NCS000136_MONITORING INFO_20190910

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
IV L V `�
DOC TYPE
❑ HISTORICAL FILE
CXMONITORING REPORTS
DOC DATE
❑
YYYYMMDD

Mallinckrodt
Pharmaceuticals
September 3, 2019
North Carolina Department of Environmental Quality
Division of Energy, Minerals, and Land Resources
Stormwater Permitting Unit
512 N. Salisbury Street
Raleigh, NC 27604
RECEIVED
SEP 10 2919
DENR-LAND QUALITY
STORMWATER PERMITTING
Re: Semi-annual Stormwater Monitoring Report for — Year 8 Period 2
Mallinckrodt Raleigh Pharmaceutical Plant [SpecGx LLC]
NPDES Individual Stormwater Permit No. NCS000136
Attention: Central Files
Attached are two (2) signed copies of the Stormwater Discharge Outfall (SDO) Monitoring Report
for Year 8 — Period 2 (June 1, 2019 through November 30, 2019) as required by Part Ill, Section
E of the above -referenced permit.
Please note that our permit expired on December 31, 2016 and we submitted a permit renewal
application to your office on June 1, 2016 prior to the renewal application deadline. It is our
understanding that the NCDEQ-DEMLR requires Mallinckrodt to continue monitoring our
stormwater outfalls under the same "semi-annual' frequency specified in our current permit until
we receive a new permit. Therefore, the next semi-annual storm water sample will be collected
between December 1, 2019 and May 31, 2020 unless we hear otherwise from your office.
If anyone in your office has any questions concerning this report, please do not hesitate to call me
at 919-878-2895.
Regards,
SpecGx LLC
Tim Roberts
Principal Environmental Engineer
Attachments (2)
Submitted via Federal Express Tracking # 776141797259
cc: Shane I-loover- Mallinckrodt, w/Attachments
Daphne Jones — Solutions -TES w/Attachments
8801 Capital Boulevard • Raleigh, NC 27616 • 919.878.2800 T • 919.878.2823 F • w .mallinckrodt.com

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
PERMIT NO. NCS000136
CERTIFICATE OF COVERAGE NO. Not Applicable (NA)
FACILITY NAME SpecGx LLC (Ma
PERSON COLLECTING SAMPLES
CERTIFIED LABORATORY PACE
P rt B• S ecific Monitorin Re uirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2019
(This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY Wake County
PHONE NO. [phone]
PLEASE SIGN ON THE REVERSE 4
a
Outfall'
No.
Date
Sample
Collected,
moldd/yr
Total
-.Suspended
`Solids, mg/L=
pH,
Standard
units
Conductivity,
us/cm
Chemical
Oxygen
Demand,
mg/L
Total
Nitrogen,
mg/L
Nitrate-
Nitrite;-
mg/L
Ammonia
Nitrogen,
mg/L
Sulfate,
mg/L
Ammonium
Sulfate,
mg/L
(calculated
result
Benchmark
-
100
6.0 - 9.0'
NA
120
30
10
7.2
500
19;
Outfall 001
8/14/2019
14.7
6.51
162
45.0
1.60
0.895
0.135
3.93 J
0.64
Outfall 002
8/14/2019
36.5
6.21
176
5.68 J
0.839
1 0.270
0.233
2.70 J
1.10
Outfall003B
8/14/2019
8.20
7.26
391
41.0
1.71
<0.0197
0.323
23.4
1.52
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
J — Laboratory qualifier indicating an estimated concentration for test result that was above method detection but below the reported detection limit.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
Dart D: Vn6irin Mnintcnnnro Grtivity Mnnitnrina Renuirements
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00556
00530:
00400
Oil and Grease,
mg/L
Total Suspended
Solids,+'
m /L .
pH,
Standard units
New Motor Oil Usage,
Annual average gal/mo
Benchmark
15.
100 -
6.0 —9.0
NA
NA
NA
NA
NA
NA
G�
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
STORM EVENT CHARACTERISTICS:
Date 08/14/2019 (first event sampled)
Total Event Precipitation (inches): 0.38 (12 hr period)
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
S W U-245-031308
Page I of 2

Raleigh, North Carolina 27699-1617
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
1 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic
crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent
Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use
the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22, and for cathode ray tube manufacture use
the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be
waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those
facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic
organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are
exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the
all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
(Signature)
NA
(Date)
"I certify, under penalty of law, that this document and all attachments were prepared under my direction
or supervision in accordance with a system designed to assure that qualified personnel properly gather
and evaluate the information submitted. Based on my inquiry of the person or persons who manage the
system, or those persons directly responsible for gathering the information, the information submitted is,
to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing
violations."
(Signature of Permittee)
(Date)
(� �--�, I�C�
S WU-245-031308
Page 2 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
PERMIT NO. NCS000136 SAMPLES COLLECTED DURING CALENDAR YEAR: 2019
CERTIFICATE OF COVERAGE NO. Not Applicable (NA) (This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME SpecGx LLC (Mallinckrodt Pharmaceuticals) COUNTY Wake County
PERSON COLLECTING SAMPLES Sean Jarvah — DAA PHONE NO. [phone]
CERTIFIED LABORATORY PACE National - NCDEQ Certification # 375
PLEASE SIGN ON THE REVERSE 4
R is
rart B. S eafic
Outfall
No.
Mondonn
Date
Sample
Collected,
molddlyr
a uiremen
Total
Suspended
Solids, mg/L
pH,
Standard
units
Conductivity,
us/cm
Chemical
Oxygen
Demand,
mg/L
Total
Nitrogen,
mg/L
Nitrate-
Nitrite,
mg/L
Ammonia
Nitrogen,
mg/L
Sulfate,
mg/L
Ammonium
Sulfate,
mg/L
(calculated
result
Benchmark
100
6.0 — 9.0
NA
120
30
10
7.2
500
19
Outfall 001
8/1412019
14.7
6.51
162
45.0
1.60
0.895
0.135
3.93 J
0.64
Outfall 002
1 8/14/2019
1 36.5
6.21
176
5.68 J
0.839
0.270
0.233
2.70 J
Mu
Outfall003B
8/14/2019
8.20
7.26
391
41.0
1.71
<0.0197
0.323
23.4
1.52
Note: If you report a sampled value in excess of the benchmarK value, or outsiae the Dencnmark range iui PM, yuu nwsi unPici ncm i el i OF i leF c ica N0u>w.
J — Laboratory qualifier indicating an estimated concentration for test result that was above method detection but below the reported detection limit.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
nn..:..a........ .. A.Ai..ih. Mnnitnrinn Rannirnmant¢
ran ✓. vci,wic
Outfall
No.
ma,nicna,,..�.-...... �.
Date
Sample Collected,
mo/dd/yr
�........... ... .._ _.. _..._..-_
00556
00530
00400
Oil and Grease,
mg/L
Total Suspended
Solids,
m /L
pH,
Standard units
New Motor Oil Usage,
Annual average gal/mo
Benchmark
15
100
6.0 — 9.0
NA
NA
NA
NA
NA
NA
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
STORM EVENT CHARACTERISTICS:
Date 08/14/2019 (first event sampled)
Total Event Precipitation (inches): 0.38 (12 hr period)
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
S WU-245-031308
Page 1 of2

Raleigh, North Carolina 27699-1617
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
1 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic
crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent
Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use
the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22, and for cathode ray tube manufacture use
the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be
waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those
facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic
organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are
exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the
all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan."
NA
Name (Print name)
NA
Title (Print title)
NA NA
(Signature) (Date)
" I certify, under penalty of law, that this document and all attachments were prepared under my direction
or supervision in accordance with a system designed to assure that qualified personnel properly gather
and evaluate the information submitted. Based on my inquiry of the person or persons who manage the
system, or those persons directly responsible for gathering the information, the information submitted is,
to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing
violations."
S
(Signature of Permittee)
(Date)
7I-�i�(�
S W U-245-031308
Pal-e 2 of 2

Mallinckrodt
Pharmaceuticals
March 12, 2019
North Carolina Department of Environmental Quality
Division of Energy, Minerals, and Land Resources
Stormwater Permitting Unit
512 N. Salisbury Street
Raleigh, NC 27604
Re: Semi-annual Stormwater Monitoring Report for — Year 8 Period
Mallinckrodt Raleigh Pharmaceutical Plant [SpecGx LLC]
NPDES Individual Stormwater Permit No. NCS000136
Attention: Central Files
RECEIVED
MAR 14 2019
DENR-LAND QUALITY
STORMWATER PERMITTING
Attached are two (2) signed copies of the Stormwater Discharge Outfall (SDO) Monitoring Report
for Year 7 — Period 1 (December 1, 2018 through May 31, 2019) as required by Part III, Section
E of the above -referenced permit.
Please note that our permit expired on December 31, 2016 and we submitted a permit renewal
application to your office on June 1, 2016 prior to the renewal application deadline. It is our
understanding that the NCDEQ-DEMLR requires Mallinckrodt to continue monitoring our
stormwater outfalls under the same "semi-annual" frequency specified in our current permit until
we receive a new permit. Therefore, the next semi-annual storm water sample will be collected
between June 1, 2019 and November 30, 2019 unless we hear otherwise from your office.
If anyone in your office has any questions concerning this report, please do not hesitate to call me
at 919-878-2895.
Regards,
SpecGx LLC
Tim Roberts
Principal Environmental Engineer
Attachments (2)
Submitted via Federal Express Tracking # 774677460748
cc: Shane Hoover- Mallinckrodt, w/Attachments
Daphne Jones — Solutions-IES w/Attachments
8801 Capital Boulevard - Raleigh, NC 27616 - 919.878.2800 T • 919.878.2823 F • w .mallinckrodt.com

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
PERMIT NO. NCS000136 SAMPLES COLLECTED DURING CALENDAR YEAR: 2019
CERTIFICATE OF COVERAGE NO. Not Applicable INA) (This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME SpecGx LLC (Mallinckrodt Pharmaceuticals)
PERSON COLLECTING SAMPLES Sean Jarvah — DAA
CERTIFIED LABORATORY ESC Lab Sciences Lab # ENV375
Part R, Snecific Monitoring Requirements
COUNTY Wake County
PHONE NO. (9191 873-1060
PLEASE SIGN ON THE REVERSE 4
Outfall
No.
Date
Sample
Collected,
mo/dd/yr
Total
Suspended
Solids, mg/L
pH,
Standard
units
Conductivity,
us/cm
Chemical
Oxygen
Demand,
mg/L
Total
Nitrogen,
mg/L
Nitrate-
Nitrite,
mg/L
Ammonia
Nitrogen,
mg/L
Sulfate,
mg/L
Ammonium
Sulfate,
mg/L
(calculated
result
Benchmark
-
100
6.0 — 9.0
NA
120
30
10
7.2
500
19
Outfall001
2/18/2019
1 14.1
6.80
148
13.9
1.04
0.702
0.143
33.6
0.67
Outfall 002
2118/2019
7.55
6.31
140
8.09 J
1.48
0.616
0.736
4.24 J
3.47
Outfall 003E
2/18/2019
1.46 J
7.40
362
35.8
3.03
2.04
0.319
82.6
1.50
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement I ier 1 or I ier 1 responses.
J — Laboratory qualifier indicating an estimated concentration for test result that was above method detection but below the reported detection limit.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
Part D: Vehicle Maintenance Activitv Monitorina Requirements
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Oil and Grease,
mg/L
Total Suspended
Solids,
m /L
pH,
Standard units
New Motor Oil Usage,
Annual average gal/mo
Benchmark
15
100
6.0 — 9.0
NA
NA
NA
NA
NA
NA
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
STORM EVENT CHARACTERISTICS:
Date 02/18/2019 (first event sampled)
Total Event Precipitation (inches): 0.60 (13.5 hr period)
RECEIVED
MAR 14 2019
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
DENR-LAND QUALITY
STORMWATER PERMITTING
SWU-245-031308
Pagel of 2

Raleigh, North Carolina 27699-1617
Da IF (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
1 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic
crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent
Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use
the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use
the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be
waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those
facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic
organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are
exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the
all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
NA NA
(Signature) (Date)
"I certify, under penalty of law, that this document and all attachments were prepared under my direction
or supervision in accordance with a system designed to assure that qualified personnel properly gather
and evaluate the information submitted. Based on my inquiry of the person or persons who manage the
system, or those persons directly responsible for gathering the information, the information submitted is,
to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing
violations."
S
(Signature of Permittee) (Date)
S W U-245-031308
Page 2 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
PERMIT NO. NCS000136 SAMPLES COLLECTED DURING CALENDAR YEAR: 2019
CERTIFICATE OF COVERAGE NO. Not Applicable (NA) (This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME SpecGx LLC (Mallinckrodt Pharmaceuticals)
PERSON COLLECTING SAMPLES Sean Jarvah — DAA
CERTIFIED LABORATORY ESC Lab Sciences Lab # ENV375
Part R- Snnrifir Mnnitnrinn Remuimments
COUNTY Wake County
PHONE NO. [phone]
PLEASE SIGN ON THE REVERSE 4
Outfall
No.
Date
Sample
Collected,
mo/dd/yr
Total
Suspended
Solids, mg/L
pH,
Standard
units
Conductivity,
us/cm
Chemical
Oxygen
Demand,
mg/L
Total
Nitrogen,
mg/L
Nitrate-
Nitrite,
mg/L
Ammonia
Nitrogen,
mg/L
Sulfate,
mg/L
Ammonium
Sulfate,
mg/L
(calculated
result
Benchmark
-
100
6.0 — 9.0
NA
120
30
10
7.2
500
19
Outfall001
2/1812019
14.1
6.80
148
13.9
1.04
0.702
0.143
33.6
0.67
Outfall 002
1 2/18/2019
7.55
6.31
140
8.09 J
1.48
0.616
0.736
4.24 J.
3.47
Outfall 003E
2/18/2019
1.46 J
7.40
362
35.8
3.03
2.04
0.319
82.6
1.50
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or I ier 2 responses.
J — Laboratory qualifier indicating an estimated concentration for test result that was above method detection but below the reported detection limit.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
Part n. Vehirle Maintenance Activitv Monitorina Requirements
Outfall
No.
Date
Sample Collected,
mo/dd/yr
00556
00530
00400
Oil and Grease,
mg/L
Total Suspended
Solids,
m /L
pH,
Standard units
New Motor Oil Usage,
Annual average gal/mo
Benchmark
15
100
6.0 — 9.0
NA
NA
NA
NA
NA
NA
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
STORM EVENT CHARACTERISTICS:
Date 02/18/2019 (first event sampled)
Total Event Precipitation (inches): 0.60 (13.5 hr period)
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
S W U-245-031308
Pagel of 2

Raleigh, North Carolina 27699-1617
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
1 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic
crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent
Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use
the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use
the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be
waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those
facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic
organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are
exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the
all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
NA NA
(Signature) (Date)
"I certify, under penalty of law, that this document and all attachments were prepared under my direction
or supervision in accordance with a system designed to assure that qualified personnel properly gather
and evaluate the information submitted. Based on my inquiry of the person or persons who manage the
system, or those persons directly responsible for gathering the information, the information submitted is,
to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing
violations."
(Signature.ofPermittee) -- —_
3/o`f1C\
-(Date) — - -
SWU-245-031308
Page 2 of 2