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HomeMy WebLinkAboutNCG100023_MONITORING INFO_20191112STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. 14C G 1 00 a DOC TYPE ❑ HISTORICAL FILE L MONITORING REPORTS DOC DATE ❑ 00 7 I I Q YYYYM M D D Mid Atlantic Engineering & Environmental Solutions October 10, 2019 NCDEQ/DWR Attention: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVE® NOV 12 2019 CENT RAL FILES DWR SECTION Subject: STORMWATER SAMPLING RESULTS M 8t M MOTOR COMPANY, INC. 9316 US HIGHWAY BUSINESS 220 NORTH RANDLEMAN, RANDOLPH COUNTY, NORTH CAROLINA PERMIT NUMBER NCGl00023 MID -ATLANTIC JOB NO. 00OR2005.00 To Whom It May Concern: 409 Rolm VlQW Court Raleigh, NC 27610 office 919.15D."1a 6a'mile 919.250.99S0 MAAONLINE.COM Attached please find the Stormwater Discharge Monitoring Report (DMR) and analytical report for the sampling conducted at the above -referenced site. Stormwater samples were collected from Outfalls 001, 002 and 003 on August 22, 2019 and analyzed for total suspended solids (TSS), pH, total recoverable lead and oil and grease. As indicated on the attached DMR, all parameters were reported below or within their respective benchmark values for all three outfalls. If you have any questions or need additional information, please contact me at 919-250-9918. Sincerely, MID -ATLANTIC ASSOCIATES, INC. Ron Davis Stormwater Services Manager Attachments: Stormwater Discharge Monitoring Report Laboratory Analytical Report EXPERIENCED CUSTOMER FOCUSED INNOVATIVE STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT CERTIFICATE OF COVERAGE NO. NCGl00023 FACILITY NAME M&M Motor Company, Inc., Randleman, NC PERSON COLLECTING SAMPLE(S) Heath McCaskill CERTIFIED LABORATORY(S) Pace Analytical Lab #12 Lab # Part A: Stormwater Benchmarks and Monitoring Results SAMPLES COLLECTED DURING CALENDAR YEAR:2019 COUNTY Randolph PHONE NO. (800) 441-3668 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 For sampling periods with no discharge, you must submit this discharge monitoring form noting "No Flow' or "No Discharge" within 30 days of the end of that period to comply with permit reporting requirements. Outfall No. Date Sample Collected, mo/dd/year Total Rainfall, inches 00400 00530 ---- 77023 01051 78141 pH, Standard Units Total Suspended Solids (TSS), mg/L Non -polar O&G/TPH (Method 1664 SGT-HEM), mg/L Ethylene Glycol, mg/L Lead, Total Recoverable, mg/L Total Toxic Organics3, mg/L Benchmark - - 6.0 — 9.01 100/502 15 8,000 (Tiers 2 and 3) 0.03 1.0 Outfall001 08/22/19 7.34 7.6 <4.9 <5.0 <0.005 NA Outfall002 08/22/19 7.48 8.0 <4.9 <5.0 <0.005 NA Outfall003 08/22/19 S 7.46 8.2 <4.9 <5.0 <0.005 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or I ter i responses in the Generai Permit. 1See If pH values outside this range are recorded in sampled stormwater discharges, but ambient precipitation PH levels are lower, then the lower threshold of this benchmark range is the PH of the precipitation (within instrument accuracy)instead of 6 S.U. Readings from an on -site or local rain gauge (or local precipitation data) must be documented to demonstrate background concentrations were below the benchmark pH range of 6-9. 2See General Permit text to identify whether the more protective benchmark applies for especially sensitive receiving waters. 3For purposes of this permit the definition of Total Toxic Organics is that list as stated in Appendix D, Table II of Chapter 40 Code of Federal Regulations (CFR) Part 122. Form SWU-251, last revised October 25, 2012 Page 1 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the discharger shall sign the following certification statement: Solvent Management Plan Certification Statement "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) Signature Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 MailServiceCenter Raleigh, North Carolina27699-1617 Date "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge a nd belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee or Designee) i-0 (Date) Form SWU-251, last revised October 25, 2012 Page 2 of 2 acmnalytical wewpecelab&= Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 September 05, 2019 Chuck Hoffman Mid -Atlantic Associates, Inc 409 Rogers View Court Raleigh, NC 27610 RE: Project: M&M Motor Company Pace Project No.: 92442796 Dear Chuck Hoffman: Enclosed are the analytical results for sample(s) received by the laboratory on August 26, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, i_ .< �� Illlllr Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Ron Davis, Mid Atlantic Associatees, Inc. *440RAWF REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 1 of 15 aceAnalytical w ..pscelaos.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: M&M Motor Company Pace Project No.: 92442796 Indiana Certification IDs 7726 Moller Road, Indianapolis, IN 46268 Illinois Certification #: 200074 Indiana Certification M C-49-06 Kansas/NELAP Certification #: E-10177 Kentucky UST Certification #: 80226 Kentucky WW Certification #: 98019 Michigan Department of Environmental Quality, Laboratory #9050 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification M E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Ohio VAP Certification #: CL0065 Oklahoma Certification #: 2018-101 Texas Certification #: T104704355 West Virginia Certification #: 330 Wisconsin Certification #: 999788130 USDA Soil Permit #: P330-16-00257 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 15 aceAnalytical e a vpawlos.cae Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: M&M Motor Company Pace Project No.: 92442796 Lab ID Sample ID 92442796001 Outfall No.1 92442796002 Outfall No.2 92442796003 Outfall No.3 SAMPLE ANALYTE COUNT Method Analysts Analytes Reported Laboratory EPA 16648 JMS 1 PASI-C EPA 8015 Alcohol -Glycol CPH 1 PASI-I EPA6010D DS 1 PAST -A SM 254OD-2011 NAL 1 PASI-A EPA 1664E JMS 1 PASI-C EPA 8015 Alcohol -Glycol CPH 1 PASI-I EPA 601 OD IDS 1 PASI-A SM 254OD-2011 NAL 1 PASI-A EPA 1664B JMS 1 PASI-C EPA 8015 Alcohol -Glycol CPH 1 PASI-I EPA6010D DS 1 PASI-A SM 254OD-2011 NAL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 15 aceAnalytical www.pemlebs.cwn Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: M&M Motor Company Pace Project No.: 92442796 Sample: Outfall No.1 Lab ID: 92442796001 Collected: 08/22/19 05:23 Received: 08/26/19 09:05 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg/L 4.9 1 08/29/19 06:18 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol NO mg/L 5.0 1 0812811919:05 107-21-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Lead ND ug/L 5.0 1 09/03/1919:03 09/0411917:26 7439-92-1 2540D Total Suspended Solids AnalyBcal Method: SM 2540D-2011 Total Suspended Solids 7.6 mg/L 2.6 1 08/29/19 10:46 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/05/2019 12:30 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 15 JoceAnalyficalo w ..paoelabs.cvrn Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)075-9092 ANALYTICAL RESULTS Project: M&M Motor Company Pace Project No.: 92442796 Sample: Outfall No.2 Lab ID: 92442796002 Collected: 08/22/19 05:38 Received: 08/26/19 09:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg/L 4.9 1 08/29/19 06:18 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg/L 5.0 1 08/28/19 18:46 107-21-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Lead ND ug/L 5.0 1 09/0311919:03 09104/1917:29 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 8.0 mg/L 2.6 1 08/29/19 10:46 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/05/2019 12:30 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 15 aceAnalytical e w ..pacelaes.mrn Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)075-9092 ANALYTICAL RESULTS Project: M&M Motor Company Pace Project No.: 92442796 Sample: Outfall No.3 Lab ID: 92442796003 Collected: 08/22/19 05:28 Received: 08/26/19 09:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg/L 4.8 1 08/29/19 06:19 8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol Ethylene glycol ND mg/L 5.0 1 08/28/19 18:56 107-21-1 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Lead ND ug/L 5.0 1 09/03/19 19:03 09/04/19 17:38 7439-92-1 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 8.2 mg/L 2.6 1 08/29/19 10:47 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/05/2019 12:30 AM without the written consent of Pace Analytical Services, L-C. Page 6 of 15 aceAnalytical wawpace/abs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: M&M Motor Company Pace Project No.: 92442796 QC Batch: 495072 Analysis Method: EPA 1664B QC Balch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92442796001, 92442796002, 92442796003 METHOD BLANK: 2667482 Matrix: Water Associated Lab Samples: 92442796001, 92442796002, 92442796003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L NO 4.8 08/29/19 06:09 LABORATORY CONTROL SAMPLE: 2667483 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 19.2 19.5 101 64-132 MATRIX SPIKE SAMPLE: 2667484 92442234002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L NO 19.2 20.0 101 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 09/05/2019 12:30 AM without the written consent of Pace Analytical Services, L-C. Page 7 of 15 aceAnalytical' wwwpacelabs.cwn Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: M&M Motor Company Pace Project No.: 92442796 QC Batch: 518926 Analysis Method: EPA 8015 Alcohol -Glycol QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified Associated Lab Samples: 92442796001, 92442796002, 92442796003 METHOD BLANK: 2393596 Matrix: Water Associated Lab Samples: 92442796001, 92442796002, 92442796003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethylene glycol mg/L NO 5.0 08/28/19 17:42 LABORATORY CONTROL SAMPLE: 2393597 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Ethylene glycol mg/L 25 20.1 81 48-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2393598 2393599 MS MSD 92442796001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec e/ Rec Limits RPD Qual Ethylene glycol mg/L ND 25 25 22.0 30.5 88 122 34-153 32 R1 Results presented on this page are in the units indicated by the'tlnits' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 09/05/2019 12:30 AM without the written consent of Pace Analytical Services. LLC. Page 8 of 15 aceAnalytical" wwwpacelaextArn QUALITY CONTROL DATA Project: M&M Motor Company Pace Project No.: 92442796 QC Batch: 495754 Analysis Method: EPA 601 OD QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92442796001, 92442796002, 92442796003 Pace Analytical Services, LLC 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 METHOD BLANK: 2670857 Matrix: Water Associated Lab Samples: 92442796001, 92442796002, 92442796003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Lead ug/L ND 5.0 09/04/19 16:23 LABORATORY CONTROL SAMPLE: 2670858 Spike LCS LCS %Rec Parameter Units Conc. Result % Rec Limits Qualifiers Lead ug/L 500 483 97 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2670859 2670860 MS MSD 92442359001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug/L ND 500 500 499 491 100 98 75-125 2 Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/05/2019 12:30 AM without the written consent of Pace Analytical Services, L-C. Page 9 of 15 ace Analytical wwwpacelab&com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilte, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: M&M Motor Company Pace Project No.: 92442796 OC Batch: 495128 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92442796001, 92442796002, 92442796003 METHOD BLANK: 2667750 Matrix: Water Associated Lab Samples: 92442796001, 92442796002, 92442796003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 08/29/19 10:43 LABORATORY CONTROL SAMPLE: 2667751 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 242 97 90-110 SAMPLE DUPLICATE: 2667767 92442898001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 240 225 6 D6 SAMPLE DUPLICATE: 2667768 92442786002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 259 343 28 D6 Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 09/05/2019 12:30 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 15 aceAnalytical a ..pawlebs.= Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: M&M Motor Company Pace Project No.: 92442796 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL- Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPAguidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-I Pace Analytical Services - Indianapolis SAMPLE QUALIFIERS Sample: 92442796001 [1] The samples were received outside of required temperature range. Analysis was completed upon client approval. Sample: 92442796002 [1] The samples were received outside of required temperature range. Analysis was completed upon client approval. Sample: 92442796003 [1 ] The samples were received outside of required temperature range. Analysis was completed upon client approval. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/05/2019 12:30 AM without the written consent of Pace Analytical Services, LLC. Pagel 1 of 15 aceAnalytical` xwxtpawiabs.can Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)075-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: M&M Motor Company 92442796 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92442796001 Outfall No.1 EPA 1664B 495072 92442796002 Outfall No.2 EPA 1664B 495072 92442796003 Outfall No.3 EPA 1664B 495072 92442796001 Outfall No.1 EPA 8015 Alcohol -Glycol 518926 92442796002 Outfall No.2 EPA 8015 Alcohol -Glycol 518926 92442796003 Outfall No.3 EPA 8015 Alcohol -Glycol 518926 92442796001 Outfall No.1 EPA 3010A 495754 EPA 6010D 495804 92442796002 Outfall No.2 EPA 3010A 495754 EPA 6010D 495804 92442796003 Outfall No.3 EPA 3010A 495754 EPA6010D 495804 92442796001 Outfall No.1 SM 2540D-2011 495128 92442796002 Outfall No.2 SM 254OD-2011 495128 92442796003 Outfall No.3 SM 254OD-2011 495128 Date: 09/05/2019 12:30 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 15 Document Name: Document Revised: February 7, 2018 _ s�CBAlh31ylIC8� Sample Condition Upon Recei t SCUR Page 1 of 2 Document No.: Issuing Authority: F•CAR•CS•033•Rev.06 Pace Carolinas Qualit Office Laboratory receiving samples: �--�/ Asheville ❑ Eden[:]Greenwood ❑ Huntersville L� Raleigh❑ Mechanicsville❑ •I Client Name: Project a: WO# : 92442796 d Ex LJUSPS t �� II I II 119111� II I II III Courier: Q ad Ea ❑UPS ❑LISPS ❑Client ❑ Commercial ❑Pace ❑Other:_ 92442796 / Custody Seel Present? ❑Yes No Seals Intact? ❑❑ LYes No C/yr(' —/,� Date/Initials Person Examiningcontents:.��✓ 46 lq' Packing Material: []Bubble Wrap 36,bble Bags []None ❑ Other Biological Tissue Wizen? Thermometer � []Yes ❑No RN/A RGunlo: 92TO48. Type of ice: Rjwet ❑Blue ❑None L� Cooler Temp ('C): 17 . Y Correction Factor: Add/Subtract I-C) 0.0 Books Ten ip Co.I ected lie). Temp117 be above freezing to 6•C NSPu es out of temp criteria. Samples an ice, tooling process hasbegun USDA Regulated Soil ( N/A, water sample) Did samples o,-riginn to in a quarantine zone within the United Stales: CA, NY, or SC (check maps)? Ditl samples originate from a foreign source (internationally, ❑Yes L o rrXX Comment s/Discrepancy: Chain of Custody Present? es J3NO ❑N/A 1. Samples Arrived within Hold Time? es ONO ❑N/A 2. Short Hold Time Analysis 472 hr.)? Elves No EINIA 3. Rush Turn Around Time Requested? ❑Yes nd, ❑N/A 4. Sufficient Volume? yes No N/A S. Correct Containers Used? -Pace Containers Used? rr!�yye�e$ 12K$ []No❑N/A ONO N A 6. Containers Intact? t_yyes No N A 7. Dissolved analysis: Samples Field Filtered? ❑v ON. N/A a. Sample Labels Match COC? -Includes Dale/Time/ID/Analysis Matrix: es of []No ❑N/A _ 9. Heads ace In VOA Vials (a5-6mrn)? Trip Blank Present? Trip Blank Custody Seals Present? Yes ❑Yes ves ONO ❑No No ONLA © /A /A loVt a /. 11. COMMENTS/SAMPLE DISCREPANCY Person contacted: l i11.6 1 1I L) ff y!- Date/Time: Project Manager SCURF Review: yl a Project Manager SRF Review: I(�� _ c Field Data Required? Dyes ONO 11 Date: 0 '� 71 Date: Page 13 of 15 Document Name: Document Revised: February 7, 2018 aceMalydral„ Sample Condition Upon Recel t(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office 'Check mark top half of box If pH and/or dechlorination Is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliforrrt, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box Is to list number of bottle Project If W®# : 92442796 PM: TIH Due Date: 09/05/19 CLIENT: 92—MID QTLAN 2 E d n c J < 2 Fi E n c J a z E d n c J < 2 ry o ? V N V $ i N v Z x p Z °a a a H 0 rN4 / x o 2 ii C m v ? n jZ . 9 c J ( 2 ,V a x p z a E a Q u m ON a z u e V g d a o 1 = y 6 y a T n 2 w J o E a E c as E G E W 5 E v ¢ `u Q d of E E a `° aE E 1 ,.� > E O > E O > E o r in Y E ,•/-�, E N E 1QN', E E i E E J 1 3 2 3 3 n a 5 6 7 B 9 10 ll 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot d Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 14 of 15 %5 y,G CHAIN -OF -CUSTODY / Analytical Reque t Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fief is must be completed accurately. - - - -..""' 2 Seelmn C Requlred Client Information: Requimd Protect Information: Invoice Information: Page ' 1 Of 1 Company: Mid Alli nlic Associales, foe. Report To: H.1f.n. Chmc Al:ereon: Address: 409 R000 V.e Cl Copy To: Company Name: Raleinh. NC 27610 Address: Email: Purchase Order>: Pace Duero. Re ulat0 Aocnc Prone: Fa Project ReGwsIM Due Dale: Name: WM Mole, Company. Inc. Pam Project Manapec tyrick.hmks(dpemlabsmm - StateI Location Project N: Pace Profile o; 5921 NC R ucsteo Anal sis Filtemd (YNI' - - ' Z r TRIX Coos - COLLECTED z Preservatives > ;,= • L•'y, '.+•t .* Pinti^9 Wvo dw " O WTn yrt $ V w W�ae wary P SAMPLE ID prow P SwSaea Y 0 D '-' N j 0 0. � START END w m H One Character per boa. $ IAd. 0.91, -) A*o. or 0 _ : v Io H Sample Ws must bo unique tR.ue i8 x w o ii0 _ ?'^in w f = a DATE TIME DATE TIME d u p e$- n n inZ i x U x O z z Z O Q V) r U' o — C `•i"'� 1t :1' �' Oulrall No.1 l•Vr 5-22 5;-'3 T-Z? 5:j3 P, 7 1I11 I Z XX X 7,3y,h v 4 �2-' Oudall No Wi 4=22 5:31 }' L7 5:0 1 I Z X X i X T -3' Oudall No VVT Y-Z2 r zp Y-2z �!1j 7 4 I Z - 5 . 6 7 g: 9 . 5.10Z 72>r ADDmONAI CAMMFMS - .." 1:Fnj RELINOUI5HED 9Y/AFFl_LIpTgN..vTEx mME t-,YAa -•" - 9YIAFFRMITION J.-'"+ten -t �k++-i ..DATE'.. p.VME �. •,. ..Y.- SIMPLE CANDITIONS-. 7 N PRINT Nam of SAMPLER: r7 mcc45 I TPI i S z q L z_ SIGNATURE of SAMPLER: � J, LI DATE Igncd /