NCG030605_MONITORING INFO_20200110

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/v
DOC TYPE
❑ HISTORICAL FILE
❑K MONITORING REPORTS
DOC DATE
❑ duo u b l o
YYYYM M DD

DOC TYPE I ❑ HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE 1 ❑
YYYYM M D D

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted I .0 D 10
CERTIFICATE OF COVERAGE NO. N0003 0 6 0 5
FACILITY NAME _
COUNTY Cherokee
Inc
PERSON COLLECTING SAMPLES Danielle Loyd
LABORATORY Pace Analytical Lab Cert. ft 40
Comments on sample collection or analysis:
Part A: stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2019
SAMPLE PERIOD ❑ Jan -June Q July -Dec
or ❑ Monthly' (month)
FUTARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
RE,C E's /�/ ❑zero -flow ❑Water supply ❑SA
JAN 10 2a2a ❑other
CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
DWR SECTION
No discharge this periodj2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
pH
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics
g
Benchmarks
-
- -
100 mg/L or 50 mg/L4
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
SD02
11/23/19
0.60
66.9
6.4
0.0101
ND
0.0534
NO
NO
SD03
11/23/19
0.60
10.2
6.8
0.0063
ND
0.0137
NO
ND
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
' See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
Signature
Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
n No discharge this period ?2
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches'
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/L^
Parameter Code
-
46529
NCOIL
00552
COS30
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/l/2018-05/31/2021 SWU-245, last revised 11/1/2018
_ . _ - _ _ -_ Page.2 of 3. _ _

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an oriainal copv of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results (or at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
4-1
Signature of Permittee
Permit Date: 11/1/2018-05/31/2021
Date
SWU-245, last revised 11/1/2018
Page 3 of 3

Environmental ,
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deq.nc.gdv/about/divisions/energy-mineral-land-resources/
npde s-storm Ovate r-g p s
Permit No.: N/C/ / / / /, / / / or Certificate of Coverage No.: N_/C/G/Q 1310 /b /0151
Facility Name: Mon Im,
County: VVIPiVUK
Inspector: —VA—
Date of Inspection:
Time of Inspection:
I
Total Event Precipitation (inches):
Phone No.
All permits require qualitative monitoring to be performed during a "measurable storm event."
c:
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Pennittee or Designee)
II
q
1. Outfall �D�p
Description: ,
Outfall No. -y Structure (pipe, ditch, etc.): {' ig,
Receiving Stream:
Gv h
Describe the industrial activities that occur wit in the outfall drainage area:
Page 1 of 2
SWII-242, Lastmoditied 06/01/2019

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: ( IefAy IT) 11 G414{' (q► MAA
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): N&
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
1 © 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids_ in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
l0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
02 3 4 5
7. Is there any foam in the stormwater discharge'? o Yes • No.
8.
9.
Is there an oil sheen in the stormwater discharge? OYes p No.
Is there evidence of erosion or deposition at the outfall? o Yes • No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018

Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report "
Forguidnnce onfilling out thisform, please visit https:Hdeq.iic.gov/about/divisions/eiierey-mineral-land-resources/
n pdes-storm water-gps
Pennit No.: N/C/ / / / / /, / / or Certificate of Coverage No.: N/C/G/ 0/3 /0 /6 / 0/ S
Facility Name:
County: _
Inspector:
Date of Inspection: -2:3 " I q
Time of Inspection: QYN
Total Event Precipitation (inches): 0.601,
No. 023- W-56
All permits require qualitative monitoring to be performed during a "measurable storm event."
u
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
Outfall. The previous measurWe storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Pennittee or Designee)
1. Outfall Description: j,
Outfall No. S 3 Structure (pipe, ditch, etc.): 6kV�
Receiving Stream:
the industrial activities that occur within the outfall drainage area:
Page I of 2
S W U-242, Last moth fled OG/01/20 i g

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: G�A V
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): N I A
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
O2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, wherd I'•ismo Sofids and 5 is the surface covered with floating solids:
V 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
O 2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes • No.
8. Is there an oil sheen in the stormwater discharge? OYes A No.
9. Is there evidence of erosion or deposition at the outfall? O Yes ® No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low.clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. 'These conditions warrant. further investigation.
Page 2 of 2
S W U-242. Last aunhlied 06/01 /1018

laceAnalytical'
www.Decslehscom
December 10, 2019
Danielle Loyd
Moog Components
1995 NC Hwy 141
Murphy, NC 28906
RE: Project: STORMWATER SD-02
Pace Project No.: 92455202
Dear Danielle Loyd:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 26, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 27

aceAnalytical
www.Dacelabs.com
CERTIFICATIONS
Project: STORMWATER SD-02
Pace Project No.: 92455202
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
LouisianalNELAP Certification # LA170028
FloridalNELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
FloridalNELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
VirginialVELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
f TxSdi��T3A\ ZiI:7_`t�I �L•\:/c1A6969
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 27

Pace Analytical Services, LLC
aceAnalytical e 2225 Riverside Dr.
Asheville, NC 28804
www.paceleb.com [phone]
SAMPLE ANALYTE COUNT
IProject: STORMWATER SD-02
Pace Project No.: 92455202
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92455202001 SD2 EPA 16648
HH
1
PASI-C
EPA 608.3
SEM
29
PASI-C
EPA 200.7 Rev 4.41994
SH7
12
PASI-A
EPA 245.1 Rev 3.01994
SOO
1
PASI-A
EPA 625.1
BPJ
58
PASI-C
EPA 624.1
DLK
34
PASI-C
SM 254OD-2011
MJP
1
PASI-A
,i EPA 420.4 Rev 1.0 1993
i
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 27

m
aceAnalytical
www.pacelebs.com
f_\.I_\��1UL•i�:7�Y�1y��
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER SD-02
Pace Project No.: 92455202
Sample: SD2 Lab ID: 92455202001 Collected: 11/23/1912:42 Received: 11/26/19 10:20 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual
1664 SGT•HEM, TPH
Analytical Method: EPA 1664B
TotaLPelroleum.Hydrocarbons
ND_mglL
4,8_i
12/10/1910:25
608 PCB Pest RVE
Analytical Method:
EPA 608.3 Preparation Method:
EPA
608.3
Aldrin
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 18:30
309-00-2
alpha-BHC
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 18:30
319-84-6
beta-BHC
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 18:30
319-85-7
delta-BHC
NO
ug/L
0.050
1
11/27/19 09:44
12/0411918:30
319-86-8
gamma-BHC(Lindane)
NO
ug/L
0.050
1
11/2711909:44
12/0411918:30
58-89-9
Chlordane (Technical)
NO
ug/L
0.50
1
11/27/1909:44
12/04M918:30
57-74-9
alpha -Chlordane
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 18:30
5103-71-9
gamma -Chlordane
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 18:30
5103-74-2
4,4'-DDD
NO
ug/L
0.050
1
11/2711909:44
12104/1918:30
72-64-8
4 4'-DDE
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 18:30
72-55-9
4,4'-DDT
NO
ug/L
0.050
1
11/27/1909:44
12/04/19 18:30
50-29-3
. Dieldrin
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 18:30
60-57-1
EndosulfanI
NO
ug/L
0,050
1
11/2711909:44
12104/1918:30
959-98-8
Endosulfan II
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 18:30
33213-65-9
Endosulfan sulfate
NO
ug/L
0.050
1
11/27/1909:44
12/04/19 18:30
1031-07-8
Endrin
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 18:30
72-20-8
Endrin aldehyde
NO
ug/L
0,050
1
11/27/19 09:44
12/04/19 18:30
7421-93-4
Heptachlor
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 18:30
76-44-8
Heptachlor epoxide
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 18:30
1024-57-3
PCB-1016 (Aroclor 1016)
NO
ug/L
0.50
1
11/27/19 09:44
12/04/19 18:30
12674-11-2
PCB-1 221 (Aroclor 1221)
NO
ug/L
0.50
1
11/27/19 09:44
12/04/19 18:30
11104-28-2
PCB-1232 (Aroclor 1232)
NO
ug/L
0.50
1
11/27/19 09:44
12/04/19 18:30
11141-16-5
, PCB-1242 (Aroclor 1242)
NO
ug/L
0.50
1
11/27/19 09:44
12/04/19 18:30
53469-21-9
PCB-1248 (Aroclor 1248)
NO
ug/L
0.50
1
11/27/19 09:44
12/04/19 18:30
12672-29-6
PCB-1254 (Aroclor 1254)
NO
ug/L
0.50
1
11/27/19 09:44
12/04/19 18:30
11097-69-1
PCB-1260 (Arocor 1260)
NO
ug/L
0.50
1
11/27/19 09:44
12/04/19 18:30
11096-82-5
Toxaphene
NO
ug/L
0.50
1
11/27/19 09:44
12104/1918:30
8001-35-2
Surrogates
Tetrachloro-m-xylene(S)
127
%
10-130
1
11/27/19 09:44
12/04/19 18:30
877-09-8
Decachlorobiphenyl(S)
101
%
10-130
1
11/27/19 09:44
12/04/19 18:30
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Rev
4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Antimony
NO
ug/L
5.0
1
11/27/19 01:21
12/03/19 01:19
7440-36-0
Arsenic
NO
ug/L
10.0
1
11/27/19 01:21
12/03/19 01:19
7440-38-2
Beryllium
NO
ug/L
1.0
1
11/27/19 01:21
12/03/19 01:19
7440-41-7
Cadmium
NO
ug/L
1.0
1
11/27/19 01:21
12/03/19 01:19
7440-43-9
Chromium
0.6
_.-10.1�
ug/L
ug/L
5.0
5.0
1
1
11/27/19 01:21
11/27/19 01:21
12/03/19 01:19
12/03/1901:19
744047-3
7440-50-8
Copper
Lead
NO
ug/L
5.0
1
11/27/19 01:21
12/03/19 01:19
7439-92-1
Nickel
8.1
ug/L
5.0
1
11/27/19 01:21
12/03/19 01:19
7440-02-0
Selenium
NO
ug/L
10.0
1
11/27/19 01:21
12/03/19 01:19
7782-49-2
Silver
NO
ug/L
5.0
1
11/27/19 01:21
12/03/19 01:19
7440-22-4
Thallium
ND
ug/L
10.0
1
11/27/19 01:21
12/03/19 01:19
7440-28-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
'Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 27

(�IaceAnalyficalo
www.pacelebs.com
ANALYTICAL RESULTS
Project: STORMWATER SD-02
Pace Project No.: 92455202
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: SD2 Lab ID: 92455202001 Collected: 11/2311912:42 Received: 11/26/1910:20 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua]
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Zinc 53.4__ug/L 10.0 1 11/27/1901:21 12/03/1901:19 7440-66-6
245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Mercury NO ug/L 0.20 1 12/04/1917:44 12/05/1914:04 7439-97-6
625 MSSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
'Acenaphthene
NO
ug/L
5.0
1
11/27/1914:36
12103/1919:47
83-32-9
'..Acenaphthylene
NO
ug/L
5.0
1
11/27/19 14:36
12/0311919:47
208-96-8
Anthracene
ND
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
120-12-7
Benzo(a)anthracene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
56-55-3
Benzo(a)pyrene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
50-32-8
Benzo(b)0uoranthene
NO
ug/L
5.0
1
11/2711914*36
12/03/19 19:47
205-99-2
Benzo(g,h,i)perylene
NO
ug/L
5.0
1
11127/19 14:36
12/03/19 1947
191-24-2
Benzo(k)0uoranthene
NO
ug/L
5.0
1
11/27/191436
12103/1919:47
207-08-9
4-Bromophenylphenyl ether
NO
ug/L
5.0
1
11/27/19 14:36
12/0311919:47
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
11/27/1914:36
12/03/19 19:47
85-68-7
4-Chloro-3-methylphenol
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
59-50-7
bis(2-Chloroethoxy)methane
NO
ug/L
10.0
1
11/27/19 1436
12/03/19 19:47
111-91-1
bis(2-Chloroethyl) ether
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
111-44-4
2-Chloronaphthalene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
91-58-7
2-Ch]orophenol
NO
ug/L
5.0
1
11127/1914:36
12/03/1919:47
95-57-8
4-Chloropheny]phenyl ether
NO
ug/L
5.0
1
11/27/19 1436
12/03/19 19:47
7005-72-3
Chrysene
ND
ug/L
5.0
1
11/27/191436
12103/1919:47
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
53-70-3
3,3'-Dichlorobenzidine
NO
ug/L
25.0
1
11/27/19 14:36
12/03/19 19:47
91-94-1
12,4-Dichlorophenol
ND
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
120-83-2
'.Diethy]phthalate
NO
ug/L
5.0
1
11/27/19 14:36
12/0311919:47
84-66-2
2,4-Dimelhylphenol
NO
ug/L
10.0
1
11/27/19 14:36
12/03/19 19:47
105-67-9
Dimelhylphthalale
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
11/27/19 14:36
12/03/191947
84-74-2
14,6-Dinitro-2-methylphenol
NO
ug/L
20.0
1
11/27/19 14:36
12/03/19 19:47
534-52-1
.2,4-Dinitrophenol
NO
ug/L
50.0
1
11/27/19 1436
12/03/19 1947
51-28-5
2,4-Dinitrotoluene
NO
ug/L
5.0
1
11/27/19 1436
12/03/19 19:47
121-14-2
2,6-Dinitrotoluene
NO
ug/L
5.0
1
11/27/19 1436
12/03/19 19:47
606-20-2
Di-n-octylphtha]ate
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
117-84-0
bis(2-Ethylhexyl)phthalate
NO
ug/L
5.0
1
11127/1914:36
12/03/19 19:47
117-81-7
Fluoranthene
ND
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
206-44-0
iFluorene
ND
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
87-68-3
Hexachlorobenzene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/191947
118-74-1
Hexachlorocyclopentadiene
NO
uglL
10.0
1
11/27/19 14:36
12/03/19 19:47
77-47-4
Hexachloroethane
NO
ug/L
5.0
1
11/2711914:36
12/031191947
67-72-1
lndeno(1,2,3-cd)pyrene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
193-39-5
'lsophorone
NO
ug/L
10.0
1
11/27/19 14:36
12103/1919:47
78-59-1
Naphthalene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
91-20-3
..Nitrobenzene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
98-95-3
REPORT
OF LABORATORY
ANALYSIS
This report shall not
be reproduced, except
in full,
Date: 12/10/2019 05:51 PM
without
the written consent
of Pace Analytical Services,
LLC.
Page 5 of 27

aceAnalytical
www.pacelabs.cpm
I
ANALYTICAL RESULTS
Project: STORMWATER SD-02
Pace Project No.: 92455202
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: SD2 Lab ID: 92455202001 Collected: 11/23/1912:42 Received: 11/26/19 10:20 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
1625 MSSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
2-Nitrophenol
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
88-75-5
4-Nitrophenol
NO
ug/L
50.0
1
11/27/19 14:36
12/03/191947
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
62-75-9
IN-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
621-64-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
1
11/27/19 14:36
12/03/19 19:47
86-30-6
2,2'-Oxybis(1-chloropropane)
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
108-60-1
Pentachlorophenol
NO
ug/L
10.0
1
11/27/19 14:36
12/03/19 19:47
87-86-5
Phenanthrene
NO
ug/L
5.0
1
11/27/19 14:36
1210311919:47
85-01-8
Phenol
ND
ug/L
5.0
1
11/27/1914:36
12/03/19 19:47
108-95-2
Pyrene
ND
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
129-00-0
1,2,4-Tdchlorobenzene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:47
120-82-1
2,4,6-Tdchlorophenol
NO
ug/L
10.0
1
11/27/19 14:36
12/03/19 19:47
88-06-2
Surrogates
Nitrobenzene-d5 (S)
34
%
10-120
1
11/27/19 14:36
12/03/19 19:47
4165-60-0
�2-Fluorobiphenyl(S)
38
%
15-120
1
11/27/19 14:36
12/03/19 19:47
321-60-8
Terphenyl-d14(S)
85
%
11-131
1
11/27/19 14:36
12/03/1919:47
1718-51-0
Phenol-d6(S)
11
%
10-120
1
11/27/19 14:36
12/03/19 19:47
13127-88-3
2-Fluorophenol(S)
11
%
10-120
1
11/27/19 14:36
12/03/19 19:47
367-12-4
2,4,6-Tdbromophenol (S)
54
%
10-137
1
11/27/19 14:36
12/03/19 19:47
118-79-6
624 Volatile Organics) Analytical Method: EPA 624.1
Benzene
NO
ug/L
1.0
1
12/05/19 15:18
71-43-2
Bromodichloromethane
NO
ug/L
2.0
1
12/05/1915A8
75-27-4
Bromoform
NO
ug/L
2.0
1
12/05/19 15:18
75-25-2
Bromomethane
NO
ug/L
2.0
1
12/05/19 15:18
74-83-9
Carbon tetrachloride
NO
ug/L
2.0
1
12/05/19 15:18
56-23-5
Chlorobenzene
NO
ug/L
2.0
1
12/05/19 15:18
108-90-7
Chloroethane
NO
ug/L
2.0
1
12/05/19 15:18
75-00-3
Chloroform
ND
ug/L
2.0
1
12/05/19 15:18
67-66-3
Chloromelhane
NO
ug/L
2.0
1
12/05/19 15:18
74-87-3
Dibromochloromethane
NO
ug/L
2.0
1
12/05/19 15:18
124-48-1
1,2-Dichlorobenzene
NO
ug/L
2.0
1
12/05/19 15:18
95-50-1
1,3-Dichlorobenzene
NO
ug/L
2.0
1
12/05/19 15:18
541-73-1
11,4-Dichlorobenzene
NO
ug/L
2.0
1
12/05/19 15:18
106-46-7
1,1-Dichloroethane
NO
ug/L
2.0
1
12/05/19 15:18
75-34-3
1,2-Dichloroethane
NO
ug/L
2.0
1
12/05/19 15:18
107-06-2
1,1-Dichloroethene
NO
ug/L
2.0
1
12/05/19 15:18
75-35-4
cis-1,2-Dichloroethene
NO
ug/L
2.0
1
12/05/19 15:18
156-59-2
trans-1,2-Dichloroethene
NO
ug/L
2.0
1
12/05/19 15:18
156-60-5
1 2 Dichloropropane
NO
ug/L
2.0
1
12/05/19 15:18
78-87-5
,L cis-1,3-Dichloropropene
NO
ug/L
2.0
1
12/05/19 15:18
10061-01-5
trans-1,3-Dichloropropene
NO
ug/L
2.0
1
12/05/19 15:18
10061-02-6
Ethylbenzene
NO
ug/L
1.0
1
12/05/1915:18
100-41-4
Methylene Chloride
NO
ug/L
2.0
1
12/05/19 15:18
75-09-2
1,1,2,2-Tetrachloroethane
NO
ug/L
2.0
1
12/05/19 15:18
79-34-5
Tetrachloroethene
NO
ug/L
2.0
1
12/05/19 15:18
127-18-4
Toluene
NO
ug/L
1.0
1
12/05/19 15:18
108-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/10/2019 05:51 PM without the writlen consent of Pace Analytical Services, LLC. Page 6 of 27

(�IaceAnalj4ical-
W%ini,pecilabil.com
ANALYTICAL RESULTS
Project: STORMWATER SD-02
Pace Project No.: 92455202
Pace Analytical services, LLC
2225 Riverside Or.
Asheville, NC 28804
[phone]
Sample: SD2 Lab ID: 92455202001 Collected: 11/23/19 12:42 Received: 11/26/19 10:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
624 Volatile Organics Analytical Method: EPA 624.1
1,1, 1 -Trichloroethane
ND
ug/L
2.0
1
12/05/19 15:18
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1
12/05/19 15:18
79-00-5
Trichloroethene
ND
ug/L
2.0
1
12/05/19 15:18
79-01-6
'r Trichloro0uoromethane
ND
ug/L
2.0
1
12/05/19 15:18
75-69-4
Vinyl chloride
NO
ug/L
2.0
1
12/05/19 15:18
75-01-4
Surrogates
4-Bromo6uorobenzene (S)
105
a/
70-130
1
12/05/19 15:18
460-00-4
Toluene-d8 (S)
103
%
70-130
1
12/05/19 15:18
2037-26-5
1,2-Dichloroethane-d4(S)
109
a/
70-130
1
12/05/1915:18
17060-07-0
2540D Total Suspended Solids Analytical Method: SM 2540D-2011
LTotal. Suspended. Solids 66.9 mg/L./ 7A 1 11/27/1912:23
,420.4 Phenolics, Total Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Phenol ND mg/L 0.020 1 12/03/19 09:35 12/03/19 12:59 108-95-2
Date: 12/10/201905*51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 27

aceAnalytical
wwr.0acalabs.com
QUALITY CONTROL DATA
Project: STORMWATER SD-02
Pace Project No.: 92455202
QC Batch: 513867 Analysis Method: EPA 1664E
OC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH
Associated Lab Samples: 92455202001
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
2754405
Spike LCS
LCS
%Rec
Parameter
Units
Conc. Result
%Rec
Limits
Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 15.6
78
64-132
MATRIX SPIKE SAMPLE:
2754406
92455125001 Spike
MS
MS
e/ Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
NO 19.2
5.4
22
64-132 M1
Results presented on this page are in the units Indicated by the "Uolti column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 27

0
aceAnalytical
www.penlebs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
STORMWATER SD-02
Pace Project No.:
92455202
OC Batch:
512899 Analysis Method: EPA 245.1 Rev 3.0 1994
OC Batch Method:
EPA 245.1 Rev 3.0 1994 Analysis Description: 245.1 Mercury
Associated Lab Samples:
92455202001
METHOD BLANK: 2749676
i
Associated Lab Samples: 92455202001
Parameter Units
Mercury ug/L
I
LABORATORY CONTROL SAMPLE: 2749677
Parameter Units
' Mercury ug/L
b
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.20 12/05/1912:50
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
2.5 2.6 104 85-115
,MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2749678
2749679
MS
MSD
92455457003 Spike
Spike
MS
MSD MS MSD e/ Rec
Parameter Units Result Conc.
Conc.
Result
Result %Rec %Rec Limits RPD Qual
I Mercury uglL 55.9 2.5
2.5
56.7
58.0 34 84 70-130 2 M6
'.MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2749680
2749681
MS
MSD
92455457005 Spike
Spike
MS
MSD MS MSD e/ Rec
Parameter Units Result Conc.
Conc.
Result
Result e/ Rec % Rec Limits RPD Qual
Mercury ug/L NO 2.5
2.5
2.7
2.5 103 99 70-130 4
Results presented on this page are In the units indicated by the -Units" column except where an alternate unit Is presented to the right of Me result.
REPORT Of LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Dale: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 27

ace Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: STORMWATER SD-02
Pace Project No.: 92455202
QC Batch: 511985 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92455202001
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 2745906
Matrix:
Water
Associated Lab Samples: 92455202001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Antimony
ug/L
NO
5.0
12/03/19 00:31
i Arsenic
ug/L
NO
10.0
12/03/19 00:31
Beryllium
ug/L
NO
1.0
12/03/19 00:31
Cadmium
uglL
NO
1.0
1210311900:31
Chromium
ug/L
NO
5.0
12/03/19 00:31
Copper
ug/L
NO
5.0
12/03/19 00:31
Lead
ug/L
NO
5.0
12/03/19 00:31
Nickel
ug/L
NO
5.0
12/03/19 00:31
"Selenium
ug/L
NO
10.0
12/03/1900:31
Silver
ug/L
ND
5.0
12/0311900:31
Thallium
ug/L
NO
10.0
12/03/19 00:31
,Zinc
ug/L
NO
10.0
12/03/19 00:31
LABORATORY CONTROL SAMPLE:
2745907
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
e/ Rec Limits Qualifiers
Antimony
ug/L
500
479
96
85-115
Arsenic
ug/L
500
481
96
85-115
Beryllium
ug/L
500
470
94
85-115
Cadmium
ug/L
500
464
93
85-115
Chromium
ug/L
500
457
91
85-115
Copper
ug/L
500
466
93
85-115
Lead
ug/L
500
467
93
85-115
Nickel
ug/L
500
459
92
85-115
Selenium
ug/L
500
468
94
85-115
Silver
ug/L
250
234
94
85-115
Thallium
ug/L
500
458
92
85-115
Zinc
11
ug/L
500
466
93
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2745908
2745909
MS
MSD
92454946001
Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits RPD
Antimony
ug/L 42.7
500
500
511
508
94 93
70-130 1
Arsenic
ug/L NO
500
600
515
517
103 103
70-130 0
Beryllium
ug/L NO
500
500
450
448
90 90
70-130 0
Cadmium
ug/L NO
500
500
507
506
101 101
70-130 0
Results presented on this page are In the units Indicated by the "UmW column except whore an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Dale: 12/10/2019 05:51 PM without the wnnen consent of Pace Analytical Services, I.I.C.
Qual
Page 10 of 27

aceAnalytical
ww.pacelahe.cont
QUALITY CONTROL DATA
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER SD-02
Pace Project No.: 92455202
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2745908
2745909
MS
MSD
92454946001
Spike
Spike
MS
MSD
MS
MSD
% Rae
Parameter
Units
Result
Cone.
Cone.
Result
Result
%Rec
%Rec
Limits
RPD Oual
Chromium
ug/L
0.23
500
500
676
666
90
88
70-130
1
mglL
Copper
ug/L
0.14
500
500
669
666
106
106
70-130
0
mg/L
Lead
ug/L
0.0084
500
500
429
426
84
84
70-130
1
mg/L
Nickel
ug/L
0.68
500
500
1100
1090
85
82
70-130
1
mg/L
Selenium
ug/L
ND
500
500
260
255
52
51
70-130
2 M1
Silver
ug/L
0,023
250
250
304
304
112
112
70-130
0
mglL
Thallium
ug/L
ND
500
500
376
378
74
75
70-130
0
Zinc
ug/L
1.1
500
500
1560
1550
97
94
70-130
1
mglL
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2745910
2745911
MS
MSD
92455213001
Spike
Spike
MS
MSD
MS
MSD
% Rae
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Oual
Antimony
ug/L
0.0037J
500
500
488
497
97
99
70-130
2
mg/L
,Arsenic
ug/L
ND
500
500
496
508
99
101
70-130
2
'Beryllium
ug/L
ND
500
500
457
474
91
95
70-130
4
Cadmium
ug/L
ND
500
500
473
486
95
97
70-130
3
Chromium
ug/L
0.035
500
500
483
497
90
92
70-130
3
mg/L
Copper
ug/L
0,081
500
500
563
581
96
100
70-130
3
mg/L
Lead
ug/L
0.0025J
500
500
459
471
91
94
70-130
2
mg/L
Nickel
uglL
0.034
500
500
479
491
89
91
70-130
3
mg/L
Selenium
ug/L
ND
500
500
513
526
103
105
70-130
2
Silver
ug/L
ND
250
250
238
245
95
98
70-130
3
Thallium
ug/L
0.0037J
500
500
447
457
89
91
70-130
2
mglL
Zinc
ug/L
0.077
500
500
536
547
92
94
70-130
2
mg/L
Results presented on this page are in the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, -I-C.
Page 11 of 27

aceAnalytical
wwx.pecelabs.com
QUALITY CONTROL DATA
Project: STORMWATER SD-02
Pace Project No.: 92455202
, OC Batch: 513061 Analysis Method: EPA 624.1
QC Batch Method: EPA 624.1 Analysis Description: 624 MSV
Associated Lab Samples: 92455202001
METHOD BLANK: 2750399
Associated Lab Samples: 92455202001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Tdchloroethane
ug/L
NO
2.0
12/05/19 12:49
1,1,2,2-Tetrachloroethane
ug/L
NO
2.0
12/05/19 12:49
1,1,2-Tdchloroethane
ug/L
NO
2.0
12/05/19 12:49
�1,1-Dichloroethane
ug/L
NO
2.0
12/05/19 12:49
1,1-Dichloroelhene
uglL
NO
2.0
12/05/19 12:49
1,2-Dichlorobenzene
ug/L
NO
2.0
12/05/19 12:49
1,2-Dichloroethane
ug/L
NO
2.0
12/05/19 12:49
1,2-Dichloropropane
ug/L
NO
2.0
12/05/19 12:49
11,3-Dichlorobenzene
ug/L
NO
2.0
12/05/19 12:49
1,4-Dichlorobenzene
ug/L
NO
2.0
12/05/1912:49
,Benzene
ug/L
NO
1.0
1210511912:49
Bromodichloromelhane
ug/L
NO
2.0
12/05/19 12:49
i Bromoform
ug/L
NO
2.0
12/05/19 12:49
Bromomethane
ug/L
NO
2.0
12/05/191249
Carbon tetrachloride
ug/L
NO
2.0
12I05/19 1249
Chlorobenzene
ug/L
NO
2.0
12/05/191249
Chloroethane
ug/L
NO
2.0
12/05/19 12:49
Chloroform
ug/L
ND
2.0
12/05/19 12:49
Chloromethane
ug/L
NO
2.0
12/05/19 12:49
'cis-1,2-Dichloroelhene
ug/L
NO
2.0
12/05/19 1249
cis-1,3-Dichloropropene
ug/L
NO
2.0
12/05/19 1249
Dibromochloromethane
ug/L
NO
2.0
12/0511912:49
Ethylbenzene
ug/L
NO
1.0
12/05/191249
Methylene Chloride
ug/L
NO
2.0
12/05/19 1249
Tetrachloroethene
ug/L
NO
2.0
12/05/19 1249
Toluene
ug/L
NO
1.0
12/05/19 12:49
trans-1,2-Dichloroethene
ug/L
NO
2.0
12/05/191249
trans-1,3-Dichloropropene
ug/L
NO
2.0
12/05/19 1249
Trichloroethene
ug/L
NO
2.0
12/05/19 12:49
Tdchlorofluoromethane
ug/L
NO
2.0
12/05/19 12:49
Vinyl chloride
ug/L
NO
2.0
12/05/19 12:49
1,2-Dichloroethane-d4 (S)
e/
108
70-130
12/05/19 12:49
4-Bromolluorobenzene (S)
e/
108
70-130
12/05/19 12:49
Toluene -dB (S)
%
104
70-130
12/05/19 12:49
LABORATORY CONTROL SAMPLE: 2750400
Qualifiers
Pace Analytical Services, LLC
2225 Riverside or.
Asheville, NC 28804
[phone]
Spike LCS LCS % Rao
Parameter Units Conc. Result e/ Rao Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 23.0 115 70-130
1;1,2,2-Tetrachloroelhane ug/L 20 18.0 90 60-140
Results presented on this page are in the units Indicated by dot "Unlls' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the wMten consent of Pace Analytical Services, LLC.
Page 12 of 27

(�IaceAnalyfical'
www.pacalaha.com
QUALITY CONTROL DATA
Project: STORMWATER SD-02
Pace Project No.: 92455202
LABORATORY CONTROL SAMPLE:
Parameter
2750400
Units
Spike
Cone.
LCS
Result
LCS
e/ Rae
e/ Rec
Limits
1,1,2-Tdchloroethane
ug/L
20
22.2
111
70-130
1,1-Dichloroethane
ug/L
20
22.2
111
70-130
1,1-Dichloroethene
ug/L
20
22.5
113
50-150
1,2-Dichlorobenzene
ug/L
20
19.2
96
65-135
1,2-Dichloroethane
ug/L
20
21.9
110
49-155
1,2-Dichloropropane
ug/L
20
22.2
111
35-165
1,3-Dichlorobenzene
ug/L
20
18.8
94
70-130
'1,4-Dichlorobenzene
ug/L
20
19.2
96
65-135
,'Benzene
ug/L
20
21.1
106
65-135
Bromodichloromethane
ug/L
20
22.7
114
65-135
Bromoform
ug/L
20
20.0
100
70-130
Bromomelhane
ug/L
20
20.6
103
15-185
Carbon tetrachloride
ug/L
20
23.3
116
70-130
Chlorobenzene
ug/L
20
19.5
97
65-135
Chloroethane
ug/L
20
17.2
86
40-160
"Chloroform
ug/L
20
22.2
111
70-135
Chloromethane
ug/L
20
17.7
88
1-205
cis-1,2-Dichloroethene
ug/L
20
21.4
107
68-146
cis-1,3-Dichloropropene
ug/L
20
23.6
118
25-175
Dibromochloromethane
ug/L
20
20.1
101
70-135
�Ethylbenzene
ug/L
20
18.9
95
60-140
Methylene Chloride
ug/L
20
19.1
96
60-140
Tetrachloroethene
ug/L
20
18.8
94
70-130
Toluene
ug/L
20
21.0
105
70-130
trans-1,2-Dichloroethene
ug/L
20
22.6
113
70-130
trans-1,3-Dichloropropene
ug/L
20
23.4
117
50-150
Trichloroethene
ug/L
20
22.8
114
65-135
Tdchlomfluoromethane
ug/L
20
24.1
121
50-150
Vinyl chloride
ug/L
20
20.4
102
5-195
1,2-Dichloroethane-d4(S)
%
104
70-130
4-Bromofluorobenzene(S)
e/
102
70-130
Toluene-dB(S)
%
102
70-130
SPIKE 8 MATRIX SPIKE DUPLICATE: 2750401 2750402
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
MS MSD
92455195001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual
1, 1, 1 -Trichloroethane
ug/L
NO
20
20
21.5
17.8
107
89
52-162
19
1, 1,2,2-Tetrachloroethane
ug/L
NO
20
20
15.5
12.3
77
62
46-157
22
1,1,2-Trichloroethane
ug/L
NO
20
20
20.1
17.1
101
85
52-150
16
1,1-Dichloroethane
ug/L
NO
20
20
20.6
17.4
103
87
59-155
17
1,1-Dichloroethene
ug/L
NO
20
20
22.8
19.2
114
96
1-234
17
1,2-Dichlorobenzene
ug/L
NO
20
20
15.6
12.2
78
61
18-190
24
1,2-Dichloroethane
ug/L
NO
20
20
21.0
17.6
105
88
49-155
17
1,2-Dichloropropane
ug/L
NO
20
20
21.1
17.3
105
86
1-210
20
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 27

(�55?eAnalyticals`
atyw.pacalabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER SD-02
Pace Project No.: 92455202
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2750401
2750402
MS
MSD
92455195001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD Dual
1,3-Dichlorobenzene
ug/L
NO
20
20
15.3
12.3
77
61
59-156
22
1,4-Dichlorobenzene
ug/L
NO
20
20
15.3
11.9
76
59
18-190
25
Benzene
ug/L
NO
20
20
19.6
16A
98
82
37-151
18
Bromodichloromethane
ug/L
NO
20
20
20.9
18.4
104
92
35-155
13
Bromoform
uglL
NO
20
20
17.6
13.9
88
70
45-169
23
Bromomethane
ug/L
NO
20
20
12.5
12.7
62
63
1-242
1
Carbon tetrachloride
ug/L
NO
20
20
22.1
17.7
110
89
70-140
22
Chlorobenzene
ug/L
NO
20
20
16.6
13.4
83
67
37-160
21
Chloroethane
ug/L
NO
20
20
18.0
15.1
90
76
14-230
18
Chloroform
uglL
ND
20
20
22.2
17.8
111
89
51-138
22
Chloromethane
ug)L
ND
20
20
16.7
14.5
84
73
1-273
14
cis-1,2-Dichloroethene
ug/L
NO
20
20
20.5
17.5
102
87
45-174
16
cis-1,3-Dichloropropene
ug/L
NO
20
20
21.5
18.3
107
92
1-227
16
Dibromochloromethane
ug/L
NO
20
20
17.6
14.5
88
72
53-149
19
Ethylbenzene
ug/L
NO
20
20
16.1
12.8
81
64
37-162
23
'Methylene Chloride
ug/L
NO
20
20
18.9
15.8
95
79
1-221
18
Tetrachloroethene
ug/L
NO
20
20
16.2
12.0
81
60
64-148
30 Mt
Toluene
ug/L
NO
20
20
19.2
15.6
96
78
47-150
20
'trans-1,2-Dichloroethene
ug/L
NO
20
20
21.5
17.6
107
88
54-156
20
trans-1,3-Dichloropropene
ug/L
NO
20
20
20.6
17.3
103
87
17-183
17
Trichloroethene
ug/L
NO
20
20
21.1
17.0
105
85
70-157
21
iTdchlorofluoromethane
ug/L
ND
- 20
20
22.4
19.0
112
95
17-181
16
'Vinyl chloride
ug/L
NO
20
20
19.8
16.4
99
82
1-251
19
'.1,2-Dichloroethane-d4(S)
%
110
108
70-130
4-Bromofluorobenzene(S)
%
99
102
70-130
Toluene-d8 (S)
%
104
105
70-130
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12110/2019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 27

aceAnalytical
www.pacelebs.com
,QUALITY CONTROL DATA
Project: STORMWATER SD-02
Pace Project No.: 92455202
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
I QC Batch: 512063
Analysis
Method:
EPA608.3
QC Batch Method: EPA 608.3
Analysis
Description:
608 PCB Pest Red Vol
Associated Lab Samples: 92455202001
METHOD BLANK: 2746029
Matrix:
Water
Associated Lab Samples: 92455202001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
4,4'-DDD
uglL
NO
0.050
12/04/1918:59
4,4'-DDE
ug/L
NO
0.050
12/04/19 18:59
4,4'-DDT
ug/L
NO
0.050
12/04/19 18:59
Aldrin
ug/L
NO
0.050
12/04/19 18:59
' alpha-BHC
ug/L
NO
0.050
12/04/19 18:59
alpha -Chlordane
ug/L
NO
0.050
12/04/1918:59
beta-BHC
ug/L
NO
0.050
12104/1918:59
Chlordane (Technical)
ug/L
NO
0.50
12/04/19 18:59
delta-BHC
ug/L
NO
0.050
12/04/19 18:59
Dieldrin
ug/L
NO
0.050
12/04/19 18:59
'.'Endosulfan 1
ug/L
NO
0.050
12/04/19 18:59
Endosulfan II
ug/L
NO
0.050
12/04/19 18:59
i Endosulfan sulfate
ug/L
ND
0.050
12/04/19 18:59
Endrin
ug/L
NO
0.050
12/04/19 18:59
Endrin aldehyde
uglL
NO
0.050
12/04/19 18:59
,gamma-BHC (Lindane)
ug)L
NO
0.050
12/04/19 18:59
igamma-Chlordane
uglL
NO
0.050
12/04/19 18:59
!Heptachlor
ug/L
NO
0.050
12/0411918:59
(Heptachlor epoxide
ug/L
NO
0.050
12/04/191859
PCB-1016 (Arocor 1016)
uglL
NO
0.50
12/04/19 18:59
PCB-1 221 (Aroclor 1221)
uglL
NO
0.50
1210411918:59
PCB-1232 (Aroclor 1232)
ug/L
NO
0.50
12/04/19 18:59
PCB-1242 (Aroclor 1242)
ug/L
NO
0.50
12/04/19 18:59
PCB-1248 (Aroclor 1248)
ug/L
NO
0.50
12/04/19 18:59
PCB-1254 (Aroclor 1254)
ug/L
NO
0.50
12/04/19 18:59
PCB-1260 (Aroclor 1260)
ug/L
NO
0.50
12I04/19 18:59
Toxaphene
ug/L
NO
0.50
12104/1918:59
Decachlorobiphenyl (S)
%
126
10-130
12/04/19 18:59
Tetrachloro-m-xylene (S)
%
123
10-130
12/04/19 18:59
LABORATORY CONTROL SAMPLE: 2746030
Spike
LCS
LCS %Rec
Parameter
Units
Conc.
Result
% Rec Limits
Qualifiers
4,4'-DDD
ug/L
0.25
0.28
113
31-141
4,4'-DDE
ug/L
0.25
0.26
106
30-145
4,4'-DDT
ug/L
0.25
0.29
115
25-160
Aldrn
ug/L
0.25
0.24
96
42-140
alpha-BHC
ug/L
0.25
0.26
103
37-140
alpha -Chlordane
ug/L
0.25
0.28
112
45-140
beta-BHC
uglL
0.25
0.33
131
17-147
Rmu Its presented on this page are In the units indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/1012019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 27

laceAnalyticale
usher pacalahs.cem
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER SD-02
Pace Project No.: 92455202
LABORATORY CONTROL SAMPLE:
2746030
Spike
LCS
LCS
%Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
delta-BHC
ug/L
0.25
0.27
109
19-140
Dieldrin
ug/L
0.25
0.28
111
36-146
Endosulfan I
ug/L
0.25
0.27
110
45-153
Endosulfan II
ug/L
0.25
0.28
112
1-202
Endosulfan sulfate
ug/L
0.25
0.29
114
26-144
Endrin
ug/L
0.25
0.28
114
30-147
Endrin aldehyde
ug/L
0.25
0,21
83
50-150
gamma-BHC (Lindane)
ug/L
0.25
0.27
107
32-140
gamma -Chlordane
ug/L
0.25
0.20
79
45-140
_
'. Heptachlor
ug/L
0.25
0.25
100
34-140
Heptachlor epoxide
ug/L
0.25
0.28
110
37-142
Decachlorobiphenyl (S)
%
126
10-130
Tetrachloro-m-xylene (S)
%
115
10-130
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE:
2746031
2746032
MS
MSD
92455195001
Spike
Spike
MS
MSD
MS MSD
%Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec e/ Rec
Limits
RPD Qual
.4,4'-DDD
ug/L
NO
0.25
0.25
0.29
0.30
114
121
31-141
6
14,4'-DDE
ug/L
NO
0.25
0.25
0.27
0.28
108
113
30-145
5
4,4'-DDT
ug/L
NO
0.25
0.25
0.29
0.30
116
122
25-160
5
Aldrin
ug/L
NO
0.25
0.25
0.25
0.28
102
112
42-140
10
alpha-BHC
ug/L
NO
0.25
0.25
0.26
0.28
104
112
37-140
8
alpha -Chlordane
ug/L
NO
0.25
0.25
0.28
0.29
111
117
45-140
6
beta-BHC
ug/L
NO
0.25
0.25
0.31
0.34
123
134
17-147
9
delta-BHC
ug/L
NO
0.25
0.25
0.28
0.29
111
117
19-140
5
Dieldrin
ug/L
NO
0,25
0.25
0.27
0.29
109
115
36-146
6
Endosulfan I
uglL
NO
0.25
0.25
0.27
0.28
107
114
45-153
6
Endosulfan 11
uglL
NO
0.25
0.25
0.27
0.29
108
116
1-202
7
Endosulfan sulfate
ug/L
NO
0.25
0.25
0.28
0.30
113
120
26-144
6
Endrin
ug/L
NO
0.25
0.25
0.28
0.30
111
119
30-147
6
Endrin aldehyde
ug/L
NO
0.25
0.25
0.24
0.26
96
103
50-150
7
gamma-BHC (Lindane)
ug/L
NO
0.25
0.25
0.27
0.29
110
117
32-140
7
gamma -Chlordane
ug/L
NO
0.25
0.25
0.20
0.21
79
84
45-140
6
Heptachlor
ug/L
NO
0.25
0.25
0.27
0.29
107
116
34-140
8
Heptachlor epoxide
ug/L
NO
0.25
0.25
0.27
0.29
108
115
37-142
7
Decachlorobiphenyl (S)
%
125
132
10-130
SO
Tetrachloro-m-xylene(S)
a/
122
132
10-130
SO
Results presented on this page are in the units Indicated by the "Uults" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 27

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: STORMWATER SD-02
Pace Project No.: 92455202
QC Batch: 512091 Analysis Method: EPA 625A
1. QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Associated Lab Samples: 92455202001
METHOD BLANK: 2746155
Associated Lab Samples: 92455202001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
NO
5.0
12/02/19 15:43
2,2'-Oxybis(1-chloropropane)
ug/L
NO
5.0
12IO2/19 1543
2,4,6-Trichlorophenol
ug/L
NO
10.0
12/02/19 1543
2,4-Dichlorophenol
ug/L
NO
5.0
12/02/19 15:43
2,4-Dimethylphenol
ug/L
NO
10.0
12/02/19 15:43
2,4-Dinitrophenol
ug/L
NO
50.0
12/02/19 1543
2,4-Dinitrotoluene
ug/L
NO
5.0
12/02/19 15:43
2,6-Dinitrotoluene
ug/L
'ND
5.0
12/02/19 15:43
2-Chloronaphthalene
ug/L
ND
5.0
12/02/19 15:43
2-Chlorophenol
ug/L
ND
5.0
12102/1915:43
2-Nitrophenol
ug/L
NO
5.0
12/02/19 15:43
3,3'-Dichlorobenzidine
ug/L
NO
25.0
12/02/19 15:43
4,6-Dinitro-2-melhylphenol
ug/L
NO
20.0
12/02/19 15:43
4-Bromophenylphenyl ether
ug/L
ND
5.0
12/02/19 15:43
)4-Chloro-3-melhylphenol
Ug/L
NO
5.0
12/02/19 15:43
4-Chlorophenylphenyl ether
ug/L
ND
5.0
12/02/19 15:43
4-Nitrophenol
�Acenaphthene
ug/L
NO
50.0
12/02/19 15:43
ug/L
NO
5.0
12/02/1915:43
Acenaphthylene
ug/L
NO
5.0
1=2/1915:43
,Anthracene
ug/L
NO
5.0
12/02/19 15:43
:Benzo(a)anthracene
ug/L
NO
5.0
12/02/19 15:43
Benzo(a)pyrene
ug/L
NO
5.0
12/02/19 15:43
Benzo(b)Iluoranthene
ug/L
NO
5.0
12/02/1915:43
Benzo(g,h,i)perylene
ug/L
NO
5.0
12/02/19 15:43
Benzo(k)fiuoranthene
ug/L
ND
5.0
12/021191543
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
12/02/19 15:43
bis(2-Chloroethyl) ether
ug/L
ND
5.0
12/02/19 15:43
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
12/02/191543
Butylbenzylphthalate
ug/L
NO
5.0
12/02/19 15:43
Chrysene
ug/L
NO
5.0
12/02/19 15:43
Di-n-butylphthalate
ug/L
NO
5.0
12/02/19 15:43
Di-noctylphthalate
ug/L
NO
5.0
12/0211915:43
Dibenz(a,h)anthracene
ug1L
ND
5.0
12/02/19 15:43
Diethylphthalate
ug/L
ND
5.0
12/02/1915*43
Dimethylphthalate
ug/L
NO
5.0
12/02/19 15:43
Fluoranthene
ug/L
NO
5.0
12/02/19 15:43
Fluorene
ug/L
NO
5.0
12/02/19 15:43
Hexachloro-1,3-butadiene
ug/L
NO
5.0
12/02/19 15:43
Hexachlorobenzene
UgIL
ND
5.0
12/02/19 15:43
Hexachlorocyclopentadiene
UgIL
NO
10.0
12/02/19 15:43
Hexachloroethane
ug/L
ND
5.0
12/02/19 15:43
Qualifiers
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This repel shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services. L-C. Page 17 of 27

aceAnal ical"
MWw.paoefebe.com
Project: STORMWATER SD-02
Pace Project No.: 92455202
METHOD BLANK: 2746155
Associated Lab Samples: 92455202001
QUALITY CONTROL DATA
Matrix: Water
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Indeno(1,2,3-cd)pyrene
ug/L
NO
5.0
12/02/19 15:43
Isophorone
ug/L
NO
10.0
12/02/191543
N-Nitroso-di-n-propylamine
ug/L
NO
5.0
12/02/19 15:43
N-Nilrosodimethylamine
uglL
NO
5.0
12/02/19 15:43
N-Nitrosodiphenylamine
ug/L
NO
10.0
12/02/19 15:43
Naphthalene
ug/L
NO
5.0
12/02/19 15:43
Nitrobenzene
ug/L
NO
5.0
12/02/19 15:43
Pentachlorophenol
ug/L
NO
10.0
12/0211915:43
Phenanthrene
ug/L
ND
5.0
12/02/19 15:43
"Phenol
ug/L
ND
5D
12/02/191543
Pyrene
ug/L
NO
5.0
12/021191543
2,4,6-Tribromophenol(S)
%
67
10-137
12/02/19 15:43
2-Fluorobiphenyl (S)
%
75
15-120
12/02/19 15:43
2-Fluorophenol(S)
%
50
10-120
12/02/19 15:43
I Nitrobenzene-d5 (S)
%
82
10-120
12/02/19 15:43
Phenol-d6 (S)
%
35
10-120
12/02/19 15:43
Terphenyl-d14(S)
e/
72
11-131
12/02/1915:43
,LABORATORY CONTROL SAMPLE: 2746156
Spike
LCS
LCS
%Rec
Parameter
Units
Conc.
Result
e/ Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
uglL
50
41.2
82
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
49.1
98
36-166
2,4,6-Trichlorophenol
ug/L
50
42.9
86
37-144
2,4-Dichlorophenol
ug/L
50
44.2
88
39-135
2,4-Dimethylphenol
ug/L
50
46.6
93
32-120
2,4-Dinitrophenol
ug/L
250
254
102
1-191
2,4-Dinitrotoluene
ug/L
50
47.8
96
39-139
2,6-Dinitrotoluene
ug/L
50
49.8
100
50-158
2-Chloronaphthalene
ug/L
50
47.7
95
60-120
2-Chlorophenol
ug/L
50
43.8
88
23-134
27Nitrophenol
ug/L
50
48.3
97
29-181
3,3'-Dichlorobenzidine
ug/L
100
85.9
86
1-262
4;6-Dinitro-2-methylphenol
ug/L
100
106
106
1-181
4-Bromophenylphenyl ether
ug/L
50
42.2
84
53-127
4-Chloro-3-methylphenol
ug/L
100
98.8
99
22-147
4-Chlorophenylphenyl ether
uglL
50
43.4
87
25-158
4-Nitrophenol
ug/L
250
229
92
1-132
Acenaphthene
ug/L
50
45.0
90
47-145
Acenaphthylene
ug/L
50
47.6
95
33-145
Anthracene
ug/L
50
47.1
94
27-133
Benzo(a)anlhracene
ug/L
50
49.8
100
33-143
Benzo(a)pyrene
ug/L
50
50.4
101
17-163
Benzo(b)fiuoranthene
ug/L
50
53.0
106
24-159
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of rho result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the n"en consent of Pace Analytical Services, -I-C. Page 18 of 27

aceAnalytical
wyna.pacelabs.com
QUALITY CONTROL DATA
Project: STORMWATER SD-02
Pace Project No.: 92455202
LABORATORY CONTROL SAMPLE:
Parameter
2746156
Units
Spike
Conc.
LCS
Result
LCS
% Rec
%Rec
Limits
Benzo(g,h,i)perylene
ug/L
50
46.0
92
1-219
Benzo(k)Fluoranthene
ug/L
50
52.4
105
11-162
bis(2-Chloroethoxy)methane
ug/L
50
43.8
88
33-184
bis(2-Chloroethyl) ether
uglL
50
46.6
93
12-158
bis(2-Ethylhexypphthalate
ug/L
50
51.6
103
8-158
Butylbenzylphthalate
ug/L
50
51.5
103
1-152
Chrysene
ug/L
50
44.0
88
17-168
Di-n-butylphthalate
ug/L
50
47.2
94
1-120
Di-n-oclylphthalate
ug/L
50
54.9
110
4-146
Dibenz(a,h)anthracene
ug/L
50
48.0
96
1-227
I Diethylphthalate
ug/L
50
44.0
88
1-120
Dimethylphthalate
ug/L
50
42.8
86
1-120
Fluoranthene
ug/L
50
46.8
94
26-137
Fluorene
ug/L
50
47.0
94
59-121
Hexachloro-1,3-butadiene
ug/L
50
38.2
76
24-120
,Hexachlorobenzene
ug/L
50
41.7
83
1-152
Hexachlorocyclopentadiene
ug/L
50
32.6
65
25-150
Hexachloroethane
ug/L
50
43.2
86
40-120
Indeno(1,2,3-cd)pyrene
ug/L
50
46.8
94
1-171
Isophorone
ug/L
50
46.3
93
21-196
iN-Nitroso-di-n-propylamine
ug/L
50
50.6
101
1-230
:N-Nitrosodimethylamine
uglL
50
41.6
83
25-150
IN-Nitrosodiphenylamine
ug/L
50
44.1
88
25-150
(Naphthalene
ug/L
50
46.0
92
21-133
Nitrobenzene
ug/L
50
47.7
95
35-180
Pentachlorophenol
ug/L
100
83.7
84
14-176
Phenanthrene
ug/L
50
45.7
91
54-120
Phenol
ug/L
50
47.3
95
5-120
Pyrene
ug/L
50
47.7
95
52-120
2,4,6-T6bromophenol(S)
e/
93
10-137
2-Fluorobiphenyl(S)
%
84
15-120
2-Fluorophenol(S)
%
87
10-120
Nitrobenzene-d5 (S)
%
95
10-120
Phenol-d6 (S)
p/
95
10-120
Terphenyl-d14 (S)
e/
95
11-131
SPIKE 8 MATRIX SPIKE DUPLICATE: 2746157 2746158
Pace Analytical Services, LLL
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
MS MSD
92449985006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
1,2,4-Tdchlorobenzene
ug/L
NO
100
100
6T9
73.8
68
74
44-142
8
2,2'-Oxybis(1-chloropropane)
ug/L
NO
100
100
88.3
101
88
101
36-166
13
2,4,6-Trichlorophenol
ug/L
ND
100
100
40.6
73.4
41
73
37-144
58
2,4-Dichlorophenol
ug/L
ND
100
100
49.6
82.6
50
83
39-135
50
2,4-Dimethylphenol
ug/L
ND
100
100
84.3
95.6
84
96
32-120
13
Results presented on this page are In the units indicated by the -Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproducer, except in full,
Dale: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, -LC. Page 19 of 27

aceAnalytical
www.pacdahs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER
SD-02
Pace Project No.: 92455202
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE:
2746157
2746158
MS
MSD
92449985006
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter
Units
Result
Conc.
Cones
Result
Result
%Rec
%Rec
Limits RPD Oual
i
2,4-Dinitraphenol
ug/L
NO
500
500
73.6J
269
15
54
1-191
2,4-Dinitrotoluene
ug/L
NO
100
100
99.6
106
100
106
39-139
6
2,6-Dinitrotoluene
ug/L
NO
100
100
103
109
103
109
50-158
6
2-Chloronaphthalene
ug/L
ND
100
100
91.6
105
92
105
60-120
13
2-Chlorophenol
ug/L
NO
100
100
46A
79.3
46
79
23-134
52
2-Nitrophenol
ug/L
NO
100
100
47.1
86.5
47
86
20-182
59 Rt
3,3'-Dichlorobenzidine
ug/L
NO
200
200
167
177
84
89
1-262
6
4,6-Dinitro-2-methylphenol
ug/L
NO
200
200
72.5
137
36
69
1-181
62 R1
4-Bromophenylphenyl ether
ug/L
ND
100
100
81.6
86.9
82
87
53-127
6
4-Chloro-3-methylphenol
ug/L
NO
200
200
170
201
85
101
22-147
17
4-Chlorophenylphenyl ether
ug/L
NO
100
100
88.8
94.4
89
94
25-158
6
4-Nitrophenol
ug/L
NO
500
500
142
241
28
48
1-132
51
Acenaphthene
ug/L
NO
100
100
89.6
95.7
90
96
47-145
7
Acenaphthylene
uglL
NO
100
100
94.3
101
94
101
33-145
7
Anthracene
uglL
NO
100
100
93.2
96.9
93
97
27-133
4
I Senzo(a)anthracene
ug/L
NO
100
100
97.8
103
98
103
33-143
5
Benzo(a)pyrene
ug/L
NO
100
100
100
104
100
104
17-163
4
Benzo(b)fluoranthene
ug/L
NO
100
100
107
112
107
112
24-159
4
Benzo(g,h,i)perylene
ug/L
NO
100
100
91.5
90.9
91
91
1-219
1
Benzo(k)fluoranthene
ug/L
ND
100
100
105
111
105
111
11-162
5
bis(2-Chloroethoxy)methane
ug/L
NO
100
100
79.7
91.0
80
91
33-184
13
,bis(2-Chloroethyl) ether
ug/L
NO
100
100
82.0
93.0
82
93
12-158
13
bis(2-Ethylhexyl)phthalate
ug/L
NO
100
100
102
104
102
104
8-158
2
lButylbenzylphthalate
ug/L
NO
100
100
102
103
102
103
1-152
1
Chrysene
ug/L
ND
100
100
87.3
922
87
92
17-168
5
Di-n-butylphthalate
uglL
ND
100
100
94.4
99.0
94
99
1-120
5
Di-n-octylphthalate
uglL
NO
100
100
107
114
107
114
4-146
6
Dibenz(a,h)anthracene
ug/L
NO
100
100
95.6
97.9
96
98
1-227
2
Diethylphthalate
ug/L
NO
100
100
92.6
97.4
93
97
1-120
5
Dimethylphthalate
ug/L
NO
100
100
89.2
94.2
89
94
1-120
5
Fluoranthene
ug/L
NO
100
100
92.9
99.7
93
100
26-137
7
Fluorene
ug/L
ND
100
100
96.5
102
97
102
59-121
6
Hexachloro-1,3-butadiene
ug/L
ND
100
100
60.3
64.4
60
64
24-120
7
Hexachlorobenzene
ug/L
NO
100
100
80.1
85.1
80
85
1-152
6
Hexachlorocyclopentadiene
ug/L
NO
100
100
48.0
55.7
48
56
25-150
15
Hexachloroethane
ug/L
NO
100
100
68.6
72.4
69
72
40-120
5
Indeno(1,2,3-cd)pyrene
ug/L
NO
100
100
92.9
93.9
93
94
1-171
1
Isophorone
uglL
ND
100
100
84.9
97.0
85
97
21-196
13
N-Nitroso-di-n-propylamine
ug/L
NO
100
100
92.8
107
93
107
1-230
14
N-Nitrosodimethylamine
ug/L
NO
100
100
66.3
71.1
66
71
25-150
7
N-Nitrosodiphenylamine
ug/L
NO
100
100
87.5
91.3
88
91
25-150
4
Naphthalene
ug/L
NO
100
100
80.4
88.8
80
89
21-133
10
Nitrobenzene
ug/L
NO
100
100
86.9
99.8
87
100
35-180
14
Pentachlorophenol
ug/L
ND
200
200
61.0
111
31
56
14-176
58
Phenanthrene
ug/L
ND
100
100
90.0
95.4
90
95
54-120
6
Phenol
ug/L
NO
100
100
40.6
59.8
41
60
5-120
38
Results presented on this
page are In the units Indicated by Me'Units' column
except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the nHen consent of Pace Analytical Services, LLC. Page 20 of 27

aceAnalytical
www.pacolahs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER SD-02
Pace Project No.: 92455202
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2746157 2746158
MS MSD
92449985006 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone, Conc. Result Result % Rao p/ Rec Limits RPD Dual
Pyrene ug/L ND 100 100 93.6 95.7 94 96 52-120 2
2,4,6-Tdbromophenol (S) % 46 78 10-137
2-Fluorobiphenyl(S) % 82 88 15-120
2-Fluorophenol (S) % 33 59 10-120
Nitrobenzene-d5(S) % 88 97 10-120
Phenol-d6 (S) % 41 56 10-120
Terphenyl-d 14(S) % 82 69 11-131
Results oreaenled on thla page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 12/101201905:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the n"en consent of Pace Analytical Services, LLC.
Page 21 of 27

(12ceAnalytIcale
www.pacelaba.cpin
Project: STORMWATER SD-02
Pace Project No.: 92455202
QC Batch: 512118
QC Batch Method: SM 254OD-2011
Associated Lab Samples: 92455202001
METHOD BLANK: 2746362
Associated Lab Samples: 92455202001
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE: 2746363
li
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2746364
Parameter
Units
Total Suspended Solids
mg/L
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 254OD-2011
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 11/2711912:22
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 248 99 90-110
92455018001 Dup
Result Result
142 152
RPD Qualifiers
7
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit la presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 27

(�IaceAnalytlllcale
www.pacelaEs.cpm
QUALITY CONTROL DATA
Project: STORMWATER SD-02
Pace Project No.: 92455202
OC Balch: 512392 Analysis Method: EPA 420.4 Rev 1.0 1993
OC Batch Method: EPA 420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics
Associated Lab Samples: 92455202001
METHOD BLANK: 2747669 Matrix: Water
Associated Lab Samples: 92455202001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phenol mg/L NO 0,020 12/03/1912:44
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
2747670
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Phenol
mg/L
0.05
0.049
97
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2747671
2747672
MS
MSD
92455086001
Spike
Spike MS
MSD
MS MSD
%Rec
Parameter
Units Result
Conc.
Conc. Result
Result
%Rec e/ Rec
Limits RPD Dust
(Phenol
mg/L NO
0.05
0.05 0.048
0.046
95 92
90-110 3
'MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2747673
2747674
MS
MSD
it 92455086002 Spike
Spike
MS
MSD MS MSD %Rec
I' Parameter Units Result Conc.
Cones
Result
Result %Rec %Rec Limits RPD Qual
Phenol mg/L ND 0.05
0.05
0,046
0,043 92 86 90-110 7 M1
Results presented on this page are in the units indicated by the'Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproducer, except in full,
Date: 12/10/2019 05:51 PM withaut the vnden consent of Pace Analytical Services, LLC.
Page 23 of 27

Pace Analytical Services, LLC
® 2225 Riverside Dr.
it aceAnalytical Asheville, NC 28804
www.Dacelabaxom [phone]
QUALIFIERS
I, Project: STORMWATER SD-02
I, Pace Project No.: 92455202
, DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
POL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyle is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D)- Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
II Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analyles.
TNI - The NELAC Institute. -
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 27

m
aceAnalytical
www.pacelabs.com
i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828(254-7176
Project:
Pace Project No.:
STORMWATER SD-02
92455202
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92455202001
SD2
EPA 1664B
513867
92455202001
SD2
EPA 608.3
512063
EPA 608.3
512391
92455202001
SD2
EPA 200.7 Rev 4.4 1994
511985
EPA 200.7 Rev 4.4 1994
511999
92455202001
SD2
EPA 245.1 Rev 3.01994
512899
EPA 245.1 Rev 3.01994
512943
92455202001
SD2
EPA625.1
512091
EPA 625.1
512416
92455202001
SD2
EPA 624.1
513061
92455202001
SD2
SM 254OD-2011
512118
92455202001
SD2
EPA 420.4 Rev 1.0 1993
512392
EPA 420.4 Rev 1.0 1993
512538
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 27

'Nr7111"r��r T•ii TT1
; J4 00zUz be, or N
CHAIN -OF -CUSTODY Analytical Request Document
LAB USE CWv*
Pace Analytical `
'
�
IIIII� III II IIIIII I I III
Chain -of -Custody is a LEGAL DOCUMENT � Complete all rclevent fields
m
92455202 as
a
Company:l/^' ` `1 ��1
U,
billing Information:
4 I
Coreserretive Type 11ab Project Manager:
ntainer P_
ty l
Address_ J i r
Aiv t�1t.�1 14� (Ylti'�11V�t
1 lug
Repo�To:
' It awl �1 t'L II,iA^'✓1
Email To: lj/�, y\ 1 r �/�
f-4'IGL/l�r 1lltT
" Preservative Types nitric acid, Rlsulfuric
himin(3)hvd)he.aric aci tisecs sd Iid.(Rl mtle.niu eu.1aetate,
(s)memonsunihyodiumbisuume.(U)sodiumt,,?d,t)O(9lne.ane(A)ascom�a acfd.lalammonium sulfate.
(q ammonium M1ytlroxitle. (0)TSP, (U)Unpreservrd, (0)Omer
Analyses Lab Profile/Line:
Copy To:
{�.^j• l•'��1 i1,j
Sit. Co cction Info/Addrrss: a 'a fs1
Icie-IN Ncv rtbiii ILJ t 11� (, hY,' 1`G AV, ri�
Customer NAaLLmu�ej/Numbb/er.
State: County/Gly: Time Zone Collected:
ET
Lab Sample Receipt Checklist:
MProject
/�V11lIVti�1 Ti,1� '^7D~I� ( /
ti
t�G 21;1t:41irG�L I IPTI IMTI IR L/)
.\
L _
L/
'�-Y'
Custody Seals Present/intact Y N NA
Custody r signuree Pioneer v NA
Collector Signatui¢ PiesCn[ Y N NA
T` �- -06
PhOnC:[(�j'yQ (5115 r
Site/Facility ID IL
Compliance Monitoring?
Email' L1)GY (. 6a'AA'Ua.1 .Qtii'1
I I Yes ( I No
�_
potcles Inmct Y N VA
Correct Bottles 1 N NA
sufficientaeRe Volume yY N NA
Samples Received On 1¢¢ + N
�^N
Collected By (print): z
U
Purchase Order 4:
Quote 4:
DW PWS ID 4:
DW Location Code:
1�i.iY 111 .I1X LUY
Collectetl By (sig azure):
Turnaround Date Required:
Immediate y Packed o 1Ice:
_i
`
_
NA
USA - Readepace ell.Accqblc NA
USDA Aegul at¢d Soite ^^Y r�'HA
IIA
�j I 1j
f%/��.�I
Yes NO
I I I )
C�-�
d•
_
Sam les in Holdin Tine "' N
Nenldu:al Chloelne9P11-ent Y N 1
Cl Strips:
Sample Disposal:
Rush:
Field Filtered (il applicable):
I I Dispmeasappropriate I I Retum
I I Archie¢
( ]Same Day I I Next Day
( 12 Day [ ) 3 Day I ]4Day I 1 5 Day
I I Yes I I No
�^
Sample pH Acceptable t Y N NA
pH strips: S
1 IHold:
(Expetl4e Chages Apply)
Analysis:
f-�,
c
_y
V
'J
•�
Sulfide Present Y N '1A
Lead Acetate Strips:
wastewater WW),
' Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), [
C
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue ITS), Bioassay (B), Vapor IV), Other (OT)
�.(l
`,�
LAB USE LUSE ONLY:
Res It of
Lab Sample k / Comments:
Comp / Collected (or
Composite End
Customer Sample ID Matrix' Grab Composite Start) Cl Cons
�,
L•
i
1-:—
I
Date Time Date Time
il`V'1
(s
d•)31LI
I)NZZ
X
t,li7_
i.Ni
ie
ii•7;'Irl
(t�i
1
X
-
�17�,
;hir
r-
ri;7aik
lai2
�
y
��r
W
16
'1m
%,
T
c)
i/i/ l
C-�
i I L3-Iri
I i.N
r D L
W-1
Cx
Customer Remarks/Special Conditions/Possible Hazards:
Type of Ice Used:
YP
Wet1 Blue Dry None
SHORT HOLDS PRESENT (<]2 hoursW/Ab
Sample Temperature Info: ,l
Temp Blank Received: Y �NA
Packing Material Used: (t
-Z. �Y�
Lab Tracking 4:Therm
2410504
IDN: Cl `�j 1�. i
nR--- —
Cooler ITemp Upon Receipt: (. i%oC
Cooler 1 Therm Corr. Factor: J) oC
Samples received via:
Radchenl samples) screened (<500 cpm): Y N NA
FEDE% UPS Client Courier Pace Courier
Cooler I Corrected Temp: /. V PC
^
Comments: r
R
-nquishetl tY/C' mp (Sigwtur
.l1
1.
te/Time:
�'e/Tmae
y y (Si ma re)
Received b Com an 6
V �7�
Date/Time: /C `L,
I I .. IQ
1
MTIt LAB USE ONLY
Table il;
Atttnum:Reli
ulshed by/ ompany: (Signature)
Rect4ved by/Company: (Sigdature)
)
Date/Time:
Template:
rip Blank Received: 1�' Qf f NA
HCL MCOH TSP 'Other
(/
Prelogm:
Relinquished by/Company: (Signature)
Oate/Time:
Received by/Company: (Signature)
Date/Timec
pM:_ _ _ .. _. - _ _ r
.. _. - _ -_
_:Non Con(or !lT(s): Pager
YES�NO/ of:
on

♦
Document Plame:
Poament Revised: Februar( 7, 2018
v
Sample Condition Upon Recelpt(SCUR)
page 1 of 2
Document No :
155Ia18 AUu,oritY
aceAnal}Rical
!
F-CAR-CS-033-Rev.06
Pace Catolinas Quality Office
`Check mark top half of box if pH and/lir dechlorination is ~
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (dater) DOC, LLHg
"Bottom half of box is to list number of bottle
Project I lob} ; g2455202
PM: CDl Due Date: 12/12/19
CLIENT: 93-Mo09Comv
O
V
O
N
ry
L
V
¢
J
J
J
n
p
z
V
_
—U'
v
y
f
r
j
_
E
o
rr
z
c
O
d
;i > n z M J
1 a v- m
3
a
E
i
E
a
E
a
E
E
E
E
S
E
a
E
N
E
E
<
E
E
a
¢
E
ry
4
E
O0,
E
E
a
O
E
o
7 E of 0 o n o
J
J
J
J
~
2
N
z\
I
I I
0\
NN\\1
3
I\
!
I
\\\
s
I
FF-
9
\
I\I
\\
i\N\\10
12
\N
\
\
\\N
pH Adjustment
Log for Preserved Samples
Sample I
Type of Preservative
pH upon receipt
Date preservation adjusted
Time pmervation
adlisled
I Amount of Preservative Lot
added
WIIeeClerthere IS adlSCrenancVattoctmgPlOrthCarolina compliance samples, a copy m oua ionu rp a suin—%Ii�.�.,......-....___... _. __....
Out of hold, incorrect preservative, not of temp, Incorrect containers.
Page 27 of 27

laceAnalyfical
tom.pacelabs.com
December 10, 2019
Danielle Loyd
Moog Components
1995 NC Hwy 141
Murphy, NC 28906
RE: Project: STORMWATER-SD-03
Pace Project No.: 92455195
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Dear Danielle Loyd:
Enclosed are the analytical results for sample(s) received by the laboratory on November 26, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
A-
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
Q PCCREO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, -LC.
Page 1 of 27

aceAnalytical
www.Dacelabs.wm
Project: STORMWATER-SD-03
". Pace Project No.: 92455195
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
FlondWNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 27

Pace Analytical Services, LLC
;I m 2225 Riverside Dr.
aceAnalytical Asheville. NC 28804
W"'Paodaluxom
[phone]
it
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
STORMWATER-SD-03
92455195
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92455195001
SD3
EPA 1664E
HH
1
PASI-C
EPA 608.3
SEM
29
PASI-C
EPA 200.7 Rev 4.41994
SH7
12
PASI-A
EPA 245.1 Rev 3.0 1994
SOO
1
PASI-A
EPA 625.1
Bpi
58
PASI-C
EPA624.1
DLK
34
PASI-C
SM 2540D-2011
CJL
1
PASI-A
EPA 420.4 Rev 1.0 1993
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 27

aceAnalytical
www.pacelaha.cam
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER-SD-03
1 Pace Project No.: 92455195
Sample: SD3 Lab ID: 92455195001 Collected: 11/23/1912:20 Received: 11/2611910:20 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual
1664 SGT-HEM, TPH Analytical Method: EPA 1664E
Total,P-etroleum"Hydrocarbons ND mg/L 4.8 1 12/10/1910:25
608 PCB Pest RVE Analytical Method: EPA 608.3 Preparation Method: EPA 608.3
Aldrin
alpha-BHC
beta-BHC
delta-BHC
i gamma-BHC (Lindane)
Chlordane (Technical)
alpha -Chlordane
,gamma -Chlordane
4,4'-DDD
14,4'-DDE
4.4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epoxide
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl(S)
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 17:46
309-00-2
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 1746
319-84-6
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 17:46
319-85-7
NO
ug/L
0,050
1
11/27/19 09:44
12/04/19 17:46
319-86-8
NO
ug/L
0,050
1
11/27/19 09:44
12/04/19 17:46
58-89-9
NO
ug/L
0.50
1
11/27/19 09:44
12/04/19 17:46
57-74-9
NO
ug/L
0.050
1
11127/19 09:44
12/04/19 17:46
5103-71-9
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 17:46
5103-74-2
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 17:46
72-54-8
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 17:46
72-55-9
ND
ug/L
0.050
1
11/27/19 09:44
12/04/19 17:46
50-29-3
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 17:46
60-57-1
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 17:46
959-98-8
NO
ug/L
0.050
1
11/27/1909:44
12/04/19 17:46
33213-65-9
NO
ug/L
0.060
1
11/2711909:44
12/04/19 17:46
1031-07-8
NO
ug/L
0.050
1
11/2711909:44
12104/1917:46
72-20-8
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 17:46
7421-93-4
NO
ug/L
0.050
1
11/27/19 09:44
12/04/19 17:46
76-44-8
NO
ug/L
0.050
1
11/27/1909:44
12/04/19 17:46
1024-57-3
NO
ug/L
0.50
1
11/27/19 09:44
12/04/19 17:46
12674-11-2
NO
ug/L
0.50
1
11/27/19 09:44
12/04/19 17:46
11104-28-2
NO
ug/L
0.50
1
11127/19 09:44
12/04/19 17:46
11141-16-5
ND
ug/L
0.50
1
11/27/19 09:44
12/04/1917*46
53469-21-9
NO
ug/L
0.50
1
11/27/1909:44
12/04/19 17:46
12672-29-6
NO
ug/L
0.50
1
11/27/19 09:44
12/04/19 17:46
11097-69-1
NO
ug/L
0.50
1
11/27/19 09:44
12/04/19 17:46
11096-82-5
NO
ug/L
0.50
1
11/2711909:44
12/04/19 17:46
8001-35-2
138
%
10-130
1
11/27/19 09:44
12/04/19 17:46
877-09-8 S3
144
%
10-130
1
11/27/19 09:44
12/04/19 17:46
2051-24-3 S3
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Antimony
NO
ug/L
5.0
1
11/27/19 01:21
12/03/19 01:16
7440-36-0
Arsenic
NO
ug/L
10.0
1
11/27/1901:21
12/0311901:16
7440-38-2
Beryllium
NO
ug/L
1.0
1
11/27/19 01:21
12/03/19 01:16
7440-41-7
Cadmium
NO
ug/L
1.0
1
11/27/19 01:21
12/03/19 01:16
7440-43-9
Chromium
NO
ugIL
5.0
1
11/27/19 01:21
12/03/19 01:16
744047-3
6.3—ugIL-
5.0
1
11/27/19 01:21
12/03/19 01:16
7440-50-8
Lead
ND—ug/L
5.0
1
11/27/19 01:21
12/0311901:16
7439-92-1
Nickel
NO
ug/L
5.0
1
11/27/19 01:21
12/03/19 01:16
7440-02-0
Selenium
NO
ug/L
10.0
1
11/27/19 01:21
12/03/19 01:16
7782-49-2
Silver
ND
ug/L
5.0
1
11/27/19 01:21
12/03/19 01:16
7440-22-4
Thallium
NO
ugIL
10.0
1
11/27/19 01:21
12/03/19 01:16
7440-28-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 27

(�IaceAnalyficale
www.pacelaba.com
ANALYTICAL RESULTS
Project: STORMWATER-SD-03
Pace Project No.: 92455195
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: SD3 Lab ID: 92455195001 Collected: 11/23/1912:20 Received: 11/26/1910:20 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual
„ 200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Q Zinc
13.7-ug/L�D
10.0
1
11/27/19 01:21
12/03/19 01:16
7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1
Rev 3.0 1994 Preparation
Method: EPA 245.1
Rev 3.0 1994
�IMercury
NO
ug/L
0.20
1
12/04/191744
12/05/1914:02
7439-97-6
625 MSSV
Analytical Method: EPA 625.1
Preparation Method: EPA 625.1
Acenaphthene
NO
ug/L
5.0
1
11/27/19 14:36
12/0311919:12
83-32-9
Acenaphthylene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
208-96-8
'Anthracene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
120-12-7
Benzo(a)anthracene
NO
ug/L
5.0
1
11/27/19 1436
12/03/19 19:12
56-55-3
Benzo(a)pyrene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
50-32-8
�Benzo(b)Buoranthene
NO
ug/L
5.0
1
11/27/1914:36
12/03/191912
205-99-2
IBenzo(g,h,i)perylene
NO
ug/L
5.0
1
11/27/19 1436
12/03/19 19:12
191-24-2
Benzo(k)fluoranthene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
207-08-9
'4-Bromophenylphenyl ether
NO
uglL
5.0
1
11/27/19 14:36
12/0311919:12
101-55-3
Butylbenzylphthalate
NO
ug/L
5.0
1
11/2711914:36
12/0311919:12
85-68-7
'4-Chloro-3-methylphenol
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
59-50-7
bis(2-Chloroethoxy)methane
NO
ug/L
10.0
1
11/27/19 1436
12/03/19 19:12
111-91-1
bis(2-Chloroethyl) ether
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
111-44-4
2-Chloronaphthalene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
91-58-7
2-Chlorophenol
NO
ug/L
5.0
1
11127/191436
12/0311919: 12
95-57-8
4-Chlorophenylphenyl ether
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
7005-72-3
Chrysene
NO
ug/L
5.0
1
11127/1914:36
12/03/19 19:12
218-01-9
Dibenz(a.h)anlhracene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
53-70-3
3,3'-Dichlorobenzidine
NO
ug/L
25.0
1
11/27/19 14:36
12/03/19 19:12
91-94-1
2,4-Dichlorophenol
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
120-83-2
Diethylphthalate
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
84-66-2
2,4-Dimethylphenol
NO
ug/L
10.0
1
11/27/19 14:36
12/03/19 19:12
105-67-9
Dimethylphthalate
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
131-11-3
Di-n-bulylphthalate
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
84-74-2
4,6-Dinitro-2-methylphenol
NO
ug/L
20.0
1
11/27/19 14:36
12I03/19 19:12
534-52-1
2,4-Dinilrophenol
NO
ug/L
50.0
1
11/27/19 14:36
12/03/19 19:12
51-28-5
2,4-Dinitrololuene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 1912
121-14-2
2,6-Dinitrololuene
NO
ug/L
5.0
1
11127/1914:36
12103/1919:12
606-20-2
Di-n-octylphthalate
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
117-84-0
bis(2-Ethylhexyl)phthalate
NO
ug/L
5.0
1
11/27/19 1436
12/03/19 19:12
117-81-7
Fluoranthene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
206-44-0
Fluorene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 1912
86-73-7
Hexachloro-1,3-butadiene
NO
ug/L
5.0
1
11/27/19 1436
12/03/19 1912
87-68-3
Hexachlorobenzene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
118-74-1
Hexachlorocyclopentadiene
NO
uglL
10.0
1
11/27/191436
1210311919: 12
77-47-4
Hexachloroethane
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
67-72-1
Indeno(1,2,3-cd)pyrene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
193-39-5
Isophorone
NO
ug/L
10.0
1
11127/1914:36
12/03/19 19:12
78-59-1
Naphthalene
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 19:12
91-20-3
Nitrobenzene
NO
ug/L
5.0
1
11/27/1914:36
12/03/1919: 12
98-95-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the wneen consent of Pace Analytical Services, L-C.
Page 5 of 27

m
aceAnalytical
www.pacatabs.cum
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER-SD-03
Pace Project No.: 92455195
Sample: SD3
Lab ID: 92455195001 Collected: 11/23/19 12:20
Received: 11/26/19 10:20 Matrix: Water
Parameters
Results
Units
Report Limit
OF
Prepared
Analyzed
CAS No. Oual
625 MSSV
Analytical Method: EPA 625.1
Preparation Method:
EPA 625.1
2-Nitrophenol
NO
ug/L
5.0
1
11/27/1914:36
12/03/19 19:12
88-75-5
4-Nitrophenol
NO
ug/L
50.0
1
11/27/19 14:36
12/031191912
100-02-7
N-Nitrosodimethylamine
NO
ug/L
5.0
1
11/27/19 14:36
12/03119 19:12
62-75-9
N-Nitroso-di-n-propylamine
NO
ug/L
5.0
1
11/27/19 14:36
12/03/19 1912
621-64-7
N-Nilrosodiphenylamine
NO
ug/L
10.0
1
11/27/19 14:36
12/03/19 19:12
86-30-6
2,2'-Oxybis(1-chloropropane)
NO
uglL
5.0
1
11/27/19 14:36
12/03/19 19:12
108-60-1
Pentachlorophenol
NO
ug/L
10.0
1
11/27/19 14:36
12/03/19 19:12
87-86-5
Phenanthrene
NO
ug/L
5.0
1
11/27/19 14:36
12/0311919:12
85-01-8
IPhenol
NO
ug/L
5.0
1
11127/191436
12/03/1919:12
108-95-2
Pyrene
NO
ug/L
5.0
1
11/27/19 1436
12/03/19 19:12
129-00-0
I1,2,4-Tdchlorobenzene
NO
ug/L
5.0
1
11/27/1914:36
1210311919: 12
120-82-1
2,4,6-Tdchlorophenol
NO
ug/L
10.0
1
11127/19 14:36
12/03/19 19:12
88-06-2
'Surrogates
Nitrobenzene-d5 (S)
65
%
10-120
1
11/27/19 14:36
12/03/19 1912
4165-60-0
2-Fluorobiphenyl (S)
70
%
15-120
1
11/27/19 14:36
12/03/19 1912
321-60-8
Terphenyl-d 14(S)
85
%
11-131
1
11/27/19 14:36
12/03/19 19:12
1718-51-0
Phenol-d6 (S)
22
%
10-120
1
11/27/19 14:36
12/03/19 19:12
13127-88-3
2-Fluorophenol (S)
22
%
10-120
1
11/27/19 14:36
12/03/19 19:12
367-12-4
2,4,6-Tribromophenol (S)
63
%
10-137
1
11/27/19 14:36
12/03/19 19:12
118-79-6
C624 Volatile.Organics
Analytical Method:
EPA 624.1
Benzene
NO
ug/L
1.0
1
12/0511915:00
71-43-2
Bromodichloromethane
NO
ug/L
2.0
1
12105/1915:00
75-27-4
Bromoform
NO
ug/L
2.0
1
12/05/19 15:00
75-25-2
Bromomethane
NO
ug/L
2.0
1
12/05/1915:00
74-83-9
Carbon tetrachloride
NO
ug/L
2.0
1
12/05/19 15:00
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
12/05/191500
108-90-7
Chloroethane
ND
ug/L
2.0
1
12/05/19 15:00
75-00-3
Chloroform
NO
ug/L
2.0
1
12/05/19 15:00
67-66-3
Chloromethane
NO
ug/L
2.0
1
12/05/19 15:00
74-87-3
Dibromochloromethane
NO
ug/L
2.0
1
12/05/19 15:00
124-48-1
1,2-Dichlorobenzene
NO
ug/L
2.0
1
12/05/19 15:00
95-50-1
1,3-Dichlorobenzene
NO
ug/L
2.0
1
12/05/19 15:00
541-73-1
1 ,4-Dichlorobenzene
NO
ug/L
2.0
1
12/05/19 1500
106-46-7
1,1-Dichloroethane
NO
ug/L
2.0
1
12/05/19 15:00
75-34-3
1,2-Dichloroethane
NO
ug/L
2.0
1
12/05/19 15:00
107-06-2
1,1-Dichloroethene
NO
ug/L
2.0
1
12/05/19 15:00
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
1
12/05/19 15:00
156-59-2
trans-1,2-Dichloroethene
NO
ug/L
2.0
1
12/05/19 15:00
156-60-5
1 �2-Dichloropropane
NO
ug/L
2.0
1
12/05/19 15:00
78-87-5
cis-1,3-Dichloropropene
NO
ug/L
2.0
1
12/05/19 15:00
10061-01-5
trans-1,3-Dichloropropene
NO
ug/L
2.0
1
12/05/19 15:00
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/05/19 15:00
100-41-4
Methylene Chloride
NO
ug/L
2.0
1
12/05/19 15:00
75-09-2
6,2,2-Tetrachloroethane
NO
ug/L
2.0
1
12/05/19 15:00
79-34-5
Telrachloroelhene
NO
ug/L
2.0
1
12/05/19 15:00
127-18-4 Ml
To
l
NO
ug/L
1.0
1
12/05/19 15:00
108-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 27

aceAnalytical
www.pacelabscom
I_Pr1W1111I101aA0*1111111k
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER-SD-03
Pace Project No.: 92455195
Sample: S03 Lab ID: 92455195001 Collected: 11/23/1912:20 Received: 11/26/19 10:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Opal
624 Volatile Organics Analytical Method: EPA 624.1
1,1.1-Trichloroethane
ND
ug/L
2.0
1
12/05/19 15:00
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1
12/05/19 15:00
79-00-5
Trchloroethene
ND
ug/L
2.0
1
12/05/19 15:00
79-01-6
Trichlorofluoromelhane
NO
ug/L
2.0
1
12/05/19 15:00
75-69-4
Vinyl chloride
ND
ug/L
2.0
1
12/05/19 15:00
75-01-4
Surrogates
'4-Bromofluorobenzene(S)
105
%
70-130
1
12/05/19 15:00
460-00-4
Toluene-d8(S)
106
%
70-130
1
12/05/19 15:00
2037-26-5
„1,2-Dichloroethane-d4(S)
107
%
70-130
1
12/05/19 15:00
17060-07-0
2540D Total Suspended Solids Analytical Method: SM 2540D-2011
':Total Suspended Solids 10:2 mg/L 2.5 1 11/26/1917:30
420.4 Phenolics, Total Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Phenol ND mg/L 0.020 1 12/03/19 09:35 12/03/19 12:59 108-95-2
REPORT OF LABORATORY ANALYSIS
This report Shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, L-C.
Page 7 of 27

aceAnalytical
www.penlabs.cort
Project: STORMWATER-SD-03
Pace Project No.: 92455195
QC Batch: 513867
QC Batch Method: EPA 1664E
Associated Lab Samples: 92455195001
LABORATORY CONTROL SAMPLE: 2754405
Parameter Units
Total Petroleum Hydrocarbons mg/L
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 SGT-HEM, TPH
Spike LCS LCS % Rec
Cones Result %Rec Limits Qualifiers
20 15.6 78 64-132
I, MATRIX SPIKE SAMPLE:
2754406
92455125001 Spike
MS MS %Rec
Ii Parameter
Units
Result Conc.
Result %Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
NO 19.2
5.4 22 64-132 M1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of fine result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full,
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 27

aceAnalytical
www.pacelebs.cem
I Project: STORMWATER-SD-03
Pace Project No.: 92455195
QC Batch: 512899
QC Batch Method: EPA 245.1 Rev 3.0 1994
Associated Lab Samples: 92455195001
METHOD BLANK: 2749676
Associated Lab Samples: 92455195001
Parameter Units
(Mercury ug/L
LABORATORY CONTROL SAMPLE: 2749677
Parameter Units
Mercury ug/L
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 245.1 Rev 3.0 1994
Analysis Description: 245.1 Mercury
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 0.20 12/05/1912:50
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
2.5 2.6 104 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2749678
2749679
MS
MSD
92455457003 Spike
Spike
MS
MSD
MS MSD %Rec
Parameter Units Result Conc.
'Mercury
Conc.
Result
Result
%Rec %Rec Limits RPD Qua[
ug/L 55.9 2.5
2.5
56.7
58.0
34 84 70-130 2 M6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2749680
2749681
MS
MSD
92455457005 Spike
Spike
MS
MSD MS MSD e/ Rec
Parameter Units Result Conc.
Conc.
Result
Result % Rec % Rec Limits RPD Qual
Mercury ug/L NO 2.5
2.5
2.7
2.5 103 99 70-130 4
i
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 27

m
ace Analytical
www.pacelaba.corn
QUALITY CONTROL DATA
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville. NC 28804
[phone]
Project: STORMWATER-SD-03
Pace Project No.: 92455195
QC Batch: 511985
Analysis Method:
EPA 200.7 Rev 4.4
1994
QC Balch Method: EPA 200.7 Rev 4.4 1994
Analysis Description:
200.7 MET
Associated Lab Samples: 92455195001
'.' METHOD BLANK: 2745906
Matrix: Water
Associated Lab Samples: 92455195001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
, Antimony
ug/L
NO
5.0
12/03/19 00:31
Arsenic
ug/L
NO
10.0
12/03/19 00:31
�i Beryllium
ug/L
NO
1.0
12/03/19 00:31
Cadmium
ug/L
ND
1.0
12/03/19 00:31
Chromium
ug/L
NO
5D
12/03/19 00:31
'r Copper
ug/L
NO
5.0
12/03/19 00:31
Lead
ug/L
NO
5.0
12/03/19 00:31
.Nickel
ug/L
NO
5.0
12/03/19 00:31
Selenium
uglL
NO
10.0
12103/19 00:31
Silver
ug/L
NO
5.0
12/03/19 00:31
Thallium
ug/L
NO
10.0
12/03/19 00:31
Zinc
ug/L
NO
10.0
12/03/19 00:31
LABORATORY CONTROL SAMPLE: 2745907
Spike
LCS
LCS % Rec
Parameter
Units
Cone.
Result
%Rec Limits
Qualifiers
Antimony
uglL
500
479
96
85-115
'Arsenic
ug/L
500
481
96
85-115
Beryllium
ug/L
500
470
94
85-115
Cadmium
ug/L
500
464
93
85-115
Chromium
ug/L
500
457
91
85-115
,Copper
ug/L
500
466
93
85-115
Lead
ug/L
500
467
93
85-115
,Nickel
ug/L
500
459
92
85-115
Selenium
ug/L
500
468
94
85-115
'Silver
ug/L
250
234
94
85-115
Thallium
ug/L
500
458
92
85-115
Zinc
ug/L
500
466
93
85-115
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE:
2745908
2745909
MS
MSD
92454946001
Spike
Spike
MS
MSD MS MSD
% Rae
Parameter Units
Result
Conic.
Conc.
Result
Result %Rec %Rec
Limits RPD Qual
Antimony ug/L
42.7
500
500
511
508
94 93
70-130 1
Arsenic ug/L
NO
500
500
515
517
103 103
70-130 0
Beryllium ug/L
NO
500
500
450
448
90 90
70-130 0
Cadmium ug/L
ND
500
500
507
506
101 101
70-130 0
Results presented on MIs page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 27

lace Analytical
wtars.pacelabs.corn
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER-SD-03
Pace Project No.: 92455195
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2745908
2745909
MS
MSD
92454946001
Spike
Spike
MS
MSD
MS
MSD
e/ Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD Qual
Chromium
ug/L
0.23
500
500
676
666
90
88
70-130
1
mg/L
,Copper
ug/L
0.14
500
500
669
666
106
106
70-130
0
mg/L
Lead
ug/L
0.0084
500
500
429
426
84
84
70-130
1
mg/L
Nickel
ug/L
0.68
500
500
1100
1090
85
82
70-130
1
mg/L
Selenium
ug/L
ND
500
500
260
255
52
51
70-130
2 M1
Silver
ug/L
0.023
250
250
304
304
112
112
70-130
0
mg/L
Thallium
ug/L
ND
500
500
376
378
74
75
70-130
0
Zinc
ug/L
1.1
500
500
1560
1550
97
94
70-130
1
mg/L
,MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2745910
2745911
MS
MSD
92455213001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
e/ Rec
e/ Rec
Limits
RPD Qual
'Antimony
ug/L
0.0037J
500
500
488
497
97
99
70-130
2
mg/L
Arsenic
ug/L
ND
500
500
496
508
99
101
70-130
2
Beryllium
ug/L
ND
500
500
457
474
91
95
70-130
4
Cadmium
ug/L
ND
500
500
473
486
95
97
70-130
3
Chromium
ug/L
0.035
500
500
483
497
90
92
70-130
3
mg/L
Copper
ug/L
0.081
500
500
563
581
96
100
70-130
3
i
mg/L
Lead
ug/L
0.0025J
500
500
459
471
91
94
70-130
2
mg/L
Nickel
ug/L
0.034
500
500
479
491
89
91
70-130
3
mg/L
Selenium
ug/L
ND
500
500
513
526
103
105
70-130
2
Silver
ug/L
ND
250
250
238
245
95
98
70-130
3
Thallium
ug/L
0.0037J
500
500
447
457
89
91
70-130
2
mg/L
Zinc
ug/L
0.077
500
500
536
547
92
94
70-130
2
mg/L
Results presented on this page are In the units Indicated by me "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, -I-C.
Page 11 of 27

aceAnalytical
www.pacelabs.cem
QUALITY CONTROL DATA
Project: STORMWATER-SD-03
Pace Project No.: 92455195
OC Batch: 513061 Analysis Method: EPA 624.1
OC Batch Method: EPA 624.1 Analysis Description: 624 MSV
Associated Lab Samples: 92455195001
METHOD BLANK: 275039E
" Associated Lab Samples:
400-1S4bYp➢il
Matrix: Water
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,1,1-Tdchloroethane
ug/L
NO
2.0
12/05/19 12:49
i1, 1,2,2-Tetrachloroethane
ug/L
NO
2.0
12/05/19 12:49
1, 1,2-Trichloroethane
ug/L
NO
2.0
12/05/19 12:49
1, 1 -Dichloroethane
ug/L
NO
2.0
12/05/19 12:49
1,1-Dichloroethene
ug/L
NO
2.0
12/05/1912:49
1,2-Dichlorobenzene
ug/L
NO
2.0
12/05/19 12:49
.1,2-Dichloroethane
ug/L
NO
2.0
12/05/191249
1,2-Dichloropropane
ug/L
NO
2.0
12/05/19 12:49
„1,3-Dichlorobenzene
ug/L
NO
2.0
12/05/1912:49
1,4-Dichlorobenzene
ug/L
NO
2.0
12/05/1912A9
Benzene
ug/L
NO
1.0
12/05/19 12:49
Bromodichloromelhane
ug/L
NO
2.0
12105/191249
'Bromoform
ug/L
NO
2.0
12/05/191249
Bromomethane
ug/L
NO
2.0
12I05/1912:49
;Carbon tetrachloride
ug/L
NO
2.0
12/05/19 12:49
Chlorobenzene
ug/L
NO
2.0
12/05/19 12:49
Chloroethane
ug/L
NO
2.0
12/05/19 12:49
Chloroform
ug/L
NO
2.0
12/05/19 1249
Chloromethane
ug/L
NO
2.0
12/05/1912:49
cis-1,2-Dichloroethene
ug/L
NO
2.0
12/05/19 12:49
cis-1,3-Dichloropropene
ug/L
NO
2.0
12/05/19 12:49
Dibromochloromethane
ug/L
NO
2.0
12/0511912:49
Ethylbenzene
ug/L
NO
1.0
12105/1912:49
Methylene Chloride
ug/L
NO
2.0
12/05/19 12:49
Tetrachloroethene
ug/L
NO
2.0
12/05/19 12:49
Toluene
ug/L
NO
1.0
12/05/19 12:49
trans-1,2-Dichloroethene
uglL
NO
2.0
12/05/19 1249
trans-1,3-Dichloropropene
ug/L
NO
2.0
12/05/19 12:49
Trichloroelhene
ug/L
NO
2.0
12/05/19 1249
Trichlorofluoromethane
ug/L
NO
2.0
12/05/19 12:49
Vinyl chloride
ug/L
NO
2.0
12/05/19 12:49
1,2-Dichloroethane-d4 (S)
%
108
70-130
12105/1912:49
4-Bromofluorobenzene (S)
%
108
70-130
12/05/19 12:49
Toluene-d8(S)
%
104
70-130
12/05/19 12:49
LABORATORY CONTROL SAMPLE:
2750400
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
1,1,1-Thchloroethane
ug/L
20
23.0
115 70-130
1,1,2,2-Tetrachloroethane
ug/L
20
18.0
90 60-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/10/2019 05:51 PM without the written consent of Pace Analylical Services, LLC.
Page 12 of 27

m
lace Analytical
w;ins.pacelabs.com
QUALITY CONTROL DATA
Project: STORMWATER-SD-03
Pace Project No.: 92455195
LABORATORY CONTROL SAMPLE: 2750400
Spike
LCS
LCS
%Rec
Parameter
Units
Conic.
Result
% Rec
Limits
1,1,2-Trichloroethane
ug/L
20
22.2
111
70-130
1,1-Dichloroethane
uglL
20
22.2
111
70-130
1,1-Dichloroethene
ug/L
20
22.5
113
50-150
1,2-Dichlorobenzene
ug/L
20
19.2
96
65-135
1,2-Dichloroethane
ug/L
20
21.9
110
49-155
1,2-Dichloropropane
ug/L
20
22.2
111
35-165
1,3-Dichlorobenzene
ug/L
20
18.8
94
70-130
1,4-Dichlorobenzene
ug/L
20
19.2
96
65-135
Benzene
ug/L
20
21.1
106
65-135
Blnmodlchloromethane
ug/L
20
22.7
114
65-135
Bromoform
ug/L
20
20.0
100
70-130
Bromomethane
ug/L
20
20.6
103
15-185
Carbon tetrachloride
ug/L
20
23.3
116
70-130
Chlorobenzene
ug/L
20
19.5
97
65-135
Chloroethane
ug/L
20
17.2
86
40-160
iChloroform
ug/L
20
22.2
111
70-135
Chloromethane
ug/L
20
17.7
88
1-205
cis-1,2-Dichloroethene
ug/L
20
21.4
107
68-146
'cis-1,3-Dichloropropene
ug/L
20
23.6
118
25-175
Dibromochloromethane
ug/L
20
20.1
101
70-135
Ethylbenzene
ug/L
20
18.9
95
60-140
Methylene Chloride
ug/L
20
19.1
96
60-140
Tetrachloroethene
ug/L
20
18.8
94
70-130
Toluene
ug/L
20
21.0
105
70-130
trans-1,2-Dichloroethene
ug/L
20
22.6
113
70-130
trans-1,3-Dichloropropene
ug/L
20
23.4
117
50-150
Trchloroethene
ug/L
20
22.8
114
65-135
Trichlorofluoromelhane
ug/L
20
24.1
121
50-150
Vinyl chloride
ug/L
20
20.4
102
5-195
1,2-Dichloroethane-d4 (S)
%
104
70-130
4-Bromolluorobenzene (S)
%
102
70-130
Toluene-d8 (S)
i
e/
102
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2750401
2750402
MS MSD
1, 1, 1-Trichloroethane
1, 1,2,2-Tetrachlomethane
1, 1,2-Trichloroethane
1.1-Dichloroethane
1, 1 -Dichloroethene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
92455195001
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
MS MSD MS MSD e/ Rec
Result Result %Rec %Rec Limits RPD Qual
ug/L
NO
20
20
21.5
17.8
107
89
52-162
19
ug/L
NO
20
20
15.5
12.3
77
62
46-157
22
ug/L
NO
20
20
20.1
17.1
101
85
52-150
16
ug/L
NO
20
20
20.6
17.4
103
87
59-155
17
ug/L
NO
20
20
22.8
19.2
114
96
1-234
17
uglL
NO
20
20
15.6
12.2
78
61
18-190
24
ug/L
NO
20
20
21.0
17.6
105
88
49-155
17
ug/L
NO
20
20
21A
17.3
105
86
1-210
20
Results presented on this page are In the units indicated by the "Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, -I-C. Page 13 of 27

lace Analytical
www.pacgfilln com
Project:
Pace Project No.:
J
STORMWATER-SD-03
92455195
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2750401
MS
92455195001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2750402
MS
Result
MSD
Result
MS
% Rec
MSD
p/ Rec
%Rec
Limits
RPD Oual
1,3-Dichlorobenzene
ug/L
NO
20
20
15.3
12.3
77
61
59-156
22
1,4-Dichlorobenzene
ug/L
NO
20
20
15.3
11.9
76
59
18-190
25
Benzene
ug/L
NO
20
20
19.6
16.4
98
82
37-151
18
Bromodichloromethane
ug/L
ND
20
20
20.9
18.4
104
92
35-155
13
Bromoform
ug/L
NO
20
20
17.6
13.9
88
70
45-169
23
Bromomethane
ug/L
NO
20
20
12.5
12.7
62
63
1-242
1
Carbon tetrachloride
ug/L
NO
20
20
22.1
17.7
110
89
70-140
22
Chlorobenzene
ug/L
NO
20
20
16.6
13.4
83
67
37-160
21
ug/L
ND
20
20
18.0
15.1
90
76
14-230
18
IChloroelhane
Chloroform
ug/L
ND
20
20
22.2
17.8
111
89
51-138
22
Chloromelhane
ug/L
NO
20
20
16.7
14.5
84
73
1-273
14
cis-1,2-Dichloroethene
ug/L
NO
20
20
20.5
17.5
102
87
45-174
16
cis-1,3-Dichloropropene
ug/L
NO
20
20
21.5
18.3
107
92
1-227
16
Dibromochloromethane
ug/L
ND
20
20
17.6
14.5
88
72
53-149
19
Ethylbenzene
ug/L
ND
20
20
16.1
12.8
81
64
37-162
23
Methylene Chloride
ug/L
NO
20
20
18.9
15.8
95
79
1-221
18
Tetrachloroethene
ug/L
NO
20
20
16.2
12.0
81
60
64-148
30 Ml
'Toluene
ug/L
NO
20
20
19.2
15.6
96
78
47-150
20
,trans-1,2-Dichloroelhene
ug/L
NO
20
20
21.5
17.6
107
88
54-156
20
.trans-1,3-Dichloropropene
ug/L
NO
20
20
20.6
17.3
103
87
17-183
17
Tdchloroethene
ug/L
NO
20
20
21.1
17.0
105
85
70-157
21
iTrichlorolluoromethane
ug/L
NO
20
20
22.4
19.0
112
95
17-181
16
Vinyl chloride
ug/L
NO
20
20
19.8
16.4
99
82
1-251
19
1,2-Dichloroethane-d4(S)
%
110
108
70-130
4-Bromofluorobenzene(S)
%
99
102
70-130
Toluene-d8(S)
%
104
105
70-130
Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, I.I.C. Page 14 of 27

(�5ace Analytical
www.D+celeb+.com
I
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
STORMWATER-SD-03
Pace Project No.:
92455195
OC Balch:
512063 Analysis Method: EPA 608.3
QC Batch Method:
EPA 608.3 Analysis Description: 608 PCB Pest Red Vol
Associated Lab Samples:
92455195001
METHOD BLANK: 2746029
Matrix:
Water
Associated Lab Samples: 92455195001
Blank
Reporting
Parameter
I14,4'-DDD
Units
Result
Limit
Analyzed
Qualifiers
ug/L
ND
0.050
12/04/19 18:59
4,4'-DDE
ug/L
ND
0.050
12/04/19 18:59
'14,4'-DDT
ug/L
ND
0.050
12/04/1918:59
Aldrin
ug/L
ND
0.050
12/04/19 18:59
.,alpha-BHC
ug/L
NO
0.050
12104/1918:59
'lalpha-Chlordane
ug/L
ND
0.050
12/04/19 18:59
beta-BHC
ug/L
ND
0.050
12/04/191859
Chlordane( Technical)
ug/L
ND
0.50
12/04/1918:59
delta-BHC
ug/L
ND
0.050
12/04/19 18:59
Dieldrin
ug/L
NO
0.050
12/04/19 18:59
Endosulfan I
ug/L
ND
0.050
12/04/19 18:59
Endosulfan II
ug/L
ND
0.050
12/04/19 18:59
Endosulfan sulfate
ug/L
ND
0.050
12/04/19 18:59
Endrin
ug/L
ND
0.050
12104/1918:59
Endrin aldehyde
uglL
ND
0.050
12/04/19 18:59
(gamma-BHC (Lindane)
ug/L
ND
0.050
12/04/19 18:59
'gamma -Chlordane
ug/L
ND
0.050
12/04/191859
Heptachlor
ug/L
ND
0.050
12/04/19 18:59
Heplachlor epoxide
ug/L
ND
0.050
12/04/1918:59
PCB-1016 (Aroclor 1016)
ug/L
ND
0.50
12/04/19 18:59
PCB-1221 (Aroclor 1221)
ug/L
ND
0.50
12/04/19 1859
PCB-1232 (Aroclor 1232)
ug/L
ND
0.50
12/04/19 18:59
PCB-1242 (Aroclor 1242)
ug/L
ND
0.50
12/04/19 18:59
PCB-1248 (Aroclor 1248)
ug/L
NO
0,50
12/04/19 18:59
PCB-1254 (Aroclor 1254)
ug/L
NO
0.50
12/04/19 18:59
PCB-1260 (Aroclor 1260)
ug/L
ND
0.50
12/04/19 18:59
Toxaphene
ug/L
ND
0.50
12/0411918:59
Decachlorobiphenyl (S)
%
126
10-130
12/04/19 18:59
Tetrachloro-m-xylene(S)
%
123
10-130
12/04/19 18:59
LABORATORY CONTROL SAMPLE: 2746030
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
%Rec Limits
Qualifiers
4;4'-DDD
ug/L
0.25
0.28
113
31-141
4,4'-DDE
ug/L
0.25
0.26
106
30-145
4,4'-DDT
ug/L
0.25
0.29
115
25-160
Aldrin
ug/L
0.25
0.24
96
42-140
alpha-BHC
ug/L
0.25
0.26
103
37-140
alpha -Chlordane
ug/L
0.25
0.28
112
45-140
beta-BHC
ug/L
0.25
0.33
131
17-147
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the wnden consent of Pace Analytical Services, LLC. Page 15 of 27

aceAnalytical
www.paceleEs.com
QUALITY CONTROL DATA
Project: STORMWATER-SD-03
Pace Project No.: 92455195
LABORATORY CONTROL SAMPLE:
2746030
Spike
LCS
LCS
%Rec
Parameter
Units
Conc.
Result
%Red
Limits
delta-BHC
ug/L
0.25
0.27
109
19-140
Dieldrin
ug/L
0.25
0.28
111
36-146
Endosulfan I
ug/L
0.25
0.27
110
45-153
Endosulfan II
ug/L
0.25
0.28
112
1-202
Endosulfan sulfate
ug/L
0.25
0.29
114
26-144
Endrin
ug/L
0.25
0.28
114
30-147
Endrin aldehyde
ug/L
0.25
0.21
83
50-150
- gamma-BHC (Lindane)
ug/L
0.25
0.27
107
32-140
"gamma -Chlordane
ug/L
0.25
0.20
79
45-140
Heptachlor
ug/L
0.25
0.25
100
34-140
Heptachlor epoxide
ug/L
0.25
0.28
110
37-142
Decachlorobiphenyl (S)
e/
126
10-130
Tetrachloro-m-xylene (S)
%
115
10-130
'MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2746031 2746032
Parameter
4,4'-DDD
4A-DDE
'4,4'-DDT
Aldrin
alpha-BHC
alpha -Chlordane
beta-BHC
delta-BHC
Dieldrin
Endosulfan I
Endosulfan It
Endosulfan sulfate
Endrin
Endrin aldehyde
gamma-BHC (Lindane)
gamma -Chlordane
Heptachlor
Heptachlor epoxide
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
92455195001
Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
MS
Result
MSD
Result
MS
%Rec
MSD
%Rec
% Rec
Limits
RPD
ug/L
NO
0.25
0.25
0.29
0.30
114
121
31-141
6
ug/L
NO
0.25
0.25
0.27
0.28
108
113
30-145
5
ug/L
NO
0.25
0.25
0.29
0.30
116
122
25-160
5
ug/L
NO
0.25
0.25
0.25
0.28
102
112
42-140
10
ug/L
NO
0.25
0.25
0.26
0.28
104
112
37-140
8
ug/L
NO
0.25
0.25
0.28
0.29
ill
117
45-140
6
ug/L
NO
0.25
0.25
0.31
0.34
123
134
17-147
9
ug/L
NO
0.25
0.25
0.28
0.29
ill
117
19-140
5
ug/L
NO
0.25
0.25
0.27
0.29
109
115
36-146
6
ug/L
NO
0.25
0.25
0,27
0.28
107
114
45-153
6
uglL
NO
0.25
0.25
0.27
0.29
108
116
1-202
7
ug/L
NO
0.25
0.25
0.28
0.30
113
120
26-144
6
ug/L
NO
0.25
0.25
0.28
0.30
ill
119
30-147
6
ug/L
NO
0.25
0.25
0.24
0,26
96
103
50-150
7
ug/L
ND
0.25
0.25
0.27
0.29
110
117
32-140
7
ug/L
NO
0.25
0.25
0.20
0.21
79
84
45-140
6
ug/L
NO
0.25
0.25
0.27
0.29
107
116
34-140
8
ug/L
NO
0.25
0.25
0.27
0.29
108
115
37-142
7
%
125
132
10-130
%
122
132
10-130
Results presented on this page are in the units Indicated by the "Units" column exceptwhere an alternate on It Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 27

5OAnalytical0
www.pecelebs.com
QUALITY CONTROL DATA
'li Project: STORMWATER-SD-03
Pace Project No.: 92455195
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
OC Batch: 512091
Analysis
Method:
EPA 625.1
QC Batch Method: EPA 625.1
Analysis
Description:
625 MSS
Associated Lab Samples: 92455195001
METHOD BLANK: 2746155
Associated Lab Samples: 92455195001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
NO
5.0
12/02/19 15:43
2,2'-Oxybis(1-chloropropane)
ug/L
NO
5.0
12/02/19 1543
2,4,6-Trichlorophenol
ug/L
NO
10.0
12/02/19 1543
2,4-Dichlorophenol
ug/L
NO
5.0
12/02/19 15:43
2,4-Dimethylphenol
ug/L
NO
10.0
12YO2119 15:43
2,4-Dinitrophenol
uglL
NO
50.0
12/02/19 15:43
2,4-Dinitrotoluene
ug/L
NO
5.0
12/02/19 15:43
-2,6-Dinitrotoluene
ug/L
NO
5.0
12/02/19 15:43
2-Chloronaphthalene
ug/L
NO
5.0
12/02/19 15:43
12-Chlorophenol
ug/L
NO
5.0
12/02/19 15:43
2-Nitrophenol
ug/L
NO
5.0
1210211915:43
3,3'-Dichlorobenzidine
ug/L
NO
25.0
12/02/19 15:43
'4,6-Dinitro-2-methylphenol
ug/L
NO
20.0
12102/1915:43
4-Bromophenylphenyl ether
ug/L
NO
5.0
12/02/19 1543
4-Chloro-3-methylphenol
ug/L
NO
5.0
12/02/19 15:43
4-Chlorophenylphenyl ether
ug/L
NO
5.0
12/02/19 15:43
4-Nitrophenol
ug/L
NO
50.0
12/02/19 15:43
Acenaphthene
ug/L
NO
5.0
12/02/19 15:43
Acenaphthylene
ug/L
NO
5.0
12/02/19 15:43
Anthracene
ug/L
NO
5.0
12/021191543
Benzo(a)anthracene
ug/L
NO
5.0
12/02/19 15:43
Benzo(a)pyrene
ug/L
NO
5.0
12/02/19 15:43
Benzo(b) luomnthene
ug/L
NO
5.0
12/02/19 1543
Benzo(g,h,i)perylene
ug/L
NO
5.0
12/02/19 15:43
Benzo(k)Fluoranthene
ug/L
NO
5.0
12/02/191543
bis(2-Chloroethoxy)methane
ug/L
NO
10.0
12/0211915:43
bis(2-Chloroethyl) ether
ug/L
NO
5.0
12/02/19 1543
bis(2-Ethylhexyl)phthalate
ug/L
NO
5.0
12/0211915:43
Butylbenzylphthalate
ug/L
NO
5.0
12/02/19 15:43
Chrysene
ug/L
NO
5.0
12/02/191543
Di-n-butylphthalate
ug/L
NO
5.0
12/02/191543
Di-n-octylphthalate
ug/L
NO
5.0
12/02/19 15:43
D benz(a,h)anthracene
ug/L
NO
5.0
12/02/19 15:43
Diethylphthalate
ug/L
NO
5.0
12/02/19 15:43
Dimethylphthalate
ug/L
NO
5.0
12/02/19 15:43
Fluoranthene
ug/L
NO
5.0
12/02/19 15:43
F uorene
ug/L
NO
5.0
12/02/19 15:43
Hexachloro-1,3-butadiene
ug/L
NO
5.0
12/02/19 15:43
Hexachlorobenzene
ug/L
NO
5.0
12/02/19 15:43
Hexachlorocyclopentadiene
ug/L
NO
10.0
12102/191543
Hexachloroethane
ug/L
NO
5.0
12/02/191543
Qualifiers
Results presented on this page are In the units indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/1012019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 27

lace Analytical
www.Wcelabs.corn
QUALITY CONTROL DATA
II Project: STORMWATER-SD-03
Pace Project No.: 92455195
METHOD BLANK: 2746155
Matrix:
Water
',. Associated Lab Samples: 92455195001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Indeno(1,2,3-cd)pyrene
ug/L
NO
5.0
12/02/19 15:43
Isophorone
ug/L
NO
10.0
12/02/19 15:43
N-Nitroso-di-n-propylamine
ug/L
NO
5.0
12J0211915:43
N-Nitrosodimethylamine
ug/L
NO
5.0
12/02/19 15:43
N-Nitrosodiphenylamine
ug/L
NO
10.0
12102/191543
Naphthalene
ug/L
NO
5.0
12/02/1915:43
Nitrobenzene
ug/L
NO
5.0
12/0211915:43
" Pentachlorophenol
ug/L
NO
10.0
12/02/19 15:43
Phenanthrene
ug/L
NO
5.0
12102/1915:43
Phenol
ug/L
NO
5.0
12/02/19 15:43
Pyrene
ug/L
NO
5.0
12/0211915:43
, 2,4,6-Tnbromophenol (S)
%
67
10-137
12/02/19 15:43
:,2-Fluorobiphenyl (S)
%
75
15-120
12/02/19 15:43
'2-Fluorophenol (S)
%
50
10-120
12/02/19 15:43
Nitrobenzene-d5 (S)
%
82
10-120
12/02/19 15:43
Phenol-d6 (S)
%
35
10-120
12/02/19 15:43
'Terphenyl-dl4(S)
%
72
11-131
12/02/19 15:43
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2746156
Units
Spike
Conic.
1-CS
Result
LCS
% Rec
e/ Rec
Limits
1,2,4-Tdchlorobenzene
ug/L
50
41.2
82
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
49.1
98
36-166
2,4,6-Trichlorophenol
ug/L
50
42.9
86
37-144
2,4-Dichlorophenol
ug/L
50
44.2
88
39-135
2,4-Dimethylphenol
ug/L
50
46.6
93
32-120
2,4-Dinitrophenol
ug/L
250
254
102
1-191
2,4-Dinitrotoluene
ug/L
50
47.8
96
39-139
2,6-Dinitrotoluene
ug/L
50
49.8
100
50-158
2-Chloronaphthalene
ug/L
50
47.7
95
60-120
2-Chlorophenol
ug/L
50
43.8
88
23-134
2-Nitrophenol
ug/L
50
48.3
97
29-181
3,3'-Dichlorobenzidine
ug/L
100
85.9
86
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
106
106
1-181
4-Bmmophenylphenyl ether
ug/L
50
42.2
84
53-127
4-Chloro-3-methylphenol
ug/L
100
98.8
99
22-147
4-Chlorophenylphenyl ether
ug/L
50
43.4
87
25-158
4-Nitrophenol
ug/L
250
229
92
1-132
Acenaphthene
ug/L
50
45.0
90
47-145
Acenaphthylene
ug/L
50
47.6
95
33-145
Anthracene
ug/L
50
47.1
94
27-133
Benzo(a)anthracene
ug/L
50
49.8
100
33-143
Benzo(a)pyrene
ug/L
50
50.4
101
17-163
Benzo(b)fluoranthene
ug/L
50
53.0
106
24-159
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
Results presented on this page are In the units indicated by the -Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 27

laceAnalAcal'
ww.pacelabs.com
QUALITY CONTROL DATA
Project: STORMWATER-SD-03
Pace Project No.: 92455195
Pace Analytical Services, LLD
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
2746156
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Benzo(g,h,i)perylene
uglL
50
46.0
92
1-219
Benzo(k)fiuoranthene
ug/L
50
52.4
105
11-162
bis(2-Chloroethoxy)methane
ug/L
50
43.8
88
33-184
bis(2-Chloroethyp ether
ug/L
50
46.6
93
12-158
bis(2-Ethylhexygphthalale
ug/L
50
51.6
103
8-158
Butylbenzylphlhalate
ug/L
50
51.5
103
1-152
Chrysene
ug/L
50
44.0
88
17-168
Di-n-butylphthalate
ug/L
50
47.2
94
1-120
Di-n-octylphthalate
ug/L
50
54.9
110
4-146
Dibenz(a,h)anlhracene
ug/L
50
48.0
96
1-227
IDielhylphthalate
ug/L
50
44.0
88
1-120
Dimethylphthalale
ug/L
50
42.8
86
1-120
Fluoranthene
ug/L
50
46.8
94
26-137
Fluorene
ug/L
50
47.0
94
59-121
Hexachloro-1,3-butadiene
ug/L
50
38.2
76
24-120
Hexachlorobenzene
ug/L
50
41.7
83
1-152
Hexachlorocyclopenladiene
ug/L
50
32.6
65
25-150
',Hexachloroethane
ug/L
50
43.2
86
40-120
Indeno(1,2,3-cd)pyrene
ug/L
50
46.8
94
1-171
Isophorone
ug/L
50
46.3
93
21-196
N-Nitroso-di-n-propylamine
ug/L
50
50.6
101
1-230
'N-Nitrosodimethylamine
ug/L
50
41.6
83
25-150
N-Nitrosodiphenylamine
ug/L
50
44.1
88
25-150
Naphthalene
ug/L
50
46.0
92
21-133
Nitrobenzene
ug/L
50
47.7
95
35-180
Pentachlorophenol
ug/L
100
83.7
84
14-176
Phenanthrene
ug/L
50
45.7
91
54-120
Phenol
ug/L
50
47.3
95
5-120
Pyrene
ug/L
50
47.7
95
52-120
2,4,6-Tnbromophenol (S)
p/
93
10-137
2-Fluorobiphenyl (S)
%
84
15-120
2-Fluorophenol (S)
%
87
10-120
Nitrobenzene-d5(S)
%
95
10-120
Phenol-d6 (S)
%
95
10-120
Terphenyl-d 14(S)
%
95
11-131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2746157
2746158
MS
MSD
92449985006
Spike
Spike
MS
MSD
MS MSD % Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec e/ Rec Limits RPD
1,2,4-Tnchlorobenzene
ug/L
ND
100
100
67.9
73.8
68
74 44-142 8
2,2'-Oxybis(1-chloropropane)
ug/L
ND
100
100
88.3
101
88
101 36-166 13
2,4,6-Tnchlorophenol
ug/L
NO
100
100
40.6
73.4
41
73 37-144 58
2,4-Dichlorophenol
ug/L
NO
100
100
49.6
82.6
50
83 39-135 50
2,4-Dimethylphenol
ug/L
ND
100
100
84.3
95.6
84
96 32-120 13
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Dale: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 27

ace Analytical
www.pacele0vcorn
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER-SD-03
Pace Project No.: 92455195
MATRIX SPIKE 8 MATRIX SPIKE
DUPLICATE:
2746157
2746158
MS
MSD
92449985006
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result e/ Rec
% Rec
Limits RPD Oual
2,4-Dinitrophenol
ug/L
NO
500
500
73.6J
269
15
54
1-191
2,4-Dinitrotoluene
ug/L
NO
100
100
99.6
106
100
106
39-139
6
2,6-Dinitrotoluene
ug/L
NO
100
100
103
109
103
109
50-158
6
2-Chloronaphthalene
ug/L
NO
100
100
91.6
105
92
105
60-120
13
�12-Chlorophenol
ug/L
NO
100
100
46.4
79.3
46
79
23-134
52
2-Nibophenol
ug/L
NO
100
100
47.1
86.5
47
86
29-182
59 R1
3,3'-Dichlorobenzidine
ug/L
NO
200
200
167
177
84
89
1-262
6
' 4,6-Dinitro-2-methylphenol
ug/L
NO
200
200
72.5
137
36
69
1-181
62 Rl
4-Bromophenylphenyl ether
ug/L
NO
100
100
81.6
86.9
82
87
53-127
6
.4-Chloro-3-methylphenol
ug/L
NO
200
200
170
201
85
101
22-147
17
4-Chlorophenylphenyl ether
ug/L
NO
100
100
88.8
94.4
89
94
25-158
6
.4-Nitrophenol
ug/L
NO
500
500
142
241
28
48
1-132
51
''Acenaphthene
ug/L
NO
100
100
89.6
95.7
90
96
47-145
7
Acenaphthylene
ug/L
NO
100
100
94.3
101
94
101
33-145
7
Anthracene
ug/L
NO
100
100
93.2
96.9
93
97
27-133
4
Benzo(a)anthracene
ug/L
NO
100
100
97.8
103
98
103
33-143
5
Benzo(a)pyrene
ug/L
NO
100
100
100
104
100
104
17-163
4
Benzo(b)fluoranthene
ug/L
NO
100
100
107
112
107
112
24-159
4
Benzo(g,h,i)perylene
ug/L
NO
100
100
91.5
90.9
91
91
1-219
1
,Benzo(k)fluoranthene
ug/L
ND
100
100
105
111
105
111
11-162
5
Ibis(2-Chloroethoxy)methane
uglL
NO
100
100
79.7
91.0
80
91
33-184
13
�bis(2-Chloroethyl) ether
ug/L
NO
100
100
82.0
93.0
82
93
12-158
13
bis(2-Ethylhexypphthalate
ug/L
NO
100
100
102
104
102
104
8-158
2
Butylbenzylphthalate
ug/L
NO
100
100
102
103
102
103
1-152
1
Chrysene
ug/L
NO
100
100
87.3
92.2
87
92
17-168
5
Di-n-butylphthalate
ug/L
ND
100
100
94.4
99.0
94
99
1-120
5
Di-n-octylphthalate
ug/L
NO
100
100
107
114
107
114
4-146
6
Di be nz(a, h)anthracene
ug/L
ND
100
100
95.6
97.9
96
98
1-227
2
Diethylphthalate
ug/L
NO
100
100
92.6
97.4
93
97
1-120
5
Dimethylphthalate
ug/L
NO
100
100
89.2
94.2
89
94
1-120
5
Fluoranthene
ug/L
NO
100
100
92.9
99.7
93
100
26-137
7
Fluorene
ug/L
NO
100
100
96.5
102
97
102
59-121
6
Hexachloro-1,3-butad iene
ug/L
ND
100
100
60.3
64.4
60
64
24-120
7
Hexachlorobenzene
ug/L
ND
100
100
80.1
85.1
80
85
1-152
6
HexachlorocycAopentadiene
ug/L
ND
100
100
48.0
55.7
48
56
25-150
15
Hexachloroethane
ug/L
ND
100
100
68.6
72.4
69
72
40-120
5
Inderoll, 2,3-cd)pyrene
ug/L
ND
100
100
92.9
93.9
93
94
1-171
1
Isophorone
ug/L
NO
100
100
84.9
97.0
85
97
21-196
13
N-Nitroso-di-n-propylamine
ug/L
NO
100
100
92.8
107
93
107
1-230
14
N-Nitrosodimelhylamine
ug/L
NO
100
100
66.3
71.1
66
71
25-150
7
N-Nilrosodiphenylainine
ug/L
ND
100
100
87.5
91.3
88
91
25-150
4
Naphthalene
ug/L
ND
100
100
80.4
88.8
80
89
21-133
10
Nitrobenzene
ug/L
ND
100
100
86.9
99.8
87
100
35-180
14
Pentachlorophenol
ug/L
ND
200
200
61.0
111
31
56
14-176
58
Phenanthrene
ug/L
NO
100
100
90.0
95.4
90
95
54-120
6
Phenol
ug/L
NO
100
100
40.6
59.8
41
60
5-120
38
Ii Results presented on this page are In
the units Indicated by the'Unib- column except where an alternate unit
Is presented
to the right of the result.
REPORT OF
LABORATORY
ANALYSIS
This
report shall not be reproduced, except
in full,
Dale: 12/10/2019 05:51 PM
without
the written consent of Pace Analytical
Services, LLC.
Page 20 of 27

lace Analytical
unre.pacelaha.cem
QUALITY CONTROL DATA
Project: STORMWATER-SD-03
Pace Project No.: 92455195
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE: 2746157
2746158
MS
MSD
92449985006 Spike
Spike
MS
MSD MS
MSD
%Rec
Parameter
Units Result Conc.
Conc.
Result
Result e/ Rec
%Rec
Limits RPD Oual
Pyrene
ug/L ND 100
100
93.6
95.7 94
96
52-120 2
. 2,4,6-Tdbromophenol(S)
e/
46
78
10-137
2-Fluorobiphenyl (S)
e/
82
88
15-120
2-Fluorophenol(S)
%
33
59
10-120
Nitrobenzene-d5(S)
%
88
97
10-120
Phenol-d6 (S)
%
41
56
10-120
Terphenyl-d14 (S)
%
82
69
11-131
Results presented on this page are In Me units Indicated by me "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 27

it
aceAnalyfil l
www.pacelaha.calp
Project: STORMWATER-SD-03
Pace Project No.: 92455195
OC Batch: 511928
OC Batch Method: SM 25400-2011
Associated Lab Samples: 92455195001
METHOD BLANK: 2745618
j' Associated Lab Samples: 92455195001
Parameter Units
Total Suspended Solids mg/L
,.LABORATORY CONTROL SAMPLE:
Parameter
2745619
Units
Total Suspended Solids
mg/1-
;ISAMPLE DUPLICATE: 2745620
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2745621
Parameter
Units
Total Suspended Solids
mg/L
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 254OD-2011
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 2.5 11/26/19 17:14
Spike 1-CS LCS % Rec
Conc. Result %Rec Limits Qualifiers
250 244 97 90-110
92455115001 Dup
Result Result RPD Qualifiers
29.3 34.7 17
92455086005 Dup
Result Result RPD Qualifiers
NO NO
Results presented on this page are in the units Indicated by the "Units" column except whore an alternate unit is presented to the right of the result.
Date: 12/10/201905:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 22 of 27

m
aceAnalytical
ViWisligh ba.coln
Project: STORMWATER-SD-03
Pace Project No.: 92455195
QC Batch: 512392
QC Batch Method: EPA 420.4 Rev 1.0 1993
L� Associated Lab Samples: 92455195001
METHOD BLANK: 2747669
Associated Lab Samples: 92455195001
Parameter Units
Phenol mg/L
LABORATORY CONTROL SAMPLE: 2747670
Parameter Units
Phenol mg/L
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 420.4 Rev 1.0 1993
Analysis Description: 420.4 Phenolics
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.020 12/03/1912:44
Spike LCS LCS e/ Rec
Conc. Result %Rec Limits Qualifiers
0.05 0.049 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2747671
2747672
MS
MSD
92455086001 Spike
Spike
MS
MSD
MS MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result
%Rec %Rec Limits RPD Qual
(Phenol mg/L ND 0.05
0.05
0.048
0,046
95 92 90-110 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2747673
2747674
MS
MSD
92455086002 Spike
Spike
MS
MSD
MS MSD %Rec
Parameter Units Result Conc.
Conc.
Result
Result
%Rec %Rec Limits RPD Qual
Phenol mg/L ND 0.05
0.05
0.046
0.043
92 86 90-110 7 Mt
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 12/10/2019 05:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L-C.
Page 23 of 27

laceAnalytical'
www.pecelabxxom
QUALIFIERS
Project: STORMWATER-SD-03
Pace Project No.: 92455195
DEFINITIONS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC -Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
ii POL- Practical Ouantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitnte by EPA
Method 8260,
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 27

ace Analytical e
www.pacelan.cort
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
STORMWATER-SD-03
92455195
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92455195001
SD3
EPA 1664E
513867
,92455195001
SD3
EPA 608.3
512063
EPA608.3
512391
92455195001
SD3
EPA 200.7 Rev 4.4 1994
511985
EPA 200.7 Rev 4.4 1994
511999
. 92455195001
SD3
EPA 245.1 Rev 3.0 1994
512899
EPA 245.1 Rev 3.0 1994
512943
92455195001
SD3
EPA 625.1
512091
EPA 625.1
512416
192455195001
SD3
EPA 624.1
513061
�'92455195001
I I
SD3
SM 2540D-2011
511928
92455195001
SD3
EPA 420.4 Rev 1.0 1993
512392
EPA 420.4 Rev 1.0 1993
512538
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/10/2019 05:51 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 27

CHAIN -OF -CUSTODY Analytical Request Document
Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields
LAB USE
y,y.WO# : 92455195
11611E 111161111116�1611
ALS24SSISS
or
Addresses t •I �stnr�� (� r.
Container PreservativeT e "
Lah Project Manager:
: ( I �
I :
Rep IGI '
j/ \ n
Email To:C`�L`YC�C,�
" Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric
aced. (a) sodium hydroxide. (5) tine acrlate,
�.t
L N 1Crr!GI s L S�
(61 methanol, (JI sodium bisvllate, (B) sodium thiosulfate. 19) hexanC
([)ammonium hydro..itle, ID) TSP,(U)Unpreserved, (0) Other
(A) ascorbic acid, IBl:wmonium ...U'te,
Co yTo:
Site Coll ction Info/Address. Ll
Analyses
Lab Profile/Line:
Customer Project Ndme/NUmbCC
State : County/city: Time Zone COICC[ed
Lab Sample Receipt Checklist:
I PT [ ) MT ( I CT �,]"ET
i
Custody Seals Preoenc/intact Y 1+ NA
Custody Signatures Present Y d NA
Pllone:�.Z>j�j75715 iir3'5VL
Site/Facility ID R:
Compliance Monitoring?
Email:�IC,yG}�p il`�i
I I Yes I ]No
Collector Signature Present N 14A
1Q,L1Y
Bottles lntart N NA
Correct Bottles w N NA
Collected By (print): -
Purchase Order N:
DW PWS ID P:
`�
`
0(�,/)., I•'�I C.tVA
Quote ll:
DW Location Code:
-
.�.
C
'—�
Sufi ieient volume Y� N NA
Samples Received on Ice N Ilk
von - uaaas Acce btu �'2^• 1 P✓��
pace pea }�
USDSamA Relar,gulated Soils 6 11/41
Collected 8 si nature
V( g
Sp y/
��'?�.
I :
Turnaround Dale Required;
q
immediately Packed on Ice:
I�fii f1 L'��Ij
I (Yes I ]No
j
L^i
,._1
�
�
C r.
Respdua in Holding Teed` Y N NA
Residual Chlorine PrcSent Y N FaD
Sample Disposal:
Rush:
Field filtered fir applicable):
�
1 I Dispose as appropriate ( I Rtmed
( I Same Day ( I Next Day
I I Yes I INo
Cl Strips: —
( I Archive:
( 12 Day ( 13 Day ( I a Day 115 Day
,�
'^
Sample pH Aecaptabl v N NA
( I Hold:
(Expedite Ch A I
arBps Apply)
Analysis:
�\
J
�
,�
J
\ \I
J
--
pH SLripp:
Sulfide Present Y N N�
teaa Aeetace strips:
' Matrix Codes (Insert in Matrix box below]: Drinking Water (DW). Ground Water (GW). Wastewater (WW),
V
- _
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WPI. Air (AR), Tissue ITS), Bioassay (B), Vapor (V), Other (Off
v
'J
�"
i
LAB USE ONLY:
cab sample a /Comments:
Comp/
Collected (or
Res
if of
e�
Customer Sample 10
P
Matrix'
Grab
Composi Le Start)
Composite End
Cl
Ctns
7 c�
Date
Time
Date
I Time
G
•�_
v'
C—
/ `�
�1: ?
Ik I
I[!-t',-1gi
II Z%:I
I
I
I
Special Conditions / Possible Hazards: Type of Ice Used: \ 'Wet) Blue Dry None
Packing Material Used: /
Qs
Radchem samples) screened (<500 cpm): Y N <
pany:(Signature) Date/Time: Received by/Company:(Signature)
G{ it-LS
pang:(Signature) Date/Time: Received by/Company:(Signature)
pany: (Signature) - Date/Tinre: Received by/Company: Signature)
SHORT HOLDS PRESENT (02 hours): YC N) N/A
Lab Tracking d: 2 410 5 0 3
UPS Client Courier `721g'Qborit
/ Jl(j MTiL LAB USE ONLY
/x-yr Tabled:
I Prelogin:
Lab Sample Temperature Info:
Temp Blank fteceiY Y �JA
Therm IDN: %Gl /
/Cooler 1 Temp Upon Receipt:'-� oC
,Cooler I Therm Corr. Factor: — oC
Cooler 1 Corrected Temp: �L r,_oC
Comments:
Trip Blank Received: Y kN,/ NA
HCL McOH TSP Other
Non Cnnfor (s): Page:
YES /� oh

Document Name:
ndition Upon Rec
Document fdo.:
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliferm, TOE, Oil and Grease, ORO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
February 7, 2018
of 2
Issuing
Project WO#:92455195
PM: CD1 Due Date: 12/12/19
CLIENT: 93—MoogComp
C
'a a
9
J
n
J
¢
J
C
O
Z
O
2
¢
o
Z
v
U
O O E o 1 o
J Vj J a N O
E
E
oyb
E
E
E
E
E
a
E
E E E E
E i E m E E f E '> '� E o o
1 O v o a o m m n ry v
N
J
o
N
J
x
N
J
m
ti
J
s
.-1
N
m
fl
2
m
H
N
x
V
m
3
1
a
,-,r
a
•1 I"
a a a a o > >
3
\
1
\\ \\
7
\-\\
I\
\
10l\I
I
\\\
N
—I\\
pH Adjustment Log for Preserved 53mples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time nuervatiOn nmaunl of Preservative tot N
dsted added
aursted
LefdDcatian Office (i.e.
mote: svnanever Isere is a aiscrepancy arrecung norm ununua w�nµ...i�� ».„.�, .. ...,., _....._ _. _..... __ _..
Out of hold, Incorrect preservative, out of temp, Incorrect containers.
Page 27 of 27