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HomeMy WebLinkAboutNCG030427_MONITORING INFO_20190702STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V U& 03 C)Llci, DOC TYPE, ❑ HISTORICAL FILE [(MONITORING REPORTS DOC DATE ❑ b a YYYYM M DD Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted 6/03/2019 CERTIFICATE OF COVERAGE NO. NCG03 0 4 2 7 SAMPLE COLLECTION YEAR 2019 FACILITY NAME GKN Driveline Alamance SAMPLE PERIOD ❑ Jan -June ❑ July -Dec COUNTY Alamance n M p /+I� C��1 or ❑� Monthly' month PERSON COLLECTING SAMPLES Mark Kline RECEIUC 6DISCHARGING TO CLASS ❑ORW ` HQW ❑Trout ❑PNA LABORATORY Pace Analytical Lab Cert. # 12;40 JUL 0 2 2019 []zero -flow ❑■ Water Supply ❑SA Comments on sample collection or analysis: ❑Other CENT'kAL FILES DWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 Part A: Stormwater Benchmarks and Monitoring Results ❑ No dischorpe this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxsc Organics Benchmarks - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141 01 5/13/2019 0.25" 6.8 mg/L 7.0 <0.005 mg/L .006 mg/L 0.0974 mg/L <0.005 mg/L N/A ( 02 5/13/2019 1 0.25" 56.2 mg/L 6.9 0.0072 mg/L <0.005 mg/L 0.0336 mg/L 6.6 mg/L N/A 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page-1of3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the ail the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Ricky Hiatt Name (Print name) EHS Coordinator Title (Printtitle) Signatupyo, Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑■ No discharge this period?z Outfall No. Date Sample. Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainol copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee Permit Date: 11/1/2018-05/31/2021 Date SWU-245, last revised 11/1/2018 _Page 3of3__ _ I lit aceAnalytical® wwwpecelebs.cam I) u CERTIFICATIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ,) Project: MONTHLY STORMWATER Pace Project No.: 92429430 1i Charlotte Certification IDs i� 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 �i Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 ii North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 1 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 I I 1 III North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This repel shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.L.C. Page 2 of 13 11 Pace Analytical Services, LLC ® aceAnalytical 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 w vpacelabs cam � (704)875-8062 1, I I SAMPLE ANALYTE COUNT t Project: MONTHLY STORMWATER Pace Project No.: 92429430 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92429430001 OUTFALL 001 EPA 1664E JMS 1 PASI-C EPA 608.3 SEM 29 PASI-C EPA 200.7 Rev 4.41994 SH1 3 PASI-A i EPA 625.1 RES 58 PASI-C EPA 624.1 DLK 34 PASI-C SM 2540D-2011 MJP 1 PASI-A EPA 9040C ECH 1 PASI-A EPA 420.4 Rev 1.0 1993 KDF7 1 PASI-A 92429430002 OUTFALL 002 EPA 1664E JMS 1 PASI-C ,I EPA 608.3 SEM 29 PASI-C ,I EPA 200.7 Rev 4.41994 SH7 3 PASI-A I EPA 625.1 RES 58 PASI-C EPA 624.1 DLK 34 PASI-C SM 254OD-2011 MJP 1 PASI-A EPA 9040C ECH 1 PASI-A ' EPA 420.4 Rev 1.0 1993 KDF1 1 PASI-A I REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 li �I 'I aceAnalytical0 ..pacelabscom I Project: MONTHLY STORMWATER Pace Project No.: 92429430 �Sample: OUTFALL 001 ll Parameters Oil and Grease Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) alpha -Chlordane gamma -Chlordane 4,4'-DDD „4,4'-DDE 4,4'-DDT Dieldrin �IEndosulfan I � Endosulfan II Endosulfan sulfate i Endrin �',Endrin aldehyde Heptachlor ' Heptachlor epoxide ' PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) 1 PCB-1260 (Aroclor 1260) Toxaphene Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) Copper Lead Zinc Acenaphthene IAcenaphthylene 'Anthracene lBenzo(a)anthracene ;Benzo(a)pyrene Be nzo (b)fl uoranthe ne Benzo(g,h,i)perylene Benzo(k)fluoranthene 4-Bromophenylphenyl ether Butyl be nzyl p hth a late 4-Chlo ro-3-methyl phe nol bis(2-C hlo roethoxy) m elh a ne bis(2-Chloroethyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether ,I II I I I.W. 0o'4cu2019 04:45 PM ANALYTICAL RESULTS Lab ID: 92429430001 Results Units Collected: 05/13/19 09:10 Report Limit DF NO mg/L 5.0 1 NO ug/L 0.050 1 ND ug/L 0.050 1 NO ug/L 0,050 1 ND ug/L 0.050 1 NO ug/L 0.050 1 ND ug/L 0.50 1 NO ug/L 0.050 1 ND ug/L 0.050 1 NO ug/L 0.050 1 ND ug/L 0.050 1 ND ug/L 0.050 1 ND ug/L 0.050 1 ND ug/L 0.050 1 ND ug/L 0.050 1 ND ug/L 0.050 1 NO ug/L 0.050 1 ND ug/L 0.050 1 NO ug/L 0.050 1 NO ug/L 0.050 1 NO ug/L 0.50 1 NO ug/L 0.50 1 ND ug/L 0.50 1 ND ug/L 0.50 1 NO ug/L 0.50 1 ND ug/L 0.50 1 ND ug/L 0.50 1 ND ug/L 0.50 1 188 % 10-130 1 118 % 10-130 1 NO ug/L 5.0 1 6.0 ug/L 5.0 1 97.4 ug/L 10.0 1 ND ug/L 5.0 1 ND ug/L 5.0 1 ND ug/L 5.0 1 ND ug/L 5.0 1 ND ug/L 5.0 1 ND ug/L 5.0 1 NO ug/L 5.0 1 NO ug/L 5.0 1 NO ug/L 5.0 1 NO ug/L 5.0 1 NO ug/L 5.0 1 ND ug/L 10.0 1 NO ug/L 5.0 1 ND ug/L 5.0 1 ND ug/L 5.0 1 NO ug/L 5.0 1 S3 REPORT OF LABORATORY ANALYSIS Qualifiers This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L-C. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 13 aceAnalytical wwnpacelabs.cnm ANALYTICAL RESULTS I "i Project: MONTHLY STORMWATER II Pace Project No.: 92429430 Samples OUTFALL 001 i Parameters Lab ID: 92429430001 Results Units Collected: 05/13/19 0910 Report Limit OF Qualifiers Chrysene NO ug/L 5.0 1 Dibenz(a,h)anthracene NO ug/L 5.0 1 3,3'-Dichlorobenzidine NO ug/L 25.0 1 2,4-Dichlorophenol NO ug/L 5.0 1 Diethylphthalale NO uglL 5.0 1 i2,4-Dimethylphenol NO ug/L 10.0 1 Dimethylphthalate NO ug/L 5.0 1 Di-n-butylphthalate NO ug/L 5.0 1 4,6-Dinitro-2-methylphenol NO ug/L 20.0 1 2,4-Dinitrophenol ND ug/L 50.0 1 2,4-Dinitrotoluene NO ug/L 5.0 1 . 2,6-Dinitrololuene NO ug/L 5.0 1 Di-n-octylphthalate NO ug/L 5.0 1 bis(2-Ethylhexyl)phthalate NO ug/L 5.0 1 Fluoranthene NO ug/L 5.0 1 Fluorene NO ug/L 5.0 1 I Hexachloro-1,3-butadiene NO ug/L 5.0 1 ',Hexachlorobenzene NO ug/L 5.0 1 Hexachlorocyclopentadiene NO ug/L 10.0 1 Hexachloroethane NO ug/L 5.0 1 Indeno(1,2,3-cd)pyrene NO ug/L 5.0 1 ,'Ilsophorone NO ug/L 10.0 1 ,Naphthalene NO ug/L 5.0 1 Nitrobenzene NO ug/L 5.0 1 2-Nitrophenol NO ug/L 5.0 1 4-Nilrophenol ND ug/L 50.0 1 N-Nitrosodimethylamine NO ug/L 5.0 1 N-Nitroso-di-n-propylamine NO ug/L 5.0 1 N-Nitrosodiphenylamine NO ug/L 10.0 1 2,2'-Oxybis(1-chloropropane) NO ug/L 5.0 1 Pentachlorophenol NO ug/L 10.0 1 Phenanthrene ND uglL 5.0 1 Phenol NO ug/L 5.0 1 'Pyrene NO ug/L 5.0 1 '1,2,4-Trichlorobenzene NO ug/L 5.0 1 '2,4,6-Trichlorophenol NO ug/L 10.0 1 INitrobenzene-d5(S) 67 % 10-120 1 '.2-Fluorobiphenyl (S) 71 % 15-120 1 'Terphenyl-d 14 (S) 80 % 11-131 1 j Phenol-d6 (S) 41 % 10-120 1 '2-Fluorophenol(S) 56 % 10-120 1 l2,4,6-Tribromophenol(S) 100 % 10-137 1 .Benzene ND ug/L 1.0 1 Bromodichloromethane NO ug/L 2.0 1 !Bromoform ND ug/L 2.0 1 Bromomelhane NO ug/L 2.0 1 Carbon tetrachloride NO ug/L 2.0 1 Chlorobenzene NO ug/L 2.0 1 Chloroethane ND ug/L 2.0 1 REPORT OF LABORATORY ANALYSIS t This report shall not be reproduced, except in full, Dale: 05/29/2019 04:45 PM without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 13 l i aceAnalyical® wwwpacelabs.com II ANALYTICAL RESULTS �IProject: MONTHLY STORMWATER Pace Project No.: 92429430 II Sample: OUTFALL 001 Parameters Lab ID: 92429430001 Collected: 05/13/19 09:10 Results Units Report Limit DF "Chloroform ND ug/L 5.0 1 Chloromelhane ND ug/L 2.0 1 Dibromochloromethane ND ug/L 2.0 1 ,1,2-Dichlorobenzene ND ug/L 2.0 1 1,3-Dichlorobenzene NO ug/L 2.0 1 1,4-Dichlorobenzene NO ug/L 2.0 1 1,1-Dichloroethane ND ug/L 2.0 1 ','1,2-Dichloroethane NO ug/L 2.0 1 1,1-Dichloroethene ND ug/L 2.0 1 cis-1,2-Dichloroethene ND ug/L 2.0 1 trans-1,2-Dichloroethene ND ug/L 2.0 1 '''1,2-Dichloropropane ND ug/L 2.0 1 'cis-1,3-Dichloropropene ND ug/L 2.0 1 l trans-1,3-Dichloropropene ND ug/L 2.0 1 Ethylbenzene ND ug/L 1.0 1 Methylene Chloride ND ug/L 5.0 1 4,1,2,2-Telrachloroethane NO ug/L 2.0 1 Tetrachloroelhene ND ug/L 2.0 1 i Toluene ND ug/L 1.0 1 1,1,1-Trichloroethane ND ug/L 2.0 1 11,1,2-Trichloroethane ND ug/L 2.0 1 iTrichloroethene NO ug/L 2.0 1 lTrichlorofluoromethane NO ug/L 2.0 1 (Vinyl chloride ND ug/L 2.0 1 I4-Bromofluorobenzene (S) 98 % 70-130 1 (Toluene-d8 (S) 101 % 70-130 1 11,2-Dichloroethane-d4 (S) 100 % 70-130 1 ?otal Suspended Solids 6.8 mg/L 2.5 1 �pH at 25 Degrees C 7.0 Std. Units 0.10 1 Ph'henol ND mg/L 0.020 1 m H3 REPORT OF LABORATORY ANALYSIS Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 I This report shall not be reproduced, except in full, Dale: 05/29/2019 04:45 PM without the written consent of Pace Analytical Services, L-C. Page 6 of 13 � laceAnalyficale w»wpacelabs.cam I Project: MONTHLY STORMWATER �I Pace Project No.: 92429430 ',Sample: OUTFALL 002 Parameters Oil and Grease 1 Aldrin alpha-BHC hbeta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) alpha -Chlordane gamma -Chlordane 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin I Endosulfan I �Endosulfan II Endosulfan sulfate I Endrin Endrin aldehyde ,Heptachlor 1 Heptachlor epoxide IPCB-1016 (Aroclor 1016) ,PCB-1221 (Aroclor 1221) IPCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) IPCB-1248 (Aroclor 1248) IPCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) lToxaphene Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) Copper Lead Zinc Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Be nzo (b)fl uora nth a ne Benzo(g,h,i)perylene Benzo(k)fi uora nth a ne 4-Bromophenylphenyl ether Butyl be nzy Ip hth a late 4-Chloro-3-methylp hen of bi s(2-C h l o roeth oxy) m eth a ne bis(2-Chloroethyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether l� 'I I Date: 05/29/2019 04:45 PM ANALYTICAL RESULTS Lab ID: 92429430002 Results Units Collected: 05/13/19 09:25 Report Limit OF 6.6 mg/L 5.0 1 NO ug/L 0.050 1 NO ug/L 0.050 1 NO ug/L 0.050 1 NO ug/L 0.050 1 NO ug/L 0.050 1 NO ug/L 0.50 1 NO ug/L 0.050 1 ND ug/L 0.050 1 ND ug/L 0.050 1 ND ug/L 0.050 1 NO ug/L 0.050 1 NO ug/L 0.050 1 NO ug/L 0.050 1 NO ug/L 0.050 1 NO ug/L 0.050 1 NO ug/L 0.050 1 ND ug/L 0,050 1 ND ug/L 0.050 1 ND ug/L 0.050 1 ND ug/L 0.50 1 NO ug/L 0.50 1 ND ug/L 0.50 1 ND ug/L 0.50 1 ND ug/L 0.50 1 NO ug/L 0.50 1 NO ug/L 0.50 1 NO ug/L 0.50 1 82 % 10-130 1 58 % 10-130 1 7.2 ug/L 5.0 1 NO ug/L 5.0 1 33.6 ug/L 10.0 1 NO ug/L 5.0 1 ND ug/L 5.0 1 ND ug/L 5.0 1 NO ug/L 5.0 1 NO ug/L 5.0 1 NO ug/L 5.0 1 ND ug/L 5.0 1 ND ug/L 5.0 1 ND ug/L 5.0 1 NO ug/L 5.0 1 NO ug/L 5.0 1 ND ug/L 10.0 1 ND ug/L 5.0 1 NO ug/L 5.0 1 NO ug/L 5.0 1 NO ug/L 5.0 1 REPORT OF LABORATORY ANALYSIS Qualifiers This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, -LC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 13 1 aceAnalytical wwnpacelabs.com ANALYTICAL RESULTS 1 II Project: MONTHLY STORMWATER Pace Project No.: 92429430 Sample: OUTFALL 002. Parameters Lab ID: 92429430002 Results Units Collected: 05/13/19 09:25 Report Limit DF Qualifiers Chrysene NO ug/L 5.0 1 Dibenz(a,h)anthracene ND ug/L 5.0 1 13,3'-Dichlorobenzidine NO ug/L 25.0 1 �2,4-Dichlorophenol NO ug/L 5.0 1 Diethylphthalate ND ug/L 5.0 1 '2,4-Dimethylphenol NO ug/L 10.0 1 Dimelhylphthalate NO ug/L 5.0 1 'IDi-n-butylphthalate NO ug/L 5.0 1 '4,6-Dinitro-2-methylphenol NO ug/L 20.0 1 2,4-Dinitrophenol NO ug/L 50.0 1 2,4-Dinitrotoluene NO ug/L 5.0 1 2,6-Dinitrotoluene NO ug/L 5.0 1 Di-n-octylphthalale NO ug/L 5.0 1 �,bis(2-Ethylhexypphthalate NO ug/L 5.0 1 Fluoranthene NO ug/L 5.0 1 Fluorene NO ug/L 5.0 1 Hexachloro-1,3-butadiene NO ug/L 5.0 1 Hexachlorobenzene ND ug/L 5.0 1 Hexachlorocyclopentadiene NO ug/L 10.0 1 Hexachlomethane NO ug/L 5.0 1 lndeno(1,2,3-cd)pyrene NO ug/L 5.0 1 Isophorone NO ug/L 10.0 1 Naphthalene NO ug/L 5.0 1 Nitrobenzene NO ug/L 5.0 1 2-Nitrophenol ND ug/L 5.0 1 '4-Nitrophenol NO ug/L 50.0 1 N-Nitrosodimethylamine NO ug/L 5.0 1 ;N-Nitroso-di-n-propylamine NO ug/L 5.0 1 'N-Nilrosodiphenylamine NO ug/L 10.0 1 )2,2'-Oxybis(1-chloropropane) NO ug/L 5.0 1 IPenlachlorophenol ND ug/L 10.0 1 IPhenanthrene NO ug/L 5.0 1 lPhenol NO ug/L 5.0 1 iPyrene NO ug/L 5.0 1 .1,2,4-Trichlorobenzene NO ug/L 5.0 1 2,4,6-Trichlorophenol ND ug/L 10.0 1 Nitrobenzene-d5 (S) 54 % 10-120 1 .2-Fluorobiphenyl(S) 51 % 15-120 1 7erphenyl-d14 (S) 52 % 11-131 1 Phenol-d6 (S) 31 % 10-120 1 2-Fluorophenol(S) 43 % 10-120 1 2,4,6-Tribromophenol(S) 65 % 10-137 1 Benzene NO ug/L 1.0 1 Bromodichloromelhane NO ug/L 2.0 1 Bromoform NO ug/L 2.0 1 Bromomethane NO ug/L 2.0 1 Carbon tetrachloride NO ug/L 2.0 1 Chlorobenzene NO ug/L 2.0 1 Chloroethane t NO ug/L 2.0 1 REPORT OF LABORATORY ANALYSIS it This report shall not be reproduced, except in full, Date: 05/29/2019 04:45 PM without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 13 II II II aceAnalytical® I vmwpacelabs.wm l!, i I Ii Project: MONTHLY STORMWATER II Pace Project No.: 92429430 Sample: OUTFALL 002 Parameters Chloroform II Chloromethane Di b romochloro melha ne 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene I.1,1-Dichloroethane l,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 'cis-1,3-Dichloropropene !Itrans-1,3-Dichloropropene Ethylbenzene Methylene Chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichlo roetha ne 1 1 2-Trich to roetha n e �Trichloroethene Trichlorofluoromethane Vinyl chloride �4-Bromofiuorobenzene (S) Toluene -rift (S) i11,2-Dichloroethane-d4 (S) ,Total Suspended Solids pH at 25 Degrees C Phenol ANALYTICAL RESULTS Lab ID: 92429430002 Results Units Collected: 05/13/19 09:25 Report Limit DF NO ug/L 5.0 1 NO ug/L 2.0 1 NO ug/L 2.0 1 NO ug/L 2.0 1 NO ug/L 2.0 1 NO ug/L 2.0 1 ND ug/L 2.0 1 NO ug/L 2.0 1 NO ug/L 2.0 1 NO ug/L 2.0 1 NO ug/L 2.0 1 ND ug/L 2.0 1 NO ug/L 2.0 1 NO ug/L 2.0 1 ND ug/L 1.0 1 ND ug/L 5.0 1 ND ug/L 2.0 1 NO ug/L 2.0 1 NO ug/L 1.0 1 NO ug/L 2.0 1 NO ug/L 2.0 1 ND ug/L 2.0 1 ND ug/L 2.0 1 NO ug/L 2.0 1 99 % 70-130 1 100 % 70-130 1 102 % 70-130 1 56.2 mg/L 5.0 1 6.9 Std. Units 0.10 1 NO mg/L 0.020 1 H3 REPORT OF LABORATORY ANALYSIS Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, Date: 05/29/2019 04:45 PM without the written consent of Pace Analytical Services, L-C. Page 9 of 13 li aceAnalytical yr Pecelabs.War QUALIFIERS i Project: MONTHLY STORMWATER , Pace Project No.: 92429430 DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit, PQL- Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S -Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up 'I U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA ,I Method 8260, N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. I LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. {I Rt RPD value was outside control limits. 9 S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample. q n REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/29/2019 04:45 PM without the written consent of Pace Analytical Services, LLC, I ' Page 10 of 13 Document Name: Document Revised: fel—ly 71101, Sample Condition Upon Receipt(SCUR) Pa o ] of 2 y :aceMal}?cala Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersvillex Raleigh❑ Mechanicsville❑ „ Client Name. -�� lw®#:924.29430 • C �V Project R � ❑Cier: iah ,❑FeC Ex UPS ❑❑UUSP r— `❑/Client II�II� I�� I I�III III I �II 92428430 Custody Seal Present? Dyes Seals Intact? []Yesa / Date/Initials Person Examining Contents: 'V j`a �C `l Packing Material: []Bubble Wrap ble Bags ❑None ❑ Other Biological Tissue Frozen? TheirnometRr•: []Yes(]No-4�1({jA N§f GUMD: 92TO48t/ Type of Ice: KWet ❑Blue ❑None Cooler Temp('C): '(l y.- .cS Correction Factor: Add/Subtract('C) 0.0 v •. Tempshoule be out of to peritng toVC mpl Cooler Temp Corrected ('C): "�` ❑Samples ou[at temp criteria. Samples an ice, cooling process hashegun USDA Regulated Soil �A, water sample) Did samples erg ate in'a quarantine zone within the United Slates: CA, NY, or SC (check maps)? Did samples originate from a foreign source pmer 11 ally, r1.._, t1 i..u,aue uv..an end P,mnn Rlrn17r�1Yrs n Comments/Discre anc : Chain of Custody Present? es []NO ON/A 1. Samples Arrived within Hold Time? es ❑No ❑N/A 2. Short Hold Time Analysis(<71 hr.j? Yes o N/A 3. Rush Turn Around Time Requested? Dyes o ❑N/A 4. Sufficient Volume? rs QN. ❑N/A S. Correct Containers Used? -Pace Containers Used? a []No Na QN/A ❑N/A Containers Intact? eN []NO ❑N/A 7, Dissolved analysis: Samples Field Filtered? ❑Yes []NO /A a. Sample Labels Match COC? -Includes Date/Time/ID/Ana sis Matrix: II []NO V ❑N/A 9. Headspace in VOA Vials (>5-6mm)? s ❑No ❑/AN 10. Trip Blank Present? Trip Blank Custody Seals Present? []Yes ❑Na Yes Duo N/A /A 33. COMMENTS/SAMPLE DISCREPANCY r0C Ile( 'P r A C` �IIJIIG Lot ID of Ipllt containers: 'I CLIENT NOTIFICATION/RESOLUTION I !� Person contacted: Date/11me: Field Data Required? ❑Yes ❑NO Project Manager SCURF Review: LL Date: Project Manager SRF Review: Dale: Page 11 of 13 Document Name: Document Revised: February 7, 2018 Sample Condition Upon ReceiptiSCUR) age' of 2 CBAIk73410j� Document No.: Issuing Authority: F-CAR-CS-033-Rev06 Pace Carolinas Quality Office 'Check mark tap half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. E.ceptions: VOA, Coliform,TOC, Oil and Grease, DRO/8015 (waterl DOC, LLHg "Bottom half of box is to list number of bottle Project# WO# : 92429430 PM: MWB Due Date: 05/29/19 CLIENT: 92-OKN L 4 L = � O N a E ] 4 ce 9 � u E m ] G co a L Y E 6 com < i `u ] 4 y N � S Y a ,E IA 6 m � a 3 a E Z 6 m m _ p 2 ID c ' a E N 6 m O N' � o — E V 6 m y 2 y Y E v 1'L m 3 _ U ¢ Z ZY = E Q N U• Q Y s E w •=-I U• Q G 2 V g° E Q E T l'1 Q � a E u H ° Q _ N i 6 E Q E m U• Q V Z Z Ez `A n /a•1 b Q o E OI li O ? o Z ° E P U' > i o E P l7 > Q o o Ei OI 1p C Q � N u Q Q ° > Q U• a n .1 U• > ? 'Q vgi E 1~/1 1 n Z '^ E N 6 M n ,mn ` z aL E ry m Q 9 .e Y g Q of ti Q Q o E N > z m > E U• O 1 I LI c z l' I I N XNN I 3 5 5 6 7 1 e S I \N\\ [I-\\\N-kl \N 10 11 12 pH Adjustment Log for Preserved Samples sample to Type of Preservative pH upon receipt Dale preservallon adjusted Time preservation adjusted Amount of Preservative added Lot 11 Note: Whenewthere is a discrepancy attecvng Nortn Lanllma camp <„ r:,=,,,p,=., e �wr � - •• --•^ •^• ••- •^ Out of hold, incorrect preservative, out of temp, incorrect containers. Page 12 of 13 CHAIN -OF -CUSTODY I Analytical Request Document The Chairtaf-Custody is a LEGAL DOCUMENT. All relevant fields mmt be wmpleted accurately. Sectlon A SeNonSe C R�I�d M� on: Page, I Of Cwqm .. GM Orl"MSAdmanw Report To: Mark Kfine A0O^ Hewf.tft Rd Mebma. NC aac R"W.t�Ag� IF. hlorMW, pm w Looacan NC r I I I T.-I 8 p =emWes Zi SAMPLE I D 7 T T.. Z3 < GATE TA1E n wl 44 x x Ix ix x x x x I I I Ix ix I -IT ;F, Z x x x x x x x a. Pb. I I ey 7 L .1 PPoNT -77 A 4-YLE�J� Astance: Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted y/r/2ars CERTIFICATE OF COVERAGE No.NCG03 0 4 2 7 RECEIVED FACILITY NAME GKN DHveline Alamance COUNTY Alamance PERSON COLLECTING SAMPLES Ricky Hiatt LABORATORY Pace Analytical Lab Cert. # 12:40 11,Mi,rl .iAL FILES Comments on sample collection or analysis: OVVR OLG ION Part A: Stormwater Benchmarks and Monitoring Results Avu 06 2019 SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or Q Monthly' T (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑■ Water Supply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 n No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss Benchmarks - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141 01 6/20/2019 2.0 82.6mg/L 5.5 0.0059 mg/L <0.005 mg/L 0.13 mg/L <0.005 mg/L N/A 02 6/20/2019 2.0 99.3 mg/L 5.4 0.0052 mg/L <0.005 mg/L 0.0554 mg/L <0.005 mg/L N/A ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfali. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Ricky Hiatt Name (Print name) EHS Coordinator Title (Print title) Signature Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n No dischor9e this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches3 New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. see General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 -- - - 'Page2 of-- FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERSTIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal copv of this DMR, including all '1Vo Dischorge"reports within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signatu/4 of Permittee Date Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 _ -Page3 of - - - - li aceAnalytical i~pecelabs.= July 05, 2019 Ricky Hiatt GKN Driveline {4 1067 Trollingwood Hawfield Rd. a Mebane, NC 27302 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 RE: Project: Monthly Stormwater Pace Project No.: 92434143 Dear Ricky Hiatt: Enclosed are the analytical results for sample(s) received by the laboratory on June 21, 2019. This report is a summary of the results based upon our understanding of your data quality objectives. Please contact us if itemized quality control results are needed. These results relate only to the samples included in this report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Dave Bruce, GKN Driveline P REPORT OF LABORATORY ANALYSIS li This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 aceAnalytical® w aacelabs.00m CERTIFICATIONS Project: Monthly Stormwater Pace Project No.: 92434143 Pace Ana lyticaI Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 , Charlotte Certification IDs d 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 I' aceAnalytical wwwpacela6s.cnm I I� I SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: i, Pace Project No.: Monthly Stormwaler 92434143 - Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92434143001 OUTFALL 001 EPA 1664B JMS 1 PASI-C I. EPA 608.3 SEM 29 PASI-C II EPA 200.7 Rev 4.41994 SH1 3 PASI-A EPA 625.1 PKS 58 PASI-C EPA 624.1 SAS 34 PASI-C SM 2540D-2011 JP1 1 PASI-A SM 4500-H+B-2011 SMK 1 PASI-A EPA 420.4 Rev 1.01993 KDR 1 PASI-A 92434143002 OUTFALL 002 EPA 1664B JMS 1 PASI-C EPA 608.3 SEM 29 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A EPA 625.1 PKS 58 PASI-C 'I EPA 624.1 SAS 34 PASI-C SM 25400-2011 JP1 1 PASI-A SM 4500-11+13-2011 SMK 1 PASI-A i� EPA 420.4 Rev 1.01993 KDF1 1 PASI-A Ilil REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, I without the widen consent of Pace Analytical Services, LLC. Page 3 of 13 IJ i ;i aceAnalytical mtw.pacelabs.com i I' Project: Pace Project No.: Monthly Slormwater 92434143 ANALYTICAL RESULTS Sample: OUTFALL 001 Parameters Lab ID: 92434143001 Results Units Collected: 06/20/19 15:22 Report Limit OF Oil and Grease NO mg/L 5.0 1 , Aldrin NO ug/L 0.050 1 alpha-BHC NO ug/L 0.050 1 beta-BHC NO ug/L 0.050 1 delta-BHC NO ug/L 0.050 1 gamma-BHC (Lindane) NO ug/L 0.050 1 „Chlordane (Technical) NO ug/L 0.50 1 ,alpha -Chlordane NO ug/L 0.050 1 ',,gamma -Chlordane NO ug/L 0.050 1 4,4'-DDD NO ug/L 0.050 1 '4,4'-DDE NO ug/L 0.050 1 4,4'-DDT NO ug/L 0.050 1 'Dieldrin NO ug/L 0.050 1 Endosulfan I NO ug/L 0.050 1 �'Endosulfan II ND ug/L 0.050 1 'Endosulfan sulfate NO ug/L 0.050 1 Endrin NO ug/L 0.050 1 Endrin aldehyde NO ug/L 0.050 1 Heptachlor NO ug/L 0.050 1 Heptachlor epoxide ND ug/L 0.050 1 PCB-1016 (Aroclor 1(D16) NO ug/L 0.50 1 PCB-1221 (Aroclor 1221) NO ug/L 0.50 1 PC13-1232 (Aroclor 1232) NO ug/L 0.50 1 PCB-1242 (Aroclor 1242) NO ug/L 0.50 1 PCB-1248 (Aroclor 1248) NO ug/L 0.50 1 PCB-1254 (Aroclor 1254) NO ug/L 0.50 1 ,PCB-1260 (Aroclor 1260) NO ug/L 0.50 1 'Toxaphene NO ug/L 0.50 1 Tetrachloro-m-xylene (S) 64 % 10-130 1 Decachlorobiphenyl (S) 42 % 10-130 1 Copper 5.9 ug/L 5.0 1 ,Lead ND ug/L 5.0 1 'Zinc 130 ug/L 10.0 1 Acenaphthene NO ug/L 5.0 1 Acenaphthylene NO ug/L 5.0 1 'Anthracene ND ug/L 5.0 1 Benzo(a)anthracene NO ug/L 5.0 1 Benzo(a)pyrene NO ug/L 5.0 1 Benzo(b)fiuoranthene NO ug/L 5.0 1 Benzo(g,h,i)perylene NO ug/L 5.0 1 Benzo(k)fiuoranthene NO ug/L 5.0 1 4-Bromophenylphenyl ether NO ug/L 5.0 1 Bulylbenzylphthalate NO ug/L 5.0 1 4-Chloro-3-methylphenol NO ug/L 5.0 1 bis(2-Chlomethoxy)methane NO ug/L 10.0 1 bis(2-Chloroethyl) ether NO ug/L 5.0 1 2-Chloronaphthalene NO ug/L 5.0 1 2-Chlorophenol NO ug/L 5.0 1 4-Chlorophenylphenyl ether NO ug/L 5.0 1 REPORT OF LABORATORY ANALYSIS Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, Dale: 07/05/2019 04:31 PM without the written consent of Pace Analytical Services, -LC. Page 4 of 13 aceAnalytical wwwpecelabs.com I Pace Analytical Services, LLC 9800 Kin cey Ave. Suite 100 HuntersOle, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Monthly Stormwater �I Pace Project No.: 92434143 r Sample: OUTFALL 001 Parameters Lab ID: 92434143001 Results Units Collected: 06/20/1915:22 Report Limit OF Chrysene NO ug/L 5.0 1 Dibenz(a,h)anthracene ND ug/L 5.0 1 3,3'-Dichlorobenzidine ND ug/L 25.0 1 2,4-Dichlorophenol NO ug/L 5.0 1 Diethylphthalale NO ug/L 5.0 1 2,4-Dimethylphenol NO ug/L 10.0 1 Il Dimethylphthalate NO ug/L 5.0 1 Di-n-butylphthalate ND ug/L 5.0 1 4,6-Dinitro-2-methylphenol NO ug/L 20.0 1 i 2,4-Dinitrophenol NO ug/L 50.0 1 12,4-Dinitrotoluene NO ug/L 5.0 1 2,6-Dinitrotoluene NO ug/L 5.0 1 'Di-n-octylphthalate NO ug/L 5.0 1 bis(2-Ethylhexyl)phthalate NO ug/L 5.0 1 Fluoranthene NO ug/L 5.0 1 Fluorene NO ug/L 5.0 1 Hexachloro-1,3-butadiene ND ug/L 5.0 1 Hexachlorobenzene ND ug/L 5.0 1 Hexachlorocyclopentadiene NO ug/L 10.0 1 Hexachloroethane NO ug/L 5.0 1 Indeno(1,2,3-cd)pyrene ND ug/L 5.0 1 'Isophorone NO ug/L 10.0 1 '.Naphthalene NO ug/L 5.0 1 'Nitrobenzene NO ug/L 5.0 1 2-Nilrophenol ND ug/L 5.0 1 4-Nilrophenol NO ug/L 50.0 1 N-Nitrosodimethylamine NO ug/L 5.0 1 N-Nitroso-di-n-propylamine NO ug/L 5.0 1 N-Nitrosodiphenylamine NO ug/L 10.0 1 2,2'-Oxybis(1-chloropropane) NO ug/L 5.0 1 Pentachlorophenol NO ug/L 10.0 1 Phenanthrene ND ug/L 5.0 1 Phenol NO ug/L 5.0 1 Pyrene NO ug/L 5.0 1 1,2,4-Trichlorobenzene NO ug/L 5.0 1 2,4,6-Trichlorophenol NO ug/L 10.0 1 Nitrobenzene-d5 (S) 67 % 10-120 1 2-Fluorobiphenyl(S) 67 % 15-120 1 Terphenyl-d 14 (S) 81 % 11-131 1 Phenol-d6 (S) 38 % 10-120 1 2-Fluorophenol (S) 51 % 10-120 1 2,4,6-Tribromophenol(S) 86 % 10-137 1 Benzene NO ug/L 1.0 1 Bromodichloromethane NO ug/L 2.0 1 Bromoform ND ug/L 2.0 1 Bromomethane NO ug/L 2.0 1 Carbon tetrachloride NO ug/L 2.0 1 Chlorobenzene NO ug/L 2.0 1 Chloroethane II NO ug/L 2.0 1 Qualifiers REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 07/05/2019 04:31 PM without the written consent of Pace Analytical Services, L-C. Page 5 of 13 Pace Analytical Services, LLC aceAnapical® 9800 Kincey Ave. S 28078 100 Huntersville, NC 28078 wmvpacelabs.cam (704)875-9092 ANALYTICAL RESULTS d Project: Monthly Stormwater Pace Project No.: 92434143 „ Sample: OUTFALL 001 Lab ID: 92434143001 Collected: 06/20/19 15:22 Parameters Results Units Report Limit DF Qualifiers Chloroform ND ug/L 5.0 1 Chloromethane ND ug/L 2.0 1 Dibromochloromethane ND ug/L 2.0 1 1,2-Dichlorobenzene ND ug/L 2.0 1 • 1,3-Dichlorobenzene ND ug/L 2.0 1 1,4-Dichlorobenzene ND ug/L 2.0 1 1,1-Dichloroethane ND ug/L 2.0 1 • 1,2-Dichloroethane ND ug/L 2.0 1 •1,1-Dichloroethene ND ug/L 2.0 1 cis-1,2-Dichloroethene ND ug/L 2.0 1 !trans-1,2-Dichloroethene ND ug/L 2.0 1 1,2-Dichloropropane ND ug/L 2.0 1 ibis-1,3-Dichloropropene ND ug/L 2.0 1 trans- 1, 3-Dichloropropene ND ug/L 2.0 1 Ethylbenzene ND ug/L 1.0 1 • Methylene Chloride ND ug/L 5.0 1 1,1,2,2-Telrachloroethane ND ug/L 2.0 1 Tetrachloroethene ND ug/L 2.0 1 Toluene ND ug/L 1.0 1 1,1,1-Trichloroethane ND ug/L 2.0 1 '1,1,2-Trichloroethane ND ug/L 2.0 1 'Trichloreethene ND ug/L 2.0 1 'Trichlorofluoromelhane ND ug/L 2.0 1 'Vinyl chloride ND ug/L 2.0 1 4-Bromofluorobenzene (S) 98 % 70-130 1 Toluene -dB (S) 102 % 70-130 1 11,2-Dichloroethane-d4 (S) 115 % 70-130 1 Total Suspended Solids 82.6 mg/L 8.2 1 pH at 25 Degrees C 5.5 Std. Units 1.0 1 H3 Phenol ND mg/L 0.020 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/05/2019 04:31 PM without the written consent of Pace Analytical Services, L-C. Page 6 of 13 I� a I' 1 II, I aceAnalytical wwwpacelabs.mm I h ANALYTICAL RESULTS Project: Monthly Stormwater Pace Project No.: 92434143 Sample: OUTFALL 002 it Parameters I Lab ID: 92434143002 Results Units Collected: 06/20/19 15:40 Report Limit DF _ Oil and Grease NO mg/L 5.0 1 Aldrin NO ug/L 0.050 1 alpha-BHC NO ug/L 0.050 1 beta-BHC NO ug/L 0.050 1 ��delta-BHC NO ug/L 0.050 1 I' gamma-BHC (Lindane) NO ug/L 0,050 1 ,I Chlordane (Technical) NO ug/L 0.50 1 'alpha -Chlordane NO ug/L 0.050 1 gamma -Chlordane NO ug/L 0.050 1 4,4'-DDD NO ug/L 0.050 1 4,4'-DOE NO ug/L 0.050 1 I'4,4'-DDT NO ug/L 0.050 1 i,Dieldrin NO ug/L 0.050 1 Endosulfan I NO ug/L 0.050 1 Endosulfan II NO ug/L 0.050 1 Endosulfan sulfate NO ug/L 0.050 1 j Endrin NO ug/L 0.050 1 Endrin aldehyde NO ug/L 0.050 1 Heptachlor NO ug/L 0.050 1 Heptachlor epoxide NO ug/L 0.050 1 PCB-1016 (Aroclor 1016) NO ug/L 0.50 1 PCB-1 221 (Aroclor 1221) NO ug/L 0.50 1 PCB-1232 (Aroclor 1232) NO ug/L 0.50 1 PCB-1242 (Aroclor 1242) NO ug/L 0.50 1 PCB-1248 (Aroclor 1248) NO ug/L 0.50 1 PCB-1254 (Aroclor 1254) NO ug/L 0.50 1 IPCB-1260 (Aroclor 1260) NO ug/L 0.50 1 IToxaphene NO ug/L 0.50 1 Tetrachloro-m-xylene (S) 33 % 10-130 1 IDecachlorobiphenyl (S) 41 % 10-130 1 Copper 5.2 ug/L 5.0 1 Lead NO ug/L 5.0 1 Zinc 55.4 ug/L 10.0 1 'Acenaphthene NO ug/L 5.0 1 �Acenaphlhylene NO ug/L 5.0 1 Anlhracene NO ug/L 5.0 1 Benzo(a)anthracene NO ug/L 5.0 1 Benzo(a)pyrene NO ug/L 5.0 1 Benzo(b)fluoranlhene NO ug/L 5.0 1 Benzo(g,h,i)perylene NO ug/L 5.0 1 Benzo(k)fluoranthene NO ug/L 5.0 1 4-Bromophenylphenyl ether NO ug/L 5.0 1 Butylbenzylphthalate NO ug/L 5.0 1 4-Chloro-3-methylphenol NO ug/L 5.0 1 bis(2-Chloroethoxy)methane NO ug/L 10.0 1 bis(2-Chloroethyl) ether NO ug/L 5.0 1 2-Chloronaphthalene NO ug/L 5.0 1 2-Chlorophenol NO ug/L 5.0 1 4-Chlorophenylphenyl ether NO ug/L 5.0 1 Qualifiers REPORT OF LABORATORY ANALYSIS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, Dale: 07/05/2019 04:31 PM without the written consent of Pace Analytical Services, L-C. Page 7 of 13 aceAnalytical w wpacelz6soom �I ANALYTICAL RESULTS Project: Monthly Stormwater Pace Project No.: 92434143 Sample: OUTFALL 002 Lab ID: 92434143002 Collected: 06/20/19 15:40 Parameters Results Units Report Limit DF Chrysene ND ug/L 5.0 1 Dibe nz(a,h) a nth race ne ND ug/L 5.0 1 3,3'-Dichlorobenzidine ND ug/L 25.0 1 2,4-Dichlorophenol ND ug/L 5.0 1 � Diethylphthalate ND ug/L 5.0 1 2,4-Dimethylphenol ND ug/L 10.0 1 Dimethylphthalate ND ug/L 5.0 1 Di-n-butylphthalate �. ND ug/L 5.0 1 4,6-Dinitro-2-methylphenol ND ug/L 20.0 1 2,4-Dinilrophenol ND ug/L 50.0 1 2,4-Dinitrotoluene ND ug/L 5.0 1 2,6-Dinitrotoluene ND ug/L 5.0 1 Di-n-oclylphthalale ND ug/L 5.0 1 bis(2-Ethylhexyl)phthalate ND ug/L 5.0 1 Fluoranthene ND ug/L 5.0 1 Fluorene ND ug/L 5.0 1 �Hexachloro-1,3-buladiene ND ug/L 5.0 1 Hexachlorobenzene ND ug/L 5.0 1 Hexachlorocyclopentadiene ND ug/L 10.0 1 Hexachloroethane ND ug/L 5.0 1 lndeno(1,2,3-cd)pyrene ND ug/L 5.0 1 Isophorone ND ug/L 10.0 1 Naphthalene ND ug/L 5.0 1 Nitrobenzene ND ug/L 5.0 1 12-Nitrophenol ND ug/L 5.0 1 4-Nitrophenol ND ug/L 50.0 1 N-Nitrosodimethylamine ND ug/L 5.0 1 N-Nitroso-di-n-propylamine �N-Nitrosodiphenylamine ND ug/L 5.0 1 ND ug/L 10.0 1 2,2'-Oxybis(1-chloropropane) ND ug/L 5.0 1 Pentachlorophenol ND ug/L 10.0 1 Phenanthrene ND ug/L 5.0 1 Phenol ND ug/L 5.0 1 Pyrene ND ug/L 5.0 1 .1,2,4-Trichlorobenzene ND ug/L 5.0 1 2,4,6-Trichlorophenol ND ug/L 10.0 1 Nitrobenzene-d5(S) 31 % 10-120 1 2-Fluorobiphenyl(S) 31 % 15-120 1 Terphenyl-d14(S) 66 % 11-131 1 Phenol-d6 (S) 20 % 10-120 1 2-Fluorophenol(S) 26 % 10-120 1 2,4,6-Tribromophenol(S) 65 % 10-137 1 Benzene ND uglL 1.0 1 Bromodichloromethane ND ug/L 2.0 1 Bromoform ND ug/L 2.0 1 Bromomethane ND ug/L 2.0 1 Carbon tetrachloride ND uglL 2.0 1 Chlorobenzene ND ug/L 2.0 1 Chloroethane �I ND ug/L 2.0 1 Qualifiers i. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/05/2019 04:31 PM without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 13 aceAnalytical wmvpecelebs.cwn ANALYTICAL RESULTS Project: Monthly Stormwater Pace Project No.: 92434143 t Sample: OUTFALL 002 Lab ID: 92434143002 Collected: 06120/19 15:40 Parameters Results Units Report Limit DF Chloroform ND ug/L 5.0 1 Chloromelhane ND ug/L 2.0 1 Dibromochloromethane ND ug/L 2.0 1 �1,2-Dichlorobenzene ND ug/L 2.0 1 '.1,3-Dichlorobenzene ND ug/L 2.0 1 p 1,4-Dichlorobenzene ND ug/L 2.0 1 1,1-Dichloroethane ND ug/L 2.0 1 1,2-Dichloroethane ND ug/L 2.0 1 i1,1-Dichloroethene ND ug/L 2.0 1 cis-1,2-Dichloroethene ND ug/L 2.0 1 '4ans-1,2-Dichloroethene ND ug/L 2.0 1 :1,2-Dichloropropane ND ug/L 2.0 1 cis-1,3-Dichloropropene ND ug/L 2.0 1 trans-1,3-Dichloropropene ND ug/L 2.0 1 'Ethylbenzene ND ug/L 1.0 1 • Methylene Chloride NO ug/L 5.0 1 1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 Tetrachloroethene - ND ug/L 2.0 1 Toluene ND ug/L 1.0 1 1,1,1-Trichloroethane ND ug/L 2.0 1 1,1,2-Trichloroethane ND ug/L 2.0 1 Trichloroethene ND ug/L 2.0 1 Trichlorohuoromethane ND ug/L 2.0 1 'Vinyl chloride ND ug/L 2.0 1 4-Bromofluorobenzene (S) 99 % 70-130 1 Toluene-d8 (S) 102 % 70-130 1 '1,2-Dichloroethane-d4 (S) 114 % 70-130 1 Total Suspended Solids 99.3 mg/L 17.5 1 pH at 25 Degrees C 5.4 Still. Units 1.0 1 Phenol ND mg/L 0.020 1 Date: 07/05/2019 04:31 PM 1•.91 REPORT OF LABORATORY ANALYSIS Qualifiers This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L-C. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 13 I I ace Analytical � vmwpecelabs.com I QUALIFIERS •i Project: Monthly Stormwater Pace Project No.: 92434143 DEFINITIONS Pace Analytical Services, LLC 9800Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC -Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. I' RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyle in a specific matrix. S- Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) CUP- Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. I. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte 'ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/05/2019 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 13 Document Name: Document Revised: February 7, 2018 Sample Condition upon Receipt(SCUR) Page 1 of 2 aceMaM«l• Document No.: issuing Authority: FCAR-05033-Re 06 Pace Carolinas Duality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersvillen/ Raleigh[] Mechanicsville❑ E Protect I Client Name: Vito# : 92434143 Cqurier. ❑Fed Ex ❑UPS ❑USPS ❑CHent 92.434143 II I III IIII I III ❑Commercial •�❑Pace Other:_ / � I Custody Seal Present? ❑Yes '❑No Seals Intact? ❑Yes QNo t— Date/Initials Verson Examining Contents: / Packing Material: ❑Bubble Wrap❑Bubble Bags ❑None ❑ Other Biological Tissue erotent \' \ I ❑Yes ONO ❑N/A/ Thermometer/. 92T048 Type of Ice: swet ❑blue ❑None ti `❑IP wn10: .� V Cooler Terrip('CI: C It Correction Factor: Add/Subtract ('C) 0.0 Tempshould be above freezing to VC Cooler Temp Corrected ('C): ❑Samples cut of temp onterla. Samples an ice, cooling process hasbegun USDA Regulated Soil (❑,N/A, water sample) Did samples originate In a quarantine tone within the United States: CA, NY, or SC (check mapsl? Did samples originate from a foreign source (Imemationally, ...,ao.,,mn Al 17r1Yac rlNn . Yes NO - - - - - — Comments/Discrepancy: Ruin of Custody Present? 3YU ❑NO QN/A 1. Samples Arrived within Hold Time? Yes QNol N/A 2. Short Hold Time Analyshe72hc)? nYw ,NO N/A 3. Rush Tum Around Time Requested? (]Yes i CI&O QN/A 4. Sufficient Volume? yes ONo QN/A S. Correct Containers Used? `Qy I]No' I]N/A 6. -Pace CoAtainers Used? QYes No ONJA Containers Intact? QYes ❑No N/A 7. Dissolved analysis: Samples Field Filtered? QYes - []NO ;Qfl/A g. Sample Labels Match COC? .Oym ❑Ho []N/A 8. -Includes0ate/Time/ID/Ana sis Matrix: Headspace in VOA Vials (55-6mm)? V� QNo ❑N/A 10. Trip Blank Present? QYes ❑No LQN/A 11. TrIpBIank Custody Seals Present? [3yU No . ' N/A COMMENTS/SAMPLE DISCREPANCY Field Data Required? []Yes ❑No 6 ') it CA l-1 1 Ib r <r{- ^A -, -, rs i�i P I f.Vl t l'1u� � �� Lot ID of split containers CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/tlme: Project Manager SCURF Review: Date: Project Manager SRF Review:Date: i i I Page 11 of �13 t II ceMalytiral Document Name: Sample Condition Upon Recelpt(SCUR) Document Revised: February 7, 2018 Pa e 1 of 2 Document No.: F-CAR-CS-033-Rev.06 Issuing Aumamy: Pace Carolinas Dualit fNfrte 'Check mark top half of box If pH and/or dechlorination is verified and within the,acceptahce range for preservation samples. E.ceptions: VOA, Collform, TOC, oil and Grease, DRO/8015 (water) DOC, UHg "Bottom half of box is to list number of bottle Project# W10# : 92434143 PM: MWB Due Date: 07/08/19 CLIENT: 92—GKN 86 y M V A V ` V u 2 2 N yyt V n V V V V Q \ Z V L il p O Q I o n yn p V Q O Z ca m N q S n > > > n Z V .a O ¢ -' rL q 2 j a 7 S H 7 S b S v E n A N n u V u U V iy, E E o 2 a a Q S a c y T A E Q W E a a s u a a E a F°F d a EnE „�i '^ sr, a E E E .o E E E E. E yy w i m E E E E i 'i .E o a n o n _ "").. '"I.. ti — n n aE n 4 4 4 �• = 'yy„ i,1 )J' 4 V N V m N i J nm 'a N J nao 1A asas 2 nm r=i. V ¢ ti a real a > P o Q > U' > N H N & 'm a U i o =' o - m . as 3 a c 1 ,� f 2 IN i I I 3 4 fi 7 9 9 10 11 12 pH Adjustment Log for Preserved Samples sample to Type of Preservative pH upon receipt Date pmservadenadj.md Time pseservalloe adjusted Amount of Preservative added Leta �....c,n..., ,m... u e Note: wheneverthere Is a discrepancy affprting North Carolina compliance samples, a copy of this farm will he lento the North Carolina DEI Out of hold, Incorrect preservative, out of temp, Incorrect containers. Page 12 of CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed acc ,ralely,. Section A Section a Section C Required Client Information- Required Project Information: Invoice Information- P.19 e : 1 Of 1 Company: GM Dni line- Alamace, I Report To: RirAy Hell Attention: AEdrass: 1067 TrdlmynsoHaelds Rd Copy To: Company Name: MWam,. NC 27302 Andless Regulaton, Agency Email: PurpNasa Order A: Pace Quote' I Phwe. 19191215-i W Faz liplaimpt Name: MontNy Slommvaler P. Project Manager. malVrew.prenartl pacelahamm, _" - I.'Statol Location - Requested Due Date IP,ojed Y: Pace Profile p: 4804-9 1 NC -. Ro Anal iFltemtl M.. -1'. Z _ .R. woe g ct COLLECTED Preservatives U- di�kma WY.e+ GW W c s V O— w Wa�WeWaln u G .� SAMPLE ID a a u START ENO u H' One Character Per hee. W,Pe wP ' :b - a (A-7 0-91,-0 "O m Sample ltls must be unique � Is o x r w Tt2TT,., G// w w ;it O m �1 PATE TIMOunrowlfE S Z Z 2 of(� 2 '� O - c r i 0 I e jLl �-/'j Y % X X %% X X X l Cu, Pp, Zn 2 Oufol 002 vrt ' S •'Y /,.. t 1 0 , J /r X x x x x x x x x �> co. Po. Zn 3.. .4 1 ,6 7 8_. _. 9 . 11 � w "i`/ -i:AOOm_MNLCOMMENI9 , �. S •T,L- PEl1WU151®BT /AiFIWTgNR,�.S. JOAiE i pCCpTEp BYI_AFF6JATION _ TIME , SAMPLE CONDITONS _Y��/ �TME"_ -i _I G-4 Ag �� ^O/ATTE w/(//2 `lZ3 :'ems/% f ��.`—��� E6 r�,f�Iu✓ C.G,/-�y 1 C� �1 SAMPLER NAME AND SIGNATURE . • -� � • • . :; •_ � :` : -. -- -- _ �.^. _ PRINT Name w u i n a a z E u 2 SIGNATURE of SAMPLER / DATE DATE Si9nctl: 1 y; / <. (J O_ /