HomeMy WebLinkAboutNCG030296_COMPLETE FILE - HISTORICAL_20161031STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
DOC TYPE
217HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE
❑ a0/ (P I Q 3 }
YYYYM M DD
aceAnalyifcal
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October 21, 2016
Robert Simpson
Parker Hannifin Corporation
101 Canterbury Rd.
Kings Mountain, NC 28086
RE: Project: STORMWATER
Pace Project No.: 92315897
RLCEIVED
OCT 31 2016
CENTRAL FILES
DWR SECTION
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntemille. NC 28078
(704)875-9092
Dear Robert Simpson:
Enclosed are the analytical results for sample(s) received by the laboratory on October 13, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
c qyl `$cu oni
Angela Baioni
angela.baioni@pacelabs.com
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 19
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CERTIFICATIONS
Project: STORMWATER
Pace Project No.: 92315897
Pace Analytical Services, LLC
98001Gncey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
VirginialVELAP Certification #: 460221
Asheville Certification IDs
'2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
This report shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, LLC. Page 2 of 19
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project:
Pace Project No.:
STORMWATER
92315897
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92315897001
SW01.100716A
EPA 1664B
JMS
1
PASI-C
EPA200.7
JMW
3
PASI-A
SM 2540D
MJSt
1
PASI-A
EPA 9040
ALC
1
PASI-A
92315897002
SW02.100716B
EPA1664B
JMS
1
PASI-C
EPA 200.7
JMW
3
PASI-A
SM 2540D
MJSt
1
PASI-A
EPA 9040
ALC
1
PASI-A
92315897003
SW03-100716C
EPA 1664B
JMS
1
PASI-C
EPA 200.7
JMW
3
PASI-A
SM 2540D
MJSt
1
PASI-A
EPA9040
ALC
1
PASI-A
92316897004
SW04-100716D
EPA 1664E
JMS
1
PASI-C
EPA 200.7
JMW
3
PASI-A
SM 2540D
MJSt
1
PASI-A
EPA 9040
ALC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the witten consent of Pace Analytical Services, LLC. Page 3 of 19
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PROJECT NARRATIVE
Project: STORMWATER
Pace Project No.: 92315897
Method:
EPA 1664E
Description:
HEM, Oil and Grease
Client:
Parker Hannifin Corporation
Date:
October 21, 2016
Pace Analytical Services, LLC
9900 Kincey Ave. Suite 100
Huntersville, NC 29078
(704)975-9092
General Information:
4 samples were analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPOs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 19
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Project: STORMWATER
Pace Project No.: 92315897
Method:
EPA 200.7
Description:
200.7 MET ICP
Client:
Parker Hannifin Corporation
Date:
October 21, 2016
Pace Analytical Services, LLC
9800 Kncey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
General Information:
4 samples were analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (Including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 19
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I
PROJECT NARRATIVE
Project: STORMWATER
Pace Project No.: 92315897
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: Parker Hannifin Corporation
Date: October 21, 2016
Pace Ana"cal Services, LLC
98001Gncey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
General Information:
4 samples were analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: 333072
D6: The precision between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1845850)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 19
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PROJECT NARRATIVE
Project: STORMWATER
Pace Project No.: 92315897
Method:
EPA 9040
Description:
9040 pH
Client:
Parker Hannifin Corporation
Date:
October 21, 2016
Pace Analytical Services, LLC
98001Wcey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
General Information:
4 samples were analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
HIS: Analysis initiated outside of the 15 minute EPA required holding time.
• SW01-100716A (Lab ID: 92315897001)
• SW02-100716B (Lab ID: 92315897002)
• SW03-100716C (Lab ID: 92315897003)
• SW04-100716D (Lab ID: 92315897004)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 19
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: STORMWATER
Pace Project No.: 92315897
Sample: SW01-100716A Lab ID: 92315897001 Collected: 10/07/16 10:15 Received: 10/13/16 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg/L
5.0
1
10/21/16 08:45
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation
Method:
EPA 200.7
Copper
NO ug/L
5.0
1 10/1411620:10
10/16/1610:55 7440-50-8
Lead
NO ug/L
5.0
1 10/14/16 20:10
10/16/16 10:55 7439-92-1
Zinc
13.6 ug/L
10.0
1 10/14/16 20:10
10/16/16 10:55 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND mg/L
5.0
1
10/13/16 17:12
9040 pH
Analytical Method: EPA 9040
pH
7.2 Sid. Units
0.10
1
10/17/16 15:13 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/21/2016 04:42 PM i. without the mitten consent of Pace Analytical Services, LLC. Page 8 of 19
Pace Analytical Services, LLC
5ace 9800 Kincey ve. 100
Amlytical Hunterslle, NCte 28078(704)875-9092
I
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92315897
Sample: SW02-10071613
Lab ID: 92315897002 Collected: 10/07/16
10:15
Received* 10113116 10:00 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qua]
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mg/L
5.0
1
10/21116 08:45
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper
NO ug/L
5.0
1
10/14/16 20:10
10/16/16 10:58
7440-50-8
Lead
NO ug/L
5.0
1
1011411620:10
10/1611610:58
7439-92-1
Zinc
24.2 ug/L
10.0
1 .
10/14/16 20:10
10/16/16 10:58
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
NO mg1L
2.5
1
10/13/16 17,12
9040 pH
Analytical Method: EPA 9040
pH
6.1 Std. Units
0.10
1
10/17/16 15:13
H6
Date: 10/21/2016 04:42 PM
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
without the written consent of Pace Analytical Services, L-C.
Page 9 of 19
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvdle, NC 28078
(704)875-9092
Project: STORMWATER
Pace Project No.: 92315897
Sample: SW03-100716C Lab ID: 92315897003 Collected: 10/07/16 10:15 Received: 10/13/16 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
HEM, Oil and Grease
Oil and Grease
200.7 MET ICP
Copper
Lead
Zinc
2540D Total Suspended Solids
Total Suspended Solids
9040 pH
pH
Date: 10/21/2016 04:42 PM
Analytical Method: EPA 1664B
ND mg/L
5.0
1
10/21/1608:45
Analytical Method: EPA 200.7 Preparation Method:
EPA 200.7
NO ug/L
5.0
1 10/14/16 20:10
10/16116 11:02 7440-50-8
NO ug/L
5.0
1 10/14/16 20:10
10/16116 11:02 7439-92-1
17.4 ug/L
10.0
1 10/14116 20:10
10/16/16 11:02 7440-66-6
Analytical Method: SM 2540D
2.9 mg/L
2.5
1
10/13/16 17:12
Analytical Method: EPA 9040
6.5 Sid. Units
0.10
1
10/17/16 15:13
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L-C.
H6
Page 10 of 19
Pace Analytical Services, LLC
aceftlytical a 9800 Kincey Ave. Suse 100
Muntersville, NC 28078
I .parolebaoom (704)875-9092
I
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92315897
Sample: SW04-100716D Lab ID: 92315897004 Collected: 10/07/16 10:15 Received: 10/13/16 10:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg/L
5.0
1
10/21/16 08:45
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper
6.0 ug/L
5.0
1 10/14/16 20:10
10/16/16 11:05 7440-50-8
Lead
NO ug/L
5.0
1 10/14/16 20:10
10/16/16 11:05 7439-92-1
Zinc
35.6 ug/L
10.0
1 10/14/16 20:10
10/16/16 11:05 7440-66-6
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
15.9 mg/L
3.1
1
10/13/16 17:13
9040 pH
Analytical Method: EPA 9040
pH
6.6 Std. Units
0.10
1
10/17/16 15:13 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/21/2016 04:42 PM without the written consent of Pace Analytical Services, L-C. Page 11 of 19
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
980(i nnoey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: STORMWATER
Pace Project No.: 92315897
=
QC Batch: 334036
Analysis Method:
EPA 1664B
QC Batch Method: EPA 16643
Analysis Description:
1664 HEM, Oil and Grease
Associated Lab Samples: 92315897001, 92315897002, 92315897003, 92315897004
METHOD BLANK: 1851541
Matrix: Water
Associated Lab Samples: 92315897001, 92315897002, 92315897003, 92315897004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Oil and Grease
mg/L
NO 5.0 10/21/16 08:45
LABORATORY CONTROL SAMPLE:
1851542
Spike LCS
LCS %Rec
Parameter
Units
Conic. Result
%Rec Limits Qualifiers
Oil and Grease
mg/L
40 37.6
94 78-114
MATRIX SPIKE SAMPLE:
1851543
92315825004 Spike
MS MS % Rec
Parameter
Units
Result Conic.
Result %Rec Limits Qualifiers
Oil and Grease
mg/L
ND 40
35.2 88 78-114
Results presented on this page are In the units Indicated by the 'Units' column except where an ahemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/21/2016 04:42 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 19
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntenville, NC 28078
(704)875-9092
Project: STORMWATER
Pace Project No.: 92315897
OC Batch: 333145
Analysis Method: EPA
200.7
QC Batch Method: EPA200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 92315897001, 92315897002,
92315897003, 92315897004
METHOD BLANK: 1846078
Matrix:
Water
Associated Lab Samples: 92315897001, 92315897002,
92315897003, 92315897004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Copper
ug/L
ND 5.0
10/16/1610:16
Lead
ug/L
NO 5.0
10/16/1610:16
Zinc
ug/L
NO 10.0
1011611611:41
LABORATORY CONTROL SAMPLE:
1&46079
Spike
LCS
LCS %Rae
Parameter
Units
Cone.
Result
% Rae Limits Qualifiers
Copper
ug/L
500
502
100 85-115
Lead
ug/L
500
484
97 85-115
Zinc
ug/L
500
503
101 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1846080
1846081
MS
MSD
92315630005
Spike
Spike MS
MSD MS MSD
% Rae
Parameter
Units Result
Cone.
Cone. Result
Result % Rec % Rae
Limits
RPD Qual
Copper
ug/L 0.0062
500
500 513
517 101 102
70-130
1
mg/L
Lead
ug/L ND
500
500 466
471 93 94
70-130
1
Zinc
ug/L ND
500
500 498
505 98 99
70-130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1846082
1846083
MS
MSD
92315938002
Spike
Spike MS
MSD MS MSD
%Rec
Parameter
Units Result
Cone.
Cone. Result
Result % Rae % Rae
Limits
RPD Oual
Copper
ug/L NO
500
500 499
497 99 99
70-130
0
Lead
ug/L NO
500
500 469
472 94 94
70-130
1
Zinc
ug/L 486
500
500 965
968 96 97
70-130
0
Results presented on this page are In the units Indicated by the 'Units' column except where an axemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 10/21/2016 04:42 PM without the wnften consent of Pace Analytical Services, L-C. Page 13 of 19
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: STORMWATER
Pace Project No.: 92315897
QC Batch: 333072
Analysis Method: SM 2540D
QC Batch Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92315897001, 92315897002, 92315897003, 92315897004
METHOD BLANK: 1845847
Matrix: Water
Associated Lab Samples: 92315897001, 92315897002, 92315897003, 92315897004
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Suspended Solids
mg/L
ND 2.5 10/13/16 17:11
LABORATORY CONTROL SAMPLE:
1845848
Spike LCS 1-CS h Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 238 95 90-110
SAMPLE DUPLICATE: 1845849
92315897001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
ND ND
SAMPLE DUPLICATE: 1845850
92315630001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
93.3 103 10 D6
Resuha presented on this page are In the units Indicated by the "Units" column except where an akemate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 10/21/2016 04:42 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 19
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QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92315897
QC Batch: 333423 Analysis Method: EPA 9040
OC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92315897001, 92315897002, 92315897003, 92315897004
SAMPLE DUPLICATE: 1847788
92315235001 Dup
Parameter Units Result Result RPD Qualifiers
pH Sid. Units 7.1 7.2 1 H6
SAMPLE DUPLICATE: 1847789
92315307006 Cup
Parameter Units Result Result RPD Qualifiers
pH Sid. Units 6.9 7.0 0 H6
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Results presented on this page are In the units Indicated by the'dnits' column except where an alternate unit is presented to me dam of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/21/2016 04:42 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 19
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QUALIFIERS
Project: STORMWATER
Pace Project No.: 92315897
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Ouantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
98001Gncey Ave. Suite 100
Hunlersville, NC 28078
(704)875-9092
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each anayte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPO - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited anayles.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
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Date: 10/21/2016 04:42 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 19
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)879-9092
Project:
Pace Project No.:
STORMWATER
92315897
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92315897001
SW01-100716A
EPA 16646
334036
92315897002
SW02-100716B
EPA 1664B
334036
92315897003
SW03-100716C
EPA 1664E
334036
92315897004
SW04-100716D
EPA 1664B
334036
92315897001
SW01-100716A
EPA200.7
333145
EPA 200.7
333294
92315897002
SW02.100716B
EPA 200.7
333145
EPA 200.7
333294
92315897003
SW03-100716C
EPA200.7
333145
EPA 200.7
333294
92315897004
SW04-100716D
EPA 200.7
333145
EPA 200.7
333294
92315897001
SW01-100716A
SM 2540D
333072
92315897002
SW02-100716B
SM 2540D
333072
92315897003
SW03.100716C
SM 2540D
333072
92315897004
SW04-100716D
SM 2540D
333072
92315897001
SW01-100716A
EPA9040
333423
92316897002
SW02.100716B
EPA9040
333423
92315897003
SW03-100716C
EPA 9040
333423
92315897004
SW04-100716D
EPA9040
333423
Date: 10/21/2016 04:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Without the written consent of Pace Analytical Services, LLC.
Page 17 of 19
I
1
,
I
i
I
Document Name: Document Revised: Sept. 21, 2016
Sam le Condition U on Recei t(SCUR Page 1 of 2
aceAnalyticW Document No.: Issuing Authority:
F-CAR-CS-033-Rev.00 Pace Quality Office
Client Name:
I A WfD
Project H:
Courier; MFed Ex ❑UPS ❑LISPS ❑Cllent
❑ Commercial [-]Pace []Other:_
Custody Seal Present? ❑Yes
WO#:92315597
1I111I 11I 1111 I1111I1
92315897
ONO 6 L R
Date/Initials Person Examining Contents:
Packing Material: []Bubble Wrap (YBubble Bags ❑None ❑Other:_
Thermometer V. []Blue❑None []Samples on ice, cooling process has begun
I, Gun ID: Type of Ice:
Correction Factor: 0,� Cooler Temp Corrected('C): 0s'% Biological Tissue Frozen? ❑Yes []No❑N/A
Temp should be above fre)ting to VC
USDA Regulated soil (RN/A, water sample)
Did samples �rlginate in a quarantine tone within the United States: CA, NY, or 5C (check maps)? Did samples originate from a foreign source (Intern� tonally,
....., ". m.no f-Tv.. fWNO
R NO Seals Intact? ❑Yes
❑yes sVNO
Comments /Dlscre anc :
Chain of Custody Present?
Y s
No
❑N/A
1.
Samples Arrived within Hold Time?
elye,
❑�No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
[]Yes
[lrJNo
❑N/A
3.
Rush Turn Around Tlme Requested?
❑Yes
No
N/A
4.
Sufficient Volume?
$
No
❑N/A
5:
Correct Containers Used?
Yes
[]No
❑N/A
6.
-Pace Containers Used?
Yes
[]NO
N/A
Containers Intact?
Yes
ONO
N A
7.
Samples Field filtered?
No
NA
B.
Note if sediment is visible in the dissolved container
Sample labels Match COC?
11yes
dyes
ONO
❑N/A
9.
} r F a
c
-Includes Date/Time/ID/Analysis Matrix: '�
A
v ;.1 D t'•e -.
All containers needing acid/base preservatlon have been
SCURF?
�
1✓JYes
[0]No
❑N/Atar�
�:
checked and documented on page tweet
VOA, Coliform, TOC, Oil and Grease, DR013015
Exceptions:
(water) DOC LLHg
Samples checked for dechlorination?
Yes
❑no
❑N/A
11.
Heads ace In VOA Vials >5.6mm)?
QYes
❑No
N/A
12.
❑Yes
ONO
IJZN/A
13.
Trip Blank Present?
gN/A
Trip Blank Custody Seals Present?
[]Yes❑Im
Dery TAn P6n4 1 of u lif nurchatedl-
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepancy:
Project Manager SCURF Review:
Project Manager SRF Review: I
Note: Whenever there Is a discrepancy affecting North Carolina comp
Out of hold, incorrect preservative, out of temp, incorrect containersl
Laboratoryr ceivingsamples:
Asheville Edenn Greenwood
a copy
Huntersville 11
Field Data Required? LJYes UNo
Date/Time:
Date: I 0-13 _1
Date: I 0-t37(0
: sent to the North Carolina OEHNR Certification Office (i.e.
Raleigh❑ MechanicsvllleEl
Page 18 of 19
d CHAIN -OF -CUSTODY I Analytical Request Document
dareNefCta
.._ .. The ChairwbCustotly'a aLEGAL DOCUMENT. All relevam fields must be completed aCryratey.
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June 07. 2016
Robert Simpson
Parker Hannifin Corporation
101 Canterbury Rd.
Kings Mountain, NC 28086
RE: Project: STORMWATER SAMPLING
Pace Project No.: 92298447
Dear Robert Simpson:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite too
Hunlersville, NC 28078
(704)875-9092
I� C & v 300%
dun-54Ae .0-`Z,4(0
RECEIVED
JUN 2 0 MIS
CENTRAL FILES
DWR SECTION
Enclosed are the analytical results for sample(s) received by the laboratory on May 20, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
Container for sample ID 051916B/002 broke on shipment transit, analysis Oil & Grease.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
W,a—
Liamm Harrison
liamm.harrison@pacelabs.com
Project Manager
REPORT OF LABORATORY ANALYSIS
This report shall not W reproduced, except in full,
Without the written consent of Pace Analytical Services, Inc..
Page 1 of 27
aceAnalytical
0 P6cvbbS,mmm
June 07, 2016
Page 2
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 26078
(704)878-9092
Page 2 of 27
ateAnalj6cal
M .pacebb&=
Project: STORMWATER SAMPLING
Pace Project No.: 92298447
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the whiten consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 700
Huntersville, NC 28078
(704)8759092
Page 3 of 27
mAnalytical
w pacafabs can
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project:
Pace Project No.:
STORMWATER SAMPLING
92298447
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92298447001
SW01-051916A
EPA 200.7
CDF
3
PASI-A
SM 2540D
MJP
i
PASI-A
EPA 9040
TEP
1
PASI-A
92298447002
SW02.051916B
EPA 200.7
CDF
3
PASI-A
SM 2540D
MJP
1
PASI-A
EPA 9040
TEP
1
PASI-A
92298447003
SW03-051916C
EPA 200.7
CDF
3
PASI-A
SM 2540D
MJP
1
PASI-A
EPA 9040
TEP
1
PASI-A
92298447004
SW04.051916D
EPA200.7
CDF
3
PASI-A
SM 2540D
MJP
1
PASI-A
EPA 9040
TEP
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 27
aceAnalytical e
e rpxalsbs.con
PROJECT NARRATIVE
Project: STORMWATER SAMPLING
Pace Project No.: 92298447
Method:
EPA 200.7
Description:
200.7 MET ICP
Client:
Parker Hannifin Corporation
Date:
June 07, 2016
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunterswile, NC 28078
(704)875-9092
General Information:
4 samples were analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 27
aceAnalylical a
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PROJECT NARRATIVE
Project: STORMWATER SAMPLING
Pace Project No.: 92298447
Method:
SM 2540D
Description:
2540D Total Suspended Solids
Client:
Parker Hannifin Corporation
Date:
June 07, 2016
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite too
Huntersville, NC 28078
(704)875-9092
General Information:
4 samples were analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDS) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
OC Batch: WET/45099
D6: The precision between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1739746)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 27
aceAnalytical e
xww.pecelabs.cm
PROJECT NARRATIVE
Project: STORMWATER SAMPLING
Pace Project No.: 92298447
Method:
EPA 9040
Description:
9040 pH
Client:
Parker Hannifin Corporation
Date:
June 07, 2016
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
General Information:
4 samples were analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
H6: Analysis initiated outside of the 15 minute EPA required holding time.
• SW01-051916 A (Lab ID: 92298447001)
• SW02-051916 B (Lab ID: 92298447002)
• SW03-051916 C (Lab ID: 92298447003)
• SW04-051916 D (Lab ID: 92298447004)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
withoul the written consent of Pace Analytical Services. Inc..
Page 7 of 27
aceAnalylical e
w w.pboslaas.cam
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project: STORMWATER SAMPLING
Pace Project No.: 92298447
Sample: SWOt-051916A Lab ID: 92298447001 Collected: 05/19/1611:30 Received: 05120/1608:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper
ND ug/L
5.0
1 05/23/16 18:30
05/26/16 00:58 7440-50-8
Lead
ND ug/L
5.0
1 05/23/16 18:30
05/26/16 00:58 7439-92-1
Zinc
19.4 ug/L
10.0
1 05/23/16 18:30
05/26/16 00:58 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
2.6 mg/L
2.5
1
05/24/16 11:47
9040 pH
Analytical Method: EPA 9040
pH
6.7 Sid. Units
0.10
1
05/25/16 11:50 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2016 08:16 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 27
5ceAna1j6ca1
w Pecsbes.cam
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
(704)8759092
Project: STORMWATER SAMPLING
Pace Project No.: 92298447
Sample: SW02-051916 B Lab ID: 92298447002 Collected: 05/19/16 11:30 Received: 05/20/16 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper
ND ug/L
5.0
1 05/2311618:30
05/2611601:50 7440-50-8
Lead
ND ug/L
5.0
1 05/23/1618:30
05/26/1601:50 7439-92-1
Zinc
31.6 ug/L
10.0
1 05/23/16 18:30
05/26/16 01:50 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND mg/L
5.0
1
05/24/16 11:47
9040 pH
Analytical Method: EPA 9040
pH
6.3 Sid. Units
0.10
1
05/25/16 11:50 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2016 08:16 AM without the wdtten consent of Pace Analytical Services, Inc.. Page 9 of 27
aceAnaljftal e
w ..pecembs,com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: STORMWATER SAMPLING
Pace Project No.: 92298447
Sample: SW03-051916 C Lab ID: 92298447003 Collected: 05119/16 11:30 Received: 05/20/16 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
200.7 MET ICP
Copper
Lead
Zinc
2540D Total Suspended Solids
Total Suspended Solids
9040 pH
pH
Date: 06/07/2016 08:16 AM
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
ND ug/L
5.0
1
05/23/16 18:30 05/26/16 01:59 7440-50-8
ND ug/L
5.0
1
05/23/16 18:30 05/26/16 01:59 7439-92-1
24.4 ug/L
10.0
1
05/23/16 18:30 05/26/16 01:59 7440-66-6
Analytical Method: SM 2540D
12.9 mg/L
5.6
1
05/24/1611:47
Analytical Method: EPA 9040
6.6 Sid. Units
0.10
1
05/25/16 11:50 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 27
aceAnalytical a
...Pacekbs.=
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project: STORMWATER SAMPLING
Pace Project No.: 92298447
Sample: SW04.051916 D Lab ID: 92298447004 Collected: 05/19/16 11:30 Received: 05/20/16 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
200.7 MET ICP
Copper
Lead
Zinc
2540D Total Suspended Solids
Total Suspended Solids
9040 pH
pH
Date: 06/07/2016 08:16 AM
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
ND ug/L
5.0
1
05123/1618:30 05/2611602:03 7440-50-8
ND ug/L
5.0
1
05/23/16 18:30 05/26/16 02:03 7439-92-1
18.7 ug/L
10.0
1
05123/1618:30 05126/1602:03 7440-66-6
Analytical Method: SM 2540D
3.7 mg/L
2.5
1
05/2411611:48
Analytical Method: EPA 9040
6.7 Sid. Units
0.10
1
05/25/16 11:50 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, Inc..
Page 11 of 27
aceAnalytical
...pecelebacorn
QUALITY CONTROL DATA
Project: STORMWATER SAMPLING
Pace Project No.: 92298447
UL; batch: MPRP/21798 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92298447001
METHOD BLANK: 1739813 Matrix: Water
Associated Lab Samples: 92298447001
Parameter
Copper
Lead
Zinc
Blank Reporting
Units Result Limit Analyzed
ug/L ND 5.0 05/25/16 23:13
ug/L NO 5.0 05/25/16 23:13
ug/L NO 10.0 05/26/1616:44
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
LABORATORY CONTROL SAMPLE:
1739814
Spike
LCS LCS % Rae
Parameter
Units
Conc.
Result / Rae Limits Qualifiers
Copper
ug/L
500
490 98 85-115
Lead
ug/L
500
456 91 85-115
Zinc
ug/L
500
448 90 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1739815
1739816
MS
MSD
92298144005
Spike
Spike
MS
MSD
MS
MSD
e/ Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rae
e/ Rae
Limits
RPD Qual
Copper
ug/L
25.9
500
500
499
501
95
95
70-130
0
Lead
ug/L
7.4
500
500
434
432
85
85
70-130
0
Zinc
ug/L
59.0
500
500
480
475
84
83
70-130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1739817
1739818
MS
MSD
92298607001
Spike
Spike
MS
MSD
MS
MSD
% Rae
Parameter Units
Result
Cone.
Cone.
Result
Result
% Rae
% Rae
Limits
RPD Qua]
Copper ug/L
9.6
500
500
488
491
96
96
70-130
1
Lead ug/L
NO
500
500
438
437
87
87
70-130
0
Zinc ug/L
41.5
500
500
462
465
84
85
70-130
1
Results presented on this page are In the units indicated by One -Unba^ column except where an alternate unit is presented to One right of Me result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 06/07/2016 08:16 AM without the written consent of Pace Analytical Services, Inc..
Page 12 of 27
aceAnalytical
wrw.pecelebs.can
QUALITY CONTROL DATA
Project: STORMWATER SAMPLING
Pace Project No.: 92298447
u u batch: MPKP/21799 Analysis Method: EPA200.7
OC Batch Method: EPA200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92298447002, 92298447003, 92298447004
METHOD BLANK: 1739819 Matrix: Water
Associated Lab Samples: 92298447002, 92298447003, 92298447004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Copper
ug/L
NO 5.0
05/26/16 01:44
Lead
ug/L
NO 5.0
05/26/16 01:44
Zinc
ug/L
NO 10.0
05126/1601:44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite too
Huntersville, NC 28078
(704)875-9092
LABORATORY CONTROL SAMPLE:
1739820
Spike
LCS LCS % Rec
Parameter
Units
Conic.
Result % Rec Limits Qualifiers
Copper
ug/L
500
483 97 85-115
Lead
ug/L
500
444 89 85-115
Zinc
ug/L
500
429 86 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1739821 1739822
MS MSD
92298447002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conic. Conc. Result Result %Rec % Rec Limits RPD Qual
Copper ug/L ND 500 500 497 479 99 95 70-130 4
Lead ug/L NO 500 500 449 433 90 86 70-130 3
Zinc ug/L 31.6 500 500 461 445 86 83 70-130 3
Results presented on Nis page are In Me units Indicated by Me -Unite' column except where an altemate unit is presented to Me right of Me result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2016 08:16 AM without the written consent of Pace Analytical Services, Inc.. Page 13 of 27
aceAnalytical
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QUALITY CONTROL DATA
Project: STORMWATER SAMPLING
Pace Project No.: 92298447
QC Batch: WET/45099 Analysis Method: SM 2540D
OC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92298447001, 92298447002, 92298447003, 92298447004
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
METHOD BLANK: 1739744 Matrix: Water
Associated Lab Samples: 92298447001, 92298447002, 92298447003, 92298447004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L NO 2.5 05/24/16 11:43
LABORATORY CONTROL SAMPLE: 1739745
Spike LCS LCS %Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 240 96 90-110
SAMPLE DUPLICATE: 1739746
92298318001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 94.0 106 12 D6
SAMPLE DUPLICATE: 1739747
92298447002 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L ND 12.0
Results presented on Mia papa are In Me units Indicated by the 'Units" column except where an alternate unit is presented to Me right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2016 08:16 AM without the written consent of Pace Analytical Services, Inc..
Page 14 of 27
aceAnalytical e
we»:ptrceAh.arn
QUALITY CONTROL DATA
Project: STORMWATER SAMPLING
Pace Project No.: 92298447
QC Batch: WET/45117 Analysis Method: EPA 9040
OC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92298447001, 92298447002, 92298447003, 92298447004
SAMPLE DUPLICATE: 1740634
92298574001 Dup
Parameter Units Result Result RPD Qualifiers
pH Std. Units 7.2 7.2 0 H6
SAMPLE DUPLICATE: 1740635
92298608001 Dup
Parameter Units Result Result RPD Qualifiers
pH Std. Units 7.1 7A 0 H6
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Results presentee on this pair. are In Me units Indicated by Me'Units' column except w ern an alternate unit is presented to Me riBet of Me resuR.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2016 08:16 AM without the written consent of Pace Analytical Services, Inc..
Page 15 of 27
aceAnalytical
..pacel9esmn
QUALIFIERS
Project: STORMWATER SAMPLING
Pace Project No.: 92298447
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
Date: 06/07/2016 08:16 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 27
aceAnalj6cal.
~paces.=
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincay Ave. Suite 100
Huntersville, NC 28078
(704A75-9092
Project:
Pace Project No.:
STORMWATER SAMPLING
92298447
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92298447001
SW0I-051916A
EPA 200.7
MPRP/21798
EPA200.7
ICP/19558
92298447002
SW02-051916E
EPA 200.7
MPRP/21799
EPA200.7
ICP/19559
92298447003
SW03-051916C
EPA 200.7
MPRP/21799
EPA 200.7
ICP/19559
92298447004
SW04-051916D
EPA 200.7
MPRP/21799
EPA 200.7
ICP/19559
92298447001
SWOt-051916A
SM 2540D
WET/45099
92298447002
SW02-051916 B
SM 2540D
WET/45099
92298447003
SW03-051916 C
SM 2540D
WET/45099
92298447004
SW04-051916 D
SM 2540D
WET/45099
92298447001
SW0l-051916A
EPA 9040
WET/45117
92298447002
SW02-051916E
EPA 9040
WET/45117
92298447003
SW03-051916C
EPA9040
WET/45117
92298447004
SW04-051916D
EPA 9040
WET/45117
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2016 08:16 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of 27
I Document Name: Document Revlsed:April 25, 2016
aceAnalytical Sample Condition Upon Receipt(SCUR) Page 1 of 2
i - I Document No.: Issuing Authority:
F-CHR-CS-Dna- 19 Pace Huntersville Quality Office
Client Name: ,, II Paee 2 of 2 for Internal Use ONLY
Pa/K� n Project 1 WO# : 92299447
ann F'n Courier: 0 ed Ex UUPS ❑LISPS ❑Client
❑ Commercial ❑Pace ❑Other: 11111111111111111111111
92298447
Custody Seal Present? ❑Yes ONO Seals Intact? ❑Yes []NO
�� Date/Initials Person Examining Contents s�
Packing Material: ❑Bubble Wrap QBubble Bags ❑None! ❑Other:_
Thermometer: T1505 Type of Ice: Wet 08lue ❑None BSamples on ice, cooling process has begun
Correction Factor: 0.0'C Cooler Temp Corrected ('C): (
<� (- Biological Tissue Frozen? [:]Yes ❑Q No NN'/A
Temp should be above freezing to 6°C
USDA Regulated Sbil (Q N/A, water sample)
Dld samples% Iginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source Qntemay'onally,
❑Yes ❑ry0 including Hawali and Puerto Rico)? ❑Yes ❑(Jo
Comments/Discrepancy:
Chald of CustodyPresent?
ONOA
1.
Samples Arrived within Hold Time?
ONO
2.
Short Hold Time Analysis (<72 hr.)?
WeSONO
3.
Rush Turn Around Time Requested?
4.
Sufficient Volume?
5.
Correct Containers Used?
6.
-Pace Containers Used?
es
ONO
❑N/A
Containers Intact?
❑Y s
ONO '
N/A
7.
Samples Field Filtered?
Oyes
ONO
N/A
8.
Note If sediment Is visible in the dissolved container
Sample Labels Match CDC?
Yes
❑No
❑N/a
9.
-Includes Date/nme/ID/Anal sis Matrix:
All containers needing acid/base preservation have been
10' w'�IMaz
checked? -
❑Ves
ONO
❑N/A
Ail containers needing preservation are found to be In
compliance with EPA recommendation?
(HNDs, HzSO., HCI<2; NaOH >9 Sulfide, NaOH>12 Cyanide)
Oyes
ONO
❑N/A
xnoao".:
Exceptions: VOA, Coliform, TOC, Oil and Grease,
"+urwrr
DRO/8015 (water) DOC,LLHg
❑Yes
ONO
N/A
Samples checked for dechlorination?
❑Yes
ONO
❑N/A
11.
'
Heads ace in VOA Vlals (>5-6mm)?
OYes
ONO
❑N/A
12.
Trip Blank Present?
Oyes
ONO
❑N/A
13.
Trip Blank Custody Seals Present?
❑Yes
ONO
❑N/A
Pace Trip Blank Lot R (if purchased):
[CAI ION RESOUJIION
Person Contacted:
Comments/Sample
Discrepancy:
Project Manager SCURF Review:
Field Data Required? ❑Yes ❑No
Date/Time:
Date: T:ci-C lt.,
Project Manager SRF Review: L..-.it Date: r? j.2-C 1 U
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, Incorrect preservative, out of temp, Incorrect containers)
Page 18 of 27
P ceAnalytical-
ww.aiulrei.[v2
CHAIN -OF -CUSTODY if Analytical Request Document
Th. Chain-of-Cusmtly is a LEGAL DOCUMENT. All relevant fields must be completed accurately. r
N
G
On
Section A Section B
Required Client Informalion: R.qulr.d Protectan: Section C Page: ofCy
CompeOy: Invoice Inform
fteporl To: ABembn: ' / r
Agar ems:/ /[/ Covr To: i 1997260
!/ —m Z r REGU YAGENCY
Addr
! NPDES 7—GROUND WATER i DRINKING WATER
Purchase Ordar NO_ Fn . Rao,mm: /v i UST RCRA OTHER
O `PaWPhil-
®Rt!;d--0Da,. T: PmjCCI Number: Mamup; Site LUCaIIOn
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(A-Z. 9.91: ) AR Samp)C ID. MUST BE UNIQUE Tnaue TS
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7
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ELINOUISHED BY I AFFILIATION
DATE
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ACCEPTED BY I AFFILIATION
DATE
TIME
yzU
SAMPLE CONDITIONS
Gr��'Iv^�
'MWrlam Nd.: By ppnuq has lam Wu a,u>dSpdg P.ce. NET b day paY n apple am
SAMPLER NAME AND SIGNATURE
E
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PRINT Name of SAMPLER: N -
C/y
SIGNATURE of SAMPL DATE Sign 5—
M.,aIY
anmuun ini.e..n........e, y.A
. pcnnMm la any m.urei na wnlw 30 treys. F-ALL-Q-020rev.07. 15-May-2007
ENVOLaboratories
Accurate. Timely. Responsive. Innovative.
4810 Executive Park Court, Suite ill
Jacksonville FL, 32216-6069
Phone: 904.296.3007 FAX: 904.296.6210
Monday, June 6, 2016
Pace Analytical (PA007)
Attn: Liamm Harrison
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
RE: Laboratory Results for
Project Number: Stormwater Sampling, Project Name/Desc: 92298447
ENCO Workorder(s): BZ02257
Dear Liamm Harrison,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, May 24, 2016.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Jacksonville.
Data from outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chris Tompkins
Project Manager
Enclosure(s)
HNX
This report relates only W the sample as re ed by the laboratory, and may only be tepmducal In ful.
Page 20 of 27
page 1 of a
PRO]ECT NARRATIVE
Client: Pace Analytical (PA007)
Project: 92298447
ENCO Project ID: BZ02257
Overview
Cam ti
www.encolabs.com
All samples submitted were analyzed by Environmental Conservation Laboratories, Inc. in accordance with the
methods referenced in the laboratory report. Any particular difficulties encountered during sample handling and
processing will be discussed in the Remarks section below.
Analysis: EPA 1664B
Affected Samples: SW02-051916 B[BZ02257-02]
Sample SW02-051916 was received in the laboratory broken and the analysis was canceled. The client was
notified.
Chris Tompkins
Project Manager
Page 21 of 27
FlNAL This report relates w* to the sample as re W try the latmatory, aM maY o* oe woo .a i ao MI. Pape 2 of 8
W W W.enmlabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SWOT-051916A
Lab ID: BZOM7.01
Sampled:
05/19/16 11:30
Received: 0S/24/16 11:D0
Parameter
EPA 1664E
Hold Date/Time(s)
06/16/16
Prep Date/Time(s)
06/03/16
10:41
An awls Date/Timefsl
06/03/16 17:58
Client ID: SW03-051916C
lab ID: BZ02257-03
Sampled:
05/19/16 11:30
Received: 05/24/16 11:00
Parameter
EPA 1664B
Hold Date/Time(,)
06/16/16
Prep Date/Time(,)
06/03/16
10:41
Analysis Dare/Time(s)
06/03/16 17:58
aletd ID: SW04-051916D
lab ID: BZ02257-04
Sampled:
05/19/16 11:30
Received: 05/24/1611:00
Pammstsl
EPA 16648
Hold Date/Time(,)
06/16/16
Prep Date/Time(s)
06/03/16
10:41
AmWsis Date/Time(sl
06/03/16 17:56
Page 22 of 27
FINAL This report rdata Wy to Me sample as recayed by tte laboratory, and may mN in MI. Page 3 of 8
SAMPLE DETECTION SUMMARY
Has mu Em
3 0.628 1.31
w .encolab&ieem
Me
thod tlste
PA 1664E
�=
Results MES
ma
EQL
thllts M€Y199 Notin
Oil & Grease (HEM)
0.924 3
0.616
1.28
rng/L EPA 16698
aient ID: SW04-051916 D
Lab ID:
SZ02257-04
Analvice
Ri llYi fin
NDL
Em
volu Method N91e2
Oil & Grease (HEM)
1.13 ]
0.619
1.29
m9/L EPA 16648
Page 23 of 27
IINAl ibis report relates only to the sample as re w by the bbaretory, am may only oe reproou in ail. Page 4 of 8
ANALYTICAL RESULTS
Description: SW01-051916 A tab Sample ID: BZ02257-01
Matrix: Water Sampled: 05/19/1611:30
Project: 92298447 Sampled By:
Classical Chemistry Parameters
^-� Jact n,r ¢rcAs>anaryre(AC 4477
Analrte fCAS Numberl Results Flag Multi PE 4DL POE BatCh Method
Oil & Grease (HEM) [C-0007]^ 0.732 1 mg/L 0.262 0.628 1.31 6F03004 EPA 1664B
Description: SW03-051916 C
Matrix: Water
Project: 92298447
Classical Chemistry Parameters
Lab Sample ID: BZ02257-03
Sampled: 05/ 19/ 16 11:30
Sampled By:
Analvte !CAS Numberl Resg]ft Flag Units III Hu ]JZy Batch
Oil & Grease (HEM) [C-0007]^ 0.924 1 mg/L 0.257 0.616 1.28 6F03004
Description: SW04-051916 D Lab Sample I0:BZ02257-04
Matrix: Water Sampled: 05/19/16 11:30
project: 92298447 Sampled By:
Classical Chemistry Parameters
Analvta fCAS Number!
Oil & Grease (HEM) [C-0D07]^
GE N CmP
W Ww.encolabs.com
Received: 05/24/16 11:00
Work Order: BZ02257
Analyzed By NoteI
06/03/1617:58 SMA
Received: 05/24/16 11:00
Work Order: BZ02257
Method ADalnsd am m9lu
EPA 16648 06/03/16 17:58 SMA
Received: 05/24/16 11:00
Work Order: BZ02257
Results flag Sulu l2E Ku Mi. Batch Method Analy[!A BY KRIM
1.13 1 m9/1- 0.258 0.619 1.29 6F03004 EPA 1664E 06/03/16 17:58 SMA
Page 24 of 27
FIW1L This report relates oNy to the sample as r , al by the Wboralory, artl may o* be reprotuc in N8. Page 5 of 8
www.encolabs.com
QUALITY CONTROL DATA
Classical Chemistry parameters - Quality Control
Batch 6F03004 - EPA 1664B
Blank (6F03004-BLKI)
Prepared: 06/03/2016 10:41 Analyzed: 06/03/2016 17:58
Spike Source a/.REC
RPD
Anahrg
Resift
Flag
COL
Units
Level Result %REC t[mits RPD
Limit Notes
Oil & Grease (HEM)
0.622
U
1.30
mg/L
LCS (6F03004-BSI)
Prepared: 06/03/2016 10:41 Analyzed: 06/03/2016 17:58
Spike Source %REC
RPD
Anatvte
Resift
F.Im
P4L
[Ruts
Level Result ^/eREC LImjtf RPD
Limit Notes
Oil & Grease (HEM)
141
5.00
mg/L
160 88 78-114
LCS Dup (6F03004-BSD1)
Prepared: 06/03/2016 10:41 Analyzed: 06/03/2016 17:58
Spike Source %REC
RPD
ADdhfte
Result
Flag
COL
Unib
Level Result %REC Limits RPD
u mit Notes
Oil & Grease (HEM)
137
5.00
mg/L
154 89 78-114 3
18
Matrix Spike (6F03004-MSI)
Prepared: 06/03/2016 10:41 Analyzed: 06/031201617:58
Source: BZ02299-01
Spike Source %REC
RPD
Analvte
Result
Flag
POL
1.101113
Level Result %REC Limits RPD
Limit RR$i
Oil & Grease (HEM)
34.2
1.26
mg/L
40.2 0.604 U 85 78-114
Page 25 of 27
FINAL This report relates only W t sample a$ rx ,fd by the Ial>mto y, and may only lie repro: mW in full. Pape 6 of 8
www.encolab&mrn
FLAGS/NOTES AND DEFINITIONS
B The anatyte was detected in the associated method blank.
D The sample was analyzed at dilution.
I The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyze was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyze is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
N The analysis indicates the presence of an analyze for which there is presumptive evidence (85% or greater
confidence) to make a'tentative identification".
Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
Page 26 of 27
FlNAL Tltls report rdxtes only to tJV sample as r¢eivxl by ttre laboratory, aM may onb be rep� In U. Pape 7 or 8
Chain .ot= Custody
Workorder: 92299447 Workorder Name: SIORMVVATER SAMPLING
Results Requested By: 6/612016
eAnalytical
Report 13nvoice To
L Reqt steflAnalysis,
Liamm Harrison
Pace Analytical Charlotte P.1 Of t4
9800 Kincey Ave. Suite 100 .7
HUntersville, NC 28078
Phone (704)875-9092
7-
Email: fiamm.hamson@pacelabs.com
:,State of Sample Origin; NC 1: Yresomiad Contatners
"Collect
l In
La5lD
Matrix
I
I
LAB USE ONLY
1
SW01-051918 A
511912016 11 30
92298447001
Water
x
2
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5119/2016 11:30
92208447002
wale.
x
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SW03-05191r C
511912016 11 30
92298447003
walm
x
15i19/2016
11:30
9229B 4700
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x
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Transfers
Released By
Date/Time
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I Received on Ice or N Samples lnta
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Friday, May 20. 20113 10.20104 AM
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4
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CHAIN -OF -CUSTODY / Analytical Request Document
The Chain-af-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Required Client Information: Required Project on: Invoice Infomfa'
Company: `n L.G �; Report To: c Attention:
Page: of
1997260
Adtlr �s:/
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Copy To:
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REGU66TC19Y AGENCY .
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Banking Water DW
' Water WT
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SAMPLE ID Oil OL
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(A-Z, D-O l :) Air AIR
Sample IOs MUST BE UNIQUE Tissue. TS
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SIGNATURE of SAMPL
DATE Signed // —/
(MM/DDIYY): J
i1--ALL-0-020rev.07, 15-May-2007
Feb 03, 2016
NPDES General Permit COC: NCG030296
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Hydraulics
Adrian Gutierrez
Engineering Manager
Parker Hannifin Corporation
Gear Pump Division
101 Canterbury Road
Kings Mountain, NC 28086
Tel: (704) 730-5707
Fax: (260)342-4184
RECEIVED
FEB .10 2016
IZENTRAL FILES
UM SECTION
Re: NPDES Stormwater Sampling (YEAR 3, PERIOD 2 Bi-annual results)
Parker Hannifin Corporation
Gear Pump Division
101 Canterbury Road
Kings Mountain, Gaston County, North Carolina 28086
Parker Hannifin Corp. (Parker Hannifin) located at 101 Canterbury Road, Kings
Mountain, Gaston County, North Carolina, is pleased to submit the attached stormwater
sampling results for our facility to meet the NPDES General Permit (COC NCG030296)
stormwater sampling requirements for Year 3, Period 2 sampling. Parker Hannifin
sampled the identified four outfalls at the site on 12/17/15, as per the NPDES General
Permit Requirements. The stormwater samples were analyzed for parameters listed in
Section B Table 1 (pH, Total Suspended Solids, Non -Polar Oil & Grease, Copper, Total
Recoverable Lead, and Total Recoverable Zinc). Total Toxic Organic Compounds
(TTO) were not analyzed since the facility is not categorized as a metal finishing
operation. The rainfall amounts were measured during the rain event and recorded as
required.
Based on the sampling results, the analytical results were below the Benchmark Values
presented in Section B, Table 3 of the Stormwater General Permit.
Respectfully submitted,
Parker Hannifin Co ,
Adrian 'utierrez
Engineering Manager
s
aceAnalytical
w rpacemhamm
December 30, 2015
Robert Simpson
Parker Hannifin Corporation
101 Canterbury Rd.
Kings Mountain, NC 28086
RE: Project: STORMWATER SAMPLING
Pace Project No.: 92280576
Dear Robert Simpson:
Pace Anatocal Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875>9092
Enclosed are the analytical results for sample(s) received by the laboratory on December 18, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
\,�r Pv— cG./vJy—
Liamm Harrison
liamm.harrison@pacelabs.com
Project Manager
Endosures
REPORT OF LABORATORY ANALYSIS
This report shall net be reproduced, except in full,
without the whiten consent of Pace Analytical Services, Inc.
Page 1 of 20
ace Analytical
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Project: STORMWATER SAMPLING
Pace Project No.: 92280576
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
FloridalNELAP Certification #: E87627
Kentucky LIST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. _ Page 2 of 20
aceAnalytical e
SAMPLE ANALYTE COUNT
Pace Ana"cal Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project
Pace Project No.:
STORMWATER SAMPLING
92280576
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92280576001
SW01-121715A
EPA1664B
JMS
1
PASI-C
EPA 200.7
CDF
3
PASI-A
SM 2540D
MDW
1
PASI-A
EPA 9040
MLS
1
PASI-A
92280576002
SW02-1217158
EPA 1664B
JMS
1
PASI-C
EPA 200.7
CDF
3
PASI-A
SM 25400
MDW
1
PASI-A
EPA 9040
MLS
1
PASI-A
92280576003
SW03-121715C
EPA 1664B
JMS
1
PASI-C
EPA 200.7
CDF
3
PASI-A
SM 2540D
MDW
1
PASI-A
EPA9040
MLS
1
PASI-A
92280576004
SW04-121715D
EPA 16648
JMS
1
PASI-C
EPA 200.7
CDF
3
PASI-A
SM 2540D
MDW
1
PASI-A
EPA 9040
MLS
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
vvrff ud the written consent of Pace Analytical Services. Inc.. Page 3 of 20
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PROJECT NARRATIVE
Project: STORMWATER SAMPLING
Pace Project No.: 92280576
Method:
EPA 16648
Description:
HEM, Oil and Grease
Client:
Parker Hannifin Corporation
Date:
December 30, 2015
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
General Information:
4 samples were analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within OC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 4 of 20
aceAnaly6cale
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PROJECT NARRATIVE
Project: STORMWATER SAMPLING
Pace Project No.: 92280576
Method:
EPA 200.7
Description:
200.7 MET ICP
Client:
Parker Hannifin Corporation
Date:
December 30, 2015
Pace Analytl al Services, Inc.
98001Gncey Ave. Suite 100
Huntersville, NC 28078
(704)875s9092
General Information:
4 samples were analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold limes with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All anatytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory controi spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MPRP/20342
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92280569001
Ml: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
MS (Lab ID: 1634425)
• Lead
MSD (Lab ID: 1634426)
• Lead
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 20
e
aceAnalylical
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PROJECT NARRATIVE
Project: STORMWATER SAMPLING
Pace Project No.: 92280576
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: Parker Hannifin Corporation
Date: December 30, 2015
Pave Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
General Information:
4 samples were analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Addidonal Comments
:14;[G ttelSIa1-Zd:7_\I101:ZY/ :I_\W&I1.1
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 20
s
aceAnalytical
...perdehimrn
PROJECT NARRATIVE
Project: STORMWATER SAMPLING
Pace Pmject No.: 92280576
Method:
EPA 9040
Desviption:
9040 pH
Client:
Parker Hannifin Corporation
Date:
December 30, 2015
General Information:
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Hunters ille, NC 28078
(704)8759092
4 samples were analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below or on the
chainof custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
H6: Analysis initiated outside of the 15 minute EPA recommended holding time.
• SW01-121715A (Lab ID: 92280576001)
• SW02-121715E (Lab ID: 92280576002)
• SW03-121715C (Lab ID: 92280576003)
• SW04-121715D (Lab ID: 92200576004)
Method Blank:
All analyfes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within OC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: WET/42121
06: The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1635112)
- pH
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 7 of 20
•
aceAnafytical
w•rpsm'aoamn
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
98001Gncey Ave. Suite 100
Huntersmile, NC 28078
(704)8759092
Project: STORMWATER SAMPLING
Pace Project No.: 92280576
Sample: SW01-121715A Lab ID: 92280576001 Collected: 12/1711507:15 Received: 1211811510,30 Matrix, Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mg/L
5.0
1
12/30/15 05:03
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper
NO ug/L
5.0
1 12/21/1518:00
12124/1504:39 7440-50-8
Lead
ND ug/L
5.0
1 12121/1518:00
12/2411504:39 7439-92-1
Zinc
28.7 ug/L
10.0
1 12121/1518:00
12/24/1504:39 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND mg/L
2.5
1
12123/15 13:38
9040 pH
Analytical Method: EPA 9040
pH
6.4 Std. Units
0.10
1
12/'21/15 11:15 H6
N
REPORT OF LABORATORY ANALYSIS
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Date: 12/30/2015 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 20
aceAnalytical e
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
98001GnceyAve. Suite 100
Huntersville, NC 28078
1704)875-9092
Project: STORMWATER SAMPLING
Pace Project No.: 92280576
Sample: SW02-121715B t.ablD: 92280576002 Collected: 1211711507:25 Received: 12118/1510:30 Matrix: Water
Parameters Results Units Report Limit OF Prepared Anatyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mg/L
5.0
1
12/30/15 05:04
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method:
EPA 200.7
Copper
NO ug/L
5.0
1 12121/1518:00
12/24/1504:42 7440-50-8
Lead
NO ug/L
5.0
1 1212111518:00
12124/1504:42 7439-92-1
Zinc
18.6 ug/L
10.0
1 1212111518:00
1212411504,42 744066-6
2540D Total Suspended Solids
Analytical Method: SM 25400
Total Suspended Solids
NO mg/L
2.5
1
12/23115 13:38
9040 pH
Analytical Method: EPA 9040
pH
6.2 Sid. Units
0.10
1
12/21/15 11:15 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except m full,
Date: 12/30I2015 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 20
(�55'ceAnalyNcal'
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project: STORMWATER SAMPLING
Pace Project No.: 92280576
Sample: SW03-121715C Lab ID: 92280576003 Collected: 12/1711507:35 Received: 12/18/1510:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mglL
5.0
1
12/30115 05:04
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper
ND ug/L
5.0
1 12/21/1518:00
12/24/1504.45 7440-50-8
Lead
ND ug/L
5.0
1 12121/1518:00
1212411504:45 7439-92-1
Zinc
12.8 ug/L
10.0
1 12/21/15 18:00
12/24/15 04:45 7440-66-6
2540D Total Suspended Solids
Anatytini Method: SM 2540D
Total Suspended Solids
NO mg/L
5.1
1
12/23/15 13:39
9040 pH
Analytical Method: EPA 9040
pH
6.5 Std. Units
0.10
1
12/21/1511:15 H6
REPORT OF LABORATORY ANALYSIS
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Date: 12/30/2015 04:10 PM without the wntlen consent of Pace Analytical Services, Inc.. Page 10 of 20
aceAnalytical e
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
(704)875-9092
Project: STORMWATER SAMPLING
Pace Project No.: 92280576
Sample: SW04-121715D Lab ID: 92280576004 Collected: 12/17/15 07:45 Received: 12/18/15 10:30 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mg/L
5.0
1
12130/15 05:04
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method:
EPA 200.7
Copper
NO ug/L
5.0
1 12121/15 18:00
1224/15 04:48 744050-8
Lead
NO ug/L
5.0
1 12/21/1518:00
12/24/1504:48 7439-92-1
Zinc
20.1 ug/L
10.0
1 12121/1518:00
122411504:48 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 25400
Total Suspended Solids
3.3 mg/L
2.5
1
12/23/15 13:40
9040 pH
Analytical Method: EPA 9040
pH
6.6 Sid. Units
0.10
1
1222/1515:25 D6,H6
REPORT OF LABORATORY ANALYSIS
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Date: 12/30/2015 0410 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 20
aceAnaly ical e
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincay Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project:
STORMWATER SAMPLING
Pace Project No.:
92280576
OC Batch:
GCSV/23704 Analysis Method: EPA 1664E
QC Batch Method:
EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples:
92280576001, 92280576002, 92280576003, 92280576004
METHOD BLANK: 1638918 Matrix: Water
Associated Lab Samples: 92280576001, 92280576002, 92280576003, 92280576004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L NO 5.0 12/30/15 04:59
LABORATORY CONTROL SAMPLE & LCSD:
1638919
1638920
Spike
LCS LCSD
LCS LCSD
% Rec Max
Parameter
Units Conc.
Result Result
% Rec % Rec
Limits RPD RPD Qualifiers
Oil and Grease
mg/L 40
38.0 38.6
95 96
78-114 2 30
Raves p aanted on this page ara in the unite indirab by t 'UnW oMtnnn except wore an alMrnaM unit is pteaenWi M t dgM of Me raautt
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 12/30/2015 04:10 PM without the written consent of Pace Analytical Services, Inc.
Page 12 of 20
ace Analytical"
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QUALITY CONTROL DATA
Project: STORMWATER SAMPLING
Pace Project No.: 92280576
QC Batch: MPRPI20342
Analysis Method: EPA 200.7
OC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 92280576001, 92280576002, 92280576003, 92280576004
METHOD BLANK: 1634423
Matrix: Water
Associated Lab Samples: 92280576001, 92280576002, 92280576003, 92280576004
Blank Reporting
Parameter Units
Result Limit
Analyzed
Copper ug/L
NO 5.0
1224/1510:20
Lead ug/L
ND 5.0
1224/1510:20
Zinc ug/L
ND 10.0
1224/1510:20
Qualifiers
Pave Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
LABORATORY CONTROL SAMPLE:
1634424
Spike
LCS 1-CS %Rec
Parameter
Units
Conc.
Result %Rec Limits Qualifiers
Copper
ug/L
500
475 95 85-115
Lead
ug/L
500
465 93 85-115
Zinc
ug/L
500
463 93 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1634425
1634426
MS
MSD
92280569001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conic.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper
ug/L
NO
500
500
477
478
95
95
70-130
0
Lead
ug/L
ND
500
500
254
242.
51
48
70-130
5 M1
Zinc
ug/L
10.1
500
500
430
444
84
87
70-130
3
Results presented on this Papa am in the units indicated by Me 'Units' column aacapt whom an altamats unit is pica ndaut to the dpet of Um result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/302015 04:10 PM without the written consent of Pace Analytical Services, Inc..
Page 13 of 20
aceAnaly ical"
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QUALITY CONTROL DATA
Project: STORMWATER SAMPLING
Pace Project No.: 92280576
QC Batch: WET/42146 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92280576001, 92280576002, 92280576003, 92280576004
METHOD BLANK: 1636284 Matrix: Water ,
Associated Lab Samples: 92280576001, 92280576002, 92280576003, 92280576004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mill- NO 2.5 12/23/15 13:30
LABORATORY CONTROL SAMPLE: 1636285
Spike LCS LCS
Parameter Units Conn Result % Rec
Total Suspended Solids mg/L 250 252 101
SAMPLE DUPLICATE: 1636286
92280529041 Dup
Parameter Units Result Result RPD
Total Suspended Solids mglL 8920 9400
SAMPLE DUPLICATE: 1636287
92280576003 Dup
Parameter Units Result Result RPD
Total Suspended Solids mg/L NO NO
5
Pace Artatocal Services, Inc
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(7D4)8759092
% Rec
Limits Qualifiers
90-110
Qualifiers
Qualifiers
Rasulle praserttetl on this page are In the units Imitated by Me 'Units- Column except e4pra an alternate unit is presentee ro the right of Me resuh.
REPORT OF LABORATORY ANALYSIS
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Date: 121302015 04:10 PM without the written consent of Pace Analytical Services, Inc..
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project:
STORMWATER SAMPLING
Pace Project No.:
92280576
QC Batch:
WETI42094 Analysis Method: EPA 9040
QC Batch Method:
EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92280576001, 92280576002, 92280576003
SAMPLE DUPLICATE: 1634108
92280338001 Cup
Parameter Units Result Result RPD Qualifiers
PH Std. Units 8.6 8.6 0 H6
Resuas presentee on Nm page am in Ma units indicawcl by the 'Units' column except M an alWor ms unit m amsenled to the dgM of No result.
REPORT OF LABORATORY ANALYSIS
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Date: 12t302015 04:10 PM wiNout the written consent of Pace Analytical Services, Inc..
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Project: STORMWATER SAMPLING
Pace Project No.: 92280576
QC Batch: WET142121
QC Batch Method: EPA 9040
Associated Lab Samples: 92280576004
SAMPLE DUPLICATE: 1635112
Parameter Units
pH
Sid. Units
QUALITY CONTROL DATA
Analysis Method: EPA 9040
Analysis Description: 9040 pH
92280576004 Dup
Result Result RPD Qualifiers
6.6 6.7 2 D6,H6
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Results prasenta4 on this page an in the unite mdicat by the'Unae' column except whore an aliamals unit is presanteC to Ute right al that MUM
REPORT OF LABORATORY ANALYSIS
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Date: 12/30/2015 04:10 PM without the written consent of Pace Analytical Services, Inc..
Page 16 of 20
(�15'ceAnalyfical
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QUALIFIERS
Project: STORMWATER SAMPLING
Pace Project No.: 92280576
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MOIL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
9800 Kircey Ave. Suite 100
Huntersviae, NC 28078
(704)075-9092
S - Surrogate -
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data am displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
OUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chlomethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenyfamine using Method 8270. The result reported for
each anatyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
H6 Anatysis initiated outside of the 15 minute EPA recommended holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12I302015 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 20
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: STORMWATER SAMPLING
Pare Project No.: 92280576
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntetsville, NC 28078
(704)875-9092
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
97280576001
SW01-121715A
EPA 1664B
GCSV/23704
92280576002
SW02-121715B
EPA 1664E
GCSV/23704
92280576003
SW03-121715C
EPA1664B
GCSV/23704
92280576004
SW04-121715D
EPA 1664B
GCSV/23704
92280576001
SW0I-121715A
EPA 200.7
MPRP/20342
EPA 200.7
92280576002
SW02.121715B
EPA 200.7
MPRP/20342
EPA 200.7
92280576003
SW03-121715C
EPA 200.7
MPRP/20342
EPA 200.7
92280576004
SW04-121715D
EPA 200.7
MPRP/20342
EPA 200.7
92280576001
SWOt-121715A
SM 2540D
WET/42146
92280576002
SW02-121715B
SM 2540D
WET/42146
92280576003
SW03-121715C
SM 2540D
WET/42146
92280576004
SW04-121715D
SM 2540D
WET/42146
92280576001
SWOt-121715A
EPA 9040
WET/42094
92280576002
SW02-121715B
EPA 9040
WET/42094
92280576003
SW03-121715C
EPA 9040
WET/42094
92280576004 SW04-121715D EPA 9040 WET/42121
Dale: 12/302015 04:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
ICP/18362
ICP/18362
ICP/18362
ICP/18362
Page 18 of 20
Document Name: _ Document Revised: 2�(OC
Sample Condition Upon Recei t(SCUR) Page i of T
aceAnalytical Document No.: Issuing Authority:
F-CHR-CS-003-rev.17 Pace Huntersvllle Quality I
Client Name: Projectp: W®# , 92280576
.�a� I�i �'' �Aj��11
Courier: Lltf ecr Ex LJUPS ❑USPS Client tllll� ��II I�III
❑Commercial ❑Pace ❑Other:
92280576
Custody Seal an Cooler/Box Present? []Yes !o Seals Intact? ❑Yes No I: -
Packing Material:�E5B bu ble Wrap ubble Bags []None[:]Other:Thermometer J! 1505 -
Used: Type of ice: Wet ❑Blue [I, None
.:`.
�mples on Ice, cooling process has begun
Cooler Temp Corrected('C)i 3.S Biological Tissue Frozen? ❑Yesgr.ONo.,. N/A
Temp should be above fre g to 6°C Conection Factor. 0.0'C Date and Initiate of Person Examining.Conteiits:: C WAS
USDA Regulated Soil ( N/A, water sample)
Did samples originate In a quarantine zone within the United States: CA, NY, or SC ([heck maps)? Did samples originate from afareign source (internationally
❑Yes No including Hawa`u and Puehu RJ )?:..: ❑Yes 9;T
If Yes to either question, RII out a Regulated Soil Checklist and Include with 6CUR/COC paperwork.
COMMENTS:.
Chain of Custody Present?
Yes
[]No
❑N/A
1.
Chain of Custody Filled Out?
GKI
❑No
❑N/A
2.
Chain of Custody Relinquished?
❑No
❑N/A
3.
Sampler Name and/or Signature on COL?
,...,Ties
Lyres
[]No
❑N/A
4.
Samples Arrived within Hold Time?
es❑�,/No
Short Hold Time Analysis (<72 hr)?
❑Yes
3K
0�
❑N/A
6.
Turn
Rush Turn Around Time Requested?
[]Yes Yes
❑N/A
7.
Sufficient Volume?
es
❑No
❑N/A
B.
Correct Containers Used?
es
[:IN,
❑N/A
9. '
-Pace Containers Used
Yes
EINO
❑N/n
Containers Intact?
es
ON.
❑N/A
0.
Filtered Volume Received for Dissolved Tests?
❑Y
❑No
/A
11. Note if sediment is visible in the dissolved container
Sample Labels Match COC?
Yes
❑No
❑N/A
12.
1.
-Includes Date/Time/10/Analysis Matrix: W`
All containers needing acid/base preservation have been
checked?
Yes
[:]No
❑N/AAll
containers needing preservation are found to be in
compliance with EPA recommendation?
(HNO3, HrSOr, H0<2; NaOH >9 Sulfide, NaOH>12 Cyanide)
CKYes
❑No
❑N/A
Exceptions: VOA, Coliform, TOC, Oil and Grease,
DROJBOIS (water) DOC,LLH
Yes
No
❑N/A
-
Samples checked for dechlorization
❑yes
❑No
/A
14.
Heads ace In VOAVia6(>5-6mm)?
❑Yes
[]NO
/A
15. - -- --" ---"-
Trip Blank Present?
[]Yes
❑No
/A
16. - -
Trip Blank Custody Seals Present?
❑Yes
[]No
/A
Pace Trip Blank Lot W (if purchased):
CLIENT NOTIFICATION/RESOLUTION •- Field Data�Required? ❑Yes ❑No
Person Contacted:
Comments/Resolution:
Date/Time: -
Project Manager SCURF Review: 6R Z 11-121 /// I Date: tZ`/
Note: Whenever there ha discrepancy affecting North Caro na compliance samples, a copy of this form will be sent to the North Carolina DEHNR Cert"diradon Office (i.e. Out of
hold, Incorrect preservative, out of temp, incorrect containers).
Page 19 of 20
Pec Analytical°
CHAIN -OF -CUSTODY / Analytical Request Document o
The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant field$ must Be completed a=ralely. N
O
0
Section A Section B Section C
P°0°I of
Required Clicnl Information: Required ProjecInformation: Invoice Information:
Company Report To: Aaem an ,�
J) C
2000366
Atldma:
O C
Copy Te:
Lompe am
RE LATORY AGENCY
Adtlms J
FNNPDES F- GROUNDWATER (- DRINKING WATER
F UST r RCRA r' OTHER
EmaN To:plr
Purcnasa Omcr Na.:
aC•J
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Romr. coa
Phone:
f
Pmlecl N°m0✓y
Mro. Pa Icn I
Site Location
Wa
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STATE:
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equested Duo DWO/TAT:
Project Number.
Pam Pmlm P:
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Requested
Analysis
Filtered
(YIN)
Section D MBMa Lodes
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RegWrod Cllonl blormoam Mnmlx I cope
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COLLECTED
Preservatives
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Drinkirp Water DW
Water WT
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Waale Water WaY
CpAfp$IlE
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SAMPLE ID
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ADDITIONAL COMMENTS
EUNOUISNED BY I AFFILIATION
DATE
TIME
ACCEPTED BY I AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
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ORIGINAL
SAMPLER NAME AND SIGNATURE
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PRINT Name of SAMPLER:
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'bnporlanl NMu: By alpning Illb lonnyou aramg me Peens NET ap MyIaymonl w.n.avid egrgmnp le lab d. mgiof 1.5%putrromh Im nnyimro:wa.1 PICe wm,nWM,. F-ALL."20rev.07, 15-May-2007
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NC®ENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidanceonfilling out thisform,please visit: htto//portalncdenrorg/web/wahvs/au/nodessw#tab-4
Permit No.: N/C/ G/0 / 3/ 0/ 0/ 0/ 0/ or Certificate of Coverage No.:
Facility Name: Parker Hannifin -Gear Pump Division
County: Cleveland/Gaston Phone No. 704-730-2000
Inspector: Robert Simpson
Date of Inspection: 12/17/2015
Time of Inspection: 7715 AM (Outfall No. 1)
Total Event Precipitation (inches): 1.25
Was this a "Representative Storm Event' or "Measureable Storm Event" as defined by the permit?
(See information below.)
® Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event' or during a "measureable storm event" However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event' is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, Iyertifythis re t is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
Page 1 of 2
SWU-242, Last modified 10/25/2012
1. Outfall Description:
Outfall No. 1 Structure (pipe, ditch, etc.)
Receiving Stream: McGill Creek
Describe the industrial activities that occur within the outfall drainage area: Gear pumo
manufacturing, parking lot frontage road runoff.
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: clear, light
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
lO 2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of Floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids:
O 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
Ol 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012 -
NC®ENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out thisform, please visit: htto //oortal.ncdenr org/web/wq/ws/su/nodessw#tab-4
Permit No.: N/C/ G/0 / 3/ 0/ 0/ 0/ 0/ or Certificate of Coverage No.:
Facility Name: Parker Hannifin -Gear Pump Division
County: Cleveland/Gaston Phone No. 704-730-2000
Inspector: Robert Simpson
Date of Inspection: 12/17/2015
Time of Inspection: 712S AM (Outfal] No. 2)
Total Event Precipitation (inches): 1.25
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
® Yes ❑ No
Please verify whether Qualitative Monitoring mustbe performed during a "representative storm
event' or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
i
A "measurable storm event' is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify th,#f this reps is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
Pagel of 2
SWU-242, Last modified 10/25/2012
1. Outfall Description:
Outfall No. 2 Structure (pipe, ditch, etc.)
Receiving Stream: McGill Creek
Describe the industrial activities that occur within the outfall drainage area: Gear pump
manufacturing, parking lot frontage road runoff.
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: clear. light
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
O2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of Floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids:
O2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
G2 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012
NC®ENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out thisform, please visit: htto://oortalncdenrorg/web/wa/ws/su/nodessw#tab-4
Permit No.: N/C/ G/0 / 3/ 0/ 0/ 0/ 0/ or Certificate of Coverage No.:
Facility Name: Parker Hannifin -Gear Pump Division
County: Cleveland/Gaston Phone No. 704-730-2000
Inspector: Robert Simpson
Date of Inspection: 12/17/2015
Time of Inspection: 7:35 AM (Outfall No. 3)
Total Event Precipitation (inches): 1.25
Was this a "Representative Storm Event' or "Measureable Storm Event" as defined by the permit?
(See information below.)
® Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
i
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the j
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office_
By this
(Signature of
certify,t N report
or Designee)
and complete to the best of my knowledge:
SWU-242, Last modified 10/25/2012
Page 1 of 2
1. Outfall Description:
Outfall No. 3 Structure (pipe, ditch, etc.)
Receiving Stream: McGill Creek
Describe the industrial activities that occur within the outfall drainage area: Gear pump
manufacturing, parking lot frontage road runoff.
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: clear, light
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
lO 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids:
Ol 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
Ol 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012
tr
NC®ENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out thisjorm, please visit: htto //portal ncdenr ore/web/wq/ws/su/npdessw#tab-4
Permit No.: N/C/ G/0 / 3/ 0/ 0/ 0/ 0/ or Certificate of Coverage No.:
Facility Name: Parker Hannifin -Gear Pump Division
County: Cleveland/Gaston Phone No. 704-730-2000
Inspector: Robert Simpson
Date of Inspection: 12 17/2015
Time of Inspection: 7:45 AM (Outfall No.4)
Total Event Precipitation (inches): 1.25
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
® Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event" However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event' is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains'approval from the local DWQ Regional Office.
By this signature, I certify thatbis report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
Pagel of 2
SWU-242, Last modified 10/25/2012
1. Outfall Description:
Outfall No. 4 Structure (pipe, ditch, etc.)
Receiving Stream: McGill Creek
Describe the industrial activities that occur within the outfall drainage area: Gear pum j2
manufacturing, parking lot frontage road runoff.
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: clear. light
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
lO 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
Ol 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
Ol 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012