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HomeMy WebLinkAboutNCG030296_COMPLETE FILE - HISTORICAL_20161031STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. DOC TYPE 217HISTORICAL FILE ❑ MONITORING REPORTS DOC DATE ❑ a0/ (P I Q 3 } YYYYM M DD aceAnalyifcal amrpa:ahbsnm October 21, 2016 Robert Simpson Parker Hannifin Corporation 101 Canterbury Rd. Kings Mountain, NC 28086 RE: Project: STORMWATER Pace Project No.: 92315897 RLCEIVED OCT 31 2016 CENTRAL FILES DWR SECTION Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntemille. NC 28078 (704)875-9092 Dear Robert Simpson: Enclosed are the analytical results for sample(s) received by the laboratory on October 13, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, c qyl `$cu oni Angela Baioni angela.baioni@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 19 1 2ceAnalyfical' rnrwpaxhbanm CERTIFICATIONS Project: STORMWATER Pace Project No.: 92315897 Pace Analytical Services, LLC 98001Gncey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 North Carolina Drinking Water Certification #: 37706 Florida/NELAP Certification #: E87627 North Carolina Field Services Certification #: 5342 Kentucky UST Certification #: 84 North Carolina Wastewater Certification #: 12 VirginialVELAP Certification #: 460221 Asheville Certification IDs '2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 This report shall not be reproduced, except in full, without the wntten consent of Pace Analytical Services, LLC. Page 2 of 19 aXAnalytical. aT-MCa`AASS:VI'1 SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: STORMWATER 92315897 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92315897001 SW01.100716A EPA 1664B JMS 1 PASI-C EPA200.7 JMW 3 PASI-A SM 2540D MJSt 1 PASI-A EPA 9040 ALC 1 PASI-A 92315897002 SW02.100716B EPA1664B JMS 1 PASI-C EPA 200.7 JMW 3 PASI-A SM 2540D MJSt 1 PASI-A EPA 9040 ALC 1 PASI-A 92315897003 SW03-100716C EPA 1664B JMS 1 PASI-C EPA 200.7 JMW 3 PASI-A SM 2540D MJSt 1 PASI-A EPA9040 ALC 1 PASI-A 92316897004 SW04-100716D EPA 1664E JMS 1 PASI-C EPA 200.7 JMW 3 PASI-A SM 2540D MJSt 1 PASI-A EPA 9040 ALC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the witten consent of Pace Analytical Services, LLC. Page 3 of 19 aceAnalytical a rmrGs'.ehbszrn I PROJECT NARRATIVE Project: STORMWATER Pace Project No.: 92315897 Method: EPA 1664E Description: HEM, Oil and Grease Client: Parker Hannifin Corporation Date: October 21, 2016 Pace Analytical Services, LLC 9900 Kincey Ave. Suite 100 Huntersville, NC 29078 (704)975-9092 General Information: 4 samples were analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPOs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 19 laceAnal)ftal' wmvpeceAbxarm rrre�rx�r,rri�_ri►�i= Project: STORMWATER Pace Project No.: 92315897 Method: EPA 200.7 Description: 200.7 MET ICP Client: Parker Hannifin Corporation Date: October 21, 2016 Pace Analytical Services, LLC 9800 Kncey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 General Information: 4 samples were analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 200.7 with any exceptions noted below. Initial Calibrations (Including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 19 2ceAnalj4icalo as»:prxhbswn I PROJECT NARRATIVE Project: STORMWATER Pace Project No.: 92315897 Method: SM 2540D Description: 2540D Total Suspended Solids Client: Parker Hannifin Corporation Date: October 21, 2016 Pace Ana"cal Services, LLC 98001Gncey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 General Information: 4 samples were analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. QC Batch: 333072 D6: The precision between the sample and sample duplicate exceeded laboratory control limits. • DUP (Lab ID: 1845850) • Total Suspended Solids Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 19 72ceAnaljdical' amrFa'wAbsxm PROJECT NARRATIVE Project: STORMWATER Pace Project No.: 92315897 Method: EPA 9040 Description: 9040 pH Client: Parker Hannifin Corporation Date: October 21, 2016 Pace Analytical Services, LLC 98001Wcey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 General Information: 4 samples were analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. HIS: Analysis initiated outside of the 15 minute EPA required holding time. • SW01-100716A (Lab ID: 92315897001) • SW02-100716B (Lab ID: 92315897002) • SW03-100716C (Lab ID: 92315897003) • SW04-100716D (Lab ID: 92315897004) Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 19 aceAnalytical wnpaekbscortr ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92315897 Sample: SW01-100716A Lab ID: 92315897001 Collected: 10/07/16 10:15 Received: 10/13/16 10:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 10/21/16 08:45 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper NO ug/L 5.0 1 10/1411620:10 10/16/1610:55 7440-50-8 Lead NO ug/L 5.0 1 10/14/16 20:10 10/16/16 10:55 7439-92-1 Zinc 13.6 ug/L 10.0 1 10/14/16 20:10 10/16/16 10:55 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 5.0 1 10/13/16 17:12 9040 pH Analytical Method: EPA 9040 pH 7.2 Sid. Units 0.10 1 10/17/16 15:13 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/21/2016 04:42 PM i. without the mitten consent of Pace Analytical Services, LLC. Page 8 of 19 Pace Analytical Services, LLC 5ace 9800 Kincey ve. 100 Amlytical Hunterslle, NCte 28078(704)875-9092 I ANALYTICAL RESULTS Project: STORMWATER Pace Project No.: 92315897 Sample: SW02-10071613 Lab ID: 92315897002 Collected: 10/07/16 10:15 Received* 10113116 10:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO mg/L 5.0 1 10/21116 08:45 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper NO ug/L 5.0 1 10/14/16 20:10 10/16/16 10:58 7440-50-8 Lead NO ug/L 5.0 1 1011411620:10 10/1611610:58 7439-92-1 Zinc 24.2 ug/L 10.0 1 . 10/14/16 20:10 10/16/16 10:58 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids NO mg1L 2.5 1 10/13/16 17,12 9040 pH Analytical Method: EPA 9040 pH 6.1 Std. Units 0.10 1 10/17/16 15:13 H6 Date: 10/21/2016 04:42 PM REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full, without the written consent of Pace Analytical Services, L-C. Page 9 of 19 aceAnalXical e wam:prehuscan ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvdle, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92315897 Sample: SW03-100716C Lab ID: 92315897003 Collected: 10/07/16 10:15 Received: 10/13/16 10:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual HEM, Oil and Grease Oil and Grease 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids 9040 pH pH Date: 10/21/2016 04:42 PM Analytical Method: EPA 1664B ND mg/L 5.0 1 10/21/1608:45 Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 NO ug/L 5.0 1 10/14/16 20:10 10/16116 11:02 7440-50-8 NO ug/L 5.0 1 10/14/16 20:10 10/16116 11:02 7439-92-1 17.4 ug/L 10.0 1 10/14116 20:10 10/16/16 11:02 7440-66-6 Analytical Method: SM 2540D 2.9 mg/L 2.5 1 10/13/16 17:12 Analytical Method: EPA 9040 6.5 Sid. Units 0.10 1 10/17/16 15:13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L-C. H6 Page 10 of 19 Pace Analytical Services, LLC aceftlytical a 9800 Kincey Ave. Suse 100 Muntersville, NC 28078 I .parolebaoom (704)875-9092 I ANALYTICAL RESULTS Project: STORMWATER Pace Project No.: 92315897 Sample: SW04-100716D Lab ID: 92315897004 Collected: 10/07/16 10:15 Received: 10/13/16 10:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 10/21/16 08:45 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 6.0 ug/L 5.0 1 10/14/16 20:10 10/16/16 11:05 7440-50-8 Lead NO ug/L 5.0 1 10/14/16 20:10 10/16/16 11:05 7439-92-1 Zinc 35.6 ug/L 10.0 1 10/14/16 20:10 10/16/16 11:05 7440-66-6 2640D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 15.9 mg/L 3.1 1 10/13/16 17:13 9040 pH Analytical Method: EPA 9040 pH 6.6 Std. Units 0.10 1 10/17/16 15:13 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/21/2016 04:42 PM without the written consent of Pace Analytical Services, L-C. Page 11 of 19 aceAnalytical aawprxhbs:om QUALITY CONTROL DATA Pace Analytical Services, LLC 980(i nnoey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92315897 = QC Batch: 334036 Analysis Method: EPA 1664B QC Batch Method: EPA 16643 Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92315897001, 92315897002, 92315897003, 92315897004 METHOD BLANK: 1851541 Matrix: Water Associated Lab Samples: 92315897001, 92315897002, 92315897003, 92315897004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L NO 5.0 10/21/16 08:45 LABORATORY CONTROL SAMPLE: 1851542 Spike LCS LCS %Rec Parameter Units Conic. Result %Rec Limits Qualifiers Oil and Grease mg/L 40 37.6 94 78-114 MATRIX SPIKE SAMPLE: 1851543 92315825004 Spike MS MS % Rec Parameter Units Result Conic. Result %Rec Limits Qualifiers Oil and Grease mg/L ND 40 35.2 88 78-114 Results presented on this page are In the units Indicated by the 'Units' column except where an ahemate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/21/2016 04:42 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 19 ace Analytical rme(aahbispnr I QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntenville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92315897 OC Batch: 333145 Analysis Method: EPA 200.7 QC Batch Method: EPA200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92315897001, 92315897002, 92315897003, 92315897004 METHOD BLANK: 1846078 Matrix: Water Associated Lab Samples: 92315897001, 92315897002, 92315897003, 92315897004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 10/16/1610:16 Lead ug/L NO 5.0 10/16/1610:16 Zinc ug/L NO 10.0 1011611611:41 LABORATORY CONTROL SAMPLE: 1&46079 Spike LCS LCS %Rae Parameter Units Cone. Result % Rae Limits Qualifiers Copper ug/L 500 502 100 85-115 Lead ug/L 500 484 97 85-115 Zinc ug/L 500 503 101 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1846080 1846081 MS MSD 92315630005 Spike Spike MS MSD MS MSD % Rae Parameter Units Result Cone. Cone. Result Result % Rec % Rae Limits RPD Qual Copper ug/L 0.0062 500 500 513 517 101 102 70-130 1 mg/L Lead ug/L ND 500 500 466 471 93 94 70-130 1 Zinc ug/L ND 500 500 498 505 98 99 70-130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1846082 1846083 MS MSD 92315938002 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Cone. Cone. Result Result % Rae % Rae Limits RPD Oual Copper ug/L NO 500 500 499 497 99 99 70-130 0 Lead ug/L NO 500 500 469 472 94 94 70-130 1 Zinc ug/L 486 500 500 965 968 96 97 70-130 0 Results presented on this page are In the units Indicated by the 'Units' column except where an axemate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 10/21/2016 04:42 PM without the wnften consent of Pace Analytical Services, L-C. Page 13 of 19 aceAnalyftcal e arw.pe:ahbscom f QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92315897 QC Batch: 333072 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92315897001, 92315897002, 92315897003, 92315897004 METHOD BLANK: 1845847 Matrix: Water Associated Lab Samples: 92315897001, 92315897002, 92315897003, 92315897004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 10/13/16 17:11 LABORATORY CONTROL SAMPLE: 1845848 Spike LCS 1-CS h Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 238 95 90-110 SAMPLE DUPLICATE: 1845849 92315897001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 1845850 92315630001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 93.3 103 10 D6 Resuha presented on this page are In the units Indicated by the "Units" column except where an akemate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/21/2016 04:42 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 19 Zce Analytical wmxpa'dAbsxm QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92315897 QC Batch: 333423 Analysis Method: EPA 9040 OC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92315897001, 92315897002, 92315897003, 92315897004 SAMPLE DUPLICATE: 1847788 92315235001 Dup Parameter Units Result Result RPD Qualifiers pH Sid. Units 7.1 7.2 1 H6 SAMPLE DUPLICATE: 1847789 92315307006 Cup Parameter Units Result Result RPD Qualifiers pH Sid. Units 6.9 7.0 0 H6 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units Indicated by the'dnits' column except where an alternate unit is presented to me dam of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/21/2016 04:42 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 19 ZeAnaljifical' /� wewperohbswn I QUALIFIERS Project: STORMWATER Pace Project No.: 92315897 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Ouantitation Limit. RL - Reporting Limit. Pace Analytical Services, LLC 98001Gncey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each anayte is a combined concentration. Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPO - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited anayles. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PAST-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA required holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/21/2016 04:42 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 19 aceAnalytical e avepaxkbscom 1 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)879-9092 Project: Pace Project No.: STORMWATER 92315897 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92315897001 SW01-100716A EPA 16646 334036 92315897002 SW02-100716B EPA 1664B 334036 92315897003 SW03-100716C EPA 1664E 334036 92315897004 SW04-100716D EPA 1664B 334036 92315897001 SW01-100716A EPA200.7 333145 EPA 200.7 333294 92315897002 SW02.100716B EPA 200.7 333145 EPA 200.7 333294 92315897003 SW03-100716C EPA200.7 333145 EPA 200.7 333294 92315897004 SW04-100716D EPA 200.7 333145 EPA 200.7 333294 92315897001 SW01-100716A SM 2540D 333072 92315897002 SW02-100716B SM 2540D 333072 92315897003 SW03.100716C SM 2540D 333072 92315897004 SW04-100716D SM 2540D 333072 92315897001 SW01-100716A EPA9040 333423 92316897002 SW02.100716B EPA9040 333423 92315897003 SW03-100716C EPA 9040 333423 92315897004 SW04-100716D EPA9040 333423 Date: 10/21/2016 04:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Without the written consent of Pace Analytical Services, LLC. Page 17 of 19 I 1 , I i I Document Name: Document Revised: Sept. 21, 2016 Sam le Condition U on Recei t(SCUR Page 1 of 2 aceAnalyticW Document No.: Issuing Authority: F-CAR-CS-033-Rev.00 Pace Quality Office Client Name: I A WfD Project H: Courier; MFed Ex ❑UPS ❑LISPS ❑Cllent ❑ Commercial [-]Pace []Other:_ Custody Seal Present? ❑Yes WO#:92315597 1I111I 11I 1111 I1111I1 92315897 ONO 6 L R Date/Initials Person Examining Contents: Packing Material: []Bubble Wrap (YBubble Bags ❑None ❑Other:_ Thermometer V. []Blue❑None []Samples on ice, cooling process has begun I, Gun ID: Type of Ice: Correction Factor: 0,� Cooler Temp Corrected('C): 0s'% Biological Tissue Frozen? ❑Yes []No❑N/A Temp should be above fre)ting to VC USDA Regulated soil (RN/A, water sample) Did samples �rlginate in a quarantine tone within the United States: CA, NY, or 5C (check maps)? Did samples originate from a foreign source (Intern� tonally, ....., ". m.no f-Tv.. fWNO R NO Seals Intact? ❑Yes ❑yes sVNO Comments /Dlscre anc : Chain of Custody Present? Y s No ❑N/A 1. Samples Arrived within Hold Time? elye, ❑�No ❑N/A 2. Short Hold Time Analysis (<72 hr.)? []Yes [lrJNo ❑N/A 3. Rush Turn Around Tlme Requested? ❑Yes No N/A 4. Sufficient Volume? $ No ❑N/A 5: Correct Containers Used? Yes []No ❑N/A 6. -Pace Containers Used? Yes []NO N/A Containers Intact? Yes ONO N A 7. Samples Field filtered? No NA B. Note if sediment is visible in the dissolved container Sample labels Match COC? 11yes dyes ONO ❑N/A 9. } r F a c -Includes Date/Time/ID/Analysis Matrix: '� A v ;.1 D t'•e -. All containers needing acid/base preservatlon have been SCURF? � 1✓JYes [0]No ❑N/Atar� �: checked and documented on page tweet VOA, Coliform, TOC, Oil and Grease, DR013015 Exceptions: (water) DOC LLHg Samples checked for dechlorination? Yes ❑no ❑N/A 11. Heads ace In VOA Vials >5.6mm)? QYes ❑No N/A 12. ❑Yes ONO IJZN/A 13. Trip Blank Present? gN/A Trip Blank Custody Seals Present? []Yes❑Im Dery TAn P6n4 1 of u lif nurchatedl- CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Project Manager SCURF Review: Project Manager SRF Review: I Note: Whenever there Is a discrepancy affecting North Carolina comp Out of hold, incorrect preservative, out of temp, incorrect containersl Laboratoryr ceivingsamples: Asheville Edenn Greenwood a copy Huntersville 11 Field Data Required? LJYes UNo Date/Time: Date: I 0-13 _1 Date: I 0-t37(0 : sent to the North Carolina OEHNR Certification Office (i.e. Raleigh❑ MechanicsvllleEl Page 18 of 19 d CHAIN -OF -CUSTODY I Analytical Request Document dareNefCta .._ .. The ChairwbCustotly'a aLEGAL DOCUMENT. All relevam fields must be completed aCryratey. Saem A Seem a Secem C Reeulmd Cllem admpeerl: Aepueed Pm)an eJomulbn: hlvoks Ylierlllallon: Page, 1 Of 1 Cemoery Pa Namdm Cwoamien Re To: - Addrpa' 101 Came Rd. CM Te: Nanw Kmp ewn m NC 28M np—pmw. Em A: Purtauu Order �: ls: Prpe: Q Fu PmpO Nero: Smmlealm laaarO9er. aamn .me: 2Gus:!:Tut':'.Sbti[lontbnlS�:=iT:9'i'Y, Remasud Oue mm. p"" a: f 1 NC COLLECTED � Preservatives y• 'an 21 _ z �awaa. ow r wr rr.uw.r 3 w p a SAMPLE ID a � s srAAr END w WSamPN lee cruel to uraRw iyr n C s 0 O m9 t 4 a Y F u_0i y 55 al 2 1 1 x2z 7/� 2 IIIJ X x 5"103-100-2,1Z C. �s ?S�l Y :9a Myo:: Cea`'�a=ae il'.�4>`etRiONiITeoAmlla�'•-' �..vX �,';.y� :'Ar�ll�}¢111nor� 5..9NE" 4+ .7 �yq.v,AmRVrmB* �slannwei Y u TOE 'TYryKg.',r-9�@tPc�i�wb.,�,,, r l :LS✓li Ip 1 10.0u O.'1,•,.. n:...�...1 � �� � fr ®�+� Y� � ti•:A:ta�:`..'I �'bT.Y:+nl���ii �17c• ... t Z� � d11 m m a ceAnalytical e asrw.peuslabs.corn June 07. 2016 Robert Simpson Parker Hannifin Corporation 101 Canterbury Rd. Kings Mountain, NC 28086 RE: Project: STORMWATER SAMPLING Pace Project No.: 92298447 Dear Robert Simpson: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite too Hunlersville, NC 28078 (704)875-9092 I� C & v 300% dun-54Ae .0-`Z,4(0 RECEIVED JUN 2 0 MIS CENTRAL FILES DWR SECTION Enclosed are the analytical results for sample(s) received by the laboratory on May 20, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. Container for sample ID 051916B/002 broke on shipment transit, analysis Oil & Grease. If you have any questions concerning this report, please feel free to contact me. Sincerely, W,a— Liamm Harrison liamm.harrison@pacelabs.com Project Manager REPORT OF LABORATORY ANALYSIS This report shall not W reproduced, except in full, Without the written consent of Pace Analytical Services, Inc.. Page 1 of 27 aceAnalytical 0 P6cvbbS,mmm June 07, 2016 Page 2 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 26078 (704)878-9092 Page 2 of 27 ateAnalj6cal M .pacebb&= Project: STORMWATER SAMPLING Pace Project No.: 92298447 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the whiten consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 700 Huntersville, NC 28078 (704)8759092 Page 3 of 27 mAnalytical w pacafabs can SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Project: Pace Project No.: STORMWATER SAMPLING 92298447 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92298447001 SW01-051916A EPA 200.7 CDF 3 PASI-A SM 2540D MJP i PASI-A EPA 9040 TEP 1 PASI-A 92298447002 SW02.051916B EPA 200.7 CDF 3 PASI-A SM 2540D MJP 1 PASI-A EPA 9040 TEP 1 PASI-A 92298447003 SW03-051916C EPA 200.7 CDF 3 PASI-A SM 2540D MJP 1 PASI-A EPA 9040 TEP 1 PASI-A 92298447004 SW04.051916D EPA200.7 CDF 3 PASI-A SM 2540D MJP 1 PASI-A EPA 9040 TEP 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 27 aceAnalytical e e rpxalsbs.con PROJECT NARRATIVE Project: STORMWATER SAMPLING Pace Project No.: 92298447 Method: EPA 200.7 Description: 200.7 MET ICP Client: Parker Hannifin Corporation Date: June 07, 2016 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunterswile, NC 28078 (704)875-9092 General Information: 4 samples were analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 200.7 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 27 aceAnalylical a wwwpwelabs a= PROJECT NARRATIVE Project: STORMWATER SAMPLING Pace Project No.: 92298447 Method: SM 2540D Description: 2540D Total Suspended Solids Client: Parker Hannifin Corporation Date: June 07, 2016 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite too Huntersville, NC 28078 (704)875-9092 General Information: 4 samples were analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDS) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. OC Batch: WET/45099 D6: The precision between the sample and sample duplicate exceeded laboratory control limits. • DUP (Lab ID: 1739746) • Total Suspended Solids Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 27 aceAnalytical e xww.pecelabs.cm PROJECT NARRATIVE Project: STORMWATER SAMPLING Pace Project No.: 92298447 Method: EPA 9040 Description: 9040 pH Client: Parker Hannifin Corporation Date: June 07, 2016 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 General Information: 4 samples were analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. H6: Analysis initiated outside of the 15 minute EPA required holding time. • SW01-051916 A (Lab ID: 92298447001) • SW02-051916 B (Lab ID: 92298447002) • SW03-051916 C (Lab ID: 92298447003) • SW04-051916 D (Lab ID: 92298447004) Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, withoul the written consent of Pace Analytical Services. Inc.. Page 7 of 27 aceAnalylical e w w.pboslaas.cam ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Project: STORMWATER SAMPLING Pace Project No.: 92298447 Sample: SWOt-051916A Lab ID: 92298447001 Collected: 05/19/1611:30 Received: 05120/1608:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper ND ug/L 5.0 1 05/23/16 18:30 05/26/16 00:58 7440-50-8 Lead ND ug/L 5.0 1 05/23/16 18:30 05/26/16 00:58 7439-92-1 Zinc 19.4 ug/L 10.0 1 05/23/16 18:30 05/26/16 00:58 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 2.6 mg/L 2.5 1 05/24/16 11:47 9040 pH Analytical Method: EPA 9040 pH 6.7 Sid. Units 0.10 1 05/25/16 11:50 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/07/2016 08:16 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 27 5ceAna1j6ca1 w Pecsbes.cam ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)8759092 Project: STORMWATER SAMPLING Pace Project No.: 92298447 Sample: SW02-051916 B Lab ID: 92298447002 Collected: 05/19/16 11:30 Received: 05/20/16 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper ND ug/L 5.0 1 05/2311618:30 05/2611601:50 7440-50-8 Lead ND ug/L 5.0 1 05/23/1618:30 05/26/1601:50 7439-92-1 Zinc 31.6 ug/L 10.0 1 05/23/16 18:30 05/26/16 01:50 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 5.0 1 05/24/16 11:47 9040 pH Analytical Method: EPA 9040 pH 6.3 Sid. Units 0.10 1 05/25/16 11:50 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/07/2016 08:16 AM without the wdtten consent of Pace Analytical Services, Inc.. Page 9 of 27 aceAnaljftal e w ..pecembs,com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER SAMPLING Pace Project No.: 92298447 Sample: SW03-051916 C Lab ID: 92298447003 Collected: 05119/16 11:30 Received: 05/20/16 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids 9040 pH pH Date: 06/07/2016 08:16 AM Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 ND ug/L 5.0 1 05/23/16 18:30 05/26/16 01:59 7440-50-8 ND ug/L 5.0 1 05/23/16 18:30 05/26/16 01:59 7439-92-1 24.4 ug/L 10.0 1 05/23/16 18:30 05/26/16 01:59 7440-66-6 Analytical Method: SM 2540D 12.9 mg/L 5.6 1 05/24/1611:47 Analytical Method: EPA 9040 6.6 Sid. Units 0.10 1 05/25/16 11:50 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 27 aceAnalytical a ...Pacekbs.= ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Project: STORMWATER SAMPLING Pace Project No.: 92298447 Sample: SW04.051916 D Lab ID: 92298447004 Collected: 05/19/16 11:30 Received: 05/20/16 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids 9040 pH pH Date: 06/07/2016 08:16 AM Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 ND ug/L 5.0 1 05123/1618:30 05/2611602:03 7440-50-8 ND ug/L 5.0 1 05/23/16 18:30 05/26/16 02:03 7439-92-1 18.7 ug/L 10.0 1 05123/1618:30 05126/1602:03 7440-66-6 Analytical Method: SM 2540D 3.7 mg/L 2.5 1 05/2411611:48 Analytical Method: EPA 9040 6.7 Sid. Units 0.10 1 05/25/16 11:50 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the wntten consent of Pace Analytical Services, Inc.. Page 11 of 27 aceAnalytical ...pecelebacorn QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92298447 UL; batch: MPRP/21798 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92298447001 METHOD BLANK: 1739813 Matrix: Water Associated Lab Samples: 92298447001 Parameter Copper Lead Zinc Blank Reporting Units Result Limit Analyzed ug/L ND 5.0 05/25/16 23:13 ug/L NO 5.0 05/25/16 23:13 ug/L NO 10.0 05/26/1616:44 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1739814 Spike LCS LCS % Rae Parameter Units Conc. Result / Rae Limits Qualifiers Copper ug/L 500 490 98 85-115 Lead ug/L 500 456 91 85-115 Zinc ug/L 500 448 90 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1739815 1739816 MS MSD 92298144005 Spike Spike MS MSD MS MSD e/ Rec Parameter Units Result Cone. Cone. Result Result % Rae e/ Rae Limits RPD Qual Copper ug/L 25.9 500 500 499 501 95 95 70-130 0 Lead ug/L 7.4 500 500 434 432 85 85 70-130 0 Zinc ug/L 59.0 500 500 480 475 84 83 70-130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1739817 1739818 MS MSD 92298607001 Spike Spike MS MSD MS MSD % Rae Parameter Units Result Cone. Cone. Result Result % Rae % Rae Limits RPD Qua] Copper ug/L 9.6 500 500 488 491 96 96 70-130 1 Lead ug/L NO 500 500 438 437 87 87 70-130 0 Zinc ug/L 41.5 500 500 462 465 84 85 70-130 1 Results presented on this page are In the units indicated by One -Unba^ column except where an alternate unit is presented to One right of Me result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 06/07/2016 08:16 AM without the written consent of Pace Analytical Services, Inc.. Page 12 of 27 aceAnalytical wrw.pecelebs.can QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92298447 u u batch: MPKP/21799 Analysis Method: EPA200.7 OC Batch Method: EPA200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92298447002, 92298447003, 92298447004 METHOD BLANK: 1739819 Matrix: Water Associated Lab Samples: 92298447002, 92298447003, 92298447004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L NO 5.0 05/26/16 01:44 Lead ug/L NO 5.0 05/26/16 01:44 Zinc ug/L NO 10.0 05126/1601:44 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite too Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1739820 Spike LCS LCS % Rec Parameter Units Conic. Result % Rec Limits Qualifiers Copper ug/L 500 483 97 85-115 Lead ug/L 500 444 89 85-115 Zinc ug/L 500 429 86 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1739821 1739822 MS MSD 92298447002 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conic. Conc. Result Result %Rec % Rec Limits RPD Qual Copper ug/L ND 500 500 497 479 99 95 70-130 4 Lead ug/L NO 500 500 449 433 90 86 70-130 3 Zinc ug/L 31.6 500 500 461 445 86 83 70-130 3 Results presented on Nis page are In Me units Indicated by Me -Unite' column except where an altemate unit is presented to Me right of Me result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/07/2016 08:16 AM without the written consent of Pace Analytical Services, Inc.. Page 13 of 27 aceAnalytical a»w.psoa'abs.cwn QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92298447 QC Batch: WET/45099 Analysis Method: SM 2540D OC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92298447001, 92298447002, 92298447003, 92298447004 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 METHOD BLANK: 1739744 Matrix: Water Associated Lab Samples: 92298447001, 92298447002, 92298447003, 92298447004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L NO 2.5 05/24/16 11:43 LABORATORY CONTROL SAMPLE: 1739745 Spike LCS LCS %Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 240 96 90-110 SAMPLE DUPLICATE: 1739746 92298318001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 94.0 106 12 D6 SAMPLE DUPLICATE: 1739747 92298447002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND 12.0 Results presented on Mia papa are In Me units Indicated by the 'Units" column except where an alternate unit is presented to Me right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/07/2016 08:16 AM without the written consent of Pace Analytical Services, Inc.. Page 14 of 27 aceAnalytical e we»:ptrceAh.arn QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92298447 QC Batch: WET/45117 Analysis Method: EPA 9040 OC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92298447001, 92298447002, 92298447003, 92298447004 SAMPLE DUPLICATE: 1740634 92298574001 Dup Parameter Units Result Result RPD Qualifiers pH Std. Units 7.2 7.2 0 H6 SAMPLE DUPLICATE: 1740635 92298608001 Dup Parameter Units Result Result RPD Qualifiers pH Std. Units 7.1 7A 0 H6 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Results presentee on this pair. are In Me units Indicated by Me'Units' column except w ern an alternate unit is presented to Me riBet of Me resuR. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/07/2016 08:16 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 27 aceAnalytical ..pacel9esmn QUALIFIERS Project: STORMWATER SAMPLING Pace Project No.: 92298447 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. POL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA required holding time. Date: 06/07/2016 08:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 16 of 27 aceAnalj6cal. ~paces.= QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 9800 Kincay Ave. Suite 100 Huntersville, NC 28078 (704A75-9092 Project: Pace Project No.: STORMWATER SAMPLING 92298447 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92298447001 SW0I-051916A EPA 200.7 MPRP/21798 EPA200.7 ICP/19558 92298447002 SW02-051916E EPA 200.7 MPRP/21799 EPA200.7 ICP/19559 92298447003 SW03-051916C EPA 200.7 MPRP/21799 EPA 200.7 ICP/19559 92298447004 SW04-051916D EPA 200.7 MPRP/21799 EPA 200.7 ICP/19559 92298447001 SWOt-051916A SM 2540D WET/45099 92298447002 SW02-051916 B SM 2540D WET/45099 92298447003 SW03-051916 C SM 2540D WET/45099 92298447004 SW04-051916 D SM 2540D WET/45099 92298447001 SW0l-051916A EPA 9040 WET/45117 92298447002 SW02-051916E EPA 9040 WET/45117 92298447003 SW03-051916C EPA9040 WET/45117 92298447004 SW04-051916D EPA 9040 WET/45117 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/07/2016 08:16 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of 27 I Document Name: Document Revlsed:April 25, 2016 aceAnalytical Sample Condition Upon Receipt(SCUR) Page 1 of 2 i - I Document No.: Issuing Authority: F-CHR-CS-Dna- 19 Pace Huntersville Quality Office Client Name: ,, II Paee 2 of 2 for Internal Use ONLY Pa/K� n Project 1 WO# : 92299447 ann F'n Courier: 0 ed Ex UUPS ❑LISPS ❑Client ❑ Commercial ❑Pace ❑Other: 11111111111111111111111 92298447 Custody Seal Present? ❑Yes ONO Seals Intact? ❑Yes []NO �� Date/Initials Person Examining Contents s� Packing Material: ❑Bubble Wrap QBubble Bags ❑None! ❑Other:_ Thermometer: T1505 Type of Ice: Wet 08lue ❑None BSamples on ice, cooling process has begun Correction Factor: 0.0'C Cooler Temp Corrected ('C): ( <� (- Biological Tissue Frozen? [:]Yes ❑Q No NN'/A Temp should be above freezing to 6°C USDA Regulated Sbil (Q N/A, water sample) Dld samples% Iginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source Qntemay'onally, ❑Yes ❑ry0 including Hawali and Puerto Rico)? ❑Yes ❑(Jo Comments/Discrepancy: Chald of CustodyPresent? ONOA 1. Samples Arrived within Hold Time? ONO 2. Short Hold Time Analysis (<72 hr.)? WeSONO 3. Rush Turn Around Time Requested? 4. Sufficient Volume? 5. Correct Containers Used? 6. -Pace Containers Used? es ONO ❑N/A Containers Intact? ❑Y s ONO ' N/A 7. Samples Field Filtered? Oyes ONO N/A 8. Note If sediment Is visible in the dissolved container Sample Labels Match CDC? Yes ❑No ❑N/a 9. -Includes Date/nme/ID/Anal sis Matrix: All containers needing acid/base preservation have been 10' w'�IMaz checked? - ❑Ves ONO ❑N/A Ail containers needing preservation are found to be In compliance with EPA recommendation? (HNDs, HzSO., HCI<2; NaOH >9 Sulfide, NaOH>12 Cyanide) Oyes ONO ❑N/A xnoao".: Exceptions: VOA, Coliform, TOC, Oil and Grease, "+urwrr DRO/8015 (water) DOC,LLHg ❑Yes ONO N/A Samples checked for dechlorination? ❑Yes ONO ❑N/A 11. ' Heads ace in VOA Vlals (>5-6mm)? OYes ONO ❑N/A 12. Trip Blank Present? Oyes ONO ❑N/A 13. Trip Blank Custody Seals Present? ❑Yes ONO ❑N/A Pace Trip Blank Lot R (if purchased): [CAI ION RESOUJIION Person Contacted: Comments/Sample Discrepancy: Project Manager SCURF Review: Field Data Required? ❑Yes ❑No Date/Time: Date: T:ci-C lt., Project Manager SRF Review: L..-.it Date: r? j.2-C 1 U Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, Incorrect preservative, out of temp, Incorrect containers) Page 18 of 27 P ceAnalytical- ww.aiulrei.[v2 CHAIN -OF -CUSTODY if Analytical Request Document Th. Chain-of-Cusmtly is a LEGAL DOCUMENT. All relevant fields must be completed accurately. r N G On Section A Section B Required Client Informalion: R.qulr.d Protectan: Section C Page: ofCy CompeOy: Invoice Inform fteporl To: ABembn: ' / r Agar ems:/ /[/ Covr To: i 1997260 !/ —m Z r REGU YAGENCY Addr ! NPDES 7—GROUND WATER i DRINKING WATER Purchase Ordar NO_ Fn . Rao,mm: /v i UST RCRA OTHER O `PaWPhil- ®Rt!;d--0Da,. T: PmjCCI Number: Mamup; Site LUCaIIOn Paca Pmlllu /v STATE: a f = Bohan D Matrix Codas aoaui,oaaaemmn,v.,,W MATRIX r GOOF Drinki,g Wabr DW Water WT West. Water Wye Product P SoiYSetitl SL SAMPLE ID oil OL Wipe WP (A-Z. 9.91: ) AR Samp)C ID. MUST BE UNIQUE Tnaue TS Ou,er OT — 9 § n = up 0 U a( C < s 0 D a It pa < a `a COLLECTED O V j 0 < 4 W w Q z O U 0 x Preservatives > Reque ed Analysis Fiftered (Y/Nj CUMYoyie START cUWVyTE 6,oTaAa Tp d N u j=_ O m O x = s 2 O Z C al r= F L O -. N 1� N N . is Q '� I Z o t U a � a va v Pace Project No.f L I.D. DATE TIME pgif TIME 2 b Aff — I a to 03Li /Q B 6 7 6 9 10 11 2 ADDITIONAL COMMENTS ELINOUISHED BY I AFFILIATION DATE TIME�7 ACCEPTED BY I AFFILIATION DATE TIME yzU SAMPLE CONDITIONS Gr��'Iv^� 'MWrlam Nd.: By ppnuq has lam Wu a,u>dSpdg P.ce. NET b day paY n apple am SAMPLER NAME AND SIGNATURE E " _ ¢ u U w _ E y PRINT Name of SAMPLER: N - C/y SIGNATURE of SAMPL DATE Sign 5— M.,aIY anmuun ini.e..n........e, y.A . pcnnMm la any m.urei na wnlw 30 treys. F-ALL-Q-020rev.07. 15-May-2007 ENVOLaboratories Accurate. Timely. Responsive. Innovative. 4810 Executive Park Court, Suite ill Jacksonville FL, 32216-6069 Phone: 904.296.3007 FAX: 904.296.6210 Monday, June 6, 2016 Pace Analytical (PA007) Attn: Liamm Harrison 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 RE: Laboratory Results for Project Number: Stormwater Sampling, Project Name/Desc: 92298447 ENCO Workorder(s): BZ02257 Dear Liamm Harrison, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, May 24, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Jacksonville. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chris Tompkins Project Manager Enclosure(s) HNX This report relates only W the sample as re ed by the laboratory, and may only be tepmducal In ful. Page 20 of 27 page 1 of a PRO]ECT NARRATIVE Client: Pace Analytical (PA007) Project: 92298447 ENCO Project ID: BZ02257 Overview Cam ti www.encolabs.com All samples submitted were analyzed by Environmental Conservation Laboratories, Inc. in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling and processing will be discussed in the Remarks section below. Analysis: EPA 1664B Affected Samples: SW02-051916 B[BZ02257-02] Sample SW02-051916 was received in the laboratory broken and the analysis was canceled. The client was notified. Chris Tompkins Project Manager Page 21 of 27 FlNAL This report relates w* to the sample as re W try the latmatory, aM maY o* oe woo .a i ao MI. Pape 2 of 8 W W W.enmlabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: SWOT-051916A Lab ID: BZOM7.01 Sampled: 05/19/16 11:30 Received: 0S/24/16 11:D0 Parameter EPA 1664E Hold Date/Time(s) 06/16/16 Prep Date/Time(s) 06/03/16 10:41 An awls Date/Timefsl 06/03/16 17:58 Client ID: SW03-051916C lab ID: BZ02257-03 Sampled: 05/19/16 11:30 Received: 05/24/16 11:00 Parameter EPA 1664B Hold Date/Time(,) 06/16/16 Prep Date/Time(,) 06/03/16 10:41 Analysis Dare/Time(s) 06/03/16 17:58 aletd ID: SW04-051916D lab ID: BZ02257-04 Sampled: 05/19/16 11:30 Received: 05/24/1611:00 Pammstsl EPA 16648 Hold Date/Time(,) 06/16/16 Prep Date/Time(s) 06/03/16 10:41 AmWsis Date/Time(sl 06/03/16 17:56 Page 22 of 27 FINAL This report rdata Wy to Me sample as recayed by tte laboratory, and may mN in MI. Page 3 of 8 SAMPLE DETECTION SUMMARY Has mu Em 3 0.628 1.31 w .encolab&ieem Me thod tlste PA 1664E �= Results MES ma EQL thllts M€Y199 Notin Oil & Grease (HEM) 0.924 3 0.616 1.28 rng/L EPA 16698 aient ID: SW04-051916 D Lab ID: SZ02257-04 Analvice Ri llYi fin NDL Em volu Method N91e2 Oil & Grease (HEM) 1.13 ] 0.619 1.29 m9/L EPA 16648 Page 23 of 27 IINAl ibis report relates only to the sample as re w by the bbaretory, am may only oe reproou in ail. Page 4 of 8 ANALYTICAL RESULTS Description: SW01-051916 A tab Sample ID: BZ02257-01 Matrix: Water Sampled: 05/19/1611:30 Project: 92298447 Sampled By: Classical Chemistry Parameters ^-� Jact n,r ¢rcAs>anaryre(AC 4477 Analrte fCAS Numberl Results Flag Multi PE 4DL POE BatCh Method Oil & Grease (HEM) [C-0007]^ 0.732 1 mg/L 0.262 0.628 1.31 6F03004 EPA 1664B Description: SW03-051916 C Matrix: Water Project: 92298447 Classical Chemistry Parameters Lab Sample ID: BZ02257-03 Sampled: 05/ 19/ 16 11:30 Sampled By: Analvte !CAS Numberl Resg]ft Flag Units III Hu ]JZy Batch Oil & Grease (HEM) [C-0007]^ 0.924 1 mg/L 0.257 0.616 1.28 6F03004 Description: SW04-051916 D Lab Sample I0:BZ02257-04 Matrix: Water Sampled: 05/19/16 11:30 project: 92298447 Sampled By: Classical Chemistry Parameters Analvta fCAS Number! Oil & Grease (HEM) [C-0D07]^ GE N CmP W Ww.encolabs.com Received: 05/24/16 11:00 Work Order: BZ02257 Analyzed By NoteI 06/03/1617:58 SMA Received: 05/24/16 11:00 Work Order: BZ02257 Method ADalnsd am m9lu EPA 16648 06/03/16 17:58 SMA Received: 05/24/16 11:00 Work Order: BZ02257 Results flag Sulu l2E Ku Mi. Batch Method Analy[!A BY KRIM 1.13 1 m9/1- 0.258 0.619 1.29 6F03004 EPA 1664E 06/03/16 17:58 SMA Page 24 of 27 FIW1L This report relates oNy to the sample as r , al by the Wboralory, artl may o* be reprotuc in N8. Page 5 of 8 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry parameters - Quality Control Batch 6F03004 - EPA 1664B Blank (6F03004-BLKI) Prepared: 06/03/2016 10:41 Analyzed: 06/03/2016 17:58 Spike Source a/.REC RPD Anahrg Resift Flag COL Units Level Result %REC t[mits RPD Limit Notes Oil & Grease (HEM) 0.622 U 1.30 mg/L LCS (6F03004-BSI) Prepared: 06/03/2016 10:41 Analyzed: 06/03/2016 17:58 Spike Source %REC RPD Anatvte Resift F.Im P4L [Ruts Level Result ^/eREC LImjtf RPD Limit Notes Oil & Grease (HEM) 141 5.00 mg/L 160 88 78-114 LCS Dup (6F03004-BSD1) Prepared: 06/03/2016 10:41 Analyzed: 06/03/2016 17:58 Spike Source %REC RPD ADdhfte Result Flag COL Unib Level Result %REC Limits RPD u mit Notes Oil & Grease (HEM) 137 5.00 mg/L 154 89 78-114 3 18 Matrix Spike (6F03004-MSI) Prepared: 06/03/2016 10:41 Analyzed: 06/031201617:58 Source: BZ02299-01 Spike Source %REC RPD Analvte Result Flag POL 1.101113 Level Result %REC Limits RPD Limit RR$i Oil & Grease (HEM) 34.2 1.26 mg/L 40.2 0.604 U 85 78-114 Page 25 of 27 FINAL This report relates only W t sample a$ rx ,fd by the Ial>mto y, and may only lie repro: mW in full. Pape 6 of 8 www.encolab&mrn FLAGS/NOTES AND DEFINITIONS B The anatyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyze was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyze is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyze for which there is presumptive evidence (85% or greater confidence) to make a'tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. Page 26 of 27 FlNAL Tltls report rdxtes only to tJV sample as r¢eivxl by ttre laboratory, aM may onb be rep� In U. Pape 7 or 8 Chain .ot= Custody Workorder: 92299447 Workorder Name: SIORMVVATER SAMPLING Results Requested By: 6/612016 eAnalytical Report 13nvoice To L Reqt steflAnalysis, Liamm Harrison Pace Analytical Charlotte P.1 Of t4 9800 Kincey Ave. Suite 100 .7 HUntersville, NC 28078 Phone (704)875-9092 7- Email: fiamm.hamson@pacelabs.com :,State of Sample Origin; NC 1: Yresomiad Contatners "Collect l In La5lD Matrix I I LAB USE ONLY 1 SW01-051918 A 511912016 11 30 92298447001 Water x 2 SVV02 O51916 9 5119/2016 11:30 92208447002 wale. x 3 SW03-05191r C 511912016 11 30 92298447003 walm x 15i19/2016 11:30 9229B 4700 I Water x . ... . .... . ... -C Transfers Released By Date/Time Received By '— r 3 Cooler Temperature on Receipt C2 9 C Custody Sea[ jVor N I Received on Ice or N Samples lnta r N Friday, May 20. 20113 10.20104 AM 0 `tJ1T-ALL-C-00220ti.00 24M.irrh2nn9 P;te;r I of t 4 / : PaceAnalytical ` s'ns•.PacelaEa.cam CHAIN -OF -CUSTODY / Analytical Request Document The Chain-af-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Required Client Information: Required Project on: Invoice Infomfa' Company: `n L.G �; Report To: c Attention: Page: of 1997260 Adtlr �s:/ !/ Copy To: Z Uen, REGU66TC19Y AGENCY . Purchase Ortler No.. Add r �...— Pacence, w Reference, /[./ NPDE$ i GROUND WATER I— DRINKING WATER r RCRA f— UST r OTHER Project NalAe: w n Pace Project Manager: Site Location STATE. _ Requested Due Date/TAT: Project Number: f 10 Pace Profile b: /v Requesfed Analysis It It Y/N)"'" ` - ;.:t9�f.,.•;f a• a f ~ t Section D Matrix Codes Required Client lnlomuYon MATRIX /CODE Banking Water DW ' Water WT Waste Water WW Product P Soil/Solid SL SAMPLE ID Oil OL Wipe WP (A-Z, D-O l :) Air AIR Sample IOs MUST BE UNIQUE Tissue. TS Other OT I/ n. n m p U x E 00 Q K p- pe a COLLECTED z O F j ¢ F, u, p.LL z Q Z O # Preservatives ''r COMPOSITE START COMPOSITE ENpICRAe o 0 v mO' C S O= I. _0 Z Z o m f O N b •y .N y' ;A Q �T ` c o U Pace Project No./ Lab I.D. TDATETIIE �916 TDAT�TIME< , r A 3 w — o i _/ I w —o n / 5 6 T .S' 9 10 TELL] it 121 ADDITIONAL COMMENTS JtIEUNQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY/AFFILIATION DATE TIME SAMPLE CONDITIONS ry1 yzL> U • SAMPLER NAME AND SIGNATURE U c a a ~ m 'e' _ Of u U' ° L' t°n 3 = ` E is o PRINT Name of SAMPLER: SIGNATURE of SAMPL DATE Signed // —/ (MM/DDIYY): J i1--ALL-0-020rev.07, 15-May-2007 Feb 03, 2016 NPDES General Permit COC: NCG030296 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Hydraulics Adrian Gutierrez Engineering Manager Parker Hannifin Corporation Gear Pump Division 101 Canterbury Road Kings Mountain, NC 28086 Tel: (704) 730-5707 Fax: (260)342-4184 RECEIVED FEB .10 2016 IZENTRAL FILES UM SECTION Re: NPDES Stormwater Sampling (YEAR 3, PERIOD 2 Bi-annual results) Parker Hannifin Corporation Gear Pump Division 101 Canterbury Road Kings Mountain, Gaston County, North Carolina 28086 Parker Hannifin Corp. (Parker Hannifin) located at 101 Canterbury Road, Kings Mountain, Gaston County, North Carolina, is pleased to submit the attached stormwater sampling results for our facility to meet the NPDES General Permit (COC NCG030296) stormwater sampling requirements for Year 3, Period 2 sampling. Parker Hannifin sampled the identified four outfalls at the site on 12/17/15, as per the NPDES General Permit Requirements. The stormwater samples were analyzed for parameters listed in Section B Table 1 (pH, Total Suspended Solids, Non -Polar Oil & Grease, Copper, Total Recoverable Lead, and Total Recoverable Zinc). Total Toxic Organic Compounds (TTO) were not analyzed since the facility is not categorized as a metal finishing operation. The rainfall amounts were measured during the rain event and recorded as required. Based on the sampling results, the analytical results were below the Benchmark Values presented in Section B, Table 3 of the Stormwater General Permit. Respectfully submitted, Parker Hannifin Co , Adrian 'utierrez Engineering Manager s aceAnalytical w rpacemhamm December 30, 2015 Robert Simpson Parker Hannifin Corporation 101 Canterbury Rd. Kings Mountain, NC 28086 RE: Project: STORMWATER SAMPLING Pace Project No.: 92280576 Dear Robert Simpson: Pace Anatocal Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875>9092 Enclosed are the analytical results for sample(s) received by the laboratory on December 18, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, \,�r Pv— cG./vJy— Liamm Harrison liamm.harrison@pacelabs.com Project Manager Endosures REPORT OF LABORATORY ANALYSIS This report shall net be reproduced, except in full, without the whiten consent of Pace Analytical Services, Inc. Page 1 of 20 ace Analytical www.pacm'edamm Project: STORMWATER SAMPLING Pace Project No.: 92280576 Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS FloridalNELAP Certification #: E87627 Kentucky LIST Certification #: 84 West Virginia Certification #: 357 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. _ Page 2 of 20 aceAnalytical e SAMPLE ANALYTE COUNT Pace Ana"cal Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project Pace Project No.: STORMWATER SAMPLING 92280576 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92280576001 SW01-121715A EPA1664B JMS 1 PASI-C EPA 200.7 CDF 3 PASI-A SM 2540D MDW 1 PASI-A EPA 9040 MLS 1 PASI-A 92280576002 SW02-1217158 EPA 1664B JMS 1 PASI-C EPA 200.7 CDF 3 PASI-A SM 25400 MDW 1 PASI-A EPA 9040 MLS 1 PASI-A 92280576003 SW03-121715C EPA 1664B JMS 1 PASI-C EPA 200.7 CDF 3 PASI-A SM 2540D MDW 1 PASI-A EPA9040 MLS 1 PASI-A 92280576004 SW04-121715D EPA 16648 JMS 1 PASI-C EPA 200.7 CDF 3 PASI-A SM 2540D MDW 1 PASI-A EPA 9040 MLS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, vvrff ud the written consent of Pace Analytical Services. Inc.. Page 3 of 20 aceAnalytical w pewrabamm PROJECT NARRATIVE Project: STORMWATER SAMPLING Pace Project No.: 92280576 Method: EPA 16648 Description: HEM, Oil and Grease Client: Parker Hannifin Corporation Date: December 30, 2015 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 General Information: 4 samples were analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within OC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be repmduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 20 aceAnaly6cale wwrpsmhb& m PROJECT NARRATIVE Project: STORMWATER SAMPLING Pace Project No.: 92280576 Method: EPA 200.7 Description: 200.7 MET ICP Client: Parker Hannifin Corporation Date: December 30, 2015 Pace Analytl al Services, Inc. 98001Gncey Ave. Suite 100 Huntersville, NC 28078 (704)875s9092 General Information: 4 samples were analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold limes with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 200.7 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Method Blank: All anatytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory controi spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. QC Batch: MPRP/20342 A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92280569001 Ml: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. MS (Lab ID: 1634425) • Lead MSD (Lab ID: 1634426) • Lead Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 20 e aceAnalylical srepe�eGxmn PROJECT NARRATIVE Project: STORMWATER SAMPLING Pace Project No.: 92280576 Method: SM 2540D Description: 2540D Total Suspended Solids Client: Parker Hannifin Corporation Date: December 30, 2015 Pave Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 General Information: 4 samples were analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Addidonal Comments :14;[G ttelSIa1-Zd:7_\I101:ZY/ :I_\W&I1.1 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 20 s aceAnalytical ...perdehimrn PROJECT NARRATIVE Project: STORMWATER SAMPLING Pace Pmject No.: 92280576 Method: EPA 9040 Desviption: 9040 pH Client: Parker Hannifin Corporation Date: December 30, 2015 General Information: Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Hunters ille, NC 28078 (704)8759092 4 samples were analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below or on the chainof custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. H6: Analysis initiated outside of the 15 minute EPA recommended holding time. • SW01-121715A (Lab ID: 92280576001) • SW02-121715E (Lab ID: 92280576002) • SW03-121715C (Lab ID: 92280576003) • SW04-121715D (Lab ID: 92200576004) Method Blank: All analyfes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within OC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. QC Batch: WET/42121 06: The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. • DUP (Lab ID: 1635112) - pH Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Page 7 of 20 • aceAnafytical w•rpsm'aoamn ANALYTICAL RESULTS Pace Analytical Services, Inc. 98001Gncey Ave. Suite 100 Huntersmile, NC 28078 (704)8759092 Project: STORMWATER SAMPLING Pace Project No.: 92280576 Sample: SW01-121715A Lab ID: 92280576001 Collected: 12/1711507:15 Received: 1211811510,30 Matrix, Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO mg/L 5.0 1 12/30/15 05:03 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper NO ug/L 5.0 1 12/21/1518:00 12124/1504:39 7440-50-8 Lead ND ug/L 5.0 1 12121/1518:00 12/2411504:39 7439-92-1 Zinc 28.7 ug/L 10.0 1 12121/1518:00 12/24/1504:39 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 2.5 1 12123/15 13:38 9040 pH Analytical Method: EPA 9040 pH 6.4 Std. Units 0.10 1 12/'21/15 11:15 H6 N REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2015 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 20 aceAnalytical e s Pecelah&t ANALYTICAL RESULTS Pace Analytical Services, Inc. 98001GnceyAve. Suite 100 Huntersville, NC 28078 1704)875-9092 Project: STORMWATER SAMPLING Pace Project No.: 92280576 Sample: SW02-121715B t.ablD: 92280576002 Collected: 1211711507:25 Received: 12118/1510:30 Matrix: Water Parameters Results Units Report Limit OF Prepared Anatyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO mg/L 5.0 1 12/30/15 05:04 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper NO ug/L 5.0 1 12121/1518:00 12/24/1504:42 7440-50-8 Lead NO ug/L 5.0 1 1212111518:00 12124/1504:42 7439-92-1 Zinc 18.6 ug/L 10.0 1 1212111518:00 1212411504,42 744066-6 2540D Total Suspended Solids Analytical Method: SM 25400 Total Suspended Solids NO mg/L 2.5 1 12/23115 13:38 9040 pH Analytical Method: EPA 9040 pH 6.2 Sid. Units 0.10 1 12/21/15 11:15 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except m full, Date: 12/30I2015 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 20 (�55'ceAnalyNcal' ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Project: STORMWATER SAMPLING Pace Project No.: 92280576 Sample: SW03-121715C Lab ID: 92280576003 Collected: 12/1711507:35 Received: 12/18/1510:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO mglL 5.0 1 12/30115 05:04 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper ND ug/L 5.0 1 12/21/1518:00 12/24/1504.45 7440-50-8 Lead ND ug/L 5.0 1 12121/1518:00 1212411504:45 7439-92-1 Zinc 12.8 ug/L 10.0 1 12/21/15 18:00 12/24/15 04:45 7440-66-6 2540D Total Suspended Solids Anatytini Method: SM 2540D Total Suspended Solids NO mg/L 5.1 1 12/23/15 13:39 9040 pH Analytical Method: EPA 9040 pH 6.5 Std. Units 0.10 1 12/21/1511:15 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2015 04:10 PM without the wntlen consent of Pace Analytical Services, Inc.. Page 10 of 20 aceAnalytical e ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 Project: STORMWATER SAMPLING Pace Project No.: 92280576 Sample: SW04-121715D Lab ID: 92280576004 Collected: 12/17/15 07:45 Received: 12/18/15 10:30 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO mg/L 5.0 1 12130/15 05:04 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper NO ug/L 5.0 1 12121/15 18:00 1224/15 04:48 744050-8 Lead NO ug/L 5.0 1 12/21/1518:00 12/24/1504:48 7439-92-1 Zinc 20.1 ug/L 10.0 1 12121/1518:00 122411504:48 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 25400 Total Suspended Solids 3.3 mg/L 2.5 1 12/23/15 13:40 9040 pH Analytical Method: EPA 9040 pH 6.6 Sid. Units 0.10 1 1222/1515:25 D6,H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2015 0410 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 20 aceAnaly ical e avw.pac,alah&axn QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincay Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Project: STORMWATER SAMPLING Pace Project No.: 92280576 OC Batch: GCSV/23704 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92280576001, 92280576002, 92280576003, 92280576004 METHOD BLANK: 1638918 Matrix: Water Associated Lab Samples: 92280576001, 92280576002, 92280576003, 92280576004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L NO 5.0 12/30/15 04:59 LABORATORY CONTROL SAMPLE & LCSD: 1638919 1638920 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Oil and Grease mg/L 40 38.0 38.6 95 96 78-114 2 30 Raves p aanted on this page ara in the unite indirab by t 'UnW oMtnnn except wore an alMrnaM unit is pteaenWi M t dgM of Me raautt REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, Date: 12/30/2015 04:10 PM without the written consent of Pace Analytical Services, Inc. Page 12 of 20 ace Analytical" wwwpemtshamm QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92280576 QC Batch: MPRPI20342 Analysis Method: EPA 200.7 OC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92280576001, 92280576002, 92280576003, 92280576004 METHOD BLANK: 1634423 Matrix: Water Associated Lab Samples: 92280576001, 92280576002, 92280576003, 92280576004 Blank Reporting Parameter Units Result Limit Analyzed Copper ug/L NO 5.0 1224/1510:20 Lead ug/L ND 5.0 1224/1510:20 Zinc ug/L ND 10.0 1224/1510:20 Qualifiers Pave Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1634424 Spike LCS 1-CS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Copper ug/L 500 475 95 85-115 Lead ug/L 500 465 93 85-115 Zinc ug/L 500 463 93 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1634425 1634426 MS MSD 92280569001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conic. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L NO 500 500 477 478 95 95 70-130 0 Lead ug/L ND 500 500 254 242. 51 48 70-130 5 M1 Zinc ug/L 10.1 500 500 430 444 84 87 70-130 3 Results presented on this Papa am in the units indicated by Me 'Units' column aacapt whom an altamats unit is pica ndaut to the dpet of Um result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/302015 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 20 aceAnaly ical" aw.pr�lehAmm QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92280576 QC Batch: WET/42146 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92280576001, 92280576002, 92280576003, 92280576004 METHOD BLANK: 1636284 Matrix: Water , Associated Lab Samples: 92280576001, 92280576002, 92280576003, 92280576004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mill- NO 2.5 12/23/15 13:30 LABORATORY CONTROL SAMPLE: 1636285 Spike LCS LCS Parameter Units Conn Result % Rec Total Suspended Solids mg/L 250 252 101 SAMPLE DUPLICATE: 1636286 92280529041 Dup Parameter Units Result Result RPD Total Suspended Solids mglL 8920 9400 SAMPLE DUPLICATE: 1636287 92280576003 Dup Parameter Units Result Result RPD Total Suspended Solids mg/L NO NO 5 Pace Artatocal Services, Inc 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (7D4)8759092 % Rec Limits Qualifiers 90-110 Qualifiers Qualifiers Rasulle praserttetl on this page are In the units Imitated by Me 'Units- Column except e4pra an alternate unit is presentee ro the right of Me resuh. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 121302015 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 20 aceAnalytical ewepaceabswm QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER SAMPLING Pace Project No.: 92280576 QC Batch: WETI42094 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92280576001, 92280576002, 92280576003 SAMPLE DUPLICATE: 1634108 92280338001 Cup Parameter Units Result Result RPD Qualifiers PH Std. Units 8.6 8.6 0 H6 Resuas presentee on Nm page am in Ma units indicawcl by the 'Units' column except M an alWor ms unit m amsenled to the dgM of No result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12t302015 04:10 PM wiNout the written consent of Pace Analytical Services, Inc.. Page 15 of 20 aceAnalytical eaxpecelafmcom Project: STORMWATER SAMPLING Pace Project No.: 92280576 QC Batch: WET142121 QC Batch Method: EPA 9040 Associated Lab Samples: 92280576004 SAMPLE DUPLICATE: 1635112 Parameter Units pH Sid. Units QUALITY CONTROL DATA Analysis Method: EPA 9040 Analysis Description: 9040 pH 92280576004 Dup Result Result RPD Qualifiers 6.6 6.7 2 D6,H6 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results prasenta4 on this page an in the unite mdicat by the'Unae' column except whore an aliamals unit is presanteC to Ute right al that MUM REPORT OF LABORATORY ANALYSIS This report shall net be reproduced, except in full, Date: 12/30/2015 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 20 (�15'ceAnalyfical arw.p�it= QUALIFIERS Project: STORMWATER SAMPLING Pace Project No.: 92280576 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MOIL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 9800 Kircey Ave. Suite 100 Huntersviae, NC 28078 (704)075-9092 S - Surrogate - 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data am displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) OUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chlomethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenyfamine using Method 8270. The result reported for each anatyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. H6 Anatysis initiated outside of the 15 minute EPA recommended holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12I302015 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 20 e aceAnalytical aww.paah6c— QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: STORMWATER SAMPLING Pare Project No.: 92280576 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntetsville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 97280576001 SW01-121715A EPA 1664B GCSV/23704 92280576002 SW02-121715B EPA 1664E GCSV/23704 92280576003 SW03-121715C EPA1664B GCSV/23704 92280576004 SW04-121715D EPA 1664B GCSV/23704 92280576001 SW0I-121715A EPA 200.7 MPRP/20342 EPA 200.7 92280576002 SW02.121715B EPA 200.7 MPRP/20342 EPA 200.7 92280576003 SW03-121715C EPA 200.7 MPRP/20342 EPA 200.7 92280576004 SW04-121715D EPA 200.7 MPRP/20342 EPA 200.7 92280576001 SWOt-121715A SM 2540D WET/42146 92280576002 SW02-121715B SM 2540D WET/42146 92280576003 SW03-121715C SM 2540D WET/42146 92280576004 SW04-121715D SM 2540D WET/42146 92280576001 SWOt-121715A EPA 9040 WET/42094 92280576002 SW02-121715B EPA 9040 WET/42094 92280576003 SW03-121715C EPA 9040 WET/42094 92280576004 SW04-121715D EPA 9040 WET/42121 Dale: 12/302015 04:10 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch ICP/18362 ICP/18362 ICP/18362 ICP/18362 Page 18 of 20 Document Name: _ Document Revised: 2�(OC Sample Condition Upon Recei t(SCUR) Page i of T aceAnalytical Document No.: Issuing Authority: F-CHR-CS-003-rev.17 Pace Huntersvllle Quality I Client Name: Projectp: W®# , 92280576 .�a� I�i �'' �Aj��11 Courier: Lltf ecr Ex LJUPS ❑USPS Client tllll� ��II I�III ❑Commercial ❑Pace ❑Other: 92280576 Custody Seal an Cooler/Box Present? []Yes !o Seals Intact? ❑Yes No I: - Packing Material:�E5B bu ble Wrap ubble Bags []None[:]Other:Thermometer J! 1505 - Used: Type of ice: Wet ❑Blue [I, None .:`. �mples on Ice, cooling process has begun Cooler Temp Corrected('C)i 3.S Biological Tissue Frozen? ❑Yesgr.ONo.,. N/A Temp should be above fre g to 6°C Conection Factor. 0.0'C Date and Initiate of Person Examining.Conteiits:: C WAS USDA Regulated Soil ( N/A, water sample) Did samples originate In a quarantine zone within the United States: CA, NY, or SC ([heck maps)? Did samples originate from afareign source (internationally ❑Yes No including Hawa`u and Puehu RJ )?:..: ❑Yes 9;T If Yes to either question, RII out a Regulated Soil Checklist and Include with 6CUR/COC paperwork. COMMENTS:. Chain of Custody Present? Yes []No ❑N/A 1. Chain of Custody Filled Out? GKI ❑No ❑N/A 2. Chain of Custody Relinquished? ❑No ❑N/A 3. Sampler Name and/or Signature on COL? ,...,Ties Lyres []No ❑N/A 4. Samples Arrived within Hold Time? es❑�,/No Short Hold Time Analysis (<72 hr)? ❑Yes 3K 0� ❑N/A 6. Turn Rush Turn Around Time Requested? []Yes Yes ❑N/A 7. Sufficient Volume? es ❑No ❑N/A B. Correct Containers Used? es [:IN, ❑N/A 9. ' -Pace Containers Used Yes EINO ❑N/n Containers Intact? es ON. ❑N/A 0. Filtered Volume Received for Dissolved Tests? ❑Y ❑No /A 11. Note if sediment is visible in the dissolved container Sample Labels Match COC? Yes ❑No ❑N/A 12. 1. -Includes Date/Time/10/Analysis Matrix: W` All containers needing acid/base preservation have been checked? Yes [:]No ❑N/AAll containers needing preservation are found to be in compliance with EPA recommendation? (HNO3, HrSOr, H0<2; NaOH >9 Sulfide, NaOH>12 Cyanide) CKYes ❑No ❑N/A Exceptions: VOA, Coliform, TOC, Oil and Grease, DROJBOIS (water) DOC,LLH Yes No ❑N/A - Samples checked for dechlorization ❑yes ❑No /A 14. Heads ace In VOAVia6(>5-6mm)? ❑Yes []NO /A 15. - -- --" ---"- Trip Blank Present? []Yes ❑No /A 16. - - Trip Blank Custody Seals Present? ❑Yes []No /A Pace Trip Blank Lot W (if purchased): CLIENT NOTIFICATION/RESOLUTION •- Field Data�Required? ❑Yes ❑No Person Contacted: Comments/Resolution: Date/Time: - Project Manager SCURF Review: 6R Z 11-121 /// I Date: tZ`/ Note: Whenever there ha discrepancy affecting North Caro na compliance samples, a copy of this form will be sent to the North Carolina DEHNR Cert"diradon Office (i.e. Out of hold, Incorrect preservative, out of temp, incorrect containers). Page 19 of 20 Pec Analytical° CHAIN -OF -CUSTODY / Analytical Request Document o The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant field$ must Be completed a=ralely. N O 0 Section A Section B Section C P°0°I of Required Clicnl Information: Required ProjecInformation: Invoice Information: Company Report To: Aaem an ,� J) C 2000366 Atldma: O C Copy Te: Lompe am RE LATORY AGENCY Adtlms J FNNPDES F- GROUNDWATER (- DRINKING WATER F UST r RCRA r' OTHER EmaN To:plr Purcnasa Omcr Na.: aC•J L� Romr. coa Phone: f Pmlecl N°m0✓y Mro. Pa Icn I Site Location Wa q J STATE: y equested Duo DWO/TAT: Project Number. Pam Pmlm P: O Requested Analysis Filtered (YIN) Section D MBMa Lodes - `s a' y s RegWrod Cllonl blormoam Mnmlx I cope 9 6 COLLECTED Preservatives i Drinkirp Water DW Water WT � O Waale Water WaY CpAfp$IlE ev.Nt WMMSIIE Eromwe Product P $ro$ J Z SBEISolid SL SAMPLE ID wa t EyJ $ w w f P. (AZ,09/:) Air AR i Semple ID. MUST BE UN IOUE Tissue IS O a. Other OT U X Z wJ La z O 2 y IS - C N S= S O Z a 00.7E TIME DAiF.- TIME 2 O I JXIa Project Nod Lab I.D. T S _ I I % f615ace O%;1 JC x AlA '� 2 wP—a—I C� I JEff:i VIM' 4 M It I ) S 5w o 3— G -j , y a It 1 419 9191 1 1 ° 5 6 7 S 9 10 it 12 ADDITIONAL COMMENTS EUNOUISNED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS 0?l7./S , -' ..: �Z• It d 35 V ORIGINAL SAMPLER NAME AND SIGNATURE O c S PRINT Name of SAMPLER: C , cR e U N SIGNATURE oiSAMPL - _ / E OAT Sl6nodIMMBDDmI. 'bnporlanl NMu: By alpning Illb lonnyou aramg me Peens NET ap MyIaymonl w.n.avid egrgmnp le lab d. mgiof 1.5%putrromh Im nnyimro:wa.1 PICe wm,nWM,. F-ALL."20rev.07, 15-May-2007 BI w NC®ENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidanceonfilling out thisform,please visit: htto//portalncdenrorg/web/wahvs/au/nodessw#tab-4 Permit No.: N/C/ G/0 / 3/ 0/ 0/ 0/ 0/ or Certificate of Coverage No.: Facility Name: Parker Hannifin -Gear Pump Division County: Cleveland/Gaston Phone No. 704-730-2000 Inspector: Robert Simpson Date of Inspection: 12/17/2015 Time of Inspection: 7715 AM (Outfall No. 1) Total Event Precipitation (inches): 1.25 Was this a "Representative Storm Event' or "Measureable Storm Event" as defined by the permit? (See information below.) ® Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event' or during a "measureable storm event" However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event' is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, Iyertifythis re t is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Page 1 of 2 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. 1 Structure (pipe, ditch, etc.) Receiving Stream: McGill Creek Describe the industrial activities that occur within the outfall drainage area: Gear pumo manufacturing, parking lot frontage road runoff. 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: clear, light 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): None 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: lO 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of Floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids: O 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: Ol 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 - NC®ENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisform, please visit: htto //oortal.ncdenr org/web/wq/ws/su/nodessw#tab-4 Permit No.: N/C/ G/0 / 3/ 0/ 0/ 0/ 0/ or Certificate of Coverage No.: Facility Name: Parker Hannifin -Gear Pump Division County: Cleveland/Gaston Phone No. 704-730-2000 Inspector: Robert Simpson Date of Inspection: 12/17/2015 Time of Inspection: 712S AM (Outfal] No. 2) Total Event Precipitation (inches): 1.25 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ® Yes ❑ No Please verify whether Qualitative Monitoring mustbe performed during a "representative storm event' or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. i A "measurable storm event' is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify th,#f this reps is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Pagel of 2 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. 2 Structure (pipe, ditch, etc.) Receiving Stream: McGill Creek Describe the industrial activities that occur within the outfall drainage area: Gear pump manufacturing, parking lot frontage road runoff. 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: clear. light 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): None 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: O2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of Floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids: O2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: G2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 NC®ENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisform, please visit: htto://oortalncdenrorg/web/wa/ws/su/nodessw#tab-4 Permit No.: N/C/ G/0 / 3/ 0/ 0/ 0/ 0/ or Certificate of Coverage No.: Facility Name: Parker Hannifin -Gear Pump Division County: Cleveland/Gaston Phone No. 704-730-2000 Inspector: Robert Simpson Date of Inspection: 12/17/2015 Time of Inspection: 7:35 AM (Outfall No. 3) Total Event Precipitation (inches): 1.25 Was this a "Representative Storm Event' or "Measureable Storm Event" as defined by the permit? (See information below.) ® Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. i A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the j permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office_ By this (Signature of certify,t N report or Designee) and complete to the best of my knowledge: SWU-242, Last modified 10/25/2012 Page 1 of 2 1. Outfall Description: Outfall No. 3 Structure (pipe, ditch, etc.) Receiving Stream: McGill Creek Describe the industrial activities that occur within the outfall drainage area: Gear pump manufacturing, parking lot frontage road runoff. 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: clear, light 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): None 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: lO 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids: Ol 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: Ol 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 tr NC®ENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisjorm, please visit: htto //portal ncdenr ore/web/wq/ws/su/npdessw#tab-4 Permit No.: N/C/ G/0 / 3/ 0/ 0/ 0/ 0/ or Certificate of Coverage No.: Facility Name: Parker Hannifin -Gear Pump Division County: Cleveland/Gaston Phone No. 704-730-2000 Inspector: Robert Simpson Date of Inspection: 12 17/2015 Time of Inspection: 7:45 AM (Outfall No.4) Total Event Precipitation (inches): 1.25 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ® Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event" However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event' is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains'approval from the local DWQ Regional Office. By this signature, I certify thatbis report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Pagel of 2 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. 4 Structure (pipe, ditch, etc.) Receiving Stream: McGill Creek Describe the industrial activities that occur within the outfall drainage area: Gear pum j2 manufacturing, parking lot frontage road runoff. 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: clear. light 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): None 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: lO 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: Ol 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: Ol 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe None Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012