HomeMy WebLinkAboutNCG060089_MONITORING INFO_20191212P-V
STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
DOC TYPE
❑ HISTORICAL FILE
®( MONITORING REPORTS
DOC DATE
❑ �� I �a
YYYYM M DD
Dunbar Foods Corporation
P.O. Box 519 - Dunn, NC 28335 Phone 910-892-3175 Fox 910-892-4169
Attn: DWQ Central Files December 12", 2019
Division of Water Quality
1617 Mail Service Center
Raleigh, INC 27699-1617
Subject: NPDES STORMWATER GENERAL PERMIT—NCG060089 MONITORING REPORT
Attached are the results from our Stormwater sampling event completed on 11-15-19.
Please let it be known that results for all three of our outfalls were within benchmark
tolerances.
Rep^rds,
/' V `� j
41-
Michael Mulier
Field Manager
Moody Dunbar, Inc.
910-892-3175
inichael@moodydunbar.com
CERTIFICATE OF
FACILITY NAME
COUNTY 4"
STORMWATER DISCHARGE MONITORING REPORT
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG060000
Date submitted 12- (r r I q
NO. NCG06O Q
PERSON COLLECTING SAMPLES IvNk NI0I
1CK t-V'
LABORATORY EntO Lob S Lab Cert. # _
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR Q J I I
SAMPLE PERIOD ❑ Jan -June P� July -Dec
or ❑ Monthlys (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow Water Supply ❑SA
Other l f i v krf Y 4 o 9(16/C K•vGI—
FACILITY ACTIVITIES INCLUDE (check all that apply):
❑ use/process meats ❑ use animal fats/byproducts
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Total event rainfall z 1. 19 or ❑ No discharge this period'
-0utfall No.
Date Sample
Collected, mo/dd/yr
TSS,
mg/L
pH;
Standard units
COD,
mg/L
Oil and Grease,
mg/L
Fecal Coliform,
Colonies per 300 ml
Enteromcci,
Colonies per 100 ml .
Benchmark
-
100or50'
Within 6.0 - 9.0
120
30
- 10001
Soo,
Parameter Code
C0530
-.00400
003 0
00556
31616
1§1211
( - I -i
-tS-IG
.7
3
I.
' Only applies to facilities that use/process meats.
2The total precipitation must be recorded using data from anon -site rain gauge.
3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here.
4See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
'Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new oil per month? ❑ yes [71 no
(KM, complete Part B)
Permit Date:11/1/2018-05/31/2021
SWU-249, Last Revised 11/5/2018
Page 1 of 2
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor nil/mnnth
Outfall No.
Date Sample Collected
(mo/dd/yr)
24-hour rainfall amount,
- Inchesz
New Motor Oil or
Hydraulic Oil Usage
Non Polar O&G/Total
Petroleum Hydrocarbons
Total Suspended Solids
Benchmorks-
-
-
15 mg/L -
100 mg/L or 50 mg/L°
-Parameter Code.-.__..
_ ___._..
_.__-46529--
__ —NCOIL---
---- 00552 -
COS30---
Footnotes from Part A also apply to Part B
*FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original copy of this DMR including all "No Discharge" reports within 30 days of receipt of the lab results (or at end of monitoring period in the case
of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who
manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonmenyifor knowing vio)rations." 4
Signature of Permittee
0-P- ti
Date
Permit Date:11/l/2015-05/31/2021
SWU-249, Last Revised 11/5/2015
Page 2 of 2
Environmental
Quaiiry
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out thisfin-in, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stonmwater-gps
Permit No.: N/C/A /6 /G / 0 / o l 8/ Al or Certificate of Covcrage No.: N/C/G/
Facility Name:
County: jAccot
Inspector: M 116
Date of Inspection:
Time of Inspection
dl%G,-'
Total Event Precipitation (inches):
No. C117) —8cf a? — 31-75;-
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event' is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittec is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittec obtains approval from the local DEMLR
Regional Office.
13y Vtis sigrPure. I cAtify that this repoyy is accurate and complete to the best of my knowledge:
(Signature of Pennittee or Designee)
1. Outfall Description: i & 4
Outfall No. Structure (pipe, ditch, etc.): �
Describe the industrial activities that occur within the outfall drainage area:
Page 1 of 2
SWU-242. Last modified 06,012018
2. Color: Describe the color of c ischarRe using basic colors (r •d, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: y f,len f
3. Odor: Describ��� � distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.):
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 6) 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormmater discharge, where I is no solids and 5 is the surface coviced with floating solids:
01 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I i I solids and 5 is extremely muddy:
2 3 4 5
7. Is
there
any foam in the stormwater discharge? O Yes
0 No.
S. Is
there
an oil sheen in the stormwater discharge? OYcs
4lsNo.
9. Is there evidence of erosion or deposition at the outfall? O Yes 0 No.
10. Other Obvious dicators of Stormwater Pollution:
List and describe k 4-
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition ma%• be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S W U-242. Last modified 06101 /201 s
Environmental
Quality,
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this fonn, please visit https://deq.ne.gov/about/divisions/energy-mineral-land-resources/
npde s-st onn"-at er-gps
Permit No.: N_/C/ / b /6 /0 /0 /6 / I/ or Certificate of Coverage No.: N/C/G/
Facility Name: itln6, fto4si Cote
County: VkA
Inspector:
Date of Inspection: ij S- ( q
Time of Inspection:
Total Event Precipitation (inches):
Phone No.
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this sigr)jture. I ftertify)hat this reVrt is accurate and complete to the best of my knowledge:
(Signature of Pennittee or Designee)
1. Outfall escription:
Oull
Receiving Stream:
Structure (pipe, ditch, etc.): ',bi
the industrial activities that occur within the outfall drainage area:
Page I of 2
SwU-242, last modified 061012018
2. Color: Describe the color of
(Iight, medium, dark) as descriptors: 1
discharge using basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e.. smells strongly of oil, weak
chlorine odor, etc.): ftN'-
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
D 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of Iloaling solids in the
stormHatei discharge, where I is no solids and 5 is the surface covered with floating solids:
D 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solids and 5 is extremely muddy:
D 2 3 4 5
7. Is there any foam in the stonnwater discharge? O Yes O No.
S. Is there an oil sheen in the stormwater discharge? OYes ® No.
9. Is there evidence of erosion or deposition at the outfall? o Yes ® No.
10. Other Obvious 16dicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242. La,t modified 06,01/201 S
C- �
En'[m"Pwnml
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report '
For guidance on filling out this form. please visit https://deq.nc.gov/abouUdivisions/energy-mineral-land-resources/
npdes-storm W ater-gps
Permit No.: N/CC/1", l.0l Gl"dl &8/ql or Certificate of Coverage No.: N/C/G/ / / / / / /
Facility N
County:
Inspector:
Date of Inspection: , I'�
Time of Inspection
pS
Total Event Precipitation (inches):
Phone No.
All permits require qualitative monitoring to be performed during a "measurable storm event."
q..
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
13y this signature, I ceAfy that this report is accurate and complete to the best of my knowledge:
(Signature of Pcrmittce or Designee)
1. Outfall Description:
Outfall No. Structure (pipe, ditch, etc.):
Receiving Stream: G
4 Z/�
Describe the industrial activities that occur within the outfall drainage area:
Page I of 2
SWU-242. Last modified W01/2018
2 Color: Describe the color of t c disc argepsing basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: �� 01 e4 r
3. Odor: Descdbp any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): f7r e-
4. Clarith': Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy: G)
2 3 4 5
�. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where I is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I (is no solids and 5 is extremely muddy:
`i 2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes ';W No.
8. Is there an oil sheen in the stormwater discharge? OYcs ap-No.
9. Is there evidence of erosion or deposition at the outfall? o Yes 410 No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low claritv, high solids, and/or the presence of foam, oil sheen, or erosion/deposition mad be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SNVU-242. Last mollified 06,01/201€
K4itq�
ENCO LaboraftARS
Alraffate. Thaely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: 929.467.3090 FAX: 919.467.3515
Tuesday, November 26, 2019
MOODY DUNBAR FOODS (M0008)
Attn: Michael Mulier
PO BOX 519
DUNN, NC 28334
RE: Laboratory Results for
Project Number: Standard, Project Name/Desc: Stormwater
ENCO Workorder(s): CC11806
Dear Michael Mulier,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, November 15, 2019.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results far these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates ooly to :he unye as recerva; by [he laboratory, and may only be reproduce.] in full, Pace 1 of 6
ce=A(ENS
vv w.encolabsxcmn
SAMPLE SUMMARY/LABORATORY CHRONICLE
;Client ID: OuNalil
Lab ID:
CC11806-01
Sampled: 11/15/1908:15
Received: 11/15/1910:15
parameter
preparation
Hold Date /T'me(s1
Prep Date /Timef s)
Analysis Datel T'me(z)
EPA 1664B
EPA 1664B
121'13/19
11/22/19 16:52
11/25/19 15:26
9-0 2540D-1011
140 PREP
11/22/19
11/21/19 11121
11/21/19 1423
SM 522(1D-2011
Same
12/13/19
11/19!19 09:oB
11/19/19 18:01
"i Client ID: Outfall2
Lab ID:
CC11806-02
Sampled: 11/15/1908:20
Received: 11/15/1910.15
Parameter
pre oaration
Hold Date /Timef
s7
p
J'RD t /T' ()
Analysis Date/T'mejgj
EPA 16648
EPA 1664B
12il3/19
11122/19 In 52
ll/25/L9 15:26
SM 2540D-.^_01i
NO PREP
11;22/19
11/21/19 I+1:21
11/21/19 14:23
SM 5220D 2011
6a nhc
12/13/19
11/19/19 09:58
11/19/19 18:01
Client ID: Outfall3
Lab ID:
CC11806-03
Sampled: 11/15/190825
Received: 11/15/1910:15
Parameter
Preuarat'on
Hold Date/Time(s)
Prep Date/Time(,,)
Analysis Date/Time(sl
EPA 16648
EPA 16646
12i!3/19
11/22119 16:52
11/25/19 15J6
SM 2540D-2011
NO PREP
11/12/19
11i21/19 11:23
11/21/19 14:23
SM 5220D 2011
Same
12/13/19
11/19/19 09.58
11/19/19 16:01
R IwL This rePon :elates only to :ne a^.:pie as rer: ei Dy ace Iabo alort', anc nt11 only Ee reolelu[al in :NI.
Cam:
ANALYTICAL RESULTS
v .encolabs.com
Description: Outfall 1
Lab Sample ID:CC11806-01
Received: 11/15/19 10:15
Matrix: Water
Sampled: 11/15,/1908:15
Work Order: CC11806
Project: Stormwater
Sampled By: CLIENT
Classical Chemistry Parameters
nYCJ Cary ca.,.�„a y:e NC 59iJ
Analyte ICASNumberl Results
Flag Units
OF MDL POL Batch
Method Analyzed 131 Notes
Chemical Oxygen Demand^ 42
mg/L
1 30 10 9K19003
SM 5220D-1_011 11/19/19 18:01 JOC
Total Suspended Solids^ 28
mg/L
2.56 6.4 6.4 9K21029
SIA 2540D 2011 1121,r19 1423 BDC
Classical Chemistry Parameters
Analvte ICAS Numberl Results Flag Units PE MDL POL Batch Method Analyzed HX Notes
Oil & Grease (HEM) [C-0007]1 3.50 J mg/L 1 1.50 5.00 9K22013 EPA 1664B Iti25t19 15:26 SMA
Description: Outfall 2 Lab Sample ID:CC11806-02 Received: I1lq5j19 10:15
Matrix: %dater Sampled: ll/1S/1908:20 Work Order: CC 11306
Project: Stonnwater Sampled By: CLIENT
(Classical Chemistry Parameters
^ - ENCo Cary carnfeC anahfe[NC 59J)
Analvte ICAS Numberl Results Flag
Units
OF MDL P2L
Batch
Method
Analyzed
By Notes
Chemical Oxygen Demand ^ 23
mg/I-
1 10 10
91<79003
SM 5220D 2011
I1/19/19 18:01
JOC
Total Suspended Solids' = 5.0
mg/L
2 5.0 5.0
9K21029
SM 2510D-2011
11/21,'19 1-:23
ADC
Classical Chemistry Parameters
Analvte ICAS Numberl
Results
Flao
Units
of MDL PQL
Batch
Method
Analyzed
1 Notes
Oil A, Grea. (HEM) [C-000711
1.50
rng/L
1 150 5.00
9K22013
EPA 1664B
11/25/19 15:26
SMA
Description: Outfall 3
Lab Sample ID:CC11606-03
Received: 11,/15/19 10:15
Matrix: Water
Sampled: l 1/15/19 08:25
Work Order: CC11806
Project: Stonnwater
Sampled By: CLIENT
Classical Chemistry Parameters
^-ENcocaxt 5011
Analvte ICAS Numberl
Results
Fla&
Units
]jE MDL 22L
Batch
Method
Analyzed
Jay Notes
Chemical Oxygen Demand^
32
mg/L
1 10 10
9K19003
SM 5220D-2011
11/19/19 18:01
JOC
Total Suspended Solids'
<36
mg/L
14.3 36 36
9K21029
SM 2540D 2011
11/21/1914:23
BDC
Classical Chemistry Parameters
•-ENCJ:aJsonelL va-:5e'aoalrta;'rlC +:]]
Analvte ICAS Nornberl
Results
Flag
Units
PFF MDL PDL
Batch
Method
Analyzed
Ity Notes
Oil & Grease (HEM) [--0007]^
: 1.50
mg/L
1 1.50 5.00
902013
EPA 1664B
Il/25/l9 15:26
SMA
FINAL This iaWr, relates only to the sample as ie a,i Ir the laboratory, and map only to reproduced in full. Pape 4 of 8
w .encolabs.corn
SAMPLE DETECTION SUMMARY
Client ID: OutfallI
Lab ID:
CC11806-01
Analvte
ResultsRe.sults
Eta
MDL
$Sy
YAM
Method
hwsl ®
Chemical Ozy9en Demand
92
10
i0
mg/L
SM 52201) 2011
Oil 8 Grease (HEht)
3.50
)
1.50
5.00
m9/1
EPA 166?EI
Total Suspended Solids
28
6,9
6,4
mg/L
SI92543D-2011
Client ID: Outfall2
Lab ID:
CC11806-02
Analyte
Results
Flaa
MDL
POL
unn,
Method
Notes
Chemical Oxygen Demand
23
10
i0
m L
g/
5 t152z_JD-2011
Client ID: Outtall3
Lab ID:
CC11806-03
Angie
Re..ft
Flaq
MOL
2
Units
Method
Nate,
Chemical Oxygen Demand
32
10
10
mg/I-
St 1 52_19D-2111
FINAL Thu repo, elatesonlyio the sample a,ie11,ed by the is Wiat»ry, a nd ma y only be r,,�datdInUp, Pape3ofa
0�0
www.encolabs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 9K19003 -Same
Blank (9K39003-BLK3)
Prepared: 11/19/2019 09:58 Analyzed: 11/ 1912019 I8:01
Spike Source %REC
RPD
-AnalYte
ResWt
Hag
PQL
Units
Level Result °/oREC Limits
RPD
Limit
Notes
Chemical Oxygen Demand
10
u
10
mg/L
LCS (9)(19003-BS1)
Prepared: 11/19/2019 09:58 Analyzed: 11(19.2019 18&Cl
Spike Source %REC
RPO
AnalYte
Result
Fiaa
PQL
Units
Level R,sBR a/oREC Limit
RPD
Lima
Notes
Chemical Oxygen Demand
490
10
mgjL
500 98 90"110
Matrix Spike (9K19003-M51)
Prepared: 11/19[2019 09:58 Analyzed: 11/19/2019 18:01
Source: CC09955.01
Spike Source o/oREC
RPO
AnalYte
Resul
Elm
I"
Unity;
Level Result %REC Limits
RPD
11111111
Notes_
Chemlcal Clxygen Demand
600
10
MIA
526 84 97 90-110
Matrix Spike Dup (9K19003-MSDS)
Prepared: 11/19,12019 09;58 Analyzed: 11./19/2019 13:01
Source: CC09955-01
Spike Source o/oREC
RPD
AnalYte
Ressi t
Fide
P91
U.niti
Level Result %REC Limits
RPD
Limit
Notes
Chemical Oxygen Demand
600
10
mg/L
526 84 97 90-110
0
5
Batch 91029 - NO PREP
Blank (9K21029-BLKI)
Prepared & Analyzed: 11/21/2019 14:23
Spike Source %REC
RPD
AnalYte
Result
FIa9
PQL
Units
Level Result %REC Limits
RPD
Limit
Notes
"focal Suspended Solids
15
U
2,5
mg/L
LCS (91<21029-BSI)
Prepared is Analyzed: 11/21/2019 14:23
Spike Source %REC
RPD
All
R-essul
EBB
P"
Units
Level Result o/eREC Limits
RPD
Limit
Notes
'Total Suspended Solids
91
2.5
mg/L
100 91 80-120
Duplicate (91<21029-DUPI)
Prepared & Analyzed: 11121/2019 14:23
Source: CCIBIIO-01
Spike Source %REC
RPD
AnalYte
Result
F1a9
POL
UAil
Level Result %REC limits
RPD
Limit
Notes
Total Suspended Solids
260
74
mg/L
280
6
20
Duplicate (9K21029-DUP2)
Prepared & Analyzed: 11/21/2019 14:23
Source: CC09955-02
Spike Source o/oREC
RPD
AnalYte
Result
FI2111
PQ
Units
Level Result %REC Limits
RPD
Limit
Notes
lb4al Suspended Solids
530
100
and/L
550
3
20
Classical Chemistry Parameters - Quality Control
Batch 9K21013 - EPA 16648
Blank (9K22013-BLKI) Prepared: l l/22/2019 16:52 Analyzed: 11/25/2019 1S26
Spike Source %REC RPD
AnalYte Result E"la l ➢4L Un65 Level Result %REC Limits RPD Limit Notes
Oil & Grease (HEM) 1,50 U 5.00 mg/L
FINAL This report relates only b the sample as received by the laboratory) and may only 6e reproduced in full. Pane 5 of 8
w .encolabs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters -Quality Control
Batch 9K22O13 -EPA 16648 - Continued
LCS (9K22(13-B51) Preparad: 11/22/2019 16'.52 Analyzed: 11/25/2019 15:26
Spike Source 41,REC RPD
All Result Ham PQL Inits Level Result ^/oREC Limits RPD Limit Notes
Oil E Crease WEPT) 155 5.00 nig/I. 158 98 78 114
LCS Dup (9922013-BSD1) Prepared: 11/22/2019 16:92 Ana' l: 11125;2019 1526
Spike
Source
u,oREC
RPD
Analyte
Result F19
PQL
Units
Level
Result
u/oREC
Limits RPD
Limit Notes
011 & Crease (l
162
5,00
nm/L
157
103
78 114 }
18
Matrix Spike (9K22013-MS3)
Prepared: 11/22/2019 ib:52 Analyzed: 11/25''2019 15:26
Source: BC09Ja3-01
Spike
Source
-Al
RPD
Analyte
Res Plao
POL
Units
Level
Result
°,oREC
Limits RPD
Limit Notes
fill &6umse(HIiM)
186
500
mg/1.
160
8.30
111
78-1111
9NAI T➢, curt relates only;, the sample as le:eeea by toe a=-srata-y, and may Orly re reptodpced In full, r'aoe G o! 6
Coo
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
7 The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration Indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (35% or greater
confidence) to make a "tentative identification".
Greater than 25y% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC7 Calculated analyte - MDL(MRL reported to the highest reporting limit of the component analyses.
R GAL This report relate: only to the Sant pie as received by the laboratory. and may only be reproduced in full page 7 of 8
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Sample Preservation Verification
ENCO Cary C� ®d
Work Order: CC11806 Project: Stormwater
Client: MOODY DUNBAR FOODS (M0008) Project#: Standard
Logged In: 15-Nov-19 11:44 Logged By: John C King t
Preservation Check Performed By. �t �% Datef ime:
CC11806-01
'Cont*
Type .., '.'" ,
(pH) ..
`�'
pH Checked -/
• - , , ` Daterirme
pH Adjusted
Reagent UsedtCommehts} x
r
erUs
Rq` irement ,
±; In Cohtrol"
Y , •Adjusted! �_
B
250mLA+H2SO4
<2
1' 1 N/
Y l N /LNA
C
250mLA+H2SO4
<2
Y/ N/ (jJA
Y I N! &A
D
250mLP+H2SO4
<2
/ N / NA
Y /0 ! NA
CC11806-02
Cont,
r -r
Typea'�'a,s4tfi '.u.i
... n
r t
Requrement
P�inCai°itold''�
r �. erflene
pH Adjusted'�ti, Adjusted ui;
..
;o
ReagentsUsed/Comments' Y
s.. t..,..:,,
B
250rnL.A.+H2SO4
<2
Y/ N! t r
Y/ N /(,t�A
C
250mLA+H2SO4
<2
Y / N / {jA'
Y / N / pld
D
250mLP+H2SO4
<2
) / N / NA
Y / 0 / NA
CC11806-03
Cont
Type „:" ±�
Pres (pH)(Ra
1Requ_irement
pH Checked(,
.;In Control'
p H Adjusted Date�me
`Adjusted
Reagent Used/Commentsk" •A
e 3 ,.,.. �,_, ,r•.
B
256mLA+1-12SO4
<2
Y' 1 N t
Y I N ICNA
C
250mI-A+H2SO4
<2
Y/ N/ M
Y! N I NA
D
250mLP+H2SO4
<2
/ N / NA
Y ! / NA
Reagent Name ID
1
2 }
pH Strip ID: t_. 4y7l13;—
Reactant Name ID
3
4
eagent Name ID
5
6 _ ..
C:\ELMN-RPrint\wko_PreservationCheck.rpt Page 1