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HomeMy WebLinkAboutNCG030450_MONITORING INFO_20191105STORMWATER DIPIERMITS SION CODING SHEET: NCG PERMIT NO. IV C,& b�)10950 DOC TYPE. ❑ HISTORICAL FILE MONITORING REPORTS DOC DATE ❑ YYYYMMDD ® Electrolux October 29, 2019 Attn: Central Files 1 , Division of Water Resources (DAQ) 1617 Mail Service Center N11 Os Raleigh, NC 27699-1617 C 2019 �WR EC-r DES RE: Electrolux Storm Water Sampling Event (Year 1 -Period 2) jON 'ro Whom It May Concern: Attached to this cover letter please find the analytical results of sampling from a storm event on 10/16/2019 to comply with our NPD> S General Permit No. NCG030000. As you will see, the results from our storm water outfall #1 (Outlet) indicate compliance with our NPDES General Permit NCG030000 and Certificate of Coverage NCG030450 for I3lectrolux Home Products, Kinston, NC. By submitting this data we have met the monitoring requirements for Year 1 (2019) Period 2 of our permit. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. If you have any questions or require additional information feel free to call me at (252) 933-9547. Sincerely, 1 4 /:Z J wn Manufacturing Engineering/Maintenance Manager/ Environmental Coordinator Glenda Lynch Plant Manager ELECTROLUX HOME PRODUCTS NORTH AMERICA MAILING ADDRESS TELEPHONE SITE 4850 W. Vemon Avenue 252 527 5100 _ vmv,frigidaire.com Kinston, NC 28504-7544 vmv.electrolux.com USA -- : g :...: _ e rarvan W vmt..� QSW ..m.,..,. '!R �.U=®rna eixrAw. e��a. me wwias r� i wFe Electrolux h STORMWATGR DISCHARGE MONITORING REPORT & RESULTS ELECTROLUX HOME PRODUCTS NORTH AMERICA MAILING ADDRESS TELEPHONE SITE 4850 W. Vemon Avenue 252 527 5100 vmv.frigoaire.com Kinston, NC 28504-7544 w .electrolux.com USA i c�-..._g-a :•� rwPvwn yywu..wmu�y,o,.. Gihsan .rt..a....:o�� �"� ®rnoeiwnmw cm�p. me wone: Na.i cwrce Stormwater Discharge Monitoring Report - for. North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. N/ICG03 D FACILITY NAME COUNTY L4N " PERSON COLLECTING SAMPLES sV1A2k l�o� nassC,r�`,^G� 1A6s) LABORATORY yntc.10 6, - LA,6s Lab Cert. q mr n .,?' $k- 11 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR SAMPLE PERIOD ❑ Jan -June July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA [_]Zero -flow ❑Water Supply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -91 ❑ No discharge this period?z Outfall No. Date Sample P Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids P H Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss Benchmarks _ - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Lode - 46529 C0530 00400 01119 01051 01094 00552 78141 �oµ�l0 to IG 11 0.11 < ,I% 6.3 <0.009 <0.0t0 I 6.01(Z <5,00 F} ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition fo.und in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TT0), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." /Y1 Ike $rvwn Name (Print name) %11RY1N tCLr1rN L/HS rL�r `In�Cfi'/HC MAARs gt_ Title(Print �i 7 Signature Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' New Motor Oil or Hydraulic Oil Usage Non -Polar 0&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee /v a Da Permit Date:11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 3 of 3 ® Electrolux STORMWATER QUALITATIVE MONITORING REPORTS (Upstream and Downstream) ELECTROLUX HOME PRODUCTS NORTH AMERICA MAILING ADDRESS TELEPHONE SITE 4850 W. Vernon Avenue 252 527 5100 www.fdgidaire.00m Kinston, NC 28504-7544 www.electrolux.com USA �F-"B'"'":." rwrPwrs Wvm.wearo�.. Gihsan ,,:.,,r,.......� �uia ®rne rie«�iw cm�o-'ma,wnes nai cmice i III Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https:Hdeq.nc.gov/about/divisions/energy-mineral-land-resources/ npdes-s totmwater-gp s Permit No.: N/C/ 6/ o /3 / O / o/o /o / or Certificate of Coverage No.: N/C/G/ o / 3 / o / ft /5 /,o l Facility Name: C1ee4R.oiwe ffzi��rooiw s County: Lpnotrl_ Phone No. 25z— Inspector: Date of Ins Time of Inspection: / O : / 5 9n Total Event Precipitation (inches): 0.19 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permiace is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DLMLR Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. 1 Structure (pipe, ditch, etc.): D, Receiving Stream: / 'P1+c1, or Describe the industrial activities that occur within the outfall drainage area: I�1q»aF.u�....r.% J ef= drs�w�s/fet s Page I of 2 SWU-242, Last modified 06/01/2018 2. Color: Describe the color of the (light, medium, dark) as descriptors: using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): /I oit r- 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 0 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no^solids and 5 is the surface covered with floating solids: ' 11 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: n 2 3 4 5 7. is there any foam in the stormwater discharge? Q Yes 4D No. 8. Is there an oil sheen in the stormwater discharge? QYes o No. 9. Is there evidence of erosion or deposition at the outfall? Q Yes 4*No. N O 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant: exposure. 'these conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 06/O1/2018 ® Electrolux LABORATORY ANALYTICAL RESULTs (with Chain of Custody) ELECTROLUX HOME PRODUCTS NORTH AMERICA MAILING ADDRESS TELEPHONE SITE 4850 W. Vernon Avenue 252 527 5100 mmv.fdgidaire.com Kinston, NC 28504-7544 mmv.electrolux.com USA TNPYNII WWNYwmuipnmiu Gibson ✓+m:..o �ulw ® no Elmrmlw Group. Pwwotlds No. 1 choce & 1M ICROBAC° Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9J0254 Project Description No Project For: Mr. Mike Brown Electrolux Home Products North 4850 W. Vernon Avenue Kinston, NC 28504 Administration Brittany Smith Monday, October 28, 2019 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of ,your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. All results for soil "samples are reported on a'dry-weight' basis unless specified otherwise. Analytical results for water and wastes are reported on a'as received' basis unless specified otherwise. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 i 910.864.1920 p i www.microbac.com Page 1 of 10 6>MICROBACS, Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9J0254 Electrolux Home Products North Mr. Mike Brown 4850 W.Vernon Avenue I, Kinston, NC 28504 Sample Summary Report Sample Name Laboratory ID Client Matrix Outfall 1 Inlet, grab K9J0254-01 Stormwater Outfall 2 Outlet, grab K9J0254-02 Aqueous Project Name: No Project Project / PO Number: N/A Received: 10/16/2019 Reported: 10/28/2019 Sample Type Sample Begin Sample Taken Lab Received Grab 10/16/19 09:52 10/16/19 14:20 Grab 10/16/19 10:15 10/16/19 14:20 Page 2 of 10 6)MICROBAC® Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9J0254 Analytical Testing Parameters Client Sample ID: Outfall 1 Inlet, grab Sample Matrix: Stormwater Collected By: Poythress Lab Sample ID: K9J0254-01 Collection Date: 10/16/2019 9:52 Wet Chemistry Result RL Units Dilution Note Prepared Analyzed Analyst EPA 1664 Rev. B Oil & Grease (SGT-HEM) <5.00 5.00 mg/L 1 10/24/19 1141 Tam SM 2540 D-2011 Total Suspended Solids <4.17 4.17 mg/L 1 10/17/19 1005 CLB Metals Result RL Units Dilution Note Prepared Analyzed Analyst :'Metals Aqueous/EPA 200.7 Rev 4.4 1994 Lead <0.010 0.010 mg/L 1 10/17/19 1351 10/17/19 1351 TAB Zino 0.007 0,005 mg/L 1 10/17/19 1351 10/17/19 1351 TAB I Field Sampling/Testing Result RL Units Dilution Note Prepared Analyzed Analyst Rainfall Field Observation Color Odor Clarity Floating Solids Suspended Solids (Residue, Non -Filterable) Foam ilOil Sheen Erosion Evidence Other Pollution Indicators SM 2550 B-2010 ,Temperature, Field SM 4500 H+B-2011 1 pH, Field Test Total Metals - ICP EPA 200.7, Rv. 4.4 Copper 0.19 inches 1 10/24/19 2043 10/24/19 2105 BNS Clear 1 10/24/19 2043 10/24/19 2105 BNS None 1 10/24/19 2043 10/24/19 2105 BNS Yes 1 10/24/19 2043 10/24/19 2105 BNS None 1 10/24/19 2043 10/24/19 2105 BNS None 1 10/24/19 2043 10/24/19 2105 BNS None 1 10/24/19 2043 10/24/19 2105 BNS None 1 10/24/19 2043 10/24/19 2105 BNS None 1 10/24/19 2043 10/24/19 2105 BNS None 1 10/24/19 2043 10/24M9 2105 BNS 22 0.1 C 1 6.1 1.0 pH Units 1 Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH Result RL Units Dilution Note 10/16/19 0952 JMP 10/16/19 0952 JMP Analyst <0.00800 0.00800 mg/L 1 Y 10/22/19 0604 10/22/19 1411 LSJ Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864.1920 la1 wv✓w.microbac.com Page 3 0f 10 �VMICROBACS Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9J0254 Client Sample ID: Outfall2 Outlet, grab Sample Matrix: Aqueous Collected By: Poythress Lab Sample ID: K9J0254-02 Collection Date: 10/16/2019 10:15 Wet Chemistry Result RL Units Dilution Note Prepared Analyzed Analyst EPA 1664 Rev. B „Oil & Grease (SGT-HEM) 'SM 2540 D-2011 Total Suspended Solids <5.00 5.00 rrg/L <4.17 4.17 mg/L 1 10/24/19 1141 TBM 1 10/17/19 1005 CUB Metals Result RL Units Dilution Note Prepared Analyzed Analyst Metals Aqueous/EPA 200.7 Rev 4.4 1994 Lead <0.010 0.010 mg/L 1 10/17/19 1355 10/17/19 1355 TAB Zinc 0.014 0.005 mg/L 1 10/17/19 1355 10/17/19 1355 TAB n Field Sampling/Testing Result RL Units Dilution Note Prepared Analyzed Analyst Field Rainfall 0.19 inches 1 10/24/19 2043 10/24/19 2105 BNS Field Observation Color Clear 1 10/24/19 2043 10/24/19 2105 BNS Odor None 1 10/24/19 2043 10/24/19 2105 BNS . Clarity Yes 1 - 10/24/19 2043 10/24/19 2105 BNS Floating Solids None 1 10/24/19 2043 10/24/19 2105 BNS Suspended Solids (Residue, None 1 10/24/19 2043 10/24/19 2105 BNS Non -Filterable) ' Foam None 1 10/24/19 2043 10/24/19 2105 BNS Oil Sheen None 1 10/24/19 2043 10/24/19 2105 BNS Erosion Evidence None 1 10/24/19 2043 10/24/19 2105 BNS Other Pollution Indicators None 1 10/24/19 2043 10/24/19 2105 BNS SM 2550 B-2010 Temperature, Field 20 0.1 °C 1 10/16/19 1015 JMP SM 4500 H+13-2011 I 'pH, Field Test 6.3 1.0 pH Units 1 10/16/19 1015 JMP Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH Total Metals - ICP Result RL Units Dilution Note Prepared Analyzed Analyst EPA 200.7, Rv. 4.4 'Copper <0.00800 0.00800 mg/L 1 y 10/22/19 0604 10/22/19 1420 LSJ Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 in I wviw.microbac.com Page 4 of 10 OMICROBACs Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9JO254 'Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville Spike Source %REC RPD Wet Chemistry Result RL Units Level Result %REC Limits RPD Limit Notes Batch KJ90148 - Wet Chem Aqueous - SM 2540 D-2011 Blank (KJ90148-BLKt) Prepared & Analyzed: 10/17/2019 ;Total Suspended Solids <2.50 2.50 mg/L Blank (KJ90148-BLK2) Prepared & Analyzed: 10/17/2019 Total Suspended Solids <2.50 2.50 mg/L Blank (KJ90148-BLK3) Prepared & Analyzed: 10/17/2019 Total Suspended Solids <2.50 2.50 mg/L Blank (KJ90148-BLK4) Prepared & Analyzed: 10/17/2019 Total Suspended Solids <2.50 2.50 mg/L Blank (KJ9014&I3LK5) Prepared & Analyzed: 10/17/2019 ,Total Suspended Solids <2.50 2.50 mg/L LCS Dup (KJ90148-BSD1) Prepared &Analyzed: 10/17/2019 Total Suspended Solids 30.7 2.50 mg/L 31.6 97 94.5-105.4 200 200 Batch KJ92426 -Wet Chem Aqueous •EPA 1664 Rev. B Blank (KJ92426-BLK1) Prepared & Analyzed: 10124/2019 Oil & Grease (SGT-HEM) <5.00 5.00 mg/L LCS (KJ92426-BS1) Prepared & Analyzed: 10/24/2019 Oil & Grease (SGT-HEM) 19.6 5.00 mg/L 20.4 96 64-114 Matrix Spike (KJ92426.MSt) Source: K9J0311-01 Prepared & Analyzed: 10/2412019 ,Oil & Grease (SGT-HEM) 28.7 5.00 mg/L 21.7 1.47 125 78-132 1 Spike Source %REC RPD Metals Result RL Units Level Result %REC Limits RPD Limit Notes Batch KJ90158 - Metals Aqueous - EPA 200.7 Rev 4.4 1994 Blank (KJ90158-BLK1) Prepared & Analyzed: 10/17/2019 Lead <0.020 0.020 mg/L Zinc <0.010 0.010 mg/L Blank (KJ90158-BLK2) Prepared & Analyzed: 10/17/2019 Lead <0.020 0.020 mg/L Zinc <0.010 0.010 mg/L LCS (KJ90158-BS1) Prepared & Analyzed: 10/17/2019 Lead 0.245 0.020 mg/L 0.248 99 85-115 Zinc 0.247 0.010 mg/L 0.250 99 85-115 LCS (KJ90158-BS2) Prepared & Analyzed: 10/1712019 Lead 0.258 0.020 mg/L 0.248 104 85-115 Zinc 0.260 0.010 mg/L 0.250 104 85-115 LCS (KJ90158-BS3) Prepared & Analyzed: 10/17/2019 Lead 0.252 0.020 mg/L 0.248 101 85-115 Zinc 0.251 0.010 mg/L 0.250 101 85-115 Microbac Laboratories, Inc. ,I 2592 Hope Mills Rd i Fayetteville, NC 28306 1910.864.1920 p i www.microbac.com Page 5 of 10 VMICROBACO Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9J0254 Spike Source %REC RPD Metals Result RL Units Level Result %REC Limits RPD Limit Notes latch KJ90158 - Metals Aqueous - EPA 200.7 Rev 4.4 1994 LCS (KJ90158-BS4) Prepared & Analyzed: 10/17/2019 .Lead 0.241 0.020 mg/L 0.248 97 85-115 'Zinc 0.241 0.010 mg/L 0.250 96 85-115 Duplicate (KJ90158-DUP1) Source: K9J0175-01 Prepared &Analyzed: 10/17/2019 'Lead <0.010 0.010 mg/L ND 10 Zinc 0.013 0.005 mg/L 0.015 17 10 Duplicate (KJ90158-DUP2) Source: K9J0207-01 Prepared & Analyzed: 10/17/2019 Lead 0.021 0.010 mg/L 0.022 4 10 Zinc 0.955 0.005 mg/L 1.01 6 10 Duplicate (KJ90158-DUP3) Source: K9J0252-01 Prepared & Analyzed: 10/17/2019 Lead <0.010 0.010 mg/L ND 10 Zinc - 0.006 0.005 mg/L 0.006 9 10 Matrix Spike (KJ90158-MS1) Source: K9J0175-01 Prepared &Analyzed: 10/17/2019 Lead 0.226 0.010 mg/L 0.248 ND 91 70-130 Zinc 0.244 0.005 mg/L 0.250 0.015 91 70-130 Matrix Spike (KJ90158-MS2) Source: K9J0207-01 Prepared & Analyzed: 10/17/2019 Lead 0.257 0.010 mg/L 0.248 0.022 94 70-130 Zinc 1.16 0.005 mg/L 0.250 1.01 58 70-130 Matrix Spike (KJ90158-MS3) Source: K9J0252-01 Prepared & Analyzed: 10/17/2019 Lead 0.251 0.010 mg/L 0.248 ND 101 70-130 Zinc 0.253 0.005 mg/L 0.250 0.006 99 70-130 Matrix Spike Dup (KJ90158-MSD1) Source: K9J0175-01 Prepared &Analyzed: 10/17/2019 Lead 0.230 0.010 mg/L 0.248 ND 93 70-130 2 30 Zinc 0.247 0.005 mg/L 0.250 0.015 93 70-130 1 30 Matrix Spike Dup (KJ90158-MSD2) Source: K9J0207-01 Prepared &Analyzed: 10/17/2019 Lead 0.259 0.010 mg/L 0.248 0.022 96 70-130 1 30 Zinc 1.18 0.005 mg/L 0.250 1.01 67 70-130 2 30 Matrix Spike Dup (KJ90158-MSD3) Source: K9J0252-01 Prepared & Analyzed: 10/17/2019 Lead 0.242 0.010 mg/L 0.248 ND 98 70-130 4 30 Zinc 0.244 0.005 mg/L 0.250 0.006 95 70-130 4 30 Reference (KJ90158-SRMt) Prepared &Analyzed: 10/17/2019 --. Zinc 1.93 0.020 mg/L 1.92 0.010 mg/L Batch Quality Control Summary: Microbac Laboratories Inc., - Marietta, OH 2.00 96 95-105 2.00 96 95-105 Spike Source %REC RPD Total Metals - ICP Result MDL RL Units Level Result %REC Limits RPD Limit Notes Batch B9J1289 - 200.7 - EPA 200.7, Rv. 4.4 Blank (B9J1289-BLK1) Prepared &Analyzed: 10/2212019 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 10 OMICROBACS Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9J0254 Spike Source %REC RPD Total Metals - ICP Result MDL RL Units Level Result %REC Limits RPD Limit Notes Batch B9J1289 - 200.7 - EPA 200.7, Rv. 4.4 Blank (B9.11289-BLK1) Prepared & Analyzed: 10/2212019 Copper <0.00400 0.00400 0.00800 mg/L LCS (89J1289-13SI) Prepared &Analyzed: 10/22/2019 Copper 0.262 0.00400 0.00800 mg/L 0.250 105 85-115 Duplicate (89.11289-DUPI) Source: M9J1404-01 Prepared &Analyzed: 10/22/2019 'Copper <0.00400 0.00400 0.00800 mg/L ND 20 Matrix Spike (B9J1289-MS1) Source: M9J1404-01 Prepared &Analyzed: 10/2212019 Copper 0.258 0.00400 0.00800 mg/L 0.250 ND 103 70-130 Matrix Spike (B9J1289-MS2) Source: M9J1441-02 Prepared & Analyzed: 10/22/2019 Copper 0,259 0,00400 0.00800 mg/L 0.250 ND 104 70-130 Post Spike (B9J1289-PS1) Source: M9J1404-03 Prepared & Analyzed: 10/22/2019 Copper 0.245 mg/L 0.250 0.00527 95.9 75-125 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.nricrobac.conn Page 7 of 10 OMIC.ROBAC® Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9J0254 Definitions MDL: Minimum Detection Limit RL: Reporting Limit RPD: Relative Percent Difference Y: This analyte is not on the laboratory's current scope of accreditation. Cooler Receipt Log Cooler ID: Default Cooler Temp: 3.2°C Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? - Yes Chain of Custody (COC) Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes i Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC (Name, Date & Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace, or not reed.? Yes Project Requested Certification(s) Microbac Laboratories Inc., - Marietta, OH 583 Microbac Laboratories, Inc. - Fayetteville 11 Report Comments NC Dept. of the Environment and Natural Resources III ii1111l. 8iFL]1:1J:410WRIC&I Reviewed and Approved By: Samples were received in proper condition and the reported results conform to 1 applicable accreditation standard unless otherwise noted.Y The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated Brittany Smith in the footnote are present and an authorized signature is included. Administration Reported: 10/28/2019 17:25 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, INC 28306 1910.864.1920 p I yr w.microbac.com Page 8 of 10 Fayetteville Division 2592 Hope Mills Road - Fayetteville, NC 28306 (916) 86419201884•8774 faX 254- CHAIN OF CUSTODY RECORD PAGE 1 OF_, - 'NTXW 9&ADDAms; Poi PROJECTIL�DchnaN: ,.L� J4r�w.�7c TYPE OF ANALYSIS PRESERVATION I0013Ej CODE: A=Noes tM W.UrrRian f vF. � 245c CONTA"PERSON: I w N � °� ta, O { rt 9 = HNO3 (pH<2) + 48`C C = H2304 (pH-*) 4 - O: o = Naorl +<s•c E = ZN Ac taia t cVC - F=HCI G= Sodium Thlo ' PHONE Jr % �P7-F11 er; Mn� ARS Pb bATE(h16TtlDOOP wI1Nn . m;S!! ,r 4 LAa IDA aAhTPI.E TYPE DATE TIME coi1P oluo Pa Plow 7EaP•e iomNE Swjl" OKf�an t�nldll- It-IL-11 9:�z x 1- A c L� a+�kr1 2 p1�t T-/O fE- TByja,e,.Mi.m;atll:29:16 Lah lnitlals—>. pqubhatl hrt Sal. nmv Ind gonanl i Da6 Tlm. i�f; � Turnaround Hme: REGULAR RUSH j . a/. 1 I �U:26 2 to j e nV1.111d by& Uh er:lemulWl e1w Comments or3podalHazrlds: - 9 q nqa . by oua mo Re[e Yaay: {S pnaSW. Valk TIms ' 5 B ph Field: ph meld: WatarLavetSi 15 DATA FOR REG. COMPLIANCE PURPOSE? mp Hold M: Tamp Field 2: Water Level tit NO YES WHICH: m 0 0 C(cc�+rblgX �C;nS��J STORM WATER - QUALITATIVE MONITORING tK9J0254` OTHER OBVIOUS I EROSION OR INDICATORS OF STORM SITE # DATE SAMPLED COLOR ODOR CLARITY FLOATING SOLIDS SUSPENDED SOLIDS FOAM OIL SHEEN DEPOSITION AT THEfjOUTFALL STORMWATER POLLUTION J 2 G-�v-1 l 4 IPA! / (d.G ?� / `O AD F (b y!�d 1 ipl1G 3 TOTAL RAINFALL (inches): • 1 4