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HomeMy WebLinkAboutNCG030466_MONITORING INFO_20191120STORMWATER DIVISION CODING SHEET NCG PERMITS PER NO. �v C� 0-) DOC TYPE. ❑ HISTORICAL FILE t5-MONITORING REPORTS DOC DATE ❑ YYYYMMDD Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. N0003 0 L_I 6 6 FACILITYNAME FAT(1N coQPoRgTroN COUNTY PERSON COLLECTING SAMPLES U r LABORATORYPALi: ANALyrfI A L. Lab Cert. # o Comments on sample collection or analysis: tv A Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2-6 19 SAMPLE PERIOD ❑ Jan -June �Dly-Dec or ❑ Monthly' (month) DISCFPP�NGR'f1,5� ORW ❑HQW ❑Trout ❑PNA (( r ❑Zero -flow ❑Water Supply USA NOV 2 2019 ❑other CEPLEitS S BER TO SIGN ON PAGES 2 AND/OR 3 4 DWRS ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids PH Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss Benchmarks - - 100 mg/L or 50 mg/O 6.0 - 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141 001 to go Ito 19 I.11 11 IL 6,39 0-0052 �J IL 40•00 S.JIL 0•o 619•011- 4,1-I•E-;Ic Nh 00 Z 10 30 .201'7 " 3 • 2 erb I 7•o 3 c o•ooi AVJIC. 44•005 IV It 0.02 .-)IL c 4•ff � lL rvA OD � 7" ,2. 6 6 -43 1.0.005.y1L ce•ooSAVIL 0•o284-JIL_ cIf. S 4- 1L NA o0 Lq l0 ISO ,201 -) L. • 0 1 L 0,00 1. o•o o341«•l e- M•r 'x^ It. 1vR Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outiali. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. "See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) E HS Mateo e,r� Title (Print title) Signature — Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n Ain rlicrhnrno Chic norinr ;)2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 CO530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/l/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal copv of this DMR. including all "No Discharae" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 0.0 Signature of Permittee 11 1-2. 2oi9, Date Permit Date: 11/1/2018-05/31/2021 -- - -- -- -_._ SWU-245, last revised 11/1/2018 ----- ....------ .. -- - -- - - - - - - - ------- - -- _- -'Page-3 of 3 i aceAnalytical www.pecela6s.com November 08, 2019 Mark Buda Eaton 221 Heywood Rd. Arden. NC 28704 RE: Project: STORMWATER 10302019 Pace Project No.: 92451690 Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 Dear Mark Buda: Enclosed are the analytical results for sample(s) received by the laboratory on October 30, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures cc: Mark Buda, Eaton Corporation REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 aceAnalytical w ..pacelabscom Project: STORMWATER 10302019 Pace Project No.: 92451690 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLO, Page 2 of 14 aceAnalytical w ..pacelabscam SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: STORMWATER 10302019 Pace Project No.: 92451690 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92451690001 OUT 001 EPA 1664B AAC1 1 PASI-C EPA 200.7 Rev 4.41994 SHt 3 PASI-A SM 2540D-2011 JP1 1 PASI-A 92451690002 OUT 002 EPA 1664B AAC1 1 PASI-C EPA 200.7 Rev 4.41994 SH1 3 PASI-A SM 254OD-2011 JP1 1 PASI-A 92451690003 OUT 003 EPA 1664B AACt 1 PASI-C EPA 200.7 Rev 4.41994 SH1 3 PASI-A SM 2540D-2011 JP1 1 PASI-A 92451690004 OUT 004 EPA 1664B AAC1 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 254OD-2011 JP1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 aceAnalytical ' wwwpacela6s.com ANALYTICAL RESULTS Project: STORMWATER 10302019 Pace Project No.: 92451690 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: OUT 001 Lab ID: 92451690001 Collected: 10/30/19 13:30 Received: 10/30/19 16:02 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] HEM, Oil and Grease Oil and Grease 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids Analytical Method: EPA 1664E NO mg/L 4.8 1 11/07/1910:00 Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 6.8 ug/L 5.0 1 10/31/19 23:17 11/07/19 01:06 7440-50-8 NO ug/L 5.0 1 10/31/19 23:17 11/07/19 01:06 7439-92-1 61.9 ug/L 10.0 1 10/31/19 23:17 11/07/19 01:06 7440-66-6 Analytical Method: SM 2540D-2011 17.5 mg/L 6.3 1 11/04/19 23:03 Sample: OUT 002 Lab ID: 92451690002 Collected: 10/30/19 13:30 Received: 10/30/19 16:02 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Oil and Grease 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids Analytical Method: EPA 1664B ND mg/L 4.8 1 11/07/19 10:00 Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 ND ug/L 5.0 1 10/31/19 23:17 11/07/19 01:09 7440-50-8 ND ug/L 5.0 1 10/31/19 23:17 11/07/19 01:09 7439-92-1 20.0 ug/L 10.0 1 10/31/19 23:17 11/07/19 01:09 7440-66-6 Analytical Method: SM 254OD-2011 3.2 mg/L 2.5 1 11/04/1923:04 Sample: OUT 003 Lab ID: 92451690003 Collected: 10/30/19 13:30 Received: 10/30/19 16:02 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Oil and Grease 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids Date: 11/08/2019 03:41 PM Analytical Method: EPA 1664B NO mg/L 4.8 1 11/07/1910:00 Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 ND ug/L 5.0 1 10/31/19 23:17 11/07/19 01:12 7440-50-8 NO ug/L 5.0 1 10/31/19 23:17 11/07/19 01:12 7439-92-1 28.4 ug/L 10.0 1 10/31/19 23:17 11/07/19 01:12 7440-66-6 Analytical Method: SM 254OD-2011 2.6 mg/L 2.5 1 11/0411923:05 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 14 acleAnalyfical wwwpacelabs.crom ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: STORMWATER 10302019 Pace Project No.: 92451690 Sample: OUT 004 Lab ID: 92451690004 Collected: 10/30/19 13:30 Received: 10/30/19 16:02 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 4.8 1 11/07/19 10:00 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper ND ug/L 5.0 1 10/31/1923*17 11/07/1901:21 7440-50-8 Lead ND ug/L 5.0 1 10/31/1923:17 11/07/1901:21 7439-92-1 Zinc 34.2 ug/L 10.0 1 10/31/19 23:17 11/07/19 01:21 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 3.6 mg/L 2.5 1 11/04/19 23:05 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/08/2019 03:41 PM without the written consent of Pace Analytical Services LLC. Page 5 of 14 aceAnalytical wmvpecelabs com QUALITY CONTROL DATA Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: STORMWATER 10302019 Pace Project No.: 92451690 QC Batch: 508174 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92451690001, 92451690002, 92451690003, 92451690004 METHOD BLANK: 2727919 Matrix: Water Associated Lab Samples: 92451690001, 92451690002. 92451690003, 92451690004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 4.8 11/07/19 10:00 LABORATORY CONTROL SAMPLE: 2727920 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Oil and Grease mg/L 38.5 32.2 84 78-114 MATRIX SPIKE SAMPLE: 2727921 92451190001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 14.7 36 78-114 J(MI) Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/08/2019 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 aceAnalytical xxigv➢acelabs.coon QUALITY CONTROL DATA Project: STORMWATER 10302019 Pace Project No.: 92451690 QC Batch: 507063 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92451690001, 92451690002, 92451690003, 92451690004 METHOD BLANK: 2722680 Matrix: Water Associated Lab Samples: 92451690001, 92451690002, 92451690003, 92451690004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L NO 5.0 11/06/1923:44 Lead ug/L NO 5.0 11/06/1923:44 l Zinc ug/L NO 10.0 11/06/1923:44 Pace Ana lyticaI Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 2722681 Spike LCS LCS % Rec Parameter Units Conic. Result % Rec Limits Qualifiers Copper ug/L 500 480 96 85-115 Lead ug/L 500 472 94 85-115 Zinc ug/L 500 462 92 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2722682 2722683 MS MSD 92451277004 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conic. Conc. Result Result %Rec %Rec Limits RPD Qual Copper ug/L 296 500 500 777 808 96 102 70-130 4 Lead ug/L 108 500 500 564 575 91 93 70-130 2 Zinc ug/L 3020 500 500 3170 3220 29 40 70-130 2 J(M1) I' MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2722684 2722685 MS MSD i' 92451659002 Spike Spike MS MSD MS MSD e/ Rec Parameter Units Result Conc Conc. Result Result e/ Rec %Rec Limits RPD Qual Copper ug/L NO 500 500 479 487 96 97 70-130 2 Lead u9/1- ND 500 500 463 471 92 94 70-130 2 Zinc ug/L NO 500 500 460 468 92 93 70-130 2 Results presented on this page arc in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 11 /08/2019 03:41 PM without the written consent of Pace Analytical Services, L-C. Page 7 of 14 5OAnalytical wwwpacelabs com QUALITY CONTROL DATA Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: STORMWATER 10302019 Pace Project No.: 92451690 QC Batch: 507558 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92451690001, 92451690002, 92451690003, 92451690004 METHOD BLANK: 2724891 Matrix: Water Associated Lab Samples: 92451690001,92451690002,92451690003,92451690004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 11/04/19 23:01 LABORATORY CONTROL SAMPLE & LCSD: 2724892 2724899 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc, Result Result % Rec % Rec Limits RED RPD Qualifiers Total Suspended Solids mg/L 250 240 238 96 95 90-110 1 25 SAMPLE DUPLICATE: 2724900 92451703001 Cup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 229 186 21 Results presented on this page are in the units Indicated by the "Units" column except where au alternate unit is presenter) to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/08/2019 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 I j. aceAnalytica1 w pacelabs.com Project: Pace Project No.: i, DEFINITIONS STORMWATER 10302019 92451690 QUALIFIERS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count MDL-Adjusted Method Detection Limit. POL- Practical Quantilation Limit. RL - Reporting Limit -The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitnle by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS J(M1) Estimated Value. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) 'I recovery. 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/08/2019 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 aceAnalytical wwwpacelaDs.corn QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Pace Project 140: STORMWATER 10302019 92451690 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92451690001 OUT 001 EPA 1664E 508174 92451690002 OUT 002 EPA 1664B 508174 92451690003 OUT 003 EPA 1664E 508174 92451690004 OUT 004 EPA 1664B 508174 92451690001 OUT 001 EPA 200.7 Rev 4.4 1994 507063 EPA 200.7 Rev 4.4 1994 507076 92451690002 OUT 002 EPA 200.7 Rev 4A 1994 507063 EPA 200.7 Rev 4.4 1994 507076 92451690003 OUT 003 EPA 200.7 Rev 4.4 1994 507063 EPA 200.7 Rev 4.4 1994 507076 92451690004 OUT 004 EPA 200.7 Rev 4.4 1994 507063 EPA 200.7 Rev 4.4 1994 507076 92451690001 OUT 001 SM 2540D-2011 507558 92451690002 OUT 002 SM 2540D-2011 507558 92451690003 OUT 003 SM 2540D-2011 507558 92451690004 OUT 004 SM 254OD-2011 507558 Date: 11/08/2019 03:41 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 10 of 14 Document Name: Document Revised: February 7, 2018 Sample Condition.Upon Receipt(SCUR) Page 1 of2 ACeilnalXICc7( DocumentNo.: Issuing Authority`: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving sa ples: Ashevill& Eden❑ Greenwood Huntersville❑ Raleigh[] Mechanicsville❑ Client Name: W®# 92451690 Courier: ❑Fed Ex ❑UPS CUSPS / noject #; I IIVII� IOl IIII�I��II �II ❑te Commercial -Spa//'W/jJ�DI%R ❑Other L92451 Custody Seal Present? ❑Yes "EINo Seals Intact? Des r[i]No Date/Initials Person Examining Contents: Packing Material: ❑Bubble Wrap `❑Bubble Bags ❑None ❑ Other Biological Tissue F7zen? Thermomet _ [:]yes❑No�N/A ��rr 93TO6� Type of Ice: c❑V�t ❑Blue ❑FIPna �]IR Gun ID: r1 D Cooler Temp (-C): Ia l Correction Factor: Add/Subtract ('C) Temp should be above freezing to VC , Looter Temp Corrected('Q; ❑Samples out of temp,criteria, Samples on ice, cooling process has hegun USDA Regulated Soil t NN/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, q'r Sc (check maps)?. Did samples originate from a foreign source (Internationally, W--ii and Puerto Rico)?nYes ONO IJYes tJNO -- - Co m m ents/Discrepa ncY: Chain of Custody Present? Yes []NO ❑H/A 1. Samples Arrived within Hold Time? LD es []NO ❑N/A 2: Short Hold Time Analysis(472 hr.)? Ejyes_ ❑N/A 3. Rush Turn Around Time Requested? ❑ Ye ,fJo A ❑N/A I 4. I fl q %A' Sufficient Volume? Yes ❑No ❑N/A 5. Correct Containers' Used? -Pace Containers Used? XYed ,.QYes ❑No❑N/A ❑No ❑N/A '6. Containers Intact? yes ❑No ❑N/A 7. Dissolved analysis: Samples Field Filtered? Sample Labels Match COO -Includes Date/Time/ID/Analysis Matrix: Headspace In VOAVials (>5-6mm)? ❑Yes JDIrs ❑Yes ❑No ON. ❑NP ON/A ❑N/A N/A 8. 9. 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑yes ❑Yes [:]NO ❑N/A ..4DK/A 11. COMMENTS/SAMPLE DISCREPANCY I t CLIENT NOTIFICATION/RESOLUTION i Person contacted: I Project Manager SCURF Review: I Project Manager SRF Review: Date/Time: Date: Date: Field Data Required? VYes`,IJNo Page 11 of 14 �` i �..Pa`ce�nallAlCal �" Document Name: Sample Condition Upon Receipt(SCUR) Document Revised: February 7, 2018 Page 1 of 2 Document No.: F-CAR-CS-033-Rev.06 Issuing Authority: Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottle Project; W®# : 92451690 PM: CDl Due Date: 11/13/19 CLIENT: 93—CutlerH E L _ z E C L m z o M 6 to z c o N p m z n _ u = 6 m _ ~ 6 m N z o z 4 m z a C E N O to ry O E V 6 m n a LL 3 V n J E v ti a S .ZY a z ° J E E a o M a O 2 a E a _v H a = EE a E ¢ u E a o r m a a z a O E O=1 o O a O > E !- > z 0 0 E D > a 0 0 E o o `v n > a, n > n E h z m w E ai 0 i A a E an `to _ a w E a of Oti a c E ON > a v ii E E V o 1 I 2 I l 3 4 l 5 6 7 i 8 9 10 11 12 pH Adjustment Log for Preserved Samples Sample le Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot It Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEN NR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 12 of 14 .� -PaceAnalytical' .n.e: wm CHAIN -OF -CUSTODY / Analytical<Request Document The Chainof-Custody Is a LEGALDOCUMENT. All relevant fields must be completed accurately. `o c Page, of Section A Section B Section C 2 Required Client Information: Required Project Information: :Invoice Information: 2O ILJ•Li..,J O Company: Roped To: _ Attention:. G 0- rY�� Mw-11 (<MRIn ESN Ch ATAVT Address: Copy To:. Company Name: REGULATORY�AGENCY' u!G ev .I 70 4 Address: r NP.DES r GROUNDWATER r- DRINKING WATER (- UST r' RCRA r OTHER Email To: Purchase Order No.: - Pace DWlp - - ICiia n Rala,emw Phone: Fax: Project Name: Paw Pmjon Site Location 1• D P S Sia'+r' wA4k.✓ G o O Was,.c STATE: Requestdd Due DalelrAT: f I 7 Project Number: Putt P,ONe e: Requested Analysis Filtered (YIN) Seedon D Morris Codes, - - Regw.oaclicmwemrallen MATRIX f CODE - COLLECTED Preservatives ->' Drinhpy Wae:r. DW = 0 Q Water WT 8 U Wows Wme. We, a «ws,re siun corrovre D+wr.,wl w z Prptluct P. Y SOi2col SL o O O to SAMPLE ID al OL ie a. u Wpd NP '(A-Z. 0.9I:) Air AR, o. - c z. Sample lDS MUST BE UNIQUE Tissue TS O to Omer OT .0 x T.AT.TIMIw w z O ,2 m p c = J N u ,Q' J 'n O L d [' N W O 0S. F Q ~ mTI.TITIMI = 7 : 2 S Z Z O PdC¢ Project No./ Lab I.D. ool le . 1:S6p. 0 ) z aul 0o 61 I: o .. -1 t' 1 -- O Z <OA4 00k Io p R r d„ 3 A I I n 5 6 .8 9 +0 1i 12 ADDITIONAL COMMENTS RELINQUISHED BY/AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION .DATE' TIME SAMPLE CONDITIONS 1)01 PH3 S L 2 -03 00 a.qi 00. . 1.01 SAMPLER NAME AND SIGNATURE O o_ ORIGINAL az PRINT Name of SAMPLER: E o n o ~ u - o} o i SIGNATURE OI SAMPLER: DATE Signed (MMIDDIYYh --' -' .eimlmam sow: er sy. J Iwm yuu om acmprnn Pnces NEnao oar P: Peom lemn one m,eoin I la4 mer o oFls% - -n; tar on-mwicea �dl oaie wiu:u ao ea-- -- - -' -- F=ALL-0-020rev.07.+5-Ma 2007-- Y- _ PaceAnalytical- a .aa[ela0o.com CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. Ail relevant Fields must oe completed accurately. Q m a Section A Section B Section C Papa: of Roqulr Client Information: id Required Project Information Invoice Information: � Company: - Report To Attention: [) -75 0 6 {yy Address: Copy To: Company Name: REGULATORY AGENCY Address: (- NPDES r GROUNDWATER (- DRINKING WATER Email To: Purchase Order No.: Pa¢• pwr Ralorancay UST (' RCRA OTHER Phone: Fax: Protect Name- - Site Location Rogcooled Duo DmOTFAT: - /�/ Project NUmGec Pox Prolile a. STATE: Requested Analysis Filtered (YIN) section D Mount Codos - _ RNufludcrentlmormat.en MATRIX I CODE - c- COLLECTED Preservatives i odM.o-q wawr ow - C Water WT 8 wawr 1vw Product Product P w.Posne ..r^vi sme [rorciue \ .. SoivsoGd sL Z SAMPLE ID Ou oL _ Wipe WP — W w (Ad. Alt AR W Q C S BE Sample IDs MUST BE UNIQUE Tissue TS O a t _ Other OT U r z 2 y= L)0 f x_ m W a ].T]TIMEve U re y in -- o. m O O V L re r a ~ a wr j I 2 i DATE TIME a Z Z Z 0 H IV x Pace Project Nod Lab I.D. �,' z dr :'1 (J _ i p 3 5 6 T e 9 0 11 12 DATE TIME ACCEPTED BY/AFFILIATION DATE TIME SAMPLE CONDITIONS 5=RELINQUISHED SAMPLER NAME AND SIGNATURE V m _ PRINT Name of SAMPLER: - � r B U Y vY SIGNATURE of SAMPLER: DATE Sigrptl V IMMI.WYY): --__,.-,._.........._.......:........::.....�::��:�e�.:�:r �,:,,a,a: aoi naia w�m:n uu u, s. y - - rev. - aY-200