HomeMy WebLinkAboutNCG030427_MONITORING INFO_20190702STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/V U& 03 C)Llci,
DOC TYPE,
❑ HISTORICAL FILE
[(MONITORING REPORTS
DOC DATE
❑ b a
YYYYM M DD
Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted 6/03/2019
CERTIFICATE OF COVERAGE NO. NCG03 0 4 2 7 SAMPLE COLLECTION YEAR 2019
FACILITY NAME GKN Driveline Alamance SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
COUNTY Alamance n M p /+I� C��1 or ❑� Monthly' month
PERSON COLLECTING SAMPLES Mark Kline RECEIUC 6DISCHARGING TO CLASS ❑ORW ` HQW ❑Trout ❑PNA
LABORATORY Pace Analytical Lab Cert. # 12;40 JUL 0 2 2019 []zero -flow ❑■ Water Supply ❑SA
Comments on sample collection or analysis: ❑Other
CENT'kAL FILES
DWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
Part A: Stormwater Benchmarks and Monitoring Results
❑ No dischorpe this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
pH,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxsc
Organics
Benchmarks
-
-
100 mg/L or 50 mg/L4
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
01
5/13/2019
0.25"
6.8 mg/L
7.0
<0.005 mg/L
.006 mg/L
0.0974 mg/L
<0.005 mg/L
N/A
( 02
5/13/2019
1 0.25"
56.2 mg/L
6.9
0.0072 mg/L
<0.005 mg/L
0.0336 mg/L
6.6 mg/L
N/A
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page-1of3
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the ail the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Ricky Hiatt
Name (Print name)
EHS Coordinator
Title (Printtitle)
Signatupyo, Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑■ No discharge this period?z
Outfall No.
Date Sample. Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches3
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/L4
Parameter Code
-
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an oriainol copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
Permit Date: 11/1/2018-05/31/2021
Date
SWU-245, last revised 11/1/2018
_Page 3of3__ _
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aceAnalytical®
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u
CERTIFICATIONS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
,) Project: MONTHLY STORMWATER
Pace Project No.: 92429430
1i
Charlotte Certification IDs
i� 9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
�i Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
ii North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
1 Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
I I
1
III
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This repel shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.L.C.
Page 2 of 13
11
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aceAnalytical
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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(704)875-8062
1,
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SAMPLE ANALYTE COUNT
t Project: MONTHLY STORMWATER
Pace Project No.: 92429430
Analytes
Lab ID Sample ID
Method
Analysts
Reported Laboratory
92429430001 OUTFALL 001
EPA 1664E
JMS
1 PASI-C
EPA 608.3
SEM
29 PASI-C
EPA 200.7 Rev 4.41994
SH1
3 PASI-A
i
EPA 625.1
RES
58 PASI-C
EPA 624.1
DLK
34 PASI-C
SM 2540D-2011
MJP
1 PASI-A
EPA 9040C
ECH
1 PASI-A
EPA 420.4 Rev 1.0 1993
KDF7
1 PASI-A
92429430002 OUTFALL 002
EPA 1664E
JMS
1 PASI-C
,I
EPA 608.3
SEM
29 PASI-C
,I
EPA 200.7 Rev 4.41994
SH7
3 PASI-A
I
EPA 625.1
RES
58 PASI-C
EPA 624.1
DLK
34 PASI-C
SM 254OD-2011
MJP
1 PASI-A
EPA 9040C
ECH
1 PASI-A
'
EPA 420.4 Rev 1.0 1993
KDF1
1 PASI-A
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 13
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Project: MONTHLY STORMWATER
Pace Project No.: 92429430
�Sample: OUTFALL 001
ll Parameters
Oil and Grease
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Chlordane (Technical)
alpha -Chlordane
gamma -Chlordane
4,4'-DDD
„4,4'-DDE
4,4'-DDT
Dieldrin
�IEndosulfan I
� Endosulfan II
Endosulfan sulfate
i Endrin
�',Endrin aldehyde
Heptachlor
' Heptachlor epoxide
' PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
1 PCB-1260 (Aroclor 1260)
Toxaphene
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
Copper
Lead
Zinc
Acenaphthene
IAcenaphthylene
'Anthracene
lBenzo(a)anthracene
;Benzo(a)pyrene
Be nzo (b)fl uoranthe ne
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
4-Bromophenylphenyl ether
Butyl be nzyl p hth a late
4-Chlo ro-3-methyl phe nol
bis(2-C hlo roethoxy) m elh a ne
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
,I
II
I I
I.W. 0o'4cu2019 04:45 PM
ANALYTICAL RESULTS
Lab ID: 92429430001
Results Units
Collected: 05/13/19 09:10
Report Limit DF
NO
mg/L
5.0
1
NO
ug/L
0.050
1
ND
ug/L
0.050
1
NO
ug/L
0,050
1
ND
ug/L
0.050
1
NO
ug/L
0.050
1
ND
ug/L
0.50
1
NO
ug/L
0.050
1
ND
ug/L
0.050
1
NO
ug/L
0.050
1
ND
ug/L
0.050
1
ND
ug/L
0.050
1
ND
ug/L
0.050
1
ND
ug/L
0.050
1
ND
ug/L
0.050
1
ND
ug/L
0.050
1
NO
ug/L
0.050
1
ND
ug/L
0.050
1
NO
ug/L
0.050
1
NO
ug/L
0.050
1
NO
ug/L
0.50
1
NO
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
NO
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
188
%
10-130
1
118
%
10-130
1
NO
ug/L
5.0
1
6.0
ug/L
5.0
1
97.4
ug/L
10.0
1
ND
ug/L
5.0
1
ND
ug/L
5.0
1
ND
ug/L
5.0
1
ND
ug/L
5.0
1
ND
ug/L
5.0
1
ND
ug/L
5.0
1
NO
ug/L
5.0
1
NO
ug/L
5.0
1
NO
ug/L
5.0
1
NO
ug/L
5.0
1
NO
ug/L
5.0
1
ND
ug/L
10.0
1
NO
ug/L
5.0
1
ND
ug/L
5.0
1
ND
ug/L
5.0
1
NO
ug/L
5.0
1
S3
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L-C.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Page 4 of 13
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ANALYTICAL RESULTS
I
"i Project: MONTHLY STORMWATER
II Pace Project No.: 92429430
Samples OUTFALL 001
i
Parameters
Lab ID: 92429430001
Results Units
Collected: 05/13/19 0910
Report Limit OF Qualifiers
Chrysene
NO
ug/L
5.0
1
Dibenz(a,h)anthracene
NO
ug/L
5.0
1
3,3'-Dichlorobenzidine
NO
ug/L
25.0
1
2,4-Dichlorophenol
NO
ug/L
5.0
1
Diethylphthalale
NO
uglL
5.0
1
i2,4-Dimethylphenol
NO
ug/L
10.0
1
Dimethylphthalate
NO
ug/L
5.0
1
Di-n-butylphthalate
NO
ug/L
5.0
1
4,6-Dinitro-2-methylphenol
NO
ug/L
20.0
1
2,4-Dinitrophenol
ND
ug/L
50.0
1
2,4-Dinitrotoluene
NO
ug/L
5.0
1
. 2,6-Dinitrololuene
NO
ug/L
5.0
1
Di-n-octylphthalate
NO
ug/L
5.0
1
bis(2-Ethylhexyl)phthalate
NO
ug/L
5.0
1
Fluoranthene
NO
ug/L
5.0
1
Fluorene
NO
ug/L
5.0
1
I Hexachloro-1,3-butadiene
NO
ug/L
5.0
1
',Hexachlorobenzene
NO
ug/L
5.0
1
Hexachlorocyclopentadiene
NO
ug/L
10.0
1
Hexachloroethane
NO
ug/L
5.0
1
Indeno(1,2,3-cd)pyrene
NO
ug/L
5.0
1
,'Ilsophorone
NO
ug/L
10.0
1
,Naphthalene
NO
ug/L
5.0
1
Nitrobenzene
NO
ug/L
5.0
1
2-Nitrophenol
NO
ug/L
5.0
1
4-Nilrophenol
ND
ug/L
50.0
1
N-Nitrosodimethylamine
NO
ug/L
5.0
1
N-Nitroso-di-n-propylamine
NO
ug/L
5.0
1
N-Nitrosodiphenylamine
NO
ug/L
10.0
1
2,2'-Oxybis(1-chloropropane)
NO
ug/L
5.0
1
Pentachlorophenol
NO
ug/L
10.0
1
Phenanthrene
ND
uglL
5.0
1
Phenol
NO
ug/L
5.0
1
'Pyrene
NO
ug/L
5.0
1
'1,2,4-Trichlorobenzene
NO
ug/L
5.0
1
'2,4,6-Trichlorophenol
NO
ug/L
10.0
1
INitrobenzene-d5(S)
67
%
10-120
1
'.2-Fluorobiphenyl (S)
71
%
15-120
1
'Terphenyl-d 14 (S)
80
%
11-131
1
j Phenol-d6 (S)
41
%
10-120
1
'2-Fluorophenol(S)
56
%
10-120
1
l2,4,6-Tribromophenol(S)
100
%
10-137
1
.Benzene
ND
ug/L
1.0
1
Bromodichloromethane
NO
ug/L
2.0
1
!Bromoform
ND
ug/L
2.0
1
Bromomelhane
NO
ug/L
2.0
1
Carbon tetrachloride
NO
ug/L
2.0
1
Chlorobenzene
NO
ug/L
2.0
1
Chloroethane
ND
ug/L
2.0
1
REPORT OF LABORATORY ANALYSIS
t This report shall not be reproduced, except in full,
Dale: 05/29/2019 04:45 PM without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Page 5 of 13
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aceAnalyical®
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II
ANALYTICAL RESULTS
�IProject: MONTHLY STORMWATER
Pace Project No.: 92429430
II Sample: OUTFALL 001
Parameters
Lab ID: 92429430001 Collected: 05/13/19 09:10
Results Units Report Limit DF
"Chloroform
ND
ug/L
5.0
1
Chloromelhane
ND
ug/L
2.0
1
Dibromochloromethane
ND
ug/L
2.0
1
,1,2-Dichlorobenzene
ND
ug/L
2.0
1
1,3-Dichlorobenzene
NO
ug/L
2.0
1
1,4-Dichlorobenzene
NO
ug/L
2.0
1
1,1-Dichloroethane
ND
ug/L
2.0
1
','1,2-Dichloroethane
NO
ug/L
2.0
1
1,1-Dichloroethene
ND
ug/L
2.0
1
cis-1,2-Dichloroethene
ND
ug/L
2.0
1
trans-1,2-Dichloroethene
ND
ug/L
2.0
1
'''1,2-Dichloropropane
ND
ug/L
2.0
1
'cis-1,3-Dichloropropene
ND
ug/L
2.0
1
l trans-1,3-Dichloropropene
ND
ug/L
2.0
1
Ethylbenzene
ND
ug/L
1.0
1
Methylene Chloride
ND
ug/L
5.0
1
4,1,2,2-Telrachloroethane
NO
ug/L
2.0
1
Tetrachloroelhene
ND
ug/L
2.0
1
i Toluene
ND
ug/L
1.0
1
1,1,1-Trichloroethane
ND
ug/L
2.0
1
11,1,2-Trichloroethane
ND
ug/L
2.0
1
iTrichloroethene
NO
ug/L
2.0
1
lTrichlorofluoromethane
NO
ug/L
2.0
1
(Vinyl chloride
ND
ug/L
2.0
1
I4-Bromofluorobenzene (S)
98
%
70-130
1
(Toluene-d8 (S)
101
%
70-130
1
11,2-Dichloroethane-d4 (S)
100
%
70-130
1
?otal Suspended Solids
6.8
mg/L
2.5
1
�pH at 25 Degrees C
7.0
Std. Units
0.10
1
Ph'henol
ND
mg/L
0.020
1
m
H3
REPORT OF LABORATORY ANALYSIS
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
I This report shall not be reproduced, except in full,
Dale: 05/29/2019 04:45 PM without the written consent of Pace Analytical Services, L-C. Page 6 of 13
� laceAnalyficale
w»wpacelabs.cam
I
Project: MONTHLY STORMWATER
�I Pace Project No.: 92429430
',Sample: OUTFALL 002
Parameters
Oil and Grease
1 Aldrin
alpha-BHC
hbeta-BHC
delta-BHC
gamma-BHC (Lindane)
Chlordane (Technical)
alpha -Chlordane
gamma -Chlordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
I Endosulfan I
�Endosulfan II
Endosulfan sulfate
I Endrin
Endrin aldehyde
,Heptachlor
1 Heptachlor epoxide
IPCB-1016 (Aroclor 1016)
,PCB-1221 (Aroclor 1221)
IPCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
IPCB-1248 (Aroclor 1248)
IPCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
lToxaphene
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
Copper
Lead
Zinc
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Be nzo (b)fl uora nth a ne
Benzo(g,h,i)perylene
Benzo(k)fi uora nth a ne
4-Bromophenylphenyl ether
Butyl be nzy Ip hth a late
4-Chloro-3-methylp hen of
bi s(2-C h l o roeth oxy) m eth a ne
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
l�
'I
I
Date: 05/29/2019 04:45 PM
ANALYTICAL RESULTS
Lab ID: 92429430002
Results Units
Collected: 05/13/19 09:25
Report Limit OF
6.6
mg/L
5.0
1
NO
ug/L
0.050
1
NO
ug/L
0.050
1
NO
ug/L
0.050
1
NO
ug/L
0.050
1
NO
ug/L
0.050
1
NO
ug/L
0.50
1
NO
ug/L
0.050
1
ND
ug/L
0.050
1
ND
ug/L
0.050
1
ND
ug/L
0.050
1
NO
ug/L
0.050
1
NO
ug/L
0.050
1
NO
ug/L
0.050
1
NO
ug/L
0.050
1
NO
ug/L
0.050
1
NO
ug/L
0.050
1
ND
ug/L
0,050
1
ND
ug/L
0.050
1
ND
ug/L
0.050
1
ND
ug/L
0.50
1
NO
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
NO
ug/L
0.50
1
NO
ug/L
0.50
1
NO
ug/L
0.50
1
82
%
10-130
1
58
%
10-130
1
7.2
ug/L
5.0
1
NO
ug/L
5.0
1
33.6
ug/L
10.0
1
NO
ug/L
5.0
1
ND
ug/L
5.0
1
ND
ug/L
5.0
1
NO
ug/L
5.0
1
NO
ug/L
5.0
1
NO
ug/L
5.0
1
ND
ug/L
5.0
1
ND
ug/L
5.0
1
ND
ug/L
5.0
1
NO
ug/L
5.0
1
NO
ug/L
5.0
1
ND
ug/L
10.0
1
ND
ug/L
5.0
1
NO
ug/L
5.0
1
NO
ug/L
5.0
1
NO
ug/L
5.0
1
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, -LC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Page 7 of 13
1
aceAnalytical
wwnpacelabs.com
ANALYTICAL RESULTS
1
II Project: MONTHLY STORMWATER
Pace Project No.: 92429430
Sample: OUTFALL 002.
Parameters
Lab ID: 92429430002
Results Units
Collected: 05/13/19 09:25
Report Limit DF Qualifiers
Chrysene
NO
ug/L
5.0
1
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
13,3'-Dichlorobenzidine
NO
ug/L
25.0
1
�2,4-Dichlorophenol
NO
ug/L
5.0
1
Diethylphthalate
ND
ug/L
5.0
1
'2,4-Dimethylphenol
NO
ug/L
10.0
1
Dimelhylphthalate
NO
ug/L
5.0
1
'IDi-n-butylphthalate
NO
ug/L
5.0
1
'4,6-Dinitro-2-methylphenol
NO
ug/L
20.0
1
2,4-Dinitrophenol
NO
ug/L
50.0
1
2,4-Dinitrotoluene
NO
ug/L
5.0
1
2,6-Dinitrotoluene
NO
ug/L
5.0
1
Di-n-octylphthalale
NO
ug/L
5.0
1
�,bis(2-Ethylhexypphthalate
NO
ug/L
5.0
1
Fluoranthene
NO
ug/L
5.0
1
Fluorene
NO
ug/L
5.0
1
Hexachloro-1,3-butadiene
NO
ug/L
5.0
1
Hexachlorobenzene
ND
ug/L
5.0
1
Hexachlorocyclopentadiene
NO
ug/L
10.0
1
Hexachlomethane
NO
ug/L
5.0
1
lndeno(1,2,3-cd)pyrene
NO
ug/L
5.0
1
Isophorone
NO
ug/L
10.0
1
Naphthalene
NO
ug/L
5.0
1
Nitrobenzene
NO
ug/L
5.0
1
2-Nitrophenol
ND
ug/L
5.0
1
'4-Nitrophenol
NO
ug/L
50.0
1
N-Nitrosodimethylamine
NO
ug/L
5.0
1
;N-Nitroso-di-n-propylamine
NO
ug/L
5.0
1
'N-Nilrosodiphenylamine
NO
ug/L
10.0
1
)2,2'-Oxybis(1-chloropropane)
NO
ug/L
5.0
1
IPenlachlorophenol
ND
ug/L
10.0
1
IPhenanthrene
NO
ug/L
5.0
1
lPhenol
NO
ug/L
5.0
1
iPyrene
NO
ug/L
5.0
1
.1,2,4-Trichlorobenzene
NO
ug/L
5.0
1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
Nitrobenzene-d5 (S)
54
%
10-120
1
.2-Fluorobiphenyl(S)
51
%
15-120
1
7erphenyl-d14 (S)
52
%
11-131
1
Phenol-d6 (S)
31
%
10-120
1
2-Fluorophenol(S)
43
%
10-120
1
2,4,6-Tribromophenol(S)
65
%
10-137
1
Benzene
NO
ug/L
1.0
1
Bromodichloromelhane
NO
ug/L
2.0
1
Bromoform
NO
ug/L
2.0
1
Bromomethane
NO
ug/L
2.0
1
Carbon tetrachloride
NO
ug/L
2.0
1
Chlorobenzene
NO
ug/L
2.0
1
Chloroethane
t
NO
ug/L
2.0
1
REPORT OF
LABORATORY ANALYSIS
it
This report shall not be reproduced, except in full,
Date: 05/29/2019 04:45 PM
without
the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Page 8 of 13
II
II
II
aceAnalytical®
I
vmwpacelabs.wm
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i
I
Ii
Project: MONTHLY STORMWATER
II Pace Project No.: 92429430
Sample: OUTFALL 002
Parameters
Chloroform
II Chloromethane
Di b romochloro melha ne
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
I.1,1-Dichloroethane
l,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
'cis-1,3-Dichloropropene
!Itrans-1,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichlo roetha ne
1 1 2-Trich to roetha n e
�Trichloroethene
Trichlorofluoromethane
Vinyl chloride
�4-Bromofiuorobenzene (S)
Toluene -rift (S)
i11,2-Dichloroethane-d4 (S)
,Total Suspended Solids
pH at 25 Degrees C
Phenol
ANALYTICAL RESULTS
Lab ID: 92429430002
Results Units
Collected: 05/13/19 09:25
Report Limit DF
NO
ug/L
5.0
1
NO
ug/L
2.0
1
NO
ug/L
2.0
1
NO
ug/L
2.0
1
NO
ug/L
2.0
1
NO
ug/L
2.0
1
ND
ug/L
2.0
1
NO
ug/L
2.0
1
NO
ug/L
2.0
1
NO
ug/L
2.0
1
NO
ug/L
2.0
1
ND
ug/L
2.0
1
NO
ug/L
2.0
1
NO
ug/L
2.0
1
ND
ug/L
1.0
1
ND
ug/L
5.0
1
ND
ug/L
2.0
1
NO
ug/L
2.0
1
NO
ug/L
1.0
1
NO
ug/L
2.0
1
NO
ug/L
2.0
1
ND
ug/L
2.0
1
ND
ug/L
2.0
1
NO
ug/L
2.0
1
99
%
70-130
1
100
%
70-130
1
102
%
70-130
1
56.2
mg/L
5.0
1
6.9
Std. Units
0.10
1
NO
mg/L
0.020
1
H3
REPORT OF LABORATORY ANALYSIS
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
This report shall not be reproduced, except in full,
Date: 05/29/2019 04:45 PM without the written consent of Pace Analytical Services, L-C. Page 9 of 13
li
aceAnalytical
yr Pecelabs.War
QUALIFIERS
i
Project: MONTHLY STORMWATER
, Pace Project No.: 92429430
DEFINITIONS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit,
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S -Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
'I U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
,I Method 8260,
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
I
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
{I Rt RPD value was outside control limits.
9
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
q
n
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2019 04:45 PM without the written consent of Pace Analytical Services, LLC,
I '
Page 10 of 13
Document Name:
Document Revised: fel—ly 71101,
Sample Condition Upon Receipt(SCUR)
Pa o ] of 2
y :aceMal}?cala Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersvillex Raleigh❑ Mechanicsville❑
„ Client Name. -��
lw®#:924.29430
• C �V Project R �
❑Cier: iah ,❑FeC Ex UPS ❑❑UUSP r— `❑/Client II�II� I�� I I�III III I �II
92428430
Custody Seal Present? Dyes Seals Intact? []Yesa /
Date/Initials Person Examining Contents: 'V j`a �C `l
Packing Material: []Bubble Wrap ble Bags ❑None ❑ Other Biological Tissue Frozen?
TheirnometRr•: []Yes(]No-4�1({jA
N§f GUMD: 92TO48t/ Type of Ice: KWet ❑Blue ❑None
Cooler Temp('C): '(l y.- .cS Correction Factor: Add/Subtract('C) 0.0
v •. Tempshoule be out
of to peritng toVC
mpl
Cooler Temp Corrected ('C): "�` ❑Samples ou[at temp criteria. Samples an ice, cooling process
hashegun
USDA Regulated Soil �A, water sample)
Did samples erg ate in'a quarantine zone within the United Slates: CA, NY, or SC (check maps)? Did samples originate from a foreign source pmer 11 ally,
r1.._, t1 i..u,aue uv..an end P,mnn Rlrn17r�1Yrs n
Comments/Discre anc :
Chain of Custody Present?
es []NO
ON/A
1.
Samples Arrived within Hold Time?
es ❑No
❑N/A
2.
Short Hold Time Analysis(<71 hr.j?
Yes o
N/A
3.
Rush Turn Around Time Requested?
Dyes o
❑N/A
4.
Sufficient Volume?
rs QN.
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
a []No
Na
QN/A
❑N/A
Containers Intact?
eN []NO
❑N/A
7,
Dissolved analysis: Samples Field Filtered?
❑Yes []NO
/A
a.
Sample Labels Match COC?
-Includes Date/Time/ID/Ana sis Matrix:
II []NO
V
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
s ❑No
❑/AN
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes ❑Na
Yes Duo
N/A
/A
33.
COMMENTS/SAMPLE DISCREPANCY
r0C Ile( 'P r A C` �IIJIIG
Lot ID of Ipllt containers:
'I CLIENT NOTIFICATION/RESOLUTION
I
!� Person contacted:
Date/11me:
Field Data Required? ❑Yes ❑NO
Project Manager SCURF Review: LL Date:
Project Manager SRF Review: Dale:
Page 11 of 13
Document Name: Document Revised: February 7, 2018
Sample Condition Upon ReceiptiSCUR) age' of 2
CBAIk73410j� Document No.: Issuing Authority:
F-CAR-CS-033-Rev06 Pace Carolinas Quality Office
'Check mark tap half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
E.ceptions: VOA, Coliform,TOC, Oil and Grease, DRO/8015 (waterl DOC, LLHg
"Bottom half of box is to list number of bottle
Project# WO# : 92429430
PM: MWB Due Date: 05/29/19
CLIENT: 92-OKN
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pH Adjustment Log for Preserved Samples
sample to
Type of Preservative
pH upon receipt
Dale preservallon adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot 11
Note: Whenewthere is a discrepancy attecvng Nortn Lanllma camp <„ r:,=,,,p,=., e �wr � - •• --•^ •^• ••- •^
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 12 of 13
CHAIN -OF -CUSTODY I Analytical Request Document
The Chairtaf-Custody is a LEGAL DOCUMENT. All relevant fields mmt be wmpleted accurately.
Sectlon A SeNonSe C
R�I�d M� on: Page, I Of
Cwqm .. GM Orl"MSAdmanw Report To: Mark Kfine A0O^
Hewf.tft Rd
Mebma. NC
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PPoNT
-77 A 4-YLE�J�
Astance:
Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted y/r/2ars
CERTIFICATE OF COVERAGE No.NCG03 0 4 2 7 RECEIVED
FACILITY NAME GKN DHveline Alamance
COUNTY
Alamance
PERSON COLLECTING SAMPLES Ricky Hiatt
LABORATORY Pace Analytical Lab Cert. # 12:40 11,Mi,rl .iAL FILES
Comments on sample collection or analysis: OVVR OLG ION
Part A: Stormwater Benchmarks and Monitoring Results
Avu 06 2019
SAMPLE COLLECTION YEAR 2019
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or Q Monthly' T (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑■ Water Supply ❑SA
❑Other
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
n No discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
pH,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organicss
Benchmarks
-
-
100 mg/L or 50 mg/L4
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
01
6/20/2019
2.0
82.6mg/L
5.5
0.0059 mg/L
<0.005 mg/L
0.13 mg/L
<0.005 mg/L
N/A
02
6/20/2019
2.0
99.3 mg/L
5.4
0.0052 mg/L
<0.005 mg/L
0.0554 mg/L
<0.005 mg/L
N/A
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfali.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Ricky Hiatt
Name (Print name)
EHS Coordinator
Title (Print
title)
Signature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
n No dischor9e this period?z
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
inches3
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/L4
Parameter Code
-
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. see General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
-- - - 'Page2 of--
FOR PART AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERSTIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an oriainal copv of this DMR, including all '1Vo Dischorge"reports within 30 days of receipt of the lab results (or at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signatu/4 of Permittee Date
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 _
-Page3 of - - - -
li
aceAnalytical
i~pecelabs.=
July 05, 2019
Ricky Hiatt
GKN Driveline
{4 1067 Trollingwood Hawfield Rd.
a Mebane, NC 27302
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
RE: Project: Monthly Stormwater
Pace Project No.: 92434143
Dear Ricky Hiatt:
Enclosed are the analytical results for sample(s) received by the laboratory on June 21, 2019. This
report is a summary of the results based upon our understanding of your data quality objectives.
Please contact us if itemized quality control results are needed. These results relate only to the
samples included in this report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
matthew.brainard@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Dave Bruce, GKN Driveline
P
REPORT OF LABORATORY ANALYSIS
li This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13
aceAnalytical®
w aacelabs.00m
CERTIFICATIONS
Project: Monthly Stormwater
Pace Project No.: 92434143
Pace Ana lyticaI Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
, Charlotte Certification IDs
d 9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 13
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project:
i, Pace Project No.:
Monthly Stormwaler
92434143
-
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92434143001
OUTFALL 001
EPA 1664B
JMS
1
PASI-C
I.
EPA 608.3
SEM
29
PASI-C
II
EPA 200.7 Rev 4.41994
SH1
3
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
SAS
34
PASI-C
SM 2540D-2011
JP1
1
PASI-A
SM 4500-H+B-2011
SMK
1
PASI-A
EPA 420.4 Rev 1.01993
KDR
1
PASI-A
92434143002
OUTFALL 002
EPA 1664B
JMS
1
PASI-C
EPA 608.3
SEM
29
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
EPA 625.1
PKS
58
PASI-C
'I
EPA 624.1
SAS
34
PASI-C
SM 25400-2011
JP1
1
PASI-A
SM 4500-11+13-2011
SMK
1
PASI-A
i�
EPA 420.4 Rev 1.01993
KDF1
1
PASI-A
Ilil
REPORT OF LABORATORY ANALYSIS
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I without the widen consent of Pace Analytical Services, LLC. Page 3 of 13
IJ
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aceAnalytical
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i
I'
Project:
Pace Project No.:
Monthly Slormwater
92434143
ANALYTICAL RESULTS
Sample: OUTFALL 001
Parameters
Lab ID: 92434143001
Results Units
Collected: 06/20/19 15:22
Report Limit OF
Oil and Grease
NO
mg/L
5.0
1
, Aldrin
NO
ug/L
0.050
1
alpha-BHC
NO
ug/L
0.050
1
beta-BHC
NO
ug/L
0.050
1
delta-BHC
NO
ug/L
0.050
1
gamma-BHC (Lindane)
NO
ug/L
0.050
1
„Chlordane (Technical)
NO
ug/L
0.50
1
,alpha -Chlordane
NO
ug/L
0.050
1
',,gamma -Chlordane
NO
ug/L
0.050
1
4,4'-DDD
NO
ug/L
0.050
1
'4,4'-DDE
NO
ug/L
0.050
1
4,4'-DDT
NO
ug/L
0.050
1
'Dieldrin
NO
ug/L
0.050
1
Endosulfan I
NO
ug/L
0.050
1
�'Endosulfan II
ND
ug/L
0.050
1
'Endosulfan sulfate
NO
ug/L
0.050
1
Endrin
NO
ug/L
0.050
1
Endrin aldehyde
NO
ug/L
0.050
1
Heptachlor
NO
ug/L
0.050
1
Heptachlor epoxide
ND
ug/L
0.050
1
PCB-1016 (Aroclor 1(D16)
NO
ug/L
0.50
1
PCB-1221 (Aroclor 1221)
NO
ug/L
0.50
1
PC13-1232 (Aroclor 1232)
NO
ug/L
0.50
1
PCB-1242 (Aroclor 1242)
NO
ug/L
0.50
1
PCB-1248 (Aroclor 1248)
NO
ug/L
0.50
1
PCB-1254 (Aroclor 1254)
NO
ug/L
0.50
1
,PCB-1260 (Aroclor 1260)
NO
ug/L
0.50
1
'Toxaphene
NO
ug/L
0.50
1
Tetrachloro-m-xylene (S)
64
%
10-130
1
Decachlorobiphenyl (S)
42
%
10-130
1
Copper
5.9
ug/L
5.0
1
,Lead
ND
ug/L
5.0
1
'Zinc
130
ug/L
10.0
1
Acenaphthene
NO
ug/L
5.0
1
Acenaphthylene
NO
ug/L
5.0
1
'Anthracene
ND
ug/L
5.0
1
Benzo(a)anthracene
NO
ug/L
5.0
1
Benzo(a)pyrene
NO
ug/L
5.0
1
Benzo(b)fiuoranthene
NO
ug/L
5.0
1
Benzo(g,h,i)perylene
NO
ug/L
5.0
1
Benzo(k)fiuoranthene
NO
ug/L
5.0
1
4-Bromophenylphenyl ether
NO
ug/L
5.0
1
Bulylbenzylphthalate
NO
ug/L
5.0
1
4-Chloro-3-methylphenol
NO
ug/L
5.0
1
bis(2-Chlomethoxy)methane
NO
ug/L
10.0
1
bis(2-Chloroethyl) ether
NO
ug/L
5.0
1
2-Chloronaphthalene
NO
ug/L
5.0
1
2-Chlorophenol
NO
ug/L
5.0
1
4-Chlorophenylphenyl ether
NO
ug/L
5.0
1
REPORT OF LABORATORY ANALYSIS
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
This report shall not be reproduced, except in full,
Dale: 07/05/2019 04:31 PM without the written consent of Pace Analytical Services, -LC. Page 4 of 13
aceAnalytical
wwwpecelabs.com
I
Pace Analytical Services, LLC
9800 Kin cey Ave. Suite 100
HuntersOle, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Monthly Stormwater
�I Pace Project No.: 92434143
r Sample: OUTFALL 001
Parameters
Lab ID: 92434143001
Results Units
Collected: 06/20/1915:22
Report Limit OF
Chrysene
NO
ug/L
5.0
1
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
2,4-Dichlorophenol
NO
ug/L
5.0
1
Diethylphthalale
NO
ug/L
5.0
1
2,4-Dimethylphenol
NO
ug/L
10.0
1
Il Dimethylphthalate
NO
ug/L
5.0
1
Di-n-butylphthalate
ND
ug/L
5.0
1
4,6-Dinitro-2-methylphenol
NO
ug/L
20.0
1
i 2,4-Dinitrophenol
NO
ug/L
50.0
1
12,4-Dinitrotoluene
NO
ug/L
5.0
1
2,6-Dinitrotoluene
NO
ug/L
5.0
1
'Di-n-octylphthalate
NO
ug/L
5.0
1
bis(2-Ethylhexyl)phthalate
NO
ug/L
5.0
1
Fluoranthene
NO
ug/L
5.0
1
Fluorene
NO
ug/L
5.0
1
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
Hexachlorobenzene
ND
ug/L
5.0
1
Hexachlorocyclopentadiene
NO
ug/L
10.0
1
Hexachloroethane
NO
ug/L
5.0
1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
'Isophorone
NO
ug/L
10.0
1
'.Naphthalene
NO
ug/L
5.0
1
'Nitrobenzene
NO
ug/L
5.0
1
2-Nilrophenol
ND
ug/L
5.0
1
4-Nilrophenol
NO
ug/L
50.0
1
N-Nitrosodimethylamine
NO
ug/L
5.0
1
N-Nitroso-di-n-propylamine
NO
ug/L
5.0
1
N-Nitrosodiphenylamine
NO
ug/L
10.0
1
2,2'-Oxybis(1-chloropropane)
NO
ug/L
5.0
1
Pentachlorophenol
NO
ug/L
10.0
1
Phenanthrene
ND
ug/L
5.0
1
Phenol
NO
ug/L
5.0
1
Pyrene
NO
ug/L
5.0
1
1,2,4-Trichlorobenzene
NO
ug/L
5.0
1
2,4,6-Trichlorophenol
NO
ug/L
10.0
1
Nitrobenzene-d5 (S)
67
%
10-120
1
2-Fluorobiphenyl(S)
67
%
15-120
1
Terphenyl-d 14 (S)
81
%
11-131
1
Phenol-d6 (S)
38
%
10-120
1
2-Fluorophenol (S)
51
%
10-120
1
2,4,6-Tribromophenol(S)
86
%
10-137
1
Benzene
NO
ug/L
1.0
1
Bromodichloromethane
NO
ug/L
2.0
1
Bromoform
ND
ug/L
2.0
1
Bromomethane
NO
ug/L
2.0
1
Carbon tetrachloride
NO
ug/L
2.0
1
Chlorobenzene
NO
ug/L
2.0
1
Chloroethane
II
NO
ug/L
2.0
1
Qualifiers
REPORT OF LABORATORY ANALYSIS
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Dale: 07/05/2019 04:31 PM without the written consent of Pace Analytical Services, L-C. Page 5 of 13
Pace Analytical Services, LLC
aceAnapical® 9800 Kincey Ave. S 28078
100
Huntersville, NC 28078
wmvpacelabs.cam (704)875-9092
ANALYTICAL RESULTS
d
Project: Monthly Stormwater
Pace Project No.: 92434143
„ Sample: OUTFALL 001
Lab ID: 92434143001 Collected: 06/20/19 15:22
Parameters
Results
Units
Report Limit
DF Qualifiers
Chloroform
ND
ug/L
5.0
1
Chloromethane
ND
ug/L
2.0
1
Dibromochloromethane
ND
ug/L
2.0
1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
• 1,3-Dichlorobenzene
ND
ug/L
2.0
1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
1,1-Dichloroethane
ND
ug/L
2.0
1
• 1,2-Dichloroethane
ND
ug/L
2.0
1
•1,1-Dichloroethene
ND
ug/L
2.0
1
cis-1,2-Dichloroethene
ND
ug/L
2.0
1
!trans-1,2-Dichloroethene
ND
ug/L
2.0
1
1,2-Dichloropropane
ND
ug/L
2.0
1
ibis-1,3-Dichloropropene
ND
ug/L
2.0
1
trans- 1, 3-Dichloropropene
ND
ug/L
2.0
1
Ethylbenzene
ND
ug/L
1.0
1
• Methylene Chloride
ND
ug/L
5.0
1
1,1,2,2-Telrachloroethane
ND
ug/L
2.0
1
Tetrachloroethene
ND
ug/L
2.0
1
Toluene
ND
ug/L
1.0
1
1,1,1-Trichloroethane
ND
ug/L
2.0
1
'1,1,2-Trichloroethane
ND
ug/L
2.0
1
'Trichloreethene
ND
ug/L
2.0
1
'Trichlorofluoromelhane
ND
ug/L
2.0
1
'Vinyl chloride
ND
ug/L
2.0
1
4-Bromofluorobenzene (S)
98
%
70-130
1
Toluene -dB (S)
102
%
70-130
1
11,2-Dichloroethane-d4 (S)
115
%
70-130
1
Total Suspended Solids
82.6
mg/L
8.2
1
pH at 25 Degrees C
5.5
Std. Units
1.0
1 H3
Phenol
ND
mg/L
0.020
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 04:31 PM without the written consent of Pace Analytical Services, L-C. Page 6 of 13
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aceAnalytical
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h
ANALYTICAL RESULTS
Project: Monthly Stormwater
Pace Project No.: 92434143
Sample: OUTFALL 002
it Parameters
I
Lab ID: 92434143002
Results Units
Collected: 06/20/19 15:40
Report Limit DF
_
Oil and Grease
NO
mg/L
5.0
1
Aldrin
NO
ug/L
0.050
1
alpha-BHC
NO
ug/L
0.050
1
beta-BHC
NO
ug/L
0.050
1
��delta-BHC
NO
ug/L
0.050
1
I' gamma-BHC (Lindane)
NO
ug/L
0,050
1
,I Chlordane (Technical)
NO
ug/L
0.50
1
'alpha -Chlordane
NO
ug/L
0.050
1
gamma -Chlordane
NO
ug/L
0.050
1
4,4'-DDD
NO
ug/L
0.050
1
4,4'-DOE
NO
ug/L
0.050
1
I'4,4'-DDT
NO
ug/L
0.050
1
i,Dieldrin
NO
ug/L
0.050
1
Endosulfan I
NO
ug/L
0.050
1
Endosulfan II
NO
ug/L
0.050
1
Endosulfan sulfate
NO
ug/L
0.050
1
j Endrin
NO
ug/L
0.050
1
Endrin aldehyde
NO
ug/L
0.050
1
Heptachlor
NO
ug/L
0.050
1
Heptachlor epoxide
NO
ug/L
0.050
1
PCB-1016 (Aroclor 1016)
NO
ug/L
0.50
1
PCB-1 221 (Aroclor 1221)
NO
ug/L
0.50
1
PCB-1232 (Aroclor 1232)
NO
ug/L
0.50
1
PCB-1242 (Aroclor 1242)
NO
ug/L
0.50
1
PCB-1248 (Aroclor 1248)
NO
ug/L
0.50
1
PCB-1254 (Aroclor 1254)
NO
ug/L
0.50
1
IPCB-1260 (Aroclor 1260)
NO
ug/L
0.50
1
IToxaphene
NO
ug/L
0.50
1
Tetrachloro-m-xylene (S)
33
%
10-130
1
IDecachlorobiphenyl (S)
41
%
10-130
1
Copper
5.2
ug/L
5.0
1
Lead
NO
ug/L
5.0
1
Zinc
55.4
ug/L
10.0
1
'Acenaphthene
NO
ug/L
5.0
1
�Acenaphlhylene
NO
ug/L
5.0
1
Anlhracene
NO
ug/L
5.0
1
Benzo(a)anthracene
NO
ug/L
5.0
1
Benzo(a)pyrene
NO
ug/L
5.0
1
Benzo(b)fluoranlhene
NO
ug/L
5.0
1
Benzo(g,h,i)perylene
NO
ug/L
5.0
1
Benzo(k)fluoranthene
NO
ug/L
5.0
1
4-Bromophenylphenyl ether
NO
ug/L
5.0
1
Butylbenzylphthalate
NO
ug/L
5.0
1
4-Chloro-3-methylphenol
NO
ug/L
5.0
1
bis(2-Chloroethoxy)methane
NO
ug/L
10.0
1
bis(2-Chloroethyl) ether
NO
ug/L
5.0
1
2-Chloronaphthalene
NO
ug/L
5.0
1
2-Chlorophenol
NO
ug/L
5.0
1
4-Chlorophenylphenyl ether
NO
ug/L
5.0
1
Qualifiers
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
This report shall not be reproduced, except in full,
Dale: 07/05/2019 04:31 PM without the written consent of Pace Analytical Services, L-C. Page 7 of 13
aceAnalytical
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�I
ANALYTICAL RESULTS
Project: Monthly Stormwater
Pace Project No.: 92434143
Sample: OUTFALL 002
Lab ID: 92434143002
Collected: 06/20/19 15:40
Parameters
Results
Units
Report Limit
DF
Chrysene
ND
ug/L
5.0
1
Dibe nz(a,h) a nth race ne
ND
ug/L
5.0
1
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
2,4-Dichlorophenol
ND
ug/L
5.0
1
� Diethylphthalate
ND
ug/L
5.0
1
2,4-Dimethylphenol
ND
ug/L
10.0
1
Dimethylphthalate
ND
ug/L
5.0
1
Di-n-butylphthalate
�.
ND
ug/L
5.0
1
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
1
2,4-Dinilrophenol
ND
ug/L
50.0
1
2,4-Dinitrotoluene
ND
ug/L
5.0
1
2,6-Dinitrotoluene
ND
ug/L
5.0
1
Di-n-oclylphthalale
ND
ug/L
5.0
1
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
Fluoranthene
ND
ug/L
5.0
1
Fluorene
ND
ug/L
5.0
1
�Hexachloro-1,3-buladiene
ND
ug/L
5.0
1
Hexachlorobenzene
ND
ug/L
5.0
1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
Hexachloroethane
ND
ug/L
5.0
1
lndeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
Isophorone
ND
ug/L
10.0
1
Naphthalene
ND
ug/L
5.0
1
Nitrobenzene
ND
ug/L
5.0
1
12-Nitrophenol
ND
ug/L
5.0
1
4-Nitrophenol
ND
ug/L
50.0
1
N-Nitrosodimethylamine
ND
ug/L
5.0
1
N-Nitroso-di-n-propylamine
�N-Nitrosodiphenylamine
ND
ug/L
5.0
1
ND
ug/L
10.0
1
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
Pentachlorophenol
ND
ug/L
10.0
1
Phenanthrene
ND
ug/L
5.0
1
Phenol
ND
ug/L
5.0
1
Pyrene
ND
ug/L
5.0
1
.1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
Nitrobenzene-d5(S)
31
%
10-120
1
2-Fluorobiphenyl(S)
31
%
15-120
1
Terphenyl-d14(S)
66
%
11-131
1
Phenol-d6 (S)
20
%
10-120
1
2-Fluorophenol(S)
26
%
10-120
1
2,4,6-Tribromophenol(S)
65
%
10-137
1
Benzene
ND
uglL
1.0
1
Bromodichloromethane
ND
ug/L
2.0
1
Bromoform
ND
ug/L
2.0
1
Bromomethane
ND
ug/L
2.0
1
Carbon tetrachloride
ND
uglL
2.0
1
Chlorobenzene
ND
ug/L
2.0
1
Chloroethane
�I
ND
ug/L
2.0
1
Qualifiers
i. REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 04:31 PM without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Page 8 of 13
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ANALYTICAL RESULTS
Project: Monthly Stormwater
Pace Project No.: 92434143
t Sample: OUTFALL 002
Lab ID: 92434143002
Collected: 06120/19 15:40
Parameters
Results
Units
Report Limit
DF
Chloroform
ND
ug/L
5.0
1
Chloromelhane
ND
ug/L
2.0
1
Dibromochloromethane
ND
ug/L
2.0
1
�1,2-Dichlorobenzene
ND
ug/L
2.0
1
'.1,3-Dichlorobenzene
ND
ug/L
2.0
1
p 1,4-Dichlorobenzene
ND
ug/L
2.0
1
1,1-Dichloroethane
ND
ug/L
2.0
1
1,2-Dichloroethane
ND
ug/L
2.0
1
i1,1-Dichloroethene
ND
ug/L
2.0
1
cis-1,2-Dichloroethene
ND
ug/L
2.0
1
'4ans-1,2-Dichloroethene
ND
ug/L
2.0
1
:1,2-Dichloropropane
ND
ug/L
2.0
1
cis-1,3-Dichloropropene
ND
ug/L
2.0
1
trans-1,3-Dichloropropene
ND
ug/L
2.0
1
'Ethylbenzene
ND
ug/L
1.0
1
• Methylene Chloride
NO
ug/L
5.0
1
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
Tetrachloroethene -
ND
ug/L
2.0
1
Toluene
ND
ug/L
1.0
1
1,1,1-Trichloroethane
ND
ug/L
2.0
1
1,1,2-Trichloroethane
ND
ug/L
2.0
1
Trichloroethene
ND
ug/L
2.0
1
Trichlorohuoromethane
ND
ug/L
2.0
1
'Vinyl chloride
ND
ug/L
2.0
1
4-Bromofluorobenzene (S)
99
%
70-130
1
Toluene-d8 (S)
102
%
70-130
1
'1,2-Dichloroethane-d4 (S)
114
%
70-130
1
Total Suspended Solids
99.3
mg/L
17.5
1
pH at 25 Degrees C
5.4
Still. Units
1.0
1
Phenol
ND
mg/L
0.020
1
Date: 07/05/2019 04:31 PM
1•.91
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L-C.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Page 9 of 13
I I
ace Analytical
� vmwpecelabs.com
I
QUALIFIERS
•i Project: Monthly Stormwater
Pace Project No.: 92434143
DEFINITIONS
Pace Analytical Services, LLC
9800Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC -Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
I' RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyle in a specific matrix.
S- Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
CUP- Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
I. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
'ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 04:31 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 13
Document Name: Document Revised: February 7, 2018
Sample Condition upon Receipt(SCUR) Page 1 of 2
aceMaM«l• Document No.: issuing Authority:
FCAR-05033-Re 06 Pace Carolinas Duality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvillen/ Raleigh[] Mechanicsville❑
E Protect I
Client Name: Vito# : 92434143
Cqurier. ❑Fed Ex ❑UPS ❑USPS ❑CHent 92.434143 II I III IIII I III
❑Commercial •�❑Pace Other:_
/ � I
Custody Seal Present? ❑Yes '❑No Seals Intact? ❑Yes QNo t—
Date/Initials Verson Examining Contents: /
Packing Material: ❑Bubble Wrap❑Bubble Bags ❑None ❑ Other Biological Tissue erotent
\' \ I ❑Yes ONO ❑N/A/
Thermometer/. 92T048 Type of Ice: swet ❑blue ❑None ti
`❑IP wn10: .� V
Cooler Terrip('CI: C It Correction Factor: Add/Subtract ('C) 0.0 Tempshould be above freezing to VC
Cooler Temp Corrected ('C): ❑Samples cut of temp onterla. Samples an ice, cooling process
hasbegun
USDA Regulated Soil (❑,N/A, water sample)
Did samples originate In a quarantine tone within the United States: CA, NY, or SC (check mapsl? Did samples originate from a foreign source (Imemationally,
...,ao.,,mn Al 17r1Yac rlNn
. Yes NO
- - - - - —
Comments/Discrepancy:
Ruin of Custody Present?
3YU
❑NO
QN/A
1.
Samples Arrived within Hold Time?
Yes
QNol
N/A
2.
Short Hold Time Analyshe72hc)?
nYw
,NO
N/A
3.
Rush Tum Around Time Requested?
(]Yes
i
CI&O
QN/A
4.
Sufficient Volume?
yes
ONo
QN/A
S.
Correct Containers Used?
`Qy
I]No'
I]N/A
6.
-Pace CoAtainers Used?
QYes
No
ONJA
Containers Intact?
QYes
❑No
N/A
7.
Dissolved analysis: Samples Field Filtered?
QYes -
[]NO
;Qfl/A
g.
Sample Labels Match COC?
.Oym
❑Ho
[]N/A
8.
-Includes0ate/Time/ID/Ana sis Matrix:
Headspace in VOA Vials (55-6mm)?
V�
QNo
❑N/A
10.
Trip Blank Present?
QYes
❑No
LQN/A
11.
TrIpBIank Custody Seals Present?
[3yU
No
. ' N/A
COMMENTS/SAMPLE DISCREPANCY Field Data Required? []Yes ❑No
6 ') it CA l-1 1 Ib r <r{- ^A -, -, rs
i�i P I f.Vl t l'1u� � ��
Lot ID of split containers
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Date/tlme:
Project Manager SCURF Review: Date:
Project Manager SRF Review:Date:
i
i
I
Page 11 of �13
t
II
ceMalytiral
Document Name:
Sample Condition Upon Recelpt(SCUR)
Document Revised: February 7, 2018
Pa e 1 of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Aumamy:
Pace Carolinas Dualit fNfrte
'Check mark top half of box If pH and/or dechlorination is
verified and within the,acceptahce range for preservation
samples.
E.ceptions: VOA, Collform, TOC, oil and Grease, DRO/8015 (water) DOC, UHg
"Bottom half of box is to list number of bottle
Project# W10# : 92434143
PM: MWB Due Date: 07/08/19
CLIENT: 92—GKN
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pH Adjustment Log for Preserved Samples
sample to
Type of Preservative
pH upon receipt
Date pmservadenadj.md
Time pseservalloe
adjusted
Amount of Preservative
added
Leta
�....c,n...,
,m... u e
Note: wheneverthere Is a discrepancy affprting North Carolina compliance samples, a copy of this farm will he lento the North Carolina DEI
Out of hold, Incorrect preservative, out of temp, Incorrect containers.
Page 12 of
CHAIN -OF -CUSTODY I Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed acc ,ralely,.
Section A Section a Section C
Required Client Information- Required Project Information: Invoice Information-
P.19
e : 1 Of 1
Company: GM Dni line- Alamace,
I Report To: RirAy Hell
Attention:
AEdrass: 1067 TrdlmynsoHaelds Rd
Copy To:
Company Name:
MWam,. NC 27302
Andless
Regulaton, Agency
Email:
PurpNasa Order A:
Pace Quote'
I
Phwe. 19191215-i W Faz
liplaimpt Name: MontNy Slommvaler
P. Project Manager. malVrew.prenartl pacelahamm,
_" - I.'Statol
Location -
Requested Due Date
IP,ojed Y:
Pace Profile p: 4804-9
1
NC
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%
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%%
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SAMPLER NAME AND SIGNATURE
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PRINT Name
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SIGNATURE of SAMPLER
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DATE
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