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HomeMy WebLinkAboutNCG080583_MONITORING INFO_20191018STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. DOC TYPE ❑ HISTORICAL FILE MONITORING REPORTS DOC DATE ❑ �1O j. I YYYYMMDD Forensic Environmental Services of NC, LLC A March 31, 2019 Schneider Electric 105 Summit Park Drive Salisbury, NC 28146 RE: Stormwater analysis for March 2019 event Dear Mr. Pitel, oP,I L� 'Y 10/1J'l Zo)9 OCT 18 2019 CENTRAL FILES DINR SECTION Forensic Environmental Services of NC, LLC is pleased to submit the following analytical data for the stormwater sampling event that occurred March 2019. Thank you for letting Forensic Environmental Services of NC, LLC, assist you with your environmental and safety concerns. We look forward to working with you on future projects. Should you have any questions please do not hesitate to call @ 828-493-6325. Cordially, David Haynes, REM, REPA, CFC Owner / Manager Attachment: 40 e> iN) ,'C� r F Do G— N 1114 1c i N (� LJ �. LJ F✓z-� bo i,V 71u � E 3e P.O. Box 883• Hudson. NC 28638•Tel (828) 493-6325•Cell (828)493-1405 t-mail to envser@gmail.com Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client: Forensic Environmental Services of NC PO Box 883 Hudson, NC 28638 Attention: Mr. David Haynes Date Received: 04-Mar-19 Report Date: 27-Mar-19 Sample Date: 01-Mar-19 13RL #: BRL-2019-0114 Lab Sample ID: LSID-2019-00491 Client Sample ID: Outfall # 1 - Schneider Elect. Parameter Result MQL eOil & Grease CJ Reported By: blueridgelabslenoir@gmail.com Analysis Analysis Unit Method Time Date Analyst + 5 mg/I EPA 1664 n- 3/25/2019 WtrQlty S. Wohnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 1 of 3 n 10 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client: Forensic Environmental Services of NC PO Box 883 Hudson, NC 28638 Attention: Mr. David Haynes Date Received: 04-Mar-19 Report Date: 27-Mar-19 Sample Date: 01-Mar-19 BRL 4: BRL-2019-0114 Lab Sample ID: LSID-2019-00492 Client Sample ID: Outfall #1 - Schneider Elect. Parameter in • C� Reported By blueridgelabslenoir@gmaii.com Result MQL Unit Method • 0.01 mg/l 200.7 1994 Analysis Analysis Time Date Analyst 15:20 3/8/2019 KCJ S.Wohnson, D.R. Wessinger ` Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 2 of 3 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : Forensic Environmental Services of NC PO Box 883 Hudson, NC 28638 Attention: Mr. David Haynes Date Received: 04-Mar-19 Report Date: 27-Mar-19 Sample Date: 01-Mar-19 BRL u: BRL-2019-0114 Lab Sample ID: LSID-2019-00493 Client Sample ID: Outfall 91 - Schneider Elect. blueridgelabslenoir@gmail.com Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst TSS • 5 mg/I 2540D 1997 10:20 3/15/2019 KCJ • pH 5.8 HT 0.1 so 4500H+B 200 12:06 3/4/2019 KCJ Reported By: .'J. Johnson, D.R. Wessinger • Concentrations are below Minimum Quantification Limit except where noted. ® NC Laboratory Certificate No. 275 Page 3 of 3 Data Qualifiers The following is a list of data qualifiers used on Blue Ridge Labs' Reports. Any of the qualifiers may make the data unacceptable for state reporting. Data qualifiers are found in the results column and their definitions are as follows: * The concentration found is below our minimum concentration value, which is reported in the MQL column. *** The concentration reported is an estimated value. The result is above our highest standard. HT The sample was received out of hold time. IC The sample was received in an improper container. NC The sample was received without proper cooling. • NP The sample was received without proper preservatives. IC The sample was received in an improper container. HS The VOC container was received with headspace present. NR The sample was not run due to lab error: UC Unable to confirm analysis due to insufficient sample being submtted. D Sample was diluted due to physical problems with the sample. J Value is an estimate from a library search using the nearest internal standard. NCA Non -certified Analysis Revised 10/21/16 WATER QUALITY LAB & OPERATIONS, INC. P.(}.BOY 115T BANNER ELK, NC 28804 (020)090'6277 CLIENT: BLUE RIDGE LADS LOGIN TIME: ADDRESS: PD.BOX 28W] SAMPLER - CITY: LEN0R RECEIVED DATE: STATE: NC Z|P2O545 REPORTED DATE: 27'Mar-19 RESULTS REPORTED BY: NCCERTIFIED LAB #544 PAUL|SEmH0UR.SUPERVISOR El o Blue Ridge Labs, Inc. P.O. Box 2940 Lenoir, NC 28645 Telephone (828) 728-0!49 Fax (328) 728-0131 Chain of Custody NPDS Reporting _ Groundwater _ Sanitary Landfill Hazrrdous Waste Industrial or QC R,Aa f&Sac dylW, UST/Trust Fund Reporting Bill To: Field iM State Reporting bl-�' Project Name:-CC-#A/6•1 JFJt— G�LCcM/C PO Number: Ice Present: Y pVJ Preservatives f.nh Check C-Composite G- Grab Sample ID Sample Type Date Time Time & Temp HR:MM °C Field Sulfide Check Y N Field Sulfide Present / Removed Y N Resid Chlor Field Check Y N i Field echlaination Y N pH Resid Chlor PorA Temp °C Sampler Initials Analysis Requested 71 !I Relinquished Bv: - Ott j P� ke/ Date: Time: Date: Time: Upon submission of samples, client agates that invoices auc due at the time work is completed. Open accounts are due D9 da)lffollowing invoice dale. A finance charge of 1.5%per month will be imposed ou ail paafuc accounts. When relinquishing samples to Blue Ridge L3hs (BRL), buyer authorizes BRL to perform only the analysis in chatted abgve and also agrees to pa)collection and attorney fees if the account becomes delinquent. Blue Ridge Labs mseoes the right to deny documentation for any work where payment has not been made, in effect rendering that data unsupported for regulatory purposes. BRL cannot guarantee that any regulatory authority will accept any work >ubmi:ted. tberefore it is the client's responsibility to request on this form appropriate tests. NC DBNR Certified Lah 9275 Forensic Environmental Services of NC, LLC r October 15, 2018 Schneider Electric 105 Summit Park Drive Salisbury, NC 28146 RE: Stormwater analysis for September 2018 event Dear Mr. Pitel, 00 N011035 a/viQ S3ll� 1H2f1N�0 6108 8 i 100 GDAG03LI Forensic Environmental Services of NC, LLC is pleased to submit the following analytical data for the stormwater sampling event that occurred September 2018. Thank you for letting Forensic Environmental Services of NC, LLC, assist you with your environmental and safety concerns. We look forward to working with you on future projects. Should you have any questions please do not hesitate to call @ 828-493-6325. Cordially, David Haynes, REM, REPA, CFC Owner / Manager Attachment: 4) N V-) Cj 1� � fo �P �0 4� I'l 01103S 2JJAa FIG Q 1100 P.O. Box 883• Hudson, NC 28638•Tel (828) 493-6325•Cell (828)493-1405 1--mail to envser a 1-mail.com 0 10 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client: Forensic Environmental Services of NC PO Box 883 Hudson, NC 28638 Attention: Mr. David Haynes Date Received: 18-Sep-18 Report Date: 12-Oct-18 Sample Date: 17-Sep-18 BRL #: BRL-2018-0763 Lab Sample ID: LSID-2018-02974 Client Sample ID: Outfall 1 - Schneider Electric Parameter Oil & Grease Ob blueridgelabslenoir@gmail.com Result MQL Unit Method * 5 mg/I 1664-A O&G Analysis Analysis Time Date Analyst 10/2/2018 WtrQtly Reported By: S. .Johnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 1 of 3 10 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Forensic Environmental Services of NC PO Box 883 Hudson, NC 28638 Attention: Mr. David Haynes Date Received: 18-Sep-18 Report Date: 12-Oct-18 Sample Date: 17-Sep-18 BRL #: BRL-2018-0763 Lab Sample ID: LSID-2018-02975 Client Sample ID: Outfall I - Schneider Electric Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst • Pb * 0.01 mg/I 200.7 1994 13:40 9/21/2018 KCJ Reported By: S. J. �RiWcssmger " Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 2 of 3 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Forensic Environmental Services of NC PO Box 883 Hudson, NC 28638 Attention: Mr. David Haynes Date Received: 18-Sep-18 Report Date: 12-Oct-18 Sample Date: 17-Sep-18 BRL #: BRL-2018-0763 Lab Sample ID: LSID-2018-02976 Client Sample Ill: Outfall 1 - Schneider Electric Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst •TSS 7.8 6.3 mg/l 2540D 1997 4500H+B 14:31 9/21/2018 KC1 pH 6.8 HT 0.1 su 200 17:12 9/18/2018 KCJ Reported By: S. J. Johns .R. Wessinger " Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 3 of 3 • E WATER QUALITY LAB & OPERATIONS, INC. P.O. BOX 1167 BANNER ELK, NC 28604 (828)898-6277 CLIENT: BLUE RIDGE LABS LOGIN TIME: ADDRESS: P.O. BOX 2940 SAMPLER: CITY: LENOIR RECEIVED DATE: STATE: NC ZIP 28645 REPORTED DATE: I D#: 12-Oct-18 ANALYSIS:::::::.::::: LSID # : ANALYSIS RESULTS MQL'sS UNITS],SAMPLE I LOCATION ANALYSIS DATE . ':;INT..; :; OIL & GREASE 2974 <5 5.00 MG/L 2-Oct-18 PI REPORTED BY: NC CERTIFIED LAB # 544 PAUL ISENHOUR, SUPERVISOR 0 NPDS Reporting Groundwater Report To' F,.464 ic_ 1 d�llo 5 • v Blue Rid Labs, Inc.. P.O. Box 2940 Lcnoir. NC 28645 Telephone (828) 728-0149 Fax (828) 728-0131 Chain of Custody Sanitary Landfill Hazardous Waste Industrial or QC Non State Reporting UST/Trust Fund Reporting Rill To: Project Name: z 6,f % fa c PO Number Ice PresenC Y N C-Composite Field Preservatives reservatives Lab Check G- Grab Sample ID Sample "Type Date Time Time & Temp IIR:MM °C Ficld Sulfide Check Y N Field Sulfide Present / Removed Y N Resid Chlor Field Check Y N Field Dechlorination Y N pl-1 Resid Chlur PorA Temp °C Sampler Initials Analysis Requested G%- 0oT1w1j' w Al I-I)s �`l' -rrss AA E RelinquishedBy: Date: Time: Recei. d 13 Date- Time:tw d /4�pj %7f- Upon submission ofsmnpl s. client agrees that invoices lire due u1 the time wotk is completed. Open accounts Lite due 20 duys dlowine, invoice date A Iinance charge of L? % per month ovill he imposed on all piWM accounts. When relinquishing samples to Blue Ridge Lahr (nRL), buyer authorizes nRl, to perlbnn only the analysis indimed above and also agreeS to pav collection and attorney fees it the account becomes delinquent. I41ue Ridge Labs reserves the ri_hl In deny documentation for any work where payment has nvl been made, in effect rendering that data unsupported for re_milatory purposes. nRl, cannot guarantee that any regulatory authority kill accept any work submitted, t1wrefiue it is the client's responsibility to rquul on this total appropriate tests. NC DFNR CrniGed Lab H275 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG080000 Date submitted t0131/2019 CERTIFICATE OF COVERAGE NO. NCGO8 O 5 8 3 FACILITY NAME SMneitler National Gamer COUNTY MedlenWrg PERSON COLLECTING SAMPLES Gary Lob LABORATORY Pace Lebmtory Lab Cent. p 5M2 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD ❑ Jan -June ❑li July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow [_]Watersupply ❑SA ❑Other CEIVE® PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Did this facility perform Vehicle Maintenance Activities using more t �5 g)l�y 2.6g5ew oil per month? ❑0 yes ❑ no (if yes. complete Part A) Part A: Vehicle & Equipment Maintenance Areas Monitoring RequjJ@"qIis((@PAEV1g ❑ No discharge this period' DWR SEc'TIONI Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -Polar Oil & Grease mg/L Total Suspended Solids, mg/L New Motor or Hydraulic Oil Usage, gal/mon Benchmarks - - 15 100 or SW - ParometerCode - 46529 00552 C0530 NCOIL SP1 10/16/19 >.25 <4.8 mg/L 60.8 SP3 10/16/19 >.25 <4.9 mg/L 340 SP4 10/16/19 >.25 <4.8 mg/L 1950 SP5 10/16/19 >.25 <4.9 mglL 130 SP6 10/16/19 >.25 <4.8 mg/L 396 ' Monthlysampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. ' For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Conversely, where fecal coliform results exceed the dilution upper limit, report the result as ">XX". Permit Date: 11/l/2018-5/31/2021 SWU-248, last revised 11/1/2018 Page 1 of 2 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) ❑ No discharge this period Outfall No. Date Sample Collected' (mo/dd/yr( 24-hour rainfall amount, Inches' Sample Collected' mo/dd/yr Total Suspended Solids, mg/L pH, Standard units Non -Polar Oil & Grease, mg/L Permit limit _ - 100 or Sir 6.0-9.0 15 Parameter code 46529 CO530 00400 00552 Footnotes from Part A also apply to this Part B Note: If you report a sample value In excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES [I NO IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail on original copy of this DMR, including all "No Discharge" reports. within 30 dPKs of receipt of the lob results for at end of monitocna period in the case of "No Discharge"reports) to Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." vt / Signature of ermittee Date Permit Date: 11/l/2018-9/31/2021 SWU-248, last revised 11/1/2018 Page 2 of 2 (�IaceAnalytica( xwwPscdaas.cum October 31. 2019 Mr. Michael DeBraske Schneider National, Inc. PO Box 2545 Green Bay, WI 543062545 RE: Project: SNI-Charlotte NC Pace Project No.: 92450171 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. DeBraske: Enclosed are the analytical results for sample(s) received by the laboratory on October 17, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Caryssa Berg, Schneider National Mr. Michael DeBraske, GEI Consultants, Inc. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Anaytcal Services, LLC. Page 1 of 15 acmnalytical e ewwpacdabs.= Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: SNI-Charlotte NC Pace Project No.: 92450171 Charlotte Certification We 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Flodda/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 15 laceAnalyfical' a»wpecdaba.clm SAMPLE ANALYTE COUNT Project: SNI-Charlotte NC Pace Project No.: 92450171 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92450171001 Sp-1 EPA 1664E AACt 1 PASI-C SM 2540D-2011 JP1 1 PASI-A EPA9040C ECH 1 PASI-A 92450171002 SP-3 EPA 1664E HH 1 PASI-C SM 2540D-2011 - JPi ,, 1 PASI-A r .. _ • r EPA 9040C ECH 1 PASI-A 92450171003 SP-4 EPA 1664B HH 1 PASI-C SM 2540D-2011 JP1 1 PASI-A EPA 9040C ECH 1 PASI-A 92450171004 SP-5 EPA 1664B HH 1 PASI-C SM 2540D-2011 JP1 1 PASI-A EPA 9040C ECH 1 PASI-A 92450171005 SP-6 EPA 1664B HH 1 PASI-C SM 2540D-2011 JP1 1 PASI-A EPA 9040C ECH 1 PASI-A 92450171006 SP-7 EPA 1664E HH 1 PASI-C SM 2540D-2011 JP1 1 PASI-A EPA 9040C ECH 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 15 laceAnalyficale w rpwetabs.mrn ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite too Huntersville, NC 28078 (704)875-9092 Project: SNI-Charlotte NC Pace Project No.: 92450171 Sample: SPA Lab ID: 92450171001 Collected: 10116/1908:48 Received: 1011711914:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO mg/L 4.8 1 10/30/19 12:29 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 60.8 mg/L 10.0 1 10/22/19 01:48 9040 pH Analytical Method: EPA 9040C PH at 25 Degrees C 6.5 Std. Units 0.10 1 10/28/19 15:39 H3 Sample: SP-3 Lab ID: 92450171002 Collected: 10/16/1908:55 Received: 1011711914:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease NO mg/L 4.9 1 10/30/19 16:02 M1 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 340 mg/L 17.9 1 10/22/19 0149 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.7 Std. Units 0.10 1 10/28/19 15:45 H3 ' Sample: SP-4 Lab ID: 92450171003 Collected: 10/16/1909:05 Received: 10/17/1914:00 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B - Oil and Grease NO mg/L 4.8 1 10/30/19 16:04 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 1950 mg/L 71.4 1 10/22/19 01:50 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.9 Std. Units 0.10 1 10/20/19 16:02 D6,H3 Sample: SP-5 Lab ID: 92450171004 Collected: 10/16/19 09:22 Received: 10/17/19 14:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease NO mg/L 4.9 1 10/30/19 16:04 Date: 10/31/2019 07:58 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 15 (�55'ceAnajfytical* wewpeca'absem ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SNI-Charlotte NC Pace Project No.: 92450171 Sample: SP-5 Lab ID: 92450171004 Collected: 10/16/19 09:22 Received: 10/17/19 14:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 130 mg/L 12.5 1 10/22/19 01:50 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 7.0 Sid. Units 0.10 1 10/20/19 16:36 - H3 Sample: SP-6 Lab ID: 92450171005 Collected: 10/16/1909:40 Received: 10/1711914:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease NO mg/L 4.8 1 10/30/19 16:04 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 396 mg/L 20.8 1 10/22/19 01:51 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.3 Sid. Units 0.10 1 10/20/19 16:47 H3 Sample: SP-7 Lab ID: 92450171006 Collected: 10/1611909:59 Received: 10/17/1914:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 4.9 1 10/30/19 16:04 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 228 mg/L 12.5 1 10/22/19 01:51 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.5 Std. Units 0.10 1 ` 10/20/19 16:53 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Dale: 10/31/2019 07:58 AM without the written consent of Pace Analytical Services, L-C. Page 5 of 15 ace Analytical a isw.peca'aAcoom Project: SNI-Charlotte NC Pace Project No.: 92450171 QC Batch: 506605 QC Batch Method: EPA 1664B Associated Lab Samples: 92450171001 METHOD BLANK: 2720433 Associated Lab Samples: 92450171001 Parameter Units Oil and Grease mg/L QUALITY CONTROL DATA Analysis Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO - 4.8 10130/1910:53 Pace Analytical services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2720434 Spike 1-CS 1-CS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/1- 38.5 32.9 86 78-114 MATRIX SPIKE SAMPLE: 2720435 92449952001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 1.7J 38.5 33.3 82 78-114 Results presented on this page are In the units Indicated by rim -units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2019 07:58 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 15 m aceAnalytical ewwCecNeos.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SNI-Charlotte NC Pace Project No.: 92450171 QC Batch: 506716 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92450171002, 92450171003, 92450171004, 92450171005, 92450171006 , METHOD BLANK: 2720937 Matrix: Water Associated Lab Samples: 92450171002, 92450171003, 92450171004, 92450171005, 92450171006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L -s NO - 5.0 10/30/19 16:01 LABORATORY CONTROL SAMPLE: 2720938 Spike LCS LCS % Rec Parameter Units Conic. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 39.3 98 78-114 MATRIX SPIKE SAMPLE: 2720939 92450171002 Spike MS Ms % Rec Parameter Units Result Conic. Result % Rec Limits Qualifiers Oil and Grease mg/L NO 38.5 5.4 5 78-114 M7 Results presented on this page are in the units Indicated by Uu, "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2019 07:58 AM without the written consent of Pace Analytical Services, L-C. Page 7 of 15 (�55'ceAnajfyfical' aww.pecdaas.corn QUALITY CONTROL DATA Project: SNI-Charlotte NC Pace Project No.: 92450171 QC Batch: 504884 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92450171001, 92450171002, 92450171003, 92450171004, 92450171005, 92450171006 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 METHOD BLANK: 2713030 Matrix: Water Associated Lab Samples: 92450171001, 92450171002, 92450171003, 92450171004, 92450171005, 92450171006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L NO 2.5 10/22/19 01:45 LABORATORY CONTROL SAMPLE: 2713031 Spike LCS LCS % Rec Parameter Units Conic. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 242 97 90-110 SAMPLE DUPLICATE: 2713038 92450171001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 60.8 63.2 4 SAMPLE DUPLICATE: 2713039 92450171003 Dup Parameter Units Result Result RPD Qualifiers -Total Suspended Solids mgf- 1950 2130 9 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2019 07:58 AM without the written consent of Pace Analytical Services, L-C. Page 8 of 15 aceAnalytical wascpscalaes.00m QUALITY CONTROL DATA Project: SNI-Charlotte NC Pace Project No.: 92450171 QC Batch: 504653 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92450171003, 92450171004, 92450171005, 92450171006 SAMPLE DUPLICATE: 2711979 92450171003 Cup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 6.9 6.5 7 D6,113 SAMPLE DUPLICATE: 2711980 92449833003 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 5.5 5.6 3 D6,H3 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units Indicated by the "units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2019 07:58 AM without the written consent of Pace Analytical Services, L-C. Page 9 of 15 (�5ace Analytical owwpacefeescorn QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SNI-Charlotte NC Pace Project No.: 92450171 QC Batch: 506001 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92450171001, 92450171002 SAMPLE DUPLICATE: 2718169 92449718001 Cup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Sid. Units 6.9 6.7 3 D6,1-13 e .. , , SAMPLE DUPLICATE: 2718170 Parameter Units pH at 25 Degrees C Sid. Units 92450780002 Cup Result Result 5.8 5.3 RPD Qualifiers 10 D6,H3 Results presented on this page are In the units Indicated by the'Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2019 07:58 AM without the written consent of Pace Analytical Services, U.C. Page 10 of 15 (�15'ceAnalyficai' w pecdaDtcnm QUALIFIERS Project: SNI-Charlotte NC Pace Project No.: 92450171 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyze in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyle is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyze is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 10/31/2019 07:58 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 15 laceAnalyficaI9 m .Pewob&corn Project: SNI-Charlotte NC Pace Project No.: 92450171 Lab ID Sample ID 92450171001 SP-1 92450171002 SP-3 92450171003 SP4 92450171004 SP-5 92450171005 SP-6 92450171006 SP-7 92450171001 SP-1 92450171002 SP-3 92450171003 SP4 92450171004 SP-5 92450171005 SP-6 92450171006 SP-7 92450171001 SP-1 92450171002 SP-3 92450171003 SP4 92450171004 SP-5 92450171005 SP-6 92450171006 SP-7 Date: 10/31/2019 07:58 AM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE QC Batch Method QC Batch Analytical Method EPA 16648 506605 EPA 1664E 506716 EPA 1664B 506716 EPA 1664B 506716 EPA 1664B 506716 EPA 1664B 506716 SM 2540D-2011 504884 ' SM 2540D-2011 504884 SM 2540D-2011 504884 SM 2540D-2011 504884 SM 2540D-2011 504884 SM 2540D-2011 504884 EPA 9040C 506001 EPA 9040C 506001 EPA 9040C 504653 EPA 9040C 504653 EPA 9040C 504653 EPA 9040C 504653 REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in full, without the written consent of Pace Analytical Services, -LC. Analytical Batch Page 12 of 15 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Receipt(SCUR) Page 1 of 2 aceAWlytiral- Document No.: IssuingAuthoriry: F.CAR-CS-033-Rev.06 Pace Carolinas Q"Iity Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville �/ Raleigh❑ Mechanicsville El Custody Seal Present? ❑Yes QNo "Seals Intact? ❑Yes [DNo Packing Material: ❑Bubble Wrap ❑ ubble Bags ❑None ❑ Other ThermometerType of ice: Qw� ❑Blue IIs• can ID: 92T049 Cooler Temp ('Cl: 11 Correction Factor: "AAd/Subtract (-C) - 0.0 Cooler Temp Corrected ('CI: ! USDA Regulated Soil, ([3 N/A, water sample) Did samples orlginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? WO#:92450171 III1101E11111111I111Ili - 92450171 cf(( Date/Initials Perwn Examining Comems:",r�/���-/ Blologica!�Jslue Frozen? ❑Yes [21No ❑N/A ❑None Temp should be above freezing to WC ❑samples out of temp critena. Samples on ice, cooling process hasbegun Did samples originate from a foreign source (internationally, .. m.nV rhea F-INn Yes LjWo .....__..,.._..___._.___ Comments/dsae an Chain of Custody Present? � BY-. Q1. N/A s' Samples Arrived within Hold Time? (]Ya ONO N/A 2. Short Hold Time Analysb 02 hr.? Yes N/A 3. Rush Tom Around Time Requested? Yeses No N/A a. Sufficient Volume? — yes ONO N A S. CorreaContainersUsed? []Y�y°' ONO ❑N/A 6. -Pace Containers Used? Yes No N/A Containers Intact? a Yes ONO N/A 7. — Diiiolved analysis: Samples Field Fihered? Oyes No f N/A a. ' ' Sample Labels Match COC? QYes ONO ❑N/A 9. -hscludes Date/Time/ID/Analysis tRatrix: s ace in VOA Vials (a5.6mm)? Yes No N A 10. lank resent? tri Oyes Offo ❑N� 11. lank Custody Seals Present? OYes QNO ' N/A COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION ' field Data Required? UYta L)NO Person contacted: _% Datefrime: Project Manager SCURF Review: N " Date: Project Manager SRF Review: �61iL— Date: 0 Page 13 of 15 Document Name: Document Revised: February 7, 2019 Sam le Condition U on Recel t(SCUR Page 2 of 2 aceAnaryfical Document No.: issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorinatlon Is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLH8 "Bottom half of box Is to list number of bottle Project If 1 O# ; 92450171 PM: RWC Due Dale: 10/31/19 CLIENT: 82-SCHNEIDER — _ ^ V Q Q N 2 v Z � a y I V u = � n c c N 8 i ry i_ u J 8 s E i i' 8 x s - 'E y .�. _ E c r. y Z E E a a aNp Eo a a j o n` aa E E n `u E E E E E E E E� a w of m of 8 n c SE -°v1 �13w a E J J i Y Z e Y i n O' O „�} Va ii U' r�+l t� r✓1, l! N p U' y N n O m m ro m m u 3 a a a a a �Y ; -m m m 1 I � 2 I I 2 3 I � 2 4 5 I I - I / 7 6 9 IO I1 l2 pH Adjustment log for Preserved Samples sample ID Date preservation adjusted Time preservation adjusted AMDUM of Preservadre added Lot a TT7 _.__,.____.___,_.-.........r.r,:.L..n,—illh.....,1.lh.Nnnh[arolina DEHNR CMIflcation Office (i.e. Note: Whenever mere H a UHcrepdncY dim"..a..m... �..""�.. .....r__..__._ __,___-.- Out of hold, Incorrect preservallve, Out of temp, Incorrect containers. a Page 14 of 15 /i+xeauMial' CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be wmpleted accurately. Becton A Sect B section C Reaelmd CRent Inf..alan: Required Project lnfpmallon: Invoice Infamutlon: Page, 1 Of 1 Ca Y: Stdlroider Natiaal RopM To: Gatyl.ad Alt.t. Addmfa: 2420 Stwto Road Copy To: Campani, Nam: C"Mlte. NC 28269 i ACdrese: - Racralmn, Aaaaricy Email: C ct- �' -7 L,'1 pisvnace Order n; Pace CWtc PIvxY: TOc 99�Ta10 Faz lFI0,W Name: SN4Cfurbl4, NC Pose Prajw Manager: vs,,ran ae.tan, 'State I Loradon Re aiesteo Due Date: 1p,aci 0 jpacePMdi,c 2601-1 NC ' R uasrod Aral a Fillarad YM a s Z 9 COLLECTED z Preservatives > - a„1a,,, aKrt arn�reNYw aV a 8 u nwe s r SAMPLE ID a0 tt E 0 u START END p N ar F S $ ono ehuaeror per c N-Las/.-1 N. oT De N C TDAIETI.Z "t [ 0� Z. i2 0 F Samp 0Ida moat tmiaue Tn T. w � e y r m e g p a O_ p o Q o m 3 DATE TIME z t s z i 0 r n 7JD ll I A 001 1 SP.1 � YJT � _ - X % x � I I I I 2 spa var x x x ^ � QV 3 sp+ WT x x x , . 5 p91- a sP.s wr p9 x x x 005 B SPL J WT % X is . 1 09 6 SPa S Wr USS x x x.. P ,e 9 . 9 _1DjI ,2 ..� ADDITIONAL co"EMB .. . r [<, RELINlxIB11FD 8Yl AFFlWl10N a � , Ti -STYE - AwEPTED BYIAFF4IAPON DATE TIME ... SAMPIE CONCNIONB . SAMPLER NiME AND SIGNATURE $ c $ - PRINT Namv of SAMPLER: /' t0 m uRRy ,Gofa d Y a _ $ a 3$ v _ �� 2 SIGNATURE of SAMPJ DAOTE i etl N r a=L gnu" c� 0 N U , U