NCG030620_MONITORING INFO_20191212

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO,
w ko a v
DOC TYPE.
❑ ISTORICAL FILE
WNWIONITORING REPORTS
DOC DATE
❑Ia-
YYYYMMDD

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy; Mineral and Land Resources General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE No. N0003 0620
FACILITY NAME Linamar North Carolina
COUNT-,'. Buncombe
PERSON COLLECTING SAMPLES Nicole Grein
LABORATORY Pace Analytical Lab Cert. # 40
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2019
SAMPLE PERIOD ❑Jan -June [E]July-Dec
or ❑ Monthly' (month)
RECEi\ i DISCHARGING TO CLASS 0 ORW❑ HQW ❑❑Trout
1 V �U ❑ Zero -flow ❑ Water Supply
DEC Other Stormwater
(7-ENTiiAL FILES
1VM SECTION
PNA
SA
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 —)
11 No dischome this periodj2,
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
Organicss
Benchmarks
-
-
100 mg/L or 50 mg/L4
6.0 - 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
OOSS2
78141
Outfall #1
11/15/19
1
0.000 mg/L
5.9
0.000 mg/L
0.000 mg/L
0.0025 mg/L.
0.000 mg/L
0.0025 mg/L
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outtall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. -
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4See Gei e!ral Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
http://linus/northcarolina/QMS/Q (5 Documents/ENV-FM19= 02 Semi -Annual Discharge Monitoring Report Form Effective3=15-19.doc

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxlces;;an;-s into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
Si nature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX mQ/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No disrhnrnP this nPrind72
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches3
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/L4
Parameter Code
-
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
http://linus/northcarolina/QMS/QMS Documents/ENV-FM19 -02 Semi -Annual Discharge Monitoring Report Form Effective 3-15-19.doc

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DEMUR REGIONAL OFFICE? YES❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an oriainal copv of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results (or at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure thaiclualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those pers. ins directly responsible for gathering the information, the information submitted is, to the best of my knowledge a nd belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
1
Sign ure of Permif e
I2 5 I)
Date
http://lines/northcarolina/QMS/QMS Documents/ENV-FM19 -02 Semi -Annual Discharge Monitoring Report Form Effective 3-15-19.doc

aceAnalj tical
www.pacalaEs.cam
November 27. 2019
Ms. Nicole Grein
Linamar
2169 Hendersonville Road
Arden, NC 28704
RE: Project: STORMWATER & TTO 11/15//19
Pace Project No.: 92453933
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Dear Ms. Grein:
Enclosed are the analyjical results for sample(s) received by the laboratory on November 15, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen for
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 31
. ,.

Pace Analytical Service, LLC {
®
lace
2225 Riverside Dr.
Analytical
Asheville, NC 28804
www.pacalabs.com
[phone]
CERTIFICATIONS
Project: STORMWATER & TTO 11115/119
Pace Project No.'. 92453933
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not 6e reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 31

r (�Iace
Analytical
w .pacalalts.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
STORMWATER & TTO 11/1509
92453933
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92453933001
SW#1
EPA 1664E
HH
1
PASI-C
EPA 608.3
SEM
29
PASI-C
EPA 200.7 Rev 4.41994
SH1
3
PASI-A
EPA6010D
KO
12
PASI-A
EPA 7470A
SOO
1
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
GAW
34
PASI-C
SM 2540D-2011
CJL
1
PASI-A
SM 4500-H+B-2011
ECH
1
PASI-A
EPA 420.4 Rev 1.0 1993
KDF1
1
PASI-A
SM 4500-CN-E-2011
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 3 of 31

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ANALYTICAL RESULTS
Project: STORMWATER & TTO 11/15//19
Pace Project No.: 92453933
Lab ID: 92453933001 Collected: 11/15/1911:50 Received: 11/1511912:44 Matrix: Water
Pace Analytical Services, LLC t
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SW#1
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No, Oual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND
mg/L
5.0 1
11/26/19 14:00
608 PCB Pest RVE
Analytical Method:
EPA 608.3 Preparation Method: EPA 608.3
ND
ug/L
0.050 1
11/19/19 11:02
11/20/19 08:49
309-00-2
Aldrin
ND
ug/L
0.050 1
11/19/19 11:02
11/20/19 08:49
319-84-6
alpha-BHC
ND
ug/L
0,050 1
11/19/19 11:02
11/20/19 08:49
319-85-7
beta-BHC
ND
ug/L
0.050 1
11/19/19 11:02
11/20/19 08:49
319-86-8
delta-BHC
ND
ug/L
0,050 1
11/19/19 11:02
11/20/1908:49
58-89-9
gamma-BHC(Lindane)
ND
ug/L
0.50 1
11/19/19 11:02
11/20/19 08:49
57-74-9
Chlordane (Technical)
ND
ug/L
0,050 1
11119/19 11:02
11/20/19 08:49
5103-71-9
alpha -Chlordane
ND
ug/L
0.050 1
11/19/19 11:02
11/20/1908:49
5103-74-2
Camma-Chlordane
ND
ug/L
0.050 1
11/19/19 11:02
11/20/19 08:49
72-54-8
4,4'-DDD
ND
uglL
0.050 1
11/19/19 11:02
11120/19 08:49
72-55-9
•A'-DDE
ND
ug/L
0,050 1
1111911911:02
1112011908:49
50-29-3
S4'-DDT
ND
ug/L
0.050 1
11/19/19 11:02
11/20/19 08'.49
60-57-1
Dieldrin
ND
ug/L
0,050 1
11/19/19 11:02
11/20/19 08:49
959-98-8
Endosulfan I
ND
u91L
0.050 1
11/19/19 11:02
11/20/19 08:49
33213-65-9
Endosulfan ll
ND
ug/L
0.050 1
11/1911911:02
11120/19 08:49
1031-07-8
Endosulfan sulfate
ND
ug/L
0.050 1
11/19/19 11:02
11/2011908:49
72-20-8
Endrin
ND
ug/L
0.050 1
11/1911911:02
11120/19 08:49
7421-93-4
Endrin aldehyde
ND
uglL
0.050 1
11/19/19 11:02
11/20/19 08:49
76-44-8
Heptachlor
ND
ug/L
0,050 1
11/19/19 11:02
1112011908:49
1024-57-3
Heptachlor epoxide
ND
ug/L
0.5C 1
11/19/19 11:02
11/20/19 08:49
12674-11-2
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50 1
11/19/19 11:02
11/20/19 08:49
11104-28-2
PCB-1221 (Aroclor 1221)
ND
uglL
0.50 1
11/19/19 11:02
11/20/19 08:49
11141-16-5
PCB-1232 (Aroclor 1232)
ND
ug/L
0,50 1
11/1911911:02
11/20/19 08:49
53469-21-9
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50 1
11/19/19 11:02
11120/19 08:49
12672-29-6
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50 1
11/19/19 11:02
11/20/19 08:49
11097-69-1
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50 1
11/19/19 11:02
11/20/19 08:49
11096-82-5
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50 1
11/19/19 11:02
11/20/19 08:49
8001-35-2
Toxaphene
Surrogates
86
%
10-130 1
11/19/19 11:02
it/20/19 08:49
877-09-8
Telrachloro-m-xylene (S)
116
%
10-130 1
11/19/19 11:02
11/20/19 08:49
2051-24-3
Decachlorobiphenyl(S)
Analytical Method:
EPA 200.7 Rev
4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
200.7 MET ICP
ND
ug/L
5.0 1
11/22/1901:56
11/22/19 18:30
7440-50-8
Copper
ND
ug/L
5.0 1
11/22/19 01:56
11/22/19 18:30
7439-92-1
Lead
25.8
uglL
10.0 1
11/22/19 01:56
11/22/19 18:30
7440-66-6
Zinc
6010 MET ICP
Analytical Method: EPA6010D Preparation Method:
EPA 3010A
ND
mg/L
0.0050 1
11/21/1901:4,
11/26/1915:24
7440-36-0
Antimony
ND
mg/L
0.010 1
11/21/1901:43
11/26/1915:24
7440-38-2
Arsenic
ND
mg/L
0.0010 1
11/21/1901:43
11/2611915:24
7440-41-7
Beryllium
ND
mg/L
0.0010 1
11/21/1901:43
11/26/1915:24
7440-43-9
Cadmium
ND
mg/L
0.0050 1
11121/1901:43
11/2611915:24
7440-47-3
Chromium
ND
mg/L
0.0050 1
11121/1901:43
11126/1915:24
7440-50-8
Copper
REPORT OF LABORATORY ANALYSIS
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be reproduced, except in full,
Dale: 11/2712019 04:46 PM
without the written consent
of Pace Analytical Services, LLC.
Page 4 of 31

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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER 8 T7011/151119
Pace Project No.: 92453933
Sample: SW#1 Lab ID: 92453933001 Collected: 11/15/1911:50 Received: 11/15/1912:44 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Lead
ND
mg/L
0.0050
1
11/21/1901:43
11/26/1915:24
7439-92-1
Nickel
ND
mg/L
0.0050
1
11/21/19 01:43
11/26/19 15:24
7440-02-0
Selenium
ND
mg/L
0,010
1
11/21/1901:43
11/26/1915:24
7782-49-2
Silver
ND
mg/L
0.0050
1
11/21/1901:43
11/26/1915:24
7440-22-4
Thallium
ND
mg/L
0.010
1
11/21/1901:43
11/26/1915:24
7440-28-0
Zinc
0.025
mg/L
0.010
1
1121/1901:43
11/26/1915:24
7440-66-6
7470 Mercury
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Mercury
ND
mg/L
0.00020
1
11/18/19 12:13
11/18/19 16:17
7439-97-6
625 RVE
Analytical Method:
EPA625.1
Preparation Method:
EPA
625.1
Acenaphthene
ND
ug/L
5.0
1
11/21/1914:17
11/23/19 19:16
83-32-9
Acenaphthylene
ND
ug/L
5.0
1
- 11121/1914:17
11/23/19 19:16
208-96-8
Anthracenr
ND
ug/L
5.0
1
1V21/19 14:17
11/23/19 19:16
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
1121/19 14:17
11/23/19 19:16
56-55-3
Benzo(a)Fyrene
ND
ug/L
5.0
1
11/01/19 14:17
11/23/19 19:16
50-32-8
'Benzo(b)fluoranthene
ND
!Ig/L
5.0
1
11/21/19 14:17
11/23/19 19:16
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
11/21/19 14:17
11/2311919:16
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
11/2111914:17
11/23/19 19:16
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
59-50-7
bis(2-Chroreethoxy)methane
ND
ug/L
10.0
1
11/21/19 14:17
1112311919:16
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
7005-72-3
Chrysene
ND
ug/L
5.0
1
11/21/1914:17
11/23/19 19:16
218-01-9
Dibenz (a, h)anth ra cone
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
53-70-3
3,3'-Dich lorobe nzid ine
ND
ug/L
25.0
1
11/21/19 14:17
11/23/19 19:16
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
120-83-2
Diethylphthalate
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
11/21/19 14:17
11/23/19 19:16
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
84-74-2
4,6-Dinilro-2-methylphenol
ND
ug/L
20.0
1
11/2111914:17
11123/1919:16
534-52-1
'2,4-Dinilrophenol
ND
ug/L
50.0
1
11/21/19 14:17
11/23/19 19:16
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
117-84-0
bis(2- Ethyl hexyl)phth a late
ND
ug/L
5.0
1
11/21/19 14:17
11/2311919:16
117-81-7
Fluoranthene
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
20644-0
Fluorene
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
11121/19 14:17
11/23/19 19:16
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
11/21/19 14:17
11/23/19 19:16
77-47-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, L-C. Page 5 of 31

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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER & TTO 11/15//19
Pace Project No.: 92453933
Sample: Srv#1
Lab ID: 92453933001 Collected: 11/15/1911:50
Received: 11/15/19
12:44 Matrix:
Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
625 RVE
Analytical Method: EPA 625.1
Preparation Method:
EPA 625T
Hexachloroethane
ND
ug/L
5.0
1
11/21/19 14A 7
11/23/19 1916
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
193-39-5
NO
ug/L
10.0
1
11/21/19 14:17
11123/19 19:16
78-59-1
Isophorone
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
91-20-3
Naphthalene
NO
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
98-95-3
Nitrobenzene
NO
ug/L
5.0
1
11/21/19 14:17
11/23119 19:16
88-75-5
2-Nitrophenol
ND
ug/L
50.0
1
11121/1914:17
11/23/1919:16
100-02-7
4-Nitrophenol
ND
uglL
5.0
1
11/21/19 14:17
11/23/19 19:16
62-75-9
N-Nitrosodimelhylamine
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
621-64-7
N-Nitroso-di-n-propylamine
ND
ug/L
10.0
1
11/21/19 14:17
11/23119 19:16
86-30-6
N-Nitrosodiphenylamine
ND
ug/L
5.0
1
11/21/19 14:17
11/23/19 19:16
108-60-1
2,2'-Oxybis(1-chloropropane)
ND
ug/L
10.0
1
11/21119 14:17
11123/19 19:16
87-86-5
Pentachlorophenol
ND
ug/L
5'J
1
11/21/19 14:17
11/23/19 19:16
85-01-8
Phenanthrene
ND
ug/L
5.3
1
11121/19 14:17
11/23/19 1916
108-95-2
Phenol
NO
ug/L
5.0
1
11/21/19 14:17
11/231191916
129-00-0
Pyrene
1,2 4-Trichlorobenzene
ND
ug/L
5 n
1
11/21/19 14:17
11/23/19 19:16
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
11/21/19 14:17
11/23/19 1916t
88-06-2
Surrogates
93
%
10-120
1
11/21/19 14:17
11/23/19 19:16
4165-60-0
Nitrobenzene-d5 (S)
83
%
15-120
1
11/21/19 14:17
11/23/19 19:16
321-60-8
2-Fluorobiphenyl (S)
115
%
11-131
1
11/21/19 14:17
11123/19 19:16
1718-51-0
Terphenyl-d14 (S)
63
%
10-120
1
11/2111914:17
11/23119 19:16
13127-88-3
Phenol-d6 (S)
79
%
10 120
1
1112111914:17
11/23/19 19:16
367-12-4
2-Fluorophenol(S)
87
%
10-137
1
11/21/19 14:17
11/23/19 19:16
118-79-6
2,4,6-Tribromophenol(S)
624 Volatile Organics
Analytical Method:
EPA624.1
ND
mg1L
0.0010
1
11/20/1902:00
71-43-2
Benzene
Bromodichloromethane
ND
mg/L
0.0020
1
11/20/19 02:00
75-27-4
Bromoform
ND
mg/L
0.0020
1
11/20/19 02:00
75-25-2
Bromomethane
ND
mg/L
0.0020
1
11/20/19 02:00
74-83-9
Carbon tetrachloride
ND
mg/L
0.0020
1
11120/1902:00
56-23-5
ND
mg/L
0.0020
1
11/20/19 02:00
108-90-7
Chlorobenzene
ND
mg/L
0.0020
1
11/20/19 02:00
75-00-3
Chloroelhane
ND
mg/L
0.0020
1
11/20/19 02:00
67-66-3
Chloroform
ND
mg/L
0,0020
1
11/20M9 02:00
74-87-3
Chloromethane
NO
mg/L
0.0020
1
11/20/19 02:00
124-48-1
Dibromochloromethane
NO
mg&
0.0020
1
11/20/19 02:00
95-50-1
1,2-Dichlorobenzene
ND
mg/L
0,0020
1
11/20/19 02:00
541-73-1
1,3-Dichlorobenzene
ND
mg/L
0.0020
1
11/2011902:00
106-46-7
1,4-Dichlorobenzene
ND
mg/L
0.0020
1
11/20/19 02:00
75-34-3
1,1-Dichloroethane
ND
mg/L
0.0020
1
11/20119 02:00
107-06-2
1,2-Dichloroethane
ND
mg/L
0.0020
1
11/20/19 02:00
75-35-4
1,1-Dichloroethene
ND
mg/L
0.0020
1
11/20/19 02:00
156-59-2
cis-1 2-Dichloroethene
NO
mg/L
0.0020
1
11/20/19 02:00
156-60-5
trans-1,2-Dichloroethene
ND
mg/L
0.0020
1
11/20/19 02:00
78-87-5
1,2-Dichloropropane
ND
mg/L
0,0020
1
11/20/19 02:00
10061-01-5
cis-1,3-Dichloroprope.ne
ND
mg/L
0.0020
1
11/20/19 02:00
10061-02-6
trans-1,3-Dichloropropene
REPORT OF LABORATORY ANALYSIS
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r
aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER& TTO 11/151119
Pace Project No.: 92453933
','Sample: SW#1
Lab ID: 92453933001 Collected:
11/15/i911:50
Received: 11/15/191244 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
624 Volatile Organics
Analytical Method:
EPA624.1
' Ethylbenzene
ND
mg/L
0.0010
1
11/20/19 02:00
100-41-4
Methylene Chloride
ND
mg/L
0,0020
1
11/20/19 02:00
75-09-2
1,1,2,2-Tetrachloroethane
ND
mg/L
0.0020
1
11/20/19 02:00
79-34-5
Telrachloroethene
ND
mg/L
0.0020
1
11/20/19 02:00
127-18-4
Toluene
ND
mg/L -
0.0010
1
11/20/19 02:00
108-88-3
� 1,1,1-Trichloroethane
ND
mg/L
0,0020
1
11/20/19 02:00
71-55-6
1,1,2-Trichloroethane
NO
mg/L
0.0020
1
11/20/19 02:00
79-00-5
Trichloroethene
ND
mg/L
0.0020
1
11/20/19 02:00
79-01-6
TrichloroFluoromethane
ND
mg/L
0.0020
1
11/20/19 02:00
75-69-4
Vinyl chloride
NO
mg/L
0.0020
1
11/20/19 02:00
75-01-4
Surrogates
4-BromoFluorobenzene(S)
99
%
70-130
1
11/20/19 02:00
460-00-4
p Tolucne-d8(S)
97
%
70-130_
1
11120/1902:00
2037-26-5
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
11/20/19 02:00
17060-07-0
�12540D Total Suspended Solids
Analytical Method:
SM 254OD-2011
.Total Suspended Solids
ND
mi
5.0
1
11/20/19 23:05
4500H+ pH, Electrometric
Analytical Method:
SM 4500-H+B-2011
pH at 25 Degrees C
5.9
Std. Units
0.10
1
11/17/19 17:53
H3
420.4 Phenolics, Total
Analytical Method:
EPA 420.4 Rev 1.0
1993 Preparation
Method: EPA 420.4 Rev 1.0 1993
Phenol
ND
mg/L
0.020
1
11/20/19 09:12 11/20/19 13:08
108-95-2
,4500CNE Cyanide, Total
Analytical Method:
SM 45001
Preparation
Method:
SM 4500-CN-E-2011
Cyanide
ND
mg/L
0.0080
1
11/21/1909:53 11/21/1914:41
57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, L-C.
tl
Page 7 of 31

(,lace Analytical
www.pacelabs.com
Project: STORMWATER & TTO 11/15//19
Pace Project No.: 92453933
QC Batch: 511848
QC Batch Method'. EPA 1664E
Associated Lab Samples: 92453933001
LABORATORY CONTROL SAMPLE:
2745148
Parameter
Units
Total Petroleum Hydrocarbons
mg/L
MATRIX SPIKE SAMPLE:
2745149
Parameter
Units
Total Petroleum Hydrocarbons
mg/L
Pace Analytical Services, LLC ,
2225 Riverside D,.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 1664E
Analysis Description: 1664 SGT-HEM, TPH
Spike LCS LCS e/ Rec
Conc. Result % Rec Limits Qualifiers
20 18.9 94 64-132
92453480002 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
ND 20 17.9 88 64-132
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, L-C. Page 8 of 31

laceAnalj4ical'
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
STORMWATER & TTO 11/15//19
Pace Project No.:
92453933
QC Batch:
510082 Analysis Method: EPA 7470A
QC Batch Method:
EPA 7470A Analysis Description: 7470 Mercury
Associated Lab Samples:
92453933001 1,
METHOD BLANK: 2737097
Associated Lab Samples: 92453933001
Parameter Units
Mercury mg/L
Matrix: 'hater
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.00020 11/18/1915:44
LABORATORY CONTROL SAMPLE: 2737098
Spike LCS LCS % Rec
Parameter Units Cone. Result e/ Rec Limits Qualifiers
Mercury mg/L 0.0025 0.0027 107 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2737099 2737100
MS MSD
92453982001 Spike Spike MS MSD MS MSD % Rec
Parameter 'Units Result Cone. Cone. Result Result %Rec %Rec limits RPD Qual
Mercury mg/L ND 0.0025 0.0025 0.0013 0.0018 44 66 75-125 34 M1,R7
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the fight of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/2712019 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 31

ace Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project STORMWATER & TTO 11/15//19
Pace Project No.: 92453933
QC Batch: 511090
Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994
Analysis
Description: 200.7 MET
Associated Lab Samples: 92453933001
METHOD BLANK: 2741966
Matrix: Water
Associated Lab Samples: 92453933001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Copper ug/L
ND 5.0
11122/1912:25
Lead ug/L
NO 5.0
11122/1912:25
Zinc ug/L
ND 10.0
11/22/1912:25
LABORATORY CONTROL SAMPLE: 2741967
Spike
LCS
LCS % Rec
Parameter Units
Cone.
Result % Rec Limits Qualifiers
Copper ug/L
500
482
96 85-115
Lead ug/L
500
468
94 85-115
-
Zinc ug/L
500
465
93 85-115
.,
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2741968
2741969
MS
MSD
92453552003
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Copper ug/L 10.3
500
500 507
501 99 98
70-130
1
Lead ug/L NO
500
500 444
441 89 88
70-130
1
Zinc ug/L 0.078
500
500 535
525 91 89
70-130
2
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2741970
2741971
MS
MSD
92453933001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Copper ug/L NO
500
500 492
484 98 96
70-130
2
Lead ug/L ND
500
500 488
473 98 95
70-130
3
Zinc ug/L 25.8
500
500 512
498 97 94
70-130
3
Results presented on this page are In the units Indicated by the 'Units" column except Where an altemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, L-C. Page 10 of 31

1-aceAnalyficalo
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
STORMWATER & TTO 11/15//19
Pace Project No.:
92453933
OC Batch:
510826 Analysis Method: EPA 601 DID
QC Batch Method:
EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples:
92453933001
METHOD BLANK: 2740526
Associated Lab Samples: 92453933001
Parameter
Units
Antimony
mg/L
Arsenic
mg/L
Beryllium
mg/L
Cadmium
mg/L
Chromium
mg/L
Copper
mg/L
Lead
mg/L
Nickel
mg/L
Selenium
mg/L
Silver
mg/L
,Thallium
mg/L
Zinc
mg/L
LABORATORY CONTROL SAMPLE: 2740527
Parameter
Units
Antimony
mg/L
Arsenic
mg/L
Beryllium
mg/L
Cadmium
mg/L
Chromium
mg/L
,Copper
mg/L
Lead
mg/L
Nickel
mg/L
Selenium
mg/L
lSilver
mg/L
Thallium
mg/L
Zinc
mg/L
Matrix: Water
Blank
Result
Spike
Cone.
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.25
0.5
0.5
NO
ND
NO
NO
NO
NO
NO
NO
NO
ND
ND
ND
Reporting
Limit
Analyzed
0.0050
11/26/19 15:18
0.010
11/26/1915:18
0.0010
11/26/19 15:18
0,0010
11/26/19 15:18
0.0050
11/26/19 15:18
0.0050
11/26/19 15:18
0.0050
11/26/19 15:18
0.0050
11/26/19 15:18
0.010
11/26/19 15:18
0.0050
11/26/19 15:18
0.010
11/26/19 15:18
0.010
11/26/19 15:18
LCS
Result
0.48
0.47
0.49
0.47
0.47
0.48
0.47
0.47
0.47
0.25
0.47
0.46
LCS
% Rec
96
94
99
94
95
97
93
94
94
99
94
91
% Rec
Limits
Qualifiers
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
Qualifiers
a
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2740528 2740529
MS MSD
92453933001 Spike Spike MS MSD
MS
MSD
% Rec
Parameter Units
Result Cone. Cone. Result Result
%Rec
%Rec
Limits RPD Qual
Antimony
ni
NO 0.5 0.5 0.50 0.50
98
99
75-125 1
Arsenic
mg/L
NO 0.5 0.5 0.49 0.49
96
97
75-125 0
Beryllium
mg/L
NO 0.5 0.5 0.50 0.50
99
100
75-125 1
Cadmium
mg/L
NO 0.5 0.5 0.49 0.50
98
99
75-125 1
Chromium
mg/L
NO 0.5 0.5 0.49 0.49
97
98
75-125 1
Results presented on this page are In
the units indicated by the "Units" column except where an alternate unit
Is presented
to the right
or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
'
Date: 11/27/2019 04:46 PM
without the written consent of Pace Analytical Services, LLC.
Page 11 of 31

lace Analytical
www.picelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER & TTO 11/15//19
Pace Project No.: 92453933
-,
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2740528
2740529
MS
MSD
9245.,933001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD Qual
Copper mg/L ND
0.5
0.5
0.49
0.49
97
98
75-125
1
Lead mg/L ND
0.5
0.5
0.48
0.48
96
96
75-125
1
Nickel mg/L ND
0.5
0.5
0.48
0.49
96
97
75-125
1
Selenium mg/L ND
0.5
0.5
0.51
0.52
103
104
75-125
1
Silver mg/L ND
0.25
0.25
0.25
0.25
100
101
75-125
1
Thallium mg/L ND
0.5
0.5
0.47
0.47
94
94
75-125
0
Zinc mg/L 0.025
0.5
0.5
0.50
0,50
95
96
75-125
0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, L-C.
Page 12 of 31

2aceAnalytical
I www.pawlaEscam
QUALITY CONTROL DATA
Project: STORMWATER 8 TTO 11/15//19
Pace Project No.: 92453933
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
( uu nalcn: b1UbU/
Analysis Method: EPA624.1
OC Batch Method: EPA624.1
Analysis Description: 624 MSV
Associated Lab Samples: 92453933001
METHOD BLANK: 2739039
Matrix:
Water
i. Associated Lab Samples: 92453933001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,1,1-Trichloroethane
mg/L
NO
0.0020
11/19/19 18:35
1,1,2,2-Tetrachloroethane
mg/L
NO
0.0020
11/19/19 18:35
II 1,1,2-Trichloroethane
mg/L
NO
0.0020
11/19/19 18:35
1,1-Dichloroethane
mg/L
NO
0.0020
11/19/19 18:35
1,1-Dichloroethene
mg/L
NO
0.0020
11/19/19 18:35
1,2-Dichlorobenzene
mg/L
ND
0,0020
11/19/19 18:35
1,2-Dichloroethane
mg/I.
ND
0.0020
11/19/19 18:35
1,2-Dichloropropane
mg/L
NO
0.0020
11/19/19 18:35
1,3-Dichlorobenzene
mg/L
NO
0.0020
11/19/19 18:35
1,4-Dichlorobenzene
mg/L
NO
0.0020
11/19/19 18:35
Benzene
mg/L
NO
0.0010
1111911918:35
Bromodichloromethane
mg!_
NO
0.0020
11/1911918:35
Bromoform
mg/L
ND
0.0020
11119/1918:35
"Bromomelhane
mg/L
NO
0.0020
11/19/19 18:35
Carbon tetrachloride
mg/L
NO
0.0020
11/19/19 18:35
Chlorobenzene
mg/L
NO
0.0020
11/19/19 18:35
1, Chloroethane
mg/L
NO
0.0020
11/19/19 18:35
Chloroform
mg/L
ND
0.0020
11/19/19 18:35
Chloromethane
mg/L
ND
0.0020
11119/1918:35
cis-1,2-Dichloroethene
mg/L
NO
0,0020
11/19/19 18:35
cis-1,3-Dichloropropene
mg/L
NO
0,0020
11/19/19 18:35
Dibromochloromethane
mg/L
NO
0.0020
11119/1918:35
�;Ethylbenzene
mg/L
NO
0.0010
1111911918:35
Methylene Chloride
mg/L
NO
0.0020
11/1911918:35
Tetrachloroethene
mg/L
NO
0.0020
11/19/19 18:35
Toluene
mg/L
NO
0.0010
11/19/19 18:35
trans-1,2-Dichloroethene
mg/L
NO
0.0020
11/19/19 18:35
trans-1,3-Dichloropropene
mg/L
NO
0,0020
11/19/19 18:35
Trichloroethene
mg/L
NO
0.0020
11/19/19 18:35
Trichlorofluoromethane
mg/L
ND
0.0020
11119/1918:35
'IVinyl chloride
mg/L
NO
0.0020
11/19/19 18:35
1,2-Dichloroethane-d4 (S)
%
99
70-130
11/19/19 18:35
4-Bromofluorobenzene (S)
%
99
70-130
11/19/19 18:35
.Toluene-d8 (S) -
%
99
70-130
11/1911918:35
LABORATORY CONTROL SAMPLE: 2739040
Spike
LCS
LCS % Rec
Parameter
Units
Conc. Result %Rec Limits Qualifiers
1,1,1-Trichloroethane
mg/L
0.02
0.018
88 70-130
1,1,2,2-Tetrachloroethane
mg/L
0.02
0.020
100 60-140
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 31

('15ceinalytical.Dicelabs.cmn
QUALITY CONTROL DATA
Project: STORMWATER & TTO 11/15//19
Pace Project No.: 92453933
LABORATORY CONTROL SAMPLE:
Parameter
2739040
Units
Spike
Conic.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,2-Trichloroethane
mg/L
0.02
0,019
96
70-130
1,1-Dichloroethane
mg/L
0.02
0.018
89
70-130
1,1-Dichloroethene
mg/L
0.02
0.018
90
50-150
1,2-Dichlorobenzene
mg/L
0.02
0.020
98
65-135
1,2-Dichloroethane
mg/L
0.02
0,017
84
49-155
1,2-Dichloropropane
mg/L
0,02
0,019
94
35-165
1,3-Dichlorobenzene
mg/L
0.02
0.020
102
70-130
1,4-Dichlorobenzene
mg/L
0.02
0.021
104
65-135
Benzene
mg/L
0.02
0.019
93
65-135
Bromodichloromethane
mg/L
0.02
0.019
94
65-135
Bromoform
mg/L
0.02
0,018
92
70-130
Bromomethane
mg/L
0.02
0.020
102
15-185
Carbon tetrachloride
mg/L
0.02
0.018
92
70-130
Chlorobenzene
mg/L
0.02
0,019
96
65-135
Chloroethane
mglL
0.02
0.016
81
40-160
Chloroform
mg/L
0.02
0.018
92
70-135
Chloromelhane
mg/L
0.02
0.019
93
1-205
cis-1,2-Dichloroethene
mg/L
0.02
0.018
91
68-146
cis-1,3-Dichloropropene
mg/L
0.02
0.020
99
25-175
Dibromochloromethane
mg/L
0.02
0.019
96
70-135
Ethylbenzene
mg/L
0.02
0.019
97
60-140
Methylene Chloride
mg/L
0.02
0,017
87
60-140
Tetrachloroelhene
mg/L
0.02
0.018
91
70-130
Toluene _
mg/L
0.02
0.019
93
70-130
trans-1,2-Dichloroethene
mg/L
0.02
0.017
87
70-130
trans-1,3-Dichloropropene
mg/L
0.02
0.020
98
50-150
Trichloroethene
mg/L
0.02
0.018
89
65-135
Trichlorofluoromethane
mg/L
0.02
0.017
83
50-150
Vinyl chloride
mg/L
0.02
0.018
92
5-195
1,2-Dichloroethane-d4 (S)
%
93
70-130
4-Bromofluorobenzene (S)
%
94
70-130
Toluene -dB (S)
%
98
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2739041 2739042
MS MSD
92453933001 Spike Spike MS MSD MS
Parameter Units Result Conic. Cones Result Result e/ Rec
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Oiialifiers
MSD % Rec
e/ Rec Limits RPD
1,1,1-Trichloroethane
mg/L
ND
0.02
0.02
0.025
0.021
123
103
1, 1, 2,2-Tetra chloroethane
mg/L
ND
0.02
0.02
0.029
0.023
147
115
1,1,2-Trichloroethane
mg/L
ND
0.02
0.02
0,028
0.022
138
110
1,1-Dichloroethane
mg/L
ND
0.02
0.02
0.026
0.020
129
102
1,1-Dichloroethene
mg/L
ND
0.02
0.02
0.024
0.021
122
106
1,2-Dichlorobenzene
mg/L
ND
0.02
0.02
0.029
0.023
147
116
1,2-Dichloroethane
mg/L
ND
0.02
0.02
0.024
0.019
122
96
1,2-Dichloropropane
mg/L
ND
0.02
0.02
0.027
0.022
137
110
52-162 17
46-157 25
52-150 23
59-155 24
1-234 13
18-190 24
49-155 23
1-210 22
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Dual
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Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, LLC, Page 14 of 31

(�IaceAnayical'
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER
Pace Project No.: 92453933
& TTO
11/15//19
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2739041
2739042
MS
MSD
92453933001
Spike
Spike
MS
MSD
MS
MSD
": Rec
Parameter
Units
Result
Conic.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Oual
1,3-Dichlorobenzene
ing/L
ND
0.02
0.02
0.029
0,024
143
118
59-156
19
1,4-Dichlorobenzene
mg/L
ND
0.02
0.02
0,029
0.024
144
121
18-190
17
Benzene
mg/L
ND
0.02
0.02
0.027
0.022
134
109
37-151
21
Bromodichloromethane
mg/L
ND
0.02
0.02
0.027
0.021
135
106
35-155
25
Bromoform
mg/L
ND
0.02
0.02
0.027
0.021
134
105
45-169
24
Bromomethane
mg/L
ND
0.02
0.02
0.024
0.020
115
96
1-242
18
Carbon tetrachloride
mg/L
ND
0.02
0.02
0.026
0.022
128
108
70-140
17
Chlorobenzene
mg/L
ND
0.02
0.02
0.028
0.023
142
114
37-160
22
Chloroethane
mg/L
ND
0.02
0.02
0.023
0,017
114
83
14-230
32
Chloroform
mg/L
ND
0.02
0.02
0.025
0,021
126
105
51-138
18
Chloromethane
mg/L
ND
0.02
0.02
0.025
0.019
126
95
1-273
28
cis-1,2-Dichloroethene
mg/L
ND
0.02
0.02
0.026
0.020
130
102
45-174
24
cis-1,3-Dichloropropene
mg/L
ND
0.02
0.02
0.029
0.022
143
112
1-227
24
Dibromochloromethane
mg/L
ND
0.02
0.02
0.029
0.022
143
109
53-149
26
Ethylbenzene
.ng/L
ND
0.02
0.02
0.028
0,023
140
116
'37-162
19
Methylene Chloride
mg/L
ND
0.02
0.02
0.025
0.019
124
97
1-221
24
Tetrachloroethene
mg/L
ND
0.02
0.02
0.027
0,022
133
108
64-148
21
Toluene
mg/L
ND
0.02
0.02
0.09.6
0,021
129
106
47-150
19
trans-1,2-Dichloroethene
mg/L
ND
0.02
0.02
0,026
0.021
129
103
54-156
23
trans-1,3-Dichloropropene
mg/L
ND
0.02
0.02
0.028
0.022
141
112
17-183
23
Trichloroethene
mg/L
ND
0.02
0.02
0.026
0.021
128
104
70-157
21
Trichlorofluoromethane
mg/L
ND
0.02
0.02
0.024
0.020
118
99
17-181
17
Vinyl chloride
mg/L
ND
0.02
0.02
0.027
0.021
134
107
1-251
22
1,2-Dichloroethane-d4 (S)
%
93
93 .
70-130
4-Bromofluorobenzene (S)
%
96
95
70-130
Toluene-d8 (S)
%
97
98
70-130
Results presented on this page ere In the units Indicated by the "Units" column except where an alternate on It Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 31

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QUALITY CONTROL DATA
Project: STORMWATER & TTO 11/15l/19
Pace Project No.: 92453933
QC Batch: 510331
QC Batch Method: EPA608.3
Associated Lab Samples: 92453933001
Analysis Method:
Analysis Description:
EPA 608.3
608 PCB Pest Red Vol
METHOD BLANK: 273£,254
Matrix: Water
Associated Lab Samples: 92453933001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
4,4'-DDD
ug/L
ND
0.050
11/20/19 09:48
44'-DDE
ug/L
NO
0.050
11/2011909:48
4,4'-DDT
ug/L
NO
0.050
11/20/19 09:48
Aldrin
ug/L
ND
0.050
11/20/19 09:48
alpha-SHC
ug/L
NO
0.050
11/20M909:48
alpha -Chlordane
ug/L
NO
0.050
11/20/19 09:48
beta-BHC
ug/L
NO
0.050
11/20/19 09:48
Chlordane (Technical)
ug/L
ND
0,50
11120/1909:48
delta-BHC
ug/L
NO
0,050
11/2011909:48
Dieldrin
ug11_
NO
0.050
11120/19 09:48
EndosulfanI
ug/L
ND
0.050
11/2011909:48
Endosulfan ll
ug/L
NO
0.050
11/20/19 09:48
Endosulfan sulfate
ug/L
NO
0,050
11/20/19 09:48
Endrin
ug/L
NO
0.050
11/2011909:48
Endrin aldehyde
ug/L
NO
0.050
11/2011909:48
gamma-BHC(Lindane)
ug/L
NO
0,050
11/20/19 09:48
gamma -Chlordane
ug/L
NO
o.050
11/20/19 09:48
Heptachlor
ug/L
NO
0,050
11/2011909:48
Heptachlor epoxide
ug/L
NO
0.050
11/20/19 09:48
PCB-1016(Aroclor 1016)
ug/L
ND
0.50
11/20/19 09:48
PCB-1 221 (Aroclor 1221)
ug/L
NO
0.50
11/20/19 09:48
PCB-1232 (Aroclor 1232)
ug/L
NO
0.50
11/20/19 09:48
PCB-1242 (Aroclor 1242)
ug/L
NO
0.50
11/20/19 09:48
PCB-1248 (Aroclor 1248)
ug1L
NO
0.50
11/20/19 09:48
PCB-1254 (Aroclor 1254)
ug/L
NO
0.50
11/20/19 09:48
PCB-1260 (Aroclor 1260)
ug/L
NO
0.50
11/20/19 09:48
Toxaphene
ug/L
NO
0.50
11/2011909:48
Decachlorobiphenyl(S)
e/
124
10-130
11/20/19 09:48
Tetrachloro-m-xylene (S)
%
82
10-130
11/20/19 09:48
Qualifiers
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
2738255
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
uglL
0.25
0.24
98
31-141
4,4'-DDE
uglL
0.25
0.23
92
30-145
4,4'-DDT
ug/L
0.25
0.33
133
25-160
Aldrin
ug/L
0.25
0.26
102
42-140
alpha-BHC
ug/L
0.25
0.25
100
37-140
alpha -Chlordane
ug/L
0.25
0.27
108
45-140
beta-BHC
ug/I-
0.25
0.31
122
17-147
Results presented on this page are In the units Indicated by the "Units" column except where an alternate on It is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, LLC, Page 16 of 31

aceAnalytical
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QUALITY CONTROL DATA
Project: STORMWATER & TTO 11/15//19
Pace Project No.: 92453933
LABORATORY CONTROL SAMPLE:
2738255
Spike
LCS
LCS
% Rec
Parametel.m
Units
Conc.
Result
%Rec
Limits.,
delta-BHC
ug/L
0.25
0.25
99
19-140
Dieldrin
ug/L
0.25
0.27
106
36-146
Endosulfan I
ug/L
0.25
0.26
105
45-153
Endosulfan 11
ug/L
0.25
0.27
109
1-202
Endosulfan sulfate
ug/L
0.25
0.28
113
26-144
Endrin
ug/L
0.25
0.27
110
30-147
Endrin aldehyde
ug/L
0.25
0.25
101
50-150
gamma-BHC (Lindane)
ug/L
0.25
0.26
103
32-140
gamma -Chlordane
ug/L
0.25
0.19
76
45-140
Heptachlor
ug/L
0.25
0.26
104
34-140
Heptachlor epoxide
ug/L
0.25
0.27
106
37-142
Decachlorobiphenyl (S)
%
126
10-130
Tetrachloro-m-xylene (S)"
%
98
10-130
t
MATRIX SPIKE & MATRiY SPIKE DUPLICATE: 2738256
MS
92453933001 Spike
Parameter Units Result Conc.
4,4'-DDD
4,4'-DDE
4,4'-DDT
Aldrin
alpha-BHC
alpha -Chlordane
beta-BHC
delta-BHC
Dieldrin
Endosulfan I
'Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
gamma-BHC (Lindane)
gamma -Chlordane
Heptachlor
Heptachlor epoxide
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
ug/L NO
ug/L NO
ug/L NO
ug/L NO
ug/L NO
ug/L NO
ug/L ND
ug/L NO
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L NO
ug/L NO
ug/L ND
o�
2738257
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
MSD
Spike MS MSD MS MSD % Rec
Con 1. Result Result %Rec %Rec Limits RPD Qual
0.25
0.25
0.27
0.27
0.25
0.25
0.26
0.26
0.25
0.25
0.37
0.37
0.25
0.25
0.27
0.27
0.25
0.25
0.26
0.25
0.25
0.25
0.29
0.29
0.25
0.25
0.35
0.35
0.25
0.25
0.27
0.27
0.25
0.25
0.28
0.28
0.25
0.25
0.28
0.28
0.25
0.25
0.29
0.29
0.25
0.25
0.31
0.30
0.25
0.25
0.30
0.29
0.25
0.25
0.27
0.27
0.25
0.25
0.28
0.27
0.25
0.25
0.20
0.20
0.25
0.25
0.28
0.28
0.25
0.25
0.28
0.28
109
103
147
108
104
116
140
110
114
112
117
122
118
109
112
81
113
111
111
101
109
104
148
107
100
115
141
108
113
111
115
122
117
108
109
82
111
111
110
96
31-141
30-145
25-160
42-140
37-140
45-140
17-147
19-140
36-146
45-153
1-202
26-144
30-147
50-150
32-140
45-140
34-140
37-142
10-130
10-130
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
1
1
1
1
3
1
1
1
1
1
1
1
1
1
3
1
2
0
This report shall not be reproduced, except in full,
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laceAnalyficalo
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QUALITY CONTROL DATA
Project: STORMWATER & TTO 11/15/119
Pace Project No.: 92453933
QC Batch: 510965 Analysis Method: EPA625A
QC Balch Method: EPA 625.1 Analysis Description: 625 MSS
Associated Lab Samples: 92453933001
METHOD BLANK: 2741120
Associated Lab Samples: 92453933001
Parameter
Units
Matrix: Water
Blank Reporting
Result Limit
Analy:red
1,2,4-Trichloiobenzene
ug/L
ND
5.0
11/23/19 10:21
2,2'-Oxybis(1-chloropropane)
ug/L
ND
5.0
11/23/1910:21
2,4,6-Trichlorophenol
ug/L
ND
10.0
11/23/19 10:21
2,4-Dichlorophenol
ug/L
ND
5.0
11/23/19 10:21
2,4-Dlmelhylphenol
ug/L
ND
10.0
11123/1910:21
2,4-Dinitrophenol
ug/L
ND
50.0
11/23/19 10:21
2,4-Dinitroto!uene
ug/L
ND
5.0
11/23/19 10:21
2,6-Dinitrotoluene
ug/L
ND
5.0
11/23/19 10:21
2-Chloronapllthalene
ug/L
NO
5.0
11/23/1610:21
2-Chlorophenol
ug/L
ND
5.0
11/23/19 10:21
2-Nitrophenol
ug/L
ND
5.0
11123/1910:21
3,3'-Dichlorcbenzidine
ug/L
ND
25.0
11123/11)10:21
4,6-Dinitro-2-methylphenol
ug/L
ND
20.0
11/23/19 10:21
4-Bromophenylphenyl ether
ug/L
ND
5.0
11123/19 10:21
4-Chloro-3-methylphenol
ug/L
ND
5.0
11/23/19 10:21
4-Chlorophenylphenyl ether
ug/L
ND
5.0
11/23/19 10:21
4-Nitrophenol
ug/L
ND
50.0
11/23/19 10:21
Acenaphthene
ug/L
ND
5.0
11123/1910:21
Acenaphtilylene
ug/L
ND
5.0
11/23,1910:21
Anthracene
ug/L
ND
5.0
11/23/19 10:21
Benzo(a)anthracene
ug/L
ND
5.0
11/23/19 10:21
Benzo(a)pyrene
ug/L
ND
5.0
11/23/19 10:21
Benzo(b)nuoranthene
ug/L
ND
5.0
11/23/19 10:21
Benzo(g,h,i)perylene
ug/L
ND
5.0
11/2311910:21
Benzo(k)fluoranthene
ug/L
ND
5.0
11/23/19 10:21
bis(2-Chloroethoxy)melhane
ug/L
ND
10.0
11/23/19 10:21
bis(2-Chloroelhyp ether
ug/L
ND
5.0
11/23/19 10:21
bis(2-Ethylhexyl)phthalate
ug/L
NO
5.0
11/23/19 10:21
Butylbenzylphlhalate
ug/L
ND
5.0
11/2311910:21
Chrysene
ug/L
ND
5.0
11/23/19 10:21
Di-n-butylphthalate
ug/L
ND
5.0
11/23/19 10:21
Di-n-octylphthalate
ug/L
ND
5.0
11/23/1910:21
Dibenz(a,h)anthracene
ug/L
ND
5.0
11/23/19 10:21
Diethylphthalate
ug/L
ND
5.0
11/23/19 10:21
Dimethylphthalate
ug/L
ND
5.0
11/23/19 10:21
Fluoranthene
ug/L
ND
5.0
11/23/19 10:21
Fluorene
ug/L
ND
5.0
11/23/19 10:21
Hexachloro-1,3-butadiene
ug/L
ND
5.0
11/23/19 10:21
Hexachlorobenzene
ug/L
ND
5.0
11/23/1910:21
Hexachlorocyclopenladiene
ug/L
ND
10.0
11/23/19 10:21
Hexachloroethane
ug/L
ND
5.0
11123/1910:21
Qualifiers
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Results presented on this page are In the units Indicated by the' Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, U.C.
Page 18 of 31

laceAnalj4icala
Pace Analytical Services, LLC
2225 Riverside Dr.
www,pacrlahs.csm
Asheville, NC 28804
[phone]
QUALITY
CONTROL
DATA
Project: STORMWATER&TT011/15//19
Pace Project No.: 92453933
METHODBLANK: 2741120
Matrix:
Water
Associated Lab Samples: 92453933001
Blank
Reporting
. Parameter
Units
Result
Limit
Analyzed
Qualifiers
Indeno(1,2,3-cd)pyrene
ug/L
NO
5.0
11/23/19 10:21
Isophorone
ug/L
NO
10.0
11/23/19 10:21
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
11/23/1910:21
N-Nitrosodimethylamine
ug/L
NO
5.0
11/23/1910:21
N-Nitrosodiphenylamine
ug/L
NO
10.0
11123/1910:21
Naphthalene
ug/L
NO
5.0
11/23/19 10:21
Nitrobenzene
ug/L
NO
5.0
11/23/19 10:21
Pentachlorophenol
ug/L
NO
10.0
11/23/1910:21
Phenanthrene
ug/L
ND
5.0
11/23/19 10:21
Phenol
ug/L
NO
5.0
11/23/19 10:21
Pyrene
ug/L
NO
5.0
11/23/19 10:21
2,4,6-Tribromophenol (S)
%
55
10-137
11/23/19 10:21
2-Fluorubiph'a iyl (S)
%
48
15-120
1112311E 10:21
2-Fluorophenol (S)
%
53
10-120
11/23/19 10*21
Nitrobenzene-d5 (S)
%
53
10-120
11/23/19 10:21
Phenol-d6 (S)
%
41
10-120
11/23/19 10:21
Terphenyl-d14 (S)
%
76
11-131
11/23/19 10:21
y LABORATORY CONTROL SAMPLE:
2741121
Spike
LCS
LCS %Rec
Parameter
Units
Conc.
Result % Rec Limits
Qualifiers
I' 1,2,4-Trichlorobenzene
ug/L
50
35.8
72
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
40.7
81
36-166
2,4,6-Trichlono phenoI
ug/L
50
40.8
82
37-144
2,4-Dichlorophenol
ug/L
50
40.0
80
1-191
2,4-Dimethylphenol
ug/L
50
43.5
87
32-119
2,4-Dinitrophenol
ug/L
250
217
87
1-181
�2,4-Dinilrotoluene
ug/L
50
44.4
89
39-139
2,6-Dinilrotoluene
ug/L
50
45.2
90
50-158
2-Chloronaphthalene
ug/L
50
45.2
90
60-118
2-Chlorophenol
ug/L
50
42.6
85
23-134
2-Nitrophenol
ug/L
50
41.4
83
29-182
3,3'-Dichlorobenzidine
ug/L
100
86.7
87
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
91.5
91
1-181
4-Bromophenylphenyl ether
ug/L
50
35.8
72
53-127
4-Chloro-3-melhylphenol
ug/L
100
90.4
90
22-147
4-Chlorophenylphenyl ether
ug/L
50
37.9
76
25-158
4-Nitrophenol
ug/L
250
229
92
1-132
Acenaphthene
ug/L
50
41.5
83
47-145
Acenaphthylene
ug/L
50
45.4
91
33-145
,Anthracene
ug/L
50
42.5
85
1-166
Benzo(a)anthracene
ug/L
50
42.6
85
33-143
IBenzo(a)pyrene
ug/L
50
45.1
90
17-163
Benzo(b)8uoranthene
ug/L
50
47.5
95
24-159
Results presented on this page are In the units Indicated by the "Units" column eacept where an alternate unit Is presented to the right al the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 31

lace Analytical
winu pacelabs.com
QUALITY CONTROL DATA
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28604
[phone]
Project: STORMWATER & TTO 11115//19
Pace Project No.: 92453933
LABORATORY CONTROL SAMPLE:
2741121
Spike
LCS
LCS
%Rec
Parameter
Units
Conic.
Result
% Rec
Limits Qualifiers
Benzo(g,h,i)perylene
ug/L
50
40.7
81
1-219
Benzo(k)fluoranthene
uglL
50
44.0
88
11-162
bis(2-Chloroethoxy)methane
ug/L
50
40.3
81
33-184
bis(2-Chloroethyl) ether
ug/L
50
41.8
84
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
47.7
95
8-158
Butylbenzylphthalate
ug/L
50
49.8
100
1-152
Chrysene
ug/L
50
39.9
80
17-168
Di-n-butylphthalate
ug/L
50
42.5
85
1-118
Di-n-octylphlhalale
ug/L
50
51.2
102
4-146
Dibenz(a,h)anthracene
ug/L
50
40.3
81
1-227
Diethylphthalale
ug/L
50
42.3
85
1-114
Dimethylphthalate
ug/L
50
40.1
80
1-112
Fluoranthene
ug/L
50
40.6
81
26-137
°Pdorcne
ug/L
50
42.4
,. 85
59-121
liexachloro-1,3-butadiene
ug/L
50
33.8
68
24-116
Hexachlorobenzene
ug/L
50
35.5
71
1-152
Hexachlorocyclopentadiene
ug/L
50
41.6
83
25-150
Hexachlomelhane
ug/L
50
40.4
81
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
41.6
83
1-171
Isophorone
ug/L
50
43.4
87
21-196
N-Nitroso-di-n-propylamine
ug/L
50
45.6
91
1-230
N-Nitrosodimethylamine
ug/L
50
45.1
90
25-150
N-Nitrosodiphenylamine
ug/L
50
39.6
79
25-150
Naphthalene
ug/L
50
40.6
81
21-133
Nitrobenzene
ug/L
50
41.5
83
35-180
Pentachlorophenol
ug/L
100
75.7
76
14-176
Phenanthrene
ug/L
50
39.9
80
54-120
Phenol
ug/L
50
48.7
97
5-112
Pyrene
ug/L
50
42.8
86
52-115
2,4,6-Tribromophenol(S)
%
72
10-137
2-Fluorobiphenyl (S)
%
65
15-120
2-Fluorophenol(S)
%
81
10-120
Nitrobenzene-d5 (S)
%
68
10-120
Phenol-d6 (S)
%
86
10-120
Terphenyl-dl4(S)
%
69
11-131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2741131 2741132
MS
MSD
35512782001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc,
Conc.
Result
Result
% Rec
%Rec
Limits
RPD Qual
1,2,4-Trichlorobenzene
ug/L
1.5U
50
50
22.3
35A
45
71
44-142
45 R1
2,2'-Oxybis(1-chloropropane)
ug/L
2.8U
50
50
29.6
42.8
59
86
36-166
36 R1
2,4,6-Trichlorophenol
ug/L
1.5U
50
50
21.5
33A
43
67
37-144
44 R1
2,4-Dichlorophenol
ug/L
1AU
50
50
21.7
38.7
43
77
1-191
56 Rt
2,4-Dimethylphenol
ug/L
1AU
50
50
NO
NO
1
2
32-119
M1
Results presented on this page are In the units Indicated by the "units- column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 31

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER & TTO 11/15//19
Pace Project No.: 92453933
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2741131
2741132
MS
MSD
35512782001
Spike
Spike
MS v
MSD
MS
MSD
%Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua[
.:,4-Dinitrophenol
ug/L
40.5U
250
250
80.2
84.0
32
34
1-181
5
2,4-Dinitrotoluene
ug/L
1.2U
50
50
39.7
48.8
79
98
39-139
20
2,6-Dinitrotoluene
ug/L
1AU
50
50
39.8
49.2
80
98
50-158
21
2-Chloronaphthalene
ug/L
1.5U
50
50
27.5
41.1
55
82
60-118
40 M1,R1
2-Ch[orophenol
ug/L
1.2U
50
50
24.3
39.9
49
80
23-134
49 R1
2-Nitrophenol
ug/L
1.4U
50
50
34.6
44.0
69
88
29-182
24
3,3'-Dichlorobenzidine
ug/L
3.OU
100
100
ND
ND
0
0
1-262
M1
4,6-Dinitro-2-methylphenol
ug/L
15.2U
100
100
52.7
61.8
53
62
1-181
16
4-Bromophenylphenyl ether
ug/L
1.6U
50
50
29.9
39.8
60
80
53-127
28
4-Chloro-3-methylphenol
ug/L
2.8U
100
100
23.1
86.6
23
87
22-147
116 R1
4-Chlorophenylphenyl ether
ug/L
1.61.1
50
50
29.6
40.8
59
82
25-158
32 R1
4-Nitrophenol
ug/L
3.5U
250
250
66.7
72.8
27
29
1-132
9
',Arenanhthene
ug/L
1.6U
50
50
_ 30.4 ,
_ 44.1
61
88
47-145
37 R1
Acenaphthylene
ug/L
1.6U
50
50
21.5
43.7
43
87
33-145
68 R1
Anthracene
ug/L
1.7U
50
50
27.3
45.6
55
91
1-166
50 R1
Benzo(a)anthracene
ug/L
1.8U
50
50
35.9
46.3
72
93
33-143
25
Benzo(a)pyrene
ug/L
2.1U
50
50
26A
47.0
52
94
17-163
57 R1
Benzo(b)fluoranthene
ug/L
< 1.9U
50
50
42.3
51.0
85
102
24-159
:19
Benzo(g,h,i)perylene
ug/L
1AU
50
50
42.8
49.5
86
99
1-219
15
,Benzo(k)fluoranthene
ug/L
1.9U
50
50
44.0
50.8
88
102
11-162
14
bis(2-Chloroethoxy)methane
ug/L
1.8U
50
50
28.4
42.0
57
84
33-184
39 R7
bis(2-Chloroethyp ether
ug/L
1.81.1
50
50
30.9
43.6
62
87
12-158
34 R1
bis(2-Ethylhexyl)phthalate
ug/L
2.1U
50
50
41.4
58.2
83
116
8-158
34 R1
Butylbenzylphthalate
ug/L
1.6U
50
50
42.0
53.2
84
106
1-152
24
Chrysene
ug/L
1.7U
50
50
37.9
45.5
76
91
17-168
18
Di-n-butylphthalate
ug/L
1.811
50
50
38.3
49.1
77
98
1-118
25
Di-n-octylphthalate
ug/L
1.8U
50
50
45.9
60.0
92
120
4-146
27
Dibenz(a,h)anthracene
ug/L
1.6U
50
50
42.8
49.0
86
98
1-227
14
Diethylphthalate
ug/L
2.4U
50
50
38.8
48.2
78
96
1-114
21
Dimethylphthalate
ug/L
1.6U
50
50
34.9
44.8
70
90
1-112
25
Fluoranthene
ug/L
1.7U
50
50
39.8
48.3
80
97
26-137
19
Fluorene
ug/L
1.61-1
50
50
34.5
46.2
69
92
59-121
29
Hexachloro-1,3-butadiene
ug/L
2.OU
50
50
19.6
32.7
39
65
24-116
50 Rl
Hexachlorobenzene
ug/L
1.7U
50
50
29.2
39.4
58
79
1-152
30
Hexachlorocyclopenladiene
ugli-
1.71.1
50
50
23.6
39.4
47
79
25-150
50 R7
Hexachloroethane
ug/L
2.OU
50
50
23.7
38.1
47
76
40-113
47 Rt
Indeno(1,2,3-cd)pyrene
ug/L
1.6U
50
50
42.7
49.4
85
99
1-171
15
Isophorone
ug/L
1.6U
50
50
30.9
45.6
62
91
21-196
38 R1
N-Nitroso-di-n-propylamine
ug/L
2.2U
50
50
31.6
46.0
63
92
1-230
37 RI
N-Nitrosodimethylamine
ug/L
1.2U
50
50
27.7
39.7
55
79
25-150
36 R1
N-Nilrosodiphenylamine
ug/L
1.711
50
50
26.8
40.7
54
81
25-150
41 R1
Naphthalene
ug/L
1.411
50
50
28.3
42.1
57
84
21-133
39 R1
Nitrobenzene
ug/L
2.1U
50
50
44.7
59.6
89
119
35-180
29
Pentachlorophenol
ug/L
2.21-1
100
100
24.3
27.8
24
28
14-176
13
Phenanthrene
ug/L
1.71.1
50
50
37.3
46.6
75
93
54-120
22
Phenol
ug/L
0.91U
50
50
10.6
24.8
21
50
5-112
80 R1
Results presented on
this page are In
the units Indicated by the
-units" column except where an alternate
unit is presented
to the night
or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 31

laceAnalytical"
www.pacelabs.com
QUALITY CONTROL DATA
Project: STORMWATER & TTO 111151119
Pace Project No.: 92453933
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE: 2741131
MS
35512782001 Spike
Parameter
Units Result Conc.
Pyrene
ug/L 2.1U 50
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl(S)
%
2-Fluorophenol(S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
2741132
MSD
Spiky
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits RPD
50
38.7
48.8
77
98
52-115 23
47
76
10-137
54
84
15-120
32
66
.10-120
62
90
10-120
22
54
10-120
47
58
11-131
Results presented on this page are In the units Indicated by the "Units" column except where an altemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/27/201904:46 PM wilhoulthe written consentof Pace Analytical Services,LLC.
Dual
Page 22 of 31

laceAnalyficale
www.pacelabs.cam
'I
QUALITY CONTROL DATA
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
STORMWATER&TT011/15//19
Pace Project No.:
92453933
QC Batch:
510807 Analysis Method: SM 254OD-2011
QC Batch Method:
SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92453933001 "
METHOD BLANK: 2740459
Associated Lab Samples: 92453933001
Parameter Units
Total Suspended Solids mg/L
Matrix: `Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 11/2011923:02
LABORATORY CONTROL SAMPLE: 2740460
Spike LCS LCS % Red
Parameter Units Cone. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 244 98 90-110
SAMPLE DUPLICATE: 2740461
92454201001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 174 223 25
SAMPLE DUPLICATE: 2740462
92453958001 Dup
Parameter Units Result Result RPD Qualifiers
" Total Suspended Solids mg/L 216 180 18
Results presented on this page are In the units Indicated by the "units" column except where an alternate unit is presented lathe right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 31

ace Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: STORMWATER & TTO 11/15//19
Pace Project No. 92453933
QC Batch: 509992 Analysis Method: SM 4500-H+B-2011
QC Batch Method: SM 4500-H+B-2011 Analysis Description: 4500H+B pH
Associated Lab Samples: 92453933001
SAMPLE DUPLICATE: 2736833
92453583001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 7.0 6.9 2 D6,H3
SAMPLE DUPLICATE: 2736834
92453741004 Cup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 4.4 4.4 0 H3
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Results presented on this page are In the units indicated by the"Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 31

laceAnalyfical'
www.pacelabs.coro
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
STORMWATER & TTO 11/151119
Pace Project No.:
92453933
QC Batch:
510339 Analysis Method: EPA 420.4 Rev 1.0 1993
QC Batch Method:
EPA 420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics
Associated Lab Samples: 92453933001 -'-
METHOD BLANK: 2738282 Matrix: Water
Associated Lab Samples: 92453933001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phenol mg/L NO 0,020 11/20/1912:26
LABORATORY CONTROL SAMPLE: 2738283
i,
Spike
LCS
LCS
% Rec
Parameter Units
Conic.
Result
%Rec
Limits
Qualifiers
Phenol mg/L
0.05
0,048
96
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2738284
2738285
MS
MSD
92453833001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter - Units Result
Conic.
Conic.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Phenol mg/L 0,029
0.05
0.05
0.071
0.072
84
85
90-110
1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2738286
2738287
MS
MSD
92453418001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result
Conic.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Phenol mg/L NO
0.05
0.05
0.059
0.047
112
89
90-110
22 M1,R1
Results presented on this page are in the units indicated by the -Units" column except where an altemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 31

laceAnaVicale
wivw.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER & TTO 11/15/l19
Pace Project No.: 92453933
QC Batch: 510745
Analysis
Method: SM 4500-CN-E-2011
QC Batch Method: SM 4500-CN-E-2011
Analysis
Description: 450OCNE Cyanide, Total
Associated Lab Samples: 92453933001
METHOD BLANK: 2740045
Matrix: Water
Associated Lab Samples: 92453933001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Cyanide mg/L
NO 0.0080
11/21/1g 14:23
LABORATORY CONTROL SAMPLE: 2740046
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits
Qualifiers
Cyanide mg/L
0.1
0.10
101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2740047
2740048
MS
MSD
92454443002
Spike
Spike MS
MSD MS
MSD
n/ Rec
Parameter Units Result
Conc.
Conc. Result
Result " % Rec
% Rec
Limits RPD Qual
Cyanide mg/L 0,024
0.1
0.1 0.11
0.12 86
92
80-120 5
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2740049
2740050
MS
MSD
92454448002
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec
a/ Rec
Limits RPD Qual
Cyanide mg/L NO
0.1
0.1 0.029
0.075 27
74
80-120 90 M1,R1
Results presented an this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 31

(15'ceAnaIjUale
www.paalabs.com
QUALIFIERS
Project: . STORMWATER & TTO 11/15//19
Pace Project No.: 92453933
DEFINITIONS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, INC 28804
[phone]
OF - DiluCnn Factor, if reported, represents the factor applied to the reported data due to dilution of,lhe sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Toy Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
POL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MSO) - Matrix Spike (Duplicate)
OUR - Sartiple Duplicate -
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
Ml Matrix spike recovery exceeded QC limits. Balch accepted based on laboratory control sample (LCS) recovery.
Rl RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 31

lace Analytical
www.pacelabs.carn
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.'.
STORMWATER 8. TTO 11/15//19
92453933
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92453933001
SW#1
EPA 1664B
511848
92453933001
SW#1
EPA 608.3
510331
EPA 608.3
510562
92453933001
SW#1
EPA 200.7 Rev 4.4 1994
511090
EPA 200.7 Rev 4.4 1994
511122
92453933001
SW#1
EPA 3010A
510826
EPA6010D
510852
92453933001
SW#1
EPA7470A
510082
EPA 7470A
510149
92453933001
SW#1
EPA 625.1
510965
EPA 625A
511311
92453933001
SW#1
EPA 624.1
510507
92463933001
SW#1
SM 2540D-2011
510807
92453933001
SW#1
SM 4500-H+B.2011
509992
92453933001
SW#1
EPA 420.4 Rev 1.0 1993
510339
EPA 420.4 Rev 1.0 1993
510597
92453933001
SW#1
SM 4500-CN-E-2011
510745
SM 4500-CN-E-2011
510913
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/27/2019 04:46 PM without the written consent of Pace Analytical Services, LLC, Page 28 of 31

Document Name:
Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
aceAnal�tical
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving sa pies:
Asheville Eden❑ Greenwood❑ Huntersville❑ �} Raleigh[] Mechanicsville❑
Client Name: W®## :92453933
.. •.. ����/'�it71'� l YI`1 Projects 11111111111111111111111
Courier: ❑Fed Ex ❑UPS ❑USPS ❑Client
❑ Commercial opace ❑Other._ r 92453933
Custody Seal Present? []Yes�o Seals Intact? []Yeso D
Date/Initials Person Examining Contents:
Packing Material: []Bubble Wrap Bubble Bags []None ❑ Other Biological Tissue Frozen?
'Thermometer ((yy i ❑Yes ❑ND�/A
IR Gun ID: 1 tv Type of Ice: Net [—]Blue ❑Hone
Cooler Temp ("C): ,— Correction Factor: Add/Subtract (°C) b /.d
Temp should he above freezing to 6°C
Cooler Temp Corrected (`C): 3• Z samples out of temp criteria. Samples on ice, cooling process
--// hss begun
USDA Regulated Soil ( N/A, water sample)
Did samples originates a quarantine zone within the United States: CA, NY, of 5C (check maps)? Did simples originate from a foreign source (Internationally,
Va,,rr and Puerto Rlco)?❑Yes nNo
Comments/Discrepancy:
Chain of Custody Present?
Yes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
Yes
❑No
❑N/A
2.
Short Hold Time Analysis (472 hr.)?
❑Yes
No
❑N/A
_
3.
Rush Turn Around Time Requested?
❑Yes
No
❑N/A
4.
Sufficient Volume?
Myes
No
[]N/A
5.
Correct Containers Used?
-Pace Containers Used?
Yes
Yes
❑No
[]NO
❑N/A
❑N/A
6.
Containers Intact?
Yes
❑No
[]N/A
7.
.Dissolved analysis: Samples Field Filtered?
❑Yes
ZrNo
❑N/A
9.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
/ -oYes
'V '
[]No❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
-
❑N/A
10,
Trip Blank Present?
Trip Blank Custody Seals Present?
❑yes
❑Yes .
g9 No
[IN.
❑N/A
N/A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑yes [340
1
i
i
{ Lot IDof split containers:
f{ CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time: _
Project Manager SCURL K"Iew: Date-
' Date _
Project Manager SRF Review: ..
Page 29 of 31

Document Name: Document Revised: February 7, 2013
r Sample Condition Upon Receipt)SCUR) Page 1 of 2
% ,PaceAaaVjlca) Document No.: Issuing Authority:
F-CAR-CS-033-Rev.
06 Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions. VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project # WO# : 92453933
PM: UP Due Date: 12/02/19
CLIENT: 93—Linamar
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pH Adjustment
Sample ID Type of Preservative pH upon receipt
Log for Preservea z-ampies
Date preservation adjusted Time preservation Amount of Preservative Lot q
adjusted added
'Il the
-ernlina DEHNR Certification Office (i.e.
Note: Whenever there s a discrepancy affecting North Carolina compliance samples,acopy of this form vn be sent to
Out of hold, Incorrect preservative, out of temp, incorrect containers.
Page 30 of 31

M
O
I Analytical Request Document
CHAIN -OF -CUSTODY
fields must be completed accurately.
dody
is a LEGAL DOCUMENT. All relevant
�
aceMah,Ainl
The Chain-of-Cust
a
�
Section
section
Involcc lahmeatlon: -
Socha. A
Required Project information:
Required Client Information'
Allenlion: -
'Company: Lmamar Nc:`AldRoad
ReponTp: Nicol-
--
Grwin Compam'Name:
- '..Re ulato A do
-�--
Address'. 2169 Hentlersonv vflIle R
Copy To:
Atldress -
Pace Duole: �°
State/Location
Arden. NC 28704
Pu¢hase Order a:
pay project Manager: lorri, ll n colabs ym,
Email: mcalo,din linamaf.cdm
Fax_
Pd Name:
e l ro
Stofmwater.8 TT0 - - Pace Profile a: 0000 -
-sia
M
Phone: [phone]B3
Projeda;
Rc uaalbd Ansl Flltamd
Requesteue ate:"ti
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as
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-
_ Preservatives Y
-
COLLECTED a Z
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SAMPLE ID
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END s START
One Character per box.
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SAMPLER NAME AND sIGNATURE�, - �
1 DATESigned:;\ �' C r r$�'yi+�
SIGNATUREoisAMPLEft: / 1
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