Loading...
HomeMy WebLinkAboutNCG080014_MONITORING INFO_20200113PERMIT NO. DOC TYPE DOC DATE STORMWATER DIVISION CODING SHEET NCG PERMITS �cG L/ ❑ HISTORICAL FILE L�( MONITORING REPORTS ❑ oaD �l l fS YYYYMMDD DocuSign Envelope ID: 28DD87B2-A97D-4D07-AB00-C42F6AF440CF SMITH+GARONER ENGINEERS January 8, 2020 NCDEO Division of Water Resources Attention: Central Files 1601 Mail Service Center Raleigh, NC 27699-1617 ABOREss TH WEB 14 N. Boylan Avenue. Raleigh NE 27603 919.820.0577 www.smithgardne6nc.com RE. Year Two, Period 2, DMR —July 1— Becember 31, 2019 GFL Environmental, LLC — Garner Transfer Station Certificate of Coverage#NCGo80014 ECEfVED General Permit#NCG0000o0 JAN 13 1020 DENtF9AL FELES Dear Sir/Madam: SECT1pN Smith + Gardner (S+G) is pleased to submit this Year Two, Period 2 Discharge Monitoring Report (DMR) for stormwater monitoring at the GFL Environmental, LLC — Garner Transfer Station. The facility is permitted to discharge stormwater related to activities that have Vehicle Maintenance Areas under Certificate of Coverage (CDC] No. NCG080014, General Permit No. 080000. Samples were obtained from Outfatt 001 and Outfall 002 during the Year Two, Period 2 sampling event. The sample from Outfatt 001 exceeded the benchmark threshold for total suspended solids (TSS). For Outfatt 001, this is the second exceedance in a row for TSS. Outfall 001 has now entered Tier 2 status. Monthly sampling for Outfall 001 will begin in 2020. Semiannual sampling will continue during the first half of 2020 for Outfall 002. We are providing you with two (2) copies of the DMR for this submittal. If you have any questions, or require further information, please contact us at (919) 828-0577 or by email. Sincerely, SMITH GARDNER, INC. Oocu5lgned by: fA Ec9LP3�4�c... Staff Engineer, ext. 170 iessefasmithgardnerinc.com Attachments CC: Jordan Weiner (GFL) File Ee signed by: sta" Q. Sw,lflE, 3369FBAN896,145... Stacey A. Smith, P.E. Senior Engineer, ext. 127 staceyfasmithgardnerinc.com I I:\Pmjtcls\Waste InduStne, (Garner Tansftr Swwt, rarner 15.1 INPUS.vW St., mwater Sewices(2019@II 2U1ADEMLRr:pdes 2nd 2019dor, DocuSign Envelope 10: 28DD87B2-A97D-4D07-AB00-C42F6AF440CF This page intentionally left blank. DocuSign Envelope ID: 28DD87B2-A97D-4D07-AB00-C42F6AF440CF Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Resources General Permit No. NCG080000 CERTIFICATE OF COVERAGE NO. NCGOS 0 0 1 4 FACILITYNAME GFL Environmental,Inc. -Gamer Transfer Station COUNTY Wake PERSON COLLECTING SAMPLES Mary C. Kennamer LABORATORY Pace Analytical Lab Cert. ti 37738 Comments on sample collection or analysis: Date submitted January 7, 2020 SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD ❑ Jan -June ❑■ July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow [_]WaterSupply [:]SA OOtherC;NSw PLEASE REMEMBER TO SIGN ON THE REVERSE � Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?Q yes Ono (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period' Outfall No. Date Sample Collected, mo/dd/yr 00530 00400 00556 Total Suspended Solids, mg/L pH, Standard units Non -Polar Oil and Grease/TPH EPA Method 1664 (SGT-HEM), mg/L New Motor Oil Usage, Annual average gal/mo Benchmark 50 or 100 see permit Within 6.0 — 9.0 15 - 001 12/13/2019 103 8.2 <5.0 500 002 12/13/2019 22.4 7.1 <5.0 500 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) Outfall No. Date Sample Collected, mo/dd/yr 00556 00530 00400 Non -Polar Oil avid Grease/TPH EPA Method 1664 (SGT-HEM), mg/L Total Suspended Solids, mg/L pH, Standard units Permit Limit 15 50 or 100 see permit 6.0 — 9.0 I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. S W U-250 last revised April 11, 2013 Page I of 2 DocuSign Envelope ID: 28DD87B2-A97D-4D07-AB00-C42F6AF440CF STORM EVENT CHARACTERISTICS: Date 12n3i2019 (first event sampled) Total Event Precipitation (inches): 1_5 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No in the case of "No Discharae" resorts) to: Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 within 30 the lab results (or at end YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." - �DocuSlgned by: (Signature of 1/8/2020 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab- SWU-250 last revised April 11, 2013 Pace 2 of DocuSign Envelope ID: 28DD87B2-A97D-4D07-AB00-C42F6AF440CF Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Resources General Permit No. NCG080000 CERTIFICATE OF COVERAGE NO. NCG08 0 0 1 4 FACILITY NAME GFL Environmental,Inc. -Gamer Transfer Station COUNTY PERSON COLLECTING SAMPLES Mary C.Kennamer LABORATORY Pace Analytical Lab Cent. q 37738 Comments on sample collection or analysis: Date submitted January 7, 2020 SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD ❑ Jan -June ❑■ July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA []Zero -flow ❑Water Supply [:]SA Mother c;Nsw PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?❑✓ yes Ono (if yes, report your analytical results in the table immediately below) Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable) ❑ No discharge this period' Outfall No. Date Sample Collected, mo/dd/yr 00530 00400 00556 Total Suspended Solids, mg/L pH, Standard units Non -Polar Oil and Grease/TPH EPA Method 1664 (SGT-HEM), mg/L New Motor Oil Usage, Annual average gal/mo Benchmark - 50 or 100 see permit Within 6.0 — 9.0 15 001 12/13/2019 103 8.2 <5.0 500 002 12/13/2019 22.4 7.1 <5.0 500 Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable) Outfall No. Date Sample Collected, mo/dd/yr 00556 00530 00400 Non -Polar Oil and Grease/TPH EPA Method 1664 (SGT-HEM), mg/L Total Suspended Solids, mg/L pH, Standard units Permit Limit 15 50 or 100 see permit 6.0 — 9.0 I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. SWU-250 last revised April 11, 2013 Page I of 2 DocuSign Envelope ID: 28DD87B2-A97D-4D07-AB00-C42F6AF440CF STORM EVENT CHARACTERISTICS: Date 12/13/2019 (first event sampled) Total Event Precipitation (inches): 1_5 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports), to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations," DocuSlgned by: , 6rk,ln, WUTAkr (Signature of 1/8/2020 (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab- SWU-250 last revised April 11, 2013 Pa"e 2 of 2 ,...: ,xa,..�.......,,, ,.. mme ie iai N3NS" 9loz uer 01009093N 9M 83 N 9HV9+Hll WS NDI111Stl315N131tl3NtlV9 531tl15DON131SIM z NMOHSSV 's'os YT0 dVW 311S F g Y bi rY �Y R ry R o 0 3 E A s ;Jig I I Q I In @; c 1 I 1 1 1 0 9 %✓ Oi J%L a E e — r 0 PAV9jZYJ-008d-L00Yi3LBd-Z8L9O09Z :01 edolanu3 uBign�a DocuSi n Envelope ID: 28DD87B2-A97D-4D07-AB00-C42F6AF440CF c eAnalytical lwww.pecalaps.com December 24, 2019 Mary Kennamer Smith Gardner, Inc 14 N. Boylan Ave Raleigh, NC 27603 RE: Project: Garner 15-1 Pace Project No.: 92457389 Dear Mary Kennamer: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704P75-9092 Enclosed are the analytical results for sample(s) received by the laboratory on December 13, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, 4W,� pl�--D Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, without the written consent of Pace Analytical Services, LLC. Page 1 of 12 DocuSi n Envelope ID: 28DD87B2-A97D-4D07-AB00-C42F6AF440CF Pace Analytical Services, LLC s 9800 Kincey Ave. Suite aceAnalytical HunleSville, NC 2807878 wwr.pw:grtEscom (704l875-9092 CERTIFICATIONS Project: Garner 15-1 Pace Project No.: 92457389 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 12 9 DocuSi n Envelope ID: 28DD87B2-A97D-4007-AB00-C42F6AF440CF Pace Analytical Services, LLC �aceAnalytical` 9800 nceyAve. 2800 Huntersviile, NCC28078 www.pacdabs.cam (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Garner 15-1 92457389 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92457389001 001 EPA 1664E HH 1 PASI-C SM 2540D-2011 MJP 1 PASI-A EPA 9040C ECH i PASI-A 92457389002 002 EPA 1664E HH 1 PASI-C SM 25400-2011 MJP 1 PASI-A EPA 9040C ECH 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the wiitlen consent of Pace Analytical Services, LLC. Page 3 of 12 75Cvelope ID: 28DD87B2-A97D-4D07-AB00-C42F6AF440CF pace Analytical Services, LLC eAnalytical• 9800 Kincey Ave. Suite100 Huntersville, NC 28078078 YWW.DataNEt.001a (704)875-9092 ANALYTICAL RESULTS Project: Garner 15-1 Pace Project No.: 92457389 Sample: 001 Lab ID: 92457389001 Collected: 12/13/19 10:10 Received: 12/13/19 13:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 12/23/19 13:30 2540D Total Suspended Solids Analytical Method: SM 25400-2011 Total Suspended Solids 103 mg/1- 16.7 1 12/19/19 05:23 . 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 8.2 Sid. Units 0.10 1 12/22/19 18:52 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/24/2019 12:21 PM without the written consent of Pace Analytical Services, LLC, Page 4 of 12 DocuSi n Envelope ID: 28DD87B2-A97D-4D07-AB00-C42F6AF440CF Pace Analytical Services, LLC cKincey Ave. Suite 100 eAnalytical • 9800 Huntersville, NC 28078 vw.Wcd>tM.com (704)075-9092 ANALYTICAL RESULTS Project: Garner 15-1 Pace Project No:: . 92457389 Sample: 002 Lab ID: 92457389002 Collected: 12/13/19 10:00 Received: 12/13/19 13:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO mg/L 5.0 1 12/23/19 13:30 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 22.4 mg/1- 5.0 1 12/19/19 05:23 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 7.1 Sid. Units 0.10 1 12/22/19 18:46 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 12/24/2019 12:21 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 12 DocuSi n Envelope ID: 28DD87B2-A97D-4D07-AB00-C42F6AF440CF Pace Analytical Services, LLC �aceAnalyticals 9800 KinceyAve. Suite100 Huntersviile, NC 26076 wwy.DatlfAf.cem (704)875-9092 QUALITY CONTROL DATA Project: Garner 15-1 - Pace Project No.: 92457389 QC Batch: 516302 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92457389001. 92457389002 METHOD BLANK: 2766250 Matrix: Water Associated Lab Samples: 92457389001, 92457389002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L NO 5.0 12123/19 13:24 LABORATORY CONTROL SAMPLE: 2766251 Spike LCS LCS % Rec Parameter Units Conc. Result %Rec Limits Qualifiers Oil and Grease nrl 40 36.3 91 78-114 MATRIX SPIKE SAMPLE: 2766252 92456757002 Spike MS MS % Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Oil and Grease ml 27.0 40 60.5 84 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/24/2019 12:21 PM without the written consent of Pace Analytical Services, -I-C. Page 6 of 12 IF a 7velope ID: 28DD87B2-A97D-4D07-AB00-C42F6AF440CF ceAnalytical www.fra l scam Project: Garner 15-1 Pace Project No.: 92457389 QC Batch: 515678 OC Batch Method: SM 254OD-2011 Associated Lab Samples: 92457389001, 92457389002 METHOD BLANK: 2763253 Associated Lab Samples: 92457389001, 92457389002 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 2763254 Parameter Units Total Suspended Solids mg/L QUALITY CONTROL DATA Analysis Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)075-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 2.5 12/1911905:22 Spike LCS LCS % Rec Conc. Result %Rec Limits Qualifiers 250 238 95 90-110 SAMPLE DUPLICATE: 2763282 92457431005 Dup Parameter Units Result Result Total Suspended Solids mg/L 2540 3240 SAMPLE DUPLICATE: 2763283 92457431007 Dup Parameter Units Result Result " Total Suspended Solids mg/L 5980 3350 RPD Qualifiers 24 RPD Qualifiers 56 D6 Results presented on this page are in the units indicated by the 'Units- column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 12/24/2019 12:21 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 12 Doci n Envelope ID: 28DD87B2-A97D4D07-AB00-C42F6AF440CF �ceAnalytical WWW.pepalaEe.Celll QUALITY CONTROL DATA Project: Garner 15-1 Pace Project No.: 92457389 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 r Huntersville, NC 28078 (704)875-9092 QC Batch: 516221 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92457389001, 92457389002 SAMPLE DUPLICATE: 2765971 92456956004 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Sid, Units 6.3 6.2 2 D6,H3 SAMPLE DUPLICATE: 2765972 92457381001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Sid. Units 8.2 8.1 1 H3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/24/2019 12:21 PM without the wniten consent of Pace Analytical Services, L-C. Page 8 of 12 7DocuSi n Envelope ID: 28DD8782-A97D-4D07-AB00-C42F6AF440CF aceAnalytical vw.pauleEa.com QUALIFIERS Project: Garner 15-1 Pace Project No.: 92457389 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. POL - Practical Quantitation Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 RL- Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPAguidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyle is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except In full, Dale: 12/24/2019 12:21 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 12 7DocuSi n Envelope ID: 28DD87B2-A97D-4D07-AB00-C42F6AF440CF aceAnalytical" rwr.DeceleEs.cem QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Garner 15-1 Pace Project No.: 92457389 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92457389001 001 EPA 1664E 516302 92457389002 002 EPA 1664E 516302 92457389001 001 SM 2540D-2011 515678 92457389002 002 SM 2540D-2011 515678 92457389001 001 EPA 9040C 516221 92457389002 002 EPA 9040C 516221 Date:. 12/24/2019 12:21 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch Page 10 of 12 Z t 10 Z t 96ed *Check mark top half of box If pH and/or dechlorination is Project; WUM : UZ451389 verified and within the acceptance range for preservation samples. PM: NNB Due Date: 12/24/19 Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg CLIENT: 92—RSDBA NC •*Bottom half of box is to list number of bottle o e n e c @ J J J p a n a E of E t J 3 J � m m m d e m 6 r 0 T .�.. n E m S o 2 J of to m u < 2 a E 0 Z n E m yz y id V u E a ?i ty N g c J Q � _ O S E¢ Q Q j 1 J E J Q � j$( N S a E Q to Q J o 2 E ¢ Q o Z n o -t n 1 ¢ t7 J �a O � .o i > n c O E J \_ $ d m O E � c i •S > ys > ° > q E � M1 E OE �i N. an i Z J E N m 5 e J p p Q a c q E O S P n c J E O S 1 2 I 3 4 6 8 9 10 ll 12 IN I I k NNN PH Adjustment Log for Preserved Samples Sample ID Type of Preservable pH upon recelpt Date presematlon adjusted time praservatlon adjusted Amount of preservatN9 added Lot C Nate• whenever there Is a disueoanev affectim North Carolina compliance samples, a copy of this Pone will be sent to the North Carolina OEHNR Certification Office (i.e. Out of hold, Incorrect presemattm am of temp, incorrect contenpn. d00bbdV9dZV0-009V-L004-0L6V-Z8L9009Z :1]I 9d0l9nu3 uOiSnood