NCG030433_MONITORING INFO_20190705

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
DOC TYPE.
❑ HISTORICAL FILE
EV,MONITORING REPORTS
DOC DATE
❑
YYYYMMDD

CREE
June 27, 2019
NC DEQ /Division of Water Resources
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Wolfspeedm
RECEIVED
'JUL 0 5 2019
CENTRAL FILE.
DWR SECTIC
RE: Stormwater Discharge Outfall (SDO) Monitoring Report
Cree, Inc., 4600 Silicon Drive, Durham, Durham County, North Carolina
General Stormwater Permit No. NCG030000/COC NO. NCG030433
January — June 2019, SDO #1, #2, #3, #3A, #4, #5, #6 and #7
To Whom It May Concern:
Please find enclosed the semi-annual stormwater Discharge Monitoring Reports (one original and one
copy) for the eight stormwater outfalls located at Cree, Inc., 4600 Silicon Drive, Durham, Durham
County, North Carolina. The analytical reports were received from the laboratory on June 19, 2019.
Pace Analytical Services (NC Certification #40, 633, 67) conducted the analyses which completes the
first 2019 semi-annual testing requirements for the Silicon Drive site.
Discharge samples were collected at outfall #t, #2, #5, #6 and #7. No sample was collected at
outfall #4, #3, or #3A due to absence of flow, and is recorded as NO DISCHARGE. For the
sampled outfalls, and as in previous reports submitted to DEQ, levels for copper and zinc are above the
benchmark values listed in Table 3 of section 11.13 of our stormwater permit for outfall #1, #2, #5, #6
(Cu) and outfalls #5 and #6 (Zn). In September 2014, Cree was granted an exemption from the
requirement to continue following Tier Two and Tier Three response actions as stated in Section B of
the stormwater permit for these parameters. Cree will continue to monitor these levels throughout the
next semi-annual testing period and report any success in eliminating the elevated levels. Samples at
outfalls #5 and #6 were outside pH benchmarks. As required, Tier One evaluation has begun and will
be recorded in the site Stormwater Pollution Prevention Plan.
In addition, the values for Cu reported above the benchmark levels at outfalls #7, and the Zn values
reported above the benchmark levels at outfall #2 during the winter 2018 event (initiating Tier One
response actions) have returned to normal ranges at this collection event.
Please contact me at 919-407-6101 if you need additional information.
Sincerely,
Donna Lazzari '1/
Environmental Manager
4600 Silicon Drive
Durham, NC 27703 USA
Main: [phone]
1%

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted June 27, 2019
CERTIFICATE OF COVERAGE NO. NCG03 0 4 3 3
FACILITY NAME CREE, INC
COUNTY DURHAM
PERSON COLLECTING SAMP ES JANE COOPER
LABORATORY Pace Analytical Lab Cert. # 40, 633, 67
Comments on sample collection or analysis:
Three (3) certification numbers provided for the laboratory locations indicated on the results.
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2019
SAMPLE PERIOD [E]Jan-June ❑ July -Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow [:]Watersupply [:]SA
*Other class C - NSW
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
n No discharge this period j2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
pH,
Standard units
Total Copper
Total Lead
-
Total Zinc
Non -Polar O&G/
T
Total Petroleum
Hydrocarbons
Total Toxic
Organicss
Benchmarks
-
-
100 mg/L or 50 mg/L4
6.0 - 9.0
0.010 mg/L
0.07S mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
01
6/5/19
0.29
21.6
6.40
0.0112
<0.005
0.158
<4.8
<0.05
02
6/5/19
0.29
47.6
6.22
0.012
<0.005
0.180
<4.8
<0.05
05
6/5/19
0.29
19.5
4.18
0.0246
<0.005
0.771
<4.8
<0.05
06
6/5/19
0.29
68.8
5.87
0.0198
<0.005
0.105
<4.8
<0.05
07
6/5/19
0.29
10
6.55
0.0084
<0.005
0.0248
<4.8
<0.05
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
' For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
�/oN�/3- L/fZZYrr2/
Name (Print name)
Title (Print title)
/Si ture Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
n No discharge this nprind 22
Outfall No.
Date Sample Collected`
(mo/dd/yr)
24-hour rainfall amount,
Inches3
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/L°
Parameter Code
-
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021
SWU-245, last revised 11/1/2018
Page 2 of 3
W

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO Q
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an oriainal copy of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results (or at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Permittee
Permit Date: 11/1/2018-05/31/2021
Date
SWU-245, last revised 11/1/2018
Page 3 of 3

aceAnalytical
wwwpecek0a.00m
d
June 19, 2019
Elizabeth Tutino
Cree
4600 Silicon Dr.
Durham, NC 27703
RE: Project: Stormwater DUR 6-5-19
Pace Project No.: 92431928
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)8344984
Dear Elizabeth Tutino:
". Enclosed are the analytical results for sample(s) received by the laboratory on June 06, 2019. The
results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kristi Prater
[e-mail]
[phone]
Project Coordinator
Enclosures
cc: janie Cooper
REPORT OF LABORATORY ANALYSIS
This report shall not be repmouceo, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 26

Pace Analytical services, LLC
aceAnalytical0
6701 Conference Owe
sxav�cdaW min
Raleigh, NC 27607
[phone]
CERTIFICATIONS
Project: Stormwater DUR 6-5-19
Pace Project No.: 92431928
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
Virginia/VELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Wastewater Certification #: 633
North Carolina Drinking Water Certification #: 37738
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, LLC, Page 2 of 26

I
Pace Analytical Services, LLC
lacemalytiolo 6707 Conference Drive
Raleigh, NC 27607
ewwpecelebs.crom
[phone]
LI;J14l6lit T1ZYA
Project:
Pace Project No.:
Stormwater DUR 6-5-19
92431928
Lab ID
Sample ID
Matrix Date Collected Date Received
92431928001
SDO-1
Water 06/05/1918:15 06/06/1911:03
92431928002
SDO-2
Water 06/05/1917:30 0610611911:03
92431928003
SDO-5
Water 06105/1917:40 06/06/1911:03
92431928004
SDO-6
Water 0610511917:22 06/06/1911:03
92431928005
I
SDO-7
Water 06105/1918:00 06/06/1911:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 26

mAnalytical
a a w.peceleas.corn
SAMPLE ANALYTE COUNT
Project: Stormwater DUR 6-5-19
Pace Project No.: 92431928
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
92431928001
SDO-1
SM 254OD-2011
SOB
1
EPA 1664B
JMS
1
EPA 200.7 Rev 4.4 1994
DS
3
EPA625.1
PKS
23
EPA624.1
DLK
15
92431928002
SDO-2
SM 254OD-2011
SOB
1
EPA 1664E
JMS
1
EPA 200.7 Rev 4.4 1994
DS
3
EPA625.1
PKS
23
EPA 624.1
DLK
15
92431928003
SDO-5
SM 254OD-2011
SOB
1
EPA 1664E
JMS
1
EPA 200.7 Rev 4.4 1994
DS
3
EPA625.1
PKS
23
EPA 624.1
DLK
15
92431928004
SDO-6
SM 254OD-2011
SOB
1
EPA 1664E
JMS
1
EPA 200.7 Rev 4.4 1994
DS
3
EPA625.1
PKS
23
EPA624.1
DLK
15
92431928005
SDO-7
SM 254OD-2011
SOB
1
EPA 1664E
JMS
1
EPA 200.7 Rev 4.4 1994
DS
3
EPA625A
PKS
23
EPA 624.1
DLK
15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 26

aceAnalytical
wwepecelebs.com
l
If
Project: Stormwater OUR 6-5-19
Pace Project No.: 92431928
SDO.1
�i Parameters
�2540D Total Suspended Solids
'Total Suspended Solids
i
1.1664 SGT-HEM, TPH
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
/_12/a1W11111119_140*111NJV
Lab ID: 92431928001 Collected: 06/05/19 18:15 Received: 06/06/19 11:03 Matrix: Water
Results Units Report Limit OF Prepared Analyzed CAS No. Oual
Analytical Method: SM 254OD-2011
21.6 mg/L
Analytical Method: EPA 1664E
3.2 1
06/07/19 12:49
Total Petroleum Hydrocarbons
NO
mglL
4.8
1
06/11/1906:28
200.7 MET ICP
Analytical Method: EPA 200.7
Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Copper
11.2
ug/L
5.0
1
06111/19 23:04
06/13/19 20:00
7440-50-8
Lead
NO
ug/L
5.0
1
06/1111923:04
06/1311920:00
7439-92-1
Zinc
158
ug/L
10.0
1
06/11/1923:04
06/13/1920:00
7440-66-6
625 RVE
Analytical Method: EPA625.1
Preparation Method:
EPA625.1
'Anthracene
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 17:51
120-12-7
Bulylbenzylphthalale
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 17:51
85-68-7
2-Chlorophenol
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 17:51
95-57-8
1,2-Dichlorobenzene
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 17:51
95-50-1
1,3-Dichlorobenzene
NO
ug/L
5.0
1
06/11/19 20:16
06/13M9 17:51
541-73-1
2,4-Dichlorophenol
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 17:51
120-83-2
Di-n-butylphthalate
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 17:51
84-74-2
1,2-Diphenylhydrazine
NO
ug/L
5.0
1
06/11/19 20:16
06/13119 17:51
122-66-7
bis(2-Elhylhexyl)phthalate
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 17:51
117-81-7
Isophorone
NO
ug/L
10.0
1
06/11/1920:16
06/13/1917:51
78-59-1
Naphthalene
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 17:51
91-20-3
2-Nitrophenol
NO
ug/L
5.0
1
06111/1920:16
06/1311917:51
88-75-5
4-Nitrophenol
NO
ug/L
50.0
1
06/11/19 20:16
06/13/19 17:51
100-02-7
Pentachlorophenol
NO
ug/L
10.0
1
06111/1920:16
06113/1917:51
87-86-5
Phenol
NO
ug/L
5.0
1
06/11/1920:16
06/13/19 17:51
108-95-2
1,2,4-Trichlorobenzene
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 17:51
120-82-1
2,4,6-Trichlorophenol
NO
ug/L
10.0
1
06/11/19 20:16
06/13/19 17,51
88-06-2
Surrogates
Nitrobenzene-d5(S)
78
%
10-120
1
06111/1920:16
06/13/19 17:51
4165-60-0
2-Fluorobiphenyl(S)
72
%
15-120
1
06/11/19 20:16
06/13/19 17:51
321-60-8
Terphenyl-dl4(S)
77
%
11-131
1
06/11/19 20:16
06/13/1917:51
1718-51-0
Phenol-d6(S)
39
%
10-120
1
06/11/1920:16
06/1311917:51
13127-88-3
2-Fluorophenol(S)
57
%
10-120
1
06/1111920:16
06/13/19 17:51
367-12-4
2,4,6-Tribromophenol(S)
80
%
10-137
1
06/11/19 20:16
06/13/19 17:51
118-79-6
624 Volatile Organics
Analytical Method: EPA624.1
Carbon tetrachloride
NO
ug/L
2.0
1
06/14/19 22:02
56-23-5
Chloroform
NO
ug/L
5.0
1
06/14/19 22:02
67-66-3
Dibromochloromelhane
NO
ug/L
2.0
1
06/14/19 22:02
124-48-1
1,2-Dichloroethane
NO
ug/L
2.0
1
06/14M9 22:02
107-06-2
1,1-Dichloroelhene
NO
ug/L
2.0
1
06/14/19 22:02
75-35-4
Ethylbenzene
NO
ug/L
1.0
1
06/1411922:02
100-41-4
Methylene Chloride
NO
ug/L
5.0
1
06/14/19 22:02
75-09-2
Tetrachloroethene
NO
ug/L
2.0
1
06/14/19 22:02
127-18-4
Toluene
ND
ug/L
1.0
1
06/14/19 22:02
108-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 05:37 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 26

aceAnalytical e
~..pecelaW.aom
ANALYTICAL RESULTS
Project: Stormwater OUR 6-5-19
Pace Project No.: 92431928
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
oample: suu-1
Lab ID: 92431928001 Collected: 06/05/19 18:15
Received: 06/06/19 11:03 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
624 Volatile Organics
Analytical Method:
EPA 624.1
1,1,1-Trichloroethane
ND
ug/L
2.0
1
06/14/19 22:02
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1
06/14/19 22:02
79-00-5
Trichloroethene
NO
ug/L
2.0
1
06/14/19 22:02
79-01-6
Surrogates
4-BromcBuorobenzene(S)
101
%
70-130
1
06/14/19 22:02
460-00-4
Toluene-d8 (S)
97
%
70-130
1
06/14/19 22:02
2037-26-5
1,2-Dichloroethane-d4(S)
106
%
70-130
1
06/14/19 22:02
17060-07-0
Date: 06119/2019 05:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 26

aceAnalytical
wwxpxeleDs.cwn
,Project: Stormwater DUR 6-5-19
Pace Project No.: 92431928
Parameters
2540D Total Suspended Solids
Total Suspended Solids
�1664 SGT-HEM, TPH
Total Petroleum Hydrocarbons
I
200.7 MET ICP
Copper
Lead
Zinc
625 RVE
Anthracene
B utylbe nzylphtha late
2-Chlorophenol
1,2-Dichlorobenzene
1,3-Dichlorobenzene
2,4-Dichlorophenol
Di-n-butylphthalate
'1,2-Diphenylhydrazine
bis(2-Ethylhexyl) phthalate
Isophorone
Naphthalene
2-Nltrophenol
'4-Nitrophenol
Pentachlorophenol
Phenol
1,2,4-Tdohlorobenze ne
2,4,6-Trichl o ro phenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl(S)
Terphenyl-dl4 (S)
Phenol-d6 (S)
2-Fluorophenol(S)
2,4,6-Tribromophenol(S)
624 Volatile Organics
Carbon tetrachloride
Chloroform
Di bromochl orometh a ne
,1,2-Dichloroethane
,1,1-Dichloroethene
Ethylbenzene
Methylene Chloride
Tetrachloroethene
Toluene
Pace Analytical services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
ANALYTICAL RESULTS
Lab ID: 92431928002 Collected: 06/0511917:30 Received: 06/06/19 11:03 Matrix: Water
Results Units Report Limit DF
Analytical Method: SM 254OD-2011
47.6 mg/L 3.2 1
Analytical Method: EPA 1664B
ND mg/L 4.8 1
Prepared Analyzed CAS No. Oual
06/07/19 12:49
06/11/19 06:28
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
12.0 ug/L 5.0 1 06111/1923:04 06/13/1920:16 7440-50-8
NO ug/L 5.0 1 06/11/19 23:04 06/13/19 20:16 7439-92-1
180 ug/L 10.0 1 06/11/1923:04 06/13/19 20:16 7440-66-6
Analytical Method: EPA 625.1 Preparation Method: EPA 625A
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:17
120-12-7
ND
ug/L
5.0
1
06/11/19 20:16
0611311918:17
85-68-7
NO
ug/L
5.0
1
06/11/19 20:16
06/1311918:17
95-57-8
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:17
95-50-1
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:17
541-73-1
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:17
120-83-2
NO
ug/L
5.0
1
06/11/1920:16
06/13/19 18:17
84-74-2
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:17
122-66-7
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:17
117-81-7
ND
ug/L
10.0
1
06/11/19 20:16
06/13/19 18:17
78-59-1
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:17
91-20-3
NO
ug/L
5.0
1
06/11/19 20:16
06113/19 18:17
88-75-5
ND
ug/L
50.0
1
06/11/19 20:16
06/13/19 18:17
100-02-7
ND
ug/L
10.0
1
06/11/19 20:16
06/13/19 18:17
87-86-5
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:17
108-95-2
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 1817
120-82-1
NO
ug/L
10.0
1
06/11/19 20:16
06/13/19 18:17
88-06-2
53
%
10-120
1
06/11/19 20:16
06/13/19 18:17
4165-60-0
42
%
15-120
1
06/11/19 20:16
06/13/19 18:17
321-60-8
82
%
11-131
1
06/11/19 20:16
06113/1918:17
1718-51-0
32
%
10-120
1
06/1111920:16
06/13/1918:17
13127-88-3
42
%
10-120
1
06/11/19 20:16
06/13/19 18:17
367-12-4
63
%
10-137
1
06111/1920:16
06/13/1918:17
118-79-6
Analytical Method: EPA 624.1
NO
ug/L
2.0
1
06/1411922:20
56-23-5
ND
ug/L
5.0
- 1
06/14/19 22:20
67-66-3
NO
ug/L
2.0
1
06/14/19 22:20
124-48-1
ND
ug/L
2.0
1
06/14/19 22:20
107-06-2
ND
ug/L
2.0
1
06/14/19 22:20
75-35-4
ND
ug/L
1.0
1
06/14/19 22:20
100-41-4
ND
ug/L
5.0
1
06/14/19 22:20
75-09-2
ND
ug/L
2.0
1
06/14/19 22:20
127-18-4
ND
ug/L
1.0
1
06/14/19 22:20
108-88-3
REPORT OF LABORATORY ANALYSIS
I This report shall not be reproduced, except in full,
Date: 06/19/2019 05:37 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 26

aceAnalytical e
~pecUeDs.00m
ANALYTICAL RESULTS
Project: Stormwater DUR 6-5-19
Pace Project No.: 92431928
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: 500-2
Lab I0: 92431928002 Collected: 06/05/19 17:30
Received: 06/06/19 11:03 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Oual
624 Volatile Organics
Analytical Method: EPA 624A
1, 1, 1-Trichloroethane
ND ug/L
2.0
1
06/1411922:20
71-55-6
1.1,2-Trichloroethane
ND ug/L
2.0
1
06/14/19 22:20
79-00-5
Trichloroethene
ND ug/L
2.0
1
06/14/19 22:20
79-01-6
Surrogates
4-BromoFluorobenzene (S)
113 %
70-130
1
06/14/19 22:20
460-00-4
Toluene-d8 fS)
99 %
70-130
1
06/14/19 22:20
2037-26-5
1,2-Dichloroethane-d4 (S)
104 %
70-130
1
06/14/19 22:20
17060-07-0
Date: 06/19/2019 05:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytcal Services, LLC.
Page 8 of 26

laceAnalyticale
n www.pealeescdn
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, INC 27607
[phone]
Project: Stormwater OUR 6-5-19
Pace Project No.: 92431928
11
Sample: SDO-5 Lab ID: 92431928003 Collected: 06/05/19 17:40 Received: 06/06/19 11:03 Matrix: Water
I
y, Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Total Suspended Solids
1664 SGT-HEM, TPH
Total Petroleum Hydrocarbons
II
200.7 MET ICP
Copper
Lead
Zinc
625 RVE
Anthracene
B ulylbenzylphtha late
2-Chlorophenol
1,2-Dichlorobenzene
1-,3-Dichlorobenzene
214-1)ichlorophenol
Di-n-butylphthalate
1;2-Diphenylhydrazine
bis(2-Ethylhexyl) phtha late
Isophorone
Naphthalene
2=Nitrophenol
44Nitrophenol
Pentachlorophenol
Phenol
1,2,4-Trichlorobenzene
2,4, 6-Trich to ro phen of
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol(S)
2,4,6-Tribromophenol(S)
624 Volatile Organics
Analytical Method: SM 254OD-2011
19.5 mg/L 3.8 1 06/12/19 09:56
Analytical Method: EPA 1664B
NO , mg/L 4.8 1 06/11/1906:28
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
24.6 ug/L 5.0 1 06/11/19 23:04 06/13/19 2019 7440-50-8
NO ug/L 5.0 1 06111/1923:04 06/1311920:19 7439-92-1
771 ug/L 10.0 1 06/11/1923:04 06/13/1920:19 7440-66-6
Analytical Method: EPA625.1 Preparation Method: EPA625.1
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:42
120-12-7
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:42
85-68-7
ND
ug/L
5.0
1
06111/1920:16
06/13/19 18:42
95-57-8
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:42
95-50-1
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:42
541-73-1
NO
ug/L
5.0
1
06/11/19 20:16
06113/1918:42
120-83-2
NO
ug/L
5.0
1
06/11/19 20:16
06113/1918:42
84-74-2
NO
ug/L
5.0
1
06/11/19 20:16
06/13,119 18:42
122-66-7
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:42
117-81-7
NO
ug/L
10.0
1
06/11/19 20:16
06/13/19 18:42
78-59-1
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:42
91-20-3
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:42
88-75-5
NO
ug/L
50.0
1
06/11/19 20:16
06/13/19 18:42
100-02-7
ND
ug/L
10.0
1
06/11/19 20:16
06/13/19 18:42
87-86-5
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 18:42
108-95-2
NO
ug/L
5.0
1
06/11/1920A6
06/13/1918:42
120-82-1
NO
ug/L
10.0
1
06/11/19 20:16
06113/1918:42
88-06-2
90
%
10-120
1
06/11/19 20:16
06/13/19 18:42
4165-60-0
76
%
15-120
1
06/11/19 20:16
06/1311918:42
321-60-8
88
%
11-131
1
06/11/19 20:16
06/13/19 18:42
1718-51-0
52
%
10-120
1
06/11/19 20:16
06113/1918:42
13127-88-3
72
%
W-120
1
06/11/19 20:16
06/13M9 18:42
367-12-4
93
%
10-137
1
06/11/19 20:16
06/13/19 18:42
118-79-6
Analytical Method: EPA624.1
Carbon tetrachloride
NO
ug/L
2.0
1
06/14/19 22:37
56-23-5
Chloroform
NO
ug/L
5.0
1
06/14/19 22:37
67-66-3
Dibromochloromethane
NO
ug/L
2.0
1
06/14/19 22:37
124-48-1
1,2-Dichloroelhane
ND
ug/L
2.0
1
06/14/19 22:37
107-06-2
1,1-Dichloroethene
NO
ug/L
2.0
1
06/14/19 22:37
75-35-4
Ethylbenzene
NO
ug/L
1.0
1
06/14/1922:37
100-41-4
Methylene Chloride
NO
ug/L
5.0
1
06/14/19 22:37
75-09-2
Tetrachloroethene
NO
ug/L
2.0
1
06/14/19 22:37
127-18-4
Toluene
NO
ug/L
1.0
1
06/14/19 22:37
108-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 05:37 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 26

aceAnalytical e
w pecehlbs.corn
ANALYTICAL RESULTS
Project: Stormwater DUR 6-5-19
Pace Project No.'. 92431928
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: SDO-5
Lab ID: 92431928003 Collected: 06/05/19 17:40
Received: 06/06/19 11:03 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Oual
624 Volatile Organics
Analytical Method:
EPA 624.1
1,1,1-Trichloroethane
ND
ug/L
2.0
1
06/14/19 22:37
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1
06/14/19 22:37
79-00-5
Trichloroethene
NO
ug/L
2D
1
06/14/19 22:37
79-01-6
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
06/14/19 22:37
460-00-4
Toluene-d8(S)
87
%
70-130
1
06/14/19 22:37
2037-26-5
1,2-Dichlometharl(S)
103
%
70-130
1
06/14/19 22:37
17060-07-0
Date: 06/19/2019 05:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, -LC.
Page 10 of 26

Pace Analytical Services, LLC
aceAnalytical a 6701 Conference 607
Raleigh, NC 276tl7
a pwsteGaome (919)8344984
ANALYTICAL RESULTS
Project: Slormwater OUR 6-5-19
.Pace Project No.: 92431928
Sample: SDO-6 Lab ID: 92431928004 Collected: 06/05/19 17:22 Received: 06/06/19 11:03 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D-2011
Total Suspended Solids 68.8 mg/L 3.2 1 06/07/19 12:49
11
1664 SGT-HEM, TPH Analytical Method: EPA 1664E
Total Petroleum Hydrocarbons NO mg/L 4.8 1 06/11/19 06:28
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Copper
19.8
ug/L
5.0
1
06/11/1923:04
06/13/1920:22
7440-50-8
Lead
NO
ug/L
5.0
1
06/1111923:04
06/13/1920:22
7439-92-1
Zinc
105
ug/L
10.0
1
06/11/19 23:04
06/13/19 20:22
7440-66-6
625 RVE
Analytical Method: EPA 625.1
Preparation Method: EPA 625.1
Anthracene
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:08
120-12-7
Butylbenzylphthalate
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:08
85-68-7
2-Chlorophenol
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:08
95-57-8
1,2-Dichlorobenzene
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:08
95-50-1
11,3-Dichlorobenzene
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:08
541-73-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:08
120-83-2
Di-n-butylphthalate
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:08
84-74-2
1�2-Diphenylhydrazine
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:08
122-66-7
bis(2-Ethylheuyl)phthalate
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:08
117-81-7
Isophorone
NO
ug/L
10.0
1
06111/1920:16
06/1311919:08
78-59-1
Naphthalene
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:08
91-20-3
2-Nitrophenol
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:08
88-75-5
4'-Nitrophenol
ND
ug/L
50.0
1
06/11/19 20:16
06/13/19 19:08
100-02-7
Pentachlorophenol
NO
ug/L
10.0
1
06/11/19 20:16
06/13/19 19:08
87-86-5
Phenol
ND
ug/L
5.0
1
06/1111920:16
06/1311919:08
108-95-2
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:08
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
06/11/19 20:16
06/13/19 19:08
88-06-2
Surrogates
Nitrobenzene-d5 (S)
84
%
10-120
1
06/11/19 20:16
06/13/19 19:08
4165-60-0
2•Fluorobiphenyl(S)
74
%
15-120
1
06/11/1920:16
06/13/1919:08
321-60-8
Terphenyl-d14 (S)
85
%
11-131
1
06/11/19 20:16
06/13/19 19:08
1718-51-0
Phenol-d6(S)
45
%
10-120
1
06/11/19 20:16
06/13/1919:08
13127-88-3
2-Fluorophenol (S)
64
%
10-120
1
06/11/19 20:16
06/13/19 19:08
367-12-4
2,4,6-Tribromophenol(S)
88
%
10-137
1
06/11/19 20:16
06/13/19 19:08
118-79-6
624 Volatile Organics
Analytical Method:
EPA624.1
Carbon tetrachloride
NO
ug/L
2.0
1
06/14/19 22:55
56-23-5
Chloroform
NO
uglL
5.0
1
06/14/19 22:55
67-66-3
Dibromochloromethane
ND
ug/L
2.0
1
06/14/19 22:55
124-48-1
1,2-Dichloroelhane
NO
ug/L
2.0
1
06/14119 22:55
107-06-2
1',1-Dichloroethene
ND
ug/L
2.0
1
06/14/19 22:55
75-35-4
Elhylbenzene
ND
ug/L
1.0
1
06/14/19 22:55
100-41-4
Methylene Chloride
ND
ug/L
5.0
1
06/1411922:55
75-09-2
Tetrachloroethene
NO
ug/L
2.0
1
06/14/19 22:55
127-18-4
Toluene
NO
ug/L
1.0
1
06/14/19 22:55
108-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 05:37 PM without the written consent of Pace Analytical Services, LLC. Page i 1 of 26

aceAnalytical e
m ..pecweb&cnm
ANALYTICAL RESULTS
Project: Stormwater CUR 6-5-19
Pace Project No.: 92431928
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: SDO-6
Lab ID: 92431928004 Collected: 06/05119 17:22
Received: 06/06/19 11:03 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Oual
624 Volatile Organics
Analytical Method:
EPA 624.1
1,1,1-Trichloroethane
ND
ug/L
2.0
1
06/14/19 22:55
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1
06114/1922:55
79-00-5
Trichloroethene
ND
ug/L
2.0
1
06/14/19 22:55
79-01-6
Surrogates
4-Bromofluorobenzene(S)
123
%
70-130
1
06/14/19 22:55
460-00-4
Toluene-d8(S)
98
%
70-130
1
06/14/19 22:55
2037-26-5
1,2-Dichloroethane-d4 (S)
109
e/
70-130
1
06/14/19 22:55
17060-07-0
Date: 06/19/2019 05:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 26

�P aceAnalyticalB
wwxpacafebaoom
li
ANALYTICAL RESULTS
Project: Stormwater DU 6-5-19
Pace Project No.: 92431928
Pace Analytical services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: SOO-7
Parameters
Lab ID: 92431928005 Collected: 06/05/19 18:00
Results Units Report Limit OF
Received: 06/06/19 11:03 Matrix: Water
Prepared Analyzed CAS No. Oual
•2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
10
mg/L
2.8
1
06/07/19 12:49
11664 SGT-HEM, TPH
Analytical Method: EPA 16648
Total Petroleum Hydrocarbons
NO
mg/L
4.8
1
06/11/19 06:29
200.7 MET ICP
Analytical Method:
EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Copper
8.4
ug/L
5.0
1
06/11/19 23:04
06113/19 20:25
7440-50-8
Lead
NO
ug/L
5.0
1
06/11/19 23:04
06113/1920:25
7439-92-1
Zinc
24.8
ug/L
10.0
1
06/11/19 23:04
06/13/19 20:25
7440-66-6
625 RVE
Analytical Method:
EPA625.1 Preparation
Method:
EPA625.1
11
Anthracene
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:34
120-12-7
Butylbenzylphthalate
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:34
85-68-7
2-Chlorophenol
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:34
95-57-8
1,2-Dichlorobenzene
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:34
95-50-1
6-Dichlorobenzene
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:34
541-73-1
2,4-Dichlorophenol
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:34
120-83-2
Di-n-butylphthalate
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:34
84-74-2
11,2-Diphenylhydrazine
NO
ug/L
5.0
1
06/1111920:16
06/1311919:34
122-66-7
1ris(2-Ethylhexypphthalate
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:34
117-81-7
Isophorone
NO
ug/L
10.0
1
06/11/1920*16
06/13/19 19:34
78-59-1
Naphthalene
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:34
91-20-3
2-Nitrophenol
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:34
88-75-5
4-Nitrophenol
NO
ug/L
50.0
1
06/11/19 20:16
06113/1919:34
100-02-7
Pentachlorophenol
NO
ug/L
10.0
1
06/11/19 20:16
06/13/19 19:34
87-86-5
Phenol
NO
ug/L
5.0
1
06/1111920:16
06/1311919:34
108-95-2
1;2,4-Trichlorobenzene
NO
ug/L
5.0
1
06/11/19 20:16
06/13/19 19:34
120-82-1
2!4,6-Trichlorophenol
NO
ug/L
10.0
1
06/11/19 20:16
06/13/19 19:34
88-06-2
Surrogates
Nitrobenzene-d5 (S)
77
%
10-120
1
06/11/19 20:16
06/13/19 19:34
4165-60-0
2-Fluorobiphenyl(S)
68
%
15-120
1
06/11/19 20:16
06/13/19 19:34
321-60-8
Terphenyl-dl4(S)
80
%
11-131
1
06/1111920:16
06/13/19 19:34
1718-51-0
Phenol-d6(S)
40
%
10-120
1
06/11/19 20:16
06/13/19 19:34
13127-88-3
2-Fluorophenol (S)
57
%
10-120
1
06/11/19 20:16
06113/1919:34
367-12-4
2,4,6-Tdbromophenol (S)
81
%
10-137
1
06/11/19 20:16
06/13/19 19:34
118-79-6
624 Volatile Organics
Analytical Method:
EPA 624.1
Carbon tetrachloride
NO
ug/L
2.0
1
06/14/19 23:13
56-23-5
Chloroform
NO
ug/L
5.0
1
06/14/19 23:13
67-66-3
Dibromochloromethane
NO
ug/L
2.0
1
06/14/19 23:13
124-48-1
1,2-Dichloroethane
NO
ug/L
2.0
1
06/14/19 23:13
107-06-2
1',1-Dichloroethene
NO
ug/L
2.0
1
06/14/19 23:13
75-35-4
Ethylbenzene
NO
ug/L
1.0
1
06/14/19 23:13
100-41-4
Methylene Chloride
NO
ug/L
5.0
1
06/14/19 23:13
75-09-2
Tetrachloroethene
NO
ug/L
2.0
1
06/14/19 23:13
127-18-4
Toluene
NO
ug/L
1.0
1
06/1411923: 13
108-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 05:37 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 26
II

aceAnalytical e
wwnpacelaDscam
ANALYTICAL RESULTS
Project: Stormwater DUR 6-5-19
Pace Project No.: 92431928
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: SDO-7
Lab ID: 92431928005 Collected: 06/05/19 18:00
Received: 06/06/19 11:03 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Dual
624 Volatile Organics
Analytical Method:
EPA 624.1
1,1,1-Trichloroethane
ND
ug/L
2.0
1
06/14/19 23:13
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1
06/14/19 23:13
79-00-5
Trichlorcethene
ND
ug/L
2.0
1
06/14/19 23:13
79-01-6
Surrogates
4-Bromofluorobenzene(S)
87
%
70-130
1
06/14/19 23:13
460-00-4
Toluene-d8(S)
101
%
70-130
1
06/14/19 23:13
2037-26-5
1,2-Dichloroethane-d4(S)
103
%
70-130
1
06/14/19 23:13
17060-07-0
Date: 06/19/2019 05:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 26

i
aceAnalytical
wwxpeceleDsrom
i
QUALITY CONTROL DATA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Stormwater DUR 6-5-19
Pace Project No.: 92431928
QC Batch: 479759
Analysis Method:
SM 254OD-2011
QC Batch Method: SM 254OD-2011
Analysis Description:
2540D Total Suspended Solids
'Associated Lab Samples: 92431928001, 92431928002, 92431928004, 92431928005
METHOD BLANK: 2596325
Matrix: Water
Associated Lab Samples: 92431928001, 92431928002, 92431928004, 92431928005
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
�ITotal Suspended Solids mg/L
ND 2.5
06/07/19 12:52
LABORATORY CONTROL SAMPLE: 2596327
Spike LCS
LCS %Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids mg/L
250 248
99 90-110
SAMPLE DUPLICATE: 2596328
92431677001
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
(Total Suspended Solids
mg/L
ND
ND
5
'SAMPLE DUPLICATE: 2596329
92432013001
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Suspended Solids
mg/L
11.8
13.2 11
5 D6
Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/19/2019 05:37 PM without the written consent of Pace Analytical Services, I.I.C. Page 15 of 26

aceAnalXical e
w ..pscslebamm
QUALITY CONTROL DATA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Stormwater DUR 6-5-19
Pace Project No.: 92431928
QC Batch: 480605
Analysis Method:
SM 254OD-2011
OC Batch Method: SM 254OD-2011
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92431928003
METHOD BLANK: 2599961
Matrix:
Water
Associated Lab Samples: 92431928003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
NO
2.5 06/12/19 09:53
LABORATORY CONTROL SAMPLE: 2599962
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250
274
110 90-110
SAMPLE DUPLICATE: 2599963
92431729001
Cup
Max
Parameter
Units
Result
Result
RPD RPD Qualifiers
Total Suspended Solids
mg/L
NO
NO 5
SAMPLE DUPLICATE: 2599964
92431813003
Cup
Max
Parameter
Units
Result
Result
RPD RPD Qualifiers
Total Suspended Solids
mg/L
64.7
67.5 4 5
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 05:37 PM without the written consent of Pace Analytical Services, -I-C. Page 16 of 26

aceAnalytical.
www.pealeeacom
QUALITY CONTROL DATA
Project: Stormwater DUR 6-5-19
,Pace Project No.: 92431928
OC Batch: 480298 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH
,Associated Lab Samples: 92431928001, 92431928002, 92431928003, 92431928004, 92431928005
METHOD BLANK: 2598729 Matrix: Water
'Associated Lab Samples: 92431928001, 92431928002, 92431928003, 92431928004, 92431928005
a Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
'Total Petroleum Hydrocarbons mg/L ND 4.8 06/11/19 06:24
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE:
2598730
Spike
LCS
LCS
% Rec
Parameter
Units
Conic.
Result
a/ Rec
Limits
Qualifiers
,Total Petroleum Hydrocarbons
mg/L
19.2
20.0
104
64-132
MATRIX SPIKE SAMPLE:
2598731
35473405001 Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits
Total Petroleum Hydrocarbons
mg/L
_
4.8U 19.2
20.5
100
64-132
h
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 05:37 PM without the written consent of Pace Analytical Services, LLC.
Qualifiers
Page 17 of 26

aceAnalytical o
wwvpaceleescom
QUALITY CONTROL DATA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Stormwater DUR 6-5-19
Pace Project No.: 92431928
QC Batch: 480528
Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994
Analysis Description: 2001 MET
Associated Lab Samples: 92431928001,92431928002,92431928003,92431928004,92431928005
METHOD BLANK: 2599739
Matrix: Water
Associated Lab Samples: 92431928001, 92431928002, 92431928003, 92431928004, 92431928005
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Copper ug/L
NO 5.0
06/13/1919:47
Lead ug/L
ND 5.0
06/13/1919:47
Zinc ug/L
ND 10.0
06/13/1919:47
LABORATORY CONTROL SAMPLE: 2599740
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Copper ug/L
500 488
98 85-115
Lead ug/L
500 480
96 85-115
Zinc ug/L
500 496
99 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2599741
2599742
MS MSD
92431825001
Spike Spike MS
MSD MS MSD
% Rec
Max
Parameter Units Result
Conc. Conc, Result
Result % Rec % Rec
Limits
RPD RPD Qual
Copper ug/L 34.8
500 500 581
597 109 112
70-130
3 20
Lead ug/L NO
500 500 379
392 76 78
70-130
3 20
Zinc ug/L NO
500 500 411
427 82 85
70-130
4 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2599743
2599744
MS MSD
92431928001
Spike Spike MS
MSD MS MSD
e/ Rec
Max
Parameter Units Result
Conc Conc. Result
Result % Rec e/ Rec
Limits
RPD RPD Qual
Copper ug/L 11.2
500 500 521
512 102 100
70-130
2 20
Lead ug/L ND
500 500 498
498 99 99
70-130
0 20
Zinc ug/L 158
500 500 665
680 102 105
70-130
2 20
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 05:37 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 26

71ac,
Analytical
www.pemkbs.com
II
QUALITY CONTROL DATA
(Project: Stormwater DUR 6-5-19
Pace Project No.: 92431928
IQC Batch: 481255
Analysis Method:
EPA 624.1
:OC Batch Method: EPA 624.1
Analysis Description:
624 MSV
,Associated Lab Samples: 92431928001, 92431928002, 92431928003, 92431928004, 92431928005
METHOD BLANK: 2603223
Matrix: Water
,,Associated Lab Samples: 92431928001, 92431928002, 92431928003, 92431928004, 92431928005
Blank Reporting
;I Parameter
Units
Result Limit
Analyzed
'1,1,1-Trichloroethane
ug/L
NO
2.0
06/1411921:26
,11,1,2-Trichloroethane
ug/L
NO
2.0
06/14/19 21:26
,1,1-Dichloroethene
ug/L
NO
2.0
0611411921:26
1,2-Dichloroethane
ug/L
NO
2.0
06/14/19 21:26
:Carbon tetrachloride
ug/L
NO
2.0
06/14/19 21:26
Chloroform
ug/L
NO
5.0
06/14/19 21:26
Dibromochloromelhane
ug/L
NO
2.0
06/14/19 21:26
Ethylbenzene
ug/L
NO
1.0
06/14119 21:26
Methylene Chloride
ug/L
NO
5.0
06/14/19 21:26
Tetrachloroethene
ug/L
NO
2.0
06/14/19 21:26
'Toluene
ug/L
NO
1.0
06/14/19 21:26
'Trichloroethene
ug/L
NO
2.0
06/14/19 21:26
,1,2-Dichloroethane-d4 (S)
%
107
70-130
06/14/19 21:26
'4-Bromofluorobenzene (S)
%
100
70-130
06/14/19 21:26
Toluene-d8 (S)
%
` 94
70-130
06/14/19 21:26
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2603224
Units
Spike
Conc.
LCS
Result
LCS
% Rec
e/ Rec
Limits
1,1,1-Trichloroethane
ug/L
20
17.9
90
70-130
,1, 1,2-Trichloroethane
ug/L
20
19.2
96
70-130
1,1-Dichloroethene
ug/L
20
20.0
100
50-150
1,2-Dichloroethane
ug/L
20
18.2
91
49-155
Carbon tetrachloride
ug/L
20
18.6
93
70-130
Chloroform
ug/L
20
19.2
96
70-135
Dibromochloromelhane
ug/L
20
18.5
92
70-135
Ethylbenzene
ug/L
20
18.8
94
60-140
Methylene Chloride
ug/L
20
18.0
90
60-140
Tetrachloroethene
ug/L
20
16.9
84
70-130
Toluene
ug/L
20
18.7
93
70-130
Trichloroethene
ug/L
20
18.8
94
65-135
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene(S)
%
102
70-130
;Toluene-d8(S)
%
100
70-130
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Qualifiers
Results presentee on this page are In the unite indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 05:37 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 26
f

aceAnalytical
ieww.pecelabsmm
QUALITY CONTROL DATA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Stormwater DUR 6-5-19
Pace Project No.: 92431928
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2603753
2603754
MS
MSD
92431481001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conic.
Result
Result
%Rec
% Rec
Limits
RPD
RPD Dual
1,1,1-Trichloroethane
ug/L
ND
20
20
16.0
16.9
80
85
52-162
5
36
1,1,2-Trichloroethane
ug/L
ND
20
20
15.8
16.8
79
84
52-150
6
45
1,1-Dichloroethene
ug/L
ND
20
20
18.0
18.8
90
94
1-234
4
32
1,2-Dichloroethane
ug/L
ND
20
20
16.3
17,0
81
85
49-155
5
49
Carbon tetrachloride
ug/L
ND
20
20
17.0
17.4
85
87
70-140
2
41
Chloroform
ug/L
ND
20
20
17.7
18.3
88
91
51-138
3
54
Dibromochloromethane
ug/L
ND
20
20
13.4
13.6
67
68
53-149
2
50
Ethylbenzene
ug/L
ND
20
20
16.1
16.3
81
82
37-162
1
63
Methylene Chloride
ug/L
ND
20
20
16.7
16.8
83
84
1-221
1
28
Tetrachloroethene
ug/L
ND
20
20
15.3
15.3
76
76
64-148
0
39
Toluene
ug/L
ND
20
20
16.0
16.7
80
84
47-150
4
41
Trichloroethene
ug/L
ND
20
20
16.2
16.6
81
83
70-157
2
48
1,2-Dichloroethane-d4 (S)
%
93
94
70-130
4-Bromoftuorobenzene (S)
%
108
108
70-130
Toluene-d8 (S)
%
102
104
70-130
Results presented on this page are in the units indicated by the "Unix' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 05:37 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 26

aceAnalytical
,1 aarw.peabbsoom
QUALITY CONTROL DATA
,Project: Stormwater OUR 6-5-19
IIPace Project No.: 92431928
QC Batch: 480430 Analysis Method: EPA625.1
,QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Associated Lab Samples: 92431928001, 92431928002, 92431928003, 92431928004, 92431928005
'METHOD BLANK: 2599289 Matrix: Water
Associated Lab Samples: 92431928001, 92431928002, 92431928003, 92431928004, 92431928005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,2,4-Trichlorobenzene
ug/L
ND
5.0
06/12/19 13:18
12-Dichlorobenzene
ug/L
NO
5.0
06112/19 13:18
;1,2-Diphenylhydrazine
ug/L
NO
5.0
06/12/19 13:18
1,3-Dichlorobenzene
ug/L
NO
5.0
06/12/19 13:18
2,4,6-Trichlorophenol
ug/L
ND
10.0
06/12/19 13:18
2,4-Dichlorophenol
ug/L
ND
5.0
06/12/19 13:18
2-Chlorophenol
ug/L
ND
5.0
06/12/19 13:18
2-Nitrophenol
ug/L
NO
5.0
06112/1913:18
4-Nitrophenol
ug/L
NO
50.0
06/12/1913:18
Anthracene
ug/L
NO
5.0
06/12/19 13:18
bis(2-Ethylhexyl)phthalate
ug/L
NO
5.0
06/12/191318
Butylbenzylphtha late
ug/L
NO
5.0
06/121191318
Di-n-butylphthalate
ug/L
NO
5.0
06/12/19 13:18
Isophorone
ug/L
ND
10.0
06/12/19 13:18
Naphthalene
ug/L
NO
5.0
06112/1913:18
Pentachlorophenol
ug/L
NO
10.0
06/12/19 13:18
Phenol
ug/L
NO
5.0
06112/1913:18
2,4,6-Tribromophenol(S)
%
81
10-137
06/12/19 13:18
2-Fluorobiphenyl (S)
%
81
15-120
06/12/19 13:18
2-Fluorophenol(S)
%
77
10-120
06/12/19 13:18
Nitrobenzene-d5(S)
%
86
10-120
06/1211913A8
Phenol-d6 (S)
e/
59
10-120
06/12/19 13:18
Terphenyl-dl4 (S)
e/
98
11-131
06/12/19 13:18
Pace Analytical services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE & LCSD:
a
Parameter
2599290
Spike
Units Conc.
2599291
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
34.5 29.5
69
59
44-142
16
30
1,2-Dichlorobenzene
ug/L
50
34.3 28.8
69
58
32-129
17
30
1,2-Diphenylhydrazine
ug/L
50
64.9 55.9
130
112
25-150
15
30
1,3-Dichlorobenzene
ug/L
50
32.7 28.0
65
56
1-172
15
30
2,4,6-Trichlorophenol
ug/L
50
45.5 36.5
91
73
37-144
22
30
2,4-Dichlorophenol
ug/L
50
44.2 34.4
88
69
1-191
25
30
2-Chlorophenol
ug/L
50
44.5 34.8
89
70
23-134
24
30
2-Nitrophenol
ug/L
50
44.2 36.2
88
72
29-162
20
30
4-Nitrophenol
ug/L
250
189 165
76
66
1-132
14
30
Anthracene
ug/L
50
47.2 40.6
94
81
1-166
15
30
bis(2-Ethylhexygphlhalate
ug/L
50
51.4 46.1
103
92
8-158
11
30
Butylbenzylphthalate
ug/L
50
53.6 48.8
107
98
1-152
9
30
Di-n-butylphthalate
ug/L
50
47.6 42.0
95
84
1-118
12
30
� Results presented on this page are in the
units Indicated by the "Units"
column except where an alternate unit
Is
presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in full,
Dale: 06/19/2019 05:37 PM
without the written consent of Pace Analytical
Services, U.C.
Page 21 of 26

(�5ace Analytical
w p&o%abs.com
QUALITY CONTROL DATA
Project: Stormwater OUR 6-5-19
Pace Project No.: 92431928
Pace Analytical Services-, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE & LCSD:
2599290
2599291
Spike
-CS
LCSD
1-CS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Isophorone
ug/L
50
39.8
31.6
80
63
21-196
23
30
Naphthalene
ug/L
50
41.1
33.8
82
68
21-133
19
30
Pentachlorophenol
ug/L
100
104
91.1
104
91
14-176
14
30
Phenol
ug/L
50
31.0
24.8
62
50
5-112
22
30
2,4,6-Tribromophenol (S)
%
101
82
10-137
2-Fluorobiphenyl (S)
%
80
61
15-120
2-Fluorophenol(S)
%
77
57
10-120
Nitrobenzene-d5(S)
%
89
66
10-120
Phenol-d6 (S)
%
60
45
10-120
Terphenyl-dtb (S)
%
96
83
11-131
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 05:37 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 26

lan
eAnalytical
it wwwpeWeEsoom
i
QUALIFIERS
Project: Stormwater DUR 6-5-19
Pace Project No.: 92431928
DEFINITIONS
Pace Analytical services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
j; MDL- Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
i� S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
p Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 05:37 PM without the written consent of Pace Analytical Services, LLC.
i
Page 23 of 26

aceAnalytical e
mrwpacelabs.o
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Stormwater DUR 6-5-19
Pace Project No.: 92431928
Pace Analytical Services, LLC
6701 Conference: Drive
Raleigh, NC 27607
(919)8344984
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92431928001
S130-1
SM 254OD-2011
479759
92431928002
SDO-2
SM 2540D-2011
479759
92431928003
S130-5
SM 254OD-2011
480605
92431928004
SDO-6
SM 2540D-2011
479759
92431928005
SDO-7
SM 2540D-2011
479759
92431928001
SDO-1
EPA 16646
480298
92431928002
SDO-2
EPA 1664E
480298
92431928003
SOO-5
EPA 1664E
480298
92431928004
SDO-6
EPA 1664B
480298
92431928005
SDO-7
EPA 1664B
480298
92431928001
SDO-1
EPA 200.7 Rev 4.4 1994
480528
EPA 200.7 Rev 4.4 1994
480554
92431928002
SDO-2
EPA 200.7 Rev 4A 1994
480528
EPA 200.7 Rev 4.4 1994
480554
92431928003
SDO-5
EPA 200.7 Rev 4.41994
480528
EPA 200.7 Rev 4.41994
480554
92431928004
SDO-6
EPA 200.7 Rev 4A 1994
480528
EPA 200.7 Rev 4.4 1994
480554
92431928005
SDO-7
EPA 200.7 Rev 4.4 1994
480528
EPA 200.7 Rev 4.4 1994
480554
92431928001
SDO-1
EPA625.1
480430
EPA625A
480653
92431928002
SDO-2
EPA625.1
480430
EPA 625.1
480653
92431928003
SDO-5
EPA 625.1
480430
EPA 625.1
480653
92431928004
SDO-6
EPA 625.1
480430
EPA 625.1
480653
92431928005
S100-7
EPA625.1
480430
EPA 625A
480653
92431928001
S130-1
EPA624.1
481255
92431928002
S130-2
EPA 624.1
481255
92431928003
SDO-5
EPA 624A
481255
92431928004
SDO-6
EPA 624.1
481255
92431928005
SDO-7
EPA 624A
481255
Date: 06/19/2019 05:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 24 of 26

WOW 92431928
l 924319ta
QIAU"W-Cn=Y Atalyeral Reglcrt Dauua*
wl3scm-Alrrv.ms./1�. bmlmtmamlbseb -
�.-
Irev lbm
PaceAnaWc, l
b. I3iLLPOP3AaD-(asole satdbiev'66
ALL SHADED AREAS ale fa IAS USE ONLY
m^mm+: tw. rtsaft,.d:mta.
R 1 313 R 1 1-1 1 1 1
Ilqul T¢1tme6aFv
F>m0 T¢�mn
�rrmamTmm:OJ.b..>a. Plml.w..m, DIMv�lmwmµ MI ramn.pmt4 PI ��
RI•.....�Nadm tl..l..[Pl.m..arbm Dl.o+Wmmuc mv. Dl.mmNo.elYc
r T¢
Cc3marbHAl1�.®YSa®M1lw -
I
W .mr.m.Wa.M W m. Pi wer+l.lvl Or .
Ard'xi
WbRtmeA.le _
Damnv Rq.a McgT4.epv: Sbvmm.ta R@KiD
Da.tTNry: TYn. call mDrarc
34L 4alp[ Prc41.<:
Rrta4 erb Pixxm:c/Scutt T v
d.[W/ slqu[nw. ecveoc xyG[
Rac4m..t .mtY Ma
raaRbev btamm�R7
F+mO:Pmoev6Peem.
Ix 1 ra lift
I
1
10
a
muce.r uavnu. v...eoc I Iw
3e[eM Saba
�mlbaed BP brl.tkl.rr P.iv Pmdmm 64tv:QaF®
OW PWS01
ocur.
owlmum rme:
-I
i
v
d I
weCR p
y
�c m^,""
atticl.m vaa:
awl.. amt..a m to
- .IV. K4 Ie rp. �i
T ome ap9Rd
hmmSn.IPY3dl cnt ..
' W9C
FIDOFW>r0001FPIbR.k
P Imq.u. mmmm.. l I..•.: I Sa.m 7Rut on
I
1 Imau:e 11a Dn
Yv
I I1%Iv.
m
P�
.�lo b .a1asW Slue t a
1I13D"Pm 1
I n.o 1 ISPA
1 I lac . �Pwc A.pD
IYii
I6
tD
�
O I
�
1 C9lsIM Mfm[ T . �(
SmOL Cvi�J vva
•MmebbEa Pam[b NwbbubtlskPNdt�YMapWTGlmY tYYni (:MTIMl6wY4ryIN'k
rme.Dnsausmawao lul wro. DwTA.I.w TI�(rs1R®rWv.Pvmu.m Nrl
c4
O
0
-
>hw: +its
:ml[We Yevm[ Y 3
��
O®nv Swmbe
.YVY•
foam,
"'�b�
O led
1
FO-
Z
w tat m.S:
D.b
T6R
D.b
Tae
SDO-1
OT
Grab
6/5/19
6:15
8
x
x
x
x
SDO-2
OT
I Grab
6/5/19
530
8
x
x
x
%
SOO5
OT
Grab
6/5/19
SAO
S
I x
x
x
x
_
SDO6
Or
Grab
6/5/19
5:22
8
X
X
%
x
SDO.7
OT
Grab
6/5/19
6:00
a
x r
X
%
x
I
'
I
OaatetRmmYs/SPWIfabDmsl.�ItleMmtdC
�R WIm Wd: Bw Dry Mmm
LIWINQPS Mv3EM llrl M1m..l: Y If 1VA
wSmvIe Tm M..1dx
OM1nasmRrvmp.
v.daa rn.mlr D,ra
bbTmdh�3:
Tma blu. 1 r a @
m
I yvak�n'It ba- �fi�lt ro nna9'laz
_
i
�.� � tpaa .«.,a'
��''11,,���������� Lt�e�aa)
S.na.snaheJ3b:
[ml.claw mr. Ma¢ 4a
33,,''1�
^'W TIILUYMY T {3m17t1AT.
WdI ..VolRIbMA{6LO I b IIA
FDIFx UPS faun Pv fmb
fmtec 1 a.c.aTae Tap:
1
D.
-
`�
Mfllw115E d6i
c®b:
11103
.b..
.PIwDa4
m:
D-Wl
raRRm. Pamva! r x ru
mnpom
k-6-01c
ma:
IG ll.pl Tsr QIC
.mv bRb.o.w:RY�mta.l
Date/rbc
RmI.N b3/ram..m:O1Vvta.l
D.blrimc
Rm P.ammttnbk —
R
�

TTO: 40CFR469.12
1,2,4 Trichoorobenzene
Chloroform
1,2 Dichlorobenzene
1,3, Dichlorobenzene
1,4, Dichlorobenzene
ethylbenzene
1,1,1 Trichloroethane
methylene chloride
naphthalene
2 Nitrophenol
phenol
bis (2-ethylhexyl) phthalate
tetrachloroethylene
toluene
trichloroethylene
2 Chlorophenol ::
2;4 Dichlorophenol
4 Nifrophenol
pentachlorophenol
di-n-butyl phthalate`
anthracene
1,2 Diphenylhydrazine
isophorone
butyl benzyl pthalate
1,1 Dichloroethylene
2,4,6 Trichlorophenol
Carbon tetrachloride
1,2 Dichloroethane
1,1,2 Trichloroethane
dichlorobromomethane
WO#:92431928 1
PH: KPD Due Date: 06/17/19
I CLIENT: 91-Cree Inc
Page 26 of 26