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HomeMy WebLinkAboutNCG030531_MONITORING INFO_20200110/ 'vl 4 STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /v DOC TYPE ❑ HISTORICAL FILE ❑MONITORING REPORTS DOC DATE ❑ ��� U YYYYM M DD DOC TYPE 1 ❑ HISTORICAL FILE ❑ MONITORING REPORTS DOC DATE ❑ YYYYMMDD KINGS �� m Ill NVW9IANAVIr3NAL 1755 S. Battleground Avenue, Kings Mountain, NC 28086 USA Tel: 704-739-4227 • Fax: 704-739-4223 m www.kmiinc.net • email: kmil755@aol.com December 31, 2019 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 �Fr,F4�1�D 3AN I 0 2az CDE,ISECTJ(Ds Re: Request for Metals Exemption and Submission of December 2019 Semi -Annual Stormwater Discharge Monitoring Report Kings Mountain International, Inc. General Permit NCG030000 - Certificate of Coverage NCG030531 Dear Stormwater Permitting Unit: Attached please find one original and one copy of the Stormwater Discharge Monitoring Report for Kings Mountain International, Inc., under General Permit number NCG030000. This submission is for stormwater discharge sampling performed during the Tier 3 sample collected for the month of December 2019. Kings Mountain International, Inc. elects to employ the TTO sampling waiver. In compliance with the waiver, we provide the following signed certification statement on this discharge monitoring report. "Based on my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for Total Toxic Organics (TTO), I certify that to the best of my knowledge and belief, no leak, spill, or dumping of concentrated toxic organics into the stormwater or onto areas which are exposed to rainfall or stormwater runoff has occurred since the filing of the last discharge monitoring report. 1 further certify that this facility is implementing all the provisions of the Solvent Management Plan included in the Stormwater Pollution Prevention Plan." If you have any questions regarding this Stormwater Discharge Outfall (SDO) Monitoring Report, please contact me at your convenience. Sincerely, President of Operations International, Inc. Enclosures: Stormwater Discharge Monitoring Report, Qualitative Monitoring, Pace Analytical Report Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 12/31/19 CERTIFICATE OF COVERAGE NO. NCG030000 FACILITY NAME Kings Mountain Internaional, Inc. COUNTY Cleveland PERSON COLLECTING SAMPLES Bob Jafarkhani LABORATORY Pace Labs Lab Cert. # 12 & 40 Comments on sample collection or analysis: Don Jones Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly' DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply _]SA ®Other Stormwater PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 71 No dischoroe this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids PH Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss Benchmarks ===> - - 100 mg/L or 50 mg/O 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 5DO #00S 12/17/19 1.5" ND 6.9 .0031J ND .043 1.6J Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceeciance for the same parameter at the same ouiraii. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible fora waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management ;plan.into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." _bON /}-L ,O Name (Print name) (Signatu v�✓�s ,.9.3 I. (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format "<XX mg/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Non -polar O&G/TPH by EPA 1664(SGT-HEM) Total Suspended Solids pH Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/2S/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Zahid Khan Mail an oriainal and one copy of this DMR including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." is (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 1 EXTE Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https://de(i.nc.gov/about/divisions/energy-mineral-lancl- resources /energy-minera l-la nd- perm its /stonnwater- permits/ npdes- industria l-sw#tab-4 Permit No.: N/C/ G/ 0/ 3/ 0/ 0/ 0/ 0/ or Certificate of Coverage No.: Facility Name: Kings Mountain International, Inc County: Cleveland Phone No. 704-739-4227 Inspector: i Date of Inspection: 1� / 17 Z I � Time of Inspection:? • 3d Q • m q u Total Event Precipitation (inches): All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event' is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: re of Permittee or Designee) 1. Outfall Description: Outfall No. 005 Structure (pipe, ditch, etc.): Ditch Receiving Stream: Describe the industr1al activitiesthat oc r within the outfall drainage area: Pagel of 2 SWU-242, Last modified 07/28/2017 2. Color: Describe the color of the (light, medium, dark) as descriptors: L arge using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): AL as -e- 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids: CI 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 3 4 5 7. Is there any foam in the stormwater discharge? O Yes KNo. p 8. Is there an oil sheen in the stormwater discharge? O Yes jot No. id 9. Is there evidence of erosion or deposition at the outfall? O Yes $NO. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 1 SWU-242, Last modified 07/28/2017 ace Analytical www.pacNaba.com December 27, 2019 Donna Goins Kings Mountain International 1755 S Battleground Ave Kings Mountain, NC 28086 RE: Project: KMI Stormwater Pace Project No.: 92458013 Dear Donna Goins: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntemville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on December 18, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. A revised report is being submitted on 12/27/19 to include an additional comment about the sample ID, per client request. If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor Ezell taylor.ezell@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Mr Ivan Cooper, Kings Mountain International Don Jones, Kings Mountain International Ryan Wagenknight REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.L.C. Page 1 of 13 0 aceAnalytical wr .pccdeEs.com [*IA11yR7_vli[Q161 Project: KMI Stormwater Pace Project No.: 92458013 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville. NC 28078 (704)875-9092 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 LouisianalNELAP Certification # LA170028 FlondalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Flonda1NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 e lace Analytical wwx.pacelaWcam Project: KMI Stormwaler Pace Project No.: 92458013 Lab ID Sample ID 92458013001 SDO #005 SAMPLE SUMMARY Matrix Date Collected Date Received Water 12/17/19 07:30 12/18/19 10:20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 13 Pace Analytical Services, LLC laceAnalyticale 9800 KinceyAve. Suite 100 Huntersville, NC 28078078 ww pacelebs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: KMI Stormwater 92458013 Analyses Lab ID Sample ID Method Analysts Reported Laboratory 92458013001 SDO #005 EPA 1664B HH 1 PASI-C EPA 200.7 Rev 4.4 1994 DS 3 PASI-A SM 254OD-2011 CJL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 13 ace Analytical wrino,.pacelainixam ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: KMI Stormwater Pace Project No.: 92458013 Sample: SOO #005 Lab ID: 92458013001 Collected: 12/17/19 07:30 Received: 12/18/19 10:20 Matrix: Water Report Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Initial VolumefWeight: 1000 mL Final VolumefWeight: 1 mL Oil and Grease 1.6J mg/L 5.0 1.3 1 12/26/19 07:29 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Initial Volume/Weight: 15 mL Final Volume/Weight 15 mL Copper 0.0031J mg/L 0.0050 0.0021 1 12/20/1902:02 12/23/1917:15 7440-50-8 Lead NO mg/L 0.0050 0.0016 1 12/20/1902:02 12/2311917:15 7439-92-1 Zinc 0.043 mg/L 0.010 0.0039 1 12/20/1902:02 12/23/1917:15 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Initial Volume/Weight: 1000 mL Final Volume/Weight: 1000 mL Total Suspended Solids NO mg/L 2.5 2.5 1 12/23/19 18:06 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, Date: 12/2712019 03:36 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 ace Analytical rar.paalas.cem QUALITY CONTROL DATA Project: KMI Stormwater Pace Project No.: 92458013 QC Batch: 516669 Analysis Method: EPA 1664E OC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92458013001 METHOD BLANK: 2768017 Matrix: Water Associated Lab Samples: 92458013001 Blank Reporting Parameter Units Result Limit MDL Analyzed Oil and Grease mg/L ND 5.0 1.3 12/26/19 07:24 LABORATORY CONTROL SAMPLE: 2768018 Parameter I Units Oil and Grease mg/L MATRIX SPIKE SAMPLE: 2768019 Parameter Units Oil and Grease mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Spike LCS LCS % Rec Conc. Result %Rec Limits Qualifiers 40 37.1 93 78-114 92457268001 Spike ME MS %Rec Result Conc. Result %Rec Limits Qualifiers NO 40 38.3 90 78-114 Results presented on this page are In the units Indicated by the "Uhns" column exceptwhere an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2019 03:36 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 (�IaceAnalytical' www.paelebs.com QUALITY CONTROL DATA Project: KMI Stormwater Pace Project No.: 92458013 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 515915 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92458013001 METHOD BLANK: 2764607 Matrix: Water Associated Lab Samples: 92458013001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Copper mg/L ND 0.0050 0.0021 12/23/1915:56 Lead mg/L ND 0.0050 0.0016 12/23/1915:56 Zinc mg/L ND 0.010 0.0039 12/23/1915:56 LABORATORY CONTROL SAMPLE: 2764608 Spike LCS LCS e/ Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg/L 0.5 0.49 99 85-115 Lead mg/L 0.5 0.49 97 85-115 Zinc mg/L 0.5 0.46 92 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2764609 2764610 MS MSD 92457138001 Spike Spike MS MSD MS MSD e/ Rec Max Parameter Units Result Conc. Conc. Result Result % Rec e/ Rec Limits RPD RPD Qual Copper mg/L 15.6 ug/L 0.5 0.5 0.54 0.53 104 104 70-130 0 20 Lead mg/L NO 0.5 0.5 0.49 0.49 98 97 70-130 1 20 Zinc mg/L 29.1 ug/L 0.5 0.5 0.51 0.51 96 96 70-130 0 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2764611 MS 92457857003 Spike Parameter Units Result Conc. Copper mg/L ND 0.5 Lead mg/L ND 0.5 Zinc mg/L 15.9 ug/L 0.5 2764612 MSD Spike MS MSD MS MSD % Rec Max Conc. Result Result %Rec %Rec Limits RPD RPD Qual 0.5 0.52 0.52 104 104 70-130 0 20 0.5 0.51 0.51 101 101 70-130 0 20 0.5 0.50 0.50 98 98 70-130 0 20 Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2019 03:36 PM without the written consent of Pace Analytical Services, LLC, Page 7 of 13 (�IaceAnalytical' wwy.pecelebs.cam QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: KMI Stormwater Pace Project No.: 92458013 OC Batch: 516468 Analysis Method: SM 254OD-2011 OC Batch Method: SM 2540D-2011 Analysis Description: 25400 Total Suspended Solids Associated Lab Samples: 92458013001 METHOD BLANK: 2767250 Matrix: Water Associated Lab Samples: 92458013001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 2.5 12/23/19 17:59 LABORATORY CONTROL SAMPLE: 2767251 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 251 244 97 90-110 SAMPLE DUPLICATE: 2767252 92457943001 Cup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg/L 9.7 ND 25 SAMPLE DUPLICATE: 2767253 92457944002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg/L 92.9 89.3 4 25 Results presented on this page are In the units Indicated by the 'units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2019 03:36 PM without the written consent of Pace Analytical Services, L-C. Page 8 of 13 laceAnalytical www.bacelabi QUALIFIERS Project: KMI Stonnwater Pace Project No.: 92458013 DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. POL- Practical Ouantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(0) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) OUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2019 03:36 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 ace Analytical www.0acelabs.cam QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: KMI Stormwaler Pace Project No.: 92458013 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92458013001 SDO #005 EPA 1664E 516669 92458013001 SDO #005 EPA 200.7 Rev 4.4 1994 515915 EPA 200.7 Rev 4.4 1994 515943 92458013001 SDO #005 SM 2540D-2011 516468 Date: 12/27/2019 03:36 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproducer, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 13 "Nument'Name: Document Revised: February 7, 2018 �m Ie CandllU on Recel IsCUR'' Page oft OocumentNo.: Issuing Autltortty: dCb/(!l86�Ifa/e F-GIR-CS-03ga1ev.06 Pace Grollnas Ouallty Office Laboratory recelving samples: Asheville ❑ Eden[] Greenwood ❑ Hunters vllla Raleigh❑ MachanlcsvllleD Courier: ❑Fc ❑ Commercial Custody. Seal Present? ❑yes No Sealslnlaet? Pstejlaleds Posen, Examining Peeking Material: [-]Bubble Wrap ubble Bags ❑None ❑ -0tker ° Biological Tissue Froten? ❑Yes., ❑No�]N%A Thermometer:,- Gun 10: 9=58 TYPa pile. et []BlueONdnt Cooler Temp ('Cj: ;� - Y Correction Factor: Add/Subtrut CC) 0.0T - /I Temp should be above freezing to 6'C Cooler Temp Corrected ('C): a'r ❑Sampler out ofIt* erltcon. Samples an ice, c➢oling process haibegun USDA Regulated Sall N/A, water Sample) DIdsamples originate, a quarantine zone within the United States: CA; NY, or SC_(check maps)? Old saryplescrlglnate from a foreign source llrnarnatlonsay, I�Nes Nn Inrludkr Howell and PueAn Almis hlvx Mm. ' Commentsiourre anc . Chain of Cut to V Present?. Yen Oft EINIA 3. Samples Arrived within Hold Timer Ya: ❑No NA 2. Short Hold Time Ana' 1s c72 hr, ? r1yes o N A 3. Rush Turn Amunlie Tine Rapuestedi ves; o N/A 6. . Sufficient Volume? `u. No N/A S. Carted Containers Used? Pace Containers Used? Yet []NO ONO QN/A MNIA 6, Containers Intact? Z Yes Oft N A 7• Dlssolvad roil dr: Samples Field Flitered] Sample lanais Match COq .Inciudes date me ID Anal sits matrix: Mies Qvia o_ PQN/A N/A 8: 9:t�UeS Headsaceln VDAVlals>5.6mmR Ym ONO a 1 10.. Trip Blank Fiesent? Trio Blank CustodySeale Present? UYes Yri QNo No n/A Meld Data Requhed? (,J:'es ONO Person contacted: _ _ _ _ Date/11me: ,Project Manager SCURF Review: -102) .Project Manager SRF Review: it V . Date: I z/i9 q -0ete: I Z::,21 I Page 11 of 1: Document Name: Document Revised: February 7, 2018 aceAnai Ical� _ in Sam le Condition Up" "Recol SCUR Page 1 of 2 .Document No.: Issuing Authority: / RCAR•CS-033•Row06 Pace Carollms Quality Office *Check mark top half of box If pH and/or dachlorinatlon is verified and within the acceptance range for preservation samples. Exceptions: VOA, Colifcrm, TOC, Oil and Grease, DRO/Sol$ (water) DOC, LLHS "Bottom half of box is to list number of bottle Y �0■■� aon MEN on MOMMONNE MIMI HIMMMOBEIN logo Emmons IS MEN MOMEMENINE Sample to Type of Prose rvalive pH upon retalm Data preservation adjusted Time preaaNstion'i, adjusted Amount of Preservative added Lot Note: Wheneverthere is a discrepancy effecting North Caroline Compliance samples, I COPY Of lhla form will el lent to the North Carolina OEHNR Unification Office (Le: Out of hold, Incorrect praservaeve, out of tamp. incorrect comolnert. Page 12 of 13 ceAnglytjcat CHAIN -OF -CUSTODY I Analytical Request Dodument TM IT.inaltu y is a LEGAL DOCUMENT. V rek aq f9ft mal Ge conVaW acprmety- SectIoa A Suction B �t. C , SP,.WA E-I.: R.Q� dart �a. R..,� lNmre i 1, oc. .9atmlim: C� Kings MwnWin Intemational Rq To: 0. Jones Deena Gaim 1755 SWh Batftgr nd Ave. C.P7T-. lcoopwgced..com Name: IGngsMDlmIainInwmtbn@Ijm C.. VLX�MN�' "i oaiimliin4oc kiiu i 'm4ip UmeLvW. NC 28086 dwQkmihfG F. NPDES r-. GR04NDWATER LIST r. RCR). r- DRNKMG WATER f-I OTHER Emil T.: donna@kmurwnet 70M7394227 F. PmJw KMI Stomwaler TavIwEzeU M R.p� �AT. 3729-2 ArvalyB19'Fillaivid (YJNQ" -5,;i VSid MaYu c.a.s Z COLLECTED 1191 WT p SAMPLE ID o SargMIDS WSTAVUNKIUE X 0 -e 1q.9 C- C5 1 6 o P. mo/L 2 DATE TIME x PME 3F m m 02 z z 20 b I D SIDO 0005 OT G 'I Ix I I I I I I I I xI I I It ,.!,2� g 'SDO 9005 OrI-izl I x x x x 'SDO #005 or G Z47-40 7-?oq IL I x NOR !"!III' '.ohAIIHlwf" 'U'" &ixm fflilr"'mAl. SAMPLE�M� 14474 2- 6- �02,'D — -3S 'PACE .2-1 AJ y 3z: 1 Avo F-ALL-Q-Mmv.07. 16-Feb2007 aceAnalXical'- ...•..caoaa•a. mm CHAIN -OF -CUSTODY / Analytical Request Document The Chain-06Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. I Section A Section B Section C Page: of Required Client Information: Required ProjeT,t Information: Invoke Information: Company: Kings Mountain International Report To: Don Jones Attention: Donna Gains Address: 1755 South Battleground Ave. eg Copy To icwper@cecinc.com @ Company Name. Kings Mountain International, Inc - •r. t *+ 1 rU5 i + •� - REGULATORY�AGENCY.��r Cleveland, INC 28086 don@kmiinc.nel Address: W. NPOES r: GROUNDWATER r; DRINKING WATER Cm UST 17; RCRA r OTHER Email To: donna@kmIIDC.Det Purchase Order No.: Paw Onom R.Tfamnm: Phone: 704-739-4227 Fax: Protect Name: KMI Stormwater Pa Pml0C1 Taylor Ezell Site Location z e!' STATE: INC - Requested ore oateRAT: Project Number P Pmrle a. - 3729-2 '-'Requested' Analysis. 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