NCS000315_MONITORING INFO_20181115

MIJ70
STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
L 0 D° 316
' v
DOC TYPE
❑ HISTORICAL FILE
MONITORING REPORTS
DOC DATE
u / D I
❑
YYYYMMDD

neAveo
sotutions
November 13, 2018
Division of Energy, Mineral and Land Resources
Stormwater Permitting Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612
Re: Semi -Annual Storm Water Sampling Results for Year 9, Period 2
Nexco Solutions, LLC
3930 Glenwood Avenue
Charlotte, Mecklenburg County, North Carolina
EPA ID 4NCD 061 263 315
To Whom It May Concern:
3 Waterway Square Place
Suite 1000 ,
The Woodlands, TX 77380
Nov 10 2513
OFNR-LAND QUALITY
STQRMWATER PERMITTING
Nexeo Solutions, LLC (Nexeo) conducted the semi-annual analytical monitoring event for Year 9, Period 2 at the
Nexeo facility located at 3930 Glenwood Drive in Charlotte, Mecklenburg County, North Carolina, on October 26,
2018, as prescribed in the National Pollutant Discharge Elimination System (NPDES) permit (NCS000315). Per
the requirements, the storm water sample was collected from the storm water discharge outfall (SDO) 001 during a
representative storm event that consisted of 2.04 inches of total rainfall, as measured by the local United States
Geological Survey (USGS) rain gage (number 351412080541245 CRN-53 at I -larding High School, Charlotte,
North Carolina). More than 72 hours of 0.00 inches of rainfall occurred prior to the sampling.
During the sampling event, a visual inspection for qualitative monitoring was conducted as specified in Table 4 of
the NPDES permit. No atypical conditions were noted during the field inspection. In accordance with Section C. of
the permit, in the event that an atypical condition is noted at a stormwater discharge outfall, the permittee shall
document the suspected cause of the condition and any actions taken in response to the discovery in the Stormwater
Pollution Prevention Plan (SPPP). The inspection results are presented in Table I.
Table 1
Discharge Characteristic
Inspection Result
Color
Clear
Odor
None identified
Clarity
Clear
Floating Solids
None identified
Suspended Solids
None identified
Foam
None identified
Oil Sheen
None identified
Erosion/Deposition at the Outfall
None identified
Other Obvious Indicators of Stormwater Pollution
None identified
The sample was collected in laboratory -supplied bottles, preserved with ice, and transported with a trip blank to the
Test America, Inc, laboratory in Savannah, Georgia. The sample was then analyzed for total suspended solids, oil
NexeoSolutiorts.com I Connect.

neAveo®
solutions
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
and grease, chemical oxygen demand, toluene, total xylenes, and pH. None of the results exceeded its corresponding
benchmarks.
All of the results of the storm water sample analyses along with their corresponding benchmark values as listed in
the permit are presented below in Table 2, and the laboratory results are included as Enclosure 1.
Table 2
Discharge Characteristic
Result
Benchmark Value
Total Suspended Solids
59 milligrams/liter (mg/L)
100 mg/1-
Oil and Grease
<2.7 mg/L
30 mg/L
Chemical Oxygen Demand
29 mg/L
120 mg/L
Toluene
<0.001 mg/L
0.055 mg/L
Xylenes, Total
<0.002 mg/L
6.7 mg/L
pFl
R.17 (field reported) / 7.0 (lab reported)
6-9
Total Rainfall
2.04 inches
Required to be> 0.1 inches
Nexeo will continue semi-annual monitoring under the expired permit NCS000315 until the new permit is issued.
We will conduct the next monitoring event (Year 10, Period 1) between January I and June 30, 2019, and will
submit the results per the requirements of the permit. Should you have any questions or require additional
information, please contact me at 704-391-6877.
Sincerely,
Nexeo Solutions, LLC
Timothy Nightwine
Facility Manager
cc: Chris Byerman, Nexeo Solutions, LLC
NexeoSolutions.com i Connect.

TestAmenca
■ THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel:[phone]
TestAmerica Job ID: 680-159860-1
Client Project/Site: NexeoSolutions - Charlotte
For:
EHS Support, LLC
100 Georgia Ave
Daphne, Alabama 36526
Attn: Amy Bauer
Authorized for release by:
11/7/2018 5:57:11 PM
Jerry Lanier, Project Manager I
[phone]
[e-mail]
��ff:Nv D
....... LINKS ':...... .....
, pENRLANppERMt�tNp
iReview your project SjpRMWATER
iresults through
i
totadAccess,
Have a Question?
Ask
i Th e The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
i, parameters, exceptions are noted in this report. This report may not be reproduced except in full,
Ex p Q and with written approval from the laboratory. For questions please contact the Project Manager
Qat the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
��/ISit'US at:
www.testarneticainc.cnm Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: EHS Support, LLC
Project/Site: NexeoSolutions - Charlotte
TestAmerica Job ID: 680-159860-1
Table of Contents
CoverPage ..............................................
1
Table of Contents .........................................
2
Case Narrative ...........................................
3
Sample Summary .........................................
5
Method Summary ...........................................
6
Definitions/Glossary .......................................
7
Detection Summary ........................................
8
Client Sample Results ......................................
9
Surrogate Summary .......................................
10
QC Sample Results ........................................
11
QC Association Summary ...................................
14
Lab Chronicle ............................................
15
Chain of Custody ..........................................
16
Receipt Checklists .........................................
17
Certification Summary ......................................
18
Page 2 of 18
TeslAnnerica Savannah
11 /7/2018

Case Narrative
Client: EHS Support, LLC
Project/Site: NexeoSolutions - Charlotte
Job ID: 680-159860-1
Laboratory: TestAmerica Savannah
Narrative
CASE NARRATIVE
Client: EHS Support, LLC
Project: NexeoSolutions - Charlotte
Report Number: 680-159860-1
TestAmerica Job ID: 680-159860-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
'RECEIPT
The samples were received on 10/27/2018; the samples arrived in good condition, properly preserved and on ice. The temperature of the
,coolers at receipt was 2.9 C.
VOLATILE ORGANIC COMPOUNDS (GC -MS)
Samples OUTFALL 001 (680-159860-1) and TRIP BLANK (680-159860-2) were analyzed for Volatile Organic Compounds (GC -MS) in
accordance with EPA Method 624. The samples were analyzed on 11/05/2018.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with analytical batch
680-546278.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
OIL AND GREASE AND TPH
Sample OUTFALL 001 (680-159860-1) was analyzed for Oil and Grease and TPH in accordance with EPA Method 1664A. The samples
were prepared and analyzed on 11/01/2018.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated
with preparation batch 680-545810.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample OUTFALL 001 (680-159860-1) was analyzed for total suspended solids in accordance with SM 2540D. The samples were
analyzed on 11/01/2018.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CHEMICAL OXYGEN DEMAND
Sample OUTFALL 001 (680-159860-1) was analyzed for chemical oxygen demand in accordance with SM 5220D. The samples were
analyzed on 11101/2018.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVITY (PH)
Sample OUTFALL 001 (680-159860-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The samples were analyzed
TestAmerica Savannah
Page 3 of 18 11/7/2018

Case Narrative
Client: EHS Support, LLC
Project/Site: NexeoSolutions - Charlotte
Job ID: 680-159860-1 (Continued)
Laboratory: TestAmerica Savannah (Continued)
on 10/3012018.
TestAmerica Job ID: 680-159860-1
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This sample(s) was performed in
the laboratory outside the 15 minute timeframe.
'1 No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica Savannah
Page 4 of 18 11/7/2018

Client: EHS Support, LLC
Project/Site: NexeoSolutions - Charlotte
Lab Sample ID
680-159860-1
680-159860-2
Client Sample ID
OUTFALL 001
TRIP BLANK
Sample Summary
TestAmerica Job ID: 680-159860-1
Matrix Collected Received
Water 10/26/1812:30 10/2711809:55
Water 10/26/18 00:00 10/27/18 09:55
TestAmerica Savannah
Page 5 of 18 11/7/2018

Method Summary
Client: EHS Support, LLC
Project/Site: NexeoSolutions - Charlotte
TestAmerica Job ID: 680-159860-1
Method
Method Description
Protocol
Laboratory
624
Volatile Organic Compounds(GC/MS)
40CFRI36A
TALSAV
1664A
HEM and SGT-HEM
1664A
TALSAV
SM 25401)
Solids, Total Suspended (TSS)
SM
TAL SAV
SM 4500 H+ B
pH
SM
TA SAV
SM 5220D
COD
SM
TALSAV
,1664A
HEM and SGT-HEM (Aqueous)
1664A
TALSAV
Protocol References:
1664A = EPA-821-98-002
40CFR 1 36A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater', 40CFR, Part 136, Appendix A, October 26, 1984 and
subsequent revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater'
Laboratory References:
TAIL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 6 of 18 11/7/2018

Definitions/Glossary
,l Client: EHS Support, LLC
Project/Site: NexeoSolutions- Charlotte
Qualifiers
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
Abbreviation These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit(DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, cr additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limitof Detection (DOD/DOE)
LOQ Limit of Quantuation ooD/DOE)
MDA Minimum Detectable Activity(Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
INC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
POLL Practical Quantitafion Limit
,QC Quality Control
RER Relative Error Ratio (Radiochemistry)
'RL Reporting Limit or Requested Limit(Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
iTEF Toxicity Equivalent Factor (Dioxin)
TEO Toxicity Equivalent Quotient(Dioxin)
TestAnnerica Job ID: 680-159860-1
TestAmerica Savannah
Page 7 of 18 11/7/2018

Detection Summary
O
Client: EHS Support, LLC
Project/Site: NexeoSolutions - Charlotte
TestAnnerica Job ID:
680-159860-1
F
Client Sample ID: OUTFALL 001
Lab Sample ID:
680-159860-1
Analyte
Result Qualifier
NONE NONE
Unit
oil Fac D Method
Prep Type
1 I
^�
pH
To HF
SU
1 SM 4500 HI B
Total/NA
L
Temperature
20.3 HF
Degrees C
1 SM 4500 Ht B
TotalINA
Analyte
Result Qualifier
RL MDL
Unit
oil Fac D Method
Prep Type
Chemical Oxygen Demand
29
10
mg/L
1 SM 5220D
TotalINA
Analyte
Result Qualifier
RL RL
Unit
oil Fac D Method
Prep Type
Total Suspended Solids
59
2.0
mg/L
1 SM 2540D
Total/NA
l
Client Sample ID: TRIP BLANK
Lab Sample ID:
680-159860-2
CNo Detections.
L�Tl
fl
❑
This Detection Summary does not include radiochemical test results.
TestAnnerica Savannah
C1
Iq
Page 8 of 18 11/7/2018

Client Sample Results
Client: EHS Support, LLC
°. Project/Site: NexeoSolutions - Charlotte
Client Sample ID: CUTFALL 001
Date Collected: 10/26/18 12:30
Date Received: 10/27/18 09:55
Method: 624 - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier RL
Toluene <1.0 1.0
Xylenes, Total <2.0 2.0
Surrogate
%Recovery Qualifier
Limits
Toluene-d8(Surr)
94
79- 119
1,2-Dichlomethane-d4 (Surr)
109
70. 130
4-13romofluorobenzene (Surr)
103
71 _ 121
Dibmmofluommethane(Sum)
104
77-129
General Chemistry
Analyte
Result Qualifier
NONE
pH
7.0 HF
Temperature
20.3 HF
Analyte
Result Qualifier
RL
HEM (Oil & Grease)
2.7
2.7
Chemical Oxygen Demand
29
10
Analyte
Result Qualifier
RL
Total Suspended Solids
59
2.0
TestAmerica Job ID: 680-159860-1
Lab Sample ID: 680-159860-1 4
Matrix: Water
f% l
L__J
MDL
Unit
D
Prepared
Analyzed
oil Fac
ug/L
ll/05/18 20:06
ug/L
11/05/18 20:06
1
L�
Prepared
Analyzed
Dil Fac
71/O5/18 20:06
1
`
11/05118 20,06
1
11/05/18 2006
1
0
11105118 20:06
1
n
NONE
Unit
D
Prepared
Analyzed
oil Fac
Su
10/30/18 19:07
1
Degrees C
10/30/18 19:07
1
MDL
Unit
D
Prepared
Analyzed
Dil Fac
mg/L
11/01/1809:05
11/01/1811:15
1
J
mg/L
11/01/1812:31
1
RL
Unit
D
Prepared
Analyzed
Dil Fac
U
m9/L
11/01/18 10:28
1
':Client Sample ID: TRIP BLANK Lab Sample ID: 680-159860-2
Date Collected: 10126118 00:00 Matrix: Water
Date Received: 10/27/18 09:55
Method: 624 - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Toluene 11.0 1.0 ug/L 11/05/1817:03 1
Xylenes, Total <2.0 20 ug/L 11/05/1817:03 1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed oil Fac
Toluene-0 (Sum)
95
79 _ 119
11/0 5/18 1703 1
1,2-Dichlomethane-d4(Swr)
109
70-130
11/0511817.03 1
4-Bromofluorobenzene (Surr)
101
71 _ 121
11/05/16 17.03 1
-... ........ ne .. ... ...........
Dibrompfluoromefhene (Surr)
.... 106 ....._
106
__ ...__._......... ..
77. 129
.-...... ...... .-............./ _.03 _.
71/OY18 /7:03 /
TestArnerica Savannah
Page 9 of 18 11/7/2018

Surrogate Summary
51
Client: EHS Support, LLC
TestAmerica Job ID: 680-159860-1
-
Project/Site: NexeoSolutions -Charlotte
Method: 624 - Volatile Organic Compounds
(GC/MS)
Matrix: Water
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
=J
TOL
DCA
BFB
DBFM
Lab Sample to Client Sample to
(79.119)
(70-130)
(71.121)
(77-129)
680-159860-1 OUTFALL 001
94
109
103
104
n
680-159860-2 TRIP BLANK
95
109
101
106
J
LCS 680-54627814 Lab Control Sample
101
115
105
110
'
LCSD 580-546278/5 Lab Control Sample Dup
100
113
106
106
MB 680-54627818 Method Blank
96
107
101
105
Surrogate Legend
TOL = Toluene-d8 (Surr)
n
DCA = 1,2-Dichloroethane-d4 (Surr)
FJ
BFB=4-BromoOuorobenzene(Surr)
DBFM = Dibromo0uoromethane (Surr)
Ly��1
TestAmerica Savannah
Page 10 of 18 11/7/2018

QC Sample Results
Client: EHS Support, LLC TestAmerica Job ID: 680-159860-1
Project/Site: NexeoSolutions - Charlotte
Method: 624 - Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 680-54627818 Client Sample ID: Method Blank
Matrix: Water Prep Type: TOtalINA
Analysis Batch: 546278
MB MB
Analyto Result Qualifier RL MDL Unit D Prepared Analyzed oil Fac
Toluene <1.0 1.0 ug/L 11/05/1816: 17 1
Xylenes, Total c2.0 2.0 ug/L 11/05/18 16:17 1
Me Me
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed oil Fac
Toluene-d8(Sun)
96
79-119
11/05081677 1
1,2-Dichloroethane-d4(Sun)
107
70_130
11/0511816: 17 1
4-Bromofluombenzene (Sun)
101
71 _ 121
11105118 16:17 1
Dibromofluoromethane (Sun)
105
77. /29
_
11/0Y78 16:17 1
Lab Sample ID: LCS 680-546278/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 546278
Spike
LCS LCS
%Rec.
Analyto
Added
Result Qualifier Unit
D %Rec Limits
Toluene
20.0
20.0 ug/L
100 47-150
Xylenes, Total
40.0
41.4 ug/L
104 78 _ 119
LCS LCS
Surrogate
%Recovery Qualifier
Limits
Toluene-all(Surr)
101
79 - 119
1,2-Dichlomethane-d4(Surr)
115
70-130
4-Bromofluombenzene (Surr)
105
71 - 121
Dibmmofluommethane (Surr)
110
77. 129
Lab Sample ID: LCSD 680-54627815
Client Sample ID:
Lab Control Sample Dup
Matrix: Water
Prep Type: TotalINA
Analysis Batch: 546278
Spike
LCSD LCSD
%Rec. RPD
Analyto
Added
Result Qualifier
Unit D %Rec
Limits RPD Limit
Toluene
20.0
19.8
ug/L 99
47 _ 150 1 30
Xylenes, Total
40.0
42.0
ug/L 105
78-119 1 30
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
Toluene-0 (Surr)
100
79 - 119
1,2-Dichloroethane-& (Surr)
113
70- 130
4-6romofluombenzene (Surr)
106
71 _ 121
........................ ..
Dibromofluoromethane (Surr)
... ...... ...... ... ...... .....
106
77-12 ....._.... _....,.__...... __....._. _. ... _.. ... _.. _....._ ... _.. ... _.._
77- 129
Method: 1664A - HEM and SGT-HEM
I Lab Sample ID: MB 680-54581011-A
Matrix: Water
Analysis Batch: 545835
MB MB
Analyte Result Qualifier RL
HEM (Oil & Grease) <5.0 5.0
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 545810
MDL Unit D Prepared Analyzed oil Fac
mg/L 11/01/1809:05 11/01/1811.15 1
TestAmerica Savannah
Page 11 of 18 11/7/2018

QC Sample Results
Client: EHS Support, LLC TestAmerica Job ID: 680-159860-1
Project/Site: NexeoSolutions - Charlotte
Method: 1664A - HEM and SGT-HEM (Continued)
Lab Sample ID: LCS 680-545810/2-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: TOtalINA
Analysis Batch: 545835 Prep Batch: 545810
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
HEM (Oil & Grease) 40.0 31.20 mg/L 78 78 - 114
Lab Sample ID: LCSD 680-54581013-A Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: TOtalINA
,l Analysis Batch: 545835 Prep Batch: 545810
Spike LCSD LCSD %Rec. RPD
All Added Result Qualifier Unit D %Rec Limits RPD Limit
i' HEM (Oil & Grease) 40.0 34.20 mg/L 86 78 - 114 9 18
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-54582411 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 545824
Me Me
Analyte Result Qualifier RL RL Unit D Prepared Analyzed oil Fac
Total Suspended Solids <1.0 1.0 mglL 11/Ot/18 10:28 1
Lab Sample ID: LCS 680-54582412 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 545824
Spike LCS LCS %Rec.
I Analyte Added Result Qualifier Unit D %Rec Limits
Total Suspended Solids 20.0 24.0 mg/L 120 80 - 120
Lab Sample ID: LCSD 680-54582413
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 545824
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
Total Suspended Solids
20.0
24.0
mg/L 120 80-120 0 25
'Method: SM 4500 H+ B - pH
Lab Sample ID: LCS 680-545612/29
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 545612
Spike
LCS LCS
%Rec.
Aral
Added
Result Qualifier
Unit D %Rec Limits
PH
7.00
7.0
SU 101 63.158
Lab Sample ID: 680-159860-1 DU
Client Sample ID: OUTFALL 001
Matrix: Water
Prep Type: TOtalINA
Analysis Batch: 545612
Sample Sample
DU DU
RPD
Analyto
Result Qualifier
Result Qualifier
Unit D RPD Limit
pH
7.0 HF
TO
SU 0.1 40
Temperature
20.3 HF
20.5
Degrees C 0a
TestAmerica Savannah
Page 12 of 18 11/7/2018

QC Sample Results
Client: EHS Support, LLC
Project/Site: NexeoSolutions - Charlotte
11
Method: SM 5220D - COD
1� Lab Sample ID: MB 680-545899/3
Matrix: Water
Analysis Batch: 545899
Me Me
Analyte Result Qualifier RL
Chemical Oxygen Demand <10 10
Lab Sample ID: LCS 680-54589914
Matrix: Water
Analysis Batch: 545899
Amdyte
Chemical Oxygen Demand
TestAmerica Job ID: 680-159860-1 ❑���y,)l
1
131
Client Sample ID: Method Blank Q
Prep Type: Total/NA ❑
MDL Unit D Prepared Analyzed oil Fac
mg/L 11/01/18 12:31 1 a
Spike LCS LCS
Added Result Qualifier
50.0 48.0
Client Sample ID: Lab Control Sample 7
Prep Type: Total/NA �n
V
%Rec.
Unit 0 %Rec Limits
mg/L 96 90 - 110
TestAmerica Savannah
Page 13 of 18 11/7/2018

QC Association Summary
Client: EHS Support, LLC
Project/Site: NexeoSolutions - Charlotte
GC/MS VOA
Analysis Batch: 546278
TestAmerica Job ID: 680-159860-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-159860-1
OUTFALL 001
Total/NA
Water
624
680-159860-2
TRIP BLANK
Total/NA
Water
624
MB 680-54627818
Method Blank
Total/NA
Water
624
LCS 680-546278/4
Lab Control Sample
Total/NA
Water
624
LCSD 680-546278/5
Lab Control Sample Dup
Total/NA
Water
624
General
Analysis Batch: 545612
Lab Sample ID
[680-159860-1
LCS 680-545612/29
680-159860-1 DU
IPrep Batch: 545810
j
Lab Sample ID
680-159860-1
MB 680-54581011-A
LCS 680-545810/2-A
LCSD 680-545810/3-A
�Analysis Batch: 545824
Client Sample ID
Prep Type
Matrix
Method Prep Batch
OUTFALL 001
Total/NA
Water
SM 4500 H+ B
Lab Control Sample
Total/NA
Water
SM 4500 H+ B
OUTFALL 001
Total/NA
Water
SM 4500 H+ B
Client Sample ID
OUTFALL 001
Method Blank
Lab Control Sample
Lab Control Sample Dup
Prep Type Matrix Method Prep Batch R
ToWUNA
Water
1664A
Total/NA
Water
1664A
Total/NA
Water
1664A
Total/NA
Water
1664A�
jn
Lab Sample to
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-159860-1
OUTFALL 001
Total/NA
Water
SM 25400
MB 680-545824/1
Method Blank
Total/NA
Water
SM 2540D
LCS 680-545824/2
Lab Control Sample
Total/NA
Water
SM 2540D
LCSD 680-545824/3
I.
Lab Control Sample Dup
Total/NA
Water
SM 2540D
Analysis Batch: 545835
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-159860-1
OUTFALL001
Total/NA
Water
1664A
545810
MB 680-545810/1-A
Method Blank
Total/NA
Water
1664A
545810
LCS 680-545810/2-A
Lab Control Sample
Total/NA
Water
1664A
545810
LCSD 680-545810/3-A
Lab Control Sample Dup
Total/NA
Water
1664A
545810
Analysis Batch: 545899
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-159860-1
OUTFALL 001
Total/NA
Water
SM 5220D
MB 680-545899/3
Method Blank
Total/NA
Water
SM 5220D
LCS 680-545899/4
Lab Control Sample
ToWUNA
Water
SM 5220D
TestAmerica Savannah
Page 14 of 18
11 /7/2018

Lab Chronicle
Client: EHS Support, LLC
Project/Site: NexeoSolutions - Charlotte
TestAmerica Job ID: 680-159860-1
Client Sample ID: OUTFALL 001 Lab Sample ID: 680-159860-1
Date Collected: 10/26/18 12:30 Matrix: Water
Date Received: 10/27/18 09:55
Batch Balch
Dil
Initial
Final
Balch
Prepared
Prep Type
Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Analysis 624
1
5 mL
5 mL
546278
11/05/18 20:06
WAS
TAL SAV
Instrument ID: CMSC
TotaI/NA
Prep 1664A
925 mL
500 mL
545810
11/01/18 09:05
JAS
TAL SAV
Total/NA
Analysis 1664A
1
545835
11/01/1811:15
JAS
TAL SAV
Instrument ID: NOEOUIP
Total/NA
Analysis SM 2540D
1
500 mL
1000 mL
545824
11/01/1810:28
BTD
TAL SAV
Instrument ID: NOEOUIP
Total/NA
Analysis SM 4500 H+ B
1
545612
10/30/18 19:07
BTD
TAL SAV
Instrument ID: MANTECH
Total/NA
Analysis SM 5220D
1
2 mL
2 mL
545B99
11/01/1812.31
JER
TAL SAV
Instrument ID: SPC7
Client Sample ID: TRIP BLANK
Lab Sample ID:
680-159860-2
Date Collected:
10126/18 00:00
Matrix: Water
Date Received:
10/27/18 09:55
Batch Batch
oil Initial Final Batch Prepared
Prep Type
Type Method
Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA
Analysis 624
1 Still 5 mL 546278 11/05/18 17:03 WAS
TAL SAV
InstrumentlD: CMSC
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 15 of 18 11/7/2018

iintmurl-lUd Uldl-IULLe
-21338-8-aueen-city=Drive - 490508 Chain -of ^Custody Record=
Charlotte, KC 28280 Charlotte
Phone: [phone] Fax:
Regulatory Program: I]ovr :rocs ❑RCRA L'-'j, Dux,:
:2 5 5 7 7 7 TestArr�erica -
tqE LEADER IN ENVIRONMENTAL TESTING
TestAmer)ca Laboratories, Inc.
TAL821010218)
Client Contact
Project Manager: B L1E
Site Contact: Qz ll
Dale: 1012-Clig
COC No:
Company Name: 41EVEO SOLOTIAS (- -CAh
Tel/Fax; 'Z,51
Lab Contact: L tJt
Carrier:
_�_ ot__COCS
Address: 000 t1@9 lU Si Q
Analysis Turnaround Time
i
u
aD
ry
u
u
_ z
y
c
f
E
i
,.N
A
Q
o
Y
Sampler:
Ci;ylStateZD: j 713SO
[j CALENDAR DAYS ' I WoR¢INB DAYS
For Lab Use Only:
Walk-in Client:
Lab Sampling:
Phone:
TAT a dMerent Rom Bobw
>.! 2 weeLs
❑ 1
0 2 eats
❑ tdA,
Fax:
Project Name: _ 1.0
Site:
Job! SDG No.;
POt
Sample Identification
Sample
Date
Sample
Time
Sample
Type
c.cr,Rl
Matrix
rot
cool
Sample Specllic Notes'
O F 1l col
1012001230
G
w
01'("iKKX
m
o—�
m
0
N
f) �
w
0
O_
c
W
0
n
qn
'raservalion,Used: T= ice;. 2= HCI; :Se H2SO4;; 4=HNOT;._ S=NaOH;,6=
Other
'•
'
'
.
�'
t
:
< . .
'ossible Hazard Identification:
Ere any samples from a listed EPA Hazardous Waste? Please Lha any EPA Waste Codes for the sample in the
Jomments Section if the lab is to dispose of the sample.
Sample Disposal (A Ice may be assessed if samples are retained longer than t month)
❑Rcturn to Q01 I OupOW'W lee ❑Ar[M1mC lw Men(M1s
INon.H d ❑na ,,ae'e L )$Ein tr,iwt Ljft oRB L ]u'knevm
Special In tructions/OC Requirements a Comments:
L;nj}t vej.mt,fpr T0I"Le1)b 2nQ �<ylene3e io •�el� br^e4kaA�
Custody Seals Intact: j] Yes { i No
Custody Seal No.: juave, Temp. (` ): Obs'd: Corrd: Tinerm ID No.:
Relinouishetl by:
Company:
Ante 4Gro,
DatelTime:
AC/181400
Received by;
Company:
Daterlime:
Relinquished by:
Company;
Date/Time:
Received by:
Company:
DalerTime:
1'1nquished by:
N
Company:
DaterTime:
< . ed m Labor ry by:
_! "
Company:
DaterTime:
/� Z'2. / o rUs
(.9/Z.

Login Sample Receipt Checklist
'i Client: EHS Support, LLC
Login Number: 759860
List Number: 1
Creator: Laughlin, Paul D
Question Answer Comment
y�
:Lj
Job Number: 680-159860-1
4
List Source: TestAmerica Savannah
Radioactivity wasn't checked or is <l= background as measured by a survey
N/A
meter.
v
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
(�
(?J
The cooler or samples do not appear to have been compromised or
True
tampered with.
^�
❑
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
I jLJ 0
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
N/A
i; There are no discrepancies between the containers received and the COC.
True
iSamples are received within Holding Time (excluding tests vrith immediate
True
HTs)
Sample containers have legible labels.
True
j'Containers are not broken or leaking.
True
(Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
'Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4"),
Multiphasic samples are not present.
True
j�Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
TestAmerica Savannah
Page 17 of 18 11/7/2018

Accreditation/Certification Summary
Client: EHS Support, LLC
Project/Site: NexeoSolutions - Charlotte
Laboratory: TestAmerica Savannah
The accreditations/certifications listed below are applicable to this report.
1.
I
Authority Program
South Carolina State Program
EPA Region Identification Number
4 98001
Accreditatian/Certification renewal pending - accreditation/certification considered valid.
TestArnerica Job ID: 680-159860-1
Expiration Date
06-30-18
TestAnnerica Savannah
Page 18 of 18
11/7/2018