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HomeMy WebLinkAboutNCG060089_MONITORING INFO_20191212P-V STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. DOC TYPE ❑ HISTORICAL FILE ®( MONITORING REPORTS DOC DATE ❑ �� I �a YYYYM M DD Dunbar Foods Corporation P.O. Box 519 - Dunn, NC 28335 Phone 910-892-3175 Fox 910-892-4169 Attn: DWQ Central Files December 12", 2019 Division of Water Quality 1617 Mail Service Center Raleigh, INC 27699-1617 Subject: NPDES STORMWATER GENERAL PERMIT—NCG060089 MONITORING REPORT Attached are the results from our Stormwater sampling event completed on 11-15-19. Please let it be known that results for all three of our outfalls were within benchmark tolerances. Rep^rds, /' V `� j 41- Michael Mulier Field Manager Moody Dunbar, Inc. 910-892-3175 inichael@moodydunbar.com CERTIFICATE OF FACILITY NAME COUNTY 4" STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG060000 Date submitted 12- (r r I q NO. NCG06O Q PERSON COLLECTING SAMPLES IvNk NI0I 1CK t-V' LABORATORY EntO Lob S Lab Cert. # _ Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR Q J I I SAMPLE PERIOD ❑ Jan -June P� July -Dec or ❑ Monthlys (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow Water Supply ❑SA Other l f i v krf Y 4 o 9(16/C K•vGI— FACILITY ACTIVITIES INCLUDE (check all that apply): ❑ use/process meats ❑ use animal fats/byproducts PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall z 1. 19 or ❑ No discharge this period' -0utfall No. Date Sample Collected, mo/dd/yr TSS, mg/L pH; Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform, Colonies per 300 ml Enteromcci, Colonies per 100 ml . Benchmark - 100or50' Within 6.0 - 9.0 120 30 - 10001 Soo, Parameter Code C0530 -.00400 003 0 00556 31616 1§1211 ( - I -i -tS-IG .7 3 I. ' Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from anon -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 'Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new oil per month? ❑ yes [71 no (KM, complete Part B) Permit Date:11/1/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor nil/mnnth Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, - Inchesz New Motor Oil or Hydraulic Oil Usage Non Polar O&G/Total Petroleum Hydrocarbons Total Suspended Solids Benchmorks- - - 15 mg/L - 100 mg/L or 50 mg/L° -Parameter Code.-.__.. _ ___._.. _.__-46529-- __ —NCOIL--- ---- 00552 - COS30--- Footnotes from Part A also apply to Part B *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original copy of this DMR including all "No Discharge" reports within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonmenyifor knowing vio)rations." 4 Signature of Permittee 0-P- ti Date Permit Date:11/l/2015-05/31/2021 SWU-249, Last Revised 11/5/2015 Page 2 of 2 Environmental Quaiiry Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisfin-in, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/ npdes-stonmwater-gps Permit No.: N/C/A /6 /G / 0 / o l 8/ Al or Certificate of Covcrage No.: N/C/G/ Facility Name: County: jAccot Inspector: M 116 Date of Inspection: Time of Inspection dl%G,-' Total Event Precipitation (inches): No. C117) —8cf a? — 31-75;- All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event' is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittec is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittec obtains approval from the local DEMLR Regional Office. 13y Vtis sigrPure. I cAtify that this repoyy is accurate and complete to the best of my knowledge: (Signature of Pennittee or Designee) 1. Outfall Description: i & 4 Outfall No. Structure (pipe, ditch, etc.): � Describe the industrial activities that occur within the outfall drainage area: Page 1 of 2 SWU-242. Last modified 06,012018 2. Color: Describe the color of c ischarRe using basic colors (r •d, brown, blue, etc.) and tint (light, medium, dark) as descriptors: y f,len f 3. Odor: Describ��� � distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 6) 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormmater discharge, where I is no solids and 5 is the surface coviced with floating solids: 01 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I i I solids and 5 is extremely muddy: 2 3 4 5 7. Is there any foam in the stormwater discharge? O Yes 0 No. S. Is there an oil sheen in the stormwater discharge? OYcs 4lsNo. 9. Is there evidence of erosion or deposition at the outfall? O Yes 0 No. 10. Other Obvious dicators of Stormwater Pollution: List and describe k 4- Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition ma%• be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S W U-242. Last modified 06101 /201 s Environmental Quality, Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this fonn, please visit https://deq.ne.gov/about/divisions/energy-mineral-land-resources/ npde s-st onn"-at er-gps Permit No.: N_/C/ / b /6 /0 /0 /6 / I/ or Certificate of Coverage No.: N/C/G/ Facility Name: itln6, fto4si Cote County: VkA Inspector: Date of Inspection: ij S- ( q Time of Inspection: Total Event Precipitation (inches): Phone No. All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this sigr)jture. I ftertify)hat this reVrt is accurate and complete to the best of my knowledge: (Signature of Pennittee or Designee) 1. Outfall escription: Oull Receiving Stream: Structure (pipe, ditch, etc.): ',bi the industrial activities that occur within the outfall drainage area: Page I of 2 SwU-242, last modified 061012018 2. Color: Describe the color of (Iight, medium, dark) as descriptors: 1 discharge using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e.. smells strongly of oil, weak chlorine odor, etc.): ftN'- 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: D 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of Iloaling solids in the stormHatei discharge, where I is no solids and 5 is the surface covered with floating solids: D 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: D 2 3 4 5 7. Is there any foam in the stonnwater discharge? O Yes O No. S. Is there an oil sheen in the stormwater discharge? OYes ® No. 9. Is there evidence of erosion or deposition at the outfall? o Yes ® No. 10. Other Obvious 16dicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242. La,t modified 06,01/201 S C- � En'[m"Pwnml Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report ' For guidance on filling out this form. please visit https://deq.nc.gov/abouUdivisions/energy-mineral-land-resources/ npdes-storm W ater-gps Permit No.: N/CC/1", l.0l Gl"dl &8/ql or Certificate of Coverage No.: N/C/G/ / / / / / / Facility N County: Inspector: Date of Inspection: , I'� Time of Inspection pS Total Event Precipitation (inches): Phone No. All permits require qualitative monitoring to be performed during a "measurable storm event." q.. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. 13y this signature, I ceAfy that this report is accurate and complete to the best of my knowledge: (Signature of Pcrmittce or Designee) 1. Outfall Description: Outfall No. Structure (pipe, ditch, etc.): Receiving Stream: G 4 Z/� Describe the industrial activities that occur within the outfall drainage area: Page I of 2 SWU-242. Last modified W01/2018 2 Color: Describe the color of t c disc argepsing basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: �� 01 e4 r 3. Odor: Descdbp any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): f7r e- 4. Clarith': Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: G) 2 3 4 5 �. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I (is no solids and 5 is extremely muddy: `i 2 3 4 5 7. Is there any foam in the stormwater discharge? O Yes ';W No. 8. Is there an oil sheen in the stormwater discharge? OYcs ap-No. 9. Is there evidence of erosion or deposition at the outfall? o Yes 410 No. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low claritv, high solids, and/or the presence of foam, oil sheen, or erosion/deposition mad be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SNVU-242. Last mollified 06,01/201€ K4itq� ENCO LaboraftARS Alraffate. Thaely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 929.467.3090 FAX: 919.467.3515 Tuesday, November 26, 2019 MOODY DUNBAR FOODS (M0008) Attn: Michael Mulier PO BOX 519 DUNN, NC 28334 RE: Laboratory Results for Project Number: Standard, Project Name/Desc: Stormwater ENCO Workorder(s): CC11806 Dear Michael Mulier, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, November 15, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results far these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates ooly to :he unye as recerva; by [he laboratory, and may only be reproduce.] in full, Pace 1 of 6 ce=A(ENS vv w.encolabsxcmn SAMPLE SUMMARY/LABORATORY CHRONICLE ;Client ID: OuNalil Lab ID: CC11806-01 Sampled: 11/15/1908:15 Received: 11/15/1910:15 parameter preparation Hold Date /T'me(s1 Prep Date /Timef s) Analysis Datel T'me(z) EPA 1664B EPA 1664B 121'13/19 11/22/19 16:52 11/25/19 15:26 9-0 2540D-1011 140 PREP 11/22/19 11/21/19 11121 11/21/19 1423 SM 522(1D-2011 Same 12/13/19 11/19!19 09:oB 11/19/19 18:01 "i Client ID: Outfall2 Lab ID: CC11806-02 Sampled: 11/15/1908:20 Received: 11/15/1910.15 Parameter pre oaration Hold Date /Timef s7 p J'RD t /T' () Analysis Date/T'mejgj EPA 16648 EPA 1664B 12il3/19 11122/19 In 52 ll/25/L9 15:26 SM 2540D-.^_01i NO PREP 11;22/19 11/21/19 I+1:21 11/21/19 14:23 SM 5220D 2011 6a nhc 12/13/19 11/19/19 09:58 11/19/19 18:01 Client ID: Outfall3 Lab ID: CC11806-03 Sampled: 11/15/190825 Received: 11/15/1910:15 Parameter Preuarat'on Hold Date/Time(s) Prep Date/Time(,,) Analysis Date/Time(sl EPA 16648 EPA 16646 12i!3/19 11/22119 16:52 11/25/19 15J6 SM 2540D-2011 NO PREP 11/12/19 11i21/19 11:23 11/21/19 14:23 SM 5220D 2011 Same 12/13/19 11/19/19 09.58 11/19/19 16:01 R IwL This rePon :elates only to :ne a^.:pie as rer: ei Dy ace Iabo alort', anc nt11 only Ee reolelu[al in :NI. Cam: ANALYTICAL RESULTS v .encolabs.com Description: Outfall 1 Lab Sample ID:CC11806-01 Received: 11/15/19 10:15 Matrix: Water Sampled: 11/15,/1908:15 Work Order: CC11806 Project: Stormwater Sampled By: CLIENT Classical Chemistry Parameters nYCJ Cary ca.,.�„a y:e NC 59iJ Analyte ICASNumberl Results Flag Units OF MDL POL Batch Method Analyzed 131 Notes Chemical Oxygen Demand^ 42 mg/L 1 30 10 9K19003 SM 5220D-1_011 11/19/19 18:01 JOC Total Suspended Solids^ 28 mg/L 2.56 6.4 6.4 9K21029 SIA 2540D 2011 1121,r19 1423 BDC Classical Chemistry Parameters Analvte ICAS Numberl Results Flag Units PE MDL POL Batch Method Analyzed HX Notes Oil & Grease (HEM) [C-0007]1 3.50 J mg/L 1 1.50 5.00 9K22013 EPA 1664B Iti25t19 15:26 SMA Description: Outfall 2 Lab Sample ID:CC11806-02 Received: I1lq5j19 10:15 Matrix: %dater Sampled: ll/1S/1908:20 Work Order: CC 11306 Project: Stonnwater Sampled By: CLIENT (Classical Chemistry Parameters ^ - ENCo Cary carnfeC anahfe[NC 59J) Analvte ICAS Numberl Results Flag Units OF MDL P2L Batch Method Analyzed By Notes Chemical Oxygen Demand ^ 23 mg/I- 1 10 10 91<79003 SM 5220D 2011 I1/19/19 18:01 JOC Total Suspended Solids' = 5.0 mg/L 2 5.0 5.0 9K21029 SM 2510D-2011 11/21,'19 1-:23 ADC Classical Chemistry Parameters Analvte ICAS Numberl Results Flao Units of MDL PQL Batch Method Analyzed 1 Notes Oil A, Grea. (HEM) [C-000711 1.50 rng/L 1 150 5.00 9K22013 EPA 1664B 11/25/19 15:26 SMA Description: Outfall 3 Lab Sample ID:CC11606-03 Received: 11,/15/19 10:15 Matrix: Water Sampled: l 1/15/19 08:25 Work Order: CC11806 Project: Stonnwater Sampled By: CLIENT Classical Chemistry Parameters ^-ENcocaxt 5011 Analvte ICAS Numberl Results Fla& Units ]jE MDL 22L Batch Method Analyzed Jay Notes Chemical Oxygen Demand^ 32 mg/L 1 10 10 9K19003 SM 5220D-2011 11/19/19 18:01 JOC Total Suspended Solids' <36 mg/L 14.3 36 36 9K21029 SM 2540D 2011 11/21/1914:23 BDC Classical Chemistry Parameters •-ENCJ:aJsonelL va-:5e'aoalrta;'rlC +:]] Analvte ICAS Nornberl Results Flag Units PFF MDL PDL Batch Method Analyzed Ity Notes Oil & Grease (HEM) [--0007]^ : 1.50 mg/L 1 1.50 5.00 902013 EPA 1664B Il/25/l9 15:26 SMA FINAL This iaWr, relates only to the sample as ie a,i Ir the laboratory, and map only to reproduced in full. Pape 4 of 8 w .encolabs.corn SAMPLE DETECTION SUMMARY Client ID: OutfallI Lab ID: CC11806-01 Analvte ResultsRe.sults Eta MDL $Sy YAM Method hwsl ® Chemical Ozy9en Demand 92 10 i0 mg/L SM 52201) 2011 Oil 8 Grease (HEht) 3.50 ) 1.50 5.00 m9/1 EPA 166?EI Total Suspended Solids 28 6,9 6,4 mg/L SI92543D-2011 Client ID: Outfall2 Lab ID: CC11806-02 Analyte Results Flaa MDL POL unn, Method Notes Chemical Oxygen Demand 23 10 i0 m L g/ 5 t152z_JD-2011 Client ID: Outtall3 Lab ID: CC11806-03 Angie Re..ft Flaq MOL 2 Units Method Nate, Chemical Oxygen Demand 32 10 10 mg/I- St 1 52_19D-2111 FINAL Thu repo, elatesonlyio the sample a,ie11,ed by the is Wiat»ry, a nd ma y only be r,,�datdInUp, Pape3ofa 0�0 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9K19003 -Same Blank (9K39003-BLK3) Prepared: 11/19/2019 09:58 Analyzed: 11/ 1912019 I8:01 Spike Source %REC RPD -AnalYte ResWt Hag PQL Units Level Result °/oREC Limits RPD Limit Notes Chemical Oxygen Demand 10 u 10 mg/L LCS (9)(19003-BS1) Prepared: 11/19/2019 09:58 Analyzed: 11(19.2019 18&Cl Spike Source %REC RPO AnalYte Result Fiaa PQL Units Level R,sBR a/oREC Limit RPD Lima Notes Chemical Oxygen Demand 490 10 mgjL 500 98 90"110 Matrix Spike (9K19003-M51) Prepared: 11/19[2019 09:58 Analyzed: 11/19/2019 18:01 Source: CC09955.01 Spike Source o/oREC RPO AnalYte Resul Elm I" Unity; Level Result %REC Limits RPD 11111111 Notes_ Chemlcal Clxygen Demand 600 10 MIA 526 84 97 90-110 Matrix Spike Dup (9K19003-MSDS) Prepared: 11/19,12019 09;58 Analyzed: 11./19/2019 13:01 Source: CC09955-01 Spike Source o/oREC RPD AnalYte Ressi t Fide P91 U.niti Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 600 10 mg/L 526 84 97 90-110 0 5 Batch 91029 - NO PREP Blank (9K21029-BLKI) Prepared & Analyzed: 11/21/2019 14:23 Spike Source %REC RPD AnalYte Result FIa9 PQL Units Level Result %REC Limits RPD Limit Notes "focal Suspended Solids 15 U 2,5 mg/L LCS (91<21029-BSI) Prepared is Analyzed: 11/21/2019 14:23 Spike Source %REC RPD All R-essul EBB P" Units Level Result o/eREC Limits RPD Limit Notes 'Total Suspended Solids 91 2.5 mg/L 100 91 80-120 Duplicate (91<21029-DUPI) Prepared & Analyzed: 11121/2019 14:23 Source: CCIBIIO-01 Spike Source %REC RPD AnalYte Result F1a9 POL UAil Level Result %REC limits RPD Limit Notes Total Suspended Solids 260 74 mg/L 280 6 20 Duplicate (9K21029-DUP2) Prepared & Analyzed: 11/21/2019 14:23 Source: CC09955-02 Spike Source o/oREC RPD AnalYte Result FI2111 PQ Units Level Result %REC Limits RPD Limit Notes lb4al Suspended Solids 530 100 and/L 550 3 20 Classical Chemistry Parameters - Quality Control Batch 9K21013 - EPA 16648 Blank (9K22013-BLKI) Prepared: l l/22/2019 16:52 Analyzed: 11/25/2019 1S26 Spike Source %REC RPD AnalYte Result E"la l ➢4L Un65 Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 1,50 U 5.00 mg/L FINAL This report relates only b the sample as received by the laboratory) and may only 6e reproduced in full. Pane 5 of 8 w .encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters -Quality Control Batch 9K22O13 -EPA 16648 - Continued LCS (9K22(13-B51) Preparad: 11/22/2019 16'.52 Analyzed: 11/25/2019 15:26 Spike Source 41,REC RPD All Result Ham PQL Inits Level Result ^/oREC Limits RPD Limit Notes Oil E Crease WEPT) 155 5.00 nig/I. 158 98 78 114 LCS Dup (9922013-BSD1) Prepared: 11/22/2019 16:92 Ana' l: 11125;2019 1526 Spike Source u,oREC RPD Analyte Result F19 PQL Units Level Result u/oREC Limits RPD Limit Notes 011 & Crease (l 162 5,00 nm/L 157 103 78 114 } 18 Matrix Spike (9K22013-MS3) Prepared: 11/22/2019 ib:52 Analyzed: 11/25''2019 15:26 Source: BC09Ja3-01 Spike Source -Al RPD Analyte Res Plao POL Units Level Result °,oREC Limits RPD Limit Notes fill &6umse(HIiM) 186 500 mg/1. 160 8.30 111 78-1111 9NAI T➢, curt relates only;, the sample as le:eeea by toe a=-srata-y, and may Orly re reptodpced In full, r'aoe G o! 6 Coo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. 7 The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration Indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (35% or greater confidence) to make a "tentative identification". Greater than 25y% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC7 Calculated analyte - MDL(MRL reported to the highest reporting limit of the component analyses. R GAL This report relate: only to the Sant pie as received by the laboratory. and may only be reproduced in full page 7 of 8 ��7[\\N\ ID' 76 CIIII��.l Volt D" jrof Cwv 14C 27�11 1 f67461t) Peg Rarl..strai ar,tva". Requested Turnaround Times MOODY DUNSaStandardfRFOODS (MOG081 if, oaf.,, po BOX 5iq Standard DUf4NI, 14C 28334 C'e ---------- C4 .:14i M I :� Expedited N (910) 892- 3 175 jjch apt Muller tri ------ Due ebbie D aw Gl t co CI samylat{sl5pnamv (� (, 1 i �' 1 ! �� �— `— rt�\j �a, I ���, ?13C11N.a Tai,d 4 01 1 1 ample commeras ­47 5" CA'11rer" are, 'al 6. A. —motML - .7,tt 4 X I Ourtfall 2 7. "'z L r E r, ;�403 �S-Hl!s'04 NO Na0f, 0,0a", (W;aI a ------- 55 sial"aw sw.sa", "far, �l"Ilfarnafrl A -A, matrix : GW-Gr,,,f art, ,aW 80 e'a DW 0""f"ag ��% a "fTbIraj fff�lrlb adcadq',a':"t'dr,, M,, ,f Iriff I", 'afta,,f F, rice L,b� ll� in �Irftfll.ta� Sample Preservation Verification ENCO Cary C� ®d Work Order: CC11806 Project: Stormwater Client: MOODY DUNBAR FOODS (M0008) Project#: Standard Logged In: 15-Nov-19 11:44 Logged By: John C King t Preservation Check Performed By. �t �% Datef ime: CC11806-01 'Cont* Type .., '.'" , (pH) .. `�' pH Checked -/ • - , , ` Daterirme pH Adjusted Reagent UsedtCommehts} x r erUs Rq` irement , ±; In Cohtrol" Y , •Adjusted! �_ B 250mLA+H2SO4 <2 1' 1 N/ Y l N /LNA C 250mLA+H2SO4 <2 Y/ N/ (jJA Y I N! &A D 250mLP+H2SO4 <2 / N / NA Y /0 ! NA CC11806-02 Cont, r -r Typea'�'a,s4tfi '.u.i ... n r t Requrement P�inCai°itold''� r �. erflene pH Adjusted'�ti, Adjusted ui; .. ;o ReagentsUsed/Comments' Y s.. t..,..:,, B 250rnL.A.+H2SO4 <2 Y/ N! t r Y/ N /(,t�A C 250mLA+H2SO4 <2 Y / N / {jA' Y / N / pld D 250mLP+H2SO4 <2 ) / N / NA Y / 0 / NA CC11806-03 Cont Type „:" ±� Pres (pH)(Ra 1Requ_irement pH Checked(, .;In Control' p H Adjusted Date�me `Adjusted Reagent Used/Commentsk" •A e 3 ,.,.. �,_, ,r•. B 256mLA+1-12SO4 <2 Y' 1 N t Y I N ICNA C 250mI-A+H2SO4 <2 Y/ N/ M Y! N I NA D 250mLP+H2SO4 <2 / N / NA Y ! / NA Reagent Name ID 1 2 } pH Strip ID: t_. 4y7l13;— Reactant Name ID 3 4 eagent Name ID 5 6 _ .. C:\ELMN-RPrint\wko_PreservationCheck.rpt Page 1