HomeMy WebLinkAboutNCG080583_MONITORING INFO_20191018STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
DOC TYPE
❑ HISTORICAL FILE
MONITORING REPORTS
DOC DATE
❑ �1O j. I
YYYYMMDD
Forensic Environmental Services of NC, LLC
A
March 31, 2019
Schneider Electric
105 Summit Park Drive
Salisbury, NC 28146
RE: Stormwater analysis for March 2019 event
Dear Mr. Pitel,
oP,I L�
'Y 10/1J'l Zo)9
OCT 18 2019
CENTRAL FILES
DINR SECTION
Forensic Environmental Services of NC, LLC is pleased to submit the following analytical data for the
stormwater sampling event that occurred March 2019.
Thank you for letting Forensic Environmental Services of NC, LLC, assist you with your
environmental and safety concerns. We look forward to working with you on future projects. Should
you have any questions please do not hesitate to call @ 828-493-6325.
Cordially,
David Haynes, REM, REPA, CFC
Owner / Manager
Attachment:
40
e> iN)
,'C� r F Do G— N
1114
1c i N (� LJ �. LJ F✓z-�
bo i,V 71u
� E
3e
P.O. Box 883• Hudson. NC 28638•Tel (828) 493-6325•Cell (828)493-1405
t-mail to envser@gmail.com
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client:
Forensic Environmental Services of NC
PO Box 883
Hudson, NC 28638
Attention:
Mr. David Haynes
Date Received:
04-Mar-19
Report Date:
27-Mar-19
Sample Date:
01-Mar-19
13RL #:
BRL-2019-0114
Lab Sample ID:
LSID-2019-00491
Client Sample ID:
Outfall # 1 - Schneider Elect.
Parameter Result MQL
eOil & Grease
CJ
Reported By:
blueridgelabslenoir@gmail.com
Analysis Analysis
Unit Method Time Date Analyst
+ 5 mg/I EPA 1664 n- 3/25/2019 WtrQlty
S. Wohnson, D.R. Wessinger
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 1 of 3
n
10 Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client: Forensic Environmental Services of NC
PO Box 883
Hudson, NC 28638
Attention: Mr. David Haynes
Date Received:
04-Mar-19
Report Date:
27-Mar-19
Sample Date:
01-Mar-19
BRL 4:
BRL-2019-0114
Lab Sample ID:
LSID-2019-00492
Client Sample ID:
Outfall #1 - Schneider Elect.
Parameter
in
•
C�
Reported By
blueridgelabslenoir@gmaii.com
Result MQL Unit Method
• 0.01 mg/l 200.7 1994
Analysis Analysis
Time Date Analyst
15:20 3/8/2019 KCJ
S.Wohnson, D.R. Wessinger
` Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 2 of 3
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client :
Forensic Environmental Services of NC
PO Box 883
Hudson, NC 28638
Attention:
Mr. David Haynes
Date Received:
04-Mar-19
Report Date:
27-Mar-19
Sample Date:
01-Mar-19
BRL u:
BRL-2019-0114
Lab Sample ID:
LSID-2019-00493
Client Sample ID:
Outfall 91 - Schneider Elect.
blueridgelabslenoir@gmail.com
Analysis
Analysis
Parameter
Result MQL Unit Method Time
Date
Analyst
TSS
• 5 mg/I 2540D 1997 10:20
3/15/2019
KCJ
• pH
5.8 HT 0.1 so 4500H+B 200 12:06
3/4/2019
KCJ
Reported By:
.'J. Johnson, D.R. Wessinger
• Concentrations are below Minimum Quantification Limit except where noted.
® NC Laboratory Certificate No. 275
Page 3 of 3
Data Qualifiers
The following is a list of data qualifiers used on Blue Ridge Labs' Reports. Any of the
qualifiers may make the data unacceptable for state reporting. Data qualifiers are
found in the results column and their definitions are as follows:
* The concentration found is below our minimum concentration value, which is
reported in the MQL column.
*** The concentration reported is an estimated value. The result is above our
highest standard.
HT The sample was received out of hold time.
IC The sample was received in an improper container.
NC The sample was received without proper cooling.
• NP The sample was received without proper preservatives.
IC The sample was received in an improper container.
HS The VOC container was received with headspace present.
NR The sample was not run due to lab error:
UC Unable to confirm analysis due to insufficient sample being submtted.
D Sample was diluted due to physical problems with the sample.
J Value is an estimate from a library search using the nearest internal standard.
NCA Non -certified Analysis
Revised 10/21/16
WATER QUALITY LAB & OPERATIONS, INC.
P.(}.BOY 115T
BANNER ELK, NC 28804
(020)090'6277
CLIENT: BLUE RIDGE LADS LOGIN TIME:
ADDRESS: PD.BOX 28W] SAMPLER -
CITY: LEN0R RECEIVED DATE:
STATE: NC Z|P2O545 REPORTED DATE: 27'Mar-19
RESULTS
REPORTED BY: NCCERTIFIED LAB #544
PAUL|SEmH0UR.SUPERVISOR
El
o Blue Ridge Labs, Inc.
P.O. Box 2940
Lenoir, NC 28645
Telephone (828) 728-0!49 Fax (328) 728-0131
Chain of Custody
NPDS Reporting _ Groundwater _ Sanitary Landfill Hazrrdous Waste Industrial or QC
R,Aa f&Sac dylW,
UST/Trust Fund Reporting
Bill To:
Field
iM State Reporting bl-�'
Project Name:-CC-#A/6•1 JFJt— G�LCcM/C
PO Number:
Ice Present: Y pVJ
Preservatives f.nh Check
C-Composite
G- Grab
Sample ID
Sample
Type
Date
Time
Time &
Temp
HR:MM
°C
Field
Sulfide
Check
Y N
Field
Sulfide
Present /
Removed
Y N
Resid
Chlor
Field
Check
Y N
i
Field
echlaination
Y N
pH
Resid
Chlor
PorA
Temp
°C
Sampler
Initials
Analysis Requested
71
!I
Relinquished Bv:
- Ott j P� ke/
Date: Time:
Date: Time:
Upon submission of samples, client agates that invoices auc due at the time work is completed. Open accounts are due D9 da)lffollowing invoice dale. A finance charge of 1.5%per month will be imposed ou ail paafuc accounts.
When relinquishing samples to Blue Ridge L3hs (BRL), buyer authorizes BRL to perform only the analysis in chatted abgve and also agrees to pa)collection and attorney fees if the account becomes delinquent. Blue Ridge Labs
mseoes the right to deny documentation for any work where payment has not been made, in effect rendering that data unsupported for regulatory purposes. BRL cannot guarantee that any regulatory authority will accept any work
>ubmi:ted. tberefore it is the client's responsibility to request on this form appropriate tests. NC DBNR Certified Lah 9275
Forensic Environmental Services of NC, LLC
r
October 15, 2018
Schneider Electric
105 Summit Park Drive
Salisbury, NC 28146
RE: Stormwater analysis for September 2018 event
Dear Mr. Pitel,
00
N011035 a/viQ
S3ll� 1H2f1N�0
6108 8 i 100
GDAG03LI
Forensic Environmental Services of NC, LLC is pleased to submit the following analytical data for the
stormwater sampling event that occurred September 2018.
Thank you for letting Forensic Environmental Services of NC, LLC, assist you with your
environmental and safety concerns. We look forward to working with you on future projects. Should
you have any questions please do not hesitate to call @ 828-493-6325.
Cordially,
David Haynes, REM, REPA, CFC
Owner / Manager
Attachment:
4)
N V-)
Cj
1�
�
fo �P
�0
4�
I'l
01103S 2JJAa
FIG Q 1100
P.O. Box 883• Hudson, NC 28638•Tel (828) 493-6325•Cell (828)493-1405
1--mail to envser a 1-mail.com
0
10 Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
Client:
Forensic Environmental Services of NC
PO Box 883
Hudson, NC 28638
Attention:
Mr. David Haynes
Date Received:
18-Sep-18
Report Date:
12-Oct-18
Sample Date:
17-Sep-18
BRL #:
BRL-2018-0763
Lab Sample ID:
LSID-2018-02974
Client Sample ID:
Outfall 1 - Schneider Electric
Parameter
Oil & Grease
Ob
blueridgelabslenoir@gmail.com
Result MQL Unit Method
* 5 mg/I 1664-A O&G
Analysis Analysis
Time Date Analyst
10/2/2018 WtrQtly
Reported By:
S. .Johnson, D.R. Wessinger
* Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 1 of 3
10
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149 blueridgelabslenoir@gmail.com
Client : Forensic Environmental Services of NC
PO Box 883
Hudson, NC 28638
Attention: Mr. David Haynes
Date Received: 18-Sep-18
Report Date: 12-Oct-18
Sample Date: 17-Sep-18
BRL #: BRL-2018-0763
Lab Sample ID: LSID-2018-02975
Client Sample ID: Outfall I - Schneider Electric
Analysis Analysis
Parameter Result MQL Unit Method Time Date Analyst
• Pb * 0.01 mg/I 200.7 1994 13:40 9/21/2018 KCJ
Reported By:
S. J. �RiWcssmger
" Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 2 of 3
Blue Ridge Labs
PO Box 2940
Lenoir, NC 28645
828-728-0149
blueridgelabslenoir@gmail.com
Client :
Forensic Environmental Services of NC
PO Box 883
Hudson, NC 28638
Attention:
Mr. David Haynes
Date Received:
18-Sep-18
Report Date:
12-Oct-18
Sample Date:
17-Sep-18
BRL #:
BRL-2018-0763
Lab Sample ID:
LSID-2018-02976
Client Sample Ill:
Outfall 1 - Schneider Electric
Analysis
Analysis
Parameter
Result MQL Unit Method
Time
Date Analyst
•TSS
7.8 6.3 mg/l 2540D 1997
4500H+B
14:31
9/21/2018 KC1
pH
6.8 HT 0.1 su 200
17:12
9/18/2018 KCJ
Reported By:
S. J. Johns .R. Wessinger
" Concentrations are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page 3 of 3
•
E
WATER QUALITY LAB & OPERATIONS, INC.
P.O. BOX 1167
BANNER ELK, NC 28604
(828)898-6277
CLIENT: BLUE RIDGE LABS LOGIN TIME:
ADDRESS: P.O. BOX 2940 SAMPLER:
CITY: LENOIR RECEIVED DATE:
STATE: NC ZIP 28645 REPORTED DATE:
I D#:
12-Oct-18
ANALYSIS:::::::.:::::
LSID # :
ANALYSIS
RESULTS
MQL'sS
UNITS],SAMPLE
I
LOCATION
ANALYSIS
DATE
. ':;INT..; :;
OIL & GREASE
2974
<5
5.00
MG/L
2-Oct-18
PI
REPORTED BY: NC CERTIFIED LAB # 544
PAUL ISENHOUR, SUPERVISOR
0
NPDS Reporting Groundwater
Report To'
F,.464 ic_ 1 d�llo 5
• v
Blue Rid Labs, Inc..
P.O. Box 2940
Lcnoir. NC 28645
Telephone (828) 728-0149 Fax (828) 728-0131
Chain of Custody
Sanitary Landfill Hazardous Waste Industrial or QC Non State Reporting
UST/Trust Fund Reporting
Rill To:
Project Name: z 6,f % fa c
PO Number
Ice PresenC Y N C-Composite
Field Preservatives
reservatives Lab Check G- Grab
Sample ID
Sample
"Type
Date
Time
Time &
Temp
IIR:MM
°C
Ficld
Sulfide
Check
Y N
Field
Sulfide
Present /
Removed
Y N
Resid
Chlor
Field
Check
Y N
Field
Dechlorination
Y N
pl-1
Resid
Chlur
PorA
Temp
°C
Sampler
Initials
Analysis Requested
G%-
0oT1w1j'
w
Al
I-I)s
�`l'
-rrss AA E
RelinquishedBy: Date: Time: Recei. d 13 Date- Time:tw
d /4�pj %7f-
Upon submission ofsmnpl s. client agrees that invoices lire due u1 the time wotk is completed. Open accounts Lite due 20 duys dlowine, invoice date A Iinance charge of L? % per month ovill he imposed on all piWM accounts.
When relinquishing samples to Blue Ridge Lahr (nRL), buyer authorizes nRl, to perlbnn only the analysis indimed above and also agreeS to pav collection and attorney fees it the account becomes delinquent. I41ue Ridge Labs
reserves the ri_hl In deny documentation for any work where payment has nvl been made, in effect rendering that data unsupported for re_milatory purposes. nRl, cannot guarantee that any regulatory authority kill accept any work
submitted, t1wrefiue it is the client's responsibility to rquul on this total appropriate tests. NC DFNR CrniGed Lab H275
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG080000
Date submitted t0131/2019
CERTIFICATE OF COVERAGE NO. NCGO8 O 5 8 3
FACILITY NAME SMneitler National Gamer
COUNTY MedlenWrg
PERSON COLLECTING SAMPLES Gary Lob
LABORATORY Pace Lebmtory Lab Cent. p 5M2
Comments on sample collection or analysis:
SAMPLE COLLECTION YEAR 2019
SAMPLE PERIOD ❑ Jan -June ❑li July -Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow [_]Watersupply ❑SA
❑Other
CEIVE® PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more t �5 g)l�y 2.6g5ew oil per month? ❑0 yes ❑ no (if yes. complete Part A)
Part A: Vehicle & Equipment Maintenance Areas Monitoring RequjJ@"qIis((@PAEV1g ❑ No discharge this period'
DWR SEc'TIONI
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches3
Non -Polar Oil & Grease
mg/L
Total Suspended Solids,
mg/L
New Motor or Hydraulic Oil Usage,
gal/mon
Benchmarks
-
-
15
100 or SW
-
ParometerCode
-
46529
00552
C0530
NCOIL
SP1
10/16/19
>.25
<4.8 mg/L
60.8
SP3
10/16/19
>.25
<4.9 mg/L
340
SP4
10/16/19
>.25
<4.8 mg/L
1950
SP5
10/16/19
>.25
<4.9 mglL
130
SP6
10/16/19
>.25
<4.8 mg/L
396
' Monthlysampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
' For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
° See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -
numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the
detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX".
Permit Date: 11/l/2018-5/31/2021 SWU-248, last revised 11/1/2018
Page 1 of 2
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) ❑ No discharge this period
Outfall
No.
Date Sample
Collected'
(mo/dd/yr(
24-hour rainfall
amount,
Inches'
Sample Collected'
mo/dd/yr
Total Suspended
Solids,
mg/L
pH,
Standard units
Non -Polar Oil &
Grease,
mg/L
Permit limit
_
-
100 or Sir
6.0-9.0
15
Parameter code
46529
CO530
00400
00552
Footnotes from Part A also apply to this Part B
Note: If you report a sample value In excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES [I NO
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail on original copy of this DMR, including all "No Discharge" reports. within 30 dPKs of receipt of the lob results for at end of monitocna period in the
case of "No Discharge"reports) to
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
vt /
Signature of ermittee Date
Permit Date: 11/l/2018-9/31/2021 SWU-248, last revised 11/1/2018
Page 2 of 2
(�IaceAnalytica(
xwwPscdaas.cum
October 31. 2019
Mr. Michael DeBraske
Schneider National, Inc.
PO Box 2545
Green Bay, WI 543062545
RE: Project: SNI-Charlotte NC
Pace Project No.: 92450171
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Dear Mr. DeBraske:
Enclosed are the analytical results for sample(s) received by the laboratory on October 17, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
nicole.gasiorowski@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Caryssa Berg, Schneider National
Mr. Michael DeBraske, GEI Consultants, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Anaytcal Services, LLC.
Page 1 of 15
acmnalytical e
ewwpacdabs.=
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
(704)875-9092
CERTIFICATIONS
Project: SNI-Charlotte NC
Pace Project No.: 92450171
Charlotte Certification We
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Flodda/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 15
laceAnalyfical'
a»wpecdaba.clm
SAMPLE ANALYTE COUNT
Project: SNI-Charlotte NC
Pace Project No.: 92450171
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92450171001
Sp-1
EPA 1664E
AACt
1
PASI-C
SM 2540D-2011
JP1
1
PASI-A
EPA9040C
ECH
1
PASI-A
92450171002
SP-3
EPA 1664E
HH
1
PASI-C
SM 2540D-2011
- JPi
,, 1
PASI-A
r ..
_
• r EPA 9040C
ECH
1
PASI-A
92450171003
SP-4
EPA 1664B
HH
1
PASI-C
SM 2540D-2011
JP1
1
PASI-A
EPA 9040C
ECH
1
PASI-A
92450171004
SP-5
EPA 1664B
HH
1
PASI-C
SM 2540D-2011
JP1
1
PASI-A
EPA 9040C
ECH
1
PASI-A
92450171005
SP-6
EPA 1664B
HH
1
PASI-C
SM 2540D-2011
JP1
1
PASI-A
EPA 9040C
ECH
1
PASI-A
92450171006
SP-7
EPA 1664E
HH
1
PASI-C
SM 2540D-2011
JP1
1
PASI-A
EPA 9040C
ECH
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 15
laceAnalyficale
w rpwetabs.mrn
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite too
Huntersville, NC 28078
(704)875-9092
Project: SNI-Charlotte NC
Pace Project No.: 92450171
Sample: SPA
Lab ID: 92450171001 Collected:
10116/1908:48
Received:
1011711914:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed CAS No.
Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mg/L
4.8
1
10/30/19 12:29
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
60.8 mg/L
10.0
1
10/22/19 01:48
9040 pH
Analytical Method: EPA 9040C
PH at 25 Degrees C
6.5 Std. Units
0.10
1
10/28/19 15:39
H3
Sample: SP-3
Lab ID: 92450171002 Collected:
10/16/1908:55
Received:
1011711914:00 Matrix: Water
Parameters
Results Units Report Limit
OF
Prepared
Analyzed CAS No.
Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mg/L
4.9
1
10/30/19 16:02
M1
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
340 mg/L
17.9
1
10/22/19 0149
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.7 Std. Units
0.10
1
10/28/19 15:45
H3 '
Sample: SP-4
Lab ID: 92450171003 Collected:
10/16/1909:05
Received:
10/17/1914:00 Matrix:Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed CAS No.
Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
-
Oil and Grease
NO mg/L
4.8
1
10/30/19 16:04
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
1950 mg/L
71.4
1
10/22/19 01:50
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.9 Std. Units
0.10
1
10/20/19 16:02
D6,H3
Sample: SP-5 Lab ID: 92450171004 Collected: 10/16/19 09:22 Received: 10/17/19 14:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease NO mg/L 4.9 1 10/30/19 16:04
Date: 10/31/2019 07:58 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 15
(�55'ceAnajfytical*
wewpeca'absem
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: SNI-Charlotte NC
Pace Project No.: 92450171
Sample: SP-5
Lab ID: 92450171004 Collected: 10/16/19 09:22 Received:
10/17/19 14:00 Matrix: Water
Parameters
Results Units Report Limit OF Prepared
Analyzed CAS No.
Qual
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
130 mg/L 12.5 1
10/22/19 01:50
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
7.0 Sid. Units 0.10 1
10/20/19 16:36 -
H3
Sample: SP-6
Lab ID: 92450171005 Collected: 10/16/1909:40 Received:
10/1711914:00 Matrix: Water
Parameters
Results Units Report Limit DF Prepared
Analyzed CAS No.
Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mg/L 4.8 1
10/30/19 16:04
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
396 mg/L 20.8 1
10/22/19 01:51
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.3 Sid. Units 0.10 1
10/20/19 16:47
H3
Sample: SP-7
Lab ID: 92450171006 Collected: 10/1611909:59 Received:
10/17/1914:00 Matrix: Water
Parameters
Results Units Report Limit OF Prepared
Analyzed CAS No.
Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg/L 4.9 1
10/30/19 16:04
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
228 mg/L 12.5 1
10/22/19 01:51
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.5 Std. Units 0.10 1 `
10/20/19 16:53
H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Dale: 10/31/2019 07:58 AM
without the written consent of Pace Analytical Services, L-C.
Page 5 of 15
ace Analytical
a isw.peca'aAcoom
Project: SNI-Charlotte NC
Pace Project No.: 92450171
QC Batch: 506605
QC Batch Method: EPA 1664B
Associated Lab Samples: 92450171001
METHOD BLANK: 2720433
Associated Lab Samples: 92450171001
Parameter Units
Oil and Grease mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 1664E
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO - 4.8 10130/1910:53
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
(704)875-9092
LABORATORY CONTROL SAMPLE:
2720434
Spike
1-CS
1-CS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/1-
38.5
32.9
86
78-114
MATRIX SPIKE SAMPLE:
2720435
92449952001 Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
1.7J 38.5
33.3
82
78-114
Results presented on this page are In the units Indicated by rim -units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/31/2019 07:58 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 15
m
aceAnalytical
ewwCecNeos.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: SNI-Charlotte NC
Pace Project No.: 92450171
QC Batch: 506716
Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E
Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92450171002, 92450171003, 92450171004, 92450171005, 92450171006 ,
METHOD BLANK: 2720937
Matrix: Water
Associated Lab Samples: 92450171002, 92450171003, 92450171004, 92450171005, 92450171006
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Oil and Grease
mg/L
-s NO - 5.0 10/30/19 16:01
LABORATORY CONTROL SAMPLE:
2720938
Spike LCS LCS % Rec
Parameter
Units
Conic. Result % Rec Limits Qualifiers
Oil and Grease
mg/L
40 39.3 98 78-114
MATRIX SPIKE SAMPLE:
2720939
92450171002 Spike MS Ms % Rec
Parameter
Units
Result Conic. Result % Rec Limits Qualifiers
Oil and Grease
mg/L
NO 38.5 5.4 5 78-114 M7
Results presented on this page are in the units Indicated by Uu, "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/31/2019 07:58 AM without the written consent of Pace Analytical Services, L-C.
Page 7 of 15
(�55'ceAnajfyfical'
aww.pecdaas.corn
QUALITY CONTROL DATA
Project: SNI-Charlotte NC
Pace Project No.: 92450171
QC Batch: 504884 Analysis Method: SM 254OD-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92450171001, 92450171002, 92450171003, 92450171004, 92450171005, 92450171006
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
METHOD BLANK: 2713030
Matrix:
Water
Associated Lab Samples: 92450171001,
92450171002, 92450171003, 92450171004, 92450171005, 92450171006
Blank
Reporting
Parameter
Units
Result
Limit Analyzed Qualifiers
Total Suspended Solids
mg/L
NO
2.5 10/22/19 01:45
LABORATORY CONTROL SAMPLE:
2713031
Spike
LCS LCS % Rec
Parameter
Units
Conic.
Result % Rec Limits Qualifiers
Total Suspended Solids
mg/L
250
242 97 90-110
SAMPLE DUPLICATE: 2713038
92450171001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 60.8 63.2 4
SAMPLE DUPLICATE: 2713039
92450171003 Dup
Parameter Units Result Result RPD Qualifiers
-Total Suspended Solids mgf- 1950 2130 9
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/31/2019 07:58 AM without the written consent of Pace Analytical Services, L-C.
Page 8 of 15
aceAnalytical
wascpscalaes.00m
QUALITY CONTROL DATA
Project: SNI-Charlotte NC
Pace Project No.: 92450171
QC Batch: 504653 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Associated Lab Samples: 92450171003, 92450171004, 92450171005, 92450171006
SAMPLE DUPLICATE: 2711979
92450171003 Cup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.9 6.5 7 D6,113
SAMPLE DUPLICATE: 2711980
92449833003 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 5.5 5.6 3 D6,H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Results presented on this page are In the units Indicated by the "units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/31/2019 07:58 AM without the written consent of Pace Analytical Services, L-C.
Page 9 of 15
(�5ace Analytical
owwpacefeescorn
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: SNI-Charlotte NC
Pace Project No.: 92450171
QC Batch: 506001 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Associated Lab Samples: 92450171001, 92450171002
SAMPLE DUPLICATE: 2718169
92449718001 Cup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Sid. Units 6.9 6.7 3 D6,1-13
e .. , ,
SAMPLE DUPLICATE: 2718170
Parameter Units
pH at 25 Degrees C Sid. Units
92450780002 Cup
Result Result
5.8 5.3
RPD Qualifiers
10 D6,H3
Results presented on this page are In the units Indicated by the'Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/31/2019 07:58 AM without the written consent of Pace Analytical Services, U.C. Page 10 of 15
(�15'ceAnalyficai'
w pecdaDtcnm
QUALIFIERS
Project: SNI-Charlotte NC
Pace Project No.: 92450171
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
(704)875-9092
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyze in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyle is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyze is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 10/31/2019 07:58 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 15
laceAnalyficaI9
m .Pewob&corn
Project: SNI-Charlotte NC
Pace Project No.: 92450171
Lab ID Sample ID
92450171001 SP-1
92450171002
SP-3
92450171003
SP4
92450171004
SP-5
92450171005
SP-6
92450171006
SP-7
92450171001
SP-1
92450171002
SP-3
92450171003
SP4
92450171004
SP-5
92450171005
SP-6
92450171006
SP-7
92450171001
SP-1
92450171002
SP-3
92450171003
SP4
92450171004
SP-5
92450171005
SP-6
92450171006
SP-7
Date: 10/31/2019 07:58 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
QC Batch Method
QC Batch Analytical Method
EPA 16648
506605
EPA 1664E
506716
EPA 1664B
506716
EPA 1664B
506716
EPA 1664B
506716
EPA 1664B
506716
SM 2540D-2011
504884 '
SM 2540D-2011
504884
SM 2540D-2011
504884
SM 2540D-2011
504884
SM 2540D-2011
504884
SM 2540D-2011
504884
EPA 9040C
506001
EPA 9040C
506001
EPA 9040C
504653
EPA 9040C
504653
EPA 9040C
504653
EPA 9040C
504653
REPORT OF LABORATORY ANALYSIS
This report Shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, -LC.
Analytical
Batch
Page 12 of 15
Document Name: Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR) Page 1 of 2
aceAWlytiral- Document No.: IssuingAuthoriry:
F.CAR-CS-033-Rev.06 Pace Carolinas Q"Iity Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville �/ Raleigh❑ Mechanicsville El
Custody Seal Present? ❑Yes
QNo "Seals Intact?
❑Yes
[DNo
Packing Material: ❑Bubble Wrap ❑ ubble Bags ❑None ❑ Other
ThermometerType of ice: Qw� ❑Blue
IIs• can ID: 92T049
Cooler Temp ('Cl: 11 Correction Factor: "AAd/Subtract (-C) - 0.0
Cooler Temp Corrected ('CI: !
USDA Regulated Soil, ([3 N/A, water sample)
Did samples orlginate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
WO#:92450171
III1101E11111111I111Ili -
92450171 cf((
Date/Initials Perwn Examining Comems:",r�/���-/
Blologica!�Jslue Frozen?
❑Yes [21No ❑N/A
❑None
Temp should be above freezing to WC
❑samples out of temp critena. Samples on ice, cooling process
hasbegun
Did samples originate from a foreign source (internationally,
.. m.nV rhea F-INn
Yes LjWo
.....__..,.._..___._.___
Comments/dsae an
Chain of Custody Present?
�
BY-.
Q1.
N/A
s'
Samples Arrived within Hold Time?
(]Ya
ONO
N/A
2.
Short Hold Time Analysb 02 hr.?
Yes
N/A
3.
Rush Tom Around Time Requested?
Yeses
No
N/A
a.
Sufficient Volume? —
yes
ONO
N A
S.
CorreaContainersUsed?
[]Y�y°'
ONO
❑N/A
6.
-Pace Containers Used?
Yes
No
N/A
Containers Intact?
a Yes
ONO
N/A
7. —
Diiiolved analysis: Samples Field Fihered?
Oyes
No
f
N/A
a. ' '
Sample Labels Match COC?
QYes
ONO
❑N/A
9.
-hscludes Date/Time/ID/Analysis tRatrix:
s ace in VOA Vials (a5.6mm)?
Yes
No
N A
10.
lank resent?
tri
Oyes
Offo
❑N�
11.
lank Custody Seals Present?
OYes
QNO
' N/A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION '
field Data Required? UYta L)NO
Person contacted: _% Datefrime:
Project Manager SCURF Review: N " Date:
Project Manager SRF Review: �61iL— Date: 0
Page 13 of 15
Document Name:
Document Revised: February 7, 2019
Sam le Condition U on Recel t(SCUR
Page 2 of 2
aceAnaryfical
Document No.:
issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorinatlon Is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLH8
"Bottom half of box Is to list number of bottle
Project If 1 O# ; 92450171
PM: RWC Due Dale: 10/31/19
CLIENT: 82-SCHNEIDER
—
_
^
V
Q
Q
N
2
v
Z
�
a
y
I
V
u
=
�
n
c
c
N
8
i
ry
i_
u
J
8
s
E
i
i'
8
x
s
-
'E
y
.�.
_
E
c
r.
y
Z
E
E
a
a
aNp
Eo
a
a
j
o
n`
aa
E
E
n
`u
E
E
E
E
E
E
E
E�
a
w
of
m
of
8
n
c
SE
-°v1
�13w
a
E
J
J
i
Y
Z
e
Y
i
n
O'
O
„�}
Va
ii
U'
r�+l
t�
r✓1,
l!
N
p
U'
y
N
n
O
m
m
ro
m
m
u
3
a
a
a
a
a
�Y
;
-m
m
m
1
I
�
2
I
I
2
3
I
�
2
4
5
I
I
-
I
/
7
6
9
IO
I1
l2
pH Adjustment
log for Preserved Samples
sample ID
Date preservation adjusted
Time preservation
adjusted
AMDUM of Preservadre
added
Lot a
TT7
_.__,.____.___,_.-.........r.r,:.L..n,—illh.....,1.lh.Nnnh[arolina
DEHNR CMIflcation
Office (i.e.
Note: Whenever mere H a UHcrepdncY dim"..a..m... �..""�.. .....r__..__._ __,___-.-
Out of hold, Incorrect preservallve, Out of temp, Incorrect containers.
a
Page 14 of 15
/i+xeauMial'
CHAIN -OF -CUSTODY I Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be wmpleted accurately.
Becton A Sect B section C
Reaelmd CRent Inf..alan: Required Project lnfpmallon: Invoice Infamutlon: Page, 1 Of 1
Ca Y: Stdlroider Natiaal RopM To: Gatyl.ad Alt.t.
Addmfa: 2420 Stwto Road Copy To: Campani, Nam:
C"Mlte. NC 28269
i
ACdrese:
- Racralmn, Aaaaricy
Email: C ct- �' -7 L,'1
pisvnace Order n;
Pace CWtc
PIvxY: TOc 99�Ta10 Faz
lFI0,W Name: SN4Cfurbl4, NC
Pose Prajw Manager: vs,,ran ae.tan,
'State I Loradon
Re aiesteo Due Date:
1p,aci 0 jpacePMdi,c
2601-1
NC
' R
uasrod
Aral
a Fillarad
YM
a
s
Z
9
COLLECTED
z
Preservatives
>
-
a„1a,,, aKrt
arn�reNYw aV
a
8
u
nwe s
r
SAMPLE ID a0 tt
E
0
u
START
END
p
N
ar
F
S
$
ono ehuaeror per
c
N-Las/.-1 N. oT
De
N
C
TDAIETI.Z
"t
[
0�
Z.
i2
0
F
Samp 0Ida moat tmiaue Tn T.
w
�
e
y
r
m
e
g
p
a
O_
p
o
Q
o
m
3
DATE
TIME
z
t
s
z
i
0
r
n
7JD ll I
A
001
1
SP.1 �
YJT
�
_
-
X
%
x
�
I I
I
I
2
spa
var
x
x
x
^ �
QV
3
sp+
WT
x
x
x
,
.
5
p91-
a
sP.s
wr
p9
x
x
x
005
B
SPL J
WT
%
X
is
.
1
09
6
SPa S
Wr
USS
x
x
x..
P
,e
9
. 9
_1DjI
,2
..� ADDITIONAL co"EMB .. .
r [<, RELINlxIB11FD 8Yl AFFlWl10N a � ,
Ti
-STYE
- AwEPTED BYIAFF4IAPON
DATE
TIME
... SAMPIE CONCNIONB .
SAMPLER NiME AND SIGNATURE
$
c
$
-
PRINT Namv of SAMPLER: /'
t0
m
uRRy ,Gofa
d
Y a
_ $ a
3$
v _
�� 2
SIGNATURE of SAMPJ
DAOTE i etl
N
r
a=L
gnu"
c�
0
N
U , U