NCG030390_MONITORING INFO_20190627

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
�V O
DOC TYPE
❑ HISTORICAL FILE
[�,MONITORING REPORTS
DOC DATE
DOI � u
❑
YYYYM M D D

=— Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Reso/ur es eneral Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. No;wJl L L
FACILITY NAME E'
COUNTY ,-IA
PERSON COLLEC NG
LABORATORY roCe
Comments on sample
Lab Cert. #
or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION AR gel
SAMPLE PERIOD Jan -June ❑ July -Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply []SA
❑Other
KECF1\/Fp
JUN 2 7 2019
CENT FWL FILES
0WR SECT
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics
Benchmarks ===>
-
-
100 mg/L or 50 mg/L4
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
,3m G
Vd,
7, u
/3/
�-
140— E
-�
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
"See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date:ll/1/2012-10/31/2017 SWU-245, last revised 10/2S/2012
Page 1 of 3

N_te;: !;you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER B: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Resources
Attn: DWR Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee) (Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

B L O
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, N.C. 27699-1617
Sir or Madam:
W E R S
P.O. Box 187
172 South Andrews Ave.
Hot Springs, NC 28743
828-622-7500
Enclosed is analysis for a recent storm water event. We have two outfalls, one flows to the
French Broad River and the other to Spring Creek. The event took place on 6/5/19, samples were
collected after 45 minutes of rain that produced .3 inches of rain in that period of time. Both
outfalls are from roof and parking lot drains and there are no manufacturing or storage activity
outside of the building.
I have taken over collecting and reporting on the storm water here at Peerless Blowers. This
being my first time was unaware of maintaining water temperature when sending our samples. I
did not send the samples on ice and had Pace Analytical proceed with footnotes.
bo�� Ael->
Don Wallin
Materials/Maintenance Director

�acehialytical
/ waw.pecelabs.com
June 19, 2019
Mr. Donald Wallin
MIMIC, Peerless Blowers
172 South Andrews Avenue
Hot Springs, NC 28743
RE: Project: Outfall #2
Pace Project No.: 92432236
Dear Mr. Wallin:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on June 07, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
SQ Pce--,
TNI
(�eO�tAS�Pi�
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page I of 23

aceAnalytical o
rnvwpacelabs.mm
Pace Analytical Services, LLC
2225 Riverside Dn
Asheville, NC 28804
[phone]
lot 21:anyEvil0 kqW
Project: Outfall #2
Pace Project No.: 92432236
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VvginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 23

accAtlytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Outfall #2
92432236
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92432236001
Outfall #2
EPA 1664E
JMS
1
PASI-C
EPA 200.7 Rev 4.4 1994
DS
3
PASI-A
EPA625.1
BPJ
58
PASI-C
EPA624.1
DLK
34
PASI-C
SM 2540D-2011
MJP
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 23

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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville, NC 288a4
[phone]
Project: Outfall #2
Pace Project No.: 92432236
Sample: Outfall #2
Lab ID: 92432236001 Collected:
06/05/19
13:30
Received: 06/07/19 10:20 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND
mg/L
4.8
1
06/13/19 06:22
200.7 MET ICP
Analytical Method:
EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Copper
7.7
ug/L
5.0
1
06/13/19 16:11
06117/1905:43
7440-50-8
Lead
5.8
ug/L
5.0
1
06/13/19 16:11
06/17/19 05:43
7439-92-1
Zinc
204
ug/L
10.0
1
06/13/19 16:11
06/17/19 05:43
7440-66-6
625 MSSV
Analytical Method:
EPA 625.1
Preparation Method:
EPA 625.1
Acenaphthene
ND
ug/L
24.5
5
06110/1917:28
0611211918:56
83-32-9
Acenaphthylene
ND
ug/L
24.5
5
0611011917:28
06/12/19 18:56
208-96-8
Anthracene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
120-12-7
Benzo(a)anthracene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
56-55-3
Benzo(a)pyrene
ND
ug/L
24.5
5
06/10/19 17:28
06112/1918:56
50-32-8
Senzo(b)Ouoranlhene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
191-24-2
Benzo(k)Fluoranthene
ND
ug/L
24.5
5
06110/1917:28
06/12/19 18:56
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
101-55-3
Butylbenzylphthalate
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
85-68-7
4-Chloro-3-m ethylphenol
ND
ug/L
245
5
06/10/19 17:28
06/12/19 18:56
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
49.0
5
06/10/19 17:28
06/1211918:56
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
111-44-4
2-Chloronaphthalene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
91-58-7
2-Chlorophenol
ND
ug/L
24.5
5
06/1011917:28
06/1211918:56
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
7005-72-3
Chrysene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
123
5
06/10/19 17:28
06/12/1918:56
91-94-1
2,4-Dichlorophenol
ND
ug/L
24.5
5
06/10/19 17:28
06112/1918:56
120-83-2
Diethylphthalate
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
84-66-2
2,4-Dimethylphenol
ND
ug/L
49.0
5
06/10/19 17:28
0611211918:56
105-67-9
Dimethylphthalate
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
131-11-3
Di-n-butylphthalate
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
98.0
5
06/10/19 17:28
06/12/19 18:56
534-52-1
M1
2,4-Dinitrophenol
ND
ug/L
245
5
06/10/19 17:28
06/12/19 18:56
51-28-5
M1
2,4-Dinitrotoluene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
121-14-2
2,6-Dinitrotoluene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
606-20-2
Di-n-octylphthalate
ND
ug/L
24.5
5
06/10/19 17:28
06/1211918:56
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
117-81-7
Fluoranthene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
206-44-0
Fluorene
ND
ug/L
24.5
5
06110/1917:28
06/12/19 18:56
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
87-68-3
Hexachlorobenzene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
49.0
5
06/10/19 17:28
06/12/19 18:56
77-47-4
M1
Hexachloroethane
ND
ug/L
24.5
5
06/1011917:28
06112/1918:56
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
193-39-5
sophorone
ND
ug/L
49.0
5
06/1011917:28
06/12/1918:56
78-59-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 12:25 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 23

/ �aceAnalytical®
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville. NC 28804
[phone]
Project: Outfall #2
Pace Project No.: 92432236
Sample: Outfall #2
Lab ID: 92432236001 Collected: 06/05/19 13:30
Received: 06/07/19 10:20 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
625 MSSV
Analytical Method: EPA 625.1
Preparation Method: EPA 625.1
Naphthalene
NO
ug/L
24.5
5
06/10/19 17:28
06/1211918:56
91-20-3
Nitrobenzene
NO
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
98-95-3
2-Nitrophenol
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
88-75-5
4-Nitrophenol
ND
ug/L
245
5
06/10/19 17:28
06/12/19 18:56
100-02-7
N-Nitrosodimelhylamine
NO
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
24.5
5
06/1011917:28
06/1211918:56
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
49.0
5
06/10/19 17:28
06/12/19 18:56
86-30-6
2,2'-Oxybis(1-chloropropane)
NO
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
108-60-1
Pentachlorophenol
NO
ug/L
49.0
5
06/10/19 17:28
06/12/19 18:56
87-86-5
Phenanthrene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
85-01-8
Phenol
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
108-95-2
Pyrene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
24.5
5
06/10/19 17:28
06/12/19 18:56
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
49.0
5
06110/1917:28
06/12/19 18:56
88-06-2
Surrogates
Nitrobenzene-d5 (S)
58
%
10-120
5
06/10/19 17:28
06/12/19 18:56
4165-60-0 D3
2-Fluorobiphenyl(S)
64
%
15-120
5
06/10/19 17:28
06/12/19 18:56
321-60-8
Terphenyl-d14 (S)
82
%
11-131
5
06/10/19 17:28
06/12/19 18:56
1718-51-0
Phenol-d6 (S)
28
%
10-120
5
06/10/19 17:28
06/12/19 18:56
13127-88-3
2-Fluorophenol (S)
41
%
10-120
5
06/10/19 17:28
06/12/19 18:56
367-12-4
2,4,6-Tribromophenol(S)
62
%
10-137
5
06/10/19 17:28
06/12/19 18:56
118-79-6
624 Volatile Organics
Analytical Method:
EPA 624.1
'
Benzene
ND
ug/L
1.0
1
06/10/19 15:19
71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
06/10/19 15:19
75-27-4
Bromoform
ND
ug/L
2.0
1
06/10/19 15:19
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/10/19 15:19
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
06/10/19 15:19
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
06/10/19 15:19
108-90-7
Chloroethane
ND
ug/L
2.0
1
06110/1915:19
75-00-3
Chloroform
ND
ug/L
5.0
1
06110/1915:19
67-66-3
Chloromethane
ND
ug/L
2.0
1
06/10/19 15:19
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
06110/1915:19
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
06/10/19 15:19
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
06/10/19 15:19
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
06/10/19 15:19
106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1
06/1011915:19
75-34-3
1,2-Dichloroethane
NO
ug/L
2.0
1
06/10/19 15:19
107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1
06/10/19 15:19
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
1
06/10/19 15:19
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.0
1
06/10/19 15:19
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
1
06/10/19 15:19
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2.0
1
06/10/19 15:19
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
2.0
1
06/10/19 15:19
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/10/19 15:19
100-41-4
Methylene Chloride
ND
ug/L
5.0
1
06/10/19 15:19
75-09-2
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
06/10/19 15:19
79-34-5
REPORT OF LABORATORY ANALYSIS
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Date: 06/19/2019 12:25 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 23

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2225 R(verside Dr.
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[phone]
ANALYTICAL RESULTS
Project: Outfall #2
Pace Project No.: 92432236
Sample: Outfall #2
Lab ID: 92432236001 Collected: 06/05/19 13:30 Received:
06/07/19 10:20 Matrix: Water
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
624 Volatile Organics
Analytical Method: EPA 624.1
Telrachloroethene
ND ug/L 2.0 1
06/10/19 15:19
127-18-4
Toluene
ND ug/L 1.0 1
06/10/19 15:19
108-88-3
1,1,1-Trichloroelhane
ND 1 2.0 1
06/10/19 15:19
71-55-6
1,1,2-Trichloroethane
ND ug/L 2.0 1
06/1011915:19
79-00-5
Trichloroelhene
NO ug/L 2.0 1
06/1011915:19
79-01-6
Trichlorofluoromethane
ND ug/L 2.0 1
06110/1915:19
75-69-4
Vinyl chloride
ND ug/L 2.0 1
06/10/19 15:19
75-01-4
Surrogates
4-Bromofluorobenzene (S)
99 % 70-130 1
06/10/19 15:19
460-00-4
Toluene-d8 (S)
98 % 70-130 1
06/10/19 15:19
2037-26-5
1,2-Dichloroethane-d4 (S)
99 % 70-130 1
06/10/19 15:19
17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
83.3 mg/L 16.7 1
06/12/19 05:01
REPORT OF LABORATORY ANALYSIS
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Dale: 06/19/2019 12:25 PM
without the written consent of Pace Analytical Services, L-C.
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Outfall #2
Pace Project No.: 92432236
QC Batch: 480856
Analysis Method:
EPA 16646
QC Batch Method: EPA 1664E
Analysis Description:
1664 SGT-HEM, TPH
Associated Lab Samples: 92432236001
METHOD BLANK: 2601099
Matrix: Water
Associated Lab Samples: 92432236001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Petroleum Hydrocarbons
mg/L
NO 4.8
06/13/19 06:17
LABORATORY CONTROL SAMPLE:
2601100
Spike LCS
LCS %Rec
Parameter
Units
Conc. Result
%Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
19.2 20.4
106 64-132
MATRIX SPIKE SAMPLE:
2601101
92432427001 Spike
MS MS %Rec
Parameter
Units
Result Conc.
Result %Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND 19.2
19.1 99 64-132
Results presented on this page are In the units indicated by the'Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/19/2019 12:25 PM without the written consent of Pace Analytical Services, L-C. Page 7 of 23

��ace,Analyficale`
w�w[pecelacs.com
QUALITY CONTROL DATA
Project: Outfall #2
Pace Project No.: 92432236
QC Batch. 480942 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92432236001
Pace Analytical Services, LLCM
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 2601435
Matrix: Water
Associated Lab Samples: 92432236001
'
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Copper
ug/L
ND
5.0
06/17/19 04:24
Lead
ug/L
ND
5.0
06/17/19 04:24
Zinc
ug/L
NO
10.0
06/17/19 04:24
LABORATORY CONTROL SAMPLE:
2601436
Spike
LCS
LCS %Rec
Parameter
Units
Conc.
Result
%Rec Limits Qualifiers
Copper
ug/L
500
456
91 85-115
Lead
ug/L
500
444
89 85-115
Zinc
ug/L
500
456
91 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2601437
2601438
MS
MSD
92431704001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units Result
Conc.
Conc.
Result
Result %Rec %Rec
Limits
RPD Qual
Copper
ug/L 8.7
500
500
494
484 97 95
70-130
2
Lead
ug/L <5.0
500
500
472
456 94 91
70-130
3
Zinc
ug/L 11.5
500
500
495
485 97 95
70-130
2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2601439
2601440
MS
MSD
92431833001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units Result
Conc.
Conc.
Result
Result %Rec %Rec
Limits
RPD Qual
Copper
ug/L 1710
500
500
2130
1750 85 9
70-130
20 M1
Lead
ug/L 125
500
500
501
498 75 75
70-130
1
Zinc
ug/L 2820
500
500
3180
2970 71 29
70-130
7 M1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/19/2019 12:25 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 23

171aceAnalj6cal
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Outfall #2
Pace Project No.: 92432236
QC Batch: 480087 Analysis Method: EPA 624.1
QC Batch Method: EPA 624.1 Analysis Description: 624 MSV
Associated Lab Samples: 92432236001
METHOD BLANK: 2597664
Associated Lab Samples: 92432236001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
NO
2.0
06/1011912:21
1,1,2,2-Tetrachloroethane
ug/L
NO
2.0
06/10/19 12:21
1,1,2-Trichloroethane
ug/L
NO
2.0
06/10/19 12:21
1,1-Dichloroethane
ug/L
NO
2.0
06/10/19 12:21
1,1-Dichloroethene
ug/L
NO
2.0
06/10/19 12:21
1,2-Dichlorobenzene
ug/L
NO
2.0
06/10/19 12:21
1,2-Dichloroethane
ug/L
ND
2.0
06/10/19 12:21
1,2-Dichloropropane
ug/L
ND
2.0
06/10/19 12:21
1,3-Dichlorobenzene
ug/L
ND
2.0
06/10/19 12:21
1,4-Dichlorobenzene
ug/L
ND
2.0
06/10/19 12:21
Benzene
ug/L
ND
1.0
06/10/19 12:21
Bromodichloromethane
ug/L
ND
2.0
06110/1912:21
Bromoform
ug/L
ND
2.0
06110/1912:21
Bromomethane
ug/L
ND
2.0
06/10/19 12:21
Carbon tetrachloride
ug/L
ND
2.0
06/10/19 12:21
Chlorobenzene
ug/L
ND
2.0
06/10/19 12:21
Chloroethane
ug/L
ND
2.0
06/10/19 12:21
Chloroform
ug/L
ND
5.0
06110/1912:21
Chloromethane
ug/L
ND
2.0
06110/1912:21
cis-1,2-Dichloroethene
ug/L
NO
2.0
06/10/1912,21
cis-1,3-Dichloropropene
ug/L
NO
2.0
06110/1912*21
Dibromochloromethane
ug/L
NO
2.0
06/10M912:21
Ethylbenzene
ug/L
NO
1.0
06/10/19 12:21
Methylene Chloride
ug/L
NO
5.0
06/10/19 12:21
Tetrachloroethene
ug/L
NO
2.0
06/10/19 12:21
Toluene
ug/L
ND
1.0
06/10/19 12:21
trans-1,2-Dichloroethene
ug/L
NO
2.0
06/10/19 12:21
trans-1,3-Dichloropropene
ug/L
ND
2.0
06/101191221
Trichloroethene
ug/L
ND
2.0
06/10/19 12:21
Trichlorofluoromethane
ug/L
ND
2.0
06/1011912:21
Vinyl chloride
ug/L
ND
2.0
06/10/19 12:21
1,2-Dichloroethane-d4 (S)
%
99
70-130
06/10/19 12:21
4-Bromofluorobenzene (S)
%
96
70-130
06/10/19 12:21
Toluene-d8 (S)
%
95
70-130
06/10/19 12:21
Qualifiers
LABORATORY CONTROL SAMPLE: 2597665
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 16.5 82 70-130
1,1,2,2-Tetrachloroethane ug/L 20 15.6 78 60-140
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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aceAnalytical
www.pacalsbs. com
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Outfall 92
Pace Project No.: 92432236
LABORATORY CONTROL SAMPLE:
Parameter
2597665
Units
Spike
Conc.
LCS
Result
LCS
%Rec
% Rec
Limits
1,1,2-Trichloroethane
ug/L
20
17.9
90
70-130
1,1-Dichloroethane
ug/L
20
17.0
85
70-130
1,1-Dichloroethene
ug/L
20
16.6
83
50-150
1,2-Dichlorobenzene
ug/L
20
18.0
90
65-135
1,2-Dichloroethane
ug/L
20
16.6
83
49-155
1,2-Dichloropropane
ug/L
20
17.4
87
35-165
1,3-Dichlorobenzene
ug/L
20
18.2
91
70-130
1,4-Dichlorobenzene
ug/L
20
17.9
89
65-135
Benzene
ug/L
20
16.7
84
65-135
Bromodichloromethane
ug/L
20
16.7
83
65-135
Bromoform
ug/L
20
17.1
86
70-130
Bromomethane
ug/L
20
17.2
86
15-185
Carbon tetrachloride
ug/L
20
17.1
86
70-130
Chlorobenzene
ug/L
20
17.1
86
65-135
Chloroethane
ug/L
20
17.9
90
40-160
Chloroform
ug/L
20
1T2
86
70-135
Chloromethane
ug/L
20
17.1
86
1-205
cis-1,2-Dichloroethene
ug/L
20
16.5
82
68-146
cis-1,3-Dichloropropen e
ug/L
20
17.0
85
25-175
Dibromochloromethane
ug/L
20
17.3
87
70-135
Ethyibenzene
ug/L
20
1T5
88
60-140
Methylene Chloride
ug/L
20
18.8
94
60-140
Tetrachloroethene
ug/L
20
18.2
91
70-130
Toluene
ug/L
20
16.9
85
70-130
trans-1,2-Dichloroethene
ug/L
20
16.3
82
70-130
trans-1,3-Dichloropropene
ug/L
20
17.6
88
50-150
Trichloroethene
ug/L
20
16.7
84
65-135
Trichlorofluoromethane
ug/L
20
17.9
89
50-150
Vinyl chloride
ug/L
20
18.6 -
93
5-195
1,2-Dichloroethane-d4 (S)
%
97
70-130
4-Bromofluorobenzene (S)
a/
92
70-130
Toluene-d8(S)
e/
99
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2597666
2597667
MS
MSD
92431072003
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
NO
20
20
15.0
18.2
75
91
52-162
19
1,1,2,2-Tetrachioroethane
ug/L
NO
20
20
13.8
16.2
69
81
46-157
16
1,1,2-Trichloroethane
ug/L
NO
20
20
15.2
16.8
76
84
52-150
10
1,1-Dichloroethane
ug/L
NO
20
20
14.2
16.7
71
83
59-155
16
1,1-Dichloroethene
ug/L
NO
20
20
15.5
17.6
78
88
1-234
13
1,2-Dichlorobenzene
ug/L
NO
20
20
15.2
18.2
76
91
18-190
18
1,2-Dichloroethane
ug/L
ND
20
20
13.4
16.3
67
82
49-155
19
1,2-Dichloropropane
ug/L
NO
20
20
15.4
16.9
77
85
1-210
9
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 12:25 PM without the written consent of Pace Analytical Services, -I-C. Page 10 of 23

aceAnalytical
Iwt»vpece/a6s com
i
QUALITY CONTROL DATA
Project: Outfall #2
Pace Project No.: 92432236
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2597666
MS
92431072003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2597667
MS
Result
MSD
Result
MS
e/ Rec
MSD
% Rec
%Rec
Limits
RPD Qual
1,3-Dichlorobenzene
ug/L
ND
20
20
16.0
18.8
80
94
59-156
17
1,4-Dichlorobenzene
ug/L
ND
20
20
16.2
18.8
81
94
18-190
15
Benzene
ug/L
ND
20
20
16.6
18.8
83
94
37-151
12
Bromodichloromethane
ug/L
ND
20
20
15.2
17.6
76
88
35-155
14
Bromoform
ug/L
ND
20
20
14.0
16.8
70
84
45-169
18
Bromomethane
ug/L
ND
20
20
10.7
12.0
53
60
1-242
Ti
Carbon tetrachloride
ug/L
ND
20
20
17.0
19.6
85
98
70-140
14
Chlorobenzene
ug/L
ND
20
20
15.4
18.4
77
92
37-160
18
Chloroethene
ug/L
ND
20
20
16.3
18.8
81
94
14-230
14
Chloroform
ug/L
ND
20
20
15.9
18.5
72
84
51-138
15
Chloromethane
ug/L
ND
20
20
16.3
18.3
81
91
1-273
11
cis-1,2-Dichloroethene
ug/L
ND
20
20
14.7
16.3
72
80
45-174
10
cis-1,3-Dichloropropene
ug/L
ND
20
20
14.6
16.7
73
83
1-227
13
Dibromochloromethane
ug/L
ND
20
20
15.1
17.3
75
87
53-149
14
Elhylbenzene
ug/L
ND
20
20
16.0
18.9
80
94
37-162
17
Methylene Chloride
ug/L
ND
20
20
13.6
15.9
68
79
1-221
15
Tetrachloroethene
ug/L
ND
20
20
17.5
20.5
85
100
64-148
16
Toluene
ug/L
ND
20
20
16.1
18.6
76
88
47-150
14
trans-1,2-Dichloroethene
ug/L
ND
20
20
14.9
17.2
74
86
54-156
14
trans-1,3-Dichloropropene
ug/L
ND
20
20
15.5
16.9
77
85
17-183
9
Trichloroethene
ug/L
ND
20
20
15.7
17.7
79
89
70-157
12
Trichlorofluoromethane
ug/L
ND
20
20
16.8
19.1
84
95
17-181
13
Vinyl chloride
ug/L
ND
20
20
16.8
19.5
84
98
1-251
15
1,2-Dichloroethane-d4 (S)
%
90
97
70-130
4-Bromofluorobenzene (S)
%
95
98
70-130
Toluene-d8(S)
e/
98
99
70-130
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is prose oted to the fight of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 12:25 PM without the written consent of Pace Analytical Services, -LC. Page 11 of 23

aceAnalytical
lmmvpacelaas.com
i
QUALITY CONTROL DATA
Project: Outfall #2
Pace Project No.: 92432236
QC Batch: 480044 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Associated Lab Samples: 92432236001
METHOD BLANK: 2597577
Associated Lab Samples: 92432236001
- Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
NO
5.0
06/12/19 10:41
2,2'-Oxybis(1-chloropropane)
ug/L
NO
5.0
06/12/19 10:41
2,4,6-Trichlorophenol
ug/L
NO
10.0
06/12/19 10:41
2,4-Dichlorophenol
ug/L
NO
5.0
06/12/19 10:41
2,4-Dimethylphenol
ug/L
NO
10.0
06/12/19 10:41
2,4-Dinitrophenol
ug/L
NO
50.0
06/12/19 10:41
2,4-Dinitrotoluene
ug/L
NO
5.0
06/12/1910*41
2,6-Dinitrotoluene
ug/L
NO
5.0
06/12/19 10:41
2-Chloronaphthalene
ug/L
NO
5.0
06/12/19 10:41
2-Chlorophenol
ug/L
NO
5.0
06/12/19 10:41
2-Nitrophenol
ug/L
NO
5.0
06/12/19 10:41
3,3'-Dichlorobenzidine
ug/L
ND
25.0
06/12/19 1041
4,6-Dinitro-2-methylphenol
ug/L
NO
20.0
06/12/1910*41
4-Bromophenylphenyl ether
ug/L
NO
5.0
06/12/19 10:41
4-Chloro-3-methylphenol
ug/L
NO
5.0
06/12/19 10:41
4-Chlorophenylphenyl ether
ug/L
NO
5.0
06/12/19 10:41
4-Nitrophenol
ug/L
NO
50.0
06/12/19 10:41
Acenaphthene
ug/L
ND
5.0
06/12/19 10:41
Acenaphthylene
ug/L
NO
5.0
06/12/191041
Anthracene
ug/L
ND
5.0
06/12/19 10:41
Benzo(a)anthracene
ug/L
NO
5.0
06/12/19 10:41
Benzo(a)pyrene
ug/L
ND
5.0
06/12/19 10:41
Benzo(b)fluoranthene
ug/L
NO
5.0
06/12/19 10:41
Benzo(g,h,i)perylene
ug/L
NO
5.0
06/12/1910,41
Benzo(k)fluoranthene
ug/L
NO
5.0
06/12/191041
bis(2-Chloroethoxy)methane
ug/L
NO
10.0
06/1211910:41
bis(2-Chloroethyl) ether
ug/L
NO
5.0
06/12/19 10:41
bis(2-Ethylhexyl)phthalate
ug/L
NO
5.0
06/12/19 10:41
Butylbenzylphthalate
ug/L
NO
5.0
06/12/19 10:41
Chrysene
ug/L
NO
5.0
06/12/19 10:41
Di-n-butylphthalate
ug/L
NO
5.0
06/12/19 10:41
Di-n-octylphthalate
ug/L
NO
5.0
06/12/19 1041
Dibenz(a,h)anthracene
ug/L
NO
5.0
06/12/19 1041
Diethylphthalate
ug/L
NO
5.0
06/12/19 1041
Dimethylphthalate
ug/L
NO
5.0
06/12/1910:41
Fluoranthene
ug/L
NO
5.0
06/12/19 10:41
Fluorene
ug/L
NO
5.0
06/12/19 10:41
Hexachloro-1,3-butadiene
ug/L
NO
5.0
06/12/19 10:41
Hexachlorobenzene
ug/L
ND
5.0
06/12/19 10:41
Hexachlorocyclopentadiene
ug/L
ND
10.0
06/12/19 10:41
Hexachloroethane
ug/L
NO
5.0
06/12/1910*41
Qualifiers
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville, INC 28804
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 12:25 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 23

aceAnalytical®
/ wxw.perela6s.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Outfall #2
Pace Project No.: 92432236
METHOD BLANK: 2597577
Associated Lab Samples: 92432236001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Indeno(1,2,3-cd)pyrene
ug/L
NO
5.0
06/12/19 10:41
Isophorone
ug/L
NO
10.0
06/12/19 10:41
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
06/1211910:41
N-Nitrosodimelhylamine
ug/L
ND
5.0
06112/1910:41
N-Nitrosodiphenylamine
ug/L
NO
10.0
06/12/19 10:41
Naphthalene
ug/L
NO
5.0
06112/1910:41
Nitrobenzene
ug/L
ND
5.0
06/12/19 10:41
Pentachlorophenol
ug/L
NO
10.0
06/12/19 10:41
Phenanthrene
ug/L
ND
5.0
06/12/19 10:41
Phenol
ug/L
ND
5.0
06/12/19 10:41
Pyrene
ug/L
ND
5.0
06/12/19 10:41
2,4,6-Tribromophenol(S)
%
91
10-137
06/12/19 10:41
2-Fluorobiphenyl (S)
%
77
15-120
06/12/19 10:41
2-Fluorophenol (S)
%
42
10-120
06/12/19 10:41
Nitrobenzene-d5 (S)
%
82
10-120
06/12/19 10:41
Phenol-d6 (S)
%
29
10-120
06/12/19 10:41
Terphenyl-d14 (S)
%
94
11-131
06/12/19 10:41
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2597578
Units
Spike
Conc.
LCS
Result
1-CS
%Rec
%Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
39.5
79
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
42.1
84
36-166
2,4,6-Trichlorophenol
ug/L
50
46.8
94
37-144
2,4-Dichlorophenol
ug/L
50
44.3
89
39-135
2,4-Dimethylphenol
ug/L
50
43.2
86
32-120
2,4-Dinitrophenol
ug/L
250
220
88
1-191
2,4-Dinitrotoluene
ug/L
50
44.2
88
39-139
2,6-Dinitrotoluene
ug/L
50
43.7
87
50-158
2-Chloronaphthalene
ug/L
50
38.6
77
60-120
2-Chlorophenol
ug/L
50
41.5
83
23-134
2-Nitrophenol
ug/L
50
42.3
85
29-181
3,3'-Dichlorobenzidine
ug/L
100
81.9
82
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
100
100
1-181
4-Bromophenylphenyl ether
ug/L
50
45.6
91
53-127
4-Chloro-3-melhylphenol
ug/L
100
92.4
92
22-147
4-Chlorophenylphenyl ether
ug/L
50
44.8
90
25-158
4-Nitrophenol
ug/L
250
99.9
40
1-132
Acenaphthene
ug/L
50
43.6
87
47-145
Acenaphthylene
ug/L
50
44.0
88
33-145
Anthracene
ug/L
50
46.4
93
27-133
Benzo(a)anthracene
ug/L
50
46.1
92
33-143
Benzo(a)pyrene
ug/L
50
47.2
94
17-163
Benzo(b)fluoranthene
ug/L
50
46.4
93
24-159
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Serylces, LLG
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Outfall #2
Pace Project No.: 92432236
LABORATORY CONTROL SAMPLE:
2597578
Spike
LCS
LCS
%Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Benzo(g,h,i)perylene
ug/L
50
47.5
95
1-219
Benzo(k)fiuoranthene
ug/L
50
46.5
93
11-162
bis(2-Chloroethoxy)methane
ug/L
50
45.4
91
33-184
bis(2-Chloroethyl) ether
ug/L
50
45.5
91
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
46.8
94
8-158
Butylbenzylphthalate
ug/L
50
45.4
91
1-152
Chrysene
ug/L
50
42.5
85
17-168
Di-n-butylphthalate
ug/L
50
43.8
88
1-120
Di-n-octylphthalate
ug/L
50
47.5
95
4-146
Dibenz(a,h)anthracene
ug/L
50
48.7
97
1-227
Diethylphthalate
ug/L
50
43.6
87
1-120
Dimethylphthalate
ug/L
50
44.2
88
1-120
Fluoranthene
ug/L
50
47.6
95
26-137
Fluorene
ug/L
50
44.7
89
59-121
Hexachloro-1,3-butadiene
ug/L
50
41.2
82
24-120
Hexachlorobenzene
ug/L
50
43.7
87
1-152
Hexachlorocyclopentadiene
ug/L
50
34.4
69
25-150
Hexachloroethane
ug/L
50
37.8
76
40-120
Indeno(1,2,3-cd)pyrene
ug/L
50
47.1
94
1-171
Isophorone
ug/L
50
42.5
85
21-196
N-Nitroso-di-n-propyla mine
ug/L
50
46.4
93
1-230
N-Nitrosodimethylamine
ug/L
50
29.2
58
25-150
N-Nitrosodiphenylamine
ug/L
50
44.0
88
25-150
Naphthalene
ug/L
50
42.0
84
21-133
Nitrobenzene
ug/L
50
42.9
86
35-180
Pentachlorephenol
ug/L
100
89.8
90
14-176
Phenanthrene
ug/L
50
46.6
93
54-120
Phenol
ug/L
50
19.0
38
5-120
Pyrene
ug/L
50
48.1
96
52-120
2,4,6-Tribromophenol(S)
%
92
10-137
2-Fluorobiphenyl (S)
%
81
15-120
2-Fluorophenol (S)
%
47
10-120
Nitrobenzene-d5 (S)
e/
88
10-120
Phenol-d6 (S)
e/
33
10-120
Terphenyl-d14 (S)
%
89
11-131
MATRIX SPIKE SAMPLE:
2597579
92432236001
Spike
MS
MS
%Rec
Parameter
Units
Result
Conc.
Result
%Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
NO
49.5
28.8
58
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
NO
49.5
34.9
71
36-166
2,4,6-Trichlorophenol
ug/L
ND
49.5
45.3J
92
37-144
2,4-Dichlorophenol
ug/L
ND
49.5
37.9
77
39-135
2,4-Dimethylphenol
ug/L
ND
49.5
35.7J
72
32-120
2,4-Dinitrophenol
ug/L
-
NO
248
ND
0
1-191 M1
Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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�PaceAnalytil l
w�nrpacelabs.crom
Pace Analytical Services, LLD
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Outfall #2
Pace Project No.: 92432236
MATRIX SPIKE SAMPLE:
2597579
92432236001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
%Rec
Limits Qualifiers
2,4-Dinitrotoluene
ug/L
NO
49.5
28.3
57
39-139
2,6-Dinitrotoluene
ug/L
NO
49.5
32.2
65
50-158
2-Chloronaphthalene
ug/L
NO
49.5
31.4
63
60-120
2-Chlorophenol
ug/L
NO
49.5
32.2
65
23-134
2-Nitrophenol
ug/L
NO
49.5
17.3J
35
29-182
3,3'-Dichlorobenzidine
ug/L
NO
99
44.iJ
45
1-262
4,6-Dinitro-2-methylphenol
ug/L
NO
99
NO
0
1-181 Mt
4-Bromophenylphenyl ether
ug/L
NO
49.5
37.1
75
53-127
4-Chloro-3-methylphenol
ug/L
NO
99
80.1
81
22-147
4-Chlorophenylphenyl ether
ug/L
NO
49.5
37.5
76
25-158
4-Nitrophenol
ug/L
NO
248
74.5J
30
1-132
Acenaphthene
ug/L
NO
49.5
37.1
75
47-145
Acenaphthylene
ug/L
NO
49.5
36.7
74
33-145
Anthracene
ug/L
NO
49.5
37.7
76
27-133
Benzo(a)anthracene
ug/L
NO
49.5
39.4
80
33-143
Benzo(a)pyrene
ug/L
NO
49.5
39.2
79
17-163
Benzo(b)fluoranthene
ug/L
NO
49.5
39.4
80
24-159
Benzo(g,h,i)perylene
ug/L
NO
49.5
37.1
75
1-219
Benzo(k)fiuoranthene
ug/L
NO
49.5
39.3
79
11-162
bis(2-Chloroethoxy)methane
ug/L
NO
49.5
35.1J
71
33-184
bis(2-Chloroethyl) ether
ug/L
NO
49.5
36.0
73
12-158
bis(2-Ethylhexyl)phthalate
ug/L
NO
49.5
40.9
83
8-158
Butylbenzylphthalate
ug/L
NO
49.5
41.3
83
1-152
Chrysene
ug/L
NO
49.5
36.8
74
17-168
Di-n-butylphthalate
ug/L
NO
49.5
37.1
75
1-120
Di-n-octylphthalate
ug/L
NO
49.5
39.8
80
4-146
Dibenz(a,h)anthracene
ug/L
NO
49.5
37.3
75
1-227
Diethylphthalate
ug/L
NO
49.5
37.6
76
1-120
Dimethylphthalate
ug/L
NO
49.5
37.8
76
1-120
Fluoranthene
ug/L
NO
49.5
38.8
78
26-137
Fluorene
ug/L
NO
49.5
37.7
76
59-121
Hexachloro-1,3-butadiene
ug/L
NO
49.5
26.6
54
24-120
Hexachlorobenzene
ug/L
NO
49.5
36.1
73
1-152
Hexachlorocyclopentadiene
ug/L
NO
49.5
6J
12
25-150 M1
Hexachloroethane
ug/L
NO
49.5
26.4
53
40-120
Indeno(1,2,3-cd)pyrene
ug/L
NO
49.5
38.0
77
1-171
Isophorone
ug/L
NO
49.5
31.7J
64
21-196
N-Nitroso-di-n-propylamine
ug/L
NO
49.5
35.3
71
1-230
N-Nitrosodimethylamine
ug/L
NO
49.5
21.8J
44
25-150
N-Nitrosodiphenylamine
ug/L
NO
49.5
37.6J
76
25-150
Naphthalene
ug/L
NO
49.5
31.4
63
21-133
Nitrobenzene
ug/L
NO
49.5
35.5
72
35-180
Pentachlorophenol
ug/L
NO
99
24.1J
24
14-176
Phenanthrene
ug/L
NO
49.5
38.0
77
54-120
Phenol
ug/L
NO
49.5
16.7J
34
5-120
Pyrene
ug/L
NO
49.5
40.5
82
52-120
2,4,6-Tribromophenol(S)
%
83
10-137
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 06/19/2019 12:25 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 23

41aceAnalytical
�wnapaceleDs.cam
i
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Outfall #2
Pace Project No.: 92432236
MATRIX SPIKE SAMPLE:
2597579
92432236001
Spike
MS
MS
e/ Rec
Parameter
Units
Result
Conc.
Result
e/ Rec
Limits Qualifiers
2-Fluorobiphenyl (S)
%
69
15-120
2-Fluorophenol(S)
%
41
10-120
Nitrobenzene-d5 (S)
%
_
69
10-120 D3
Phenol-d6 (S)
%
28
10-120
Terphenyl-d14 (S)
e/
82
11-131
SAMPLE DUPLICATE: 2597580
92432239001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,2,4-Trichlorobenzene
ug/L
ND
ND
2,2'-Oxybis(1-chloropropane)
ug/L
ND
ND
2,4,6-Trichlorophenol
ug/L
ND
ND
2,4-Dichlorophenol
ug/L
ND
ND
2,4-Dimethylphenol
ug/L
ND
ND
2,4-Dinitrophenol
ug/L
ND
ND
2,4-Dinitrotoluene
ug/L
ND
ND
2,6-Dinitrotoluene
ug/L
ND
ND
2-Chloronaphthalene
ug/L
ND
ND
2-Chlorophenol
ug/L
ND
ND
2-Nitrophenol
ug/L
ND
_
ND
3,3'-Dichlorobenzidine
ug/L
ND
ND
4,6-Dinitro-2-methylphenol
ug/L
ND
ND
4-Bromophenylphenyl ether
ug/L
ND
ND
4-Chloro-3-methylphenol
ug/L
ND
ND
4-Chlorophenylphenyl ether
ug/L
ND
ND
4-Nitrophenol
ug/L
ND
ND
Acenaphthene
ug/L
ND
ND
Acenaphthylene
ug/L
ND
ND
Anthracene
ug/L
ND
ND
Benzo(a)anthracene
ug/L
ND
ND
Benzo(a)pyrene
ug/L
ND
ND
Senzo(b)fluoranthene
ug/L
ND
ND
Senzo(g,h,i)perylene
ug/L
ND
ND
Benzo(k)Fluoranthene
ug/L
ND
ND
bis(2-Chlorcethoxy)methane
ug/L
ND
ND
bis(2-Chlorcethyl) ether
ug/L
ND
ND
bis(2-Ethylhexyl)phthalate
ug/L
ND
ND
Butyl benzyl phtha late
ug/L
ND
ND
Chrysene
ug/L
ND
ND
Di-n-butylphthalate
ug/L
ND
ND
Di-n-octylphthalate
ug/L
ND
ND
Dibenz(a,h)anthracene
ug/L
ND
ND
Diethyl phtha late
ug/L
ND
ND
Dimethylphthalate
ug/L
ND
ND
Fluoranthene
ug/L
ND
ND
Results prose med on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/19/2019 12:25 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 23

aceAnalytical
wmvpscelabacGm
1
i
QUALITY CONTROL DATA
Project: Outfall #2
Pace Project No.: 92432236
SAMPLE DUPLICATE: 2597580
Parameter
Units
92432239001
Result
Dup
Result
Fluorene
ug/L
ND
ND
Hexachloro-1,3-butadiene
ug/L
ND
ND
Hexachlorobenzene
ug/L
ND
ND
Hexachlorocyclopentadiene
ug/L
ND
ND
Hexachloroethane
ug/L
ND
ND
Indeno(1,2,3-cd)pyrene
ug/L
ND
ND
Isophorone
ug/L
ND
ND
N-Nitroso-di-n-propylamine
ug/L
ND
ND
N-Nitrosodimethylamine
ug/L
ND
ND
N-Nitrosodiphenylamine
ug/L
ND
ND
Naphthalene
ug/L
ND
ND
Nitrobenzene
ug/L
ND
ND
Pentachlorophenol
ug/L
ND
ND
Phenanthrene
ug/L
ND
ND
Phenol
ug/L
ND
ND
Pyrene
ug/L
ND
ND
2,4,6-Tribromophenol(S)
%
71
93
2-Fluorobiphenyl (S)
%
76
75
2-Fluorophenol (S)
%
40
44
Nitrobenzene-d5 (S)
%
85
83
Phenol-d6 (S)
%
29
32
Terphenyl-d14 (S)
%
94
88
RPD Qualifiers
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Results presented on this page are in the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical o
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I
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Outfali #2
Pace Project No.: 92432236
QC Batch: 480470
Analysis Method: SM 254OD-2011
QC Batch Method: SM 254OD-2011
Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92432236001
METHOD BLANK: 2599455
Matrix:
Water
Associated Lab Samples: 92432236001
Blank
Reporting
Parameter
Units
Result
Limit Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 06/12/19 05:01
LABORATORY CONTROL SAMPLE: 2599456
Spike
LCS LCS a/ Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Total Suspended Solids
mg/L
250
236 94 90-110
SAMPLE DUPLICATE: 2599457
92432040001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
1960
2240 13 D6
SAMPLE DUPLICATE: 2599458
92432246002
Dup
Parameter
Units
Result
Result RPR Qualifiers
Total Suspended Solids
mg/L
1310
1250 5
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical®
navvr.pecelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Project: Outfall #2
Pace Project No.: 92432236
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The Ni Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
SAMPLE QUALIFIERS
Sample: 92432236001
Ill The samples were received outside of required temperature range. Analysis was completed upon client approval.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLCM
aceAnalytical sRiverside
AshevheA ille, NC 2880404
www.Pacalabs.com [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Outfall #2
92432236
Analytical
Lab ID
Sample'ID
QC Batch Method
QC Batch
Analytical Method
Batch
92432236001
Outfall #2
EPA 1664E
480856
92432236001
Outfall #2
EPA 200.7 Rev 4.4 1994
480942
EPA 200.7 Rev 4.4 1994
481076
92432236001
Outfall #2
EPA 625.1
480044
EPA 625.1
480566
92432236001
Outfall #2
EPA 624.1
480087
92432236001
Outfall #2
SM 254OD-2011
480470
8
REPORT OF LABORATORY ANALYSIS
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"
Document Name: I DOtliment Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR) Page 1 of 2
-F't1CBill13/ICiI/
Documen[No,'. Issuing Authority.
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville LYJ EdenF1 Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicsville❑
Client Name: 912413
;.z• .. •'. .,, a.M f PP/'le �.s---�� l'✓ 2236
Project y
Courier: ❑Fed Ex [AUPS ❑USPS ❑Client ,'�
❑ Commercial ❑Pace ❑Other_ 3d,•9�1.<fb
Custody Seal Present? ❑Yes NNo Seals Intact? ❑Ycs '&No
Packing Material: ❑Bubble Wrap KjBuhble Bags ❑None ❑ Other
Thermometer: ��� Type of Ice: ❑\Net ❑Blue
[y Ill Gun lD:
Cooler Temp ("C): 13, _7 Correction Factor: Add/Subtract (°C) 0—
Cooler Temp Corrected (°C): � 7
USDA Regulated Soil (Z N/A, water sarnplo)
Did samples originate In a quarantine zone within Lhe United States: CA, NY, or SC (check maps)?
'sri,,..
Nu N/A
Time? �❑Vu ❑Id/A
Date/Initials Person Exornining Contcnts:±�;_'X/y"3
Biological Tissryur3�e��, Frozen?
[]Yes []No ,yN/A
IA
Temp should be above freezing to 6°C
�S:,mpls out of tenip criteria. Samples an ice, cooling process
has Se,,m,
Did$.,a ales originate fmnr a foreign Sour" iloty la
Indudu-a, Harroll and Puerto fllco(?❑Yes ,
Comments/Discrepa(Icy:
Short Hold Time Analysis(<72 hr.)?
❑YueJNu
3. _ _—..--_-
{. _. .—..—. —..... -
RushTurnAroundTimeRequested? ❑1'•s J
_.❑N/n
❑N/A
SIiHICIC111 Volume?__
�les
❑IJ
❑Iv/r�
5. _ __-- ---.
b.
Collect Containers Used? Q'ius ❑IJo
❑(VA
-Pace Containers Used?
•Ya•.
❑Nu
❑N/A
Containers Intact?
21y's
❑IJo
❑N/A
7.
8_--_—
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CHAIN -OF -CUSTODY I Analytical Request Document
'RIceA 'l:1' MI The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section a section C 1
Page t Of 1
Required Client information: Required Project Information: Invoice Information:
Company: mmc-Peerless Growers Report To: Don Wallin Appm.pn
Company Name.
Add:psz'. 1]I Sw'n Ardra•S Avencc Copy T.:
A cress'/J. 7 f .1 .f> '��T Re ulata A nc
Nol Spanps l
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,Jyare Analytical
www.pecela6s.mm
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
June 19, 2019
Mr. Donald Wallin
MMC, Peerless Blowers
172 South Andrews Avenue
Hot Springs, NC 28743
RE: Project: Outfall #1
Pace Project No.: 92432239
Dear Mr. Wallin:
Enclosed are the analytical results for sample(s) received by the laboratory on June 07, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 23

ace Analytical
ewxpacelabs.corn
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville; NC 28804
[phone]
CERTIFICATIONS
Project: Outfall #1
Pace Project No.: 92432239
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LAI70028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Wginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 23

Pace Analytical Services, LLC
,�aceAshevihevi Analytical ® Riverside lle, NC 2880404
r wpacelabs.= [phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Outfall #1
92432239
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92432239001
Outfall #1
EPA 1664E
JMS
1
PASI-C
EPA 200.7 Rev 4.4 1994
IDS
3
PASI-A
EPA 625.1
BPJ
58
PASI-C
EPA 624.1
DLK
34
PASI-C
SM 254OD-2011
MJP
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 23

aceAnalytical o
xwxpacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
AsheviI16, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Outfall #1
Pace Project No.: 92432239
Sample: Outfall #1
Lab ID: 92432239001 Collected:
06/05/19
13:20
Received: 06/07119 10:20 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND
mg/L
4.8
1
06/13/19 06:22
200.7 MET ICP
Analytical Method:
EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Copper
7.4
ug/L
5.0
1
06/13/19 16:11
06/17/19 05:46
7440-50-8
Lead
ND
ug/L
5.0
1
06/13/19 16:11
06/17/19 05:46
7439-92-1
Zinc
13.1
ug/L
10.0
1
06/13/19 16:11
06/17/19 05:46
7440-66-6
625 MSSV
Analytical Method:
EPA625.1
Preparation Method:
EPA625A
'
Acenaphthene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
83-32-9
Acenaphthylene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
208-96-8
Anthracene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
120-12-7
Benzo(a)anthracene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
56-55-3
Benzo(a)pyrene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
50-32-8
Benzo(b)fluoranthene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
191-24-2
Benzo(k)fluoranthene
ND
ug/L
4.9
1
06/10/19 17:28
06112/1912:19
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
101-55-3
Butylbenzylphlhalate
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
9.8
1
06/10/19 17:28
06/12/19 12:19
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
111-44-4
2-Chloronaphthalene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
91-58-7
2-Chlorophenol
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
7005-72-3
Chrysene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
24.5
1
06/10/19 17:28
06/12/19 12:19
91-94-1
2,4-Dichlorophenol
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
120-83-2
Diethylphtha late
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
84-66-2
2,4-Dimethylphenol
ND
ug/L
9.8
1
06/10/19 17:28
06/12/19 12:19
105-67-9
Dimethylphthalate
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
131-11-3
Di-n-butylphthalate
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
19.6
1
06/10/19 17:28
06112/1912:19
534-52-1
2,4-Dinitrophenol
ND
ug/L
49.0
1
06/10/19 17:28
06/12/19 12:19
51-28-5
2,4-Dinitrotoluene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
121-14-2
2,6-Dinitrotoluene
ND
ug/L
4.9
1
06110/1917:28
06/1211912:19
606-20-2
Di-n-octylphthalate
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
117-81-7
Fluoranthene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
206-44-0
Fluorene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
86-73-7
Hexachloro-1,3-buladiene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
87-68-3
Hexachlorobenzene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
118-74-1
Hexachlorocyclopenladiene
ND
ug/L
9.8
1
06/1011917:28
06112/1912:19
77-47-4
Hexachloroethane
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
193-39-5
Isophorone
ND
ug/L
9.8
1
06/10/19 17:28
06/12/19 12:19
78-59-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 23

ace Analytical
wwwpacelaas.ctlm
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Outfall #1
Pace Project No.: 92432239
Sample: Outfall #1
Parameters
ANALYTICAL RESULTS
Lab ID: 92432239001 Collected: 06/05/19 13:20 Received: 06/07/19 10,20 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Oual
625 MSSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Naphthalene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
91-20-3
Nitrobenzene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
98-95-3
2-Nitrophenol
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
88-75-5
4-Nitrophenol
NO
ug/L
49.0
1
06/10/19 17:28
0611211912:19
100-02-7
N-Nitrosodimethylamine
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
9.8
1
06/10/19 17:28
06/12/19 12:19
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
108-60-1
Pentachlorophenol
ND
ug/L
9.8
1
06/10/19 17:28
06/12/19 12:19
87-86-5
Phenanthrene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
85-01-8
Phenol
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
108-95-2
Pyrene
ND
ug/L
4.9
1
06/10/19 17:28
06/12/19 12:19
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
4.9
1
06/1011917:28
06112/1912:19
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
9.8
1
06110/1917:28
06/12/19 12:19
88-06-2
Surrogates
Nitrobenzene-d5 (S)
85
%
10-120
1
06/10/19 17:28
06/12/19 12:19
4165-60-0
2-Fluorobiphenyl (S)
76
%
15-120
1
06/10/19 17:28
06/12/19 12:19
321-60-8
Terphenyl-d14 (S)
94
%
11-131
1
06/10/19 17:28
06/12/19 12:19
1718-51-0
Phenol-d6 (S)
29
%
10-120
1
06/10/19 17:28
06/12/19 12:19
13127-88-3
2-Fluorophenol (S)
40
%
10-120
1
06/10/19 17:28
06/12/19 12:19
367-12-4
2,4,6-Tribromophenol(S)
71
%
10-137
1
06/10/19 17:28
06/12/19 12:19
118-79-6
624 Volatile Organics
Analytical Method:
EPA 624.1
Benzene
ND
ug/L
1.0
1
06/10/19 15:37
71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
06/10/19 15:37
75-27-4
Bromoform
ND
ug/L
2.0
1
06/10/19 15:37
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/10/19 15:37
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
06/10/19 15:37
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
06/10/19 15:37
108-90-7
Chloroethane
ND
ug/L
2.0
1
06110/1915:37
75-00-3
Chloroform
ND
ug/L
5.0
1
06110/1915:37
67-66-3
Chloromethane
ND
ug/L
2.0
1
06/10/19 15:37
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
06/10/19 15:37
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
06/10/19 15:37
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
06/10/19 15:37
541-73-1
1,4-Dichlorobenzene
ND
ug/L -
2.0
1
06/10/19 15:37
106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1
-
06/10/19 15:37
75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
1
06110/1915:37
107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1
06110/1915:37
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
1
06/10/19 15:37
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.0
1
06110/1915:37
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
1
06110/1915:37
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2.0
1
06/10/1915: 37
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
2.0
1
06110/1915:37
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
06/10/19 15:37
100-41-4
Methylene Chloride
ND
ug/L
5.0
1
06/10/19 15:37
75-09-2
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
06/10/19 15:37
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 12:26 PM without the written consent of Pace Analytical Services, L-C. Page 5 of 23

11�9alce Analytical
w ..pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
AshevilIC, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Outfall #1
Pace Project No.: 92432239
Sample: Outfall #1 Lab ID: 92432239001 Collected: 06/05/19 13:20 Received: 06/07/19 10:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
624 Volatile Organics Analytical Method: EPA 624.1
Tetrachloroethene
ND
ug/L
2.0
1
06/10/19 15:37
127-18-4
Toluene
ND
ug/L
1.0
1
06/10/19 15:37
108-88-3
1,1,1-Trichloroethane
ND
ug/L
2.0
1
06110/1915:37
71-55-6
1,12-Trichloroethane _
ND
ug/L
2.0
1
06/10/19 15:37
79-00-5
Trichloroethene
ND
ug/L
2.0
1
06/10/19 15:37
79-01-6
Trichloroflucromethane
ND
ug/L
2.0
1
06/10/191537
75-69-4
Vinyl chloride
ND
ug/L
2.0
1
06/10/19 15:37
75-01-4
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
06/10/19 15:37
460-00-4
Toluene-d8 (S)
97
%
70-130
1
06/10/19 15:37
2037-26-5
1,2-Dichloroethane-d4(S)
103
%
70-130
1
06/10/19 15:37
17060-07-0
2540D Total Suspended Solids
Analytical Method:
SM 254OD-2011
Total Suspended Solids
4.3
mg/L
3.8
1
06/12/19 05:01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 23

ace Analytical
wwwpacetabs.corn
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project:
Outfall #1
Pace Project No.:
92432239
QC Batch:
480856 Analysis Method: EPA 1664B
QC Batch Method:
EPA 1664E Analysis Description: 1664 SGT-HEM, TPH /
Associated Lab Samples:
92432239001
METHOD BLANK: 2601099
Associated Lab Samples: 92432239001
Parameter Units
Total Petroleum Hydrocarbons mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 4.8 06/13/19 06:17
LABORATORY CONTROL SAMPLE:
2601100
Spike LCS
LCS
% Rep
Parameter
Units
Conc. Result
% Rep
Limits
Qualifiers
Total Petroleum Hydrocarbons
mg/L
19.2
20.4
106
64-132
MATRIX SPIKE SAMPLE:
2601101
92432427001
Spike
MS
MS
% Rep
Parameter
Units
Result
Conc.
Result
%Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
NO
19.2
19.1
99
64-132
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 23

,�ace Analytical
wvwpacelebs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
AsheviII0, NC 28804
[phone]
Project:
Outfall #1
Pace Project No.:
92432239
QC Batch:
480942 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method:
EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92432239001
METHOD BLANK: 2601435 Matrix: Water
Associated Lab Samples: 92432239001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Copper ug/L NO 5.0 06/17/19 04:24
Lead ug/L NO 5.0 06/17/19 04:24
Zinc ug/L NO 10.0 06/17/19 04:24
LABORATORY CONTROL SAMPLE:
2601436
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Copper
ug/L
500
456 91 85-115
Lead
ug/L
500
444 89 85-115
Zinc
ug/L
500
456 91 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2601437
2601438
MS
MSD
92431704001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD Qual
Copper
ug/L
8.7
500
500
494
484
97
95
70-130
2
Lead
ug/L
<5.0
500
500
472
456
94
91
70-130
3
Zinc
ug/L
11.5
500
500
495
485
97
95
70-130
2
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2601439
2601440
MS
MSD
92431833001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD Qual
Copper
ug/L
1710
500
500
2130
1750
85
9
70-130
20 M1
Lead
ug/L
125
500
500
501
498
75
75
70-130
1
Zinc
ug/L
2820
5C0
500
3180
2970
71
29
70-130
7 M1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06119/2019 12:26 PM without the written consent of Pace Analytical Services, L-C. Page 8 of 23

�,acoAnalyticala
www.PasalaDs.tom
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Outfall #1
Pace Project No.: 92432239
QC Batch: 480087 Analysis Method: EPA 624.1
QC Batch Method: EPA624.1 Analysis Description: 624 MSV
Associated Lab Samples: 92432239001
METHOD BLANK: 2597664
Associated Lab Samples: 92432239001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
1,1,1-Trichloroethane
ug/L
NO
2.0
06110/1912:21
1,1,2,2-Tetrachloroethane
ug/L
NO
2.0
06/10/19 12:21
1,1,2-Trichloroethane
ug/L
NO
2.0
06/10/19 12:21
1,1-Dichloroethane
ug/L
NO
2.0
06/10/19 12:21
1,1-Dichloroethene
ug/L
NO
2.0
06110/1912:21
1,2-Dichlorobenzene
ug/L
NO
2.0
06/10/19 12:21
1,2-Dichloroethane
ug/L
NO
2.0
06/1011912:21
1,2-Dichloropropane
ug/L
NO
2.0
06/10/19 12:21
1,3-Dichlorobenzene
ug/L
NO
2.0
06/1011912:21
1,4-Dichlorobenzene
ug/L
ND
2.0
06/1011912:21
Benzene
ug/L
NO
1.0
0611011912:21
Bromodichloromethane
ug/L
ND
2.0
06/1011912:21
Bromoform
ug/L
NO
2.0
06/10/19 12:21 ,
Bromomelhane
ug/L
ND
2.0
06/1011912:21
Carbon tetrachloride
ug/L
NO
2.0
06/10/19 12:21
Chlorobenzene
ug/L
NO
2.0
06/1011912:21
Chloroethane
ug/L
ND
2.0
06/10/19 12:21
Chloroform
ug/L
ND
5.0
06/10/19 12:21
Chloromethane
ug/L
ND
2.0
06/10/19 12:21
cis-1,2-Dichloroethene
ug/L
NO
2.0
06/1011912:21
cis-1,3-Dichloropropene
ug/L
NO
2.0
0611011912:21
Dibromochlorom ethane
ug/L
NO
2.0
06/10/19 12:21
Ethylbenzene
ug/L
NO
1.0
06/10/19 12:21
Methylene Chloride
ug/L
NO
5.0
06/10/19 12:21
Tetrachloroethene
ug/L
NO
2.0
06/10/19 12:21
Toluene
ug/L
NO
1.0
06/10/19 12:21
trans-1,2-Dichloroethene
ug/L
NO
2.0
06/10/19 12:21
trans-1,3-Dichloropropene
ug/L
NO
2.0
06/10/19 12:21
Trichloroethene
ug/L
NO
2.0
06/10/19 12:21
Trichlorofluoromethane
ug/L
NO
2.0
06/10/19 12:21
Vinyl chloride
ug/L
NO
2.0
06/10/19 12:21
1,2-Dichloroethane-d4 (S)
%
99
70-130
06/10/19 12:21
4-Bromofluorobenzene (S)
%
96
70-130
06/10/19 12:21
Toluene-d8 (S)
%
95
70-130
06/10/19 12:21
LABORATORY CONTROL SAMPLE: 2597665
Spike LCS LCS %Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 16.5 82 70-130
1,1,2,2-Tetrachloroethane ug/L 20 15.6 78 60-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 12:26 PM without the written consent of Pace Analytical Services, L-C. Page 9 of 23

ace Analytical
www.pscalabs.mm
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Outfall #1
Pace Project No.: 92432239
LABORATORY CONTROL SAMPLE:
Parameter
2597665
Units
Spike
Conc.
LCS
Result
LCS
%Rec
%Red
Limits
1,1,2-Trichloroethane
ug/L
20
17.9
90
70-130
1,1-Dichloroethane
ug/L
20
17.0
85
70-130
1,1-Dichloroethene
ug/L
20
16.6
83
50-150
1,2-Dichlorobenzene
ug/L
20
18.0
90
65-135
1,2-Dichloroethane
ug/L
20
16.6
83
49-155
1,2-Dichloropropane
ug/L
20
17.4
87
35-165
1,3-Dichlorobenzene
ug/L
20
18.2
91
70-130
1,4-Dichlorobenzene
ug/L
20
17.9
89
65-135
Benzene
ug/L
20
16.7
84
65-135
Bromodichloromethane
ug/L
20
16.7
83
65-135
Bromoform
ug/L
20
17A
86
70-130
Bromomethane
ug/L
20
17.2
86
15-185
Carbon tetrachloride
ug/L
20
17.1
86
70-130
Chlorobenzene
ug/L
20
17.1
86
65-135
Chloroethane
ug/L
20
17.9
90
40-160
Chloroform
ug/L
20
17.2
86
70-135
Chloromethane
ug/L
20
17.1
86
1-205
cis-1,2-Dichloroethene
ug/L
20
16.5
82
68-146
cis-1,3-Dichloropropene
ug/L
20
17.0
85
25-175
Dibromochloromethane
ug/L
20
17.3
87
70-135
Ethylbenzene
ug/L
20
17.5
88
60-140
Methylene Chloride
ug/L
20
18.8
94
60-140
Tetrachloroethene
ug/L
20
18.2
91
70-130
Toluene
ug/L
20
16.9
85
70-130
trans-1,2-Dichloroethene
ug/L
20
16.3
82
70-130
trans-1,3-Dichloropropene
ug/L
20
17.6
88
50-150
Trichloroethene
ug/L
20
16.7
84
65-135
Trichlorofluoromethane
ug/L
20
17.9
89
50-150
Vinyl chloride
ug/L
20
18.6
93
5-195
1,2-Dichloroethane-d4(S)
%
97
70-130
4-Bromofluorobenzene (S)
e/
92
70-130
Toluene-d8 (S)
%
99
70-130
Qualifiers
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE:
2597666
2597667
MS
MSD
92431072003
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter
Units
Result
Cord,
Conc.
Result
Result
%Rec
%Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
20
20
15.0
18.2
75
91
52-162
19
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
13.8
16.2
69
81
46-157
16
1,1,2-Trichloroethane
ug/L
ND
20
20
15.2
16.8
76
84
52-150
10
1,1-Dichloroethane
ug/L
ND
20
20
14.2
16.7
71
83
59-155
16
1,1-Dichloroethene
ug/L
ND
20
20
15.5
17.6
78
88
1-234
13
1,2-Dichlorobenzene
ug/L
ND
20
20
15.2
18.2
76
91
18-190
18
1,2-Dichloroethane
ug/L
ND
20
20
13.4
16.3
67
82
49-155
19
1,2-Dichloropropane
ug/L
ND
20
20
15.4
16.9
77
85
1-210
9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 23

,�acoAnalyticalo
wwwpacelabs.corn
QUALITY CONTROL DATA
Project: Outfall #1
Pace Project No.: 92432239
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2597666
MS
92431072003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2597667
MS
Result
MSD
Result
MS
%Rec
MSD
%Rec
% Rec
Limits
RPD Qual
1,3-Dichlorobenzene
ug/L
ND
20
20
16.0
18.8
80
94
59-156
17
1,4-Dichlorobenzene
ug/L
ND
20
20
16.2
18.8
81
94
18-190
15
Benzene
ug/L
ND
20
20
16.6
18.8
83
94
37-151
12
Bromodichloromethane
ug/L
ND
20
20
15.2
17.6
76
88
35-155
14
Bromoform
ug/L
ND
20
20
14.0
16.8
70
84
45-169
18
Bromomethane
ug/L
ND
20
20
10.7
12.0
53
60
1-242
11
Carbon tetrachloride
ug/L
ND
20
20
17.0
19.6
85
98
70-140
14
Chlorobenzene
ug/L
ND
20
20
15.4
18.4
77
92
37-160
18
Chloroethane
ug/L
ND
20
20
16.3
18.8
81
94
14-230
14
Chloroform
ug/L
ND
20
20
15.9
18.5
72
84
51-138
15
Chloromethane
ug/L
ND
20
20
16.3
18.3
81
91
1-273
11
cis-1,2-Dichloroethene
ug/L
ND
20
20
14.7
16.3
72
80
45-174
10
cis-1,3-Dichloropropene
ug/L
ND
20
20
14.6
16.7
73
83
1-227
13
Dibromochloromethane
ug/L
ND
20
20
15.1
17.3
75
87
53-149
14
Ethylbenzene
ug/L
ND
20
20
16.0
18.9
80
94
37-162
17
Methylene Chloride
ug/L
ND
20
20
13.6
15.9
68
79
1-221
15
Tetrachloroethene
ug/L
ND
20
20
17.5
20.5
85
100
64-148
16
Toluene
ug/L
ND
20
20
16.1
18.6
76
88
47-150
14
trans-1,2-Dichloroethene
ug/L
ND
20
20
14.9
17.2
74
86
54-156
14
trans-1,3-Dichloropropene
ug/L
ND
20
20
15.5
16.9
77
85
17-183
9
Trichloroethene
ug/L
ND
20
20
15.7
17.7
79
89
70-157
12
Trichlorofluoromethane
ug/L
ND
20
20
16.8
19.1
84
95
17-181
13
Vinyl chloride
ug/L
ND
20
20
16.8
19.5
84
98
1-251
15
1,2-Dichloroethane-d4 (S)
%
90
97
70-130
4-Bromofluorobenzene(S)
%
95
98
70-130
Toluene-d8 (S)
%
98
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 23

1 ace Analytical
wwwpacelabs.corn
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Outfall #1
Pace Project No.: 92432239
QC Batch: 480044
QC Batch Method: EPA 625.1
Associated Lab Samples: 92432239001
Analysis Method:
Analysis Description:
EPA 625.1
625 MSS
METHOD BLANK: 2597577
Matrix: Water
Associated Lab Samples: 92432239001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
NO
5.0
06/12/1910:41
2,2'-Oxybis(1-chloropropane)
ug/L
NO
5.0
06/121191041
2,4,6-Trichlorophenol
ug/L
NO
10.0
06/12/1910:41
2,4-Dichlorophenol
ug/L
ND
5.0
06/12/1910:41
2,4-Dimethylphenol
ug/L
NO
10.0
06/12/1910:41
2,4-Dinitrophenol
ug/L
NO
50.0
06/12/1910:41
2,4-Dinitrotoluene
ug/L
NO
5.0
0611211910:41
2,6-Dinitrotoluene
ug/L
NO
5.0
0611211910:41
2-Chloronaphthalene
ug/L
NO
5.0
06/1211910:41
2-Chlorophenol
ug/L
NO
5.0
06/12/1910*41
2-Nitrophenol
ug/L
NO
5.0
0611211910*41
3,3'-Dichlorobenzidine
ug/L
NO
25.0
0611211910*41
4,6-Dinitro-2-methylphenol
ug/L
NO
20.0
06/12/191041
4-Bromophenylphenyl ether
ug/L
NO
5.0
06/12/19 10:41
4-Chloro-3-methylphenol
ug/L
NO
5.0
06/12/1910*41
4-Chlorophenylphenyl ether
ug/L
NO
5.0
06/12/19 1041
4-Nitrophenol
ug/L
NO
50.0
06112/1910,41
Acenaphthene
ug/L
NO
5.0
06112/1910:41
Acenaphthylene
ug/L
NO
5.0
06/12/1910*41
Anthracene
ug/L
NO
5.0
06/12/1910*41
Benzo(a)anthracene
ug/L
NO
5.0
06/12/1910,41
Benzo(a)pyrene
ug/L
NO
5.0
06/12/1910:41
Benzo(b)fluoranthene
ug/L
NO
5.0
06/12/1910:41
Benzo(g,h,i)perylene
ug/L
NO
5.0
06/12/1910:41
Benzo(k)fluoranthene
ug/L
NO
5.0
06/12/1910:41
bis(2-Chloroethoxy)methane
ug/L
NO
10.0
06112/1910:41
bis(2-Chloroethyl) ether
ug/L
NO
5.0
06/12/19 1041
bis(2-Ethylhexyl)phthalate
ug/L
NO
5.0
06/12/191041
Butylbenzylphthalate _
ug/L
NO
5.0
06/12/191041
Chrysene
ug/L
NO
5.0
06/12/1910:41
Di-n-butylphthalate
ug/L
NO
5.0
0611211910:41
Di-n-octylphthalate
ug/L
NO
5.0
0611211910:41
Dibenz(a,h)anthracene
ug/L
NO
5.0
06112/1910:41
Diethylphthalate
ug/L
NO
5.0
06112/1910*41
Dimethytphthalate
ug/L
NO
5.0
06/12/1910:41
Fluoranthene
ug/L
NO
5.0
06112/1910:41
Fluorene
ug/L
NO
5.0
06/12/1910:41
Hexachloro-1,3-butadiene
ug/L
NO
5.0
06/12/1910,41
Hexachlorobenzene
ug/L
NO
5.0
06/12/1910*41
Hexachlorocyclopentadiene
ug/L
NO
10.0
06/12/1910:41
Hexachloroethane
ug/L
NO
5.0
06/12/1910:41
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/19/2019 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 23

,�aceAnalyfical
www.pacelabs.crom
QUALITY CONTROL DATA
Project: Oulfall #1
Pace Project No.: 92432239
METHOD BLANK: 2597577
Associated Lab Samples: 92432239001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
06/12/19 10:41
Isophorone
ug/L
ND
10.0
06/12/19 10:41
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
06112/1910:41
N-Nitrosodimethylamine
ug/L
ND
5.0
0611211910:41
N-Nitrosodiphenylamine
ug/L
ND
10.0
06/1211910:41
Naphthalene
ug/L
ND
5.0
06/12/19 10:41
Nitrobenzene
ug/L
ND
5.0
06/1211910:41
Pentachlorophenol
ug/L
ND
10.0
06/12/19 10:41
Phenanthrene
ug/L
ND
5.0
06/1211910:41
Phenol
ug/L
ND
5.0
06/1211910:41
Pyrene
ug/L
ND
5.0
06/1211910:41
2,4,6-Tribromophenol (S)
%
91
10-137
06/12/19 10:41
2-Fluorobiphenyl (S)
%
77
15-120
06/12/19 10:41
2-Fluorophenol (S)
e/
42
10-120
06/12/19 10:41
Nitrobenzene-d5 (S)
e/
82
10-120
06/12/19 10:41
Phenol-d6 (S)
e/
29
10-120
06/12/19 10:41
Terphenyl-d 14 (S)
e/
94
11-131
06/12/19 10:41
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2597578
Units
Spike
Conc.
LCS
Result
LCS
%Rec
e/ Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
39.5
79
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
42.1
84
36-166
2,4,6-Trichlorophenol
ug/L
50
46.8
94
37-144
2,4-Dichlorophenol
ug/L
50
44.3
89
39-135
2,4-Dimethylphenol
ug/L
50
43.2
86
32-120
2,4-Dinitrophenol
ug/L
250
220
88
1-191
2,4-Dinitrotoluene
ug/L
50
44.2
88
39-139
2,6-Dinitrotoluene
ug/L
50
43.7
87
50-158
2-Chloronaphthalene
ug/L
50
38.6
77
60-120
2-Chlorophenol
ug/L
50
41.5
83
23-134
2-Nitrophenol
ug/L
50
42.3
85
29-181
3,3'-Dichlorobenzidine
ug/L
100
81.9
82
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
100
100
1-181
4-Bromophenylphenyl ether
ug/L
50
45.6
91
53-127
4-Chloro-3-methylphenol
ug/L
100
92.4
92
22-147
4-Chlorophenylphenyl ether
ug/L
50
44.8
90
25-158
4-Nitrophenol
ug/L
250
99.9
40
1-132
Acenaphthene
ug/L
50
43.6
87
47-145
Acenaphlhylene
ug/L
50
44.0
88
33-145
Anthracene
ug/L
50
46.4
93
27-133
Benzo(a)anthracene
ug/L
50
46.1
92
33-143
Benzo(a)pyrene
ug/L
50
47.2
94
17-163
Benzo(b)fluoranthene
ug/L
50
46.4
93
24-159
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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ace Analytical
amw.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville'NC 28804
[phone]
QUALITY CONTROL DATA
Project: Outfall #1
Pace Project No.: 92432239
LABORATORY CONTROL SAMPLE:
2597578
Spike
LCS
LCS
% Rao
Parameter
Units
Conc.
Result
e/ Rec
Limits
Qualifiers
Benzo(g,h,l)perylene
ug/L
50
47.5
95
1-219
Benzo(k)fiuoranthene
ug/L
50
46.5
93
11-162
bis(2-Chloroethoxy)methane
ug/L
50
45.4
91
33-184
bis(2-Chloroethyl) ether
ug/L
50
45.5
91
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
46.8
94
8-158
Butylbenzylphthalate
ug/L
50
45.4
91
1-152
Chrysene
ug/L
50
42.5
85
17-168
Di-n-butylphthalate
ug/L
50
43.8
88
1-120
Di-n-octylphthalate
ug/L
50
47.5
95
4-146
Dibenz(a,h)anthracene
ug/L
50
48.7
97
1-227
Diethylphthalate
ug/L
50
43.6
87
1-120
Dimethylphthalate
ug/L
50
44.2
88
1-120
Fluoranthene
ug/L
50
47.6
95
26-137
Fluorene
ug/L
50
44.7
89
59-121
Hexachloro-1,3-butadiene
ug/L
50
41.2
82
24-120
Hexachlorobenzene
ug/L
50
43.7
87
1-152
Hexachlorocyclopentadiene
ug/L
50
34.4
69
25-150
Hexachloroethane
ug/L
50
37.8
76
40-120
Indeno(1,2,3-cd)pyrene
ug/L
50
47.1
94
1-171
Isophorone
ug/L
50
42.5
85
21-196
N-Nitroso-di-n-propylamine
ug/L
50
46.4
93
1-230
N-Nitrosodimethylamine
ug/L
50
29.2
58
25-150
N-Nitrosodiphenylamine
ug/L
50
44.0
88
25-150
Naphthalene
ug/L
50
42.0
84
21-133
Nitrobenzene
ug/L
50
42.9
86
35-180
Pentachlorophenol
ug/L
100
89.8
90
14-176
Phenanthrene
ug/L
50
46.6
93
54-120
Phenol
ug/L
50
19.0
38
5-120
Pyrene
ug/L
50
48.1
96
52-120
2,4,6-Tribromophenol(S)
%
92
10-137
2-Fluorobiphenyl(S)
%
81
15-120
2-Fluorophenol (S)
%
47
10-120
Nitrobenzene-d5 (S)
%
88
10-120
Phenol-d6 (S)
%
33
10-120
Terpher l-d14 (S)
%
89
11-131
MATRIX SPIKE SAMPLE:
2597579
92432236001
Spike
MS
MS
%Rec
Parameter
Units
Result
Conc.
Result
%Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
NO
49.5
28.8
58
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
NO
49.5
34.9
71
36-166
2,4,6-Trichlorophenol
ug/L
NO
49.5
45.3J
92
37-144
2,4-Dichlorophenol
ug/L
NO
49.5
37.9
77
39-135
2,4-Dimethylphenol
ug/L
NO
49.5
35.7J
72
32-120
2,4-Dinitrophenol
ug/L
NO
248
NO
0
1-191 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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,�8ce Analytical
www.pacefabs.corn
QUALITY CONTROL DATA
Project: Outfall #1
Pace Project No.: 92432239
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MATRIX SPIKE SAMPLE:
Parameter
2597579
Units
92432236001
Result
Spike
Conc.
MS
Result
MS
%Rec
% Rec
Limits Qualifiers
2,4-Dinitrotoluene
ug/L
ND
49.5
28.3
57
39-139
2,6-Dinitrotoluene
ug/L
ND
49.5
32.2
65
50-158
2-Chloronaphthalene
ug/L
ND
49.5
31.4
63
60-120
2-Chlorophenol
ug/L
ND
49.5
32.2
65
23-134
2-Nitrophenol
ug/L
ND
49.5
17.3J
35
29-182
3,3'-Dichlorobenzidine
ug/L
ND
99
44.1J
45
1-262
4,6-Dinitro-2-melhylphenol
ug/L
ND
99
ND
0
1-181 Mt
4-Bromophenylphenyl ether
ug/L
ND
49.5
37.1
75
53-127
4-Chloro-3-methylphenol
ug/L
ND
99
80.1
81
22-147
4-Chlorophenylphenyl ether
ug/L
ND
49.5
37.5
76
25-158
4-Nitrophenol
ug/L
ND
248
74.5J
30
1-132
Acenaphthene
ug/L
ND
49.5
37.1
75
47-145
Acenaphthylene
ug/L
ND
49.5
36.7
74
33-145
Anthracene
ug/L
ND
49.5
37.7
76
27-133
Benzo(a)anthracene
ug/L
ND
49.5
39.4
80
33-143
Benzo(a)pyrene
ug/L
ND
49.5
39.2
79
17-163
Benzo(b)fluoranthene
ug/L
ND
49.5
39.4
80
24-159
Benzo(g,h J)perylene
ug/L
ND
49.5
37.1
75
1-219
Benzo(k)fluoranthene
ug/L
ND
49.5
39.3
79
11-162
bis(2-Chloroethoxy)methane
ug/L
ND
49.5
35AJ
71
33-184
bis(2-Chloroethyl) ether
ug/L
ND
49.5
36.0
73
12-158
bis(2-Ethylhexyl)phthalate
ug/L
ND
49.5
40.9
83
8-158
Butylbenzylphthalate
ug/L
ND
49.5
41.3
83
1-152
Chrysene
ug/L
ND
49.5
36.8
74
17-168
Di-n-butylphthalate
ug/L
ND
49.5
37.1
75
1-120
Di-n-octylphthalate
ug/L
ND
49.5
39.8
80
4-146
Dibenz(a,h)anthracene
ug/L
ND
49.5
37.3
75
1-227
Diethylphthalate
ug/L
ND
49.5
37.6
76
1-120
Dimethylphthalate
ug/L
ND
49.5
37.8
76
1-120
Fluoranthene
ug/L
ND
49.5
38.8
78
26-137
Fluorene
ug/L
ND
49.5
37.7
76
59-121
Hexachloro-1,3-butadiene
ug/L
ND
49.5
26.6
54
24-120
Hexachlorobenzene
ug/L
ND
49.5
36.1
73
1-152
Hexachlorocyclopentadiene
ug/L
ND
49.5
61
12
25-150 M1
Hexachloroethane
ug/L
ND
49.5
26.4
53
40-120
Indeno(1,2,3-cd)pyrene
ug/L
ND
49.5
38.0
77
1-171
Isophorone
ug/L
ND
49.5
31.7.1
64
21-196
N-Nitroso-di-n-propylamine
ug/L
ND
49.5
35.3
71
1-230
N-Nitrosodimethylamine
ug/L
ND
49.5
21.8J
44
25-150
N-Nitrosodiphenylamine
ug/L
ND
49.5
37.6J
76
25-150
Naphthalene
ug/L
ND
49.5
31.4
63
21-133
Nitrobenzene
ug/L
ND
49.5
35.5
72
35-180
Pentachlorophenol
ug/L
ND
99
24.1J
24
14-176
Phenanthrene
ug/L
ND
49.5
38.0
77
54-120
Phenol
ug/L
ND
49.5
16.7J
34
5-120
Pyrene
ug/L
ND
49.5
40.5
82
52-120
2,4,6-Tribromophenol (S)
%
83
10-137
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 06/19/2019 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 23

,�aceAnalytical
wwwpacelabacpm
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804'
[phone]
Project: Outfall #1
Pace Project No.: 92432239
MATRIX SPIKE SAMPLE:
2597579
92432236001
Spike
MS
MS
% Rao
Parameter
Units
Result
Conc.
Result
%Rec
Limits Qualifiers
2-Flucrobiphenyl (S)
%
69
15-120
2-Fluorcphenol(S)
%
41
10-120
Nitrobenzene-d5 (S)
%
69
10-120 D3
Phenol-d6 (S)
%
28
10-120
Terphenyl-d14 (S)
e/
82
11-131
SAMPLE DUPLICATE: 2597580
92432239001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,2A Trichlorobenzene
ug/L
ND
ND
22-0xybis(1-chloropropane)
ug/L
ND
ND
2,4,6-Trichlorophenol
ug/L
ND
ND
2,4-Dichlorophenol
ug/L
ND
ND
2,4-Dimethylphenol
ug/L
ND
ND
2,4-Dinitrophenol
ug/L
ND
ND
2,4-Dinitrotoluene
ug/L
ND
ND
2,6-Dinitrotoluene
ug/L
ND
ND
2-Chloronaphthalene
ug/L
ND
ND
2-Chlorophenol
ug/L
ND
ND
2-Nitrophenol
ug/L
ND
ND
3,3'-Dichlorobenzidine
ug/L
ND
ND
4,6-Dinitro-2-methylphenol
ug/L
ND
ND
4-Bromophenylphenyl ether
ug/L
ND
ND
4-Chloro-3-methylphenol
ug/L
ND
ND
4-Chlorophenylphenyl ether
ug/L
ND
ND
4-Nitrophenol
ug/L
ND
ND
Acenaphthene
ug/L
ND
ND
Acenaphthylene
ug/L
ND
ND
Anthracene
ug/L
ND
ND
Benzo(a)anthracene
ug/L
ND
ND
Benzo(a)pyrene
ug/L
ND
NO
Senzo(b)fluoranthene
ug/L
ND
ND
Benzo(g,h,i)perylene
ug/L
ND
ND
Benzo(k)Fluoranthene
ug/L
ND
ND
bis(2-Chloroethoxy)methane
ug/L
ND
ND
bis(2-Chloroethyl) ether
ug/L
ND
ND
bis(2-Ethylhexyl)phthalate
ug/L
ND
ND
Butylbenzylphthalate
ug/L
ND
ND
Chrysene
ug/L
ND
ND
Di-n-butylphthalate
ug/L
ND
ND
Di-n-octylphthalate
ug/L
ND
ND
Dibenz(a,h)anthracene
ug/L
ND
ND
Diethylphthalate
ug/L
ND
ND
Dimethylphthalate
ug/L
ND
ND
Fluoranthene
ug/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/19/2019 12:26 PM without the written consent of Pace Analytical Services, LLD. Page 16 of 23

aceAnalytical
www.pacelabs.ccm
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Outfall #1
Pace Project No.: 92432239
SAMPLE DUPLICATE: 2597580
Parameter
Units
92432239001
Result
Dup
Result
Fluorene
ug/L
ND
ND
Hexachloro-1,3-buladiene
ug/L
ND
ND
Hexachlorobenzene
ug/L
ND
ND
Hexachlorocyclopentadiene
ug/L
ND
ND
Hexachloroethane
ug/L
ND
ND
Indeno(1,2,3-cd)pyrene
ug/L
ND
ND
Isophorone
ug/L
ND
ND
N-Nitroso-di-n-propylamine
ug/L
ND
ND
N-Nitrosodimethylamine
ug/L
ND
ND
N-Nitrosodiphenylamine
ug/L
ND
ND
Naphthalene
ug/L
ND
ND
Nitrobenzene
ug/L
ND
ND
Pentachlorophenol
ug/L
ND
ND
Phenanthrene
ug/L
ND
ND
Phenol
ug/L
ND
ND
Pyrene
ug/L
ND
ND
2,4,6-Tribromophenol(S)
%
71
93
2-Fluorobiphenyl (S)
%
76
75
2-Fluorophenol (S)
e/
40
44
Nitrobenzene-d5 (S)
e/
85
83
Phenol-d6 (S)
%
29
32
Terphenyl-d14 (S)
e/
94
88
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
c
REPORT OF LABORATORY ANALYSIS
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Date: 06/19/2019 12:26 PM without the written consent of Pace Analytical Services, L-C. Page 17 of 23

aceAnalytical
wxwpacelabs.cpm
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, "NC 28804`
[phone]
QUALITY CONTROL DATA
Project: Outfall #1
Pace Project No.: 92432239
QC Batch: 480470
Analysis Method: SM
2540D-2011
QC Batch Method: SM 2540D-2011
Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92432239001
METHOD BLANK: 2599455
Matrix:
Water
Associated Lab Samples: 92432239001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
NO
2.5
06/12/19 05:01
LABORATORY CONTROL SAMPLE: 2599456
Spike
LCS
LCS %Rec
Parameter
Units
Conc.
Result
%Rec Limits Qualifiers
Total Suspended Solids
mg/L
250
236
94 90-110
SAMPLE DUPLICATE: 2599457
92432040001
Oup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
1960
2240
13 D6
SAMPLE DUPLICATE: 2599458
92432246002
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
1310
1250
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/19/2019 12:26 PM without the written consent of Pace Analytical Services, L-C. Page 18 of 23

aceAnalytical
/// ,,, rmw.Pacelabs.cnm
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Project: Outfall #1
Pace Project No.: 92432239
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analyles.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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Date: 06/19/2019 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 23

,�ace Analytical
x pecelsbs.=
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Outfall #1
Pace Project No.: 92432239
Lab ID
Sample ID
QC Batch Method
QC Batch
92432239001
Outfall #1
EPA 1664B
480856
92432239001
Outfall #1
EPA 200.7 Rev 4.4 1994
480942
92432239001
Outfall #1
EPA 625.1
480044
92432239001
Outfall #1
EPA 624.1
480087
92432239001
Outfall #1
SM 254OD-2011
480470
Date: 06/19/2019 12:26 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville,`4C 28804'
[phone]
Analytical
Analytical Method Batch
EPA 200.7 Rev 4.4 1994 481076
EPA 625.1 480566
Page 20 of 23

��
,,0aeeAnalXlcal'
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: February 7, 2018
Page I of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ® Eden❑ Greenwood ❑ Huntersville ❑ RRaleigh[:]Mechanicsville❑
Client Name: W tI : 92432239
Pee
r-IPS� I01NC.rr Project : III I����I�I II DI911 Courier: ❑Fed Ex ®UPS ❑LISPS ❑Client
❑Commercial []Pace ❑Other._ 914132:!39
L
Custody Seal Present? ❑Yes [KNo Seals Intact? []Yes Z)No
Date/Initials Person Examining Contents:
Packing Material: []Bubble Wrap Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: ?� []Yes []No JON/A
�-7o�E Type of Ice: ❑Wei ❑blue �Hor.!
�IR Gun ID:� Cooler Temp ('C): �, '7 r�
, o /) correction Factor: Add/Subtract ('C) Temp should be above freezing to 6'C
Cooler Temp Corrected ('C): 10 Samples out of temp criteria. Samples on ice, cooling process
has cegun
USDA Regulated Soil IN NIA, water sample)
Did samples oo�inate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
:...�.a�.� Na.,ai .,nd Puerto Rico)? Ayes ®No
IJYes yNkNo
Comments/Discrepancy:
Chain of Custody Present?
toyes
ONO
❑N/A
1.
Samples Arrived within Hold Time?
Rlyes
❑No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
Dyes
KNO
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
No
❑N/A
4.
Sufficient Volume?
®Yes
ONO
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
R]yes
Yes
ONO
ONO
❑N/A
❑N/A
6.
Containers Intact?
NYLS
Elmo
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
ONO
ONIA
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matsu:
Elves
�y/
ONO
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
Oyes
❑Yes
E]No
t�]No
4NO
❑N/A
❑N/A
❑Id/A
10.
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
� A,-
Person contacted: .I�� rn u ll'(f,,G"\_
Date/Time: _
Project Manager SCURF Review:
Project Manager SRF Review: !'
Field Data Required? ❑Yes'J1 No
Date:
Date:
Page 21 of 23

`�
Document Name:
Document Revised: February 7, 1018
/
�r
.-7C 1111ajf/ical
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality Office
'Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project !LIQ# • 924322:39
RI: UP Due Date: 06/19/19
CLIENT: 93-PEERLESS
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Aldo Onl of Preservative
added
Lot p
Plate: Whenever t here is a discrepancy affecting Nort It Carolina compliance samples, a copy of this.forin will to sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out Of temp, incorrect containers.
Page 22 of 23

/ce��jat CHAIN -OF -CUSTODY I Analytical Request Document
The Chain-of-Cuslody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information: Page : I Of i
Company: MMC-Peerless Blowers lRit,ron To: Don Wallin Attention: — �' p.r
'
Address: 172 South Andrews Av.. Copy To: Co." Name: ' /y2
Hot Spr1;77i
Address:
Re Mato A .hC .
/3
Email: r ,
Pace Quata: NC
Phone: ! Fax 4 fr- C,ZZ- Z
Project Name: Pocrless Slormwater
Pace Project Manager. [e-mail].
:' t"'' "I State 1 Location
'iRequesled Due Dale:
Project 9.
Pace Pratte P. ODDD
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Envira„mental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/
n p des -storm water-gps
Permit No.: N_IC,G/o/ 3/0110
0�1D,dl or Certificate of Coverage No.:
Facility Name: /%%4, GB,
County: 11
Inspector:
Date of Inspection: I-/- _
Phone No. 02t A%2 750�
Time of Inspection:
/
Total Event Precipitation (inches): rSi�7i
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the pennittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Pertnittee or Designee)
1. Outfall Description:
Outfall No. _�_ Structure (pipe, ditch, etc.)
Receiving Stream: /
Describe the
that occur
area:
SwU-242, Last modified 06/01/2018
Page I of 2

2. Color: Describe the color of the
(light, medium, dark) as descriptors: _
using basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct
chlorine odor, etc.):
that the discharge may have (i.e., smells strongly of oil, weak
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 3 4 5
6. Suspended Solids: Choose the number which -best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
7
8.
9.
61 2 3 4 5
Is there any foam in the stormwater discharge? o Yes O"No.
Is there an oil sheen in the stormwater discharge? OYes 1 0. _
Is there evidence of erosion or deposition at the outfall? 16 1 Yes O No.
10. Other Obvious Indicators oAf/Stormwater Pollution:
List and describe AI'M °, ©ds-
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S W U-242, Last mod if ed 06/01 /2018

t
fnVirmunenla}
Quatiry
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/
npde s-stormwater-gps
Permit No.: N_ICI, 6l ©13/1�1 or Certificate of Coverage No
/�/i
Facility Name: A� (I /J �/( � . �%.
County: //(ll /�17 �% Phone No. 74
Inspector: //%
Date of Inspection: /q "
Time of Inspection:
— / /
Total Event Precipitation (inches): /
N/C/G/tJ/�'/LI,1/3/7 /
—iii —
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event' is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. -,?— Structure (pipe, ditch, etc.):
Receiving Stream:
Describe the industrial activiti s th t occ r
r
Page 1 of 2
SWU 242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
3. Odor: Describe any distinct
chlorine odor, etc.):
that the discharge may have (Le., smells strongly of oil, weak
4. Clarity: Choose the number which best describes the clarity of the discharge, where l is clear
and 5 is very cloudy:
1 2 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where I is no solids and 5 is the surface covered with floating solids:
V 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
7.
8.
9..
10.
1 C 3 4 5
Is there any foam in the stormwater discharge? O Yes &� N�o.
Is there an oil sheen in the stormwater discharge? OYes 4No.
Is there evidence of erosion or deposition at the outfall? a Yes O No.
Other Obvious Indicators of Stormwater Pollution:
List and describe
Wi 'L' I
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/depositoni may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018

Semi-annual Stormwater Dis,arge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted jS- /,9 -/S-'
CERTIFICATE OF COVERAGE NO. N0003 o L Y 0
FACILITY NAME ��c //rsS H/�i✓c/S /irla dfon mr4so
COUNTY /%%/J� Sn�/
PERSON COLLECTING SAMPLES ��r✓/L /S
LABORATORY ®A!t Awe [riTi i Lab Cert. # °f0
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR C� OAK
SAMPLE PERIOD an -June ❑ July -Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW []Trout❑PNA
�I VD ❑Zero -flow ❑Water Supply []SAf ❑Other
AUG.16 Z018
CENTRAL FILLtFASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
DWR SECTION
❑ No discharge this period:
Outfall No.
Date.sample
i
Collected
(mo/dd/yr)
24-hour rainfall
amount;:
Inches':
-
Total Suspended Solids
PH. `
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
' 1
Total Toxic
Organics s
Benchmarks =__>
100 mg/Cor 50 mg/L°
6.0 — 9.0
0.007 mg/L .
. 0.033 mg/L
0.067 mg/L
15 mg/L
l mg/L I ;;
D
—
a s�7
-3
a
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmarK exceeaance for the same parameter aL uie same ouuau.
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
"See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Datt ./1/2012-10/31/2017 SWU-245, last revised 10 `/.2012 .
Page 1 of 3

Facilities tV- incorporate a solvent management plan into the Stormwater Pol an Prevention Plan may so certify, and the requirement forTTO mt _ oring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
=W,n ��
Name (Print name)
Title (Print title)
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L". where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. see General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
El No discharge this period?2 '
Outfall No.
Date Sample
i
Collected
(mo/dd/yr)
24-hour rainfall
amount,
3
Inches- ,..�
Non -polar 0&G/TPH by
EPA 1664 (SGT-HEM)
TotaLSuspended Solids
pH
Benchmarks =__>
15 mg/L ..
100 mg/L or50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
r
Permit Date:11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you art a sample value in excess of the benchmark, you must impler t Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
. A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION
. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER ATANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE OWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center.
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:to
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed ,
or
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
Permit Datt [1/2012-10/31/2017
as/.-y//
(Date)
SWU-245, last revised 10'-- -12012
Page 3 of 3

aceAnalytical
.pecalabs,=
August 13, 2018
Mr. Tim Banks
Madison Mfg. Co.
172 S. Andrews St.
Hot Springs, NC 28743
RE: Project: Stormwater-07/31/2018
Pace Project No.: 92393903
Dear Mr, Banks:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on July 31, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
cc: Randy Reynolds, Madison Mfg. Co.
Emily Ricker, Madison Mfg
��Q pcCRpaT�
TlJI
`9eORAt��
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

Pace Analytical Services, LLC
laceAnalj6calo
2225 Riverside Dr.
Asheville, NC 28804
wxrvpacelabs.cnm
[phone]
CERTIFICATIONS
Project: Sto"water-07/31/2018
Pace Project No.: 92393903
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florda/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
Vrginia/VELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 13

1�5ace Analytical e
1 wxwPacelabs'=
1
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
Stormwater-07/31/2018
92393903
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92393903001
0UTFALL#1
EPA 1664B
JMS
1
PASI-C
EPA 200.7 Rev 4.4 1994
DS
1
PASI-A
SM 2540D-2011
CEH
1
PASI-A
SM 4500-H+B-2011
RLO
1
PASI-A
92393903002
OUTFALL #2
EPA 1664B
JMS
1
PASI-C
EPA 200.7 Rev 4.4 1994
DS
1
PASI-A
SM 254OD-2011
CEH
1
PASI-A
SM 4500-H+B-2011
PLO
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 13

aceAnalytical e
wwwpecelab5.mm
ANALYTICAL RESULTS
Project: Stormwater-07/31/2018
Pace Project No.: 92393903
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: OUTFALL #1 Lab ID: 92393903001 Collected: 07/31/18 14:45 Received: 07/31/18 16:47 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
200.7 MET ICP
Lead
2540D Total Suspended Solids
Total Suspended Solids
4500H+ pH, Electrometric
pH at 25 Degrees C
Analytical Method: EPA 1664E
NO mg/L
4.8 1
08/13/18 04:22
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
NO ug/L
5.0 1
08/01/1802:40 08/06/1819:14 7439-92-1
Analytical Method: SM 254OD-2011
9.7 mg/L
5.2 1
08/02/18 00:03
Analytical Method: SM 4500-H+B-2011
6.7 Sid. Units
1.0 1
08/01/1807:47 H6
Sample: OUTFALL#2 Lab ID: 92393903002 Collected: 07/31/1814:55 Received: 07/31/1816:47 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mg/L
4.8 1
08/13/18 04:23
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Lead
ND ug/L
5.0 1
08/01/1802:40 08/06/1819:17 7439-92-1
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
25.7 mg/L
5.3 1
08/02/18 00:03
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
pH at 25 Degrees C
7.8 Std. Units
1.0 1
08/01/18 07:54 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 08/13/2018 12:28 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 13

0
aceAnalytical
w pacslabs.cnm
Project: Stormwate r-07/31 /2018
Pace Project No.: 92393903
OC Batch: 424552
OC Batch Method: EPA 1664B
Associated Lab Samples: 92393903001, 92393903002
METHOD BLANK: 2348252
Associated Lab Samples: 92393903001, 92393903002
Parameter Units
Oil and Grease mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 4.8 08/13/18 04:20
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville. NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
2348253
Spike
LCS
LCS
a/ Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
38.5
37.3
97
78-114
MATRIX SPIKE SAMPLE:
2348254
92394053001 Spike
MS
MS
e/ Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
NO 38.5
37.3
97
78-114
Results presented on this page are In the units Indicated by the "Units' column except where an alternate on It Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08113/2018 12:28 PM without the written consent of Pace Analytical Services, L-C.
Page 5 of 13

6
aceAnalytical
wnwpacelabs.lxun
QUALITY CONTROL DATA
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Stonnwater-07/31/2018
Pace Project No.: 92393903
OC Batch: 422234 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92393903001, 92393903002
METHOD BLANK: 2337239 Matrix: Water
Associated Lab Samples: 92393903001, 92393903002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Lead ug/L NO 5.0 08/06/1818:15
LABORATORY CONTROL SAMPLE: 2337240
Spike LCS LCS %Rec
Parameter Units Conc. Result e/ Rec Limits Qualifiers
Lead ug/L 500 458 92 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2337241 2337242
MS MSD
92393756002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result p/ Rec % Rec Limits RPD Oust
Lead ug/L ND 500 500 456 459 91 92 70-130 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/13/2018 12:28 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13

0
aceAnalytical
.pacisaba.cum
QUALITY CONTROL DATA
Project: Stormwater-07/31/2018
Pace Project No.: 92393903
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
OC Balch: 422525
Analysis
Method:
SM 254OD-2011
QC Batch Method: SM 2540D-2011
Analysis
Description:
2540D Total Suspended Solids
Associated Lab Samples: 92393903001, 92393903002
METHOD BLANK: 2338735 Matrix: Water
Associated Lab Samples: 92393903001, 92393903002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L NO 2.5 08/01/18 23:58
LABORATORY CONTROL SAMPLE: 2338736
Spike
LCS LCS
e/ Rec
Parameter
Units
Conc.
Result e/ Rec
Limits Qualifiers
Total Suspended Solids
mg/L
250
238 95
90-110
SAMPLE DUPLICATE: 2338737
92393916001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L TO 7.0 1
SAMPLE DUPLICATE: 2338738
92393878001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 17.0 17.4 2
Results presented on this page are in the units indicated by the "units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/13/2018 12:28 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 13

0
aceAnalytical
w pacalabs.cnm
QUALITY CONTROL DATA
Project: Stormwa te r-07/31/201 8
Pace Project No.: 92393903
QC Batch: 422256 Analysis Method: SM 4500-H+B-2011
QC Balch Method: SM 4500-H+B-2011 Analysis Description: 450011+13 pH
Associated Lab Samples: 92393903001, 92393903002
SAMPLE DUPLICATE: 2337290
92393903002 Cup
Parameter Units Result Result RED Qualifiers
pH at 25 Degrees C Sid. Units 7.8 7.8 0 H6
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08113/2018 12:28 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 13

ace Analytical
' wuwpaceWds.com
QUALIFIERS
Project: Stonnwater-07/31/2018
Pace Project No.: 92393903
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MOIL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte ie
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260,
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/13/2018 12:28 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

ace Analytical e
' wwwpacela6s.cnm
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Stormwater-07/31/2018
Pace Project No.: 92393903
Lab ID Sample ID QC Batch Method QC Batch
92393903001
OUTFALL #1
EPA 1664B
424552
92393903002
OUTFALL #2
EPA 1664B
424552
92393903001
OUTFALL #1
EPA 200.7 Rev 4.4 1994
422234
92393903002
OUTFALL #2
EPA 200.7 Rev 4.4 1994
422234
92393903001
OUTFALL #1
SM 254OD-2011
422525
92393903002
OUTFALL #2
SM 2540D-2011
422525
92393903001
OUTFALL #1
SM 4500-H+B-2011
422256
92393903002
OUTFALL #2
SM 4500-H+B-2011
422256
Date: 08/13/2018 12:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, -LC.
Pace Analytical Services, LLD
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Analytical
Analytical Method Batch
EPA 200.7 Rev 4.4 1994 422264
EPA 200.7 Rev 4.4 1994 422264
Page 10 of 13

Document Name: Document Revised: February 7, 2018
I Sample Condition Upon Receipt(SCUR) Page 1 of 2
iii"'aeeAnalyUCal Document No.: Issuing Authority:
(/ F-CAR-CS-033. Rev nA Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville,f Eden❑ Greenwood❑ Huntersville❑ Raleigh❑ Mechanicsville❑
IRMOClient Name: Project p: f WO# : 92393903
4s'o^ HiJ
Courier: ❑Fed Ex ❑UPS OUSPS -]Client II IIIB II I II i I I I ICI i 6II
❑ Commercial ❑Pace ❑Other:_ 92393903
Custody Seal Present? ❑Yes _2m-o�Seals Intact? ❑Yes ❑Dlor" I3
Date/Initials Person Exinw1g)Jon ends:
Packing Material: (]Bubble Wrap U861oble Bags []None ❑ other Biological Tissue Frozen?
Thermometer: �- (y E� (]Yes [-]No [�]�A
t/ Type of lee: .Wet []Blue[]None❑IR Gun ID: �7
Cooler Temp (°C): !. /.• , Correction Factor: Add/Subtract (°C)
Temp should be above freezing to 6'C
Cooler Temp Corrected (•C): _�_ „ {]5-am-ples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil ( water sample)
Did samples originate I a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samcr—ona. nn
p Ies originatefrom a foreign F source (internationally,
-..._::_ YN
VYes LJNO
...-.__,.
Comm cots/Discrepancy:
Chain of Custody Present?
2res
[]NO
❑N/A
1.
Samples Arrived within Hold Time?
YC
❑No
EINIA
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
[ Ira
❑N/A
3.
Rush Turn Around Time Requested?
❑,
IN/A
�Jo
❑
4.
Sufficient Volume?
Eyees
--,.ct,es
FIND
N/A
5.
Correct Containers Used?
-Pace Containers Used?
Ely s_
'J_✓]Yea
❑❑No
N
(-]N/A
rUA
[-]N/A
6.
Containers Intact?
Elye,
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
lam
❑el/A
A.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>5-6mm)?
Yes
• " r
❑Yes
❑No
❑No
❑N/A
AN/A
9.
10,
Trip Blank Present?
Trip Blank Custody SealS Present?
❑Yes
[]Yes
❑No
❑No
I]N/A
I
rN/A
11.
COMMENTS/SAMPLE DISCREPANCY ' Field Data Required? []Yes ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: Date:
�
Project Manager SRF Review: �/ Date: 7/ t / L
l/
Page 11 of 13

Document Name:
Document Revised: February 7, 2018
r
/.
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
aceAnalytica!
F-CAR-CS-033-Rev.06
Pace Carolinas Ouality Office
*Check marls top half of box if pH and/or dechlorination is
venrtea ano witnm me acceptance range ror presetvaoun
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Projecttt W0#_:__923_9_3_903 _.._.......,
PM: CD1 Due Date: 08/14/18
CLIENT: 93-Madisonl1f
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added
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Note: Whenever t here is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Ccrtumeomi Office (i.e.
Out of hold, Incorrect preservative, out of temp, incorrect containers.
Page 12 of 13

0//
/ FaceAnal(Xical`
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CHAIN -OF -CUSTODY I Analytical Request Document m
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant lields most be completed accurately. o
m
Section A Section B Section C
Page: m
of � D.
Required Client Information: Required Project Information'. Invoice Information'.
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PEERLESS
B L O W E R S
Madison Manufacturing Company
www.peerlessblowers.com
172 S. Andrews Avenue • PO Box 187 • Hot Springs, NC 28743 • [phone]
August 13, 2018
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Dear Sir or Madam:
Please find the enclosed analysis for a recent storm water event. We have two outfalls. One
flows into Spring Creek and the other into the French Broad River. The duration of this event
was .2" of rainfall over a 1/2-hour period.
Both outfalls are from roof and parking lot drains. We have no manufacturing or storage activity
outside.
Regards,
Tim Banks
Engineering / Quality Manager
Peerless Blowers / Madison Mfg. Co.
Enclosure:

r
PEERLESS
B L O W E R S
Madison Manufacturing Company
www.peeriessblowers.com
172 S. Andrews Avenue • PO Box 187 • Hot Springs, NC 28743 • [phone]
January 14, 2017
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Dear Sir or Madam:
Please find the enclosed analysis for a recent storm water event. We have two outfalls. One
flows into Spring Creek and the other into the French Broad River. The duration of this event
was .5" of rainfall over a 2-hour period.
Both outfalls are from roof and parking lot drains. We have no manufacturing or storage activity
outside.
Regards,
Tim Banks
Engineering / Quality Manager
Peerless Blowers / Madison Mfg. Co.
Enclosure:

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted -.g . r q 201 k,
CERTIFICATE OF C VERAGE No. NCG030 SAMPLE COLLECTION YEAR 2O
FACILITY NAMEA¢w /e5$ 3/01Jers �,?�c�, 0XV� CMS • CO - SAMPLE PERIOD ❑ Jan -June July -Dec
COUNTY sp rJ or ❑ Monthly' (month)
PERSON COLLEC G SAMPLES % ¢4 no %c�i5 RECEIVED
ECEf V DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA
LABORATORY c 144, c L b Cert. # � ❑Zero -flow ❑Water Supply ❑SA
Comments on sample collection or analysis: FEB i ❑Other
CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
DWR SECTION
Part A: Stormwater Benchmarks and Monitoring Results
No discharge this period?2
Outfall No.
Date Sample
24-hour rainfall'
- - ` -
Total Suspended Solids
pH,"
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
�i
Total Toxic'
.c 0
Collected
amount,
Standard unrts
Organics
M
(mo/dd/yr)
3
Inches
.Hydrocarbons
=__>
d00 m /Cor30 m /L
g g
6.0 — 9.0
0.007,m /L
g ..
'0.033 m /L
B
0.067 m /L
g
15 m /L
g
1 m /L
MgIL
j
!I
Monthly sampling (instead of semi-annual) must begin with the second consecutivebenchmark exceedance for the same parameter at the same outtaii.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. !
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in.the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; forsemiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit DatL /1/2012-10/31/2017
^. SWU-245, last revised 10`,/2012
Page 1 of 3
t

Facilities thy' incorporate a solvent management plan into the Stormwater Pol _ an Prevention Plan may so certify, and the requirement for TTO m, 'oring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification.statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
xy, � 7�/4S
Name (Print name) -
�JGd.J�itiG G�ua�r' /37a/�2
Title (Print title)
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
n No rlisrhnrnp thic nprinrl Pz
Outfall No.
_
Date Sample ''
Collected'
,,.:.(mo/dd/yr)_ .
24-hour rainfall
amount -
a
, -"Inches ..�.,.-EPA
-
Non -polar O&G/TPH by
1664(SGT-HEM)
-
Total .. Suspended - •Solids -
-
'
pH„ ..
Benchmarks =__>
15 mg/L.
300 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

WNote.
f you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ N04
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
(Date)
Permit Dati �1/2012-10/31/2017 SWU-245, last revised 1C '2012
Page 3 of 3

aceAnalytkal
wwwCaorlabscom
f
January 04, 2018
Buster Johnson
Madison Mfg. Co.
172 S. Andrews St.
Hot Springs, NC 28743
RE: Project: STORMWATER 12/20
Pace Project No.: 92367816
Dear Buster Johnson:
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 20, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Endosures
cc: Don Wallen, Madison Mfg
""'CC
l
AeORA1�P
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical services, LLC.
Page 1 of 13

Pace Analytical Services, LLC
0
aceAnalytical
2225 Riverside Dr.
Asheville, NC 28804
w pacelabs.com
[phone]
CERTIFICATIONS
Project: STORMWATER 12I20
Pace Project No.: 92367816
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
LouisianalNELAP Certification # LA170028
FloridalNELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
UrginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
FlondalNELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
UrginiaNELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, LLC. Page 2 of 13

aceAnalytical e
wawpemlabs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
STORMWATER 12/20
92367816 _
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92367816001
0UTFALL#1
EPA 1664B
JMS
1
PASI-C
EPA 200.7
SER
1
PASI-A
SM 2540D
SLB
1
PASI-A
SM 4500-H+B
ECH
1
PASI-A
92367816002
OUTFALL#2
EPA1664B
JMS
1
PASI-C
EPA 200.7
SER
1
PASI-A
SM 2540D
SLB
1
PASI-A
SM 4500-H+B
ECH
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 13

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ANALYTICAL'RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER 12/20
Pace Project No.: 92367816
Sample: OUTFALL #1
Lab ID: 92367816001 Collected: 12/20/17 09:20
Received:
12/20/17 17:45 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg/L 5.0 1
01/04/18 04:48
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead
ND ug/L 5.0 1
01/02/1811:30 01/0311822:18 7439-92-1
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND mg/L 2.5 1
12/26/17 13:13
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B
PH at 25 Degrees C
5.9 Sid. Units 1.0 1
12/21/17 12:00 H6
Sample: OUTFALL #2
Lab ID: 92367816002 Collected: 12/20/17 09:50
Received:
12/20/17 17:45 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg/L
5.0 1
01/04/18 04:48
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation
Method: EPA 200.7
Lead
ND ug/L
5.0 1 01/0211811:30
01103/1822:21 7439-92-1
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
90.0 mg/L
12.5 1
12/26/17 13:13
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
6.9 Std. Units
1.0 1
12/21/17 12:00 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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�';Zne'Analyficalo
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I
QUALITY CONTROL DATA
Project: STORMWATER 12/20
Pace Project No.: 92367816
QC Batch: 393144 Analysis Method: EPA 1664B
OC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92367816001, 92367816002
METHOD BLANK: 2180136 Matnx: Water
Associated Lab Samples: 92367816001, 92367816002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease ri ND 5.0 01/04/18 04:47
Pace Analytical Services, LLC
2225 Riverside D,
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
2180137
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 38.8
97
78-114
MATRIX SPIKE SAMPLE:
2180138
92367818003 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
%Rec
Limits Qualifiers
Oil and Grease
mglL
ND 40
39.6
98
78-114
Results presented on this page are In the units indicated by Me "Units" column except where an alternate unit is presented to the right of Me result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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I
QUALITY CONTROL DATA
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: STORMWATER 12/20
Pace Project No.: 92367816
OC Batch: 392646
Analysis Method: EPA 200.7
OC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 92367816001, 92367816002
METHOD BLANK: 2177819
Matrix: Water
Associated Lab Samples: 92367816001, 92367816002
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Lead ug/L
ND 5.0
01/03/1821:39
LABORATORY CONTROL SAMPLE: 2177820
Spike
LCS
LCS %Rec
Parameter Units
Cone.
Result
e/ Rec Limits
Qualifiers
Lead ug/L
500
466
93 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2177821
2177822
MS
MSD
92367767001
Spike
Spike MS
MSD MS
MSD
p/ Rec
Parameter Units Result
Cone.
Cone. Result
Result p/ Rec
% Rec
Limits
RPD Qual
Lead ug/L ND
500
500 445
443 89
89
70-130
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2177823
2177824
MS
MSD
92367818003
Spike
Spike MS
MSD MS
MSD
%Rec
Parameter Units Result
Cone.
Conc. Result
Result %Rec
%Rec
Limits
RPD Qual
Lead ug/L ND
500
500 460
465 92
93
70-130
1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate un It is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/04/2018 01:18 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 13

aceAnalytical
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QUALITY CONTROL DATA
Project: STORMWATER 12/20
Pace Project No.: 92367816
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QC Batch: 392263
Analysis
Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis
Description:
2540D Total Suspended Solids
Associated Lab Samples: 92367816001, 92367816002
METHOD BLANK: 2176234 Matrix: Water
Associated Lab Samples: 92367816001, 92367816002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL ND 2.5 12/26/17 13:10
LABORATORY CONTROL SAMPLE: 2176235
Spike LCS 1-CS % Rec
Parameter Units Conc. Result e/ Rec Limits Qualifiers
Total Suspended Solids mg/L 250 254 102 90-110
SAMPLE DUPLICATE: 2176236
92367785003 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 10.2 9.8 4
SAMPLE DUPLICATE: 2176237
92367813001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 13000 7400 55 D6
Results presented on this page are in the units indicated by the -Units- column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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I
QUALITY CONTROL DATA
Project: STORMWATER 12/20
Pace Project No.: 92367816
OC Batch: 391943 Analysis Method: SM 4500-H+B
QC Batch Method: SM 4500-H+B Analysis Description: 4500H+B pH
Associated Lab Samples: 92367816001, 92367816002
SAMPLE DUPLICATE: 2174391
92367587001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.5 6.5 0 H6
SAMPLE DUPLICATE: 2174481
92367816001 Cup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Sid. Units 5.9 6.0 2 H6
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/0412018 01:18 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 '

ace Analytical
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I
QUALIFIERS
Project: STORMWATER 12/20
Pace Project No.: 92367816
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
POL- Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyle is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
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Date: 01/04/2018 01:18 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

aceAnalytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: STORMWATER 12/20
Pace Project No.: 92367816
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92367816001
OUTFALL #1
EPA 1664E
393144
92367816002
OUTFALL#2
EPA 16648
393144
92367816001
OUTFALL#1
EPA 200.7
392646 EPA 200.7
92367816002
OUTFALL#2
EPA 200.7
392646 EPA 200.7
92367816001
OUTFALL #1
SM 2540D
392263
92367816002
OUTFALL#2
SM 2540D
392263
92367816001
OUTFALL#1
SM 4500-H+B
391943
92367816002
OUTFALL#2
SM 4500-H+B
391943
Date: 01/04/2018 01:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
392735
392735
Page 10 of 13

Name:
2017
Pace
Laboratory receiving same es:
Asheville ❑ Edeh❑ Greenwood ❑ Huntersville ❑ Raleigh❑
Mechanicsville❑
mom Client Name: nn Wo# : 92367616
MG1CI iSu1 Project II�II� II I I III'I�� I� II�
Courier: [:]Fed Ex ❑UPS ❑USPS, ❑H ent
❑ commercial ❑Pace ❑Other:— 92367816'
Custody. Seal Present? Dyes []gals Intact? ❑Yes. ❑No
Date/initials Person Examining Contents:
Packing Material: []Bubble Wrap ❑Bubble Bags None El Other Biological Tissue Frozfn?
Thermometer. r []Yes ❑No ❑N/A
r, ❑ID: �Z� Wet []Blue El Type of Ice:
Correction Factor: Cooler Temp Corrected ('C): ,a - U Temp should be above freezing to WC
❑Samples out of temp criteria. Samples an ice, cooling process
has begun
USDA Regulated Soil N/A; water sample)
Did samples originate n a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (international)�/
....a o..e..,, a;.,,n nya, nNo/
oyes- uNo
............. _.
Comments /Discrepancy:
Chain of Custody Present?
Yes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
❑ s
❑No
N/A
_2.
Short Hold Time Analysis(<72hr.)?
[]Yes
No
N/A
3.,
RushTurn Around Time Requested?
❑Yes
0.o"
❑N/A
4.
SO fficie nt Volu m e?
ods'
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
[]No
El No
[]N/A
❑N/A
6.
Containers Intact?
EfYes
[]NO
N/
7. _
Dissolved analysis: Samples Field Filtered?
❑Yes
No
N/A
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
Headspacein VOA Vials (>5-6mm)7
Trip Blank Present? -
Trip Blank Custody Seals Present?
❑es
QYes
❑Yes
❑Yes
❑No
[]NO
❑No
❑No
❑N/A
C `
❑ /A
©N(
- N/A
9.
If.
e
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample Discrepancy:
Project Manager SCURF Review:
Project. Manager SRF Reviews
Date/Time:
Date:
Date:
a
Note: Whenever there Is'a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEH NR Certification Office (i.e.
.Out of hold, incorrect preservative, out of temp, ncorrect containers)
Page 11 of 13

Document Name:
Condition Upon Rec
Document No.:
F-CAR-(
i *Check mark top half of box if pH and/or dechlorination
j is verified and within the acceptance range for
rpreservation samples.
**Bottom half of box is to list number of bottles
Document Revised: July 25, 2017
rt(SCUR) Page 2 of 2
Issuing Authority:
Pace Dualilie Offire
Project WO# : 92367�1�i.
PM: COI Due Date: 01/O5/18
CLIENT: 93-Madisonhf
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pH.Adjustment Log for Preserved Samples
SamplelD
Type of Preservative
pH uponrecelpt
Date preservation adjusted
Time preservation
adjusted
.Amount of. Preservative
added
Lot
Page 12 of 13

I,?
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CHAIN -OF -CUSTODY/ Analytical Request Document
The Ctiaimof-Ctistody is'a LEGAL DOCUMENT, Ail rdldvanl fields must bo completed accurately.
Section A .Section B Section C
Page. of
Required Client Information; Required Project lareac atlon. Invoice Information:
Dam :my , Repad Ta: j AN , /. b/Np'G3 Attention ,
21,80235
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Alai
Cany To: r/�„-6n-rsa
Company Maine;
REGULATORY. AGENCY
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Address:
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NPDES it GROUNDWATER r DRINKING WATER
UST f - RCRA THEIR tr'-- n�'
Email To:
Purchase Order No: D n
Pam Quare
Rmnranua:
Phone:
Fax:
Project Noma:
Pao Project
�
Sito Location
I
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-1_1
MTnngnri
'S' TATE:
(
Requested Due DatcITAT:'
Project Number:
Pow Pmrae a:
Regliested Analysis
Filtered (YIN) -
Section D Matrix codas
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Roeul.edcbem mkarnmen MATRIX I C005
-
COLLECTED
Preservatives
->
.i.. .
Drinking Water DW Minding
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Waste Water WW
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Sample IDs MUST BE UNIQUE Tissue TS
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_.ADDITIONAL COMMENTS,'
RELINQUISHED BY I AFFILIATION
DATE
,TIME.
ACCEPTED BY I AFFILIATION.
DATE,
TIME
SAMPLE CONDITIONS
m
Jr ORIGINAL
SAMPLER NAME -AND SIGNATURE
PRINT Nomad SAMPLER:
,
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4
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SIGNATURE of SAMPLER:.
GATE Signed _
w
MMIODIYY)i , O -.to
u+
'tmgnnva Ndo: By nitrate, Ill loan you are accepting Pace s NET se day WMnaut burls and a9mai, t0 Uto charges of 15n par month far onoa Kvr noKd mr in oo dop, F-ALL-0-020rev.07. , 5-May-2007

Semi-annual Stormwater &harize Monitoring; Report
for North Carolina Division of Water Quality General Permit No. NCG030000
r - Date submitted OSl 3 [ / / (p
iez
CERTIFICATE -OF COVERAGE NO. NCG03 0 -3 7 Q
FACILITY NAME
COUNTY 'J
PERSON COLLECT4 NG SAMPLES
LABORATORYA,,'%i./. -1-ec Lab Cent. # t{ O
Comments on sample collect. ion or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION R __ZO/ �
SAMPLE PERIOD Jan -June ❑ July -Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
[]Zero -flow ❑Water Supply []SA
RECEIVED ❑Other
JUN 0 2 2016 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
CENTRAL FILES
OWR SECTION / N ���
o,disch /n arge this period.
Outfall No.
-
Date Sample
Collected r
(mo/dd/yr)
24hourrainfall`
amount,
- Inches3.
-
Total Suspended Solids
' .' :z_
pH,
Standard untts
{�
'=A '•
Copper
\�rr
: \ l�
r
Lead
Zinc
-
Non-PolarO&G/
T
> Tota�Petroleum
Hydr co arbons
,. Air, r,
Total Tax ici
Organics 9;i
�k
J1
;h
Benchmarks =__�
-
' 400 mg/L or 50 ing/L
- 6 0 - 9.0
0.007,mg/L
-'0.033.mg/L '
0.067 mg/L
�15 r9pr
1 mg/L
I'll
II
I'
fl
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
"See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Dat /1/2012-10/31/2017^ ,SWU-245, last revised 10i/2012
Page 1 of 3

Facilities t,k -' Incorporate a solvent management plan into the Stormwater Pol )n Prevention Plan may so certify, and the requirement for TTO m(--Noring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
'JU,SLC'/ TOAr\6
Name (Print name)
0. r. MCI n05CK
Title (Prin title)
�
(Signature) U (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX me/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
kr
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
d ❑ No discharge this period?Z
t
Outfall No.
. ....
"bate $ample'
Collected'
.. (mo/dd/yr) -
".24-hour rainfall
amount,
a
.._; Inches,__ ; ;-
Non -polar 0&G/TPH.tfy
• EPA 1664 (SGT-HEM)
Total. Suspended Solids,.
- _: , _ _
-
t pH, -
Benchmarks =__>`
-
''- - -
- _ .15 mg/L ..:
100 mg/L or SO ri
6.0 — 9.0 SU
Footnotes firm Part A also apply to this Part B
* 5ee General Pli mit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit DR' ll/1/2012-10/31/2017 - SWU-245, last revised 1� "5/2012
Page 2 of 3

Note: If • report a sample value in excess of the benchmark, you must im tent Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
y
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 UCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQCentral Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of
5, 3 , I
(Date)
Permit Date /1/2012-10/31/2017 SWU-245, lastrevised 10'—,/2012
Page 3 of 3

w
.'\�
��
I L � ���

PEERLESS
BLOWERS
MADISON MANUFACTURING COMPANY
172 South Andrews Ave, Hot Springs, NC 28743, [phone]
May 31, 2016
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Dear Sir or Madam:
30 3 9U
RECEIVED
JUN
CENTRAL FILES
DWR SECTION
Please find the enclosed analysis for a recent storm water event. We have two outfalls. One
flows into Spring Creek and the other into the French Broad River. The duration of this event
was .5" of rainfall over a 1.5-hour period.
Both outfalls are from roof and parking lot drains. We have no manufacturing or storage
activity outside.
Regards,
Buster Johnson
Quality Control / Safety Director
Madison Mfg. Co.
Enclosure:

` aceArnalytical
tw Pacelabs.corn
1
May 27, 2016
Buster Johnson,
Madison Mfg. Co.
172 S. Andrews St.
Hot Springs, NC 28743
RE: Project: Stormwater 5/11
Pace Project No.: 92297139
Dear Buster Johnson:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 11, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
/t -,;:�
Chris Derouen
[e-mail]
Project Manager
Enclosures
cc: Don Wallen, Madison Mfg
pCCRf0
REPORT OF LABORATORY ANALYSIS
. te, This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Ag�R_p.1pQ
Page 1 of 19

1
aceAnalytical
wmvpacelabs.com
Project: Slormwater 5111
Pace Project No.: 92297139
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VrginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 19

aceAnalytical e
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
2225 Riverside D,
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
Stonnwater 5/11
92297139
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92297139001
Outfall #1
EPA 200.7
CDF
1
PASI-A
SM 2540D
MSH
1
PASI-A
SM 4500-H+g
MLS
1
PASI-A
92297139002
Outfall#2
EPA 200.7
CDF
1
PASI-A
SM 2540D
MSH
1
PASI-A
SM 4500-H+g
MLS
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 19

ace Analytical
' x wpacdabs.ovn
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Stormwater 5111
Pace Project No.: 92297139
Sample: Outfall #1 Lab ID: 92297139001 Collected: 05/11/16 09:20 Received: 05/11116 13:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead ND ug/L 5.0 1 05/1211619:00 05/1811603:38 7439-92-1
2540D Total Suspended Solids Analytical Method: SM 25400
Total Suspended Solids 3.6 mg/L 25 1 05/11/16 22:01
4500H+ pH, Electrometric Analytical Method: SM 4500-H+B
pH at 25 Degrees C 6.0 Std. Units 1.0 1 05/16/16 12:42 H6
Sample: Outfall #2 Lab ID: 92297139002 Collected: 05/11/16 09:50 Received: 05111/16 13:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead 7.5 ug/1- 5.0 1 05/12/16 19:00 05/18/16 03:50 7439-92-1
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 86.5 mg/1- 9.1 1 05/11/16 22:01
4500H+ pH, Electrometric Analytical Method: SM 4500-H+B
pH at 25 Degrees C 6.9 Sid. Units 1.0 1 05/16/16 12:42 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 05/27/2016 11:15 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 19

aceAnalytical
wuwpacela0.s.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Stormwater 5111
Pace Project No.: 92297139
QC Batch: MPRP/21696
Analysis Method: EPA200.7
QC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 92297139001, 92297139002
METHOD BLANK: 1731993
Matrix: Water
Associated Lab Samples: 92297139001, 92297139002
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Lead ug/L
ND 5.0
05/18/16 02:58
LABORATORY CONTROL SAMPLE: 1731994
Spike
1-CS
1-CS p/ Rec
Parameter Units
Conc.
Result
% Rec Limits Qualifers
Lead ug/L
500
477
95 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1731995
1731996
MS
MSD
92297115001
Spike
Spike MS
MSD MS MSD
p/ Rec
Parameter Units Result
Conc.
Conc. Result
Result %Rec %Rec
Limits
RED Qua]
Lead ug/L ND
500
500 474
469 95 94
70-130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1731997
1731998
MS
MSD
92297193001
Spike
Spike MS
MSD MS MSD
%Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec p/ Rec
Limits
RED Qua[
Lead ug/L ND
500
500 448
446 89 89
70-130
0
Results presented on this page are in the units indicated by the 'Units' column except where an alternate unit Is presented to the right of me result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 05/27/2016 11:15 AM without the written consent of Pace Analytical Services, Inc..
Page 5 of 19

Pace Analytical Services, Inc.
2225 Riverside Dr.
5aeeAnalj6cal Asheville, NC 28804
/ wwrpecelabs.com [phone]
QUALITY CONTROL DATA
Project: Storrnwaler 5111
Pace Project No.: 92297139
QC Balch: WET/44857
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92297139001, 92297139002
METHOD BLANK: 1731605
Matrix:
Water
Associated Lab Samples: 92297139001, 92297139002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
NO
0.25 05/11/16 22:00
LABORATORY CONTROL SAMPLE:
1731606
Spike
LCS
LCS % Rec
Parameter
Units
Conic.
Result
%Rec Limits Qualifiers
Total Suspended Solids
mg/L
250
248
99 90-110
SAMPLE DUPLICATE: 1731607
92297095001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
244
222 9 D6
SAMPLE DUPLICATE: 1731608
92297146001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
6A
NO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2016 11:15 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 19

aceA'nalytical
' wwwpacelabs.cpm
QUALITY CONTROL DATA
Project: Stormwater 5111
Pace Project No.: 92297139
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QC Batch: WET144940
Analysis
Method:
SM 4500-H+B
QC Balch Method: SM 4500-H+B
Analysis
Description:
4500H+B pH
Associated Lab Samples: 92297139001, 92297139002
SAMPLE DUPLICATE: 1734338
92297432001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.7 D6,H6
Results presented on this page are In the units Indicated by the'UnIM' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2016 11:15 AM without the written consent of Pace Analytical Services, Inc..
Page 7 of 19

ace Analytical
(/ w»wpaceJaGcmn
I
QUALIFIERS
Project: Stormwater 5/11
Pace Project No.: 92297139
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUE - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 05/27/2016 11:15 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 19

ace Analytical
mrwpacelaGCcom
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Stonnwater 5/11
Pace Project No.: 92297139
Pace Analytical Services, Inc.
2225 Riverside D,
Asheville, NC 28804
[phone]
Analytical
Lab ID
Sample ID
OC Batch Method
QC Batch
Analytical Method
Batch
92297139001
Outfall #1
EPA 200.7
MPRP/21696
EPA 200.7
ICP/19473
92297139002
Outfall #2
EPA 200.7
MPRP/21696
EPA 200.7
ICP/19473
92297139001
Outfall #1
SM 2540D
WET/44857
92297139002
Outfall #2
SM 2540D
WET/44857
92297139001
Outfall #1
SM 4500-H+B
WET/44940
92297139002
Outfall #2
SM 4500-H+B
WET/44940
Date: 05/27/2016 11:15 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 19

Document Name:
Document Revised: IBFE82016
j it"'dCBHI7dly[ICdIc
Sample Condition Upon Receipt (SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
f
F-CHR-CS-003-rev.18
Pace Huntersville Quality Office
P r • • Client Name:
qAnn �.t //1f Project III:
/ ltf / C6
Courier: ❑Fed Ex U S ❑USJ� Client
❑ Commercial ❑Pace ❑Other:_
Custody Seal Present? ❑Yes LV o Seals Intact? ❑Yes ❑No
Date/Initials Person Examining Contents:'S.r, �<il1J ly
Packing Material: Bubble Wrap []Bubble Bags toNone ❑Other:
er. ThermometGun H55Ni 15527199 ❑ Type of Ice: et ❑Blue ❑None
Correction. Factor: 0VC Cooler Temp Corrected('C): t9'o
Temp should be above free g to 6°C
USDA. Regulated Soil ( N/A, water sample)
Did samples originate in a quarantine zone within the. United States: CA, NY, or SC (check maps)?
❑yes ❑NO
Palle 2 of 2 for Internal Use ONLY
WO#:92297139
92297139
❑Samples on ice, cooling process has b n
Biological Tissue Frozen? Dyes ❑No ❑ /A
Did samples originate from a foreign source (inte�rnan�aliy,.
including Hawaii and Puerto Rico)? ❑Yes (/jNo.
COMMENTS:
Chain of. Custody Present?
2<s
❑No
❑N/A
1.
Chain of Custody Filled Out?
s
❑ o
❑N/A
2. N ht lg NISI` dta!
Chain of Custody Relinquished?
Cj<es
ON.
❑N/A
3.
Sampler Name and/or Signature on COC?
. es e
ONO
❑N/A
4.
Samples Arrived within Hold Time?
D7es
❑No
❑N/A
5.
Short Hold Time Analysis (<72 hr)?
Oyes
o
❑N/A
6..
Rush Turn Around Time Requested?.
❑Yes
a
❑N/A
7.
Sufficient Volume?
es
❑No
❑N/A
B.
Correct Containers Used?
-Pace Containers Use
es
es
ON.
ONO
❑N/A
❑N/A
9.
Containers Intact?
CJYirs
ON.
❑N/A
10.
Filtered Volume Received for Dissolved Tests?
❑Ye❑Na
N/A
11: Note if sediment is visible in the dissolved container
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix: (Al
Yes
ONO
El NIA
12:
All containers needing acid/base preservation have been
checked?
All containers needing preservation are found to be in
compliance with EPA recommendation?
(HNO., H:SOs, HCI<2;: NaOH>9 Sulf!ge Na9H>12 Cyanide)
Exceptions: VOA, Coliform, TOC; Oil and Greas
DRO/8015 (water) DOC,LLHg
�
mn'
es'
Ves
ONO
❑No
❑No.
❑N/A
❑N/A
❑N1/
13.
Samples checked for dechiorination
[-]Yes
❑ a
D hw
14..
Headspace 16VOA Vials (>5-6mm)?
❑Yes
No
❑ A
15.
Trip Blank Present?
Trip Blank Custody Seals Present?
Pace Trip,Blank Lot 4 (if purchased):
❑Yes
❑Yes
ONO
ONO
N(p
CNN/A
16.
CLIENT NOTIFICATION/RESOLUTION
Person. Contacted:
Comments/Resolution:
Project Manager SCURF Review:
Oate%Time:
Date:
Field Data Required? ❑Yes- ONO
Project Manager SRF.Review: /f Date: _
Note: Wheneverthere is a discrepancy affecting North Caro ina compliance samples, a copy of this form will be sent to the'Nor
Out of hold, incorrect preservative, out of. temp, incorrect containers)
Page 10 of 19

o r " CHAIN -OF -CUSTODY 1 Analytical Request Document
/ �aCeA�%al �Ca�, The Chaimol-Custody is a LEGAL DOCU MENT. All relevant fields must be completed accurately, o�
O
Page: / / of
m
Section A Seclion.8, Section C
s'l N
205528L a
Ro a ed Client Information: Required Project Information- Invoice Information:
9 1
Company. ..
ftoPod Tqb / / :7is
/�Y` ,yy"Y�v✓ %%.-,
Atlenbon:.r-'""
U'�..-
Access'
/'2,1.5. iJr1P✓"r.:3 .CJv`�.
CopyTo
Coy Name'
i.J G@:
REGULATORY,AGENCY -
fi
Add ess'
/
I NPOES I'- GROUND WATER ;" DRINKING WATER.
j UST �.. 'RCRA
Elinil
h?cih. Ott "v Y�/ii_'d rJrsS %Ci.m`d CQ!
Purchase ONer Nc.' ! ) //�
I"7.i GJj /[ ( W
R o .o
Roluoi c.
Pon^
Sill
Fax:
Project Name' /
Pna,piaat
hmeaq...
Site LoWtion
-STATE:
Requested Due DatOTAT:
Project Number:
r PMilu ^:
,Requested
Analysis
Filtered.(YIN)'
Section Matrlx Codes
Reoulr,acrew lmamu ma MATAIx"PcoDF
-
COLLECTED
Presemativas
`-
Drinking Water DW
g
o
U
z
O
Water WT
Waite water 'ww
$
0"
m
-
caNiusliti
courrosne
I'.M1a
Z
Proe P
STf,Ri
FNI)K
w
SolUSolid 'SL
SAMPLE ID Oil OL
d
=
o
w
Wipe WP.
(A"Z. 0.91.--) Ar. AR
"TS
O
.,
¢
Gm
N.
Sample IN MUST BE UNIOUE Tissue
y
z'2
N
Other OT
T.ATETI.e
T�FTI.E/(
1-16
w
r
<
zS
O
S
Z
Z
2
O
�'.
2
Pace Piaject Nod Lab'I.E.
[''
_J
0
102
2
3,
%✓�i.. [.4_ _.�.
l'T
/ /
i!lIA
I:^'Z.Rm
2
!
_
4
S
6
7
B
9
10
11
12
ADDITIONALCOMMENTS
RELINQUISHED BY I AFFILIATION
DATE
TIME..
ACCEPTEDDY/AFFILIATION.
DATE,
TIME
SAMPLE CONDITIONS
444
-
zz
L . C
}
ORIGINAL
SAMPLER NAME AND SIGNATURE
U
PRINT Name of SAMPLER,
��%
SIGNATURE of SAMPLER."t`ii".v.M1._
DATE
IMMIDDIYYIsigned
i, v��: reN my see de..I rig.,a-l"t-,l once NCl Jdwyt Y o-0, 1 F-ALL-C-020rev.07,16-May-200,7

antes
Accurate. Timely. Responsive. Innovative.
4810 Executive Park Court,. Suite 111
Jacksonville FL, 32216.6069
Phone: '904'296.3007 FAX: [phone]
Thursday, May 26, 2016
Pace Analytical (PA007)
Attn: Chris Derouen
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
RE: Laboratory Results for
Project Number: Stormwater 5/11, -Project Name/Desc: 92297139
ENCO Workorder(s): BZ02178 -
Dear Chris Derouen,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, May.19, 2016.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply onlyto'the samples as. submitted.
The analytical results contained in this report are in compliance with NELAC.standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory:
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Jacksonville.
Data from outside organizations will'be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
r
1—
Chris Tompkins
Project Manager
Enclosure(s)
FINAL mis report relates only to ti.a sample as receiveal by the laWtviery. aml may only M mwW,,,a l in Nil. Page I of e
Page 12 of 19

PROJECT NARRATIVE
Client: Pace. Analytical (PA007)
Project: 92297139
ENCO Project ID: BZ02178
Overview
All samples submitted were analyzed by Environmental Conservation Laboratories, Inc. in accordance with the
methods referenced in the laboratory report, Any particular difficulties encountered during sample: handling and
processing will be discussed in the Remarks section below.
Remarks
Analysis: EPA 1664A, EPA 1664B '
Affected Samples: Outfall # l[BZ02178-01], Outfall #2[BZ02178-02]
The method blank associated to the flagged samples showed a positive result above the MDL, but below the
reporting limit.. Since the magnitude of the sample result are within a factor of 10 of the associated blank.
Chris,Tompkins.
Project Manager
FlNAL Tna report relates only to tN Sample as redea:e,] by the kWretory, aM may onh to reproduce,] in hdl, Page 2 of 8
Page 13 of 19

SAMPLE SUMMARY/ LABORATORY CHRONICLE
❑Imit LD. Dutftll#1 Lab ID: OZO2178-01 -Sampled: 05/1111609:20 Received: 05/14/1610:30 1
Parameter Hold Date/Time(s) Pmo Date/Timefs) Anafy5i5 Date/Timefs)
EPA 1664E 06/08/16 05/22/16 14:43 05/22/16 15:39
Client ID;t Outfall 92 Lab to: SZ02178-02 Sampled:-05/I1/I6 09:50 Received: 05/19/16 10:30
Panameter Hold Date/Time(sl Pre, Date/Timefsl Analysis Date/Time(s)
EPA 1664E 06/08/16 05/22116' '14:43 05/22/16 15:39
FIND Th, repOn rela%, Only to tM sample as wenctl by the bb hAM, and! may OMy t a iepn,ducad in full, page 3 of 8
Page 14 of 19

(_%
SAMPLE DETECTION SUMMARY
Analrte
BravllF Elag
MPl
EQL
units
Method notes
Oil & Grease (HEM)
0.615 JB
0.615
1.28
mg/L
EPA 1664E )-01
Clleul IU: Oullall C2
lab ID:
8202178-02
AaaLft
Resullt Mae
.MBL
E91
unit4
Method Notes
Oil & Grease (HEM)
1.34 8
O.617
1.29
mg/l.
EPA 1664E 3-01
FINAL
This retort relates only to the sample as reCoivN by the Wbom:ory, and may orJy be mI rodvcN At fill. Page 4 010
Page 15 of 19

ANALYTICAL RESULTS
Description: Outfall #1
Lab Sample IDi BZ02178-01
Matrix: Water
Sampled: 05/11/1609:Z0'
Project: 92297139
Sampled By:
Classical Chemistry Parameters
Analrte MAS Numbed Resuf
an
Sl01ts
Pf MP6E"
Balch Method
Oil &Grease(HEM)[C-0007]A 0.615
A
M91L
0.256 0.615 1.28
6E24003 EPA 16648
Description: Outfall #2
Lab Sample ID:BZ02178:02
Matrix: Water
Sampled: 05/11/16.09:50
Project: 92297139
Sampled By:
Classical Chemistry Parameters
^ -EALD Vrka #r ce fie an ze(AC 4I2/
Anaivte rCASNumberl Results
fin
YAM
PE MPS P9S
Batch :Malhttd
011& Grease (HEM)[C-00071^ 1.34
8
mg/L
0.257 0.617 1.29
6E24003 EPA.1661B
FltJa TNs report relates 0Ny to trN SamDk as received W the la0 mtm, and may ady De reproduced ID U.
Received: 05/19/16 10:30
Work Order: BZ02178
Analyze A Bk Notes
05/2211615:39 SMA 3-01
Received: 05/19/16 10:30
Work Order: BZ02178
60aln BY Notes
OS/Z2/1615:39 561A 1.01
Page 5 Of 8
Page 16 of 19

� N
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 6E24003 - EPA 16648
Blank (6E24003-BLR3) Prepared: 05/22/2016 14:43 Analyzed: 05/22/2016 15:39
Spike Source %REC RPD
AnaNNP.0 Result ,Flab POI. units Level Result °]DREG Limits RPD Lim) Notes
Oil a Grease(HEM) 0.924 3 1.28 uV/L
LCS (6E34003-BSI) Prepared: 0512212016 14:43 Analyzed: 05/22/2016 15:39
Spike Source °k REC RPD
Analyte Result Rao 'P-DL Units Level Result, 41. R E C Limits RPD Lima .Notes
Oil B Grease (HEM) 146 :.B 5.00 M/L 153 95 78-114
LCS Dup (6E24003-BSDI) Prepared: 0512212016 14:43 Analyzed: 05/22/2016 15:39
Spike
Source
%REC
RPD.
Analme
Result
Flao
P9L
U11M
Level
Resull
%REC
Llmita RPD
LIMA Notes
Oil h Grease (HEM)
164
B
5.00
ing/L
152.
108
78-114 12
18
Matrix Spike (6E24003-14SI)
Prepared: 051221201614:43 Malyzed: 05/22/201615:39
Source: SZ02180.01
-Spike
Source
%REC
RPD
Analide
Result
.Daft
PQL
Units
Level
Result
'/REC
Limits RPD
L)m3 Notes
Oil & Grease (HEM)
35.4�
B
1.29
mg/L
41.4
19.1
39
78-114
QM-07
HNd1 n" report relates Doty to the sample as received W tde L14,atw, an] may Orly be repmducM in full. Page 6 of a
Page 17 of 19

FLAGS/NOTES AND DEFINITIONS
8 The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where. applicable.
E The concentration .indicated for this analyte is an estimated value above the calibration range of the
instrument. -This value is considered an estimate.
MRL Method ReportingLimit.' The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples; moisture content:
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a'tentative identificador '.
Greater than 25% concentration difference was observed. between the primary and secondary GC column.
The lower concentration is reported.
3-01 Result may be biased high due to positive results in theassociated method blank.
QM-07 The spike recovery was outsideacceptancelimits for the Ms and/or MSD. The batch was
accepted based on acceptable LCS recovery.
FINAL This report relates o y m tl+e Sample as received by tM 1aW story, RW may only be reorod"W m hii. Page J of 8
Page 18 of 19

0
Chain of Custody
Workordcr: 92297139 Workorder Name: Stormwater 5/11
r-Pke Analytical
Results Requested By: 5/25/2016
' Report 1. Invoice To - - Subcontr.ct To
Requested Analys"r.
Chris Oervu_n
Pane Analyucat Charlotte RO).�. AVOW l �
980p Ki�ce/Ave. Suite 100
I luntersnlln NC. 2807E
Phone [phone] �'�J�
Email: chest phi cdaroueii@pac:elabs.cum '
v
Slate of Sample Origin: EOEN Pmserved Containers.
collect
a
'.Itcm
Sam i�' to
P
D'vtcrTime -
Cab'm'
tfaUiz
I Va USE ONLY
1--
o' i0 ui
0/112016 09:20
'92297139001
Water
x
2
OW31192.__-
5111201609:50
92297139002
Waler
x
a
_
..
Common's'
Transfers
Released By
Dateffme
Rec ripd By
Diterrme
�
1
"� L..IN
' '
1.
r
a
Cooler Temperature on Receipt .j. 1 . °C ' 'Custod Seal Y for N Received on Ice Y or N Samples InWc Y or N I
0

Semi-annual Stormwater charge Monitoring Report
for North Carolina Division of Water Qualit General Permit No. NCG030000
Date submitted � 'c a2
CERTIFICATE OF COVERAGE NO. NCG.00300 3
FACILITY NAME
COUNTY i
PERSON COL IJECTING SAMPLES
LABORATORY cc 4 Lab Cert. li Y
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR�—
SAMPLE PERIOD ❑ Jan -June my -Dec
or ❑ Monthly' (month)
RECD S IIARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
�D ❑Zero -flow ❑Water Supply [_]SA
OCT 29 2014 ❑other
CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3
DWR SECTIpN
❑ No discharge this period?'
Outfall No.
Date Sample
Collected '
(mo/dd/yr)
24-hour rainfall
amount,
- Inches'.
"-
Total Suspended Solids
�
- = a ". ..
pH,
Standard units
_
Copper
-
Lead
Zinc
_
Non -Polarb&G/
Total Petroleum
Hydrocarbons
... ..
I ..
Total Toxic
Organics s�
Benchmarks =__>
300 mg/L or 50 mg/L°
6.0 — 9.0
0.007 mg/L
0.033 mg/L
0.067 mg/L
15 mg/L
1 mg/L ('h
ICU
io i .
„
3" L
6.4
/J,
N
I'I
6.7
it
I!
{I
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
a For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
° See General Permit, Table 3 identifying the especially sensitive; eceiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Dat(/ /1/2012-10/31/2017 SWU-245, last revised 10^ ,(2012
Page 1 of 3

Facilities tl-" incorporate a solvent management plan into the Stormwater Pol ")n Prevention Plan may so certify, and the requirement for TTO mi mooring
may be waned. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the !
solvent management plan included in the Stormwater Pollution Prevention Plan." I
Name (Print name)
Title (Print title)
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L. _
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?Z
Outfall No.
._.
"Date.Sample
Collected'
(mo/dd/yr)..._
'=-24-hour rainfall •,
amount,
a
_.....,Inches._.. ..-
'
Non -polar 0&G/TPH by
•'EPA 1664 (SGT-HEM)-
Total Suspended Solids
--"., ,
- =s PH: ,..
Benchmarks ===>
15 mg/L „'
100,mg/L or SO mg/L*
6.0 - 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
S - <
Permit Dar 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If report a sample value in excess of the benchmark, you must it went Tier 1, Tier 1, or Tier 3 responses. See General Permit text
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are
(Signature of Permittee)
Permit Data /1/2012-10/31/2017
nalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
(Date)
SWU-245, last revised 10'—,2012
Page 3 of 3

IS09001
likxc o
•1J85
E E Rgyp{ E C C E aL e/'y Tp/'y ♦ Ii
MADISON MANUFACTURING COMPANY
An Amnam of Pootless- w+namlm, loa One Madison Avenue
Post Office Box 187
Hot Springs, NC 28743-0187
828/622-7500 • Fax [phone]
October 24, 2014
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Dear Sir or Madam:
Please find the enclosed analysis for a recent storm water event. We have two outfalls. One
flows into Spring Creek and the other into the French Broad River. The duration of this event
was .3" of rainfall over a 2-hour period.
Both outfalls are from roof and parking lot drains. We have no manufacturing or storage activity
outside.
Regards,
Patricia Sams
General Manager
Madison Mfg. Co.
Enclosure:

/ aceAnalyfical
w pacelabs.=
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
October 23, 2014
Ms. Patricia Sams
Madison Mfg. Co.
172 S. Andrews St.
Hot Springs, NC 28743
RE: Project: Stormwatert 10/14
Pace Project No.: 92221473
Dear Ms. Sams:
Enclosed are the analytical results for sample(s) received by the laboratory on October 15, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
cc: Martha Wigglesworth, Madison Mfg
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 13

aceAnalytical
-w vpacelabs.cnm
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Stormwatert 10114
Pace Project No.: 92221473
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification M 12
South Carolina Certification M 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
J
CERTIFICATIONS
Florida/NELAP Certification M E87627
Kentucky UST Certification M 84
West Virginia Certification M 357
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 13

aceAnalytical
w Pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project: Stormwatert 10/14
Pace Project No.: 92221473
Lab ID Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92221473001 001 OUTFALL # 1
EPA 1664E
CLW
1
PASI-C
EPA 200.7
JMW
1
PASI-A
SM 2540D
WRC
1
PASI-A
SM 4500-H+B
MAB
1
PASI-A
92221473002 002 OUTFALL # 2
EPA 1664B
CLW
1
PASI-C
EPA 200.7
JMW
1
PASI-A
SM 2540D
WRC
1
PASI-A
SM 4500-H+B
MAB
1
PASI-A
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 13

aceAnalytical
w pacelabs.00n
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Stormwatert 10/14
Pace Project No.: 92221473
Sample: 001 OUTFALL # 1
Lab ID: 92221473001 Collected: 10/14/14 16:20
Received:
10/15/14 12:02 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mg/L 5.0 1
10/16/14 12:24
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead
ND ug/L 5.0 1
10/22/14 15:05 10/22/14 21:45 7439-92-1
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
4.0 mg/L 3.1 1
10/15/14 22,33
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
6.6 Std. Units 1.0 1
10/20/14 14:50 H6
Sample: 002 0UTFALL # 2
Lab ID: 92221473002 Collected: 10/14/14 15:20
Received:
10/15/14 12:02 Matrix: Water
Parameters
Results Units Report Limit OF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg/L
5.0 1
10/16/14 12:25
_,%.7 MET ICP
Analytical Method: EPA 200.7 Preparation
Method: EPA 200.7
Lead
ND ug/L
5.0 1 10/15/14 20:30
10/17/14 14:54 7439-92-1
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND mg/L
2.8 1
10/15/14 22:33
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
6.7 Std. Units
1.0 1
10/20/14 14:50 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/23/2014 03:43 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 13

aceAnalyiical
w .pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Slormwatert 10/14
Pace Project No.: 92221473
QC Batch: GCSV/19200
Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E
Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92221473001, 92221473002
METHOD BLANK: 1308348
Matrix: Water
Associated Lab Samples: 92221473001, 92221473002
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Oil and Grease mg/L
ND 5.0 10/16/14 12:17
LABORATORY CONTROL SAMPLE: 1308349
Spike LCS LCS % Rec
Parameter Units
Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L
40 34.6 86 78-114
MATRIX SPIKE SAMPLE: 1308350
92221354001 Spike MS MS %Rec
Parameter Units
Result Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L
1
NO 40 36.5 91 78-114
Results presented on this page are in the
units indicated by the 'Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/23/2014 03:43 PM
without the written consent of Pace Analytical Services, Inc.. Page 5 of 13

aceAnalyticalo
awvpacela0.s.can
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project:
Stormwatert 10/14
Pace Project No.:
92221473
QC Batch:
MPRP/17136 Analysis Method: EPA 200.7
QC Batch Method:
EPA 2007.Analysis Description: 200.7 MET
Associated Lab Samples:
92221473002
METHOD BLANK: 1308114
Associated Lab Samples: 92221473002
Parameter Units
ug/L
Lead
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 10/17/1413:51
LABORATORY CONTROL SAMPLE: 1308115
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Lead ug/L 500 472 94 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1308116 1308117
MS MSD
92221391003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result %Rec e/ Rec Limits RPD Qual
,ad ug/L ND 500 500 471 472 93 94 70-130 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1308118 1308119
MS MSD
92221548002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec e/ Rec Limits RPD Qual
Lead ug/L ND 500 500 450 450 89 89 70-130 0
Results presented on this page are in the units indicated by the -Units- column except where an alternate unit is presented to the right of the result.
Date: 10/23/2014 03:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 13

aceAnalytical�
wmypacelabs.00m
Pace Analytical services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Stormwatert 10114
Pace Project No.: 92221473
QC Batch: MPRP/17176 Analysis Method: EPA 200.7
QC Batch Method: EPA200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92221473001
METHOD BLANK: 1312562
Associated Lab Samples: 92221473001
Parameter Units
Lead ug/L
LABORATORY CONTROL SAMPLE: 1312563
Parameter Units
Lead ug/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 10/22/14 21:03
Spike LCS LCS e/ Rec
Conc. Result % Rec Limits Qualifiers
500 475 95 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1312564 1312565
MS MSD
92220772001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
iad ug/L 0.026 500 500 437 450 82 85 70-130 3
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1312566 1312567
MS MSD
92222286001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result % Rec e/ Rec Limits RPD Qual
Lead ug/L ND 500 500 574 710 73 100 70-130 21 R1
1 Results presented on this page are in the units indicated by the NtJmts' column except where an alternate unit is presented to the right of the result.
Date: 10/23/2014 03:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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ace Analytical
wwwpecelabs.com
Pace Analytical services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Stormwatert 10/14
Pace Project No.: 92221473
OC Batch: WET/33761
Analysis Method: SM 2540D
QC Batch Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92221473001, 92221473002
METHOD BLANK: 1308143
Matrix: Water
Associated Lab Samples: 92221473001, 92221473002
Blank Reporting
Parameter
Units Result Limit Analyzed Qualifiers
Total Suspended Solids
mg/L ND 2.5 10/15/14 22:29
LABORATORY CONTROL SAMPLE:
1308144
Spike LCS LCS % Rec
Parameter
Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids
mg/L 250 256 102 90-110
SAMPLE DUPLICATE: 1308145
92221391001 Dup
Parameter
Units Result Result RPD Qualifiers
Total Suspended Solids
mg/L ND ND
Results presented on this page are in the units indicated by the -Units- column except where an alternate unit is presented to the right of the result.
j
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/23/2014 03:43 PM
without the written consent of Pace Analytical Services, Inc.. Page 8 of 13

/�aceAnalytical-
wwwpacelabs.com
Pace Analytical services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
,l
Project: Stormwatert 10/14
Pace Project No.: 92221473
QUALITY CONTROL DATA
QC Batch: WET/33830
Analysis
Method:
SM 4500-H+B
QC Batch Method: SM 4500-H+B
Analysis
Description:
4500H+B pH
Associated Lab Samples: 92221473001, 92221473002
SAMPLE DUPLICATE: 1310694
Parameter
pH at 25 Degrees C
92221473002 Dup
Units Result Result
Std. Units 6.7 6.6
RPD Qualifiers
0 H6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 10/23/2014 03:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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aceAnalyticalo
mvvpacalabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Project: Stormwalert 10/14
Pace Project No.: 92221473
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCSO) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Services - Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
J
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 10/23/2014 03:43 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 13

Pace Analytical Services, Inc.
�1 ,,
u 2225 Riverside Dr.
acemalytical Asheville, NC 28804
w .pacelabs.com [phone]
QUALITY
CONTROL DATA CROSS
REFERENCE TABLE
Project:
Storrin atert 10/14
Pace Project No.:
92221473
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92221473001
001 OUTFALL # 1
EPA 1664E
GCSV/19200
92221473002
002 OUTFALL # 2
EPA 1664E
GCSW19200
92221473001
001 OUTFALL #1
EPA 200.7
MPRP/17176
EPA 200.7
ICP/15486
92221473002
002 OUTFALL # 2
EPA 200.7
MPRP/17136
EPA 200.7
ICP/15445
92221473001
001 OUTFALL # 1
SM 2540D
WET133761
92221473002
002 OUTFALL # 2
SM 2540D
WET/33761
92221473001
001 OUTFALL # 1
SM 4500-H+B
WET/33830
92221473002
002 OUTFALL # 2
SM 4500-H+B
WET/33830
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 10/23/2014 03:43 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 13

�. �aceAnalytical'
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CHAIN-OF-CUSTODYJAnalytical Request Document
The Chain -of -Custody is a, LEGAL _DOCUMENT. All relevant fields must be completed accurately.
0
N
:Secton A Section B. 'Section C
Pago: of ( M
Roquiretl Clontlnformefiom, Required Nofecr lnfonnoon: Invoke lnlormaeon:
7' r-s' ? 1Z
1787772
Company: ;-. ... .'. .. .'.
RepDM1 T -
Attentlon:
Address: - -
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LopyTo: -
Company Nama:
REGULATORY AGENCY
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Address: A
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-' NPDES. :GROUNDWATER . - DRINKING WATER
', _�
I� UST, '� RCRA OTHER.
Email To: ,.
Purchase Order No.:..
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Prone:
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Requested Duo Dald/TAT:: .`
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Section D
RaoeliadG Ont Nlcim$tbn. �u . '. MATRIX / CODE
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- COLLECTED
Preservatives
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� DATE
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' ADDITIONAL COMMENTS-• `'
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RELINQUISHED BY/AFFILIATION 5
t' OATE-„
TIME,
,'ACCEPTED BV/AFFILIATION
DATE
".TIME
'SAMPLE CONDITIONS
SAMPLER NAME AND SIGNATURE'
ORIGINAL PRINT Name of SAMPLER:. �� /�5
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Sined
• _ SIGNATURE of SAMPLER�'�r i! 'DATE 9
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Document Name: Sample Condltion Upon
Document Revised: June 10, 2014
���✓y
aC2AllalytlCHl
Receipt (SCUR), a
f'a e 1 of 2
Document No.;-` ;' r;
; •Issuing'Authorities.
• ^w r
r.-ASV-C$ 003.revA
Pace;Asheville Quality Office
OF Client Name:'
Courler'(Circle): Fed Ex UPS USPS t E '- :Comn
Custody Seal on Cooled Box Present: yes, no Seals it
Packing -Materiah'El Bubble Wrap; Bubble Bags .❑ :None?Q
Thermometer Used IR Gun#3 130265963 Type'of Ice Me
IR; n SN:140290365 Other.- c _
To Correction Fator.= Add / Subtract - C
s�
cial 'Pace Other
i '
lct f El yes Qj-no
Nher
ilue� None Samples on Ice; cooling process has begun
i 1
Corrected Cooier Temp.:. _ / ��5 C-
at Tissue is;Frozen Yes Nc `rvm
,'+ Date and Initlat ofp ,.son examining..,
Tempshould be above freezing to,WC C I
�+
a-
Comments:
contents:
Chalm.of Custody Present l
Yes' No
❑NIA
1:
Chain of Custody Filled Out:
e No
OwA
2.
Chain of Custody Relinquished:
Yes fio'
11WA
3
Sampler Name & Signature on COC::
es` No
13 NIA
4.'.
Samples Arrived within'Hoid?inie:
es' 13W
ONIA
5.i
Short Hold Time Analysis;(<72hr):
Ore:�� - No
wA.
6.; -'• ? ' -
Rush,TurnAround7ime.Requested:
❑LYs--VNd
❑N/A
7-.'.
Sufficient Volume:
�Ye No'
❑wA
8.'_
Correct Containers Used:
ve No,
❑N/A
g.:
face Containers Used:
Ye No
❑wA
Containers Intact::
Yes:ONO
❑N/
- 0
M red.v6lume received'forDissolved tests _
we No
N)A
11:
Sample Labels'match COCi
Yes ONO
ON/A
12;
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.. -
--
Yes No
-.ON/A
13.
All containers needing preservation are found to be in
es. Oiuo
❑N/A
compliance with EPA recommendation.
exceptions: VOA colilorm; TOC, O&G vn-DRO (walerj
Samples checked for dechlorination:
Yes' ONo
❑NIA
14: ... ...-, -
HeadspaceldVOA Vials.(>6mm):
❑ves,ON.
041A15.
Trip Blank Present:
❑Yes CINO
ZNM
16.
Trip Blank Custody Seals,Present
❑Yes ❑No
;"NIA
-
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution:
Person Contacted: DateMme:
Comments/ Resolution:
iCURF Review: Dater iB i'
SRF Review: Date: -(6 16 �`/
Note: Whenever there is a discrepancy affecting North Carolina
compliance samples;.a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( i e out of hold, incorrect
preservative, out of temp, incorrect containers)
Field Data Required? Y / N
Page 13 of 13
_ I

1
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted /O LI VIltz
CERTIFICATE OF COVERAGE NO. NCG030 3 _5
FACILITY NAME /%7,4O) SOS! W
COUNTY /ne7zySO/lI
PERSON COLLECTING SAMPLES
LABORATORY Lab Cert. #
Comments on sample collection or analysis: 1-1
Part A: Stormwater Benchmarks and Monitoring Results
J3
SAMPLE COLLECTION Y O/
SAMPLE PERIOD an -June ❑ Ju y-Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
[:]Other
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
No discharge this period?Z
Outfall No.
'
Date Sample
i
Collected
(mo/dd/yr)
24-hour rainfall'
amount,
Inches3
': - `
Total Suspended Solids
PH,, `
Standard units
• '
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
-, Hydrocarbons
.
Total Toxic
Organics s�
c
p
I,p
6
Benchmarks =__>
100 mg/L or 50 m_ g/L
6 0 - 9.0
0.007 mg/L
0.033 mg/L `
0.067 mg/L
15 mg/L
1 mg/L
I(�
�I
PTE
' Monthly sampling (instead of semi-annual) must begin with the second consecutivebenchmark exceedance fordh,g sari biraLat3ter at the same outtaii.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring repo4 w1tTa�Jy ckmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be el ft r a waivir of the rain gauge requirement.
" See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the mo�'�ftb�(j�e,9chmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacAgemiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Dat�./1/2012-10/31/2017 ^ SWU-245, last revised 10`+/2012
Page 1 of 3

Facilities tk"- incorporate a solvent management plan into the Stormwater Po )n Prevention Plan may so certify, and the requirement for TTO mi mooring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included i - ater Pollution Prevention P n."
Name (Print name)
t title)
; G r r iI L
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format "<XX me/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
n Nn rlicrhnrno thic nPrinrl ?2
Outfall No
.... _. ........
Date Sample
Collected'
(mo/dd/Yr).,..
24 hour rainfall
amount
3
-. _Inches ... ....
Non polar Ci&G/TPH by
.jEPA 1664(SGT-HEM)..'
Total Suspended Solids-
..a e,..,....
;_.
_ pH,_ _
..
Benchmarks715
fng/L100
mg/L or 50 mg/L*"
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B'
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date:11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 2 of 3

Note If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQCentral Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penal ies for submitting false information, including the possibility of fi es and imprisonment for knowing violations."
(Signature of Permittee) , (Date)
Permit Date /1/2012-10/31/2017 SWU-245, last revised 10 "{2012
Page 3 of 3