NCG120051_MONITORING INFO_20191021

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
NCG ' b 0 5
DOC TYPE
❑ HISTORICAL FILE
YMONITORING REPORTS
DOC DATE
❑ b 0 `� I
YYYYMMDD

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG120000
Date submitted 16 October 2019
CERTIFICATE OF COVERAGE NO. NCG120051
FACILITY NAME _Uwharrie Environmental
COUNTY _Montgomery
PERSON COLLECTING SAMPLES _Brian Scott
LABORATORY _ Lab Cert. #
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
R E C E I UE SAMPLE COLLECTION YEAR _2019
OCT 2 1 SAMPLE PERIOD ❑ Jan -June X July -Dec
�019 or ❑ Monthly' (month)
CENTRAL FILES DISCHARGING TO CLASS ❑ORw ❑HQw ❑Trout ❑PNA
DWR EN SECTION ❑Zero -flow ❑Water Supply [:]SA
X Other C
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
n No dischorge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Chemical Oxygen Demand
Fecal Coliform
Total Suspended Solids
Benchmarks =__>
-
-
120 mg/L
1000 count per 100 mL
100 mg/L or 50 mg10
1
No Discharge
.3"
0
0
0
2
No Discharge
.3"
0
0
0
5B
No Discharge
.3"
0
0
0
6B
No Discharge
.3"
0
0
1 - 0
7A
No Discharge
.3"
0
0
0
7C
No Discharge
.3"
0
0
0
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -
numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the
detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX".
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > SS gal of new oil per month.
Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012
Page 1 of 2

F f No discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
-
- -
15 mg/L
100 mg/L or 50 mg/L°
6.0 — 9.0 SU
7B
-No Discharge
.3"
0
0
0
Footnotes from Part A also apply to this Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART AND PART B MONITORING RESULTS:
A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR including all "No Discharge" reports within 30 days of receipt of the lab results for of end of monitoring period
in the case of "No Discharge" reports) to.
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibilityy of fines and imprisonment for knowing violations."
!l
(Signature of Permittee) (Da )
Permit Date: 11/1/2012-10/31/2017 SWU-248, last revised 10/25/2012
Page 2 of 2

CERTIFICATION OF THE EVALUATION OF OUTFALLS FOR
NON -STORM WATER DISCHARGES
Republic Services, Inc. (dba Uwharrie)
500 landfill Road
Mt. Gilead, North Carolina 27306
I certify that I have evaluated the storm water discharge of the facility and determined there is no
presence of non -storm water discharges. The method used for evaluating the discharge was a visual
inspection of discharge patterns and inspection of drainage maps and schematics, and analytical testing.
The storm water discharge review was cf nducted on The on -site drainage points observed
during the test included ��_ ( !'�% %A 7/ 7676
Title
—�-
10-i-d
Date
Qen�S W00 t=lemv,4 - 1 Y� Jp-P% Q •
le/i&//9

Im
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG120000
Date submitted 27 June 2019_
CERTIFICATE OF COVERAGE NO. NCG 120051
FACILITY NAME _Uwharrie Environmental
COUNTY _Montgomery
PERSON COLLECTING SAMPLES _Brian Scott
LABORATORY_ENCO_Labs _ Lab Cert. q _CC09930
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR _2019
SAMPLE PERIOD X Jan -June [].July -Dee
or ❑ Monthly' • (month)
E OHAIRGINGTOCLASS ❑ORW ❑HQW ❑Trout ❑
RE
C S❑Zero-flow ❑Water Supply ❑SA
JUL 0 5 2019 X Other C
CEN"I RAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4
DWR SECTION
❑ No discharge this period; 2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
inches'
Chemical Oxygen Demand
Fecal Coliform
Total Suspended Solids
Benchmarks ===>
_
-
120 mg/L
1000 count per 100 mL
100 mg/L or 50 mg/L °
1
6/13/19
.3"
100
1330
160
2
6/13/19
.3"
75
1700
470
5B
6/13/19
.3"
32
1820
27
6B
6/13/19
.3"
15
186
18
7A
No Discharge
7C
6/13/19
.3"
11
287
6.6
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
" See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -
numerical format. When results are below the applicable limits, they must be reported in the format "<XX mg/L", where XX is the numerical value of the
detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX".
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
Permit Date: 11/1/2012-30/31/2017 SWU-248, last revised 10/25/2012
Page 1 of 2

n No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Non -polar O&G/TPH by
EPA 1664(SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__> _
-
- . -
15.mg/L
100 mg/L or 50 mg/L4
6.0= 9.0 SU
7B
6/13/19
.3"
1.50
8.5
6.35
Footnotes from Part A also apply to this Part B
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an oriainal and one copy of this DMR including all "No Discharge" reports within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware thay7hefe are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Permittee)
Permit Date: 11/1/2012-10/31/2017
%-1- 9
(Date)
SWU-248, last revised 10/25/2012
Page 2 of 2

ENCO Laboraton*es
Acairate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Tuesday, June 25, 2019
Republic Services of NC (RE014)
Attn: Brian Scott
500 Landfill Road
Mt. Gilead, NC 27306
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Uwharrie Stormwater
ENCO Workorder(s): CC09910
Dear Brian Scott,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, June 13, 2019.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me
Sincerely,
Stephanie Franz
Project Manager
Enclosure(s)
FIND 4 is report relates only to [Fe sample as received by the labwetory, and may only be repreEoxM in full. Page 1 Of l U

E�ICO
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SAMPLE SUMMARY/LABORATORY
CHRONICLE
Client ID: Outfall#1
Lab ID: CCO9910-01
Sampled: 06/13/19 08:50
Received: 06/13/19
12:25
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(S)
Analysis Date/Time(s)
SM 254OD-2011
NO PREP
06/20/19
06/14/19 12:21
06/14/19 12:21
SM 5220D-2011
Same
07/11/19
06/21/19 08:08
06/21/19 11:41
Client ID: Outfall#2
Lab ID: CCO9910-02
Sampled: 06/1311909:00
Received: 06113/1912:25
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
SM 254OD-2011
NO PREP
06/20/19
06/14/19 12:21
06/14/19 12:21
SM 52200-2011
Same
07/11/19
06/21/19 08:08
06/21/19 11:41
Client 10: Outfall #58
Lab ID: CC09910-03
Sampled: 06/13/19 08:40
Received: 06/13/19
12:25
Parameter
Preparation
Holtl Date/Time(s)
Preo Date/Time(s)
Analysis Date/Time(sl
SM 2540D-2011
NO PREP
06/20/19
06/14/19 12:21
06/14/19 12:21
SM 5220D-2011
Same
07/11/19
06/21/19 08:08
06/21/19 11:41
Client ID: Outfall#68
Lab ID: CC09910-04
Sampled: 06/13/19 09:10
Received: 06/13/19
12:25
Parameter
Preparation
Hold Date/Time(s)
Preo Date/Tme(s)
Analysis Date/Time(s)
SM 2540D-2011
NO PREP
06/20/19
06/14/19 12:21
06/14/19 12:21
SM 522OD-2011
Same
07/11/19
06/21/19 08:08
06/21/19 11:41
Client ID: Outfall#7C
lab ID: CCO9910-05
Sampled: 06/13/19 09:35
Received: 06/13/19
12:25
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
SM 2540D-2011
NO PREP
06/20/19
06/14/19 07:16
06/14/19 07:16
SM 522OD-2011
Same
07/11/19
06/21/19 08:08
06/21/19 11:41
Client ID: Outfall#78
lab ID: CC09910-06
Sampled: 06/13/19 09:35
Received: 06/13/1912:35
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analy55 Date/Time(s)
EPA 1664A
EPA 1664A
07/11/19
06/21/19 15:58
06/25/19 15:18
Field
NO PREP
06/13/19 09:49
06/13/19 09:35
06/13/19 09:35
SM 2S40D-2011
NO PREP
06/20/19
06/14/19 07:16
06/14/19 07:16
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in fun. I Page 2 of f 0

v .encolabs.com
SAMPLE DETECTION SUMMARY
Client ID: Outfall #1
Lab ID:
CC09910-01
Analyte
Results
E199
MPL
SL
tOlts
Metuid Notes
Chemical Oxygen Demand
100
10
10
mg/L
SM 5220D-2011
Total Suspended Solids
160
25
25
mg/L
SM 254OD-2011
Client ID: Outfall #2
Lab ID:
CC09910-02
Analyte
Results
flag
MQ6
M
VAUE
Method Notes
Chemical Oxygen Demand
75
10
10
mg/L
SM 5220D-2011
Total Suspended Solids
470
50
50
mg/L
SM 254OD-2011
Client ID: Outfall #58
Lab ID:
CC09910-03
Anal YLe
Results
EWA
MPS
EQL
vam
Method Notes
Chemical Oxygen Demand
32
10
10
mg/L
SM 5220D-2011
Total Suspended Solids
27
6.8
6.8
mg/L
SM 254OD-2011
Client ID: Outfall #66
Lab ID:
CC09910-04
Anal vte
Results
flag
MPS
CQL
Units
Method Notes
Chemical Oxygen Demand
15
10
10
mg/L
SM 522OD-2011
Total Suspended Solids
18
3.8
3.8
mg/L
SM 2540D-2011
Client ID: Outfall #7C
Lab ID:
CC09910-05
ADaffis
Results
Ewa
MPL
E"
yam
Method Notes
Chemical Oxygen Demand
11
10
10
mg/L
SM 5220D-2011
Total Suspended Solids
6.6
3.2
3.2
mg/L
SM 254OD-2011
Client ID: Outfall #70
Lab ID:
CC09910-06
ADahQe
Results
Flag
MDL
P-4S
Wu
Method Notes
pH
6.4
0.0
0.0
pM Units
Field
Total Suspended Solids
8.5
3.7
3.7
mg/L
SM 254OD-2011
FIND This iepon relates only to the ample as received by the lalmmtory, and may only be mcmdmed in full. Pdge 3 Of 1 O

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ANALYTICAL RESULTS
Description: Outfall #1 Lab Sample ID:CC09910-01 Received: 06/13/19 12:25
Matrix: Water Sampled: 06/13/19 08:50 Work Order: CC09910
Project: Uwharrie Stormwater Sampled By: Brian 3 Scott
(Classical Chemistry Parameters
^-EACDCao caori .w41e1AC 5911
Analyte rCAS Numberl Results Flap Yn& Pi ma P4L llatch Method Analyzed py Notes
Chemical Oxygen Demand^ 100 mg/L t 10 10 91`21002 SM 522OD-2011 06/21/19 11:41 30C
Total Suspended SolidsA 160 mg/L 10 25 25 9F14032 SM 254OD-2011 06/14/19 12:21 LG
Description: Outfall #2 Lab Sample ID:CC09910-02 Received: 06/13/19 12:25
Matrix: Water Sampled: 06/13/19 09:00 Work Order: CCO9910
Project: Uwharrie Stormwater Sampled By: Brian 3 Scott
(Classical Chemistry Parameters
^ - EN CU grenorWarvlyw(AC 5911
Analyte KAS Numberl Results fan Units PE MDL e4L Batch Melho9 Analyzed By Motes
Chemical Oxygen DemandA 75 mg/L 1 10 10 9F21002 SM 5220D-2011 06/21/19 11:41 30C
Total Suspended SolidsA 470 mg/L 20 50 50 9F14032 SM 2540D-2011 06/14/19 12:21 LG
Description: Outfall #5B Lab Sample ID:CC09910-03 Received: 06/13/19 12:25
Matrix: Water Sampled: 06/13/1908:40 Work Order: CC09910
Project: Uwharrie Stormwater Sampled By: Brian 3 Scott
IClassical Chemistry Parameters
^ -EACD CaryoNiircb aruNre (AC 591]
Anahne rCAS Numbed Resuli5
Flap Units
PE MPL FPS Batch
Method
Analyzed JC Notes
Chemical Oxygen DemandA
32
mg/L
1 10 10 9F21002
SM 5220D-2011
06/21/19 11:41 30C
Total Suspended Solids-
27
mg/L
2.7 6.8 6.8 9F14032
SM 2540D-2011
06/14/19 12:21 LG
Description: Outfall #6B
Lab Sample ID:CC09910-04
Received: 06/13/19 12:25
Matrix: Water
Sampled: 06/13/19 09:10
Work Order: CCO9910
Project: Uwharrie Stormwater
Sampled By: Brian 3 Scott
Classical Chemistry Parameters
^ - EACl7 Cary re OfieO arialyre [AC 591/
Analarte rCAS Numberl Results
F39 1111AE
PE MPS PPL Batch
Method
Analyzed Py Notes
Chemical Oxygen DemandA
15
mg/L
1 10 10 9F21002
SM 522OD-2011
06/21/19 11:41 30C
Total Suspended SolidsA
18
mg/L
1.5 3.8 3.8 91`14032
SM 254OD-2011
06/14/19 12:21 LG
Description: Outfall #7C
Lab Sample ID:CC09910-05
Received: 06/13/19 12:25
Matrix: Water
Sampled: 06/13/19 09:35
Work Order: CCO9910
Project: lwharne Stormwater
Sampled By: Brian 3 Scott
Classical Chemistry Parameters
^-EA'Nfaryreror arvlyre(AC 5911
Analyte rCASNumberl Results
f3ag Units
PE MS Ell Batch
Heth49
Analyzed @y Notes
Chemical Oxygen DemandA
11
mg/L
1 10 10 9F21002
SM 5220D-2011
06/21/19 11:41 30C
Total Suspended SolidsA
6.6
mg/L
1.26 3.2 3.2 9F14001
SM 254OD-2011
06/14/19 07:16 LG
FIND This report relates only to the sample as na eave] W be laboratory, and may only t mpiotloretl in full. Page 4 Of 10

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ANALYTICAL RESULTS
Description: Outtall #7B Lab Sample ID:CC09910-06 Received: 06/13/19 12:25
Matrix: Water Sampled:06/13/19 09:35 Work Order: CC09910
Project: Uwharne Stormwater Sampled By: Brian I Scott
Classical Chemistry Parameters
^-E Caryce,VwadawfA 591/
Analyte ICAS Numbed ResuILS
flag llniti
PE
MP6
PZ
Batch Method Analysed
By Notes
Total Suspended Solids- 8.5
mi
1.47
3.7
3.7
9F14001 SM 2540D-2011 06/14/19 07:16
LG
Field Parameters
Analyte ICAS Numberl Results
Elan Units
PE
MpS
POL
al Method Analysed
By Notes
pN 6.4
PH Units
1
0.0
0.0
9F14004 Field 06113/1909:35
CLI
Classical Chemistry Parameters
Analyte rCAS Numberl
Oil is Grease (HEM) [C-0007]
Results EWA Units PE MPL PPL Batch Method Analyzed & Notes
1.50 U m0/L 1 1.50 5.00 9F21011 EPA 1664A 06/25/19 15:18 SMA
FINAL
This report relates only to the sample as received by the laborutorv, and may only be reproduced In hll I Page 5 Of 1O

�co
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9F14001 - NO PREP
Blank (9F14001-BLKI) Prepared & Analyzed: 06/14/2019 07:16
Spike Source %REC RPD
Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes
Total Suspended Solids 2.5 u 2.5 ml
LCS (911`14001-BSI) Prepared & Analyzed: 06/14/2019 07:16
Spike Source %REC
RPD
.Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Suspended Solids
93
2.5
mg/L
100 93 80-120
Duplicate (9F14001-DUPl)
Prepared & Analyzed: 06/14/2019 07:16
Source: CCOSS43-01
Spike Source %REC
RPD
.Ana Me
Result Foo
POL
Units
Level Result %REC Limits RPD
Limit Notes_
Total Suspended Solids
210
45
mg/L
230 6
20
Duplicate (9F14001-DUP2)
Prepared & Analyzed: 06/14/2019 07:16
Source: CC07678-01
Spike Source %REC
RPD
.Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Limit Notes
Total Suspended Solids
300
140
mg/L
280 8
20
Batch 91- NO PREP
Blank (9F14032-BLK1)
Prepared & Analyzed: 06/14/2019 12:21
Spike Source %REC
RPD
_Analvte
Result Flag
POL
Units
Level Result %REC Limits RPD
Ljralt Notes
Total Suspended Solids
2.5 u
2.5
m9/L
LIES (9111
Prepared &Analyzed: 06/14/2019 12:21
Spike Source %REC
RPD
AnaPzte
Result
Flag
POL
Units
Level Result %REC Limits
RPD
Lurk Notes
Total Suspended Solids
92
2.5
rail
100 92 80-120
Duplicate (9F14032-DUPI)
Prepared & Analyzed: 06/14/2019 12:21
Source: CCOSS44.01
Spike Source %REC
RPD
.Analvte
Result
Flag
POL
Units
Level Result %REC Limits
RPD
Limit Notes
Trial Suspended Solids
170
42
mg/L
180
5
20
Duplicate (9F14032-DUP2)
Prepared & Analyzed: 06/14/2019 12: 21
Source: CCO9922-01
Spike Source %REC
RPD
Analvte
Result
Flag
P-0L
Units
Level Result %REC Limits
RPD
LAIMI Notes
Tool Suspended Solids
56
20
mg/L
30
62
20 QM-12
Batch 9F21001- Same
Blank (9F21002-BLKl)
Prepared: 06/21/2019 08:08 Analyzed: 06/21/2019 11:41
Spike Source %REC
RPD
Analvte
Result
Flag
ROL
Units
Level Result %REC Limits
RPD
kjmjt [Cotes
Chemical Oxygen Demand
10
U
10
mi
FINAL This report relates only M the sample as received by the laboratory, aM may only be reproduced in full. I Page 6 Of 1 U

FJVCO
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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9F21002 - Same - Continued
LCS (91`23002-861)
Prepared: 06/21/2019 08:08 Anawed: 06/2112019 11:41
Spike Source %REC
RED
Analyte
Result Flag
ROL
Units
Level Result %REC Limits RPD
11131ft Notes_
Chemical Oxygen Demand
480
10
mg/1-
Soo 97 90-110
Matrix Spike (9F21002-MS3)
Prepared: 06/21/2019 08:08 Analyzed: 06/21/2019 11:41
Source: CCO2666-01
Spike Source %REC
RPD
_Analvte
Result Flaa
ROL
Units
Level Result %REC Limits RPD
Limit Notes
Chemical Oxygen Demand
530
10
mg/L
526 19 97 90-110
Matrix Spike Dup (9F21002-MSD1)
Prepared: 06/21/2019 08:08 Analyzed: 06/21/2019 11:41
Source: CCO2666-01
Spike Source %REC
RPD
.Analyte
Result Flao
ROL
Units
Level Result %REC Limits RPD
Limit Notes
Chemical Oxygen Demand
540
10
mg/L
526 19 99 90-110 1
10
Classical Chemistry Parameters - Quality Control
Batch 9F21011 - EPA 1664B
Blank (9F21011-BLKI)
Prepared: 06/21/2019 15:58 Analyzed: 06/25/2019 15:18
Spike Source %REC
PRO
Analyte
Result Flag
ROL
Units
Level Result %REC Limits RPD
UnIft Notes
Oil & Grease (HEM)
1.50 U
5.00
ng/L
LCS (9F21011-BS1)
Prepared: 06/21/2019 15:58 Analyzed: 06/25/2019 15:18
Spike Source %REC
RPD
_Analyte
Result Flag
ROL
Units
Level Result %REC Limits RPD
Limit Notes
Oil & Grease (HEM)
141
5.00
mg/L
157 90 78-114
LCS pap (9F21011-BSD1)
Prepared: 06/21/2019 15:58 Analyzed: 06/25/2019 15:18
Spike Source %REC
RPD
Analvte
Result Flag
ROL
Units
Level Result %REC Limits RPD
Limit Notes
Oil & Grease (HEM)
145
5.00
mg/L
160 90 78-114 3
18
Matrix Spike (9F21011-MSI)
Prepared: 06/21/2019 15:58 Analyzed: 06/25/2019 15:18
Source: BCO2554-01
Spike Source %REC
RPD
. Analvte
Result Flag
ROL
Units
Level Result %REC Limits RPD
Lir 11 Notes -
Oil & Grease (HEM)
121
5.00
mg/L
148 1.50 U 82 78-114
FINAL This report relates only to Me sample as receiveu try Me laeoratory, and may only re reproduceol in full, Page % Of O

F. N64co
www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
7 The reported value is between the laboratory method detection limit (MDQ and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification'.
Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDUMRL reported to the highest reporting limit of the component analyses.
QM-12 Precision between duplicate samples was outside acceptance limits.
FIND This report mWtes only to the sample as r eiveal try the lac 1:0ry, anal may anly as reprmu:ed in fun. I Page 8 of 10

WHIECEE:10 IM5C ....._.....- --..__...I..._.. ---...,
lOTlS Central Port Dr. 4810 Exewdva Perk Coun, Sufte 1 t i I M-/. Woodxintle IMusirial Ct.
DdaMp. FL 3 II24 daclawrma., FL 02218ae69 Cary, NC 27511 I
(mr7) W6-W14 Fax [phone] (9 ) 2W=17 Fax (904) 29E6210 [phone] Fax [phone] Page _!— of
O
Cited Name
Prgecl Number
Re,e
tell
Analyses
Requested Turnarou13
Republic Services of NC (RE014)
[none]
Times
rn
Note: Rmh rNuesis subjel al
Atltlress
Project Nam&Vew
500 Landfill Road
Uwharrie Stormwater
acrntetn—by ft wt5 CO
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Standard
QIY/STRip
Mt. Gilead, NC 27306
PO e / Bilm Into
2014:
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Tel
[phone]
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Brian Scott
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Sample ID (Field IdentilicatoN
Qate
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(see wriest
Containers
utfall
WA
6
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Outfall #
WA
6
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yp
WA
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/
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Received BY
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,{V//,3
C J +� YTL_W \•
Tenqu an Receip r
Cm49on Upon Receipt
✓_!Acceptable _Unacceptable
_ _ _
MetrIx:GWfiramC. afar SO-Sotl DW Onngn9 water slseapnml aw-burmwwww vw--. uwam'.....�,.....I'll %11--....... -•r...—....... ..__...._......____.__-
We: AD samples suNmi W W ENCO Lena we n eLCMdallLe wib Ne twNa erfd wlMtliona fated w ttb m m of IN, bN% ereese Prior unto.^ a9menrenta exist

Sample Preservation Verification
ENCO Cary
Work Order: CCO9910
Client: Republic Services of NC (RE014)
I Nil;CIO'
Project: Uwharrie Stormwater
Project #: (none]
Logged In: 13-Jun-19 12:50 �,� Logged By: John C King
I Preservation Check Performed By: f Dateffime: (L13-/2' /--S
CC09910-01
Cont`
II
Y'
T pe
Pres(pH)
Requirement.
pHChecked/
: In Control
---Date/Tme
pH.Adjusted Adjusted -
Reagent Used/Comments
B
250mLP+H2SO4
<2
Y / N / NA
I Y / N / NA
CCO9910-02
Cont.
Type
Pres (pH)
Requirement
pH Checked /
� In Control
. DateMme
Adjusted pH Adjusted
Reagent Used/Comments
B
250mLP+H2SO4
<2
Y/ N/ NA
I Y/ N I NA
CC09910-03
Cont
•^
T pe
Pres(pH)
Requirement
pH,CheckedL
-'InControl_'
�- DateTme _
pH Adjusted
„Adjusted
Reagent Used/Comments "
.,. ":.
B
250mLP+H2SO4
1 <2
Y N / NA
I Y / N / NA
CC09910-04
Cont
Type
Pres (pH)
Requirement
pH C .ecke /,
, In Control
...pl- Adjusted DateRme
.. -. Adjusted
Reagent Used/Comments '
. , .
B
250mLP+H2SO4
<2
/ N/ NA
I Y I N I NA
CCO9910-05
Cont
T pe- '..
,y _
PrespH
_Requirement.
Checked
+�In�Control
G*
- DateMme
pH Adjusted -
_ , , ,. .Adjusted
I
Reagent Used/Comments ' f
_
B
250mLP+H2SO4
<2
Y� / N / NA
Y / N / NA
CC09910-06
Cont;
Type
Pres.(pH)
Requirement
pH Checked t
- In Control
pH Adjusted DateMme
Adjusted
Reagent Used/Comments
C
250m1-A+H2SO4
<2
YIN /
Y ! N /
D
250mLA+H2SO4
<2
Y/ N/ ti�� l
Y! N/
E
250m1-P+H2SO4
<2
Reacent Name ID
1
2
pH Strip ID:
C:\ELMNT\Print\wko—PreservationCheck.rpt
Reagent Name ID Rea ent Name ID
3 1 5
4 6
Page 10 of 10
age 1

aceAnalytical
..pecelabLoar,
June 19, 2019
Ms. Stephanie Franz
ENCO Labs
102 A-Woodswinds Industrial Co
Cary, NC 27511
RE: Project: CCO9910
Pace Project No.: 92432982
Dear Ms. Franz:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvdle, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on June 13, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sarah Graham
[e-mail]
[phone]
Project Manager
Enclosures
cc: Chuck Smith, ENCO Labs
ACCRpO�
REPORT OF LABORATORY ANALYSIS
1Nt This report shall not be reproduced, except in full,
-� without the written consent of Pace Analytical Services, LLC. Page 1 of 14
BTAW ,

laceAnalytical'
www.pacelaas.ccnt
Project: CC09910
Pace Project No.: 92432982
Raleigh Certification IDS
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 14

ace Analytical"
wimpacalabs.rom
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
CC09910
92432982
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92432982001
Outfall #1
SM
9222D-2006
VVT
1
PASI-R
92432982002
Outfall #2
SM
9222D-2006
VVT
1
PASI-R
92432982003
Outfall #5B
SM
92220-2006
VVT
1
PASI-R
92432982004
Ouffall #68
SM
9222D-2006
VVT
1
PASI-R
92432982005
Outfall #7C
SM
922213-2006
VVT
1
PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wrinen consent of Pace Analytical Services, LLC. Page 3 of 14

laceAnalyfical"
w Pacelabs.com
ANALYTICAL RESULTS
Project: CC09910
Pace Project No.: 92432982
Pace Analytical Services, LLC
9800 Kul Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Outfall #1 Lab ID: 92432982001 Collected: 06/13/19 08:50 Received: 06/13/19 13:29 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform RAL
Fecal Coliforms
Date: 06/19/2019 02:33 PM
Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
1330 CFU/100 mL 1.0 1 06/13/19 15:49 06/14/19 14:19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the whiten consent of Pace Analytical Services, L-C.
Page 4 of 14

(�15?eAnalyfical'
~..pacafaesi
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: CCO9910
Pace Project No.: 92432982
Sample: Ouffall #2 Lab ID: 92432982002 Collected: 06/13/19 09:00 Received: 06/13/19 13:29 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual
MB10 9222D Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
Fecal Coliforms 1700 CFU/100 mL 1.0 1 06/13/19 15:49 06/14/19 14:19
Date: 06/19/2019 02:33 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 14

(�55?eAnail
a+`w.Pscelebxcan
ANALYTICAL RESULTS
Project: CCO9910
Pace Project No.: 92432982
Pace Analytical Services, LLC
9800 oncey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Sample: Outfall #5f3 Lab ID: 92432982003 Collected: 06/13/19 08:40 Received: 06113/19 13:29 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
M610 9222D Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
Fecal Coliforms 1820 CFU/100 mL 1.0 1 06/13/19 15:49 06/14/19 1419
Date: 06119/2019 02:33 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 14

ace Analytical
w wpawlaes.com
ANALYTICAL RESULTS
Project: CCO9910
Pace Project No.: 92432982
Pace Analytical Services, LLC
9800 Ki ncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Outfall #6B Lab ID: 92432982004 Collected: 06/13/19 09:10 Received: 06/13/19 13:29 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method SM 9222D-2006
Fecal Coliforms 186 CFU/100 mL 1.0 1 06/13/19 15:49 06/14/19 14:19
Date: 06/19/2019 02:33 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, U.C.
Page 7 of 14

laceAnalyfical*
~pacelaes.co n
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Ki ncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: CCO9910
Pace Project No.: 92432982
Sample: Outfall VC Lab ID: 92432982005 Collected: 06113/19 09:35 Received: 06/13119 13:29 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
Fecal Coliforms 287 CFU/100 mL 1.0 1 06/13/19 15:49 06/14/19 14:19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/1912019 02:33 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14

lace Analytical"
~p8wisits.com
QUALITY CONTROL DATA
Project: CCO9910
Pace Project No.: 92432982
OC Batch: 481916 Analysis Method: SM 9222D-2006
QC Batch Method: SM 92220-2006 Analysis Description: 9222D Fecal Coliform(MF) - RAL
Associated Lab Samples: 92432982001, 92432982002, 92432982003, 92432982004, 92432982005
METHOD BLANK: 2606145 Matrix: Water
Associated Lab Samples: 92432982001, 92432982002, 92432982003, 92432982004, 92432982005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 06/14/19 14:19
SAMPLE DUPLICATE: 2606146
Parameter
Fecal Coliforms
92432982001 Cup
Units Result Result RPD Qualifiers
CFU/100 mL 1330 1520 13
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 02:33 PM without the written consent of Pace Analytical Services, L-C.
Page 9 of 14

(�Ia?eAnalyficale
~..pacelaa.9.00n1
QUALIFIERS
Project: CC09910
Pace Project No.: 92432982
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
POL- Practical Ouantitation Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-R Pace Analytical Services - Raleigh
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/19/2019 02:33 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14

ace Analytical
w pecelebs.corn
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
CCO9910
92432982
Analytical
Lab ID
Sample ID
QC
Batch Method
QC Batch
Analytical Method
Batch
92432982001
Outfall #1
SM
9222D-2006
481916
SM
9222D-2006
481917
92432982002
Outfall #2
SM
9222D-2006
481916
SM
9222D-2006
481917
92432982003
Outfall #5B
SM
9222D-2006
481916
SM
9222D-2006
481917
92432982004
Outfall #6B
SM
9222D-2006
481916
SM
9222D-2006
481917
92432982005
Ouffall #7C
SM
9222D-2006
481916
SM
9222D-2006
481917
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/19/2019 02:33 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 14

Document Name:
Document Revised: Februery7, 2018
Sample Conglt!on Upon Racei t SLUR
Page 1 of2
`,H
.. BCBAR2ij�lCBir
Document No.:
Issuing Authority:
F-CAR-CS-033•Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville 0 Eden[] Greenwood [� Huntersville ❑ Raleigh Mechanicsville[]
MEMO Client Name: chfu
Courier. ffFEXq: EJUPSi❑
Custody Seal Present? ❑Yes 1*0 Seals Intact?
❑Yes ❑No
Packing Material: []Bubble Wrap []Bubble Bags lone❑ Other
Thermometer: Type of Ice: 0�at ❑slue
❑R Gun ID: 1
Cooler Tamp ('C): 2 Correction Factor Add/Subtract (°C) _o r I
Cooler Temp Corrected ("Q:
USDA Regulated Soll (Z N/A, water sample(
Did samples orlginate Ina quarantine zone within the United States: CA, NY, at SC (check maps)?
W,o 92432982
W13)iI
DataQnitlab Person Examining Contents:
Biological Tissue ten?
❑Yes []NoNJA
QNona
Temp should be above freezing to 6'C
samples out of temp cdteAa, Samples or ice, cooling process
hosbegun
Did samples odglnate from a foreign source (internadonaCy,
Yes No
'-
......... _. _.
Comments/DisWe arty:
Chain of Custody Present?
ENOQN/ASam
les Arrived within Hold EHAYi-
ON/A
2.
Short Hold Time Analysis (<7
I]N
N/A
3.
Rush Turn Around Time Requested?
Y
No
N/A
4.
Sufficient Volume?
Y
No
ON/A
S.
Correct Containers Used7
-Pace Containers Used?
y
ONO
N.
[IN/A
❑N/A
G.
Containers intact?
Yes
No
[]Nbe
7.
Dissolved analysls: Samples Field Filtared7
Y
LIN.
N/A
g.
Sample labels Match COL?
-Includes Date/rme/ID/Ana sls Metrls:
Headspace In VOA Vials(>S-Gmm?
Trip Blank Present?
Trip Blank Custody Seals Present)
JZYO,
QYes
❑Yes
Yu
❑No
EJ
[INo
No
ON/A
N/y
N/A
9.
10.
IS.
COMMENTS/SAMPLE DISCREPANCY
Lot lO of litcontalners:
CUENT NOTIFICATION/RESOLUTION
Field Data R4quired7 ❑Yes ❑No
Person contacted: Date/Time.:
Project Manager SCURF Review. Data:
Project Manager SRF Review: •'et""-- Date: 6 4 O _/ Page 12 of 14

Document Name:
Document Revised: February 7, 2018
Same la Condition Upon Recei t SCUR
Page 1 of 2
Document No.;
IssolnBAtRhDriry:
r .• C9Analyttal°
F-CAR-Rev 06
Pare CaMifnas Quality Office _
*Check mark top half of box If pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exception VOA, Collfurm, Tor Oil and Grease, OR018015 (water) DOC, LLHg
"Bottom half of box Is to list number of bottle
Project H
W®#:92432932-
PM: SMG Dow Date: 06/24/19
CLIENT: 92—ENCO
+p
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2
1
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3
1
6
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6
7
B
9
10
u
12
pH Adjustment Log for Preserved Samples
th
Sample l0
Type of Preservadve
PH upon receipt
Oate prmervatien adjusted
Time presermUon
adjusted
Amount of preservative
added
Lot
.. . __ _ ___. _,.u.._.....dn
........,.
u..n�. r....n.., ncuuv r.nM.ethn
Mnca LLe.
Note: W henaver mere b a dlSCrepUCy arra Cang Norm Ca rain..1oPnncn .uu�w=•• • "wr `^ •^•' •-•-• -'- -- -- - -- - �.
out of hold, Incorract preservative, out of temp. incorrect containers. Page 13 of 14

SUBCONTRACT ORDER
ENCO Cary
CCO9910
SFNOTNG LABORATORY: RECEIVING LABORATORY:
ENCO Cary Pace Analytical (NC) L{q 1 5
102-A Woodwinds Industrial Court 2225 Riverside Drive `J1 -r-�-� l2d V
Cary, NC 27511 Asheville, NC 28804
Phone: [phone] Phone: -
Fax: [phone] Fax: -
-projeaenager; StephanleFranz Proiiect State of Origin• North Carolina
4
r I_ 5 gt 'hzi II ;y��� �(i;l�lf
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1 11
Containers Supplied:
Outfall #2
Water 13-Jun-19 09:00
J
d,,
—
Colifonn, Fecal 9223B
1 '
Containers Supplied:
Steritemornu+Nalbio
Outfall#5B Water 13Jun-1908:40
Colifonn, Fecal9223B 20-Jun49 15:00 13-Jun-1916:35
Containers Supplied:
Steri1e250rnLP+NMio (C)
Gfc�.�. 1�. jallii�, v� I'�:.41n �•Iti r Ii'::.J.r...: �(�llk:.J ln; ii �.i�lu.�I.L �iM yil L�{L4��T���'.AId:I151���i�.Y'�16�1_��II
1 11 1
Containers Supplied:
Outfall #7C Water 134un-19 09:35
Coliform, Fecal9223B 20-Jun-19 15:00 13-tun-19 17:30
Containers Supplied:
14

ZeAnalytical"
j www.peceleos.com
i
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: CCO9910
Pace Project No.: 92432982
Sample: Outfall #2 Lab ID: 92432982002 Collected: 06/13/19 09:00 Received: 06/13/19 13:29 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
Fecal Coliforms 1700 CFU/100 mL 1.0 1 06/13/19 15:49 06/14/19 14:19
Date: 06/19/2019 02:33 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 14

aceAnaiytical
www.perolabs.com
ANALYTICAL RESULTS
Project: CCO9910
Pace Project No.: 92432982
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Outfall #5B Lab ID: 92432982003 Collected: 06/13/19 08:40 Received: 06/13/19 13:29 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual
MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method: SM 92220-2006
Fecal Coliforms 1820 CFU/100 mL 1.0 1 06/13/19 15:49 06/14/19 14:19
Date: 06/19/2019 02:33 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 14

ace Analytical
www.pacalaDs.com
ANALYTICAL RESULTS
Project: CCO9910
Pace Project No.: 92432982
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Outfall #66 Lab ID: 92432982004 Collected: 06/13/19 09:10 Received: 06/13/19 13:29 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
Fecal Coliforms 186 CFU/100 mL 1.0 1 06/13/1915:49 06/14/19 14:19
Dale: 06/19/2019 02:33 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. LLC.
Page 7 of 14

aceAnalytical
� www.peceleCs mm
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: CCO9910
Pace Project No.: 92432982
Sample: Outfall #7C Lab ID: 92432982005 Collected: 06113/19 09:35 Received: 06/13/19 13:29 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform RAL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
Fecal Coliforms 287 CFU/100 mL 1.0 1 06/13/19 15:49 06/14/19 14:19
Date: 06/19/2019 02:33 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, U.C.
Page 8 of 14

2ceAnalytica1
/ www.pacelabs.rom
I
QUALITY CONTROL DATA
Project: CCO9910
Pace Project No.: 92432982
QC Batch: 481916 Analysis Method: SM 9222D-2006
QC Batch Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF) - RAL
Associated Lab Samples: 92432982001, 92432982002. 92432982003, 92432982004, 92432982005
METHOD BLANK: 2606145 Matrix: Water
Associated Lab Samples: 92432982001, 92432982002, 92432982003, 92432982004, 92432982005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 06/14/19 14:19
SAMPLE DUPLICATE: 2606146
92432982001 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms CFU/100 mL 1330 1520 13
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the fight of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/19/2019 02:33 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 14

aceAnalytical
t www.pacalebs.cwn
QUALIFIERS
Project: CC09910
Pace Project No.: 92432982
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Ki ncey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-R Pace Analytical Services - Raleigh
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/19/2019 02:33 PM without the wntten consent of Pace Analytical Services, U.C. Page 10 of 14

aceAnalytical.
/ w»wpecelaDs.cwn
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
CCO9910
92432982
Analytical
Lab ID
Sample ID
QC
Batch Method
QC Batch
Analytical Method
Batch
92432982001
Outfall #1
SM
9222D-2006
481916
SM
922213-2006
481917
92432982002
Outfall #2
SM
9222D-2006
481916
SM
9222D-2006
481917
92432982003
Outfall #5B
SM
9222D-2006
481916
SM
9222D-2006
481917
92432982004
Outfall #6B
SM
9222D-2006
481916
SM
9222D-2006
481917
92432982005
Outfall VC
SM
9222D-2006
481916
SM
9222D-2006
481917
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Dale: 06/19/2019 02:33 PM without the written consent of Pace Analytical Services, LLC, Page 11 of 14

Document Name:
Document Revised: February 7, 2018
Sample Condition U on Racei t SCUR
Pa e 1 oft
' ,.� 8C8M2JyUC&I
Document No.:
Issuing Authority:
FdAR-CS•033•Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersvi(le ❑ Raleigh Mechanicsville❑
Is• Client Name: IWl�rd� 2�432992
Courier: P�ed& E1UPSJ ❑USPS yclient �11II®II`1 nII—
D CgmrnindI �Btl er
,._,/j 922992
Custody Seal Present? []YesCyrN Seals Intact? []Yes []No •t (p01 (l
Onte/InRWIa Person EvaminlnY Contrnts:, s�
Packing Material: []Bubble Wrap . ❑Bubble Bags [lone ❑ Other Biological Tissue zen?
[]Yes []No N(A
Thermometer:
Type of Ice: 21Net []Blue ❑None
❑ III Gun ID: _
Cooler Temp ('C): 1Q. Correctfon Factor: Add/Subtract (•C) �'Q •,
Temp should be above 1'eezing to CC
Cooler Temp Corrected ('C): ❑Sampler out of temp cd[eda. samples on to, cooling process
hasbegun
USDA Regulated Soll ( N/A, water sample)
Did same originate
lee In quarantine zone within the United States: CA NY of SC (check maps)? Old samples originate from a foreign source (nternatlonagy,
Yes No including Hawaii and Puerto RIcoJ7 ❑Yes ❑No
—"" Camments/Discre ancy:
Chain of Custody Present? Y Na N/A I.
Sam les Arrived within Hold Time? V No ❑WA 2. x --
Shad Hold Time Analysis (<71 hr.)? dy. ON EINIA 3.
Rush Turn Around Time Requested? No N/A 4.
sufficient Volume? Y No ❑N/A 5.
Correct Containers Used? ❑Na (ZIN/A 6.
-Pace Containers Used? No []N/A
Containers Intact? Yes ON.
N 7. .
Dissolved analysis: Samples Field Filtered? Y No N/A a. _
Sample Labels Mauh COC7 Yes [IN. ❑N/A 9.
-Includes Date/rime/ID/Analysis matrix..
Trip Blank
In VOA Vials (>S-6mm)7 ❑yes No 11.
Trip Blank Present? ❑Yes QNo N/ 11.
Trip Blank Custody Seals Present? Yas ONO N/A
COMMENTS/SAMPLE DISCREPANCY
Field Data Required? []Yes []No
Lot ID cf split containers: '
WENT NOTIFICATION/RESOLUTION
Person contacted: _ _ Date/Time:
Project Manager SCURF Review: p�/ Date;
Project Manager SRF Review: Date:
Page 12 of 14
COMMENTS/SAMPLE DISCREPANCY
Field Data Required? []Yes []No
Lot ID cf split containers: '
WENT NOTIFICATION/RESOLUTION
Person contacted: _ _ Date/Time:
Project Manager SCURF Review: p�/ Date;
Project Manager SRF Review: Date:
Page 12 of 14

Dowment Name:
Document Revised: February 7, 2018
Sate le Condition Upon Receipt sCUR
Page 1 of 2
Document No.:
Issuing Authority:
r -• Genna�}mCai°
F-CAR-0-033-Rev 08
pace Carolina$ Quality Office -
'Check mark tap half of box If pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptlonr. VDA, Collform, TOC, Oil and Grease, DR018015 (water) DO(; LLHg
"Bottom half of box is to list number of bottle
Project k
WO# : 92432992-
PM: SM6 Due Date: 06/24/19
CLIENT: 92-ENCO
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pH Adjustment Log for Preserved Samples
Sample 10
Type of preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot g
Note: Whenever mere is a dfscrepancy affecting North Carolina campllanm samples, a ropy of thls form will be tent m tht No" Carolina OEHNR Cartlncatw Office p.e.
Out of We. Incorrect preservadva, a of tamp. inm rrect containers. Page 13 Of 14

SUBCONTRACT ORDER
ENCO Cary
CC09910 � Z �
3 Z 9Lqy Z
SENDING LABORATORY:
RECEIVING LABORATORY:
Analytical (NC)
I- t�ppn�
`-1 q 15 c4.o�z„`-'
ry ENCO Ca
Pace
102-A Woodwinds Industrial Court
2225 Riverside Drive
l2d
Cary, NC 27511
Asheville, NC 28804
Phone:[phone]
Phone:-
Fax: [phone] Prajeet Manag©r�StePhanfe-Fxa tz
—
Fax:-
project State Qf Origin'
North Carolina
Outfall #1 Watcr
Coliform, Fecal 9223B 20-Jun-19 15:00 134un-19 16:45
Containers Supplied:
Stcrilc250mLP+NaThio (C)
13-Jun-19 08:50
M'L� — Oatfa0H2 Water 13-Jun-1909:00
momm
Colifa m, Fecal 9223B 20-Jun-19 15:00 13-Jun-19 16:55
Containers Supplied:
Stcrile25omLP+NaThiu (C)
Outfall N6B Water
Coliform, Fecal 9223B 20-Jun-19 15:00 13-Jun-19 17:05
Containers Supplied.
Sterile250mLP+Ndl'hio (C)
13-Jun-19 09:10
Outfall #7C Water1
..�•yt4 '�" - i; eP-1R�:� �In'm'{ �y'i. 1 � Y{I}';G:Vv�'9 �.,.�l�J�lt��dl:�_glr,'^i :'�.�v Trr�1 ��11�1�7
Calif,Califortn, Fecal1
11 1
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