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HomeMy WebLinkAboutNCG060095_MONITORING INFO_20191106`► , STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. NCG (� (7 D DOC TYPE ❑ HISTORICAL FILE EY, MONITORING REPORTS DOC DATE ❑ �� r YYYYMMDD Surface Modification Technologies November 1, 2019 Attn: Central Files Division of Water Quality, DENR 1617 Mail Service Center Raleigh, NC 27699-1617 To Whom It May Concern: RECEIVED NOV 06 2019 OKAL FILES WR SECTION Please find enclosed the original and a copy of our Stormwater Discharge Monitoring Report and the corresponding Stormwater Discharge Outfall Qualitative Monitoring Reports for our October monitoring event. Should you have any questions or require additional information, please do not hesitate to contact me. Regards, V 0-- Veronica McKinney Human Resources Manager Enclosures RFcevED NOV 06 2019 _r NCDENR . ,,t,\L FIL%prmwater Discharge Outfall (SDO) DWR SECTION Qualitative Monitoring Report For guidance on filling out this form, please visit: hap://oonal.ncdenr ore/web/wq/wc/su/nndevswitulb-4 Permit No.: N/C/G / 0 / 6 / 0 / 0 / 0 / 0 / or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technologies, Inc. County: Union Phone No. 704-296-6427 Inspector: ('Z r Date of Inspection: to- ILA Time of Inspection: 1 I 1 o t Total Event Precipitation (inches): Was this a Representative Storm Event? (See information below) 2Ycs ❑ No Please check your permit to verify if Qualitative Monitoring must be petforneel during a representative storn event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation, By this signature, I certify that this report is accurate and complete to t�est of my of Permittee or 1. Outfall Description: Outfall No. I— Structure (pipe, ditch, etc.) Pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Iier. si Page I of 2 S W U-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with Floating solids: 1 V 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: b2 3 4 5 7, is there any foam in the stormwater discharge? Yes No S. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. 'These conditions warrant further investigation. Page 2 of 2 SWU-242-20120613 ar NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfilling out this fornl, please visit: hop://portal.nalenr.orehvebAvg/ws/su/npdes %#Itab-4 Permit No.: N/C/G / 0 / 6 / 0 / 0 / 0 / 0/ or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technologies Inc. County: Union Phone No. 7 0 4- 2 9 6- 6 4 2 7 Inspector: R P Date of Inspection: to - l 4 - 111n Time of Inspection: 11 l o Total Event Precipitation (inches): 1.01 Was this a Representative Storm Event? (See information below) 2<yes ❑ No Please check your pennit to verify, if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has I occurred. A single storm event may contain up to 10 consecutive hours of no orecioitation. By this mat%e, I certify that this report is accurate and complete the best 9� my knowledge: of Permittee or 1. Outfall Description: Outfall No. _aq;___, Structure (pipe, ditch, etc.) pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: r-Ax - 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Ae&17&e, Page I of 2 SWU-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: l � 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: o / lJ 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: f / I) 2 3 4 5 7. Is there any foam in the stor nwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes No to. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242-20120613 Awr NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: huLJ)ortal nedenr ors,/web/wa/ws/sn1/np icsvw#tab-4 Permit No.: N/C/G / 0 / 6 / 0 / 0/ 0/ 0/ or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technologies Inc. County: Union Phone No. 704-296-6427 Inspector: R P Date of Inspection: Time of Inspection: Total Event Precipitation (inches): i to? r, Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify il'Qualitutive Monitoring must be petfbnned during a representative storm event (requirements vary). A "Representative Storm Event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours Q days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this suture, I certify that this report is accurate and complete tom best of of Permittee or 1. Outfall Description: Outfall No. ,3 Structure (pipe, ditch, etc.) pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the outfpll drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 121nr y 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): ran Lx_ Page I of 2 SWU-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 U 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: L 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge'? Yes C) 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242-20120613 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: hnp'//Donal ncdertr or�dw�bhvg/wv/ni/nndcesw#vth-d Permit No.: N/C/G / 0 / 6 / 0 / 0 0/ / 0/ or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technologies Inc. County: — Inspector: Union Phone No. 704-296-6427 Date of Inspection: In - I t` — Time of Inspection: 1 1 % 1 . r Total Event Precipitation (inches): I j I, Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring nutst be petformed during a represenlative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has to 10 consecutive hours of no precipitation. occurred.A.... single storm event may contain up . By this siggatpre,,lrcertify that this report is (Signatufc,of Permittce or I. Outfall Description: and complete to,*e�,fest of my kNwledge: Outfall No. �j _ Structure (pipe, ditch, etc.) pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the Outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: e /&p 01 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): �➢on..� Page I of 2 SWU-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: /t / 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: f 1) 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 0 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes I o 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. page 2 of 2 SWU-242-20120613 NC®ENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: h�yr//ponafncdeur.or!�hvcbhvq/w</euhmdessw#tab-4 Permit No.: N/C/G /0 / 6 / 0 / 0 / 0/ 0/ or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technologies, Inc. County: Union Phone No. 704-296-6427 Inspector: 911? Date of Inspection: to- L Lr - Ig Time of Inspection: 11 : 16, Total Event Precipitation (inches): 1 t a1 Was this a Representative Storm Event? (See information below) .40 Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to theist of my kngyvledge: (SignatuI&of Permittnc or I. Outfall Description: Outfall No. !tr_ Structure (pipe, ditch, etc.) pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the outfall drainage area: �So,�� a dZd WL4. of t-ZC21.9 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: �1/ 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): /lvp.� Page I of 2 S W 1i-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 10 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is nosolidsand 5 is the surface covered with floating solids: U 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes V� 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-20120613 kv'�A NC®ENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: hop://portaLnedc•nr.or�,/web/wq/svc/su/npdess�eittab-4 Permit No.: N/C/G / 0 / 6 / 0 / 0/ 0/ 0/ or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technologies, Inc. County: Union Phone No. 704-296-6427 Inspector: R P Date of Inspection: 'rime of Inspection: 1 1 : l l , 'total Event Precipitation (inches): 1 . a Was this a Representative Storm Event'? (See information below) .27Yes ❑ No Please check your permit to verify if Qualitalive Monitoring must he petforned during a representative storm event (requirements vary) A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours Q days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain un to 10 consecutive hours of no orecioitation. By this signature, I certify that this report is accurate and complete to tbest of (Signature of%rmittec or 1. Outfall Description: Outfall No. _ c Structure (pipe, ditch, etc.) pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): A&.1&ei Page I of 2 5 W U-242-201206 U 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: V 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: l./ 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: L/ 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes & S. Is there an oil sheen in the stormwater discharge'? Yes 1. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-20120613 �r NC®ENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisform, please visit: http://I)onafnecletir.orJweb/wci/ws/euhmclessw#tl lb-4 Permit No.: N/C/G / 0 / 6 / 0 / 0/ 0/ 0/ or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technologies, Inc. County: Union Phone No. 704-296-6427 Inspector: R IP Date of Inspection: I n • 1 t. - 1 4�% Time of Inspection: t 1 . e;L o Total Event Precipitation (inches): I a Was this a Representative Storm Event? (See information below) 2 Y s ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no nrecimiation_ By this signature I certify that this report is accurate and complete to thp>best of my (Signature of4krmittee or 1. Outfall Description: Outfall No. -7Structure (pipe, ditch, etc.) Pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the outfall drainage area: Ea I,�/2 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: ti 3. Odor: Describe any distinct odors that the discharge may have (i.c., smells strongly of oil, weak chlorine odor, etc.): /Io17�e� Page I of 2 s W U-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: V 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is nosolidsand 5 is the surface covered with floating solids: U 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: l0 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes Vc 8. Is there an oil sheen in the stormwater discharge? Yes O 9. Is there evidence of erosion or deposition at the outfall? Yes tV 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-20120613 :r NC®ENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit. hup://ponal.ncdcnr.ure/web/wq/wsLni/ondcssw#tub-4 Permit No.: N/C/G /0 / 6 / 0 / 0/ 0/ 0/ or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: _Goulston Technologies Inc. County: - Inspector: nion Phone No. 704-296-6427 Date of Inspection: 10 - 11. - 19 Time of Inspection: ( 1 ' 14 Total Event Precipitation (inches): �n t Was this a Representative Storm Event'? (See information below) 2'�Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be perfitnned during (4 representative storm event (requirements vary). A `Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours Q days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete tp�he best of my (Signaturcef Permittec or 1. Outfall Description: Outfall No. k— Structure (pipe, ditch, etc.) pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 4511�x I- 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): ISOFI 4� Page I of 2 SWU-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 0 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes N 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes Np 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-20120613 �r NC®ENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit lhup://portal.ncclemtorJweb/wnAva/tu/npciesswfttab-4 Permit No.: N/C/G / 0 / 6 / 0 / 0 / 0 / 0 / or Certificate of Coverage No.: N/C/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technologies, Inc. County: Union Phone No. 704-296-6427 Inspector: F. P Date of Inspection: 10 • 16 - I g Time of Inspection: ( 1 : xe. Total Event Precipitation (inches): /, a „ Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must he performed during a representative storm event (requirements vary). A "Representative Storm Event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to test of my (Signature of fdermittee or 1. Outfall Description: Outfall No. _Cx_ Structure (pipe, ditch, etc.) pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 7.nd., 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): n Fln 9- Page I of 2 S W U-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 & 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 6 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 6 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes CNo 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242-20120613 �r NC®ENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: hlnr//pnnaLncdenr ore/web/wq/ws/su/npdesswgtab-4 Permit No.: N/C/G / 0 / 6 / 0 / 0 / 0/ 0/ or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technoloqies, Inc. County: Union Inspector: R P Date of Inspection: 10 - 1 L� - I Time of Inspection: / / 7 2-2- Total Event Precipitation (inches): IV ,. No. 704-296-6427 Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitalive Monitoring most be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to thew of my (Signature of Pgftittee or Designee) 1. Outfall Description: Outfall No. _-1 0 Structure (pipe, ditch, etc.) pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the outfall drainage area: W-a42r� 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 71> , , , , 0 Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Page I of 2 SWU-242-20120513 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 �2) 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: D2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: V 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes 9) 9. Is there evidence of erosion or deposition at the outfall? Yes a 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242-20120613 sr NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: huw//ponal ncdenr or"Jwebhvq/ws/su/huxiessw#tab-4 Permit No.: N/C/G /0 / 6 / 0 / 0 / 0/ 0/ or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technologies Inc. County: Union Phone No. 704-296-6427 Inspector: VLV Date of Inspection: t o- t 4- t 9 Time of Inspection: 11 = 2 L( Total Event Precipitation (inches): 1, e.2 Was this a Representative Storm Event? (See information below) Vf YCs ❑ No Please check your permit to verify if Qualitative Monitoring roust be petfortned during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this sign^ature,/jI certify that this report is accurate and coin the best oft knowledge: / / // .l1- � r 7 t Permit -tee or De`.Wignce) 1. Outfall Description: Outfall No. l 1 Structure (pipe, ditch, etc.) pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: D./La, %,f 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): _r-. N„ Page I of 2 SWU-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: D 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I isnosolids and 5 is extremely muddy: /I1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 6 S. Is there an oil sheen in the stormwater discharge? Yes 6 9. Is there evidence of erosion or deposition at the outfall? Yes 6 to. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242-20120613 �r NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report rorgnidance on filling out tkisform, please visit hup://purtsl.nc(Icur.or!dwcb/wq/ws/su/npclesswHtab-4 Permit No.: N/C/G / 0 / 6 / 0 / 0 / 0 / 0 / or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technologies, Inc. County: Union Phone No. 704-296-6427 Inspector: _R Date of Inspection: to I it — 1 R Time of Inspection: I l t a t It Total Event Precipitation (inches): Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be petformed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature, I certify that this report is accurate and complete to tjx-ycst of my (Signature oo1 crmittec or 1. Outfall Description: Outfall No. 1O'2— Structure (pipe, ditch, etc.) Pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur withintthe outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: — . „ vi 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): n n � Page I of 2 S W U-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: I 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 6 8. Is there an oil sheen in the stormwater discharge? Yes D 9. Is there evidence of erosion or deposition at the outfall? Yes ➢da t0. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-20120613 �r NC®ENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this fonn, please visit: hup'//portal neclenr or<,/Webhvcl/ws/su/npcicssw#tab-4 Permit No.: N/C/G / 0 / 6 / 0 / 0 / 0/ 0/ or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technologies Inc. County: Onion Phone No. 704-296-6427 Inspector: 9? Date of Inspection: 1 D Time of Inspection: 11 11 Total Event Precipitation (inches): I , a it Was this a Representative Storm Event? (See information below) Zfl�yes ❑ No Please check your permit to verify, if Qualitative Monitoring must be penforned during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no orecioitation. By this signature, I c ify t t this report i ccurate and complete to the b of my s (Signature of Pcr ittce or Designee) 1. Outfall Description: Outfall No. /3__ Structure (pipe, ditch, etc.) pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the outfaV drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: �.0 ,i 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): /2nrt, .1, Page 1 of 2 SWU-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 2 C3) 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with Floating solids: 6 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 6) 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes Vo 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes to. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-20120613 SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted 1 ( — I — QO lg CERTIFICATE OF COVERAGE NO. NCG06QQg Z SAMPLE COLLECTION YEAR 0 I� FACILITYNAME Cmoyl -tion FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY ()n:., ❑ use/process meats ® use animal fats/byproducts PERSON COLLECTING SAMPLES R 4 13 M . SS. r S wz_ . K G DISCHARGING TO SALTWATERS? ❑YES 5jjNO LABORATORY Pace_ Lab Cert. # Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall z or n No discharge this period' Outfall No. Sample Collected, mo/dd/yr TSS; mg/L pH, Standard units' - . cOD,-. _ mg/L Oil and Grease, mg/L Fecal oliform', Colonies per 100 ml Enterococci', Colonies per 100 ml Benchmark C� 100 or 504 Within 6.0-9.0� 120' 30 1000 Soo 01 toIts I '% iiy A OF 'I 19 Y. ? 3 V or to t - % y i - L R o Ivo ' Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. ' For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ❑ no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample Collected, mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark - 30" 100 or 504 6.0 — 9.0 - ' Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. ' For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. `See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if yes, complete Part B) SWU-249 Last Revised: October 18, 2012 Page I of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of I(If // i (Date Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 aceAnalytical w w.pacelabs.crom October 28, 2019 John McTaggart Goulston Technologies 700 N. Johnson Street Monroe, NC 28110 RE: Project: Stormwater Sampling #2 Pace Project No.: 92450109 Dear John McTaggart: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on October 17, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Ms. Sally Duncan, Goulston Technologies Veronica McKinney, Goulston Technologies John McTaggart F ACc 7NIg` `geORAtOQ-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 Pace Analytical Services, LLC ® aceAnalytical 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 w vpacelabs.com (704)875-9092 CERTIFICATIONS Project: Stormwater Sampling #2 Pace Project No.: 92450109 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 2 of 13 aceAnalytical wawpacelabs.cda SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Project: Pace Project No.: Stormwater Sampling #2 92450109 Analyles Lab ID Sample ID Method Analysts Reported Laboratory 92450109001 OUTFALL#3 EPA 1664E HH 1 PASI-C SM 254OD-2011 MJP 1 PASI-A SM 5220D-2011 GC 1 PASI-A 92450109002 OUTFALL#7 EPA 1664B HH 1 PASI-C SM 254OD-2011 MJP 1 PASI-A SM 5220D-2011 GC 1 PASI-A 92450109003 OUTFALL#10 EPA1664B HH 1 PASI-C SM 254OD-2011 MJP 1 PASI-A SM 5220D-2011 GC 1 PASI-A 92450109004 OUTFALL #12 EPA 16648 HH 1 PASI-C SM 254OD-2011 MJP 1 PASI-A SM 5220D-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 aceAnalytical o w pacefabs.cwn ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Project: Stormwater Sampling#2 Pace Project No.: 92450109 Sample: OUTFALL#3 Lab ID: 92450109001 Collected: 10/16/1911:10 Received: 10/17/1911: 15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease 11.4 mg/L 5.0 1 10/22/19 15:43 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 15.6 mg/L 5.0 1 10/20/19 07:04 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 52200-2011 Chemical Oxygen Demand 114 mg/L 25.0 1 10/23/19 16:22 10/23/19 20:29 Sample: OUTFALL #7 Lab ID: 92450109002 Collected: 10/16/19 11:20 Received: 10/17/19 11:15 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 16646 Oil and Grease NO mg/L 6.0 1 10/22/19 15:44 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 4.6 mg/L 2.5 1 10/20/19 07:06 52200 COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand NO mg/L 25.0 1 10/23/19 16:22 10/23/19 20:29 Sample: OUTFALL #10 Lab ID: 92450109003 Collected: 10/16/19 11:22 Received: 10/17/19 11:15 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease 11.9 mg/L 5.0 1 10/22/19 15:44 25400 Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 27.2 mg/L 5.0 1 10/20/19 07:06 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 68.0 mg/L 25.0 1 10/23/19 16:22 10/23/19 20:29 Sample: OUTFALL #12 Lab ID: 92450109004 Collected: 10/16/19 11:27 Received: 10/17/19 11:15 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO mg/L 5.0 1 10/22/19 15:46 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/28/2019 02:29 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 13 aceAnalyticale .pa wlabs cram ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater Sampling#2 Pace Project No.: 92450109 Sample: OUTFALL#12 Lab ID: 92450109004 Collected: 10116/1911:27 Received: 10/17/1911:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 51.3 mg/L 8.3 1 10/20/19 07:06 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 40.4 mg/L 25.0 1 10/23/19 16:22 10/23/19 20:29 Date: 10/28/2019 02:29 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 5 of 13 laceAnalyticalo .pecelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater Sampling#2 Pace Project No.: 92450109 OC Batch: 505052 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92450109001, 92450109002, 92450109003, 92450109004 METHOD BLANK: 2713814 Matrix: Water Associated Lab Samples: 92450109001, 92450109002, 92450109003, 92450109004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L NO 5.0 10/22/19 15:43 LABORATORY CONTROL SAMPLE: 2713815 Spike LCS LCS %Rec Parameter Units Conic. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 41.3 103 78-114 LABORATORY CONTROL SAMPLE: 2713844 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 31.2 78 78-114 LABORATORY CONTROL SAMPLE: 2713845 Spike LCS LCS % Rec Parameter Units Conc. Result e/ Rec Limits Qualifiers Oil and Grease mg/L 40 40.2 100 78-114 MATRIX SPIKE SAMPLE: 2713816 92449594002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L NO 40 36.2 88 78-114 Results presented on this page am In the units Indicated by the "Units" column except whore an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 10/28/2019 02:29 PM without the written consent of Pace Analytical Services, L-C. Page 6 of 13 ace Analytical. wwwpacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kinney Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater Sampling #2 Pace Project No.: 92450109 OC Batch: 504602 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92450109001, 92450109002, 92450109003, 92450109004 METHOD BLANK: 2711851 Matrix: Water Associated Lab Samples: 92450109001, 92450109002, 92450109003, 92450109004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L NO 2.5 10/20/19 07:02 LABORATORY CONTROL SAMPLE: 2711852 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 250 100 90-110 SAMPLE DUPLICATE: 2711865 92450104006 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 51.3 58.0 12 D6 SAMPLE DUPLICATE: 2711866 92450104007 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 237 240 1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/28/2019 02:29 PM without the written consent of Pace Analytical Services, L-C. Page 7 of 13 aceAnalytical wwwpace'abs.can QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater Sampling #2 Pace Project No.: 92450109 QC Batch: 505348 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92450109001, 92450109002, 92450109003, 92450109004 METHOD BLANK: 2715087 Matrix: Water Associated Lab Samples: 92450109001, 92450109002, 92450109003, 92450109004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 10/23/19 20:24 LABORATORY CONTROL SAMPLE: 2715088 Spike LCS LCS e/ Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 753 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2715089 2715090 MS MSD 92449799001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result e/ Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L NO 100 100 121 121 108 108 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2715091 2715092 MS MSD 92450097003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 537 100 100 634 636 97 99 90-110 0 Results presented on this page aro in the unit. Indicated by the 'Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/28/2019 02:29 PM without the written consent of Pace Analytical Services, L-C. Page 8 of 13 1,4� eAnalytical w Pacelabs.= QUALIFIERS Project: Stormwaler Sampling N2 Pace Project No.: 92450109 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonfrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/28/2019 02:29 PM without the written consent of Pace Analytical Services, L-C. Page 9 of 13 aceAnalytical wmvpacefa6xmn QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Stormwater Sampling #2 92450109 Analytical Lab ID Sample ID QC Balch Method QC Batch Analytical Method Batch 92450109001 OUTFALL #3 EPA 1664B 505052 92450109002 OUTFALL#7 EPA 1664B 505052 92450109003 OUTFALL #10 EPA 1664E 505052 92450109004 OUTFALL #12 EPA 1664B 505052 92450109001 OUTFALL #3 SM 2540D-2011 504602 92450109002 OUTFALL #7 SM 254OD-2011 504602 92450109003 OUTFALL 910 SM 254OD-2011 504602 92450109004 OUTFALL #12 SM 2540D-2011 504602 92450109001 OUTFALL #3 SM 5220D-2011 505348 SM 5220D-2011 505409 92450109002 OUTFALL #7 SM 52200-2011 505348 SM 5220D-2011 505409 92450109003 OUTFALL #10 SM 52200-2011 505348 SM 52200-2011 505409 92450109004 OUTFALL #12 SM 5220D-2011 505348 SM 5220D-2011 505409 Date: 10/28/2019 02:29 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 13 Document Name: Document Revised: February 7, 2018 aceAnalyGsal Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Client Name: P P ❑ Commercial ace ,�.,,// ❑Other:_ Custody Seal Present? ❑Yes lyrvo Seals Intact? ❑Yes Huntersville 19 Raleigh[] Mechanicsville❑ Project q WO#:92450109 11 I nClient �II II�1�l I�I'III'�I�I� .--._ 92450109 - tr—i�t(//11 IY"0.. _ _.. .. . ' III n Date/Initials Person Examining cuntams: ,/L(} .l i ,T7� Packing Material: ❑Bubble Wrap I_yBubble Bags []None ❑ other Biological Tissue Frozen? Thermo net.er- ❑Yes ❑No Dd/A 6 Gun to: 92TO49 Type of Ice: ?'Wet [:]Blue ❑None Cooler Temp ('C)s () , i Correction Factor: Add/Subtract ('C) 0.0 Temp should he above freezing to 6°C - Cooler Temp Corrected ('Cj: a. i[]Sam des out of temp criteria. Samples on ice, cooling process hasbegun USDA Regulated Soil ((Da/A, water sample) Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check =PS)? Did samples originate from a foreign source (internationally,. ❑Yes ❑No Includinc Hawaii and Puerto RICO)? Dyes [7]No Comments/Dlscre an : Chain of Custody Present? Lyses No DWA 1. Samples Arrived within Hold Time? 1+ ref No N/A 2. Short Hold Time Analysis 02 hr.)? Yes Ej�o N/A 3. Rush Tom Around Time Requested? Yes c ❑N/A a. Sufficient Volume? ' Oct- ❑N/A S. Correct Containers Used? -Pace Containers Used? _ _51ol - u ea ❑No QN0 ❑NIA ❑N/A 6. . - Containers Intact? . es QN. N/A. 7. _ Dissolved analysis: Samples Field Filtered? Y s ❑No 01416 8. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matra: es i � [-]No ❑N/A 9. Heads ace in VOA Vials (>5-6mm ? ❑Yes No � N]ns/A 10. Trip Blank Present? .. Trip Blank Custody Seals Present? []Yet Yes ❑No No /A /A 12. COMMENTS/SAMPLE DISCREPANCY Field Data Required? Dyes []NO deb- an cofiITA(S 10-�16 Gi ha9 , nn for: ov\ Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: 112 Project Manager SRF Review: to DateMme: Date: /�'D/I (I 4/ /�',/fG',((1% Date: IV Page 11 of 13 0 0 v m 3 O pti A fi m n S n a w' y o D O_ O N m e 'e 3 'n A 2 n O � W n O S a � N A b 3 n n e S C w N 01 u Z � $ m as o y w 2 a 6 � 10 Cf O� N L IRmP BP41.1-125 mL Plastic Unpreserved (N/Al (C4) -' 111031.1-250 mL Plastic Unpreserved (N/A) BP2U-500 mt Plastic Unpreserved (N/A) �— SP1U-I liter Plastic Unpreserved(N/A)I zr aP45-125 mL Pbstk H2504 (pH < 2) (Cpi) BM-250 mL plastic HNO3 (pH <2) BP42a2S mL Plastic 2N Acetate & NaOH (P9) 8P4C-32S mL Plastic NaOH (PH> 121 (I}) I WGFU-Wide-mouthed Glass jar Unpreserved AGIU-1 lter Amber Unpreserved (N/A) (CI-) AG2H-1 0ter Amber MCI (pit < 2) AG31.1-250 ml. Amber Unpreserved (N/A)(Ci-) AG15-1 liter Amber H2SO4 (pX < 21 AG35-250mL Amber H2SO4(PH <2) zzAG3AIDG3A)-25O mL Amber NH4C1(N/A)(CI-) " OG9H- ID mL VOA MCI (N/AI ' VG9T40 mL VOA Na25203 (N/AI VG9U40 mL VOA Unp (N/A) DG9P•40 mL VOA H3PO4 (WA) VOAN (6 vials per kit fSOS kit (N/A) WGIL l3 vials per k*VPH/Gas kit (N/A) SPST-125 mL Sterne Plastic (WA — lab); SM-250 mL Sterne Plastic (NIA —lab; i zz BP3A-250 mL Plastic (NH2)2504 (93-9.71 AGWI.100 mL Amber Unpreserved vials (N/A) V5GU-20mLScintilLationvials (N/A) 0591.1-40 mL Amber Unpresemed vials �(N/A) u axAnalXical' area plash seam CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody Is a LEGAL DOCUMENT. AL relevant flews must be completed accurately. Section A Section B Section C Ppea: of RegWmd talent lntomiation: Required PmJett Isomunion: Irani. tollion: Comp Rep Report Ty Ahmgon: 2195750 V I K Add", 100 Copy To: CamPanY Name: REGULATORY AGENCY G I CGY,V� '�dre r NPDES r GROUND WATER r DRINIUNG WATER r UST RCRA r OTHER m TIT Purchase Order No.0 d Pew W%e G Ree:evfw: �o� ar ad Na Site Location F one" 'STATE: Requested Due 02MMAT PmJecl Numbe, PewpFNa A: .' Requested Analysis FiHered(Y/N).. Saction0 Matrix Codes r a aequlraaalen:Irrwaacen MyTRIx r coDF s a COLLECTED Preservatives `>' Odrxing water OW -a u z Water WT 0 O Wasis Water WW PmtllKt P of Sl=d SL SAMPLE ID 01: L o_ w w re (A-Z. 0.2 Ar AR o c Q H Sample lDS MUST BE UNIQUE Tosee TS Q w a i a Z :w y c u Other OT " x z J �a_ w o m o�0 Q 'S = a a la- 019, F. .� C DATE TIME pATI:J1nMEet a _ _ = z Z O y - Pace Project NOJ Lab I.D. + ( k 25 2 0 l k n o a a G 13 ca l dr a �a 5 e 7 e 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHEDBY/AFFILIATION. DATE TIME ACCEPTEDBY/AFFILIATION - DATE TIME SAMPLE CONDITIONS (elf f ft-LS 1 !\,. / -SAMPLER NAME AND SIGNATURE -- - --. ORIGINAL Z PRINT Name of SAMPLER: I L e e v $� O E SIGNANRE of 9AMPLER: GATE Signed 'Impgdant Nde: By Signing Me harm you are aw.epfmg Paws NET M day paynunt temps and egmn:rg b late haroe, of 1.5% per nnnm fw any irvdws net wb wioun 30 days. F.ALL-"20rev.07, 15May-2007