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HomeMy WebLinkAboutNCG030557_MONITORING INFO_20191122-------------- STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. w U& 0 3 u 55 7 DOC TYPE, ❑ HISTORICAL FILE C� MONITORING REPORTS DOC DATE ❑ ool I / l O-L a- YYYYMMDD Collins Aerospace • Avionics Fire Protection Systems • Kidde Aerospace and Defense I; Kidde Technologies Incorporated 4200 Airport Drive Wilson, NC 27USA ' Phone:252-2-237-7004 7004 Fa, : 252-246-7186 Collins Aerospace Direct 252-293-7202 tim Kidde Technologies, Inc. .collernandspace.iorn www.coll insaerospace.com Timothy J. Fernandez, M.S. EH&SGeneralist RECEIVE© November 14, 2019 NOV 2 2 2019 CENTRAL FILES Central Files DWR SECTION Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 CERTIFIED U.S. MAIL ARTICLE NUMBER: 7013 2630 0002 1841 5001 Dear Sir/Madame: This cover letter and the attached information are submitted per North Carolina Division of Energy, Mineral, and Land Resources, Storm Water General Permit NCG030000, i Certificate of Coverage number NCG030557, Part III Section E 1-2. As required we are i submitting a signed copy of the Discharge Monitoring Report (DMR), applicable laboratory analytical reports, and the sample chain of custody for the semiannual storm water outfall discharge monitoring event described below: Monitoring Year: One (1)- 2019 Monitoring Period: Two (2)- July 1 - December 31 q Permit Term Sample: Two (2)- Second of permit term Furthermore, per Part II, Section A.1.e, all stormwater outfalls have been evaluated for the presence of non-stormwater discharges. If you have any questions or require further information, please contact me by phone at (252) 293-7202 or email to timothy.fernandez(c)utas.utc.com. i Tha k u very much, I TA&s' -M-S. Eneralist Collins Aerospace Kidde Fire Protection Systems (Kidde Aerospace and Defense) Stormwater Discharge Monitoring Report for North Carolina Division.of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted November 14, 2019 CERTIFICATE OF COVERAGE NO. NCG03 0 5 5 7 FACILITY NAME Kidde Aerospace and Defense COUNTY Wilson PERSON COLLECTING SAMPLES Tim Fernandez LABORATORY Microbac Lab Cart. If ? 1 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD ❑ Jan -June Q July -Dec or ❑ Monthly' (month) E��1p9,,IJCHARGINGTOCLASS ❑ORW ❑HQW ❑Trout ❑PNA V f J ❑Zero -flow ❑Water Supply [:]SA NOV 2 2 2019 ❑other FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this periodj2 Ou[fall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH� Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics' g Benchmarks _ - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 - 01051 01094 00552 78141. #1 10/16/19 1.5" 17.20 6.5 0.003 <0.010 0.032 <5.00 Certificate #2 10/16/19 1.5" 45.30 6.5 0.003 <0.010 0.554 <5.00 Certificate #2 (Zinc Re -run) 10/16/19 1.5" - 6.5 - - 0.603 - - ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. ' Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Faiz Afzal Name (Print name) FAlr hpu l Title (Print title) � A-4 u�IH�l9 Sig a�e Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.' Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > SS gal of new oil per month. n No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L° Parameter Code - 46529 NCOIL 00552 CO530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 111112018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal copv of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of I11/9/1`1 Date Permit Date: 11/l/2018-05/31/2021 SW U-245, last revised 11/1/2018 Page 3 of 3 R�CF1`!r--n NOV 2 2 1m9 &)MICROBAC° Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9J0255 + Project Description Stormwater Sample For: Mr. Tim Fernandez Kidde Aerospace & Defence, Inc 4200 Airport Drive NW Wilson, NC 27896 I^ Administration Brittany Smith Thursday, November 7, 2019 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Dayville. If you have any questions, comments, or require further ,I assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are 'i reported on a'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the '.I samples analyzed as received Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 9 Revised Report: Amended- See Case Narrative. Kidde Aerospace & Defence, Inc i Mr. Tim Fernandez 4200 Airport Drive NW Wilson, NC 27896 �VMICROBAC` Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9JO255 Case Narrative Field pH (by client): pH 1- 6.5 Field pH (by client): pH 2-6.5 Report amended to reach allowable detention limit. B5 11/7/19 Project Name: Stormwater Sample Project / PO Number: 200420063 (2018) Received: 10/16/2019 Reported: 11/07/2019 Sample Summary Report 11 Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Outfall #1, grab K9J0255-01 Stormwater Grab 10/16/19 09:50 10/16/19 14:20 Outfall #2, grab K9J0255-02 Stormwater Grab 10/16/19 10:05 10/16/19 14:20 Outfall #2, grab (Re -run) KgJ0255-03 Stormwater Grab 10/16/19 10:05 10/16/19 14:20 Page 2 of 9 *MICROBAC"' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9J0255 Analytical Testing Parameters .i Client Sample ID: Outfall #1, grab Sample Matrix: Stormwater Collected By: Fernandez Lab Sample ID: K9J0255-01 Collection Date: 10/16/2019 9:50 Wet Chemistry Result RL Units Dilution Note Prepared Analyzed Analyst EPA 1664 Rev. B Oil & Grease (SGT-HEM) <5.00 5.00 mg/L 1 B26 1024/19 1141 TBM J SM 2540 D-2011 Total Suspended Solids 17.2 5.00 mg/L 1 10/17/19 1005 CLB Metals Result RL Units Dilution Note Prepared Analyzed Analyst Metals Aqueous/EPA 200.7 Rev 4.4 1994 Lead <0.010 0.010 mg/L 1 10/17/19 1435 10/17/19 1435 TAB !Zinc i 0.032 0.005 mg/L 1 10/17/19 1435 10/17/19 1435 TAB Total Metals - ICP/MS EPA 200.8, Rv. 5.4 Kopper itli Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH _Result RL .Units Dilution Note _Prepared Analyzed _ Analyst 0.003 0.002 mg/L 1 11/06/19 0623 11/06/19 1527 JYH Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864.1920 p I w .microbac.com Page 3 of 9 VMICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9J0255 Client Sample ID: Oulfall #2, grab Sample Matrix: Stormwater Collected By: Fernandez Lab Sample ID: K9J0255-02 Collection Date: 10/16/2019 10:05 Wet Chemistry Result RL Units Dilution Note Prepared Analyzed Analyst EPA 1664 Rev. B ' Oil & Grease (SGT-HEM) <5.00 5.00 mg/L 1 B25 10/24/19 1141 TBM SM 2540 D-2011 ,Total Suspended Solids 45.3 4.17 mg/L 1 10/17/19 1005 CLB I Metals Result RL Units Dilution Note Prepared Analyzed Analyst Metals Aqueous/EPA 200.7 Rev 4.4 1994 Lead <0.010 0.010 mg/L 1 10/17/19 1439 10/17/19 1439 TAB Zinc 0.554 0.005 mg/L 1 10/17/19 1439 10/17/19 1439 TAB Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH Total Metals - ICP/MS Result RL Units Dilution Note Prepared Analyzed Analyst ,EPA 200.8, Rv. 6.4 ,Copper 0.003 0.002 mg/L 1 11/06/19 0623 11/06/19 1531 JYH Client Sample ID: Oulfall #2, grab (Re -run) I' Sample Matrix: Stormwater Collected By: Fernandez Lab Sample ID: K9J0255-03 Collection Date: 10/16/2019 10:05 Metals Result RL Units Dilution Note Prepared Analyzed Analyst Metals AqueouslEPA 200.7 Rev 4.4 1994 Zinc 0.603 0.005 mg/L 1 10/31/19 1424 10/31/19 1424 TAB , Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864.1920 p I www.microbac.com Page 4 Of 9 OMICROBAC�' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9J0255 Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville Spike Source %REC RPD Wet Chemistry Result RL Units Level Result %REC Limits RPD Limit Notes latch KJ90148 - Wet Chem Aqueous - SM 2540 D-2011 Blank(KJ90148-BLK1) _ _ ..._.— .__ _ _ .._ _ Prepared 10/1712019 __ ..__ _.__._... _...__.._.._ -- Total Suspended Solids <2.50 9_ 2.50 m /L Blank (KJ90148-BLK2) Prepared & Analyzed: 10/17/2019 Total Suspended Solids <2.50 2.50 mg/L Blank(KJ90148-BLK_3) Prepa_red&Analyzed: 10/17/2019 Total Suspended Solids <2.50 2.50 mg/L Blank (KJ90148-BLK4) Total Suspended Solids <2.50 Blank(KJ90148-BLK_5)__ Total Suspended Solids <2.50 LCS Dup (KJ90148-BSD1) Total Suspended Solids 30.7 KJ92426 -Wet Chem Aqueous - EPA 1664 Rev. B & Analyzed: 10/17/2019 2.50 mg/L Prepared&Analyzed_10/17/2019 2.50 mg/L Prepared &Analyzed. 10/17/2019 2.50 mg/L 31.6 97 94.5105.4 200 200 Blank(KJ92426-BLKt) Prepared & Analyzed: 10/24/2019 ---------- _,__----------- _____-___-___________ Oil & Grease (SGT-HEM) <5.00 5.00 mg/L LCS(KJ92426-BSI)Prepared & Analyzed: 10/24/2019 .Oil & Grease (SGT-HEM) 19.6 5.00 mg/L 20.4 96 64-114 Matrix Spike (KJ92426.MS1) Source: K9J0311-01 Prepared & Analyzed: 10/2412019 Oil & Grease (SGT-HEM) 28.7 5.00 mg/L 21.7 1.47 125 78-132 Metals Result Batch KJ90158 - Metals Aqueous - EPA 200.7 Rev 4.4 1994 Bank (KJ90158-BLK1)_ Lead <0.020 Zinc <0.010 Blank (KJ90158-BLK2) Lead <0.020 Zinc <0.010 LCS (KJ90158-BS1)__ Lead 0.245 Zinc 0.247 ' LCS (KJ90158-BS2) Lead 0.258 Zinc 0.260 11 LCS(KJ90158-BS3) Lead 0 252 Zinc 0.251 Spike Source %REC RPD RL Units Level Result %REC Limits RPD Limit Notes Prepared & Analyzed: 10/17/2019 0.020 mglL--�____—______ 0.010 mg/L Prepared & Analyzed: 10/17/2019 0.020 mg/L 0.010 mg/L Prepared & Analyzed: 10/17/2019 0.020 mg/L 0.248 99 85-115 0.010 mg/L 0.250 99 85-115 Prepared & Analyzed: 10/17/2019 0.020 mg/L 0.248 104 85-115 0.010 mg/L 0.250 104 85-115 _ .Prepared & Analyzed. 10/17/2019 0.020 mg/L 0.248 101 85 115 0.010 mg/L 0.250 101 85-115 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com F Page 5 of 9 " &)MICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9J0255 Spike Source %REC !I Metals Result RL Units Level Result %REC Limits Batch KJ90158 - Metals Aqueous - EPA 200.7 Rev 4.4 1994 LCS (KJ90158-BS4) -- Lead Zinc Duplicate (KJ90158-DUP1) Lead ,Zinc Duplicate (KJ90158-DUP2) 0.241 0.241 <0.010 0.013 0.020 0.010 Source: K9J0175-01 0.010 0.005 Source: KSJ0207-01 mg/L 0.248 97 mg/L 0.250 96 Prepared & Analyzed: 10/17/2019 mg/L NO mg/L 0.015 Prepared & Analyzed: 10/17/2019 85-115 85-115 Lead 0.021 0.010 mg/L 0.022 Zinc 0.955 0.005 mg/L 1.01 Duplicate (KJ90158-DUP3) Source: KSJ0252-01 Prepared & Analyzed: 10/17/2019 Lead <0.010 0.010 m IL NO Zinc 0.006 0.005 mg/L 0.006 Matrix Spike (KJ90158.MS1) Source: K9J0175-01 Prepared & Analyzed: 10/17/2019 _.7..._..... _.__._ .__..._....-.._ Lead _.__. . ______...._.. 0.226 _-_...._. __._.__.-. 0.010 mg/L 0.248 NO 91 70-130 Zinc 0.244 0.005 mg1L 0.250 0.015 91 70-130 Matrix Spike (KJ90158-MS2) Source: K9J0207-01 Prepared & Analyzed: 10/17/2019 Lead 0,257 0.010 mg/L 0.248 0.022 94 70-130 Zinc 1.16 0.005 mg/L 0.250 1.01 58 70-130 Matrix Spike (KJ90158-MS3) Source: K9J0252-01 Prepared & Analyzed: 10/17/2019 Lead 0.251 0.010 mg/L 0.248 NO 101 70-130 Zinc 0.253 0.005 mg/L 0.250 0.006 99 70-130 RPD RPD Limit Notes 10 17 10 4 10 6 10 10 9 10 _Matrix Spike Du_p(KJ90158-M_SD1) Source: K9J0175-01 Prepa_r_ed&Analyzed: 10/17/20_19 Lead 0.230 0.010 mg/L 0.248 NO 93 70-130 2 30 Zinc 11 0.247 0.005 mg/L 0.250 0.015 93 70-130 1 30 Matrix Spike Dup (KJ90158.MSD2) Source: K9J0207-01 Prepared & Analyzed: 10117/2019 Lead 0.259 0.010 mg/L 0.248 0.022 96 70-130 1 30 Zinc I) 1.18 0.005 mg/L 0.250 1.01 67 70-130 2 30 Matrix Spike Dup (KJ90158-MSD3) Source: K9J0252-01 Prepared & Analyzed: 10/17/2019 Lead 0.242 0.010 mg/L 0.248 NO 98 70-130 4 30 Zinc 0.244 0.005 mg/L 0.250 0.006 95 70-130 4 30 Reference (KJ90158-SRM1) Prepared & Analyzed: 10/17/2019 Lead 1.93 0.020 mg/L 2.00 96 95-105 Zinc 1.92 0.010 mg/L 2.00 96 95-105 KJ92922 - Metals Aqueous - EPA 200.7 Rev 4.4 1994 Blank (KJ92922-BLKI) Prepared &Analyzed: 10131/2019 Zinc <0010 0010 mglL LCS (KJ92922-BS1) Prepared & Analyzed: 10/31/2019 Zinc 0.264 0.010 mg/L 0.250 105 85-115 LCS (KJ92922-BS2) _ _ Prepared & Analyzed_ 10/31/2019 Zinc 0.259 0.010 mg/L 0.250 103 85-115 Duplicate(KJ92922-DUP1) Source: K9J0401-01 Prepared&Analyzed: 10/31/2019 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I w .microbac.com Page 6 Of 9 C�l VMICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9J0255 Spike Source %REC RPD Metals Result RL Units Level Result %REC Limits RPD Limit Notes 3atch KJ92922 - Metals Aqueous - EPA 200.7 Rev 4.4 1994 _Duplicate (KJ92922_DUP1) _ _ _ _ _ Source: K9_J0401-01 Prepared &Analyzed_10/31/2019 Zinc 0127 0.005 mg/L 0.129 1 10 Duplicate (K_J9_2.9_2_2-D_UP2) So_u_r_c_e_: _K9_J_0.425_-0_8 _ P_rep_are_d&_Analyzed: 10/_31_/_201_9_______________ 'Zinc 0.406 0.005 mg/L 0.387 - 5 10 Matrix Spike (KJ92922.MS1) Source: K9J0401-01 Prepared & Analyzed: 10/31/2019 Zinc 0.362 0.005 mg/L 0.250 0.129 93 70-130 Matrix Spike(KJ92922-MS2) Source: K9J0425-08 Prepared_&Analyzed: 10/31_/_2019 Z.._ --� - 0.646 _ _---- 0.005 mg/L 0.250 0.387 104 70-130 _ --_ -- ---_ 1 Matrix Spike Du_ p (KJ92922-MSDt) K9J0401-01 & Analyzed 10/31/2019 Zinc 0 377 ,Source: 0 005 _Prepared mg/L 0.250 � 0 129 99 70-130 4 30 Matrix Spike Dup (KJ92922 .MSD2)_ _ _ Source: K9J0425-08 Prepared & Analyzed_10/31/201.9_ 'Zinc 0.655 0.005 mg/L 0.250 0.387 107 70-130 1 30 Reference (KJ92922-SRMl) Prepared &Analyzed: 10131/2019 ,Zinc 2.11 0.010 mg/L 2.00 105 95-105 Batch Quality Control Summary: Microbac Laboratories Inc., - Marietta, OH Total Metals - ICP/MS Batch 1391(0191 - 200.8 W - EPA 200.8, Result Rv. 5.4 MDL RL Spike Source Units Level Result %REC %REC RPD Limits RPD Limit Notes Blank (B9K0191-BLK1) Prepared &Analyzed: 11/06/2019 ,Copper <0.001 0.001 0.002 mg/L LCS (B9K0191-BS1) Prepared & Analyzed: 11/06/2019 !Copper 0.160 0.001 0.002 mg/L 0.160 100 85-115 Duplicate(B9K0191-DUP1) _..._..._.___________.__.__...________._______.__.____...__.___.__._.____._._._.__.__.._..._..___.....-.. Source: M9K0122-01 Prepared&Analyzed: 11/06/2019 Copper 0.004 0.001 0.002 mg/L 0.005 3.12 20 Matrix Spike (B9K0191-MS1) Source: M9K0122-01 Prepared & Analyzed: 1110612019 Copper 0.169 0.001 0.002 mg/L 0.160 0.005 103 70-130 Matrix Spike (B9K0191-MS2) Source: M9K0136-05 Prepared & Analyzed: 11/06/2019 ,Copper 0.161 0.001 0.002 mg/L 0.160 0.001 100 70-130 Post Spike (B9K0191-PS`1) .... .. '. _ Source: M9K0131-01 . _ _... . Prepared & Analyzed: 11106/2019 __.._9... ..80._._ ...._._. _. ......... _. _. ... .. _. ._..___ _. .. .__. ,Copper 81.0 u IL 80.0 3.15 973 75125 Microbac Laboratories, Inc. �I 2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864,1920 p I www.microbac.com Page 7 of 9 *MICROBAC° Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS 'I K9J0255 Definitions B25: <1 Liter of sample analyzed ,I J: The result is an estimated quantity. The associated numerical value is the approximate concentration of the analyte in the sample. MDL: Minimum Detection Limit RL: Reporting Limit RPD: Relative Percent Difference Cooler Receipt Log Cooler ID: Default Cooler Temp: 3.2°C Cooler Inspection Checklist l Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody (CDC) Present? Yes '! CDC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match CDC (Name, Date & Time?) Yes Samples arrived within hold time? Yes Correct preservatives on CDC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes ;! VOAvials have zero headspace, or not reed'? Yes Project Requested Certification(s) y Microbac Laboratories Inc., - Marietta, OH 583 NC Dept. of the Environment and Natural Resources ii Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES I Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. 1� The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated Brittany Smith in the footnote are present and an authorized signature is included. Administration Reported: 11 /07/2019 23:31 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I w .microbac.com Page S Of 9 7 I (5)MICROBAC Microbac Fayetteville SHORT HOLDS ACCEPTED M( 'K9J6255 1600 2592 Hope Mills Rd. �pr7 pp„ppppt 88pp I OF CUSTODY RECORD Fayetteville, NC 28306 �ALI9�I��Itl81fl�9Qd l3lll�lllli er 1O8Ut0IlIIItIIN{IIIISIlm i SECTION TO BE COMPLETED BY M/CROBAC Lab Report Address Invoice Address Turnaround T I Client Name:j UTAS - Kidde Technologies [X] Routine (., _.. Upon Receipt ('C) 3. � Therm ID I Address:14200 Airport Drive I ] RUSH' (notify Wb) Holding Time, 1 City. State, Zip: Wilson, INC 27896 Need by Date: Samples Received on Ice? Yes No WA I Contact: Tim Femandez Report Type Custody Seals Intact? Yes No NIA Telephone No.: 252-293-72UZ Results Only I ] Level 1 [ ] Level [ ) Levei9 I ] Level [ ] EDD famawezOutas.wc.wm Send Invoice via: [ I Mail [ )Fax' [X) email liMoIh .femarlde utas.utC.com liem Name:+A6:AX6j UTAS - Kidde Technologies Address: 4200 Airport Drive city, state, Zip: W lson, NC 27896 Contact: Tim Fernandez Telephone No.: 252-293-7202I Send Report via: I I Mail I I Fax IXI email i mothv Project: Semi Annual Storm Water Sampi Locadon: lRAS4(14200 Ai rt Dr Wilson NC PO No.: Compliance Monitoring? p9 Yes [ I No (.Y] Agency/Program (ann,tw y Sampled by (Print): Tim Femandez Sampler's Phone a: $52-293-7202 Offite-0irecl NC 041 -Storm Wator Signature: Z �p sari al rmit NCG 030000 Matrix Types: So,USolid (S). Sludge. Oil, Wpe, Drinking'NOW ( W . G ov2t W), Surface Water (SW), Waste Water pvW). Other (specie " Preservative Types: (1) HNO3. (21 H2SO4, (3) HCI, (4) NaOH, (5) Zin tare..(6) Melhani, (7) Sodium Bisulfate. (8) Sodium Thiosuifate. (9) Hexane. (U) Unreserved - IDENTIFICATION OF SAMPLES REQUESTED ANALYSIS ADDITIONAL NOTES Data Time No. of. Grab preservative aS x,, Sample ID Collected Matrix or Collected Containers Comp type.. S u — o utfall # 1 Total Suspended Solids 10/16/2019 9:46 AM 1 Liquid G U x' Outfall # 1 Copper, Lead, Zinc 10116/2019 9:48 AM 1 [.quid G HNO3 x Outfall # 1 Oil 8 Grease 10/1612019 9:50 AM 2 Liquid! G 112904 Outfall It 2 Total Suspended Solids 1011612019 10:01 AM 1 Liquid G u x Outfall 02 Copper, Lead, Zinc 1011612019 10:04 AM 1 Liquid G HNO3 x Outfall # 2 Oil & Grease 1101162019 10:05 AM 2 liquid G H2SOx x ' I B mes will/ ma 3 g- Possible Hazard Identification: [ ] Hazardous p0 Non -Hazardous. [ I Radioactive Sample Disposition: [X] Huld 6 Dispose [ )Dispose as Appropriate [ ] Return I ] archive Special lnstructionslNotes Relin�ad 'gnat a Date/Time 30ekl !o %5f Reee' a By (signature) DatelTim Y 20t0k Rclin u' l e) DateRime y (signature) Dptb `V o b G-/ 0 Relinquished By (sig ure) DateMme Receiv y (signature) DatelTime Pane 1 n11 � rtv.12'2c'201] 0