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Home My WebLink AboutNCG060286_MONITORING INFO_20191208STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. NCG d DOC TYPE ❑ HISTORICAL FILE MONITORING REPORTS DOC DATE ❑ l�.I I o YYYYMMDD November 21, 2019 CERTIFIED MAIL WITH RETURN RECEIPT ARTICLE NO: 7017 0530 0000 0188 3409 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED DEC U 8 2019 CENTRAL FILES DWR SECTIOPi Re: Reporting Year 2019 —Storm Water Discharge Monitoring Report Kellogg's Snacks — Cary Bakery One Quality Lane Cary, North Carolina Dear Sir/Madam, w � r f SNACKS Kellogg's Snacks Cary Bakery Operations One Quality Lane Cary, NC 27513 Ph 919.677.3200 Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the October and November 2019 monitoring events for: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm Water General Permit No. NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is: Mr. Mark Logue (919)677-3292 mark.logue@kellogg.com Mr. Logue is available should any questions or problems arise during the review of this DMR. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Sincerely Ste a Suro c Plant Manager Enclosures STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG060000 CERTIFICATE OF COVERAGE NO. NCG06 0 2 8 6 FACILITY NAME Kellogg's Snacks - Cary Bakery COUNTY `Hake PERSON COLLECTING SAMPLES Mark Logua LABORATORY ENCO Laboratories Date submitted 11/21/19 SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or Q Monthly' October & Novemberlmonthl Lab Cert. If 591 & 443 DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA *Other C, NSW FACILITY ACTIVITIES INCLUDE (check all that apply): ❑ use/process meats ❑ use animal fats/byproducts Part A• Stnrmwater Renchmarks and Monitorine Results PLEASE REMEMBER TO SIGN ON THE REVERSE --> Total event rainfall 202 & 0.2 or ❑ No discharge this period' Outfall No..Date ' Sample' :Collected; mo/dd/yr. TSS, ' rrg/L - �pH, ,S1:aridard units COD, mg/L Oil, and Grease, . mg/L Fecal Coliform, Colonies per, 100 ml Enterococci, Colonies per 100 ml Benchmark. ' - - 100 or'504 : '.Within 6:0=9.0 .120 30_ .loco' 5001 Parameter Codes ' '- - -CO530-, 00400 - 00340 00556 31616 61211, swot 10/13/19 52 6.1 5800 2,59 J NA NA swot 1111W9 32 6.0 530 11.50 NA NA ' Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 'Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new oil per month? ❑ yes ❑■ no (if yes, complete Part B) Permit Date: 11/l/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Date Sample Collected (mo/dd/yr)' 24-hour rainfall amount, incheS2 New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 - C0530 Footnotes from Part A also apply to Part B *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. * TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES Q NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES Q NO ❑ REGIONAL OFFICE CONTACT NAME: Thad valentine Mail an original copy of this DMR including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge' reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonmWono ing violations." '-� Sienat a of Permittee Date Permit Date: 11/1/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 2 of 2 r�e F ► C0 Laboratories Accurate. Timely. Responsive. Innovative. 102-A woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, November 20, 2019 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Mark Logue ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater ENCO Workorder(s): CC18972 Dear Mark Logue, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, November 12, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, ou'-s-ull Chuck Smith Project Manager Enclosure(s) FINX This report retinas only to the sample as recervea by the laboratory, and may only be reproduced in U. Gape 1 of 8 eNS -a www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE ClientlD: SW01 Lab ID: CC18972-01 Sampled: 11/12/19 08:15 Received: 11/12/19 0855 Parameter Preparation Hold Date/T'mefs) Preo Date/Time(s) Analysis Date/Time(s) EPA 1664B EPA 1664B 12/10/19 11/18/19 11:13 11/19/19 10:25 SM 254OD-2011 NO PREP 11/19/19 11/18/19 12:52 11/18/19 12:52 SM 5220D-2011 Same 12/10/19 11/14/19 11:35 11/14/19 16:40 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In lull. Page 2 or 8 Client ID: SW01 Chemical Oxygen Demand Total Suspended Solids SAMPLE DETECTION SUMMARY 530 10 10 mg/L 32 8.3 8.3 mg/L www.encolabs.com SM 5220D-2011 SM 2540D-2011 FINAL This report relates Only t0 the sample a5 received by the labOrahay, and may Only be repoW OCed in AN. Page 3 of 8 Description: SW01 Matrix: Surface Water Project: Stonnwater Classical Chemistry Parameters ^ - ENCO Cary rerplicd a/xlyle(NC 5911 Analyte fCAS Numberl Chemical Oxygen Demand^ Total Suspended Solids^ Classical Chemistry Parameters ^-EACOJacks Wle 777717,111,7.11 Analyte [CAS Numberl Oil & Grease (HEM) [C-00i EN w- - www.encolabs.com ANALYTICAL RESULTS Lab Sample ID: CC18972-01 Received: 11/12/19 08:55 Sampled: 11/12/1908:15 Work Order: CC18972 Sampled By: Greg Kanellis Results Fig Units OF MDL PQL Batch Method Analyzed By Notes 530 nni 1 10 10 9KI4025 SM 5220D-2011 11/14/19 16:40 JOE 32 mg/L 3.33 8.3 8.3 91 SM 254OD-2011 11/18/1912:52 BDC Results flag u";rs PE MDL p2 Bush !Method < 1.50 mg/L 1 1.50 5.00 9K18005 EPA 1664B Analyzed @x Notes 11/19/19 10:25 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 4 of 8 vvwvv.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9K14025 - Same Blank (9K14025-BLK1) Prepared: 11/14/2019 11:35 Analyzed: 11/14/2019 16:40 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (9K14025-BS1) Prepared: 11/14/2019 11:35 Analyzed: 11/14/2019 16:40 Spike Source %REC RPD .Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes - ChemicalOxygen Demand 510 10 mg/L 500 101 90-110 Matrix Spike (9K14025-MS1) Prepared: 11/14/2019 11:35 Analyzed: 11/14/2019 16:40 Source: CC12339-01 Spike Source %REC RPD .Arai Result Flag POL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 690 10 mg/L 526 210 92 90-110 Matrix Spike Dup (9K14025-MSD1) Prepared: 11/14/2019 11:35 Analyzed: 11/14/2019 16:40 11 Source: CC12339-01 .Analvte Chemical Oxygen Demand Batch 91(18021 - NO PREP Result Flag POL 690 10 Spike Source %REC RPD Units Level Result %REC Limits RPD Limit Notes mg/L 526 210 93 90-110 0.3 5 Blank (9KI8021-BLKI) Prepared &Analyzed: 1 l/ 18/201912:52 Spike Source %REC RPD Analvte Result Flag POL m Level Result %REC Limits RPD Lilt Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (9KIS021-BSI) Prepared & Analyzed: 11/18/2019 12:52 Spike Source %REC RPD .Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 92 2.5 mg/L 100 92 80-120 Duplicate (9KI8021-DUPl) Prepared & Analyzed: 11/18/2019 12:52 Source: CC19184-03 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 110 32 mg/L 120 8 20 Duplicate (9K1B021-DUP2) Prepared & Analyzed: 11/18/2019 12:52 Source: CC19184-04 Spike Source %REC RPD Analvte Result Flag POL Units Level Result o/ REC Limits RPD Limit Notes Total Suspended Solids 480 210 mg/L 530 9 20 Classical Chemistry Parameters - Quality Control Batch 9K18005 - EPA 1664E Blank (9)(18005-BLK3) Prepared: 11/18/2019 11:13 Analyzed: 11/19/2019 10:25 Spike Source %REC RPD Analvte Result Flag POL Units Level B41Llt %REC Limits RPD Limit Notes Oil &Grease (HEM) 1.50 U 5.00 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 8 EJVCO www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9K18005 - EPA 16648 - Continued LCS (9K38005-BS1) Prepared: 11/18/2019 11:13 Analyzed: 11/19/2019 10:25 Spike Source %REC RPD Analvte Result Flaq FOOL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 152 5.00 mg/L 162 94 78-114 LCS Dup (9KI8005-BSDI) Prepared: 11/18/201911:13 Analyzed: 11/19/2019 10:25 Spike Source PAREC RPD Analvte Result Flaq P0L Units Level Bes91L %REC Lim' RPD Limit Notes Oil &Grease (HEM) 165 5.00 mg/L 160 103 78-114 8 18 Matrix Spike (9KI8005-MSI) Prepared: 11/18/2019 11:13 Analyzed: 11/19/2019 10:25 Source: SC04648-01 Spike Source %REC RPD .Analy[e Result Flaq PQL Units Level Result %aREC Limits RPD Limit Notes Oil & Grease (HEM) 174 5.00 mg/L 158 30.9 90 78-114 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduC a In 011. Page 6 of 8 EN www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALL] Calculated analyte - MDUMRL reported to the highest reporting limit of the component analyses. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In hull. Page 7 of 8 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD tons Mimi Orlando FL ffi824 Oc 4010 Jacksoommmo Park Court, mille, FL 216 6069 Suite n t Cary N(:�51 tus mdusm.i Q. KOD (407) 828-5314 F. (407) 850-6945 (904f 29E3007 F. (904) 296-6210 (919f a67 3090 Fm li•t9t 45%-35t5 www.encolabs.com Page —I_ of C11am Name KELLOGGS SNACKiIAUSTIN FOODS OCE006) P,dW Numoe( [none] e, Requested Analyses Requested Turnatouno Times Note : Rush roquess suolecl !n a«.Wadee by me :deney _ Standard Expedited Due — - - `J-I Lab Workorder N � inc L 0) O V An. D L.) � T1 � Address ONE QUALITY LANE Prober Nemomex Storrnweter CM/BTa, CARY, NC 27513- PO a / Billin9 fined Tat (919) 877 3519 Fos 0 - Reporting Conran Mark Logue Samplege) Nadia, Aniiiation (Pont) v 6 Biting Cor tan Accounts Payable y Samplans)Sig to ' ! i Sto L«aeon /Time 2ana Preaervetlon !Sea Codasr �Comoma as n.xassurv) hand N Sample ID (Field Idenu(leamn) Colbdro`n Date Cdl«ttun Tune Camp l Chad 0r.t le Matrix (see codes) s=SW Total u of Conte nets - 1 X >C I X I Sample Comments_ — SW - E$aritts ..aF`..i Is 0 k'. u...z� `Y 4 4 ""si'tacoG of Containers Sample Kit Prepared By Date' tma Cpmmenis/Special Reporting Requirements Rehequ¢geal / y Retin Nha/ BY DaterTme LIlI� C7J C— OatelTima Rec �/q��/jf�//�/L, X/ - v'+�—`' L f Recurmu By Datartim s2r1 'T J Data/rm,e Relirpulehed By Datemme Br D.tertune --- Cooler u's A Tempt' on Receipt CunU Lon Uonn Receipt _x Acceptable _ Unicceplanle� GW Groundwater SO Sol OW-OMIong Water SE -Sediment SW.Sodace Water WW Withdrawals, q-All O-Otner(deted Jm comments, Prexrvethed: I lite R'CI N!M03 5-rn50-I r:Oa:aCR 00merl1 in Come t Not.: All sam{ties 1u6miee l to ENCO Labs ar. in arxemanee with the terms and conditions listed mm the rovmw nI or, loan noise prop Anne. 19reuim1e; 1EGI Sample Preservation Verification ENCO Cary Work Order: CC18972 Client: KELLOGGS SNACKS/AUSTIN FOODS (KE006) Logged In: 12-Nov-19 09:02 , , i Preservation Check Performed By: CC18972-01 Project: Stormwater Project #: [none] Logged By: Rachel Ann Yp1�ish Date/Time: Cont Type, Pres (pH) Requirement pH Checked I In Control pH Adjusted DateTme Adjusted Reagent Used/Comments B 250mLA+H2SO4 <2 Y/ N A Y/ N A C 250mLA+H2SO4 <2 Y/ N/ NA Y I N/ NA D 250mLP+H2SO4 <2 Y>/ N / NA Y (N)l NA Rea ent Name ID 1 2 pH Strip ID Reagent Name ID 3 4 Rea ent Name ID 5 6 PH Strips C910537 C:\elmnt\PI.........-_ .. rpt ' Page 1 of 1 POPP� Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, October 23, 2019 KELLOGGS SNACKS/AUSTIN FOODS(KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater (Jan,July) ENCO Workorder(s): CC11096 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, October 14, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 004�L;UA Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 8 EN E www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: SW01 Lab ID: CC11096-01 Sampled: 10/13/19 11:50 Received: 10/14/19 1410 Parameter pmoaration Hold Date/T'me(s) Prep Date/T'mefs) Analysis Date/Time(s) EPA 1664B EPA 1664E 11/10/19 10/17/19 15:03 10/18/19 15:38 SM 2540D-2011 NO PREP 10/20/19 10/17/19 14:38 10/17/19 14:38 SM 522OD-2011 Same 11/10/19 10/17/19 15:30 10/18/19 07:39 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 8 EN - - www.eD[olabs.com SAMPLE DETECTION SUMMARY Client ID: SWO1 Lab ID: CC11096-01 BDal12e Results Elan MDL P.Q6 Llllla MethoE Notes Chemical Oxygen Demand 5800 100 100 mg/L SM 5220D-2011 Oil & Grease (HEM) 2.59 3 1.50 5.00 mg/L EPA 1664B Total Suspended Solids 52 43 43 mg/L SM 2540D-2011 FINAL This report relates only to the sample as received by the laboratory, and may Only be repmduced In full. Page 3 of 8 NIL - - www.encolabs.com ANALYTICAL RESULTS Description: SWOT Lab Sample ID:CC11096-01 Received: 10/14/1914:10 Matrix: Surface Water Sampled: 10/13/19 11:50 Work Order: CC11096 Project: Stonnwater (Jan,July) Sampled By:Greg Kanellis Classical Chemistry Parameters ^ - EA'Cc Gry reRiheAanaly(e (AC 5911 Analyte ICAS Numberl Resul Flaa Units Chemical Oxygen Demand^ 5800 ri Total Suspended Solids^ 52 mg/L Classical Chemistry Parameters ^ - EN701acksonollererti5e Analyte ICAS Numberl Oil & Grease (HEM) [C-00071^ Results flag Units 2.59 J 1 DIE MDL PPOL Batch Method Analyzed 1Y Notes 10 100 100 9317035 SM 5220D-2011 10/18/19 07:39 JOC 17.2 43 43 9317038 SM 254OD-2011 10/17/19 14:38 JAH PF MOLL FRL Batch Method 1 1.50 5.00 9317013 EPA 1664B Ana1i9 BY Notes 10/18/1915:38 SMA FINAL This report relates only to the sample as received by me laboratory, and may only be reproduced In full. Page 4 Of www.encolahs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9JI7035 - NO PREP Blank (9317035-BLKS) Prepared: 10/ 17/2019 15:30 Analyzed: 10/ 18/2019 07:39 Spike Source %REC RPD .Analvte Result Flag POL Units Level ResulS %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 D 10 mg/L LCS (9317035-BSI) Prepared: 10/17/2019 15:30 Analyzed: 10/18/2019 07:39 Spike Source %REC RPD .AnaWte Result Flag ROL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 500 10 mg/L 500 101 90-110 Matrix Spike (9317035-MSI) Prepared: 10/17/2019 15:30 Analyzed: 10/18/2019 07:39 Source: CC00148-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes_ Chemical Oxygen Demand 560 10 mg/L 526 24 102 90-110 Matrix Spike Dup (9317035-MSD1) Prepared: 10/17/2019 15:30 Analyzed: 10/18/2019 07:39 Source: CCO0148-01 Analvte Chemical Oxygen Demand Batch 9J17038 - NO PREP Result Flag ROL 550 10 Spike Source %REC RPD Units Level Result %REC Limits RPD Limit Notes mg/L 526 24 100 90-110 2 5 Blank (9117038-BLX1) Prepared & Analyzed: 10/17/2019 14:38 Spike Source %REC RPD .Analvte Result Flag POL Units Level Result PAREC Limits RPD Limit Notes Toml Suspended Solids 2.5 0 2.5 mg/L LCS (9317038-BSI) Prepared & Analyzed: 10/17/2019 14:38 Spike Source %REC RPD .Analvte Result Flag POL Units Level Result -AREC Limits RPD Limit Notes Total Suspended Solids 83 2.5 mg/L 100 83 80-120 Duplicate (9317038-DUP1) Prepared & Analyzed: 10/17/2019 14:38 Source: CC14776-01 Spike Source %REC RPD AnalYte Result Flag POL Units Level Result %REC Limits RPD Limit Notes_ Total Suspended Solids 54 52 mg/L 69 25 20 QM-12 Classical Chemistry Parameters - Quality Control Batch 9.717013 - EPA 1664E Blank (9317013-BLKI) Prepared: 10/17/2019 15:03 Analyzed: 10/18/2019 15:38 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes_ Oil & Grease (HEM) 1.50 U 5.00 mg/L LCS (9317013-BSI) Prepared: 10/17/2019 15:03 Analyzed: 10/18/2019 15:38 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 126 5.00 mg/L 160 79 78-114 FINAL This report relates only to the sample as reoeivea by the laboratory, and may only be reproduced in full. Page 5 of 8 S uco www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9J17013 - EPA 1664E - Continued LCS Dup (9317013-BSDI) Prepared: 10/17/2019 15:03 Analyzed: 10/18/2019 15:38 Spike Source tyalli RPD .Analvte Result Flat, ROL Units Level Result %REC limits RPD Liter [1 Notes Oil & Grease (HEM) 168 5.00 mi 159 106 78-114 29 18 QR-06 Matrix Spike (9317013-MS1) Prepared: 10/17/2019 15:03 Analyzed: 10/18/2019 15:38 Source: CC11096-01 Spike Source %REC RPD .Analvte Result Flat, POL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 207 5.00 m9/L 148 2.59 138 78-114 QM-07 FINAL This mwn relates only to the sample as received by the laboratory, and may only be repredueed In full. Page 6 of 8 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALL] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable 1-CS recovery. QM-12 Precision between duplicate samples was outside acceptance limits. QR-06 The RPD value for the LCS/LCSD was outside of QC acceptance limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 8 �w 1g)nce,`L al Yon or Atl10Extille.oPe,k Cou4 Sude tll 1D2-A C27511M. IMuebiel Cl. Orlando, FL 326: + Jerhsonvitt, FL 322166069 Cary, NC 2J511 \ t407)82653t1 Fe.e:nmlB506na5 19W)29&"7 Faa(9W)29(T (919)467-3090 Faa(919)4673.515 Page 1 of 1 Coon: na K I_LLOGGS SNACKSAUSTIN FOODS (KE006) [none] An.". Requested Turnaround Times Note: equest subject 10 acceptanceM the tacitly Standard _Expedited Due / p N ° m Zo ad p :E mnbers ONEQUALITY LANE Prpinet rvammDnsc ormwater (JanJuly) Cur.tilllm C,ARY'. NC 27513- PO o. Bel,nq mW Tit (919) 677-3519 Faa (j - flnyn:ane Gublam Rodney Bateman Jame, Airlttlpn(Plnl) Y f�,J T�6 - /� PAID, �\ —1� ell C met dccoums Payable ISa.l-a.mn Zinn Zone Lab wOfl(Ordet - -. Prmanna idn(Soo Cones)(Combine as necessary) 1'nn, a Sample ID (F161d ldnn4fcala1 1) DOIMpa M: Date Cpllec l.n ,,a C.alft urab Merrill (bee CWoi) rate l4 pl Ceraaml re Sample Comments 11 11Co\ sw 4 x. x x , Sw 4 X X X <-- Total a of containers lJ sm n. f; td PtBpemd a Dan in,V aIt GOnln,a 11,'Sp,rCaa Rppbnmg Roquirom.rii Rglm _ly¢a B� / oat �llo wo ROCBNBC B 91 vne _� Remtn lhhVd e1 Dalemme R Bateman. nPlingUl5ng1 BV Dale/rile RttEwed By DaI9/tMe Confer n i 6 Temps nn Raceipl „ � Gopdilbn n Receipt Acceptable Unacceptable Mavis GW Groundwater SO-Sml DW-Drinking Water SE sediment SW-Sunace Water WWivastewater A -Air 0-011W, looter in comments) Pmservellon: Lice H-HCI N-HNO3 S.H2SO4 NO-NaOH O-0d,er fdotail in commons) 14.1a : All eampms :n rr,l ecl Ie ENGD Lab. are m acic.manCe in the if and comflliena befell do the reVeree 01 real form, dMeSS prior will agreements ci i51 Sample Preservation Verification ENCO Cary Work Order: CC11096 Project: Stormwater (Jan,July) Client: KELLOGGS SNACKS/AUSTIN FOODS (KE006) Project #: [none] Logged In: 14-Oct-19 14,27 Logged By: John C King Preservation Check Performed By: l Date/Time: I C)-1�r 1' p 1 431 CC11096-01 Cont Type. s.Pres PHn J H Ad usted - P �' ;Rea ent. UsedlComm, 9F-. ents ,,. Requ �ement,�. OdnUold .t. _. Adjusted _ B 250mLA+H2SO4 <2 Y/ N/ N Y/ N/ CAA: C 250mLA+H2SO4 <2 Y / N / 60 Y / N / NA' D 250m1-P+H2SO4 <2 � / N / NA Y / N / NA Reagent Name ID .1 2 pH Strip ID: ( / y)S3 Rea ent Name ID 3 4 Rea ent Name ID 5 6 C:\ELMNTAPrint\wko_PreservationCheck.rpt Page 1