kg/ Na Milli Equivalent(ME)= 516/23 equivalent wgt=22.4 ME
Ca= 7650 mg/kg/Ca Milli Equivalent(ME)= 7650/20 equivalent wgt= 383 ME
Mg= 3530 mg/kg/Mg Milli Equivalent(ME)= 3530/12 equivalent wgt= 294 ME
SAR= 22.4 Na Milli Equivalent
0.5 X (383 Ca Milli Equivalent + 294 Mg Milli Equivalent)0.1
22.4 Na Milli Equivalent
(0.5X677)0.5
= 22.4 Na Milli Equivalent
(339)0.s
= 22.4 Na Milli Equivalent
18.4
SAR= 1.2

t ,
aceAnaljttical
- www.pace/abzcoar
September 09, 2019
Mr. Stan Bryson
Tuckaseigee Water & Sewer Co.
1246 West Main Street .
Sylva, NC 28779
RE: Project: Dried Residual 8-28-19
Pace Project No.: 92443373-
SEP 1 6 2019
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Dear Mr. Bryson:
Enclosed are the analytical results for sample(s) received by the laboratory on August 28, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Gam— �---
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures -
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 4

:.,:'LAB'USE.ONLY�AffizWoikoider WOE# : J2443373
CHAIWOF-CUSTODY Analytical- Request Document nli o
N
Chain,of-Custody isplete
,a LEGAL DOCUMENT'-_Com`all relevent fields II 111 i I'll I l Il iI
L , Billing Information: � '92443373
ALL�SHADED.,,
- „� -.__._... ectManager ... ...
Container Preservative T e. Lab P.roj; _
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Company:�
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Report T
Email To:
" Preservative Types: (2) nitric acid,12) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) Anc acetate,
(6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate,.(9) hexane, (A) ascorbic acid, (B)ammonium sulfate,
(C) ammonium hydroxide; (D) TSP, (U) Unpreserved, (0) Other
Copy To:
Site Collection Info/Address:
Analyses
Lab Prbflle/Line': .
Customer Project Name/Ntimbl]r.
II
State: County/City: Time Zone Collected:
/ [ ]PT[ j MT[ ]CT [ )ET
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sample. Receipt .c
Custody Seal Present%intact Y NA
.:Custody Signatures Present -it NA
' collector-, Signature present N NA
Sutitles•intact N MA
eorrecti Eottiles ti NA
StifFi'dient volume N N!1
Samples Received.on'. ice N, NA_
VOR ;-: Neadspacc; Acceptable -` ' : e Y N >tili
' 'USoib.ategubted. soi�13 - ` Y 'N t
Samples; in bolding Time J� N NA
`.Re'aidual'Cblorine rroueriti Y .N JtC'
Cl Strips;'
Sample ;plt .Acceptable ., Y :N N!Y
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Sulfide Present. Y N NJ(
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'LAD.,OSE: ONLY:
Lab Sample. #? / Comments:
Phone:
Email
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Site/Facility ID If:
Compliance•'Monitoring?"
[ ]Yes [ ) No
Collected By_ nnt):
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Purchase Ordeal:
P u chas:
DW PWS ID rf:
DW Location'Code:
Co -he By si
Turnaround Date Required:.
Imme Mate y P- a on Ice:
[ )Yes [ ]NO
Sample DlspOsa :
( ] Dispose asappropriate [ ) Ret
l I Archive:
( ],Hold:
im
Rush;
[, ]Same Day [ ,] Next Day.
[ ] 2 Day [ ]3 Day 1 .] 4 Day [ ] S Day
(Expedite charges Apply)
Field Filtered (if applicable): -
[ ]yes . [. j No
Analysis:.'
" Matrix:Codes (Insert in Matri:
Product (P); Soil/Solid (SL), Oil
bbibelow)r Drinking Water (DW), Ground Water (GW), Wastewater (W W);
(OL); Wipe (WP), Air (AR),Tissue (TS);, Bioassay (B), Vapor'(V),,OtherJOT)
Customer Sample ID
Matrix `
Comp/
Grab
Collected (or
Composite -Start)
Composite End
Res
Cl
8 of
Ctns
Date
Time
D to
Time
4
Customer Remarks /Special Co
ditions /Possible Hazards:
Type:of,lce Used:;_ , ._ .: ` .Blue. Dry None
$HORT,HOLDS PRESENT,(<72hours):-.,rY'
N N/A
Lab Sample.Tempeature Info:
Temp'elahk Received Y' NA
celptr. C
oer.; .,em actor:.<�.'oC ':,
Ie� 1 Therm Corr..F
Co Cooler 1 Corrected Tem
`Coo
:Coo p:,��,�
Comments:
Packing MatenaPUsed
Lab, (t
Radchem sample(s).screened (<SOO cpm);: Y
B. Vla•:
inples. received -
�:FEDEX�'-' UPS. _Cif Couriers Race Courier „
Relinquished by on-'pzmy:.(Slg
ature)
If
ature)
Date/Time: ,1
Date/Time:
Date/Timei
Rec iv' d.by/Com y: (Signature)
Received by/Compan :'(Signatu e)
Received by/Company: (Signature)
Date/Time; �) rl
Date/Time:
Date/Time:
MTJL LAR USE ONLY
Table N:
Acctnum:
Template:
Prelogfn:
PM:
PB:°.
Relinquished by/Company: (Sig(rature)
Trip Y. Blank Received: . NA
HCL McOH, 75P :Other
Relinquished by/Company: (Sig
Non Conforman s):'
YES ' j
Page:
of•_

IESEARCh NAIy10CAI Report of .Analysis
�RAToR s 9/512019
F
For: Pace Analytical -Asheville
2225 Riverside Drive
Asheville, NC 28804 °C:j WC434
r
i NC O37701
Attn: Chris Derouen •.,_C,.:�_,,�e►
Client Sample ID: TWSA.DRIED RESIDUAL Lab Sample ID: 71WI-=01
Site: -Pace,Analytical-Asheville Collection Date: W2812019 13:4.0
Parameter Method Result. Units Rea Limit Anal st Analysis Date/Time
Fecal Col-iform SM 9221 C E-2006 z2 mpn]g TS: 2 BJ 81297201:9- 1135
NA = not onolyzed
P.O. Box 473 106 Short Street Keroersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page I
Page 3 of 4

Ghaln of Custody
PAM Charlotte Laboratory
Malytical"
—pa-labxcm
Workorder. 92443313. -Workorder Name: 'DrIed'Hesidual 8-2849 Res;UftsReciu6st6dbw 9/1'2/2019
K.
K VT
Chrit De�rouen
Pace ' Analytical Asheville P.O. �
1.222S.Riverside Dr.
I Asheville, NC 28804
Phone [phone]
Email: chilstophe'[e-mail]
idteivedC6
State. -of -Sample Origin- 77—P—-lhtrs*"z"-*;j-
0
LAB USE,ONLY
1
[TWS'A DPIED :RESIDUAL
9128i201'9, 13:40
92441373001
Solid
2
3,
4.
5
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acemalXical
i www.pacelabs.com
i
November 20, 2019
Mr. Stan Bryson
Tuckaseigee Water & Sewer Co.
1246 West Main Street
Sylva, NC 28779
RE: Project: TWSA Dried Residual 11/5/19
Pace Project No.: 92452297
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Dear Mr. Bryson:
Enclosed are the analytical results for sample(s) received by the laboratory on November 05, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
t- Project Manager
i Enclosures
r-.
' 1 "
REPORT OF LABORATORY ANALYSIS
s This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 22

6,P1a'ceAna1Xka1
www.pacelabs.com
I
�i ANALYTICAL RESULTS
Project: TWSA Dried Residual 11/5/19
Pace Project No.: 92452297
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: TWSA DRIED RESIDUAL
Lab ID: 92452297001
Collected: 11/05/1913.20
Received: 11/0511914:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050E
Aluminum
42000
mg/kg
857
100
11/13/1913:50
11/16/1913:13
7429-90-5
Arsenic
1.5
mg/kg
0.86
1
11/13/1913:50
11/14/1918:13
7440-38-2
Cadmium
1.4
mg/kg
0.086
1
11/13/1913:50
11/14/1918:13
7440-43-9
Calcium
12700
mg/kg
857
100
11/13/1913:50
11116/1913:13
7440-70-2
Chromium
32.0
mg/kg
0.43
1
11/13/1913:50
11/1411918:13
7440-47-3
Copper
398
mg/kg
0.43
1
11/13/1913:50
11/14/1918:13
7440-50-8
Lead
16.8
mg/kg
0.43
1
11/13/1913:50
11/14/1918:13
7439=92-1
Magnesium
3740
mg/kg
8.6
1
11/13/1913:50
11/14/1918:13
7439-95-4
Molybdenum
4.8
mg/kg
0.43
1
11/13/1913:50
11/14/1918:13
7439-98-7
Nickel
20.5
mg/kg
0.43
1
11/13/1913:50
11/14/1918:13
7440-02-0
Potassium
3260
mg/kg
428
1
11/13/1913:50
11/14/1918:13
7440-09-7
Selenium
6.0
mg/kg
0.86
1
11113/1913:50
11/14/1918:13
7782-49-2
Sodium
601
mg/kg
428
1
11/13/1913:50
11/14/1918:13
7440-23-5
Zinc
1410
mg/kg
85.7
100
11/13/1913:50
11/16/1913:13
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Mercury
1.0
mg/kg
0.044
10
11/06/1910:20
11/0611916:38
7439-97-6
,,__,40G Total Percent Solids
Analytical Method: SM 2540G-2011
Total Solids
98.9 % 0.10
1
11/06/1918:06
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
1.1 % 0.10
1
11/06/1917:59
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010A
Flashpoint
>200 deg F 70.0
1
11/07/1915*46
9045 pH Soil
Analytical Method: EPA 9045D
pH at25 Degrees C
6.1 Std. Units 0.10
1
11/11/1917:31
Plant Available Nitrogen
Analytical Method: SM 2710E 2011
f" Plant Available Nitrogen
8850 mg/kg 0.12
1
11/1811911:54
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
28700 mg/kg 40.0
1
11/18/1911:37 7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.01993 Mod.
Nitrogen, Ammonia
1180 mg/kg 44.3
5
11/12/1916:15 11/12/19 23:22 7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.01993
Nitrogen, Kjeldahl, Total
28700 mg/kg 1940
50
11/14/19 04:48 11/15/19 07:07 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.01993 Preparation
Method: EPA 353.2 Rev 2.01993
_,_Nitrogen, NO2 plus NO3
ND mg/kg 4.0
1
11/05/19 22:37 11/06/19 00:19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/20/2019 04:37 PM without the written consent of Pace Analytical Services, LLC.
Qual
H3
N2
Page 4 of 22

aceAnalytical
www.pacolabs.com
I.
ANALYTICAL RESULTS
Project: TWSA Dried Residual 11/5119
Pace Project No.: 92452297
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
oample: 1 YY.SA UKICU KCaIUUAL LaD IU: VZ45ZZ970111 Collected: 11/05/19 13:20 Received: 11/05/1914:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
J
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Rev 2.01993 Preparation Method: EPA 353.2 Rev 2.01993
Nitrogen, Nitrate ND mg/kg 4.0 1 11/05/19 22:37 11/06/19 00:19 14797-55-8
Nitrogen, Nitrite ND mg/kg 4.0 1 11/05/19 22:37 11/06/19 00:19 14797-65-0
365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.01993 Preparation Method: EPA 365.1 Rev 2.01993
Phosphorus 8730 mg/kg 226 250 11/06/1921-44 11107/1919:36 7723-14-0
Sample: TWSA DRIED RESIDUAL Lab ID: 92452297002 Collected: 11/05/1913:20 Received: 11/05/1914:10 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method: SW 846 7.3.3.2
Cyanide, Reactive ND mg/kg 0.99 1 11/07/19 20:49 11/08/1918:32 .
734S Reactive Sulfide Analytical Method: SM 4500S2F-2011 Preparation Method: SW-846 7.3.4.2
IRldfide, Reactive ND mg/kg 9.9 1 11/07/19 20:49 11/07/19 20:51
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/20/2019 04:37 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 22

6AaceAnalXical
www.pacelabs.com
t
,I
r
1:D
Project: TWSA Dried Residual 11/5119
Pace Project No.: 92452297
DEFINITIONS
QUALIFIERS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J -'Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyi ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylon"ttrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-PA Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
r H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/20/2019 04:37 PM without the written consent of Pace Analytical Services, I.I.C.
Page 18 of 22

RESEARCh & ANALYTICAL
LA ORATORIESF INCa
V For: Pace Analytical -Asheville
2225 Riverside Drive
Asheville, NC 28804
Attn: Chris Derouen
Report of Analysis
11 /8/2019
Client Sample ID: TWSA Dried Residual Lab Sample ID: 74399-01
Site: Pace Analytical -Asheville Collection Date: 11/5/2019 13:20
Parameter Method Result units Rea Limit Analyst Analysis DatelTime
Fecal Coliform SM 9221 C E-2006 <2 mpn/g TS 2 JB 11/6/2019 1110
Sample received and analyzed outside of hold time per client request.
iVA = not analyzed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 1
•ai •.a:; c-::_ic vie;
r
Page 21 of 22

SAR Calculations-11/5/2019
SAR = Sodium (Na) Milli Equivalent
_v 0.5 X (Calcium (Ca) Milli Equivalent+ Magnesium(Mg) Milli Equivalent)0.5
Na= 601 mg/kg/ Na Milli Equivalent(ME)= 601/23 equivalent wgt=26.1 ME
Ca=12700 mg/kg/Ca Milli Equivalent(ME)=12700/20 equivalent wgt= 635 ME
Mg= 3740 mg/kg/Mg Milli Equivalent(ME)= 3740/12 equivalent wgt= 311.7 ME
SAR 26.1 Na Milli Equivalent
0.5 X (635 Ca Milli Equivalent + 311.7 Mg Milli Equivalent)o.5
= 26.1 Na Milli Equivalent
(0.5 X 946.7)0.5
- 26.1 Na Milli Equivalent
473.4)0.5
= 26.1 Na Milli Equivalent
21.8
SAR= 1.2

AAwb'A l�/�ical
Jn
/ www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
December 03, 2019
Mr. Stan Bryson
Tuckaseigee Water & Sewer Co.
1246 West Main Street
Sylva, NC 28779
RE: Project: TWSA Dried Residual 11/21/19
Pace Project No.: 92454758
Dear Mr. Bryson:
Enclosed are the analytical results for sample(s) received by the laboratory on November 21, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
�=f _ REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
al;9Y` without the written consent of Pace Analytical Services, LLC.
Page 1 of 6

r•
r
��SEARc A��lyY�c��. Report of Analysis
11/26/2019
�t►�`GXF1
For: Pace Analytical -Asheville • •'''•�••'
2225 Riverside Drive: o
Asheville, NC 28804 °'
� i� NCll34 Z=
P NC tl37701
Attn: Chris Derouen %� s••0���pQ�•r; ;�
5.
Client Sample ID: TWSA Dried Residual Lab Sample ID: 75142-01
-y Site: Pace Analytical -Asheville Collection Date: 11/21/2019 13:32
Parameter Method Result Units Rep Limit Anal st Pnalysis DatelTime
Fecal Coliform SM 9221 C E-2006 <2 mpn/g TS 2 LP 11/22/2019 1330
Sample received and analyzed outside of hold time per client request.
NA = not analyzed
CC,�r 4o I�k e pry' f i v1 a Y r 9cc2 (d-�f-j.S �r weK)
iPA F)Dw 0. Mv4I,14't-t -Vtw. ovi FcW Slm��
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 1
r[.I co2 basic vtd
Page 5 of 6

G PO Box 7565
Q Asheville, NC 28802
4 • Phone: [phone]
Fax: [phone]
y Environmental Testing Solutions, Inc. Certificate of Analysis
Project name: Tuckaseigee Water & Sewer Project number: 191216.501
J Collection date: 16-Dec-19
Date received: 16-Dec-19
Sample identification: TSWA Dried Residual - Grab Sample number: 195042
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
` %TS SM 2540 G 96 0.10 % 16-Dec-19 KEK
Mulitple Tube Fermentation Procedure SM 9221-E 446.4 173 MPN 16-Dee-19 KEK
Sample identification: TWSA Dried Residual - Grab Sample number: 195043
Parameter Method Result RL Units Date Analyzed Analyst Footnotes
%TS SM 2540 G 96 0.10 % 16-Dec 19 KEK
Mulitple Tube Fermentation Procedure SM 9221-E 585.6 173 MPN 16-Dec-19 KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
r
Date reviewed: NC Certification Number: 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
Signature: NC Drinking Water Certification Number: 37786
�
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

(
CHA t-OF-CUSTODY / Analytical Reque'.
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Client Name:ET
mftv
Address:
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Av
Environmental Testing Solutions, Inc.
Report to:
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PO Box 7565, Asheville, NC 28802
Phone:- t�'s�jo- Q31� Fax:
Phone: [phone], Fax: [phone]
PO Number: Zoo 01
Project Name: I-
Reauested Analyses
Project Number:
pH Checked Upon Recei t
ClZ < 0.2 mgn Upon Receipt
.o
Preservatives
t
Sample Identification
e
b
3
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U
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Additional Comments:
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Signature of Sam
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LAB'USB:ONLY;AffixlNork'order/Login,:LatieliWereo�,LisfPace:Workorder'N,i or•�:.,,.,�;•:_,f.�„ ,, ...
CHAIN -OF; CUSTODY Analytical Request Do cumen�`
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omp,any; ALL SHAONaeOrAD
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Container Preservative Type Lab;Pro ectIVlana
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Entail To:
** Preservative Types:.(1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
+'
a 77
(6) methanol, (1) sodium bisulfate; (8) sodium thiosulfate, (0) hexane,'(A)'ascorbic acid; (B) ammonium sulfate,
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, 0 Other
Copy To:
Site Collection Info/Address:
Analyses
L"eti Profile%Liiie::•:`;-i;':;'.:;;;:.� .::, :;;.:.:,:: •.::: � ::•
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sott�res t'
%C rrec
0
z5tff-oe t'
Colle ct B int
Purchase Order #:
DW PWS ID'#:
1
..
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Ct
D W LocationCode:
xJ
- atri e
P
"ce ti 1
,- ..,. . ,.. P , P.,
Colle ed B
Turnaround Date Req
immediately Pace on Ice:
•
[ ] Yes [ ']-NO
1`• `;
Sample ID- TWSA Dried Residual (non -discharge permit # VVQ 0005763)
Sample . sa
Rush:
[ ] Same Day [ ] Next Day
Field Filtered (if applicable):
[ ].Yes. [ )'No
[ ] Dispose as appropriate [ ] Return
1h
[ Archive:
[ ] Hold:
l 2 Da13 Da4 Day 5 Day
I Y [ y [ ] [ )
(Expedite Charges Apply)
Analysis:
Time Collected
Sample date- ,� / `� . f:Y N;NA"'i;'.•:,'
* Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
#of
':`
Analysis Requested:
Res
Comp / Collected (or Composite End
Customer le ID Matrix * Grab Com osite.Start' P ClCtns
u P P )..
Aluminum (Al)Molybdenum (Mo) Total Nitrogen (N)
Date Time . - Date Time
;4, is
o al Phosphorous P
Arsenic (Ar) /o Total Solids Tot p ( )
Cadmium (Cd) Nickel (Ni) Ammonia Nitrogen (NH3-N)
•
..
C
r
;`!
Calcium (Ca) Potassium (K) Total Kjeldahl Nitrogen (TKN)
"
Chromium (Cr) Selenium (Se) Corrosivity
Copper (Cu) Sodium (Na) Ignitability
Lead (Pb) Zinc (Zn) Reactivity
Magnesium (Mg) ph
Mercury (Hg) Fecal Coliform' mpn/g
plant Available Nitrogen PAN Surface applied
Special Conditions Possible Hazards
Customer Remarks / p /
r'
..
Typr :ohlceusea: <:-,'' er , „ plus'.,,.>;rau .ry,;. ;;,;,rvone; y;,;,, •:;
„+. ,,,rtyY, , _
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�Packn�"�IVlateriaEUsed. ,s? ��<;i:,,
- {/� rya., 1,' :'•itl' ��i%'
to g,#;A
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-
y" creed• �d.. S Radch'em.`sam'le'ss ;;l
S a
::FEDEX
-`'�i`eCeiSe
es
Relin 'Company:pp��qq(Sign ture)
Date/Time:
Received by/Company: (Signature)
Date/Time:
Relm is ed by/Company: (Signature) 7
Date/Time:
Received by/Co pany: (Signature)
Date/Time:
Relinquished by/Company: (Signature)
Date/Time:
Received by/Company: (Signature)
Date/Time:
np llpon�Rece'iptC' "� � oC
'rected.T mp:'': ;;L'; �''�•
r,
Page:
of:

CH1�N-OF-CUSTODY / Analytical Requ7 ,t
Client Name:
.°.W Address: I LI (o t t)U
fi
Environmental Testing Solutions, Inc.. ' ,
Report to: M\13
PO Box 7565 Asheville NC 28802 Phone: q; j� Fax:
> >(�'' 7 d
Phone: [phone], Fax: [phone] PO Number: /0 O 8 /
J.,
..FJ•+ Prniar+Nama• .• tk1� I RanllaefM Analveae
l;i
Project Number:
�{
H Checked Upon Receipt
t
Preservatives Q
C12 < 0.2 mg/1 Upon Receipt
d
�
Sample
Identification
8
;;
N
a
1: ClPO
3 ;;
4
N z
Z
U A
U
Field
8zOz
w
A
IF
vN j .+3!
x x x Z z '+6
Temp. (°C) Comments
IN
FBI
•
Temperature CC)
•. - .
',1 •
-. a
�'
•.
�
•.
4aF�%vL {
l }(i�..
�
t,� c�/� 2' (n' �` I � ``��
Received on Ice:
Y % N
, :: , t�1
r ��l �,�
15,.1
, z 1 �- r �,
r{:� : rb
�/L
C-��
1 lb,/
Sealed Cooler:
Y / N
Samples Intact:
Additional Comments:
Printe N a of Sampler: ,
Signature of Sam

(e)
Daily Dryer Record

TWSA DRYER -.'OPERATIONS
� DAILY RECORD
DATE !
T START STOP TOTAL
RUN TIME, HRS s a / ? •`�Z / 4
15L DRYER BATCH � '
FILL CYCLE START @!Q DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
" If
TEMPERATURES°F
2ND DRYER BATCH ll 11
FILL CYCLE START @ 0O, .v-i DRY CYCLE STARTED @ s DISCHARGE CYCLE STARTED
TEMPERATURES °F
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER. BATCH -
FILL CYCLE START @�_ DRY -CYCLE STARTED @�'� DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
j:�€
�b`l
S7Z
1406
�74
T I b
15
32`7
�50
qY5
b5
�l�z
1�5
-:V
s p a
3Z.cl
1
q qq
-17 a
;5
i66
3b
��
��
`(`11
�I3s
--37
S
COMPOSITE
SAMPLE
RESET #
CALCULATION
190
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
l:ogj
l7,K(93
1ST WGT. ,
2ND WGT. I .
3RD WGT.
14 , 1% x 100
&9pj =%TOTAL SOLIDSt'
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS'
GRAMS GRAMS
1ST WGT.
2ND WGT.
13RD WGT.
S:
X 100
% TOTAL SOLIDS
( DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH-
C_

r
TWSA DRYER OPERATIONS
DAILY RECORD
DATED'
START STOP TOTAL
RUN TIME, HRS
1st DRYER BATCH ► .
FILL CYCLE START @ 1,,,�7 DRY CYCLE STARTED @-lij— DISCHARGE CYCLE STARTED @
TEMPERATURES °F
DISCHARGE
TIME EXHAUST
(I 163
g.DlOfA
b3
g:�l 13
DRY
CHANBER
CHAMBER
DISCHARGE
2NO DRYER BATCH r
FILL CYCLE START @ D: DRY CYCLE STARTED @ . ( DISCHARGE CYCLE STARTED @ =a✓
mrr Or
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
TIME
DISCHARGE
EXHAUST
r
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @_ DRY CYCLE STARTED @ I DISCHARGE CYCLE STARTED @ 6' 2
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT '
ROTOR
IN
ROTOR
OUT
0.1.
3'�I
16c�
aa'7
LiI
VDT
., L)
16 V
335
C�-©
clw
Y55
v z
5
6
Z45
06
Yk5
Li Z)b
5: 7,
L
�I 33
ti q.b
COMPOSITE
SAMPLE
RESET #
CALCULATION
i c10
DISH WGT
WET SAMPLE +DISH
DRIED SAMPLE +DISH
GRAMS
GRAMS
GRAMS
GRAMS
�. ova
g, Q
1ST WGT.
Al ' a�GGO
2ND WGT.
-9 75
3RD WGT.
x 100 '_ %TOTAL SOLIDS
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST WGT.
2ND WGT.
13RD WGT.
S:
(DRIED SAMPLE + DISH - DISH WGT.
WET SAMPLE + DISH - DISH SGT.
ALARMS OR COMMENTS -
7/18/18J H
X 100
%TOTALSOLIDS
x 100
'= % TOTAL SOLIDS

:�/
9 7 l�
CTWSA DRYER OPERATIONS ; DAILY RECORD
DATE 1- -6
START STOP TOTAL
RUN TIME, HRS
15L DRYER BATCH 2/�
FILL CYCLE START @ -.3 `DRY CYCLE STARTED @ %- b� DISCHARGE CYCLE STARTED @ l D-
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
7:5&
5:410
(o3
Cs-)
33 a
35
�2
Aga
«a
443
435
a
6
l0:ans
q
4y�
c
-�
a:3
I y u
2ND DRYER BATCH
FILL CYCLE START @ I ©-3 D DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
'rCDCDATI 1'DCC 0C
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
13
3o a
0v�
�g o
01p
�3
�' 10
349
1ad
4Y5
3
al7
C
a ` 16
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3�
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145
4 i
--f 46�
,13.3
-
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ a ''-�-f DRY CYCLE STARTED @ 3.©D DISCHARGE CYCLE STARTED @_
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
�¢
01
'
3372
4qJ
43
I
o v
D
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Y�2
l`
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9
414
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0�;;2
c>
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COMPOSITE
SAMPLE
RESET#
CALCULATION
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
� �
1ST WGT. 61.7�'�
l
4
2ND WGT. p'2©,
3RD WGT.
x i0o
i1 p�(Q1=% TOTAL SOLIDS
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST WGT.
2ND WGT.
3Ro WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '= % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

TWSA DRYER OPERATIONS
1 DAILY RECORD
DATE
START STOP TOTAL
RUNTIME, HRS
15L DRYER BATCH Q
FILL CYCLE START @_ DRY CYCLE STARTED @ V a DISCHARGE CYCLE STARTED @ )1: c29 .
ICIVIrGf�/-I
DRY
TIMER
vn�.+
CHANBER
IN.
CHAMBER
OUT
ROTOR -
IN0.1.
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
g
Jta3 .'
39C�
G
8�a©
159,
/e0
l�;bo
15-7
33-6
Ly
:!q
C2
14
,gib
2ND DRYER BATCH
FILL CYCLE START @J d -. V DRY CYCLE STARTED @
DISCHARGE CYCLE STARTED @
�3
TEMPERATURES
°F
DISCHARGE
DISCHARGE
DRY
CHANBER
CHAMBER
ROTOR
ROTOR
TIME
EXHAUST
PRODUCT
TIMER
IN
OUT
IN
OUT
0.1.
An
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ `1� �S DRY CYCLE STARTED @ <15 DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
=15
ll7
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CO M POSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST WGT.
2ND WGT. , /3 5-7
3RD WGT.
J �� ( m��l✓iro`�$ioa� X100 /
f a i� '= %TOTAL SOLIDS ��(A
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST WGT.
2ND WGT.
FWGT,
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

Si G O
TWSA DRYER. OPERATIONS
DAILY RECORD
DATE
START STOP TOTAL
RUN TIME, HRS'
1s` DRYER BATCH
FILL CYCLE START @ '•� DRY CYCLE STARTED @ DISCHARGE CYCLE -STARTED @
TEMPERATURES °F
TIME
C,D:1�
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER "
C
. b
l
x?4
o
q'7
a
3 9 1
!a
153
.�� 2�
HANBER CHAMBER ROTOR ROTOR
IN. OUT IN OUT 0.1.
,39 3& q £
3� a3 3S 16 0
3:. All
YJ46 43* ao3 e�
all-
2 ND DRYER BATCH / fl
FILL CYCLE START @ l �' DRY CYCLE STARTED @ U DISCHARGE CYCLE STARTED @! 3
TEMPERATURES °F
DISCHARGE DISCHARGE DRY CHAMBER CHAMBER ROTOR ROTOR
'ram' TIME EXHAUST PRODUCT TIMER IN OUT IN OUT 0.1.
46
4 6
(� 4a g3 D =� 3 3 ad E
L4L45 '4Af2 j J- u �23 .
I�
7/18/18JH
2 ND DRYER BATCH / fl
FILL CYCLE START @ l �' DRY CYCLE STARTED @ U DISCHARGE CYCLE STARTED @! 3
TEMPERATURES °F
DISCHARGE DISCHARGE DRY CHAMBER CHAMBER ROTOR ROTOR
'ram' TIME EXHAUST PRODUCT TIMER IN OUT IN OUT 0.1.
46
4 6
(� 4a g3 D =� 3 3 ad E
L4L45 '4Af2 j J- u �23 .
I�
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH 11 ^^ xx
FILL CYCLE START @ DRY CYCLE STARTED @ a •5g DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
' TIMER
CHANBER
IN
CHAMBER
OUT '
ROTOR
IN
ROTOR
OUT
0.1.
25�5291
0
40
40-3
c
b7
32-3
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4�9
436
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COMPOSITE
SAMPLE
RESET #
CALC U LATM
DISH WGT.
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS -
I.0�2:z
jl•213Z
1ST WGT.
2ND WGT. b i %
3RD WGT.
! 100
%TOTAL SOLIDS,
I l
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST WGT.
2ND WGT.
3RD WGT.
S:
X 100
'= %TOTAL SOLIDS
(DRIED SAMPLE .+ DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ %TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18J H
(7I
Tt.

�I TWSA DRYER OPERATIONS
DAILY RECORD
DATE
START STOP TOTAL
C
RUN TIME, HRS Ld 1A L-7 / 3- \'7- 10 1
15L DRYER BATCH x
FILL CYCLE START @ l0 3 7 DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ U=
rrnnnrn nTl mCC �C
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANGER
IN.
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
TIME
p c)
i
cgs
Ja4
3
Lo
l63
j b-.)3
414s
q3
IfLt
44S
J4
all
l7't
2ND DRYER BATCH o
FILL CYCLE START @�0:-3 DRY CYCLE STARTED @ f�`•� 0 DISCHARGE CYCLE STARTED @
rrnnnroA-ri MCC 0C
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
©5
E'0
2 O
?
'435
Of-l7
O
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Q29
/ov
:tt�'
37
1
C
-a
1
3�.�
) 95-
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ a- DRY CYCLE STARTED @ -.59 DISCHARGE CYCLE STARTED @_
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT '
ROTOR
IN
ROTOR
OUT
0.1.
o f
li
.4 a.4
155
e
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3icl
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qn
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'5'.47
qqz-
5•z�.
ibi
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6 S
I63
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Li
COMPOSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
WE SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
D.�TlJ�
/Z.f7`%9
1ST WGT.
2ND WGT. p U
3RD WGT.
1 6' l 94�� t �17S� X100
11 ' �7 J9 '= % TOTAL SOLI DS
DISH WGT
WET SAMPLE+ DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST WGT.
2ND WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH -DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH
TH

TWSA DRYER OPERATIONS
DAI LY'�R ECOR D l
- DATE
•'`START STOP TOTAL
RUN TIME, HRS `�. / -822
D FILLCYCLE B TAT y DRY CYCLE STARTED @ Ii DISCHARGE CYCLE STARTED @
F @
' TEMPERATURES °F
DISCHARGE
DISCHARGE
DRY
CHANBER
CHAMBER
ROTOR
ROTOR
TZ4
2ND DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @_ DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IIN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
0
39 oa,
. 3`7,3 .
39a
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60
3
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a
3
163
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100
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4,63
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
L t�
-C-')LL CYCLE START @ 2- 53 DRY CYCLE STARTED @ J Z DISCHARGE CYCLE STARTED @ 7J� l3
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT '
ROTOR
IN
ROTOR
OUT
O.I.
3:r,�
lb6
�96
d
3a 3
t5i
T H'
50
f q/
z-v
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353
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.5�
150
sty
tryy
yz
:240
r�►
COMPOSITE
SAMPLE 0
RESET #
CALCULATION
DISH WGT
WE SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1,3,50
1ST WGT. /�•G,9��7
2ND WGT. /a.%g
WGT.
�,. r: ---2
13RD
Gl
X 100
/v?,[�D �(� •vICJ� '_ %TOTAL SOLIDS
DISH WGT
WET SAMPLE +DISH.
DRIED SAMPLE +DISH
GRAMS
GRAMS
GRAMS GRAMS
1s,r WGT.
2ND WGT.
13RD WGT.
S:
X 100 .
% TOTAL SO LIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '= % TOTAL SOLIDS
ALARMS OR COMMENTS -
/18/18JH

TWSA*DRYER OPERATIONS
DAILY RECORD
DATE 6
START STOP TOTAL
RUN TIME, HRS
5L
1DRYER BATCH
- FILL CYCLE START @ l� - DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES °F
C
Z )43 l �0314,6 q4l 4410
2ND DRYER BATCH
FILL CYCLE START @ 16'� DRY CYCLE STARTED @ C DISCHARGE CYCLE STARTED @ a s7
TEMPERATURES °F
r,
s-z
TIME
DISCHARGE -
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
O/U/nT
O.I.
%
(�/
a:ai
IS,5
3
a
43g
* of
32
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3
a ,�54
3,
0
q/-f 6
44 (
41,6
3 l
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ -
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT '
ROTOR
IN
ROTOR
OUT
0.1.
50
COMPOSITE
SAMPLE
RESET #
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7/18/18JH

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ALARMS OR COMMENTS -
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
DATE
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7/18/18JH
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ALARMS OR COMMENTS -
7/18/18JH
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ALARMS OR COMMENTS -
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
DATE
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ALARMS OR COMMENTS -
7/18/18JH

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DAILY RECORD
DATE
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ALARMS OR COMMENTS -
l
7/18/18JH
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DAILY RECORD
DATE
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FILL CYCLE START @a DRY CYCLE STARTED @ l DISCHARGE CYCLE STARTED @ r 3 7
TFMPFRATlIRFS DF
TIME
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PRODUCT
DRY
TIMER
CHANBER
IN
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OUT
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IN
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O.I.
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12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH _ J
FILL CYCLE START @�2 DRY CYCLE STARTED @ �, 2 DISCHARGE CYCLE STARTED @ 37
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
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OUT
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SAMPLE
RESET #
CALCULATION
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WET -SAMPLE + DISH
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GRAMS
GRAMS
GRAMS GRAMS
2ND WGT.
3RD WGT.
. 9 -7095 6�����l.Id X100
'_ %TOTAL SOLIDS
10 • Y I kz
DISH WGT
WETS MPLE + DISH
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GRAMS
GRAMS
GRAMS GRAMS
1� WGT.
2"D WGT.
3RD WGT.
S:
X 100
%TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ %TOTAL SOLIDS
ALARMS OR COMMENTS -
12/12/17JH

9� -y/ %
TWSA DRYER OPERATIONS
DAILY RECORD
DATE
START STOP TOTAL
j RUN TIME, HRS
15t DRYER BATCH jj�j
FILL CYCLE START @ 6.3 �1 DRY CYCLE STARTED @ 77'0 % DISCHARGE CYCLE STARTED @1
TFMPFRATURFS OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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FILL CYCLE START @ D�°� DRY CYCLE STARTED @ ! I :1i DISCHARGE CYCLE STARTED @ •3 1
TFMPFRATURFS OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
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DRY
TIMER
CHANBER
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CHAMBER
OUT
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IN
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12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ 3.',7Z DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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SAMPLE
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WET -SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1.6qVI
•
1ST WGT.
2ND WGT. -/ Q
3 RD WGT.
18,Wl t I � (t t 1 � ' X 100
(G� 5 �/ '_ %TOTAL SOLIDS C � -' (� lei
1.
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WET SAMPLE + DISH
DRIED SAMPLE + DISH
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GRAMS
GRAMS GRAMS
1ST WGT.
2ND WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.). x 100
WET SAMPLE + DISH - DISH SGT. '= % TOTAL SOLIDS
ALARMS OR COMMENTS -
12/12/17JH

� ' s-9 S6
TWSA DRYER OPERATIONS _
DAILY RECORD
DATE
START STOP • TOTAL
RUN TIME, HRS I LP f a�� / U.' 91 / j d\\
15L DRYER BATCH
FILL CYCLE START @ '43 DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
� PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
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IN
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FILL CYCLE START @ ! D DRY CYCLE STARTED @ I a$ DISCHARGE CYCLE STARTED @ a• �g
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ d - Jr0 DRY CYCLE STARTED @ 3- DISCHARGE CYCLE STARTED @_
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT-
DRY
TIMER
CHANBER
IN `
CHAMBER
OUT
ROTOR
IN
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OUT
0.1.
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2ND WGT. S /-7
3RD WGT.
— I� • �� s�� �i �� X 100 / G
-7-7 �� '_ % TOTAL SOLIDS
RESET # DISH WGT WET SAMPLE + DISH DRIED SAMPLE + DISH
GRAMS GRAMS GRAMS GRAMS
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2ND WGT.
CALCULATIONS: 13RD WGT.
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. ` '= % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
DATE - -�
START `SiT,OP TOTAL
RUN TIME, HRS �✓ -�✓� / •.'"� / Sill
15L DRYER -BATCH
FILL CYCLE START @ llJ J� DRY CYCLE STARTED @ ` / DISCHARGE CYCLE STARTED @
rrn nnrn ATI InCC 0,
TIME
DISCHARGE
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DISCHARGE
PRODUCT
DRY
TIMER
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IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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TIME
DISCHARGE
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DISCHARGE
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CHANBER
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
D0
COMPOSITE
SAMPLE
RESET #
CALC U LATI O I\
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
031
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3RD WGT.
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% TOTAL SOLIDS f Ll 9")
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS'
GRAMS GRAMS
1ST WGT.
2ND WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH -DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS 16L
7/18/18JH

u
TWSA DRYER OPERATIONS
C) DAILY RECORD
DATE
START STOP TOTAL
RUN TIME, HRS
I� 1s` DRYER BATCH
DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ FILL CYCLE START @L
z
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
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TIMER
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IN
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FILL CYCLE START @ %O • DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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7/18/18JH N

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START DRY CYCLE STARTED @ 315� DISCHARGE CYCLE STARTED
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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CALCULATIO IN
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WET SAMPLE +DISH
DRIED SAMPLE +DISH
GRAMS
GRAMS
GRAMS GRAMS
610s2417
1STWGT. 9, a----
2ND WGT.
3RD WGT.
-7 7 el 155o r X 100 C�
%TOTAL SOLIDS. 9l0
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS"
GRAMS GRAMS
1' WGT.
2ND WGT.
3RD WGT.
S:
x 100
'= % TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT. 1 x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

q�'A\ a
TWSA DRYER OPERATIONS
DAILY RECORD
DATE 3-3- 1j
START STOP TOTAL
RUN TIME, HRS
= 15c DRYER BATCH
FILL CYCLE START @f,� 3� DRY CYCLE
STARTED @ �O DISCHARGE CYCLE STARTED @
TEMPERATURES °F
.
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
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O.I.
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2ND DRYER BATCH
FILL CYCLE START @ V DRY CYCLE STARTED @ f I DISCHARGE CYCLE STARTED @ a -Oat
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
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IN
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OUT
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IN
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH -
FILL CYCLE START @ DRY CYCLE STARTED @ 3'Zy DISCHARGE CYCLE STARTED @_
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
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SAMPLE
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CALCULATION
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS
GRAMS
1' WGT. ,
OD& l
2ND WGT.
3RD WGT.
X100 G'�
'= %TOTAL SOLIDS cl L o
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS'
GRAMS GRAMS
1ST WGT.
2ND WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH -DISH SGT. '= % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

r 1 TWSA DRYER OPERATIONS _
DAILY RECORD
a DATE J - [O L 101
START STO P TOTAL
RUN TIME, HRS
15L DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ !� % 3'4
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
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(, FILL CYCLE START @ �D : f I�{ DRY CYCLE STARTED @ I 1 °I DISCHARGE CYCLE STARTED @
TEMPERATURES °F
1.
i�
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
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0.1.
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ 02"Yq DRY CYCLE STARTED @ 3: Z 3 DISCHARGE CYCLE STARTED @ �- 3
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
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100
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SAMPLE
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CALCULATION
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1. E)32S/
Ila, 116Z-
1' WGT.
2ND WGT.
3RD WGT.
X 100
CJ 13 '= % TOTAL SOLIDS
a
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS'
GRAMS GRAMS
1ST WGT.
2ND WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGTJ x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18J H

TWSA DRYER OPERATIONS
DAILY RECORD
DATE 3
START STOP TOTAL
RUN TIME, HRS
1" DRYER BATCH �( J
FILL CYCLE START @ �`" ►✓ DRY CYCLE STARTED @ ,J[) DISCHARGE CYCLE STARTED @ /
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER'
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
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TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
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TIMER
CHANBER
IN
CHAMBER
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ROTOR
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ 3%3 DISCHARGE CYCLE STARTED @ !
TEMPERATURES DF
TIME
DISCHARGE
-EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
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GRAMS'
GRAMS
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2ND WGT..
3RD WGT.
X 100 cc��
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RESET # DISH WGT WE SAMPLE + DISH DRIED SAMPLE + DISH
GRAMS GRAMS GRAMS GRAMS
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2ND WGT.
CALCULATIONS: 3RD WGT.
X 100
'= %TOTAL SOLIDS
(DRIED SAMPLE + DISH -DISH WGTJ x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

,q 5- Y& �b
TWSA DRYER OPERATIONS
DAILY RECORD
DATE 3 ` / L�- ` ! or
START STOP- TOTAL
RUN TIME, HRS CQ : / &: LtU / f
15t DRYER BATCH
FILL CYCLE START @ ( ,'3`7 DRY CYCLE STARTED @:7,- 1,0 DISCHARGE CYCLE STARTED @
TFMPFRATURFS OF
TIME
DISCHARGE
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PRODUCT
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TIMER
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TEMPERATURES OF
TIME
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PRODUCT
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ 3• a.5 DISCHARGE CYCLE STARTED
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
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RESET #
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WET SAMPLE + DISH
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CALCULATIONS:
ALARMS OR COMMENTS -
7/18/18JH
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TWSA DRYER OPERATIONS
DAILY RECORD
DATE
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1st DRYER BATCH l
FILL CYCLE START @ f �37 DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ /��3✓r
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TEMPERATURES °F
TIME
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PRODUCT
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TIMER
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CALCULATIONS: 3RD WGT.
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ALARMS OR COMMENTS -
7/18/18JH

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2ND WGT.
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ALARMS OR COMMENTS -
7/18/18JH

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RUN TIME, HRS
TWSA DRYER OPERATIONS _
DAILY RECORD
DATE 3 —1 < `lq
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TIME
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TEMPERATURES DF
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ALARMS OR COMMENTS -
7/18/18JH
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DAILY RECORD
3RD DRYER BATCH
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TEMPERATURES °F
TIME
DISCHARGE
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TIMER
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CALCULATIONS:
ALARMS OR COMMENTS -
7/18/18JH
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DAILY RECORD
DATE `S
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ALARMS OR COMMENTS -
7/18/18JH
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TWSA DRYER OPERATIONS
DAILY RECORD DATE 3 d.' t ` J p, `
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GRAMS
GRAMS
GRAMS GRAMS
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ALARMS OR COMMENTS -
7/18/18JH
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TWSA DRYER OPERATIONS
DAILY RECORD
DATE
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f RUN TIME, HRS (>✓ =aJ /°,�,� l
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TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH i _
FILL CYCLE START @ 02. '' DRY CYCLE STARTED @ 3=z-5 DISCHARGE CYCLE STARTED @
TEMPERATURES DF
TIME
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TIMER
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CALCULATIONS: 3RD WGT.
X 100
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ALARMS OR COMMENTS -
7/18/18JH

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TWSA DRYER OPERATIONS
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DATE
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TEMPERATURES °F
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TEMPERATURES DF
TIME
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GRAMS
GRAMS
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2ND WGT.
3RD WGT.
/a/q<S Dag1 X100 J'%. 33-67 % TOTAL SOLIDS
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1" WGT.
2ND WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE-+ DISH - DISH WGT. 1 x 100
WET SAMPLE + DISH - DISH SGT. '= % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

}
TWSA DRYER OPERATIONS
DAILY.RECORD
J
DATE
START STOP
RUN TIME, HRS Ul • �� / �Qi /
TOTAL
15t DRYER BATCH
FILL CYCLE START @ te;3 (? DRY CYCLE STARTED @ : % DISCHARGE CYCLE STARTED @
TEMPERATURES OF
TIME
C"0;35
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
'7� 1 a
1 i
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6
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4
1�a
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4y e
s
a3 i•
EYJ
-41
2N° DRYER BATCH,,;
FILL CYCLE'START @'%�-� DRY CYCLE STARTED @ �cZd DISCHARGE CYCLE STARTED @
0,4 0
,Q
TEMPERATURES °F
(1
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
•CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
a
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OR a R,
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t
-7/18/18J H

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ = 50 DRY CYCLE STARTED @ 3'Z6 DISCHARGE CYCLE STARTED @ 6,
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
3;z6
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D
3cc Z .
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iLb
M
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Zz3
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L3
COMPOSITE
SAMPLE
RESET #
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS GRAMS
c 037 Z
GRAMS
51
1ST WGT. %q
2ND WGT.
3RD WGT.
% TOTAL SOLIDS
DISH WGT WET SAMPLE + DISH DRIED SAMPLE + DISH
GRAMS GRAMS GRAMS GRAMS
1' WGT.
2ND WGT.
CALCULATIONS: 3RD WGT.
X 100
% TOTAL SOLIDS
(DRIED SAMPLE'+ DISH — DISH WGT.) x 100
WET SAMPLE + DISH — DISH SGT. '= % TOTAL SOLIDS
ALARMS OR COMMENTS —
7/18/18J H

� sI
TWSA DRYER OPERATIONS _
Y' DAILY RECORD
DATE
START STOP - TOTAL
RUN TIME, HRS
1st DRYER BATCH
FILL CYCLE START @ Co��O DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ �Uf
-- _ - -.- TFMPFRATI IRFC or
DISCHARGE
DISCHARGE
DRY
CHANBER
CHAMBER
ROTOR
ROTOR
TIME
EXHAUST
PRODUCT
TIMER
IN
OUT
IN
OUT
O.I.
°I 4 5--
- -1-(P 4
37
)5 0
4qS
136
s
a s 'y
. 44
a315-
2ND DRYER BATCH
FILL CYCLE START @ / V9DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TF:KADGDATI IDCC OE:
DISCHARGE
DISCHARGE
DRY
CHANBER
CHAMBER
ROTOR
ROTOR
TIME
EXHAUST
PRODUCT
TIMER
IN
OUT
IN
OUT
0.1.
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START v • J` 3 �C� J1 �^
ART @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
3)50,
1`70
0
' 3"70
390
01"
'f . 2b
! (-o
�30-1
�5 0
�f
1 b .
4 o 5
I
t W.
arm(
51 ID
iVe
31�
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46
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2,15
vi
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L(4'5
436
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Z2,4:
t;qs
Is(
Ifw
1951
Lf(4tf 1
4-41
q q-.if
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COMPOSITE
SAMPLE
RESET #
CALCU LATI O I\
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1,
Z 5, 5(o 32 :
1STWGT..
2No WGT. 2, 6 D -
3RD WGT.
r
X100
% TOTAL SOLIDS
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1� WGT.
2ND WGT.
3RD WGT.
S:
X 100
%TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '= % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH
'�l,
�J

TWSA DRYER OPERATIONS
DAILY RECORD
DATE
START STOP TOTAL
RUN TIME, HRS
15C DRYER BATCH
- FILL CYCLE START @ DRY CYCLE STARTED @ �7 D3 DISCHARGE, CYCLE STARTED @
TEMPERATURES DF '
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER ,
IN
CHAMB'ER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
7.03
I� i;-qa,
6
21ol,
31�0
79
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51)
J4 D
7 ...__:
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8
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3-';�E
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440
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en-1
2AfD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TFMPFRATl1RFS OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
- IN
ROTOR
OUT
0.1.
l = a3
6 L
ail
a
3sa
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a: 43
l% a
a
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s
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ , = 53 DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ J
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
Sol
6
qOcf
3B5
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lGq
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7-
COMPOSITE
SAMPLE. ,
RESET #
CALCULATI01N
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
< < 0 t -1 k
23 8 -7 2,
1ST WGT. . 706 -
2ND WGT.
3RD WGT.
a91a /.0171
X 100
'= % TOTAL SOLIDS / (� 6. 0-5' �0 r
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1r WGT.
2ND WGT.
3RD WGT.
S:
X 100
'= % TOTAL SOLIDS
DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

g-7- a& t
TWSA DRYER OPERATIONS
DAILY RECORD
DATE 4-1 tD
START STOP . TOTAL
RUN TIME, HRS �Q oZ oZ / 3RD
1st DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ e DISCHARGE CYCLE STARTED .@ 6
TFMPFRATIIRFS OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
-ROTOR
IN
ROTOR
OUT
O.I.
6
3 q b
GqEo
1119 9
Iflto
a
1 sD
931
5 1
3 7.5
63
ao _-�r
Lf q Ito
414 t
4
a,33
',Il7
2NO DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ E DISCHARGE CYCLE STARTED @ a 3�
TFMPFRATIIRFS OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
83.
A56
b fv
1`7 V
j
,o
la�.�b
& 93
4-7
ADa
)144
L237
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s
/50
S
113,5
a� 4
e.
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ ZI 1
DISCHARGE CYCLE STARTED @ '
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
;2(
17 z
300
0
L-f( Z
3W
1+1 Z.
I(Z
SI-3
► I
1 -77 Z
313
-5D
43 4F
4 z2
qs L(.
r ? 5
J-w
5', 01
1 G 3
3,51
!0
`-fq -7
L4 3 -7
14Y -7
2,55
JW
56
1�
��4
+�5
L35
qq5
Z,�
of
tp',Np 1
17 g
Lf
LfIf 11
zL f
�-
COMPOSITE
SAMPLE
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
b 32(.
7--7..'t 3G8
1ST WGT.
2ND WGT.
3RD WGT.
X100 /o
v % TOTAL SOLIDS
RESET # DISH WGT WET SAMPLE + DISH DRIED SAMPLE + DISH
GRAMS GRAMS GRAMS GRAMS
15r WGT.
2ND WGT.
CALCULATIONS: 3RD WGT.
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

g7,5-3�b
0
TWSA DRYER OPERATIONS _
DAILY RECORD
DATE Z [
START STOP TOTAL
RUN TIME, HRS ; d / Qvi,3
1st DRYER BATCH % R
FILL CYCLE START @ lY -�� DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER.
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
r )°►
6D
g
D
3d,
37(
9c,
1*3
C
8
M
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4 �2, Z
4b
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33
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1 c103
39
/90
44S
-ZiL4
a.
2ND DRYER BATCH i ff
FILL CYCLE START @ D fJr'7 DRY CYCLE STARTED @ I I ' DISCHARGE CYCLE STARTED @
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
V7
/ F
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ •.J DRY CYCLE STARTED @ 3-�2 DISCHARGE CYCLE STARTED @
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
��-
44'.17.
y o-
UP
16Z
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Z)
ft
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-sp
6 ilk
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�ja°1
CIS
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yIAz
�N
2N5
COMPOSITE
SAMPLE
RESET # ,
DISH WGT
GRAMS
WET SAMPLE + DISH
GRAMS
DRIED SAMPLE + DISH
GRAMS GRAMS
�r 03�3
Qj)1ST
WGT.. / Q
lZi V 773 .
2ND WGT.
3no WGT.
X 100 `-
%TOTAL SOLIDS 3 �6
DISH WGT WET SAMPLE + DISH DRIED SAMPLE + DISH
GRAMS GRAMS GRAMS GRAMS
1l WGT.
2ND WGT.
CALCULATIONS: 13RD WGT.
X 100
'= % TOTAL SO LI DS
(DRIED SAMPLE + DISH - DISH WGTJ x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD.
DATE
START STOP TOTAL
RUN TIME, HRS
�10
1st DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ 7. D DISCHARGE CYCLE STARTED @ l D} 3
TFMPFROTI IRFC °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
'-a9
o
R r
©
&W
/q-, 3
c
i6q
3)q
5D
ifas
q3
&a
c
jo
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ab
a
q�3q
1 a
379
16b
��
4 3�
�I),�
1 �.
E0
I .3,4
13
qgq
r2- 0,5
qyo
4-1le
a3
2ND DRYER BATCH
FILL CYCLE START @ I Q iY`i DRY CYCLE STARTED @ I DISCHARGE CYCLE STARTED @
TFMPFROTI IRFC OF:
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
03
D
qQ�
33).
4e to
ls
to
D
4q
'i3
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cLo
Y39
4-q
a ,31
Ep
:39
r%
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11L 11
414 r
4/4(p
a 4
E
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
D
�a
1s a
COMPOSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST WGT.-
2 ND WGT.
3RD WGT.
rP ,
6 x100
%TOTAL SOLIDS G(p
DISH WGT WET SAMPLE + DISH DRIED SAMPLE +DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST WGT.
2ND WGT.
[FWGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. =•% TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/181H

I!
TWSA DRYER OPERATIONS
DAILY RECORD
DATE
START STOP TOTAL
RUN TIME, HRSF / La'-, gct 3
15L DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ i - �� DISCHARGE CYCLE STARTED @ &
TEMPERATURES OF.
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
C39 a
-7 ;51
AaS
319
6,9
z1a
:lil
I-lo,3
3-5T
Jaa
4.
q ;?S
• o 11 )
1 -5
a©5
qqs
2ND DRYER BATCH
FILL CYCLE START @ l DRY CYCLE STARTED @ a cT DISCHARGE CYCLE STARTED @
TFMPFRATURFS OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
• 'IN
ROTOR
OUT
O.I.
f =Iq
36i
j4oLf
j9-7.
46,c�
31
5 �
3 a
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) 77
C-
'
3
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4
aaa
C�,oD
gL43
qys
C:
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD' DRYER BATCH
FILL CYCLE START @ , DRY CYCLE STARTED @ 3-L DISCHARGE CYCLE STARTED @_
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT.
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
10
Asl
Z15 .
�P
%tA
1. 6-1
6l 3�
\ SOS
��
/ �c3
' `�l�l
`lei 1
\kk5
COMPOSITE
SAMPLE
RESET #
CALCULATIOIN
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
Ali164,5t&
1ST WGT. V-e,
2ND WGT. 6 6 75"
3RD WGT.
r�r
p
%TOTAL SOLIDS�-
DISH WGT
GRAMS
WET SAMPLE + DISH
GRAMS
DRIED SAMPLE + DISH
GRAMS GRAMS
1' WGT.
S:
2ND WGT.
3RD WGT.
• r
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE +DISH -'DISH SGT: "= %TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

g6r77�o
- c
TWSA DRYER OPERATIONS
DAILY RECORD
DATE.
START STOP TOTAL
RUN TIME, HRS ; 0
1st DRYER BATCH
FILL CYCLE START @ ° �� DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ f
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
rr -2 It-plo
348
4 p: If'f.
15D
q m
44-5
4�4r
2,2.7 •
e
197
2NO DRYER BATCH
FILL CYCLE START @ 4 _S:54 DRY CYCLE STARTED @� / - Z DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
b:l.
Il-C-a4
41 F?
-
41 T
/1-6
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5 �'
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C0
f:0"4
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ibo
444
3�
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161-1
L
0
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ ��lo DISCHARGE CYCLE STARTED @_
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
3':w
it (
aCs
-�n,6
3�Z '
��
15
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_
KI (
tz
Obi
2-() (.
ul-
Y D
L/3
2Zo
3'/1
S%Km
6
3�Z
�✓� (�
k j S
4�5
INS
6:25
qq6
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Lfgq
z7c
�H
COMPOSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
GRAMS
WET SAMPLE + DISH
GRAMS
DRIED SAMPLE + DISH
GRAMS GRAMS
11
bq,
1' WGT. `.
2ND WGT.
3RD WGT,
13, go-5-3 m 9b 74-75-1 x 100
t 3, 953 I '_ % TOTAL SOLIDS go
DISH WGT WET SAMPLE + DI$H DRIED SAMPLE + DISH
GRAMS GRAMS GRAMS GRAMS
1' WGT.
2ND WGT.
3RD WGT.
S:
X 100
%TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH --DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS
7/18/18JH

:c
TWSA DRYER OPERATIONS _
DAILY RECORD
DATE _ a '1 ej
START STOP TOTAL
RUN TIME, HRS 22
15L DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @_ DISCHARGE CYCLE STARTED @
TEMPFRATURFS OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
7:11
l(oa
- -11;�R
d
39
--�
39�
)4+
lt-7
3
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S &
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joo
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c
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445
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2NO DRYER BATCH
FILL CYCLE START @ =� DRY CYCLE STARTED @ �DISCHARGE CYCLE STARTED @
TEMPFRATURFS OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ O DISCHARGE CYCLE STARTED @
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
L11Li
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COMPOSITE
SAMPLE
RESET #
CALCU LATIO IN
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS ' '
GRAMS
GRAMS
032-7
13
1srWGT.
%
2ND WGT.
r 3 ref
3RD WGT.
X 100
1 3, %TOTAL SOLIDS Gr
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1' WGT.
2ND WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
DATE -
START STOP TOTAL
RUN TIME, HRS
1st DRYER BATCH
FILL CYCLE START @ �% DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER'
CHANGER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
D
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FILL CYCLE START @ L (J_'7' ► DRY CYCLE STARTED @ �a� DISCHARGE CYCLE STARTED @_ 2-,qv
`�-f— TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
�RD DRYER BATCH
ILL CYCLE START @ a , J 6 DRY CYCLE STARTED @ �. DISCHARGE CYCLE STARTED @_
TEMPERATURES °F
TIME ..
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
1,15,
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45
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in .
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COMPOSITE
SAMPLE
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1'7'�qj WGT. �, 9/0
2ND WGT. /,o, 9979
•
3RD WGT.
1030t x100
[3, 44 g 9' v30 (� '_ % TOTAL SOLIDS 9 6, 3 'O
DISH WGT WET SAMPLE + DISH DRIED SAMPLE + DISH
GRAMS GRAMS GRAMS GRAMS
1ST WGT.
2ND WGT.
CALCULATIONS: 3RD WGT.
x 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.1 x 100 <
WET.SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
DATE " I
START STOP TOTAL
RUN TIME, HRS I � ;) 0 / -7
I" DRYER BATCH
FILL CYCLE START @ ° ?j f DRY CYCLE STARTED @ .Da DISCHARGE CYCLE STARTED @
TGKADCDATI MCC OC
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
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2ND DRYER BATCH
FILL CYCLE START @ Q DRY CYCLE STARTED @ D,�7 DISCHARGE CYCLE STARTED @
TPKADIMATI IRGC 01:
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH y r
FILL CYCLE START @ a 'J �r` • DRY CYCLE STARTED @ ` � DISCHARGE CYCLE STARTED @_
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT_
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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COMPOSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
l
I WGT.
2ND WGT. a 76
3RD WGT.
X 100 OO
'=%TOTALSOLIDS
DISH WGT WET SAMPLE + DISH DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1' WGT.
2ND WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGTJ x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL.SOLIDS
ALARMS OR COMMENTS -
7/18/18J H
c-

TWSA DRYER OPERATIONS _
DAILY RECORD
DATE -S
START STOP TOTAL
RUN TIME, HRS (!2 =off v
1st DRYER BATCH r _
FILL CYCLE START @ t0.3'7 DRY CYCLE STARTED @ . I DISCHARGE CYCLE STARTED @ D
TFMPFRATI IRFS Or -
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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2ND DRYER BATCH
FILL CYCLE START @ 1� • DRY CYCLE STARTED @ o DISCHARGE CYCLE STARTED @ (�
TFMPFRATI IRFS OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ a ' ° DRY CYCLE STARTED @ - ZS DISCHARGE CYCLE STARTED @c_
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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COMPOSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
.GRAMS
GRAMS
GRAMS GRAMS
1ST WGT.
2ND WGT.
3RD WGT.
%TOTAL SOLIDS
DISH WGT
I WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS*
GRAMS GRAMS
1Sr WGT.
2ND WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
DATE tb -11h �
START STOP
RUN TIME, HRS
TOTAL
1st DRYER BATCH ,o11
FILL CYCLE START @ DRY CYCLE STARTED @ ; It DISCHARGE CYCLE STARTED @
1
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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1
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AND ��i
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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.q
39
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0
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @
DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
COMPOSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
WE SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
o l7 7 6 ti`�
2
J
1ST W.GT. '
a Ot d 0�
,
2ND WGT. /3, /d %6O
3RD WGT.
�5'7
x 100
'= %TOTAL SOLIDS
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST WGT.
2ND WGT..
3RD WGT.
S:
x 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

RUN TIME, HRS
TWSA DRYER OPERATIONS _
DAILY RECORD
DATE U — / 0 — `
STARTSCCTiiOP TOTAL
S
15C DRYER BATCH tj3' p
FILL CYCLE START @ DRY CYCLE STARTED @ O , a- DISCHARGE CYCLE STARTED @
TFMPFRATI IRFC 01:
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
--ROTOR
IN
ROTOR
OUT
0.1.
gra
A
qc�
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A 1
443
fo
4g15
s+v4 )vao
2ND DRYER BATCH ; JCf
FILL CYCLE START @. DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
�35
1g
7/18/18J H ( ` n
[�(� a��vwlq

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @_
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
'-0
COMPOSITE
SAMPLE
RESET #
CALCULATIOt
7/18/181H
DISH WGT
GRAMS
WET SAMPLE+ DISH
GRAMS
DRIED SAMPLE+ DISH
GRAMS GRAMS
1T WGT.
2ND WGT. /3
3RD WGT.
. �..�
_ /.3 D /
�,,�� X 100 �
7 35 — . v / a- / '= % TOTAL SOLIDS
DISH WGT WET SAMPLE + D15H DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
f WGT.
2ND WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH-; DISH WGT.) is 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SO Ins

ram. TWSA DRYER OPERATIONS
- DAILY RECORD
DATE q
START STOP - TOTAL
RUN TIME, HRS.
1st DRYER BATCH
FILL CYCLE START @ J d2 DRY CYCLE STARTED @ %; iZ u DISCHARGE CYCLE STARTED
TFMPFRATI IRFC OF'
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
;�.s
e
le
p q3 I q Li 14 4 S-- Lj'3 T�67gE
2ND DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ / / oil DISCHARGE CYCLE STARTED @
TEMPFRATURFS OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
. IN
ROTOR
OUT
0.1.
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
� � I
CILL CYCLE START @ 3 DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ L,
>r
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANGER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
o�
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0
6-7
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5:
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2-61
COMPOSITE
DRIED SAMPLE + DISH
DISH WGT
WET SAMPLE + DISH
SAMPLE
-GRAMS
GRAMS ,— '
GRAMS
GRAMS
1TWGT.:
,
- ..
2ND WGT.
3 S
..
r
3RD WGT:
•_
C '
x 100
&
'_
/ %- l D 6 o
- /.O a 7
% TOTAL SOLIDS / • / 5L
RESET #
DRIED SAMPLE + DISH
DISH WGT
WET SAMPLE + DISH
GRAMS
GRAMS
GRAMS
GRAMS
1' WGT.
2ND WGT.
CALCULATIONS:
3RD WGT,
X 100
% TOTAL SOLIDS
-
(DRIED SAMPLE + DISH-- DISH WGT)
x 100
WET SAMPLE+ DISH. -DISH
SGT.
'_ % TOTAL_SOLIDS
ALARMS OR COMMENTS -
•
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
DATE f / L
START STOP TOTAL
` RUN TIME, HRS- I F - ' / ka al� / I t) f
I" DRYER BATCH
FILL CYCLE START @ :.J� DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TFMPFRAT1 IRGrl OR
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
Lq5
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44,5 -
143
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10
2ND DRYER BATCH
r
FILL CYCLE START @ j DRY CYCLE STARTED @ �.•1 DISCHARGE CYCLE STARTED@�7
TFMPFRATI IRFC OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
L CYCLE START @ 3• t7 DRY CYCLE STARTED @ 3%j DISCHARGE CYCLE STARTED @ �� Z
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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17-5
q31
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7
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' sq
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COMPOSITE
SAMPLE
RESET #
DISH WGT
WET SAMPLE + DISH-
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
t.o�(a1
f f l°I3v
1ST WGT.
2ND WGT.
3RD WGT..
X 100
%TOTAL SOLIDS
DISH WGT WET SAMPLE + DI$H DRIED SAMPLE + DISH
GRAMS GRAMS GRAMS GRAMS
1' WGT.
2ND WGT.
CALCULATIONS: 13RD WGT.
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH-- DISH WGT.) x 100.
WET SAMPLE + DISH - DISH SGT. '=. TOTAL SOLIDS
ALARMS OR COMMENTS -

i
1
RUN TIME, HRS
TWSA DRYER OPERATIONS _
DAILY.RECORD .
DATE o�i� '" ,� g r f dv, gs
vte �� a -
START b STOPOTAI&.&," ,
15L DRYER BATCH p� `
FILL CYCLE START @ �J l� DRY CYCLE STARTED @_ d DISCHARGE CYCLE STARTED @ /
TEMPERATURES- 0F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
TTAt
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6
0,912�
301
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9:4
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ND
2DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ �� �7 DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
• IN
ROTOR
OUT
0.1.
`-7
a;
o
J43 5
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d- b q
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I (Q5
443
431
415
a;27
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
'LL CYCLE START @ DRY CYCLE STARTED @ l 'S i DISCHARGE CYCLE STARTED @;�
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANGER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
S: H C
1
330
j O
145
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Yt(z
2�z�
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Ib�
3bH
JdbLf
LI
tl Z
apt%
sir
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�= 1
f 73
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R�
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ItgZ
/��z
2'-r5 I
:7/-t
COMPOSITE
DRIED SAMPLE + DISH
DISH WGT
WET SAMPLE + DISH
SAMPLE
GRAMS
GRAMS
GRAMS GRAMS
:
t.0-5515'
56Z—
1'TWGT.
2ND WGT..
3aD WGT. ,
X100
/'03SS
-0
-/TOTALSOLIDS
RESET #
DRIED SAMPLE + DISH
DISH WGT
WET SAMPLE + DISH
GRAMS
GRAMS
GRAMS .GRAMS
1' WGT.
2ND WGT.
,
CALCULATIONS:
3RD WGT.
X 100 1,
% TOTAL SOLIDS i
(DRIED
SAMPLE + DISH-- DISH WGTJ x 100
WET SAMPLE + DISH.-
DISH SGT.. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

TWSA DRYER OPERATIONS _
DAILY RECORD
DATE 0 ��
_ START STOP TOTAL
RUN TIME, HRS CQ 33
1sc DRYER BATCH
FILL CYCLE START @' © DRY CYCLE STARTED @ ; I v< DISCHARGE CYCLE STARTED '@ l 02
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
(oq-
. G U o
41�
A40
47/%7
J66
co
1`7D
3ail
5a
45 -
135
L451 -
CR06
-7 t
q43
q,36
9011
g
1s0
`f1-e5
yo 7
5� 44 5�
2ND DRYER BATCH
FILL CYCLE START @ 6 :3 6 DRY CYCLE STARTED @ { s6� DISCHARGE CYCLE STARTED @ 2
t
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
415.
�a
17
d= h
3 �a
- /GTE
4y_3
=�
1= `7
31 .9,
1L5'v
144s
413&
Zlq,3-
d. /s
�
7 7
443
9
LHS
4ji3
7/18/18JH .

TWSA DRYER OPERATIONS'
DAILY RECORD
3RD DRYER BATCH rr��
(7 L CYCLE START @ DRY CYCLE STARTED @ ! •/ DISCHARGE CYCLE STARTED @ '
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN.
ROTOR
OUT
0.1.
110
*/ 2 .
4 2Z
/ 7 z
<--(&
�I . v l
32 6
—
�I I _
L(3pi
3'�h
i l]
��►�b
�(36
q3
2Zg,"
71r
5'4 1.
'toy
`363
) S D
4H5
1(,55
qqz
COMPOSITE
SAMPLE:
DISH WGT
GRAMS
WET SAMPLE + DISH
GRAMS
DRIED SAMPLE + DISH.
GRAMS GRAMS
1-2S.-56�
1�T WGT. / - x
."
2ND WGT. 3. 3 9 q-
3RD WGT.
X 100 Q
% TOTAL SOLIDS /
RESET # DISH WGT WET SAMPLE + DI$H DRIED SAMPLE + DISH
GRAMS GRAMS GRAMS GRAMS
1 T WGT.
2ND WGT.
CALCULATIONS: 13RD WGT
• X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH-- DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. :`_.% TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/181H

MONTHLY OPERATION', ALS
Sludge
-
PolymerUsage
# of days press was run 6
Press run cost = Hrs X $20.00 $1,038
# of days dryer was run 7 Dryer run cost = Hrs X $20.00= $1,356
Total distributed to the public= 5 tons
Total hauled to landfill= 0
Total Residual Cost for the month = $3,740.62

TWSA DRYER OPERATIONS a _
� DAILY -RECORD ,
DATE�j
START STO P TOYAL
RUN TIME, HRS. : aL7 / /
c
15L DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ s O DISCHARGE CYCLE STARTED @ D �3
TEMPERATURES °F
t'
r
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
1 S
) &3
2g9
o
a L
3?,-4
G
481,
E
SA
.3.dV
._T 0
4 a
aq
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C
-yVr
C2a$
9.4%
AS
3-7
U
qql
1-1-35-
a() to
�
��b p
2ND DRYER BATCH ry
FILL CYCLE START @ b DRY CYCLE STARTED @ i v��- DISCHARGE CYCLE STARTED @
TPhADMATI IRGC °I_
DISCHARGE
DISCHARGE
DRY
CHANGER
CHAMBER
ROTOR
ROTOR
TIME
EXHAUST
PRODUCT
TIMER
IN
OUT
IN
OUT
0.1.
6
3 a
'61)
43 5
. /9 $'
E
b
5
Z3 to 0
LDd
li 37
a
l� �6
I
4
Job
3 .
44,5
4q,4-
C219
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
!L CYCLE START @' �✓ DRY CYCLE STARTED @ < (� DISCHARGE CYCLE STARTED @
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
' ' IN
ROTOR
OUT
0.1.
cg
`75
, 6`7
D
`-f c8
405
40
1-? Z
:�a
<
1-,sz
�a
I q45.456
.44
a66-
0-b
VAX
437
L�
COMPOSITE
SAMPLE
RESET #
r
•
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1TWGT. 74/
-
2"D WGT. //. a %0 d .
3RD WGT.
A 0 qw? - X 100 v'
'=%TOTALSOLIDS
DISH WGT WET SAMPLE + DISH DRIED SAMPLE + DISH /
GRAMS GRAMS GRAMS GRAMS
1T WGT.
2ND WGT.
CALCULATIONS: 3RD WGT
X100 `-
'= %TOTAL SOLIDS _
" (DRIED SAMPLE + DISH- DISH WGTJ x 100
WET SAMPLE + DISH - DISH SGT. '= % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH -

TWSA DRYER OPERATIONS
DAILY RECORD
DATE I
f
START STOP TOTAL
t� 2
RUN TIME, HRS
I" DRYER BATCH
FILL CYCLE START @ ((� •3J DRY CYCLE STARTED @ % DISCHARGE CYCLE STARTED @
i f '
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
7A47
`% to
a93
®
3q'�'
3'� [
3W
/4
C0
5�
lo9
3
"Ng
435
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$=�'11
kq
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P
Z139
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co g
1
' 3 3
1,r, D
-445
s
a1
c
2ND DRYER BATCH r
FILL CYCLE START @ DRY CYCLE STARTED @ I �J DISCHARGE CYCLE STARTED @
TEMPERATURES °F
r�
TIME.
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
. IN
ROTOR
OUT
0.1.
Q
q
: "v
jj45
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�
a 3
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D
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435
s
C2:z' -
cv
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l 3"
t�qa,
0V
I-N5
11 q3
111145
C s
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
CILLr CYCLE START @ DRY CYCLE STARTED @ 3'Zz DISCHARGE CYCLE STARTED @ D-
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
AN
ROTOR
OUT
0.1.
soli
376
-M7
IJ_a
-IL1q -
437
• Z
t `�
3�7
p D
kub
v5
4k5
5:bz
t73
�861
`�©
�IK 5
K35
qH 3
2, o
Z-7 �
2,57 -
3'!f
COMPOSITE
SAMPLE
`RESET #
CALCULATION
0
DISH WGT
WET SAMPLE +.DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
L)
15 2-v
1Sr WGT.. •%S. S �33
2ND WGT.
3RD WGT.
1�,��34 � — /:r935y xioo '
p q_C) " % .03 S '_ % TOTAL SOLIDS �- v1
DISH WGT WET SAMPLE + DISH DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
f WGT.
2ND WGT.
3RD WGT.
S:
x 100
% TOTAL SOLIDS
(DRIED SAMPLE+ DISH•=DISH WGT.) x 100
WET SAMPLE +DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
.
DATE_
START STOP TOTAL
RUN TIME, HRS
15' DRYER BATCH _
FILL CYCLE START @� o DRY CYCLE STARTED @ 1 • /5 DISCHARGE CYCLE STARTED @
TEMPERATURES °F
C'
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR.
IN
ROTOR
OUT
0.1.
3 2`
399.
l 301
8:05
- 6
,4
J-M-5
q-,f 1,7
4 ,-;g5
S?
331
�� a .
446 -
4c? 4
144t3-
a.
` ;43-
1 A3"
a
4145
1 q34
I gjy5-
led
aq- o 1 I s4 11441 1 �. o,,-�- I q43 1 14# 3 1 4qv I;? q
2ND DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ � DISCHARGE CYCLE STARTED @ a
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
a9
814 .
o
) (3
c
:)
t
.314
q
44
l?4
e
o (�
1 �e
331
q 4s
-'Zi g
'7
3 - q.
lig6
43
lvb
a;z3
E
, ��
S 2
4111
4LfS
)�q3
a 57
C6
C.
7/18/18JH

TWSA DRYER OPERATIONS
. DAILY RECORD
3RD DRYER BATCH
LL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @l.
TEMPERATURES °F
DISCHARGE
EXH AUST
DISCHARGE',
& *iU C T•
I ^CHAMBER
•
•
COMPOSITE
SAMPLE
C.,
RESET #
CALCULATION
DISH WGT
WE SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
�..rias3-
3f,I�%�
1�WGT. .3�•�a-�QJr
2ND WGT.
3RD WGT.
3d•S3/9 toX100 ( [�
.3I• f q-%d '=%TOTAL SOLIDS
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS'
GRAMS GRAMS
1' WGT.
2ND WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGTJ x 100
WET SAMPLE + DISH -DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS - 'A &_9K+ rner- a`
7h
H

TWSA DRYER OPERATIONS
DAILY RECORD
DATE C" " it —lot
START STOP - TOTAL
RUN TIME, HRS. 3cl /
y 1s' DRYER BATCH
-aJ FILL CYCLE START @ a 3 DRY CYCLE STARTED @,��' DISCHARGE CYCLE STARTED @ 3
TFUDFRATI IRGC oC
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANGER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
399J
48
c
�10
1-1o.4
:33to
)oo
=t46
1438
qqb
aag.
�
/64
:.: 373
i�
�.�
.43 4
J4 4 s
2ND DRYER BATCH ` q
FILL CYCLE START @ !y : DRY CYCLE STARTED @ y I DISCHARGE CYCLE STARTED @ .3
TGUPGRATI IRGC or:
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
31 q
SO
-qYl0
q 37
jj eo
e
q
�3
33�
--loa
I 'f'ft5
14;3"3
9 zj�--
az16
eo
: 4 q
`11
3-7&
I5D
AIs
�3s
q
4L4 s
4 Z41
44,5
L.
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
C.LL CYCLE START @� DRY CYCLE STARTED @ 3,ZL� DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
' IN
ROTOR
OUT
0.1.
:�,zh
177h
2v
6
yl
�q
3117
I�
3�1�1
D�
fir;
si
Ltd
a37_
ZT&
L( 30
COMPOSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
GRAMS
WET SAMPLE + DISH
GRAMS
DRIED SAMPLE + DISH
GRAMS GRAMS
i
1' WGT.
S:
Z' WGT.
3RD WGT.
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
i
l i
1T WGT. /.� : &/ F %.
2ND WGT. ��.
[3ac' WGT.
f-
L�•/+b/lo — �•���� X100
'=%TOTALSOLIDS DL v/�/ ,
X 100
% TOTAL SOLIDS '
(DRIED•SAMPLE + DISN-- DISH WGT.) x f00 \
WET SAMPLE + DISH.- DISH SGT. % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

TWSA DRYER OPERATIONS r
DAILY RECORD
A- DATE
START STOP TOTAL
RUN TIME, HRS
1st DRYER BATCH ll , j
FILL CYCLE START @ W : 4 ( DRY CYCLE STARTED @ b I DISCHARGE CYCLE STARTED @ 6 0 � �'{
TPKAPPPATI IRGC Or:
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
.OUT
ROTOR
IN
ROTOR
OUT
0.1.
-7 (�
(o3
33 b
�
39
/19
3[ov
o
43011,
114W,
l
S-A
16A
350
aa'9
ro
2NO DRYER*BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TFMPFRATI IRGC %
DISCHARGE
DISCHARGE
DRY
CHANBER
CHAMBER
ROTOR
ROTOR
1'IM�
EXHAUST
PRODUCT
TIMER
IN
OUT
I
OUT
0.1.
L-
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
1)DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
rCKADCDATI WIN OF
TIME
DISCHARGE
PRODUCT
DRY
TIMER
CHANGER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
DISCHARGE
EXHAUST
d
'
0a
o
COMPOSITE
SAMPLE
RESET #
CALCU LATIO �
DISH WGT
WET -SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST W GT. o� cf • 3 /./
2ND WGT.
3RD WGT.
X 100
a a • �� 33 r , v D / '= % TOTAL SOLIDS
DISH WGT WET
SAMPLE +DISH
DRIED SAMPLE +DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST WGT.
2ND WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '= % TOTAL SOLIDS
ALARMS OR COMMENTS -
C-
12/12/17JH

TWSA DRYER OPERATIONS _
DAILY RECORD
DATE '' 1 ,7 r q
START STOP TOTAL
RUN TIME, HRS ; 3
y
15t DRYER BATCH nn
FILL CYCLE START @ -� DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ U o3
TEMPERATURES °F
(7
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER •
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
7%-A
3`16
3qi�
s.5
c
S:b�
!r g
3
6
q
4AT
!7a
eil
$:58"=..
9.-14q I
t (e�
3
1O
445
1 1435
1 a.1
No 43
2ND DRYER BATCH j
FILL CYCLE START @ o •5 DRY CYCLE STARTED @ 1 tg DISCHARGE CYCLE STARTED @ a8�
TFMPFRATI IRFS °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT.
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
ob
3a2�
q�'.
3 W
163
Li I
3310
a
-94`7
434
/8'ep'
�
oq
3 ag
JoD
'H3-
43 T
� a
l '5P�
15 0.
q is
eo
__LagJ
j44 [
ape
I 4q3
)443
lqs
CLO
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
`L L CYCLE START @ a • 5'6' DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
1
/-/.D 6
l7
l
L(
ZVI
5
c s
1
1 a
�[LA
Q-A/
D3
i 7 Z
y3
z�6
�I
l°l i
TA
KZ
2syU4.
COMPOSITE
SAMPLE
C, �/• 9a- — �,v�Os� X 100 g
q-,o '_ % TOTAL SOLIDS
ti
RESET# DISH WGT WET SAMPLE + DI$H DRIED SAMPLE + DISH
GRAMS GRAMS GRAMS GRAMS
1T WGT.
2ND WGT.
CALCULATIONS: 3RD WGT.
r
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH•- DISH WGT) x 100
WET SAMPLE+ DISH =DISH SGT. r. %TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH
DISH WGT
WET"SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
u`
1'WGT.
-
2ND WGT.
3RD WGT.

N
TWSA DRYER OPERATIONS
DAILY RECORD
DATE d. -3
START STOP TOTAL
RUN TIME, HRS.F1
1"' DRYER BATCH FILL CYCLE START @ b - rJ t DRY CYCLE STARTED @__j,*)Q_ DISCHARGE CYCLE STARTED @
TCAADCDATI IDCC OC
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
06q0
3 9
143
c�
%l 7
50
` l
2
4 zi 1 `
17 4�
�
15 o.
3140
l 611
4Ys-
3'7
3q 1
f- o
4
2ND DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TFAAPFRATI IPPC or:
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
-CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
fa•aL
r
1
�D
�� �5
3�
144s'
C
DO
*q9
q46
)4yF
a6a
y
-
4 pal
"X- axg- -A-c-, cv--opl� krifee Y-.
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @_
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN'
ROTOR
OUT
0.1.
COMPOSITE
SAMPLE
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
I + o 3 -i0
JA .. (p• t DL
1ST WGT.
2ND WGT..
San WGT.
,�,l c -& 96 -
/, 03`7d
RESET#
DISH WGT
WETSAMPLE+
GRAMS
GRAMS
CALCULATIONS:
ALARMS OR COMMENTS —
7/18/18JH
DRIED
GRAMS
1' WGT.
2NO WGT.
3RD WGT.
x 100
'= % TOTAL SOLIDS
PLE + DISH
GRAMS
X 100
= % TOTAL SOLIDS
(DRIED SAMPLE + DISH-- DISH WGT 1 x 100
WET SAMPLE + DISH — DISH SGT. '_ % TOTAL SOLIDS

TWSA DRYER OPERATIONS _
�} DAILY RECORD
DATE
START STOP - TOTAL
RUN TIME, HRS.
1"' DRYER BATCH r A
FILL CYCLE START @_1.�(Q DRY CYCLE STARTED @ %�ao� DISCHARGE CYCLE STARTED @
TEMPERATURES °F
C
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER'
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
�oz),
l �,5
-.31DC
4 fD
39:3
3a9
l)
44 to
4-3
/61
�
q;oa
-V 5
233.
6b
5�!Q
''iD"41
I$1
�113
d- oa
44 6
q4q
41 &
.
a6-1
E�
2ND DRYER BATCH
FILL CYCLE START @ D'J� DRY CYCLE STARTED @ ( ya� DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
l
4 Lf0
-
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ 10 DRY CYCLE STARTED @ 3 l DISCHARGE CYCLE STARTED @_
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN-
ROTOR
OUT
0.1.
�.
172-
s o
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100
Ll NZ
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COMPOSITE
SAMPLE
RESET #
[DISHWGT
GRAMS
WETSAMPLE + DISH
GRAMS
DRIED SAMPLE + DISH
GRAMS GRAMS
6
1�'WGT. 717953
•
2ND WGT.
3RD WGT.
-�/as�v �.(7a33 r X100
I %. % Cf qt:5'-•� !. Q oZ 33 '_ %TOTAL SOLIDS a�6
DISH WGT WET SAMPLE + DI$H DRIED SAMPLE + DISH
GRAMS GRAMS GRAMS GRAMS
1� WGT.
2ND WGT.
CALCULATIONS: 3RD WGT.
X 100
% TOTAL SOLIDS
(DRIED -SAMPLE + DISH.'- DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS
7/18/18JH

TWSA DRYER OPERATIONS _
DAILY RECORD
DATE " 02 1
START STOP TOTAL
RUN TIME, HRS
I" DRYER BATCH . ��
FILL CYCLE START @_ �� . DRY CYCLE STARTED @ � TJ DISCHARGE CYCLE STARTED @ ta ro��
TFMPFRATI IRFC or:
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
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2ND DRYER BATCH 7� j
FILL CYCLE START @ -J DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ 3U
{ TFMPFRATI IRGC RG
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
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OUT
ROTOR
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ J
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
COMPOSITE
SAMPLE
RESET #
CALCULATIOI\
DISH WGT
WET SAMPLE +DISH
DRIED SAMPLE +DISH
GRAMS
• GRAMS
GRAMS GRAMS
I' WGT.
3RD WGT.
/.d3q x100 r� 2
/ S.17:33 % TOTAL SOLIDS /Q
- Sv
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1T WGT. .
2ND WGT.
3RD WGT.
S:
ALARMS OR COMMENTS -
7/18/181H
X 100
'= % TOTAL SOLIDS
(DRIED SAMPLE + DISH-- DISH. WGT.) x 100.
WET SAMPLE + DISH - DISH SGT. , '_ % TOTAL SOLIDS
/

TWSA DRYER OPERATIONS _
DAILY RECORD
C
DATE /0 3—�
START STOP • TOTAL
RUN TIME, HRS -4
'Z
1st DRYER BATCH `�
FILL CYCLE START @ �� DRY CYCLE STARTED @ (P DISCHARGE CYCLE STARTED @ i
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER'
CHANGER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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610
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2ND DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE. CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @_
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
COMPOSITE
SAMPLE
RESET #
:_ DRIED SAMPLE + DISH
DISH WGT
WET SAMPLE + DISH
GRAMS
.GRAMS -
GRAMS GRAMS
2Z."
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.2ND WGT. �-le �.
3RD WGT..
X 100
'=%TOTALSOLIDS 0/
dq-%3
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DRIED SAMPLE + DISH
l� "J
DISH WGT
WET SAMPLE+ DISH
GRAMS
GRAMS
GRAMS GRAMS
_
1' WGT.
,
2ND WGT.
CALCULATIONS: 3 R D WGT.
X 100
'= % TOTAL SOLIDS
(DRIED"SAMPLE + DISH-- DISH WGT.) x 100
WET SAMPLE + DISH.- DISH SGT.: %TOTAL SOLIDS
ALARMS OR COMMENTS -
r
7/18/181H

C
TWSA DRYER OPERATIONS
DAILY RECORD
DATE_ —� -I9
START STOP TOTAL
RUN TIME, HRS : ' / Le ,
1"' DRYER BATCH FILL CYCLE START @ �'�/ /J�
DRY CYCLE STARTED @ o DISCHARGE CYCLE STARTED @10.21
o"Z
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.l.
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2ND DRYER BATCH
d
FILL CYCLE START @ DRY CYCLE STARTED @ 0�7 DISCHARGE CYCLE STARTED @
TFKADPP AT[ IRGC 01:
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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SAMPLE
RESET #
CALCULATION
DISH WGT
GRAMS
WET SAMPLE + D15H
GRAMS
DRIED SAMPLE + DISH
GRAMS GRAMS
1T WGT.
S:
2ND WGT.
3RD WGT.
ALARMS OR COMMENTS -
7/18/18JH
DISH WGT
'.GRAMS
WET SAMPLE + DISH
GRAMS
DRIED SAMPLE + DISH
GRAMS GRAMS
t��
�•3; .�
1'WGT.
2ND WGT.
3RD WGT.
x100 Q
%TOTAL SOLIDS
5!/
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH-- DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
t

l _
�., TWSA DRYER OPERATIONS
DAILY RECORD
t
DATE LD D f L
START STOP TOTAL
RUN TIME, HRS =3 9- (D
1" DRYER BATCH `
FILL CYCLE START @� 'LID DRY CYCLE STARTED @ %� DISCHARGE CYCLE STARTED @ ! D -3,5--
TCIIADCDATI IDCC 01:
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER •
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
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2ND DRYER BATCH
FILL CYCLE START @ li �']Cy DRY CYCLE STARTED @ 1 s 0 DISCHARGE CYCLE STARTED @
TPKAPFRATI IRGC 01:
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANGER
IN'
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH ?
�!LL CYCLE START @ ;L : 6 a DRY CYCLE STARTED @ J � � DISCHARGE CYCLE STARTED @ J
c-
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
_CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
303
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COMPOSITE
SAMPLE
DISH WGT
GRAMS
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GRAMS
DRIED SAMPLE + DISH
GRAMS GRAMS
o
1.�� 1165
1' WGT. 1.7
ND
2 WGT.
3RD WGT.
/• �51q- X100 30 ( '_ % TOTAL SOLIDS (,6-
RESET #
CALCULATION
• 5�
X 100
'= % TOTAL SOLIDS
(DRIED SAMPLE t- DISH•- DISH WGT.) x 100
WET SAMPLE + DISH,- DISH SGT., '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
C : r18/18JH
DISH WGT
GRAMS
WET SAMPLE+ DISH
GRAMS
DRIED SAMPLE + DISH
GRAMS GRAMS
1� WGT.
S:
2ND WGT.
3RD WGT.

T8©
TWSA DRYER OPERATIONS
DAILY RECORD
DATE
START STOP TOTAL
RUN TIME, HRS
15t DRYER BATCH �y l
FILL CYCLE START @ DRY CYCLE STARTED @ a • LI; DISCHARGE CYCLE STARTED
TCIIADCDATI IDCC OE
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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TFMDGRATI IRGC OF:
TIME
DISCHARGE
EXHAUST
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OUT
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! 7/18/18JH -

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @_
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
COMPOSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
WE SAMPLE +•DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS
GRAMS
1
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1' WGT.
2ND WGT.
5lJ
3RD WGT.
0
/ vS
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5,1 41-7 `� 3 ' l 0;� � y , CJ' �73
y
'_ % TOTAL SOLIDS 1 CD
DISH WGT
WET SAMPLE +DISH
DRIED SAMPLE+ DISH
GRAMS
GRAMS
GRAMS GRAMS
1S,r WGT.
2ND WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE *+ DISH'- DISH WGTJ x 100
WETSAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18J H

TWSA DRYER OPERATIONS
�a �! DAILY RECORD J
DATE M
START STOP TOTAL
RUN TIME, HRS
1st DRYER BATCH
' FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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TPRAPFRATI IR'GQ or
TI E
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
'IN
ROTOR
OUT
0.1.
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TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH /
FILL CYCLE START @ DRY CYCLE STARTED @ 3'3 DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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1-70
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RESET #
CALCULATION
WET SAMPLE+ DISH
DRIED SAMPLE+ DISH
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MS
GRAMS
GRAMS GRAMS
1ST WGT..
//
2ND WGT. -
3RD WGT.
fp
-�o�lq 100 Q / 37v
l . 31 ace 1- o !a '= % TOTAL SOLIDS
DISH WGT WET SAMPLE + DISH DRIED SAMPLE + DISH
GRAMS GRAMS' GRAMS GRAMS
.1 Sr WGT.
2ND WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(ORIED'SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

TWSA DRYER OPERATIONS _
DAILY RECORD
DATE
START STOP TOTAL
RUN TIME, HRS
1st DRYER BATCH
FILL CYCLE START @_ 6 -)-7 DRY CYCLE STARTED @7 DISCHARGE CYCLE STARTED @� .
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
1lo6
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2NO DRYER BATCH
FILL CYCLE START @ � DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ -� 3 0
- . TFMPFRATURFS or
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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441
7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH -
FILL CYCLE START @alLJb DRY CYCLE STARTED @ l DISCHARGE CYCLE STARTED @_
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
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SAMPLE
RESET #
CALCU LATI O I\
DISH WGT
WE SAMPLE + DISH
DRIED SAMPLE+ DISH
GRAMS
GRAMS
GRAMS GRAMS
l . v7r�l
lg� $ao3
1STWGT. /g. CJ
2ND WGT.
3RD WGT.
2,163�
16,, 163 y /-8 a o 1 = 17- 08,,3 �0 g
S-- '_%TOTAL SOLIDS 7 O
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS'
GRAMS GRAMS
1ST WGT.
2ND WGT.
3RD WGT.
S:
X 100
%TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 3.00
WET SAMPLE + DISH - DISH SGT. `_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18JH

TWSA DRYER OPERATIONS _
�) DAILY RECORD
DATE
START STOP TOTAL
RUN TIME, HRS r�� �")s
1" DRYER BATCH j
FILL CYCLE START @ • LPL DRY CYCLE STARTED @ o DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
°.5
1 M
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940
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2ND DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ 3- S C DISCHARGE CYCLE STARTED @ 1
1
-, TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
3;56
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7/18/18JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @_
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
COMPOSITE
SAMPLE
RESET #
CALCULATIO I
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS
GRAMS
�JLlL{I
�Z��566
1'WGT.
r�
2ND WGT.
--
3RD WGT.
l bLtLf �^�, X100 f 1107�J�� wj
a.a.2L5-(` o�� O��► a`� '=%TOTAL SO LIDS
DISH WGT
WET SAMPLE+ DISH
DRIED SAMPLE+ DISH
GRAMS
GRAMS'
GRAMS GRAMS
1' WGT.
2ND WGT.
3RD WGT.
S:
X 100
%TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '= % TOTAL SOLIDS
ALARMS OR COMMENTS -
7/18/18J H

�7-3a76
TWSA DRYER OPERATIONS J
• DAILY RECORD
DATE �� �I ))g
START STO P 1 TOTAL
RUN TIME, HRS
15t DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ 9.1 °2 DISCHARGE CYCLE STARTED @ tZ -3 2-
TFMPFRATI IRFS DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
9 : t 2,
fv
A9 to
b
45 2
o
, D 2
3 21
q
h/ 3 1p
LNS-
1 W?
(6 15 Z.
15(0
3q 5
/ oo
LW5
L43q
'L(q
3-7-7
1.6o.
Lfuq
35
LfVY
2c1
tl-i 3 2-1
1 1(9
q 3 3
2-CO
1 q Lf 5
H y 1
S
2 3�?
2ND DRYER'BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TFMPFRATI IRFS DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
C)
2—cl9
0
'III
3717
if//
156
1�kj
3.25
50.
Lf tf 5
Lf
3�
Lfg5
t 4 I
Z�j
a;5
Jto
S47
►oo
,
Lt3
4L+.(
-3
:ql
,
"7
t5o
4illy
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH _
FILL CYCLE START @ 9*66 DRY CYCLE STARTED @ S,Z3 DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
0
LIOlt
(Sti
r
V7
s6
1-[KLI
L7z
sty
-7
lob
kALAh
LA36
COMPOSITE
SAMPLE
RESET #
'CALCULATION
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAGGMS
GRAMS
GRAMS
GRAMS
-7
2ND WGT.
D.
3RD WGT.
b: ? l C7S ,b3v�"' — ��S xioo��3a-b�B 3a.�
a I �-S a1 ,_, (} 35 -� of gl by
'_ %TOTAL SOLIDS [ ��
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST WGT.
2ND WGT.
[;;D WGT,
S:
(DRIED SAMPLE + DISH - DISH WGT.).
WET SAMPLE + DISH - DISH SGT.
ALARMS OR COMMENTS -
12/12/17JH
X 100
% TOTAL SOLIDS
x 100
% TOTAL SOLIDS

TWSA DRYER OPERATIONS
DAILY RECORD
DATE
C
START STOP TOTAL
RUN TIME, HRS
15t DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ .US DISCHARGE CYCLE STARTED @ t 1 Z J
TEMPERATURES °F
c
r J
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
2-S
p
3913.
37 5
39 D,
156
55
k (opt
31 q
5o
y L4
Lf Z'g.
Lf (39
a ; 4 5
ILO 5
3 3 `f
[;Do
N qq
Lf 3�
(f14Lf
-ZZZ
2'5
t i� 1
l (
��
�
2ND DRYER*BATCH
FILL CYCLE START @ (� 35 DRY CYCLE STARTED @ ��'.' �� DISCHARGE CYCLE STARTED @
TFMPFRATl1RES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
50.
E-(q-7
Lf 35
gL(5
1-7-7
z: o
- 6
33
5c)
qq5
435
u2c\
200
\A'-� t
ATA
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ 3'qo DRY CYCLE STARTED @ a (5 DISCHARGE CYCLE STARTED @
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
anS
2,
5a
�11
Lfz6
15-7
tc,
�N
�`l
Mc:;,
413
'AKl
COMPOSITE
SAMPLE
RESET #
CALCU LATI O I\
DISH WGT
WET SAMPLE +DISH
DRIED SAMPLE+.DISH
GRAMS
GRAMS
GRAMS GRAMS
► (J2
6-6� t37'
1ST WGT. 7,7 15
2ND WGT. 7►
3R° WGT.
> 1-7, 7 19 1
q a-1 �,737.7% gpI
X100 (/TOTAL SOLIDS a "'D
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
IST WGT.
2ND WGT.
PD7W�GT����
S:
X 100
%TOTAL SOLIDS
(DRIED SAMPLE + DISH -'DISH WGT.) x 100
WET SAMPLE + DISH ' DISH SGT.' '_ %TOTAL SOLIDS
ALARMS OR COMMENTS -
12/12/17J H

TWSA DRYER OPERATIONS
DAILY RECORD
DATE Z j —f — [
START STO P TOTAL
RUN TIME, HRS l4 =� - / �q Ost
1 DRYER, BATCH
FILL CYCLE START DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @[
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER'
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
J
f
g
%
! g
�l
E'
.:393
!V,3asa
.
a3
o�
q4 4
D
4qb
2ND DRYER BATCH
r l �
a
FILL CYCLE START @ ���J DRY CYCLE STARTED @ b DISCHARGE CYCLE STARTED @ d� `•
TFMPFRATIIRFS °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
.0.1.
ff
F a •3t7
�► `]
30`7
0
1
13
j s5
3
� a
SO4i4l
q3 7
443
l 95-
C16
)"lo
Ilo
do
4'-� 9
C-Lol
a: D
/4'
38q
1-0
4
J-13s
E
-5
17 to
Al at!�Q—.66,..
' xf4
�
c
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
C',
RD DRYER BATCH
FILL CYCLE START @ amw DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ ;"56
TFMPFRATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
;35
��-7
cl7
y
'A;
%l5
16(7
3K2
!Da
�Nz
`f -b7
Ll 3L
`/ti
�y�l
Zza
�5ti
-75
Lv42-
NL
L(3
Z37
-zr(/
COMPOSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
WET -SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST WGT. 1
2ND WGT.
3RD WGT.
J°laD ' i,���33?7 x1o0 o9�g55asJ
a53 — ! 0 � `t) = Yj f346-3 '= %TOTALSOLIDS
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST WGT.
2ND WGT.
3RD WGT.
S:
(DRIED SAMPLE + DISW -'DISH WGT.
WET SAMPLE + DJSHti DISH SGT.
ALARMS OR COMMENTS -
X 100
'= % TOTAL SOLIDS
x 100 I
'= % TOTALS 0 LIDS
12/12/17JH

3 Z
TWSA DRYER OPERATIONS
DAILY RECORD
DATE
J
,
-'
START
STOP
TOTAL
RUN TIME, HRS
15C DRYER BATCH
FILL CYCLE START @ DRY CYCLE
STARTED @: DISCHARGE CYCLE STARTED @
TEMPERATURES °F
s.
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHA(VBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
316
5v
3� ..�36
a
qg
yes
a�
e
) b 6
37 g
Is"6
-414
�� s
2N0 DRYER BATCH
FILL CYCLE START @ /b Jr [ DRY CYCLE STARTED @ a` DISCHARGE CYCLE STARTED @ a-
Y
1
- Q
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
40
46 .
141
v'
00
14 V
q38
211(6
�2 3,el
CO
4:0
4ys
)43
4��s
as
- 12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ ` ' G DRY CYCLE STARTED @ ' 3 ° DISCHARGE CYCLE STARTED @
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
3,n
1�C
rJ-rG 1
V
vV ,qDk
U5/
2 Zc,�
n
�62
� T
Ls
4'i i G
I gs
K35
1 '133
1
COMPOSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
WET -SAMPLE +DISH
DRIED-SAMPLE+DISH-
GRAMS
. GRAMS
GRAMS GRAMS
rr
1TWGT. 15i�
-
2ND WGT. L /0 l9 �o
3RD WGT.
.
Is�3%5'.
15,30163 ~/,o51y= 1�f,3y5'I x100 `/3 r
I b-7463 !- o 15>-71 Vt '_%TOTALSOLIDS
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
17 WGT.
2ND WGT.
3RD WGT.
S.
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.1 x 100 .
WET SAMPLE + DISH - DISH SGT. % TOTAL SOLIDS
ALARMS OR COMMENTS -
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
' DATE
START STOP TOTAL
RUN TIME, HRS
1sc DRYER BATCH
FILL CYCLE START @ `� DRY CYCLE STARTED @ -7•y DISCHARGE CYCLE STARTED @
TFMPFRATllRFS °Fl
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
. TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN.
ROTOR
OUT
0.1.
7-°b o(
3 7 5
393
•113
C
-7: 99
-`b 19
38'
14A5
)64
00
B- : l
l C5'le
33 7
/001
44
q 39
44 (o
.221
eb
l
!
j6�
�
cZaY
c,r7
2ND DRYER BATCH,
FILL CYCLE START@ d- DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES °F
a
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
Los
aR7
o
13
©®
13
1,5e
2: b'6
a a
a
• 14As
)-137
C76
jam`7
3 33
J b©
4 4is'
�, :�
ga
a
�,©o
►
;i4
L
12/12/17JH

r
TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ ' 149 DRY CYCLE STARTED @ ���� DISCHARGE CYCLE STARTED @ 3%
TEMPERATURES °F L
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN .�
ROTOR
OUT
0.1.
Lim
c6,0
A-b7
`(KS
ICI
—J1A
41'14-
T-3og
'-1 >n3
2 2
�T(j-
b'. • A
W'q W
4-65
tiii13
Z 1-7
TH
.6%sod
\ n
-tqb
2�7
1 -,s-H
COMPOSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
WET -SAMPLE + DISH
DRIED -SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1'WGT. %J' ��10 ".
2ND WGT. %S� 9 n 7.
3RD WGT. _
.
����lo0�
xsoo
27, SL53 y_ ��0137 l�c� ba— '=%TOTALSOLIDS
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1' WGT.
2ND WGT.
3RD WGT.
S:
x 100
'= % TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ %TOTAL SOLIDS
ALARMS OR COMMENTS -
.j.
12/12/17JH

q-5'�li%
TWSA DRYER OPERATIONS
DAILY RECORD
DATE ! -7 j 9
i
START STOP TOTAL
RUN TIME, HRS
1st DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @" �a �� DISCHARGE CYCLE STARTED @ Z V
TEMPERATURES °F
A
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
. TIMER
CHANBER
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
�Q
U
(IINc�
� l /
7.9
!
j
1 t
J&
6-0
a a
-
03
D.
415
2ND DRYER•BATCH
FILL CYCLE START @C) " DRY CYCLE STARTED @ `t
J DISCHARGE CYCLE STARTED @ 'U`l
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
iL4
3'.5-7
I (Q -5
31 (p
!�;'o
gVLI
q,3`7
L(Lf 3
190
3i3
H a
1 5
?'
`fL13
L-r 3Z
q L4 z
23 7,-
7 cJ
� ` l
165
3a
1�0"
"" � �
4.35
cf q q
- zZ
� �
(; o`�
r C�
( 3
�00
4q�
q40
4�
Z3_ 3
:5 ,
_ter
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @. DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
COMPOSITE
SAMPLE -
RESET #
CALCULATIOI\
DISH WGT
WET•SAMPLE + DISH
DRIED•SAMPLE + DISH -
GRAMS
GRAMS
GRAMS GRAMS
1'WGT. (i
. "
2ND WGT. �<
3RD WGT. -
3(19- xloo g3�355
a(Qr �/y,j �� �!%0�� = aJrt•55'_a j '_%TOTAL SOLIDS �3, �7�a
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE +DISH
GRAMS
GRAMS
GRAMS GRAMS
1�T WGT.
2No WGT.
3Ro WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH'- DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
12/12/17JH

qgJ&
TWSA DRYER OPERATIONS
DAILY RECORD
DATE _ // —
' START STOP TOTAL
RUN TIME, HRS :.� / / o
1st DRYER BATCH
FILL CYCLE START @ ' —f DRY CYCLE STARTED @- 7 . DISCHARGE CYCLE STARTED @
TFMPFRATI IRFS OF
1
�C
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
7•.-a3
1501
913
163-
S36
2ND DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ e • Jr3
TFMPFRATI IRFS OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
-36L7
6
4 b q
3 F if
4 b 4
163
E` 10
43a
16
ev
= l3
/3 a
'2Lf t)
• • Da
;2a3
9'°
/ l d, I
115D
LA4-
l P
aD�
at) 6
)44s
r4qb
-445
a3b 16701
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
" DRYER BATCH i _
FILL CYCLE START @3`�.3 DRY CYCLE STARTED @ ` Q DISCHARGE CYCLE STARTED @
TEMPERATURES 0F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
3g�
�o
�s-�5
149
N 1. �)15
b 6
Z
D
'13-7
q s5
to
w3�
[
o a
�[ �(�
q q z
TAD
�I`'13.
-2-2L
;Y
COMPOSITE
SAMPLE
RESET #
CALCULATIOI\
DISH WGT
WET•SAMPLE + DISH
DRIED•SAMPLE + DISH
GRAMS
GRAMS
GRAMS
�l)Z7�
I`
`b,bU 5.
r ClGRAMS
1'TWGT.
'
2ND WGT. �cCJ i J
3RD WGT.
C
--1 6 a`] �=' 1 3 $ l °I x 1o0
U9
q 1 � / t '= % TOTAL SOLIDS � (pbcs'-- ), D e?S 15 7
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1T WGT.
2ND WGT.
3RD WGT.
S.
X 100
% TOTAL SOLIDS -_
(DRIED SAMPLE + DISH -DISH WGT.) x 100'
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
c-
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
DATE
START STOP TOTAL
RUN TIME, HRS
1s' DRYER BATCH
FILL CYCLE START @CD DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @%
TFMPFRAT[JRFS OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
• IN
CHAMBER,
OUT
ROTOR
IN
ROTOR
OUT
0.1.
3�
d •
3qS
3-7\5
395
eA
2: b 6
4Lf 7
4f3e
8-fdo
gq3
`�3 �i
;4/
2ND DRYER BATCH
FILL CYCLE START @ �Q�-� DRY CYCLE STARTED @ �� DISCHARGE CYCLE STARTED @ ' "1
TEMPERATURES °F
TIME -
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
I��o
It�3
a9�f
-q0
3q f>
4
a
E-0
a: D
I to
4qi?
#ffT
1
4!�1
6 a
z
333
. /oo
45
4,310,
4J1-,.5-
c29s
CO
3 gq
150
0
1
aa,
O-ob
3
1
4145
r,-23
F
C,
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ 'J© DRY CYCLE STARTED @ 3 'ZS DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
_ 0.1.
o
L i5
-�
3Zt
56
11g3
-5-7
L[c-[ (
1 db
trH
5
16l
- b
LN-3
210
�r1
5, cj5
kG
0
0
.4
1
1I110
COMPOSITE
SAMPLE
RESET #
CALCULATIOf
DISH WGT
WET•SAMPLE + DISH
DRIED -SAMPLE + DISH
GRAMS
GRAMS
GRAMS
GRAMS
[-0352.
17WGT.,
L .
-
-
2ND WGT:
3RD WGT.
X10o • �3���5 �'3
'= %TOTAL SOLIDS
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1T WGT.
2ND WGT..
13RD WGT.
S:
X 100
%TOTAL SOLIDS
(DRIED SAMPLE + DISH — DISH WGT.1 x 100
WET SAMPLE + DISH — DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS —
•s•
12/12/17JH

13
�i TWSA DRYER OPERATIONS
DAILY RECORD
DATE
START STOP TOTAL
RUN TIME, HRS ' % ; / J
` . 15' DRYER BATCH y / j
{ FILL CYCLE START @ / ' DRY CYCLE STARTED @ 8' •�� DISCHARGE CYCLE STARTED @
TEMPERATURES °F
C.
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
da
1�a
�g�
39
3-7113-
�
9•• ► `7lb
3 0S
, S a
qa 2-
411
)4aa, •
l5g
elo
-S3
) 6 0
41
q3 8
• - 4 qt5
1U7
134
144
23 d
C0
1 2ND DRYER•BATCH /
FILL CYCLE START @ Ia' b� DRY CYCLE STARTED @ 1 �37 DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
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12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
t
COMPOSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
WET -SAMPLE + DISH
DRIED -SAMPLE + DISH
GRAMS
GRAMS
GRAMS
l i a C6v
q
lS 3�.�J
p gGRAMS
1sTWGT.
-
-
2ND WGT. , q 3
3RD WGT.
ya& / �.913/ X100
! S-of -3 U V 9,16 c- I (G ot3 '=%TOTALSOLIDS��U
DISH WGT
GRAMS
WET SAMPLE + DISH
GRAMS
DRIED SAMPLE + DISH
GRAMS GRAMS
1' WGT.
S.
2ND WGT.
13RD WGT.
ALARMS OR COMMENTS -
12/12/17JH
c
X 100
% TOTAL SOLIDS ,
(DRIED SAMPLE + DISH - DISH WGTJ x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS

TWSA DRYER OPERATIONS
DAILY RECORD
DATE
START STOP TOTAL
RUN TIME, HRS
1s' DRYER BATCH
FILL CYCLE START @ �'� DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES °F
t.
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER.
• IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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411
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FILL CYCLE START @ �s �'� DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ v2 • +t
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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41
L41 6
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH .
FILL CYCLE START @ '� DRY CYCLE STARTED @ , '� b DISCHARGE CYCLE STARTED @,_
TEMPERATURES °F t.
DISCHARGE
DISCHARGE
DRY
CHANBER
CHAMBER.
ROTOR
ROTOR
TIME
EXHAUST
PRODUCT
TIMER
IN
OUT
IN
OUT
0.1.
9
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t1i
COMPOSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
WET -SAMPLE + DISH
DRIED -SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
(�0
moot:),
1'WGT. I �
2ND WGT.
3RD WGT. -
-
j�12 (,y"1DO _x100 = ERG �p� ►y �
0 7 UU '= % TOTAL SOLIDS
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1�T WGT.
2NO WGT.
3RD WGT.
S:
X 100
%TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGTJ x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
12/12/17JH

TWSA DRYER OPERATIONS i
DAILY RECORD a
DATE
START STOP TOTAL
RUN TIME, HRS
P DRYER BATCH
FILL CYCLE START @(0:3 DRY CYCLE STARTED DISCHARGE CYCLE STARTED @ �� • 33
TFMPFRATURFS DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
------------
0.1.
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FILL CYCLE START @3 DRY CYCLE STARTED @_ DISCHARGE CYCLE STARTED @
TFMPFRATLIRFS DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
C)DRYER BATCH j�
FILL CYCLE START @ �' 47 DRY CYCLE STARTED @ �z3 DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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SAMPLE
C.
RESET #
CALCULATION
DISH WGT
WET SAMPLE + DISH
DRIED -SAMPLE + DISH
GRAMS
' GRAMS
GRAMS
GRAMS
11o$��
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l6, 2
1'WGT.
. a
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.
2ND WGT.
DD
3RD WGT.
A5�i �
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DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1T WGT.
2ND WGT.
13RD WGT.
S.
X 100
'= % TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT. L x 100 .
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
DATE /r' ! " o`LJ " j -I
START STOP TOTAL
RUN TIME, HRS ' • 31
1S' DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @_
TFMPFRATURFS OF
C
2ND DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ I i JY DISCHARGE CYCLE STARTED @ : 675
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
►s`1
33b
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43
TIME
DISCHARGE
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DISCHARGE
PRODUCT
DRY
TIMER
CHANBER�
IN
CHAMBER
OUT
ROTOR
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O.I.
333
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12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
'I lj
FILL CYCLE START @. ;v S. DRY CYCLE STARTED @' DISCHARGE CYCLE STARTED @ '
TEMPERATURES. F '
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
,3;q
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302
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384
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COMPOSITE
SAMPLE
RESET #
DISH WGT
GRAMS
WET•SAMPLE + DISH
GRAMS
DRIED -SAMPLE + DISH -
GRAMS GRAMS
o-7 -7 5
z 5 , 0 3_�A
1ST WGT. 61a , ,9 . .
.
�
2ND WGTX r l(G.
3RD WGT.
X100
GJ p� c/ , c> 1 •� a 3 -1
% TOTAL SOLIDS
CALCULATION
ALARMS OR COMMENTS -
'S•
DISH WGT
WET SAMPLE +DISH
DRIED SAMPLE +DISH
GRAMS
GRAMS
GRAMS GRAMS
1ST WGT.
2ND WGT.
3RD WGT.
S.
X 100
%TOTAL SOLIDS
!DRIED SAMPLE + DISH - DISH WGT. 1 x 100
WET SAMPLE + DISH -DISH SGT. '_ % TOTAL SOLIDS
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
DATE
START II STOP TOTAL
RUN TIME, HRS
P DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TFMPFRATURFS OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
• IN
. CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
3 $l
3&(e
3
-_.q 5 D
3
3 `7
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2ND DRYER .BATCH FILL CYCLE START @ 6 DRY CYCLE STARTED @ A 1 DISCHARGE CYCLE STARTED @ vZ S
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER"
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
t
I a,
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PO
164
331
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33
ly-ly�p
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413
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158
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'iUA2/17JH
r

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @,3 • DRY CYCLE STARTED @ •' DISCHARGE CYCLE STARTED @
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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159
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COMPOSITE
SAMPLE
41 1
DISH WGT
WET -SAMPLE + DISH
DRIER•SAMPLE + DISH
GRAMS--- -
- GRAMS
GRAMS GRAMS
zff (g
//
1� WGT. 13, -
/i ©b -77
S2
2ND WGT-
3AD WGT. -
r"
X 100
%TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
12/12/17JH
3. 7 ' X 100
} 5, Acl 0-9 G 6 7 7 .::- N, 1 •i 3 ( % TOTAL SOLIDS
RESET # . G G
CALCULATION
DISH WGT
GRAMS
WET SAMPLE + DISH
GRAMS
DRIED SAMPLE + DISH
GRAMS GRAMS
1�T WGT.
S:
2ND WGT.
3aD WGT.

TWSA DRYER OPERATIONS
DAILY RECORD
DATE < l -oZ r-7 `l
START STOP TOTAL
RUN TIME, HRS ' - / •• 3 / al
15' DRYER BATCH -
- FILL CYCLE START @ G. 3 DRY CYCLE STARTED @ ' b 'DISCHARGE CYCLE STARTED
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
- IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
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63
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2ND DRYER BATCH
FILL CYCLE START @ 'Z DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ t
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANGER'
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
I I 3 Z�
FILL CYCLE START @ � � `I � DRY CYCLE STARTED @ ' DISCHARGE CYCLE STARTED @
TEMPERATURES °F `'
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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l ��
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COMPOSITE
SAMPLE
RESET #
DISH WGT
GRAMS
WET•SAMPLE+DISH
GRAMS
DRIED•SAMPLE+DISH-
GRAMS GRAMS
.Z.`t,s(pL 0
1STWGT. a�31e�
.
2"D WGT. aS, 3 0S
3RD WGT.
X 100 3
3,9 G ol� .56D2- - /oTOTAL SOLIDS
S:
3RD WGT.
CALCULATION
x 100
% TOTAL SOLIDS
(DRIED SAMPLE+ DISH - DISH WGT.,). x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
DATE
START STOP TOTAL
RUN TIME, HRS
1st DRYER BATCH
FILL CYCLE START @ ( • V DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ %S
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
• IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
3$ a-
3 a
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C'
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#39
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4b
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2NO DRYER'BATCH
FILL CYCLE START @ O DRY CYCLE STARTED @ J4b DISCHARGE CYCLE STARTED 03
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT.
DRY
TIMER
CHANBER'
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
326-
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1 Sq "
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12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ 3 I d DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @ V
TEMPERATURES °F '
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
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COMPOSITE
SAMPLE
RESET #
DISH WGT WET -SAMPLE +DISH DRIED-SAMPLE+DISH-
GRAMS GRAMS GRAMS GRAMS
Do 5 1'` WGT.
ZND WGT. l/
. 3RD WGT.
x10o
l !7c)©S: /_ 05�;O. 194ya '=%TOTAL SOLIDS �(p
x10o
l !7c)©S: /_ 05�;O. 194ya '=%TOTAL SOLIDS �(p
S:
CALCULATION
• x 100
%TOTAL SOLIDS
(DRIED SAMPLE + DISH -.DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '= % TOTAL SOLIDS
ALARMS OR COMMENTS -
12/12/17JH

CA
1
TWSA DRYER OPERATIONS
DAILY RECORD
DATE Id- -3 '-
START
STOP TOTAL
RUN TIME, HRS '
v
Ll ; L15 / ® -3
P DRYER BATCH
FILL CYCLE START @ l0 ' DRY CYCLE STARTED @ %� DISCHARGE CYCLE STARTED
--
TEMPERATURES °F
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
71MER
CHANBER
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
•
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3
C
30
g `5©
l (o
3.�
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4
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C2/8
C
— go4b
15
3 � -7
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2ND DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ L , 6 DISCHARGE CYCLE STARTED @
TEMPERATURES OF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER'
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
O.I.
j a d
b 4
J9,10
367
9�
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3
q3 a
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15CQ
;3a(
-16-0
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41+
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150
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12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES °F
.TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
�a
•
eo
b
COMPOSITE
SAMPLE
DISH WGT
WET -SAMPLE +DISH
DRIED•SAMPLE+DISH-
GRAMS
GRAMS
GRAMS .� GRAMS
1,0716
1-1 Acl l�.
1�T WGT.. /
2ND WGT.
3RD WGT.
1`7. gcl629`l,U�/� '=%TOTALSOLIDS��Z d
RESET #
CALCULATION
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
IsT WGT.
2ND WGT.
3RD WGT.
S:
• X 100
%TOTAL SOLIDS
jDRIED'SAMPLE + DISH - DISH WGT.1 x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
DATE /01 _ -/ - j g
START STOP TOTAL
RUN TIME, HRS
1sc DRYER BATCH
FILL CYCLE START @ '?4, 33 DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
• IN
CHAMBER
OUT
ROTOR
114
ROTOR
OUT
0.1.
q. (Dg
)100
n •
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3•�a
J13
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°I=,Sg
01
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108
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q3`7
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1�50
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4J.41 !r
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46 3
o,205
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10 6
2ND DRYER'BATCH Q
FILL CYCLE START @. �a . DRY CYCLE STARTED @' E I o DISCHARGE CYCLE STARTED @
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER•
IN
CHAMBER
OUT
ROTOR
IN
ROTOR
OUT
0.1.
I c.
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3? 7.
464
1
360
a
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12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3RD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @_
TEMPERATURES DF
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
COMPOSITE
SAMPLE
RESET #
CALCULATION
DISH WGT
GRAMS
WET -SAMPLE + DISH
GRAMS
DRIED -SAMPLE + DISH
GRAMS .
Q-Mt
`�5�
nnGRAMS
1sTWGT. �, .77
_
.
2ND WGT- �5 O_
3RD WGT. ~
�s
r �s_V a l I �r7�10r� % TOTAL SOLIDS ���
o�
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1�T WGT.
2NO WGT.
3RD WGT.
S:
X 100
% TOTAL SOLIDS
(DRIED SAMPLE + DISH - DISH WGTJ x 100
WET SAMPLE + DISH - DISH SGT. '_ % TOTAL SOLIDS
ALARMS OR COMMENTS -
12/12/17JH
C�

TWSA DRYER OPERATIONS
DAILY RECORD
DATE
START STOP TOTAL
RUN TIME, HRS ' .� / I • oZ / u
P DRYER BATCH
FILL CYCLE START @-2jj_ DRY CYCLE STARTED @ °° DISCHARGE CYCLE STARTED @ • j
TFMPFRATURFS OF
C.
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHAMBER
• IN
CHAMBER
OUT
ROTOR,
IN
ROTOR
OUT
0.1.
S- fflg
b
9.33
b
3q L.
J)
3R rI
4pt)
-
D:aS:/,5#
Z3 ag
Liv 6a�
11=15
G
3
l e
14 q5
q,, o
144
aa5
C
2 ND DRYER*BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED .@
TEMPERATURES °F
DISCHARGE
EXHAUST
--CHANBER-
i - 0-ij]
12/12/17JH

TWSA DRYER OPERATIONS
DAILY RECORD
3FtD DRYER BATCH
FILL CYCLE START @ DRY CYCLE STARTED @ DISCHARGE CYCLE STARTED @
TEMPERATURES °F '
TIME
DISCHARGE
EXHAUST
DISCHARGE
PRODUCT
DRY
TIMER
CHANBER
IN
CHAMBER.
OUT
ROTOR
IN
ROTOR
OUT
0.1.
COMPOSITE
SAMPLE
RESET #
CALCULATION
ALARMS OR COMMENTS
12/12/17JH .
DISH WGT
WET -SAMPLE +DISH
DRIED•SAMPLE+DISIj-
GRAMS
GRAMS
GRAMS GRAMS
15TWGT.
.
2ND WGT..
3RD WGT. -
61-3 1a,83aLxioo
�_ % TOTAL SOLIDS l6
DISH WGT
WET SAMPLE + DISH
DRIED SAMPLE + DISH
GRAMS
GRAMS
GRAMS GRAMS
1T WGT.
2ND WGT.
3RD WGT.
S:
X 100
'_. %TOTAL SOLIDS _
(DRIED SAMPLE + DISH - DISH WGT.) x 100
WET SAMPLE + DISH - DISH SGT. '= % TOTAL SOLIDS

0
(f)
Annual Belt Press
Record

TWSA Annual Residual
Operation Totals
2019
Sludge Hauled
to Landfill or Farm
SLUDGE FEED
Polymer Usage
Press
Run Time
Dryer Run Time
avg
% Solids
Total
Gallons
Total
D Ton
avg Ibs/
1000 al
Total
$/month
days
Hrs
Total
$/month
XXXX
avg
% Solids
Days
Loads
Hrs
Total
$/month
avg
% Solids
Total
Ton
Tipping
Fee
Hauling
Fee
DATE
Jan.
2.37
343,483
34.16
2.64
XXXX
9
99.2
17.6
9
26
108.1
XXXX
95.8
47.1
XXXX
XXXX
Feb.
2.24
407,945
38.12
1.80
XXXX
11
118.4
XXXX
17.3
11
32
130.5
XXXX
94.9
22.9
XXXX
XXXX
Mar.
2.21
460,356
42.29
2.15
XXXX
12
131.8
XXXX
17.1
12
36
147
XXXX
95.3
22.4
XXXX
XXXX
Apr.
2.13
460,940
40.83
2.21
XXXX
11
133.2
XXXX
17.9
11
32
130.8
XXXX
96.4
45.4
XXXX
XXXX
May
1.70
92,933
6.56
1.06
XXXX
2
22.9
XXXX
19.4
2
6
25.5
XXXX
96.1
0.0
XXXX
XXXX
Jun.
1.48
3,545
0.22
1.83
XXXX
1
1.0
XXXX
22.1
1
1
3.5
XXXX
98.4
48.0
XXXX
XXXX
Jul.
No Press
unin-July
XXXX
XXXX
No Dryer run in Jul
XXXX
0.0
XXXX
XXXX
Aug.
2.29
279,362
27.68
3.28
XXXX
7
72.5
XXXX
18.2
6
14
67.1
XXXX
97.3
0.0
XXXX
XXXX
Sep.
2.84
144,719
16.62
4.89
XXXX
6
51.9
XXXX
18.2
7
17
67.8
1 XXXX
97.5
5.0
XXXX
XXXX
Oct.
2.60
313,285
33.54
3.97
XXXX
9
98.1
XXXX
18.9
10
26
109
XXXX
96.9
23.8
XXXX
XXXX
Nov.
2.37
509,473
50.14
2.79
XXXX
13
152.5
XXXX
18.3
13
37
152.3
XXXX
92.4
23.60
1 XXXX
XXXX
Dec.
2.18
447,900
40.23
2.86
XXXX
13
135.4
XXXX
17.7
4
9
36.3
XXXX
93.7
210.40
XXXX
XXXX
Monthly
avg.
2.22
314,904
30.04
2.68
9
92.4
18.4
8
21
88.9
95.9
37.4
ytd total 3,463,941 330.39 1 1 94 1,016.9 $0 1 1 86 1 236 1 977.9 $ - 448.55
# of days press was run: 94 # of hours press was ran: 1016.9 # of days dryer was run: 86
Avg. # of hours press was run/day: 10.8 Estimated Annual wet ton of dewatered sludge produced: 1,792.9
Estimated annual tons Estimated tons of Class A
of Class A Residual produced: 344.5 Residual distributed to the public: 53.0
Total # of hours dryer was ran: 977.9
Avg. # of hours
dryer was run/day: 11.4