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NCG030293_MONITORING INFO_20170508
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /v 3 DOC TYPE ❑ HISTORICAL FILE MONITORING REPORTS DOC DATE ❑ U � D YYYYM M DD ENGINEERING, INC. RECEIVED September 19, 2016 MAY 08 2017 Krista Baker CENTRAL FILES Environmental, Health, and Safety DWR SECTION Colfax Fluid Handling 1710 Airport Road Monroe, North Carolina 28110 Subject: Monthly Stormwater Sampling — August 2016 Certificate of Coverage No. NCG030293 Colfax/IMO Industries — Monroe, NC Shield Project No. 1150109-02 Dear Ms. Baker: Shield Engineering, Inc. (Shield) was unable to collect stormwater samples for Stormwater Discharge Outfall (SDO) #004 at the Colfax - Monroe facility for the month of August 2016. According to rainfall data collected for the month, qualifying storm events occurred on August 5`h, August 18`h, August 27`h, and August 31", measuring 0.30, 0.79, 0.40, and 0.10 inches respectively. An additional 0.21 and 0.34 inches of rain were measured on August 7`h and August I01h, respectively. These events took place after normal business hours or within 72 hours of the last qualifying storm event. As the seasonal type of storm event has now changed to high intensity, short duration events, usually commencing in late afternoon through early evening with little to no notice for preparation, Shield will continue to monitor daily weather conditions and attempt to continue coordination of appropriate staff and resources to facilitate adequate sample collection. Shield was able to collect a sample and perform a visual assessment during the next qualifying storm event which occurred on September 2nd Colfax - Monroe Facility remains in Tier Three of the NPDES General Permit No. NCG030000. Shield greatly appreciates the opportunity to provide environmental services to Colfax. If you have any questions in reference to this document or require further information, please feel free to contact either of the undersigned at (704) 394-6913. Respectfully, SHIELD ENGINEERING, INC. V Melin M. Greene Mprk C. Boland, P.E. Senior Engineer Principal Engineer H:\Projects\2015\1150109-02 Colfax Stormwater\cover letters\cover letter - August 2016.docx 4301 Taggart Creek Road Telephone 704.39416913 Charlotte, NC 28208 wwwshieldengineering.com Fax 704.394.6968 ci Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted Io (-L-1 I I CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME Colfax/IMO Industries, Inc. PERSON COLLECTING SAMPLES Danny Hefner, Shield Engineering LABORATORY: Pace Analytical Services, Inc. Lab Cert. # 12 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 7.4.;> 1 �O SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly(month) DISCHARGING TO CLASS ❑ORW ❑HCtW ❑Trout ❑PNA [_]Zero -flow [—]Water Supply ❑SA ®Other —Class C — Dry Fork Creek PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 _D�Vo discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics' Benchmarks ===> _ - 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SDO 004 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, o� manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) EIS Coo.d \� k, Title (Print title) fit'/ K-`- (/t n wetif )Obi b (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mR/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n No dischorae this period?Z Outfall No. gDateSample24-hour rainfall amount, Inches' Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__� - 15 mg/L 100 mg/L or 50 mg/L` 6.0 - 9.0 SU Footnotes from Part A also apply to this Part B ' See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted I� 12-1II(,. CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME Colfax/IMO Industries, Inc. PERSON COLLECTING SAMPLES Danny Hefner, Shield Engineering LABORATORY: Pace Analytical Services, Inc. Lab Cert. # 12 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 7)Mb SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' (month) �jz' DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ®Other -Class C - Dry Fork Creek PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -) *Na discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics' Benchmarks ===> - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SDO 004 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) 42—� ✓z,- 74— Iti b (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n No discharge this period ?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 - 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." -1,0- M YyMIJA (Signature of Permittee) �1 (Date) Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 October 3, 2016 REC e' VED Krista M. Maxwell MAY 0 8 2017 Environmental, Health, and Safety Coordinator Colfax iHandling CENTpwRSE�I8 1710 Airport RoadCON Monroe, North Carolina 28110 Subject: Monthly Stormwater Sampling — September 2016 Certificate of Coverage No. NCG030293 1 Colfax/IMO Industries — Monroe, NC Shield Project No. 1150109-02 Dear Ms. Maxwell: Shield Engineering, Inc. (Shield) successfully collected a monthly stormwater sample for Stormwater Discharge Outfall (SDO) #004 at the Colfax — Monroe facility for the month of September 2016. During the September 2, 2016 sampling event, Shield's field measurement of pH was 8,6 at SDO #004. Total event precipitation was 0.56 inches. In addition to collection of samples, Shield performed Qualitative Monitoring at SDO #004 (attached). Colfax — Monroe facility should complete all relevant sections of the Stormwater Discharge Monitoring Report (DMR) using the results of analyses from the commercial laboratory that the Colfax facility has contracted with and the field pH value indicated above. The completed DMR form should then be mailed along with the Qualitative Monitoring Report Form to the regulatory agency's Central Files. Shield will continue to perform monthly sampling per Tier Two requirements until instructed to halt by Colfax. Shield greatly appreciates the opportunity to provide environmental services to the Colfax/IMO Industries. If you have any questions in reference to this document or require further information, please feel free to contact either of the undersigned at (704) 394-6913. Respectfully, SHIELD ENGINEERING, INC. Meli d M. reeve M irk C. Boland, PE Senio : ngine'cr, Ir ngipal Engineer ATTACHMENT W:\Projecta\2015\1150109-02 Colfax Stormwater\cover Iettersbover letter -September 2016.docx 4301 Taggart Crook Road Telephone 704.394.6913 Charlotte, NC 28208 wwwshieldengineering.com Fax 704.394,6968 6� NCENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisform,please visit: http:/[portalncdenrorg/web/wa/ws/su /nodessw#tab-4 Permit No.: N/C/0 /3 0/� ^0 or Certificate of Coverage No.: N/C/G/ U a/-6/ Z/-1/3/ ! Facility Name;: 6glfax t ;M Fka,-Wg4 County: t1n;or, Phone No. Inspector:; xn k[Qr Date of Inspection: 9-2-IA Time of Inspection: Total Event Precipitation (inches): 0.5-6 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) M Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event' or during a "measureable storm event" However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event' is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Pagel of 2 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. ()bW Structure (pipe, ditch, etc.) h PP_ Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CI ea r 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NO�s 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: D 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids: 1 11 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes 9 9. Is there evidence of erosion or deposition at the outfall? Yes 00 10. Other Obvious Indicators of Stormwater Pollution: List and describe A/o�:,e, Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted to(z -t IIL CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME Colfax/IMO Industries, Inc. PERSON COLLECTING SAMPLES Danny Hefner, Shield Engineering LABORATORY: Pace Analytical Services, Inc. Lab Cert. # 12 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR Zo 00 SAMPLE PERIOD ❑ 1an-June ❑ July -Dec �"" or ® Monthly' (month) Sq I�rn,n 6- DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ®Other —Class C — Dry Fork Creek PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics' Benchmarks ===> - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SD0004 C91l.150 4-5.D b'. `.ODS c p, �S ro I!LV— Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." K5 }a N` IY� I I Name (Print name) CoFi-t Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) I % Al (/6 (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 aceAnalyticalm m paoelaascc,n September 13, 2016 Krista Baker Colfax Fluid Handling 1710 Airport Road Monroe, NC 28110 RE: Project: STORMWATER Pace Project No.: 92311091 Dear Krista Baker: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on September 02, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, wa' qrn - �t Angela Baioni angela.baioni@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pagel of 28 aceAnalytical w rpscelabsavn CERTIFICATIONS Project: STORMWATER Pace Project No.: 92311091 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078' (704)8759092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 North Carolina Drinking Water Certification If 37706 Flodda/NELAP Certification #: E87627 North Carolina Field Services Certification #: 5342 Kentucky UST Certification #: 84 North Carolina Wastewater Certification #: 12 VirginiaNELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 28 aceAnalytical wxwpacela65.wm SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: STORMWATER 92311091 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92311091001 OUTFALL NO. 4 EPA 1664B JMS 1 PASI-C EPA608 SWB 27 PASI-C EPA 200.7 SH7 3 PASI-A EPA625 BPJ 58 PASI-C EPA 624 GAW 34 PASI-C SM 2540D MJP 1 PASI-A EPA 9040 KDF1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 28 aceAnalytical xxwpacelaGccam ANALYTICAL RESULTS Project: STORMWATER Pace Project No.: 92311091 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite too Huntersville. NC 28078'' (704)875-9092 Sample: OUTFALL NO. 4 Lab ID: 92311091001 Collected: 09/02/16 11:00 Received: 09/02/16 13:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg/L 5.0 1 09/07/1608:34 608 GCS Pesticides and PCBs Analytical Method: EPA608 Preparation Method: EPA 3510 Aldrin ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 309-00-2 alpha-BHC ND ug/L 0.050 1 09/08/16 08:50 09/0911620:14 319-84-6 beta-BHC ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 319-85-7 delta-BHC ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 319-86-8 gamma-BHC (Lindane) ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 58-89-9 Chlordane (Technical) ND ug/L 0.50 1 09/08/16 08:50 09/09/16 20:14 57-74-9 4,4'-DDD ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 72-54-8 4,4'-DDE NO ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 72-55-9 4,4'-DDT ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 50-29-3 Dieldrin NO ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 60-57-1 Endosulfan) ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 959-98-8 Endosulfan II ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 33213-65-9 Endosulfan sulfate ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 1031-07-8 Endrin ND ug/L 0.050 1 09/08/16 08:50 09/0911620:14 72-20-8 Endrin aldehyde ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 7421-93-4 Heptachlor ND ug/L 0.050 1 09/0811608:50 09/0911620:14 76-44-8 Heptachlor epoxide ND uglL 0,050 1 09/08/16 08:50 09/0911620:14 1024-57-3 PCB-1016 (Aroclor 1016) ND ug/L 0.50 1 09/08/16 08:50 09/09/16 20:14 12674-11-2 PCB-1 221 (Aroclor 1221) ND ug/L 0.50 1 09/08/16 08:50 09/09/1620: 14 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 0.50 1 09/08/16 08:50 09/09/16 20:14 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 0.50 1 09/08/16 08:50 09109/16 20:14 53469-21-9 PCB-1248 (Aroclor 1248) NO ug/L 0.50 1 09/08/16 08:50 09/09/16 20:14 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.50 1 09/08/16 08:50 09109/16 20:14 11097-69-1 PCB-1260 (Aroclor 1260) NO ug/L 0.50 1 09/08/16 08:50 09/09/16 20:14 11096-82-5 Toxaphene ND ug/L 0.50 1 09/08/16 08:50 09/09/16 20:14 8001-35-2 Surrogates Telrachloro-m-xylene (S) 62 % 20-110 1 09/08/16 08:50 09/09/16 20:14 877-09-8 Decachlorobiphenyl (S) 34 % 20-138 1 09/08/16 08:50 09/09/16 20:14 2051-24-3 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper ND ug/L 5.0 1 09/06/1621:00 09/07/1619:44 7440-50-8 Lead ND ug/L 5.0 1 09/06/1621:00 09/07/1619:44 7439-92-1 Zinc 45.3 ug/L 10.0 1 09/06/16 21:00 09/07/16 19:44 7440-66-6 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 Acenaphthene ND ug/L 5.0 1 09/07/1614:34 09/08/1615:31 83-32-9 Acenaphthylene NO ug/L 5.0 1 09/07/1614:34 09/0811615:31 208-96-8 Anthracene ND ug/L 5.0 1 0910711614:34 0910811615:31 120-12-7 Benzo(a)anthracene ND ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 56-55-3 Benzo(a)pyrene ND ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 50-32-8 Benzo(b)fluoranthene ND ug/L 5.0 1 09/07/1614:34 09/08/1615:31 205-99-2 Benzo(g,h,i)perylene ND ug/L 5.0 1 0910711614:34 09/08/1615:31 191-24-2 Benzo(k)fluoranthene ND ug/L 5.0 1 09/07/1614:34 09/08/1615,31 207-08-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12,47 PM without the wnnen consent of Pace Analytical Services, Inc.. Page 4 of 28 aceAnalytical .pacefeDscrm ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92311091 Sample: OUTFALL NO. 4 Lab ID: 92311091001 Collected: 09/02/16 11:00 Received: 09/02/16 13:55 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua[ 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 4-Bromaphenylphenyl ether NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 101-55-3 Butylbenzylphthalate ND ug/L 5.0 1 09/07116 14:34 09108/16 15:31 85-68-7 4-Chloro-3-methylphenol NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 59-50-7 bis(2-Chloroethoxy)methane ND ug/L 10.0 1 09/07/16 14:34 09/08/16 15:31 111-91-1 bis(2-Chloroethyl) ether NO ug/L 5.0 1 09/07/16 14:34 09/08/16 1531 111-44-4 2-Chloronaphthalene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 91-58-7 2-Chlorophenol NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 95-57-8 4-Ch[orophenylphenyl ether NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 7005-72-3 Chrysene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 218-01-9 Dibenz(a,h)anlhracene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 53-70-3 3,T-Dichlorobenzidine NO ug/L 25.0 1 09/07/16 14:34 09/08/16 15:31 91-94-1 2,4-Dichlorophenol ND ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 120-83-2 Diethylphthalate NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 84-66-2 2,4-Dimethylphenol NO ug/L 10.0 1 09/07/16 14:34 09108/16 15:31 105-67-9 Dimethylphthalate NO ug/L 5.0 1 09/07/16 14:34 09/08/16 1531 131-11-3 Di-n-butylphtha late NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 84-74-2 4,6-Dinitro-2-methylphenol NO ug/L 20.0 1 09/07/16 14:34 09/08/16 15:31 534-52-1 2,4-Dinitrophenol NO ug/L 50.0 1 09/07/16 14:34 09/08/16 15:31 51-28-5 2,4-Dinitrotoluene NO ug/L 5.0 1 09/07116 14:34 09/08/16 15:31 121-14-2 2,6-Dinitrotoluene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 606-20-2 Di-n-octyl p htha late NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 117-84-0 bis(2-Ethy[hexyl)phthalate NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 117-81-7 Fluoranthene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 206-44-0 Fluorene NO ug/L 5.0 1 09/07/16 14:34 09108/16 15:31 86-73-7 Hexachloro-1,3-butadiene ND ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 87-68-3 Hexachlorobenzene ND ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1 09/07/16 14:34 09/08/1615:31 7747-4 Hexachloroethane NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 67-72-1 Indeno(1,2,3-cd)pyrene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 193-39-5 Isophorone NO ug/L 10.0 1 09/07/16 14:34 09/0811615:31 78-59-1 Naphthalene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 91-20-3 Nitrobenzene NO ug/L 5.0 1 09/07/16 14:34 0910811615:31 98-95-3 2-Nitrophenol NO ug/L 5.0 1 09/07/16 14:34 09/08/1615:31 88-75-5 4-Nitrophenol NO ug/L 50.0 1 09/07/16 14:34 09108/16 15:31 100-02-7 N-Nitrosodimethylamine NO ug/L 5.0 1 09107/16 14:34 09/08/16 15:31 62-75-9 N-Nitroso-di-n-propylamine NO ug/L 5.0 1 09107/1614:34 09/08/1615:31 621-64-7 N-Nitrosodiphenylamine NO ug/L 10.0 1 09/07/16 14:34 09/08/16 15:31 86-30-6 2,2'-Oxybis(1-chloropropane) NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 108-60-1 Pentachlorophenol NO ug/L 10.0 1 09/07/16 14:34 09/08/16 15:31 87-86-5 Phenanthrene NO ug/L 5.0 1 09/0711614:34 09/08/16 15:31 85-01-8 Phenol NO ug/L 5.0 1 09/07/16 14:34 09/0811615:31 Pyrene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 129-00-0 1,2,4-Tdchlorobenzene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 120-82-1 2,4,6-Trichlorophenol NO ug/L 10.0 1 09/07/16 14:34 09108/16 15:31 88-06-2 Surrogates Nitrobenzene-d5(S) 62 % 10-120 1 09/07/16 14:34 09/08/16 15:31 4165-60-0 2-Fluorobiphenyl (S) 63 % 15-120 1 09/07/16 14:34 09/08/16 15:31 321-60-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0911312016 12:47 PM without the wntten consent of Pace Analytical Services, Inc.. Page 5 of 28 aceAnalytical �pacelabsmm ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078' (704)875-9092 Project: STORMWATER Pace Project No.: 92311091 Sample: OUTFALL NO. 4 Lab ID: 92311091001 Collected: 09/02/16 11:00 Received: 09/02/16 13:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 Surrogates Terphenyl-d14 (S) 82 % 11-131 1 09/07/16 14:34 09/0811615:31 1718-51-0 Phenol-d6 (S) 25 % 10-120 1 09/07/16 14:34 09/08/16 15:31 13127-88-3 2-Fluorophenol (S) 36 % 10-120 1 09/07/16 14:34 09/08/16 15:31 367-12-4 2,4,6-Tribromophenol(S) 85 % 10-137 1 09/07/16 14:34 09/08/16 15:31 118-79-6 624 Volatile Organics Analytical Method: EPA 624 Benzene ND ug/L 2.0 1 09/07/16 18:02 7143-2 Bromodichlommethane ND ug/L 2.0 1 09/07/16 18:02 75-27-4 Bromoform ND ug/L 2.0 1 09/07/16 18:02 75-25-2 Bromomethane ND ug/L 2.0 1 09/0711618:02 74-83-9 Carbon tetrachloride ND ug/L 2.0 1 09107/16 18:02 56-23-5 Chlorobenzene ND ug/L 2.0 1 09/07/1618:02 108-90-7 Chloroethane ND ug/L 2.0 1 09/07/16 18:02 75-00-3 Chloroform ND ug/L 2.0 1 09/07/16 18:02 67-66-3 Chloromethane ND ug/L 2.0 1 09/07/16 18:02 74-87-3 Dibromochloromethane ND ug/L 2.0 1 09/07/16 18:02 12448-1 1,2-Dichlorobenzene ND ug/L 2.0 1 09/07/16 18:02 95-50-1 1,3-Dichlorobenzene ND ug/L 2.0 1 09/07/16 18:02 541-73-1 1,4-Dichlorobenzene ND ug/L 2.0 1 09/07/16 18:02 106-46-7 1,1-Dichloroethane ND ug/L 2.0 1 09/07/16 18:02 75-34-3 1,2-Dichloroethane ND ug/L 2.0 1 09/07/16 18:02 107-06-2 1,1-Dichloroethene ND ug/L 2.0 1 09/07/16 18:02 75-354 cis-1,2-Dichloroethene ND ug/L 2.0 1 09/07/16 18:02 156-59-2 trans-1,2-Dichloroethene ND ug/L 2.0 1 09/07/16 18:02 156-60-5 1,2-Dichloropropane ND ug/L 2.0 1 09/07/16 18:02 78-87-5 cis-1,3-Dichloropropene ND ug/L 2.0 1 09/07/16 18:02 10061-01-5 trans-1,3-Dichloropropene ND ug/L 2.0 1 09/07/16 18:02 10061-02-6 Ethylbenzene ND ug/L 2.0 1 09/07/16 18:02 100-414 Methylene Chloride NO ug/L 2.0 1 09/07/16 18:02 75-09-2 1,1,2,2-Telrachloroethane ND uglL 2.0 1 09/07/16 18:02 79-34-5 Tetrachlomethene ND ug/L 2.0 1 09/07/16 18:02 127-184 Toluene ND ug/L 2.0 1 09/07/16 18:02 108-88-3 1,1,1-Trichloroethane ND ug/L 2.0 1 09/07/16 18:02 71-55-6 1,1,2-Trichloroethane ND ug/L 2.0 1 09/07/16 18:02 79-00-5 Trichloroethene ND ug/L 2.0 1 09/07/16 18:02 79-01-6 Trichloroflucromethane ND ug/L 2.0 1 09/07/16 18:02 75-69-4 Vinyl chloride ND ug/L 2.0 1 09/07/16 18:02 75-014 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 09/07/16 18:02 460-004 Toluene-d8 (S) 100 % 70-130 1 09/07/16 18:02 2037-26-5 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 09/07/16 18:02 17060-07-0 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 5.0 1 09/09/16 10:47 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 28 laceAnalytical' m pacefab&c ANALYTICAL RESULTS Project: STORMWATER Pace Project No.: 92311091 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)8759092 Sample: OUTFALL NO. 4 Lab ID: 92311091001 Collected: 09/02/16 11:00 Received: 09/02/16 13:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 9040 pH Analytical Method: EPA 9040 pH 6.1 Std. Units 0.10 1 09/06/16 10:39 H6 Date: 09/13/2016 12:47 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 28 aceAnalytical wuwpace!absmm QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 ' (704)8759092 Project: STORMWATER Pace Project No.: 92311091 OC Batch: 327559 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92311091001 METHOD BLANK: 1814964 Associated Lab Samples: 92311091001 Parameter Units Total Petroleum Hydrocarbons mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 5.0 09/07/16 08:24 LABORATORY CONTROL SAMPLE: 1814965 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 19.3 96 64-132 MATRIX SPIKE SAMPLE: 1814966 92311274001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L NO 20 13.2 fib 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 28 Pace Analytical Services, Inc. 2aeMalyfical' 9800 Kinsey Ave. Suite100 Hunlereville, NC 28078078 wxwpare/abscom - (704)875-9092 QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 QC Batch: 327492 Analysis Method: EPA200.7 OC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92311091001 METHOD BLANK: 1814749 Matrix: Water Associated Lab Samples: 92311091001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L NO 5.0 09/07/1618:13 Lead ug/L ND 5.0 09/07/1618:13 Zinc ug/L NO 10.0 09/07/1618:13 LABORATORY CONTROL SAMPLE: 1814750 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 484 97 85-115 Lead ug/L 500 455 91 85-115 Zinc ug/L 500 457 91 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1814751 1814752 MS MSD 92310898002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conic. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 0.84 500 500 1360 1410 104 113 70-130 3 mg/L Lead ug/L 0.11 500 500 562 531 90 84 70-130 6 mg1L Zinc ug/L 5.7 500 500 6240 5910 101 36 70-130 5 M6 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1814753 1814754 MS MSD 92310972008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec e/ Rec Limits RPD Qual Copper ug/L 21.4 500 500 510 527 98 101 70-130 3 Lead ug/L ND 500 500 458 474 91 95 70-130 3 Zinc ug/L 10.6 500 500 476 491 93 96 70-130 3 Results presented on this page are in the units indicated by the'Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the wniten consent of Pace Analytical Services, Inc.. Page 9 of 28 aceAnalytical (f wmvpacela0scwn I QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 QC Batch: 327676 Analysis Method: EPA 624 QC Batch Method: EPA 624 Analysis Description: 624 MSV Associated Lab Samples: 92311091001 METHOD BLANK: 1815839 Associated Lab Samples: 92311091001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1, 1, 1-Trichloroelhane ug/L ND 2.0 09/07/16 12:03 1, 1, 2,2-Tetrachloroetha ne ug/L ND 2.0 09/07/16 12:03 1,1,2-Tdchloroethane ug/L ND 2.0 09/07/16 12:03 1,1-Dichloroethane ug/L ND 2.0 09/07/16 12:03 1,1-Dichloroethene ug/L ND 2.0 09/07/16 12:03 1,2-Dichlorobenzene ug/L ND 2.0 09/0711612:03 1,2-Dichloroethane ug/L ND 2.0 09/07/16 12:03 1,2-Dichloropropane ug/L ND 2.0 09/07/16 12:03 1,3-Dichlorobenzene ug/L ND 2.0 09/07/16 12:03 1,4-Dichlorobenzene ug/L ND 2.0 09/07/16 12:03 Benzene ug/L ND 2.0 09/07/16 12:03 Bromodichloromethane ug/L ND 2.0 09/07/16 12:03 Bromoform ug/L ND 2.0 09/07/16 12:03 Bromomethane ug/L ND 2.0 09/07/16 12:03 Carbon tetrachloride ug/L NO 2.0 09/07/16 12:03 Chlorobenzene ug/L ND 2.0 09/0711612:03 Chlomethane ug/L ND 2.0 09107/1612:03 Chloroform ug/L ND 2.0 09/0711612:03 Chloromethane ug/L NO 2.0 0910711612:03 cis-1,2-Dichloroethene ug/L NO 2.0 09/07/16 12:03 cis-1,3-Dichloropropene ug/L NO 2.0 09/07/16 12:03 Dibromochloromethane ug/L NO 2.0 09/07/16 12:03 Ethylbenzene ug/L NO 2.0 09/07/16 12:03 Methylene Chloride ug/L ND 2.0 09/07/16 12:03 Tetrachloroethene ug/L ND 2.0 09/07/16 12:03 Toluene ug/L ND 2.0 09/07/16 12:03 trans-1,2-Dichloroethene ug/L ND 2.0 09/07/16 12:03 trans-1,3-Dichloropropene ug/L ND 2.0 09/07/16 12:03 Trichloroethene ug/L NO 2.0 09/07/16 12:03 Trichlorofluoromethane ug/L ND 2.0 09/07/16 12:03 Vinyl chloride ug/L NO 2.0 09/07/16 12:03 1,2-Dichloroethane-d4 (S) % 99 70-130 09/07/16 12:03 4-Bromofluorobenzene (S) % 99 70-130 09/07/16 12:03 Toluene-d8 (S) % 103 70-130 09/07/16 12:03 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntemville, NC 28078- (704)8759092 LABORATORY CONTROL SAMPLE: 1815840 Spike 1-CS 1-CS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers 1,1,1-Tdchloroethane ug/L 20 24.3 122 52-162 1, 1,2,2-Tetrachloroethane ug/L 20 20.5 103 46-157 Results presented on this page are in the units indicated by the'UniK' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the wnUen consent of Pace Analytical Services, Inc.. Page 10 of 28 Pace Analytical Services, Inc. ® 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville, NC 28078 wawpatelabsmm (704)875-9092 QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 LABORATORY CONTROL SAMPLE: 181 WO Spike LCS LCS % Rec Parameter Units Conc. Result % Red Limits Qualifiers 1,1,2-Tdchloroelhane ug/L 20 20.1 100 52-150 1,1-Dichloroethane ug/L 20 22.8 114 59-155 1,1-Dichloroethene ug/L 20 24.5 123 1-234 1,2-Dichlorobenzene ug/L 20 22.7 113 18-190 1,2-Dichloroethane ug/L 20 21.6 108 49-155 1,2-Dichloropropane ug/L 20 21.3 106 1-210 1,3-Dichlorobenzene ug/L 20 22.5 112 59-156 1,4-Dichlorobenzene ug/L 20 22.4 112 18-190 Benzene ug/L 20 22.6 113 37-151 Bromodichloromethane ug/L 20 22.0 110 35-155 Bromoform ug/L 20 21.0 105 45-169 Bromomethane ug/L 20 26.3 132 1-242 Carbon tetrachloride ug/L 20 24.4 122 70-140 Chlorobenzene ug/L 20 22.1 110 37-160 Chlorcethane ug/L 20 21.2 106 14-230 Chloroform ugll- 20 23.1 116 51-138 Chloromethane ug/L 20 23.9 120 1-273 cis-1,2-Dichloroethene ug/L 20 22.9 115 68-146 cis-1,3-Dichloropropene ug/L 20 22.2 111 1-227 Dibromochloromethane ug/L 20 23.1 116 53-149 Ethylbenzene ug/L 20 22.0 110 37-162 Methylene Chloride ug/L 20 23.9 120 1-221 Tetrachloroethene ug/L 20 22.9 114 64-148 Toluene ug/L 20 21.9 109 47-150 trans-1,2-Dichloroethene ug/L 20 24.0 120 54-156 trans-1,3-Dichloropropene ug/L 20 21.2 106 17-183 Trichloroethene ug/L 20 22.7 113 71-157 Tdchlorofluoromethane ug/L 20 23.0 115 17-181 Vnyl chloride ug/L 20 22.7 113 1-251 1,2-Dichloroethane-d4 (S) % 100 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) e/ 98 70-130 MATRIX SPIKE SAMPLE: Parameter 1815842 Units 92311128003 Result Spike Conc. MS Result MS % Red %Rec Limits Qualifiers 1,1,1-Tdchloroethane ug/L NO 20 25.8 129 46-171 1,1,2,2-Tetrachloroethane ug/L ND 20 22.1 111 73-159 1,1,2-Trichloroethane ug/L NO 20 21.5 107 64-152 1,1-Dichloroethane ug/L NO 20 24.5 122 43-172 1,1-Dichloroethene ug/L NO 20 28.6 143 48-189 1,2-Dichlorobenzene ug/L NO 20 23.2 116 54-154 1,2-Dichloroethane ug/L NO 20 22.3 ill 42-171 1,2-Dichloropropane ug/L NO 20 22.7 113 55-157 1,3-Dichlorobenzene ug/L NO 20 23.7 118 57-148 Results presented on this page are in the units indicated by the -Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 28 aceAnalytical r w»wpacelabsmm f QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kinney Ave. Suite 100 Huntersville, NC 28078' (704)875-9092 Project: STORMWATER Pace Project No.: 92311091 MATRIX SPIKE SAMPLE: 1815842 92311128003 Spike MS MS % Rao Parameter Units Result Conc. Result %Rec Limits Qualifiers 1,4-Dichlorobenzene ug/L NO 20 22.6 113 58-149 Benzene ug/L NO 20 24.7 124 54-163 Bromodichloromethane ug/L NO 20 22.6 113 56-152 Bromofonn ug/L NO 20 21.7 109 53-151 Bromomethane ug/L NO 20 23.4 117 10-200 Carbon tetrachloride ug/L NO 20 26.5 132 41-175 Chlorobenzene ug/L NO 20 23.9 119 67-152 Chloroethane ug/L NO 20 23.1 116 23-200 Chloroform ug/L NO 20 24.3 122 51-166 Chloromethane ug/L NO 20 22.8 110 40-175 cis-1,2-Dichloroethene ug/L NO 20 24.6 123 45-174 cis-1,3-Dichloropropene ug/L NO 20 22.6 113 38-146 Dibromochloromethane ug/L NO 20 23.3 117 65-144 Ethylbenzene ug/L NO 20 24.1 121 57-152 Methylene Chloride ug/L NO 20 25.0 125 40-167 Tetrachloroethene ug/L NO 20 24.9 119 59-155 Toluene ug/L NO 20 24.2 120 47-162 trans-1,2-Dichloroethene ug/L NO 20 26.0 130 47-178 trans-1,3-Dichloropropene ug/L NO 20 21.2 106 39-148 Trichloroethene ug/L NO 20 24.5 123 60-153 Tnchlorofluoromethane r ug/L NO 20 26.0 130 42-199 Vinyl chloride ug/L NO 20 23.2 116 46-176 1,2-Dichloroethane-d4 (S) % 105 70-130 4-Bromofluorobenzene (S) % 97 70-130 Toluene-d8(S) % 99 70-130 SAMPLE DUPLICATE: 1815841 92311128002 Dup Parameter Units Result Result RPD Qualifiers 1,1,1-Trichloroethane ug/L NO NO 1,1,2,2-Tetrachloroethane ug/L NO ND 1,1,2-Trichloroethane ug/L NO NO 1,1-Dichloroethane ug/L ND NO 1,1-Dichloroethene ug/L NO NO 1,2-Dichlorobenzene ug/L NO NO 1,2-Dichloroethane ug/L NO NO 1,2-Dichloropropane ug/L NO NO 1,3-Dichlorobenzene ug/L NO ND 1,4-Dichlorobenzene ug/L NO NO Benzene ug/L NO NO Bromodichloromethane ug/L NO NO Bromoform ug/L NO NO Bromomelhane ug/L NO NO Carbon tetrachloride ug/L NO NO Chlorobenzene ug/L NO NO Results presented an this page are in the units indicated by the -Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 28 f aceAnalyfi l www.pacelab&com QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 SAMPLE DUPLICATE: 1815841 Parameter Units 92311128002 Result Dup Result Chloroethane ug/L ND ND Chloroform ug/L ND ND Chloromethane ug/L ND ND cis-1,2-Dichloroethene ug/L ND ND cis-1,3-Dichloropropene ug/L ND ND Dibromochloromethane ug/L ND ND Ethylbenzene ug/L ND ND Methylene Chloride ug/L ND ND Tetrachloroethene ug/L ND ND Toluene ug/L ND ND trans-1,2-Dichloroethene ug/L ND ND trans-1,3-Dichloropropene ug/L ND ND Trichlcroethene ug/L ND ND Trichlorofluoromethane ug/L ND ND Vinyl chloride ug/L ND ND 1,2-Dichloroelhane-d4 (S) % 99 103 4-Bromofluorobenzene (S) % 98 99 Toluene-d8 (S) % 103 103 RED Qualifiers 3 1 0 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)870-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 28 aceAnalytcai® vmwpacelabs.cortr i QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 QC Batch: 327752 Analysis Method: EPA 608 QC Batch Method: EPA 3510 Analysis Description: 608 GCS Pest PCB Associated Lab Samples: 92311091001 METHOD BLANK: 1816118 Associated Lab Samples: 92311091001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 4,4'-DDD ug/L ND 0.050 09/09116 22:35 4,4'-DDE ug/L ND 0.050 09/09/16 22:35 4,4'-DDT ug/L ND 0.050 09/09/16 22:35 Aldrin ug/L ND 0.050 09/09/16 22:35 alpha-BHC ug/L ND 0.050 09/09/16 22:35 beta-BHC ug/L NO 0.050 09/09/1622:35 Chlordane(Technical) ug/L NO 0.50 09/09/16 22:35 delta-BHC ug/L NO 0.050 09/09/16 22:35 Dieldrin ug/L NO 0,050 09/09/16 22:35 Endosulfan I ug/L NO 0.050 09/09/16 22:35 Endosulfan II ug/L NO 0.050 09/09/16 22:35 Endosulfan sulfate ug/L NO 0.050 09/09/16 22:35 Endrin ug/L NO 0.050 09/09/16 22:35 Endrin aldehyde ug/L NO 0.050 09/09/16 22:35 gamma-BHC (Lindane) ug/L NO 0.050 09/09/16 22:35 Heptachlor ug/L ND 0.050 09109/1622:35 Heptachlor epoxide ug/L ND 0.050 09/09/16 22:35 PCB-1016 (Aroclor 1016) ug/L ND 0.50 09/09/16 22:35 PCB-1221 (Aroclor 1221) ug/L NO 0.50 09/09116 22:35 PCB-1232 (Aroclor 1232) ug/L ND 0.50 09/09/16 22:35 PCB-1242 (Aroclor 1242) ug/L ND 0.50 09/09/16 22:35 PCB-1248 (Aroclor 1248) ug/L ND 0.50 09/09/16 22:35 PCB-1254 (Aroclor 1254) ug/L ND 0.50 09/09/16 22:35 PCB-1260 (Aroclor 1260) ug/L ND 0.50 09/09/16 22:35 Toxaphene ug/L NO 0.50 09/09/16 22:35 Decachlorobiphenyl(S) % 72 20-138 09/09/16 22:35 Tetrachloro-m-xylene (S) % 67 20-110 09/09/16 22:35 Qualifiers Pace Analytical services, Inc. 9800 Kinney Ave. Suite 100 Huntersville, NC 28078' (704)875-9092 LABORATORY CONTROL SAMPLE: 1816119 Spike LCS LCS % Rec Parameter Units Conc. Result % Rae Limits Qualifiers 4,4'-DDD ug/L .25 0.23 93 31-141 4,4'-DDE ug/L .25 0.21 84 30-145 4,4'-DDT ug/L .25 0.19 78 25-160 Aldrin ug/L .25 0.19 77 42-122 alpha-BHC ug/L .25 0.22 88 37-134 beta-BHC ug/L .25 0.22 90 17-147 delta-BHC ug/L .25 0.22 87 19-140 Dieldrin ug/L .25 0.21 83 36-146 Endosulfan I ug/L .25 0.22 90 45-153 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 28 ace Analytical f ebexperelab&corn It QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 LABORATORY CONTROL SAMPLE: Parameter 1816119 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Endosulfan II ug/L .25 0.23 93 1-202 Endosulfan sulfate ug/L .25 0.24 96 26-144 Endrin ug/L .25 0.24 96 30-147 Endrin aldehyde ug/L .25 0.20 81 50-150 gamma-BHC (Lindane) ug/L .25 0.22 90 32-127 Heptachlor ug/L .25 0.21 84 34-111 Heptachlor epoxide ug/L .25 0.22 87 - 41-126 Decachlorobiphenyl (S) % 47 20-138 Tetrachloro-m-xylene (S) % 85 20-110 MATRIX SPIKE SAMPLE: Parameter 1816120 Units 92311094002 Result Spike Conc. MS Result MS % Rec %Rec Limits Qualifiers 4,4'-DDD ug/L NO .25 0.15 60 31-141 4,4'-DDE ug/L NO .25 0.15 59 30-145 4,4'-DDT ug/L NO .25 0.15 60 25-160 Aldrin ug/L NO .25 0.14 55 42-122 alpha-BHC ug/L NO .25 0.15 59 37-134 beta-BHC ug/L NO .25 0.17 70 17-147 delta-BHC ug/L NO .25 0.15 59 19-140 Dieldrin ug/L NO .25 0.14 56 36-146 Endosulfan I ug/L NO .25 0.16 65 45-153 Endosulfan II ug/L NO .25 0.15 62 1-202 Endosulfan sulfate ug/L NO .25 0.16 65 26-144 Endrin ug/L NO .25 0.17 68 30-147 Endrin aldehyde ug/L NO .25 0.13 53 50-150 gamma-BHC (Lindane) ug/L NO .25 0.15 59 32-127 Heptachlor ug/L NO .25 0.15 62 34-111 Heptachlor epoxide ug/L NO .25 0.14 57 41-126 Decachlorobiphenyl (S) % 21 20-138 Tetrachloro-m-xylene (S) % _ 61 20-110 SAMPLE DUPLICATE: 1816121 92311094003 Dup Parameter Units Result Result RPD Qualifiers 4,4'-DDD ug/L NO NO 4,4'-DDE ug/L NO NO 4,4'-DDT ug/L NO NO Aldrin ug/L NO NO alpha-BHC ug/L NO NO beta-BHC ug/L NO NO Chlordane (Technical) ug/L NO NO delta-BHC ug/L NO NO Dieldrin ug/L NO NO Results presented on this page are in the units indicated by the 'Units" column except where an alternate unit is presented to the fight of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 28 aceAnalytical w»wpace(ab&ccm QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 SAMPLE DUPLICATE: 1816121 92311094003 Dup Parameter Units Result Result Endosulfan I ug/L ND ND Endosulfan II ug/L ND ND Endosulfan sulfate ug/L ND ND Endrin ug/L ND ND Endrin aldehyde ug/L ND ND gamma-BHC (Lindane) ug/L ND ND Heptachlor ug/L ND ND Heptachlor epoxide ug/L ND ND PCB-1016 (Aroclor 1016) ug/L ND ND PCB-1 221 (Aroclor 1221) ug/L ND ND PCB-1232 (Aroclor 1232) ug/L ND ND PCB-1242 (Aroclor 1242) ug/L ND ND PCB-1248 (Aroclor 1248) ug/L ND ND PCB-1254 (Aroclor 1254) ug/L ND ND PCB-1260 (Aroclor 1260) ug/L ND ND Toxaphene ug/L ND ND RPD Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. 'Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented an this page are In the units indicated by the 'units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 28 ace Analytical wwwpacelaDzrnm QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 QC Batch: 327638 Analysis Method: EPA 625 QC Batch Method: EPA 625 Analysis Descnption: 625 MSS Associated Lab Samples: 92311091001 METHOD BLANK: 1815492 Associated Lab Samples: 92311091001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,2,4-Tnchlorobenzene ug/L ND 5.0 09/08/16 12:15 2,2'-Oxybis(1-chloropropane) ug/L ND 5.0 09108/1612:15 2,4,6-Trichlorophenol ug/L ND 10.0 09/08/16 12:15 2,4-Dichloraphenol ug/L ND 5.0 09/08/16 12:15 2,4-Dimethylphenol ug/L ND 10.0 09M8/16 12:15 2,4-Dinilrophenol ug/L ND 50.0 09/08/16 12:15 2,4-Dinitrotoluene ug/L ND 5.0 09/08/16 12:15 2,6-Dinitrotoluene ug/L ND 5.0 09/08/16 12:15 2-Chloronaphthalene ug/L ND 5.0 09108/1612:15 2-Chlorophenol ug/L ND 5.0 0910811612:15 2-Nitrophenol ug/L ND 5.0 09/08/16 12:15 3,3'-Dichlorobenzidine ug/L ND 25.0 09/08/16 12:15 4,6-Dinitro-2-methylphenol ug/L ND 20.0 09J08/1612:15 4-Bromophenylphenyl ether ug/L ND 5.0 09/08/16 12:15 4-Chloro-3-methylphenol ug/L ND 5.0 09/08/16 12:15 4-Chlorophenylphenyl ether ug/L ND 5.0 09/08/16 12:15 4-Nitrophenol ug/L ND 50.0 09/08/16 12:15 Acenaphthene ug/L ND 5.0 09/08/1612:15 Acenaphthylene ug/L ND 5.0 0910811612:15 Anthracene ug/L ND 5.0 09/0811612:15 Benzo(a)anthracene ug/L ND 5.0 09/0811612:15 Benzo(a)pyrene ug/L ND 5.0 09/08/16 12:15 Benzo(b)fluoranthene ug/L ND 5.0 09/08/1612:15 Benzo(g,h,i)perylene ug/L ND 5.0 09108/1612:15 Benzo(k)fluoranthene ug/L ND 5.0 09/0811612:15 bis(2-Chloroethoxy)methane ug/L ND 10.0 09/08/161215 bis(2Chloroethyl) ether ug/L ND 5.0 09/08/16 12:15 bis(2-Ethylhexyl)phthalate ug/L ND 5.0 09/0811612:15 Butylbenzylphthalate ug/L ND 5.0 09/0811612:15 Chrysene ug/L ND 5.0 09/08/16 12:15 Di-n-butylphlhalate ug/L ND 5.0 09/0811612:15 Di-n-octylphthalate ug/L ND 5.0 09108/1612:15 Dibenz(a,h)anthracene ug/L ND 5.0 09/08/16 12:15 Diethylphthalate ug/L ND 5.0 09/08/16 12:15 Dimethylphthalate ug/L ND 5.0 09/08/16 12:15 Fluoranthene ug/L ND 5.0 09/08/16 12:15 Fluorene ug/L ND 5.0 09/08/16 12:15 Hexachloro-1,3-butadiene ug/L ND 5.0 09/08/16 1215 Hexachlorobenzene ug/L ND 5.0 09/0811612:15 Hexachlorocyclopentadiene ug/L ND 10.0 09/0811612:15 Hexachloroethane ug/L ND 5.0 09/0811612:15 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the -Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 09113/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 28 aceAnalytical ' wwwpacelabs.cam QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 METHOD BLANK: 1815492 Associated Lab Samples: 92311091001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed Indeno(1,2,3-cd)pyrene ug/L ND 5.0 09/08/16 12:15 Isophorone ug/L NO 10.0 09/08/16 12:15 N-Nitroso-di-n-propylamine ug/L ND 5.0 09/08/16 12:15 N-Nitrosodimethylamine ug/L ND 5.0 09/08M612:15 N-Nitrosodiphenylamine ug/L NO 10.0 09/08/1612:15 Naphthalene ug/L ND 5.0 09/0811612:15 Nitrobenzene ug/L ND 5.0 09/08/16 12:15 Pentachlorophenol ug/L NO 10.0 09/08/16 12:15 Phenanthrene ug/L ND 5.0 09/08/16 12:15 Phenol ug/L NO 5.0 09108/1612:15 Pyrene ug/L NO 5.0 09/08/16 12:15 2,4,6-Tribromophenol(S) % 97 10-137 09/08/16 12:15 2-Fluorobiphenyl(S) % 84 15-120 09/08/16 12:15 2-Fluorophenol (S) % 49 10-120 09/08/16 12:15 Nitrobenzene-d5 (S) % 89 10-120 09/08/16 12:15 Phenol-d6 (S) % 32 10-120 09/08/16 12:15 Terphenyl-dl4 (S) % 104 11-131 09/08/16 12:15 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1815493 Units Spike Conc. LCS Result LCS %Rec % Rec Limits 1,2,4-Trichlorobenzene ug/L 50 25.3 51 44-142 2,2'-Oxybis(t-chloropropane) ug/L 50 42.7 85 36-166 2,4,6-Trichlorophenol ug/L 50 50.4 101 37-144 2,4-Dichlorophenol ug/L 50 45.1 90 1-191 2,4-Dimethylphenol ug/L 50 51.4 103 32-119 2,4-Dinitrophenol ug/L 250 173 69 1-181 2,4-Dinitrotoluene ug/L 50 50.5 101 39-139 2,6-Dinitrotoluene ug/L 50 51.4 103 50-158 2-Chloronaphthalene ug/L 50 33.0 66 60-118 2-Chlorophenol ug/L 50 39.9 80 23-134 2-Nitrophenol ug/L 50 49.7 99 29-182 3,3'-Dichlorobenzidine ug/L 100 84.7 85 1-262 4,6-Dinitro-2-methylphenol ug/L 100 112 112 1-181 4-Bromophenylphenyl ether ug/L 50 47.5 95 53-127 4-Chloro-3-methylphenol ug/L 100 75.9 76 22-147 4-Chlorophenylphenyl ether ug/L 50 41.0 82 25-158 4-Nitrophenol ug/L 250 106 42 1-132 Acenaphthene ug/L 50 37.9 76 47-145 Acenaphthylene uglL 50 41.5 83 33-145 Anthracene ug/L 50 48.9 98 1-166 Benzo(a)anthracene ug/L 50 47.6 95 33-143 Benzo(a)pyrene ug/L 50 44.9 90 17-163 Benzo(b)fluoranthene ug/L 50 47.9 96 24-159 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8769092 Qualifiers Results presented an this page are in the units indicatetl by the'Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 28 aceAnalytical wwwpecelabscwn QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 HuntersAlle, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92311091 LABORATORY CONTROL SAMPLE: 1815493 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Benzo(g,h,i)perylene ug/L 50 47.8 96 1-219 Benzo(k)fluoranthene ug/L 50 46.5 93 11-162 bis(2-Chloroethoxy)methane ug/L 50 42.6 85 33-184 bis(2-Chloroethyl) ether ug/L 50 41.1 82 12-158 bis(2-Ethylhexyl)phthalate ug/L 50 56.6 113 8-158 Butylbenzylphthalate ug/L 50 59.5 119 1-152 Chrysene ug/L 50 46.0 92 17-168 Di-n-butylphthalate ug/L 50 52.9 106 1-118 Di-n-octylphthalate ug/L 50 56.6 113 4-146 Dibenz(a,h)anthracene ug/L 50 46.4 93 1-227 Diethylphthalate ug/L 50 44.5 89 1-114 Dimethylphthalate ug/L 50 44.2 88 1-112 Fluoranthene ug/L 50 45.9 92 26-137 Fluorene ug/L 50 43.2 86 59-121 Hexachloro-1,3-butadiene ug/L 50 20.7 41 24-116 Hexachlorobenzene ug/L 50 49.7 99 1-152 Hexachlorocyclopentadiene ug/L 50 24.1 48 25-150 Hexachloroethane ug/L 50 21.1 42 40-113 Indeno(1,2,3cd)pyrene ug/L 50 46.6 93 1-171 Isophorone ug/L 50 47.2 94 21-196 N-Nitroso-di-n-propylamine ug/L 50 39.3 79 1-230 N-Nitrosodimethylamine ug/L 50 22.0 44 25-150 N-Nitrosodiphenylamine ug/L 50 46.7 93 25-150 Naphthalene ug/L 50 31.3 63 21-133 Nitrobenzene ug/L 50 46.0 92 35-180 Pentachlorophenol ug/L 100 105 105 14-176 Phenanthrene ug/L 50 47.3 95 54-120 Phenol ug/L 50 21.3 43 5-112 Pyrene ug/L 50 49.5 99 52-115 2,4,6-Tribromophenol(S) % 114 10-137 2-Fluorobiphenyl (S) % 75 15-120 2-Fluorophenol (S) % 51 W-120 Nitrobenzene-d5(S) % 81 10-120 Phenol-d6 (S) % 35 10-120 Terpheny1-d14 (S) % 100 11-131 MATRIX SPIKE SAMPLE: 1815494 92311124009 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/L NO 50 30.0 60 44-142 2,2'-Oxybis(1-chloropropane) ug/L NO 50 43.0 86 36-166 2,4,6-Trichlorophenol ug/L NO 50 55.2 110 37-144 2,4-Oichlorophenol ug/L NO 50 45.6 91 1-191 2,4-Dimethylphenol ug/L NO 50 49.1 98 32-119 2,4-Dinitrophenol ug/L NO 250 167 67 1-181 Results presented on this page are in the units indicated by the -Units-column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 28 aceAnalytcal rmwpaceWDxcam QUALITY CONTROL DATA Pace Analytical services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 ' (704)875-9092 Project: STORMWATER Pace Project No.: 92311091 MATRIX SPIKE SAMPLE: 1815494 92311124009 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifers 2,4-Dinitrotoluene ug/L ND 50 56.9 114 39-139 2,6-Dinitrotoluene ug/L ND 50 58.6 117 50-158 2-Chloronaphthalene ug/L ND 50 43.1 86 60-118 2-Chlorophenol ug/L ND 50 41.2 82 23-134 2-Nitrophenol ug/L ND 50 57.7 115 29-182 3,3'-Dichlorobenzidine ug/L ND 100 84.0 84 1-262 4,6-Dinitro-2-methylphenol ug/L ND 100 110 110 1-181 4-Bromophenylphenyl ether ug/L ND 50 49.2 98 53-127 4-Chloro-3-methylphenol ug/L ND 100 86.5 86 22-147 4-Chlorophenylphenyl ether ug/L ND 50 47.3 95 25-158 4-Nitrophenol ug/L ND 250 125 50 1-132 Acenaphthene ug/L ND 50 44.4 89 47-145 Acenaphthylene ug/L ND 50 47.3 95 33-145 Anthracene ug/L ND 50 48.3 97 1-166 Benzo(a)anthracene ug/L ND 50 49.2 98 33-143 Benzo(a)pyrene ug/L ND 50 46.0 92 17-163 Benzo(b)fuoranthene ug/L ND 50 48.4 97 24-159 Benzo(g,h,i)perylene ug/L ND 50 46.9 94 1-219 Benzo(k)fuoranthene ug/L ND 50 45.1 90 11-162 bis(2-Chloroethoxy)methane ug/L ND 50 43.9 88 33-184 bis(2-Chloroelhyl) ether ug/L ND 50 42.5 85 12-158 bis(2-Ethylhexyl)phthalate ug/L ND 50 59.6 119 8-158 Butylbenzylphthalate ug/L ND 50 60.7 121 1-152 Chrysene ug/L ND 50 47.8 96 17-168 Di-n-butylphthalate ug/L ND 50 52.7 105 1-118 Di-n-octylphthalate ug/L ND 50 59.0 118 4-146 Dibenz(a,h)anthracene ug/L ND 50 46.6 93 1-227 Diethylphthalate ug/L ND 50 46.8 94 1-114 Dimethylphthalate ug/L ND 50 45.3 91 1-112 Fluoranthene ug/L ND 50 49.4 99 26-137 Fluorene ug/L ND 50 48.3 97 59-121 Hexachloro-1,3-butadiene ug/L ND 50 24.3 49 24-116 Hexachlorobenzene ug/L ND 50 49.8 100 1-152 Hexachlarocyclopentadiene ug/L ND 50 34.8 70 25-150 Hexachloroelhane ug/L ND 50 22.3 45 .40-113 I ndeno(1,2,3-cd)pyrene ug/L ND 50 46.1 92 1-171 Isophorone ug/L ND 50 44.8 90 21-196 N-N itroso-d i-n-propyl a min a ug/L ND 50 37.6 75 1-230 N-Nitresodimethylamine ug/L ND 50 23.9 48 25-150 N-Nitrosodiphenylamine ug/L ND 50 45.5 91 25-150 Naphthalene ug/L ND 50 35.1 70 21-133 Nitrobenzene ug/L ND 50 49.1 98 35-180 Pentachlorophenol ug/L ND 100 109 109 14-176 Phenanthrene ug/L ND 50 49.4 99 54-120 Phenol ug/L ND 50 22.5 45 5-112 Pyrene ug/L ND 50 52.4 105 52-115 2,4,6-Tribromophenol(S) % 117 10-137 Results presented on this page are in the units indicated by the Numbs" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 28 aceAnalytical swepscelab&crom QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 MATRIX SPIKE SAMPLE: 1815494 92311124009 Spike MS MS %Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2-Fluorobiphenyl (S) % 87 15-120 2-Pluorophenol(S) % 55 10-120 Nitrobenzene-d5(S) % 88 10-120 Phenol-d6 (S) e/ 39 10-120 Terphenyl-dl4 (S) % 93 11-131 SAMPLE DUPLICATE: 1815495 Parameter Units 92311091001 Result Dup Result 1,2,4-Trichlorobenzene ug/L ND ND 2,2'-Oxybis(1-chloropropane) ug/L ND ND 2,4,6-Trichlorophenol ug/L ND ND 2,4-Dichlorophenol ug/L ND ND 2,4-Dimethylphenol ug/L ND ND 2,4-Dinitrophenol ug/L ND ND 2,4-Dinitrotoluene ug/L ND ND 2,6-Dinitrololuene ug/L ND ND 2-Chloronaphthalene ug/L ND ND 2-Chlorophenol ug/L ND ND 2-Nitrophenol ug/L ND ND 3,3'-Dichlorobenzidine ug/L ND ND 4,6-Dinitro-2-methylphenol ug/L ND ND 4-Bromophenylphenyl ether ug/L ND ND 4-Chloro-3-methylphenol ug/L ND ND 4-Chlorophenylphenyl ether ug/L ND ND 4-Nitrophenol ug/L ND ND Acenaphthene ug/L ND ND Acenaphthylene ug/L ND ND Anthracene ug/L ND ND Benzo(a)anthracene ug/L ND ND Benzo(a)pyrene ug/L ND ND Benzo(b)fluoranthene ug/L ND ND Benzo(g,h,i)perylene ug/L ND ND Benzo(k)fluoranthene ug/L ND ND bis(2-Chloroethoxy)methane ug/L ND ND bis(2-Chloroethyl) ether ug/L ND ND bis(2-Ethylhexyl)phthalate ug/L ND ND Butylbenzylphthalate ug/L ND ND Chrysene ug/L ND ND Di-n-butylphthalate ug/L ND ND Di-n-octylphthalate ug/L ND ND Dibenz(a,h)anthracene ug/L ND ND Diethylphthalate ug/L ND ND Dimethylphthalate ug/L ND ND Fluoranthene ug/L ND ND RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 28 aceAnalytical I www.pacelabsmn QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 SAMPLE DUPLICATE: 1815495 Parameter Units 92311091001 Result Due Result Fluorene ug/L ND NO Hexachloro-1,3-butadiene ug/L ND NO Hexachlorobenzene ug/L ND NO Hexachlorocyclopentadiene ug/L ND NO Hexachloroethane ug/L NO NO Indeno(1,2,3-cd)pyrene ug/L ND ND Isophorone ug/L ND ND N-Nitroso-di-n-propylamine ug/L NO ND N-Nitrosodimethylamine ug/L NO ND N-Nitrosodiphenylamine ug/L NO NO Naphthalene ug/L NO NO Nitrobenzene ug/L NO NO Pentachlorophenol ug/L NO NO Phenanthrene ug/L ND NO Phenol ug/L NO NO Pyrene ug/L ND NO 2,4,6-Tribromophenol (S) % 85 96 2-Fluorobiphenyl (S) % 63 79 2-Fluorophenol(S) % 36 42 Nitrobenzene-d5 (S) % 62 73 Phenol-d6 (S) % 25 25 Tefphenyl-dl4 (S) % 82 87 RPD Qualifiers 12 23 17 15 1 5 Pace Analytical Services, Inc. 9800 Kincey Ave: Suite 100 Huntersville, NC 28078 (704)8759092 Results presented on this page are in the units indicated by the'Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 28 aceAnalytical wwwpareWDscam f QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntelsvllie, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92311091 QC Batch: 327933 Analysis Method: SM 2540D OC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92311091001 METHOD BLANK: 1817160 Matrix: Water Associated Lab Samples: 92311091001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 09/09/16 10:47 LABORATORY CONTROL SAMPLE: 1817161 Spike LCS LCS % Rec Parameter Units Cone. Result % Red Limits Qualifiers Total Suspended Solids mg/L 250 248 99 90-110 SAMPLE DUPLICATE: 1817162 92311091001 Quip Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L NO NO SAMPLE DUPLICATE: 1817163 92311112005 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 13.6 17.0 22 06 Results presented on this page are in the units indicated by me 'Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM vrithout the written consent of Pace Analytical Services, Inc.. Page 23 of 28 aceAnalytical wmvpacelabsmm QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 OC Batch: 327407 Analysis Method: EPA9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92311091001 SAMPLE DUPLICATE: 1814193 Parameter pH 92310609002 Dup Units Result Result RPD Qualifiers Sid. Units 8.1 8.1 0 H6 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875i9092 Results presented on this page are in the units indicated by the'Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 24 of 28 � aceAnalytical QUALIFIERS Project: STORMWATER Pace Project No.: 92311091 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D)- Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS 06 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA required holding time. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 25 of 28 aceAnalytical newpacelxbs.= QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville. NC 28078 - (704)875-9092 Project: Pace Project No.: STORMWATER 92311091 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92311091001 OUTFALL NO.4 EPA 1664E 327559 92311091001 OUTFALL NO. 4 EPA 3510 327752 EPA 608 327914 92311091001 OUTFALL NO.4 EPA 200.7 327492 EPA200.7 327549 92311091001 OUTFALL NO.4 EPA625 327638 EPA 625 327818 92311091001 OUTFALL NO.4 EPA 624 327676 92311091001 OUTFALL NO. 4 SM 25400 327933 92311091001 OUTFALL NO.4 EPA 9040 327407 Date: 09/13/2016 12:47 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 26 of 28 Document Name: Document Revised:April 25, 2016 Sample Condition Upon Receipt(SCUR) Page 1 of 2 aceAnalytkai° Document No.: issuing Authority: !� F-CHR-CS-003-rev.19 Pace Huntersville Quality Office N fl0i Client Name: Project Courier: Fed Ex ❑UPS ❑LISPS ❑Client ❑ Commercial ©P ce ❑Other._ WIUR U4%7X-&W-+- 111111111 I IIII I II III ,92311091 Custody Seal Present? []yes 0No Seals Intact? Qyes ONO ct Date/Initials Person Examining Contents..r.-ll4 Packing Material: ❑Bubble Wrap ©Bubble Bags ❑None ❑Other:_ OiWet ❑Blue ❑None (3 amples on ice, cooling process has begun Thermometer: T1505 Type of e:� Correction factor: 0.0°C Cooler Temp Corrected (°C): Biological Tissue Frozen? []Yes ❑No QWA Temp should be above fireejAing to 6"C USDA Regulated Soil ( N/A, water sample) rid samoles orieinate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internatio ally, .. u....n ,.,d onorcn RIco171—IYes ❑Yes + o Comments/Discrepancy: Chain of Custody Present? s ❑No ❑N/A I Samples Arrived within Hold Time? LD<s [:]N/A 2. Short Hold Time Analysis (<72 hr.)? []yestarro ,❑No ❑N/A 3. Rush Turn Around Time Requested? ❑Yes ®o ❑N/A 4' Sufficient Volume? E3Y S. ONO ❑N/A 5. Correct Containers Used? � [:]No ❑N/A 6. -Pace Containers Used? E.Ydr ❑No ❑N/A Containers Intact? ❑res ❑No ❑N/A 7. Oyes- ON, ®NlW_ R. Note if sediment is visible in the dissolved container Samples Field Filtered? Sample Labels MatchCOC? (2Y9,_ [IN. ❑N/A 9. -Includes Date/Time/ID/Analysis Matrix All containers needing acid/base preservation have been ._ - lU. __ _- ..checked? __....... _ _.____... _ _. _.__... ____... All containers needing preservation are found to be in compliance with EPA recommendation? ®Ye,' [:]No ❑N/A xuo°rx<: (HNOa, H,SO,, HCI<2; NaOH >9 Sulfide, NaOH>12 Cyanide) Exceptions: VOA, Coliform, TOC, Oil and Grease, s ONO ❑N/A x.wymoa. °wa DRO/8015 (water) DOC;LLHg Samples checked for dechlorination? QYes' [:]No ❑N/A 11. Headspace in VOA Vials (>5-6mm)? ❑Yes Fr ❑N/A 12. Trip Blank Present? ❑Yes ONO 41W 13. Trip Blank Custody Seals Present? ❑Yes ONO ' q 'f r hasedl: -- Pace Trip Blank Lot (I pu c CLIENT NOTIFICATION/RESOLUTION Person Contacted:' Comments/Sample Discrepancy: Date/Time: .Field Data Required? ❑Yes ONO Project Manager SCURF Review: _(L Date: glbh Project Manager SRP Review: TL Date: q /y/, Note: Whenever there is discrepancy affecting North Carolina compliance samples, a copy ofthss form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 27 of 28 fri CHAIN -OF -CUSTODY /Analytical Request Document P1 ,tw1)fiCN The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section a Section C Required Client lnfimarmien: Required Project information- inicued lnformodir: Pa e: 1 Of 1 Company: Colfax Fluid dancing Report To: Daniel Cox Atarr ion:- Address-. 1710 Airport Road Copy To # a•_/F; (Etl;? Company Name: Mpnme, NC 28110 N-f�i-'.77 �tdG'up'[ '2f.[I!y" Address Rid,ul.ftcry A anc ` Email: tlaniel.. colfaxguldhandlin,tom Purchase Oraerp'. Paw Cueror Phone(7pU289£511 IF.x Project Name' Slormwalor Pace Project Manage, Hammhamson pawlabs.coM. '--statel locetion" Requested Due Date: Project p Pace Profile b'. 6479.2 NC -+Requested Anal sis Humid YIN 2 MATRU CODE o U COLLECTED Preservatives pil\ Wgvr eW U w Wa�ilnWater WJY Z SAMPLE ID 5oie5o0° s SRT TA END p M 1� or Ot One Character per box. Wm° N'P IAZ O-91;-0 < V # oihn OT Sample Ids must be unique T,la°e Ts ,Oj x TDATETIME u o 2. a eoLu b — 2 m. _ v a or -0 = O y U ~ a n DATE TIME x 0O ¢ ' 3i' ..r,4 ;a q.' 612`� u7•. y 17�> 4— :,_ y i�trdtApDIT10NAl COMMENTS h'4}: I"�hRELINQUISHED eYf AFFILIATroN-�i "DATE °; G; TIME ',' ''r'u� ACCEPTED BY IAFFlLIATION lt;SAMPLE GONOITION6 5 jz ..I rY r := Lf1 r)� .1� •� -ILO �. r"".. `.' f 4 a w n r isM\$t+ SAMPLER'NAME ANO SIGNATURE r� V D E E � PRINT Namc of SAMPLER: /.•cTr /,` '" `r °o'� m SIGNATURE of SAMPLER: / DATE Signetl: v g N 0 m m m d Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCGO3OOOO Date submitted CERTIFICATE OF COVERAGE NO. NO003O293 FACILITY NAME Colfax/IMO Industries, Inc. PERSON COLLECTING SAMPLES Danny Hefner, Shield Engineering LABORATORY: Pace Analytical Services, Inc. Lab Cert. # 12 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW -]Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ®Other_Class C- Dry Fork Creek PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar 0&G/Total Total Petroleum Hydrocarbons Toxic Organics5 Benchmarks =__> - - 100 mg/L or SO mg/L" 6.0 - 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 1S mg/L 1 mg/L SDO00a r c o �.005 a, D �3 —• u Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. "See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." r Name (Print name) Title (Print title) vL K�-6AVexI (Signature) /a 3 (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 5U Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWD-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) L Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 5aceAnalyfical' w»w.pacela6s.can September 13, 2016 Krista Baker Colfax Fluid Handling 1710 Airport Road Monroe, NC 28110 RE: Project: STORMWATER Pace Project No.: 92311091 Dear Krista Baker: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)878-9092 Enclosed are the analytical results for sample(s) received by the laboratory on September 02, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. � Si„nc�eprely, Angela Baioni angela.baioni@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 28 aceAnalytical e Project: STORMWATER Pace Project No.: 92311091 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite too Huntersville, NC 28078 (704)878-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 28 aceAnalytical x pacefabscorn SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Project: Pace Project No.: STORMWATER 92311091 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92311091001 OUTFALL NO.4 EPA 1664E JMS 1 PASI-C EPA608 SWB 27 PASI-C EPA 200.7 SH1 3 PASI-A EPA 625 BPJ 58 PASI-C EPA 624 GAW 34 PASI-C SM 2540D MJP 1 PASI-A EPA 9040 KDF1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 28 (�5a?eAnalytical' w vpacelabscaa ANALYTICAL RESULTS Project: STORMWATER Pace Project No.: 92311091 Pace Analytical services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: OUTFALL NO. 4 Lab ID: 92311091001 Collected: 09/02/16 11:00 Received: 09/02/16 13:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg/L 5.0 1 09107/1608:34 608 GCS Pesticides and PCBs Analytical Method: EPA608 Preparation Method: EPA 3510 Aldan ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 309-00-2 alpha-BHC ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 319-84-6 beta-BHC ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 319-85-7 delta-BHC ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 319-86-8 gamma-BHC (Lindane) ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 58-89-9 Chlordane (Technical) ND ug/L 0.50 1 09/08/16 08:50 09/09/16 20:14 57-74-9 4,4'-DDD ND ug/L 0.050 1 09/08/16 08:50 09109/16 20:14 72-54-8 4,4'-DDE ND ug/L 0.050 1 09108/1608:50 09/09/16 20:14 72-55-9 4,4'-DDT NO ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 50-29-3 Dieldrin ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 60-57-1 Endosulfan I ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 959-98-8 Endosulfan It ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 33213-65-9 Endosulfan sulfate ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 1031-07-8 Endrin ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 72-20-8 Endrin aldehyde ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 7421-934 Heptachlor ND ug/L 0.050 1 09/08116 08:50 09/09/16 20:14 7644-8 Heptachlor epoxide ND ug/L 0.050 1 09/08/16 08:50 09/09/16 20:14 1024-57-3 PCB-1016 (Aroclor 1016) NO ug/L 0.50 1 09/08/16 08:50 09109/16 20:14 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 0.50 1 09/08/16 08:50 09/09/16 20:14 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 0.50 1 09/08/16 08:50 09/09/16 20:14 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 0.50 1 09/08/16 08:50 09/09/16 20:14 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.50 1 09/08/16 08:50 09/09/16 20:14 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.50 1 09/08/16 08:50 09/09/16 20:14 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.50 1 09/08/16 08:50 09/09/16 20:14 11096-82-5 Toxaphene ND ug/L 0.50 1 09/08/16 08:50 09/09/16 20:14 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 62 % 20-110 1 09/08116 08:50 09/09/16 20:14 877-09-8 Decachlorobiphenyl (S) 34 % 20-138 1 09/08116 08:50 09/09/16 20:14 2051-24-3 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper ND ug/L 5.0 1 09/06/16 21:00 09/07/16 19:44 7440-50-8 Lead ND ug/L 5.0 1 09/06/16 21:00 09107/1619:44 7439-92-1 Zinc 45.3 ug/L 10.0 1 09/06/16 21:00 09/07/16 19:44 7440-66-6 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 Acenaphthene NO ug/L 5.0 1 09107/1614:34 09/08/16 15:31 83-32-9 Acenaphthylene NO ug/L 5.0 1 09107/1614:34 09/08/16 15:31 208-96-8 Anthracene ND ug/L 5.0 1 09/07/16 14:34 09108/16 15:31 120-12-7 Benzo(a)anthracene ND ug/L 5.0 1 09/07/16 14:34 09/08/16 1531 56-55-3 Benzo(a)pyrene ND ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 50-32-8 Benzo(b)flucranthene ND ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 205-99-2 Benzo(g,h,i)perylene ND ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 191-24-2 Benzo(k)fluoranthene ND ug/L 5.0 1 09/07/1614:34 09/08/16 15:31 207-08-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09113/2016 12:47 PM vrithout the written consent of Pace Analytical Services, Inc.. Page 4 of 28 aceAnalytical l/ www.pace/a6imn i ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Project: STORMWATER Pace Project No.: 92311091 Sample: OUTFALL NO. 4 Lab ID: 92311091001 Collected: 09/02/16 11:00 Received: 09/02/16 13:55 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 4-Bromophenylphenyl ether NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 101-55-3 Butylbenzylphthalate NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 85-68-7 4-Chloro-3-methylphenol NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 59-50-7 bis(2-Chloroethoxy)methane NO ug/L 10.0 1 09/07/16 14:34 09/08/16 15:31 111-91-1 bis(2-Chloroethyl) ether NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 111-44-4 2-Chloronaphthalene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 91-58-7 2-Chlorophenol NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 95-57-8 4-Chlorophenylphenyl ether NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 7005-72-3 Chrysene NO ug/L 5.0 1 09/07/16 14:34 09/08/1615:31 218-01-9 Dibenz(a,h)anthracene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 53-70-3 3,3'-Dichlorobenzidine NO ug/L 25.0 1 09/07/16 14:34 09/08/16 15:31 91-94-1 2,4-Dichlorophenol NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 120-83-2 Diethylphthalate NO ug/L 5.0 1 09107/1614:34 09/08/16 15:31 84-66-2 2,4-Dimethylphenol NO ug/L 10.0 1 09/07/16 14:34 09/08/16 15:31 105-67-9 Dimethylphthalate NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 131-11-3 Di-n-butylphthalate NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 84-74-2 4,6-Dinitro-2-methylphenol NO ug/L 20.0 1 09/07/16 14:34 09/08/16 15:31 534-52-1 2,4-Dinitrophenol NO ug/L 50.0 1 09/07/16 14:34 09/08/16 15:31 51-28-5 2,4-Dinitrotoluene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 121-14-2 2,6-Dinitrotoluene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 606-20-2 Di-n-octylphthalate NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 117-84-0 bis(2-Ethylhe)(yl)phthalate NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 117-81-7 Fluoranthene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 20644-0 Fluorene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 86-73-7 Hexachloro-1,3-butadiene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 87-68-3 Hexachlorobenzene NO uglL 5.0 1 09/07/16 14:34 09/0811615:31 118-74-1 Hexachlorocyclopentadiene NO ug/L 10.0 1 09/07/16 14:34 09/08/16 15:31 77-47-4 Hexachlorcethane NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 67-72-1 Indeno(1,2,3-cd)pyrene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 193-39-5 Isophorone NO ug/L 10.0 1 09/07/16 14:34 09/08/16 15:31 78-59-1 Naphthalene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 91-20-3 Nitrobenzene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 98-95-3 2-Nitrophenol NO ug/L 5.0 1 09107/1614:34 09/0811615:31 88-75-5 4-Nitrophenol NO ug/L 50.0 1 09/07/16 14:34 09/08/16 15:31 100-02-7 N-Nitrosodimethylamine NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 62-75-9 N-Nitroso-di-n-propylamine NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 621-64-7 N-Nitrosodiphenylamine NO ug/L 10.0 1 09/07/16 1434 09/08/16 15:31 86-30-6 2,2'-Oxybis(1-chlorcpropane) NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 108-60-1 Pentachlorophenol NO ug/L 10.0 1 09/07/16 14:34 09/08/16 15:31 87-86-5 Phenanthrene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 85-01-8 Phenol NO ug/L 5.0 1 09/07/16 14:34 09108/1615:31 Pyrene NO ug/L &0 1 09/07/16 14:34 09/08/16 15:31 129-00-0 1,2,4-Tdchlorobenzene NO ug/L 5.0 1 09/07/16 14:34 09/08/16 15:31 120-82-1 2,4,6-Tdchlorophenol NO ug/L 10.0 1 09/07/16 14:34 09/08/16 15:31 88-06-2 Surrogates Nitrobenzene-d5 (S) 62 % 10-120 1 09/07/16 14:34 09/08/16 15:31 4165-60-0 2-Fluorobiphenyl (S) 63 % 15-120 1 09/07/16 14:34 09/08/16 15:31 321-60-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the v ritten consent of Pace Analytical Services, Inc.. Page 5 of 28 aceAnalytical ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92311091 Sample: OUTFALL NO. 4 Lab ID: 92311091001 Collected: 09/02/16 11:00 Received: 09/02/16 13:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 Surrogates Terphenyl-d14 (S) 82 % 11-131 1 09/07/16 14:34 09/08/16 15:31 1718-51-0 Phenol-d6 (S) 25 % 10-120 1 09/07/16 14:34 09/08116 15:31 13127-88-3 2-Fluorophenol(S) 36 % 10-120 1 09/07/16 14:34 09/08/16 15:31 367-12-4 2,4,6-Tribromophenol (S) 85 % 10-137 1 09/07/16 14:34 09/08/16 15:31 118-79-6 624 Volatile Organics Analytical Method: EPA 624 Benzene ND ug/L 2.0 1 09/07/16 18:02 71-43-2 Bromodichloromethane ND ug/L 2.0 1 09/0711618:02 75-27-4 Bromoform ND ug/L 2.0 1 09/07/16 18:02 75-25-2 Bromomethane ND ug/L 2.0 1 09/0711618:02 74-83-9 Carbon tetrachloride ND ug/L 2.0 1 09/07/16 1802 56-23-5 Chlorobenzene ND ug/L 2.0 1 09107/1618:02 108-90-7 Chloroelhane ND ug/L 2.0 1 09/07/16 1802 75-00-3 Chloroform ND ug/L 2.0 1 09/07/16 18:02 67-66-3 Chloromethane ND ug/L 2.0 1 09/07/16 18:02 74-87-3 Dibromochloromethane NO ug/L 2.0 1 09/07/16 18:02 124-48-1 1,2-Dichlorobenzene ND ug/L 2.0 1 09/07/16 18:02 95-50-1 1,3-Dichlorobenzene ND ug/L 2.0 1 09/07/16 18:02 541-73-1 1,4-Dichlorobenzene ND ug/L 2.0 1 09/07/16 18:02 10646-7 1,1-Dichloroethane ND ug/L 2.0 1 09/07/16 18:02 75-34-3 1,2-Dichloroethane ND ug/L 2.0 1 09/07/16 18:02 107-06-2 1,1-Dichloroethene ND ug/L 2.0 1 09/07/16 18:02 75-35-4 cis-1,2-Dichloroethene ND ug/L 2.0 1 09/07/16 18:02 156-59-2 trans-1,2-Dichloroethene ND ug/L 2.0 1 09/07/16 1802 156-60-5 1,2-Dichloropropane ND ug/L 2.0 1 09/07/16 18:02 78-87-5 cis-1,3-Dichloropropene ND ug/L 2.0 1 09/07/16 18:02 10061-01-5 trans-1,3-Dichloropropene ND ug/L 2.0 1 09/07/16 18:02 10061-02-6 Ethylbenzene ND ug/L 2.0 1 09/07/1618:02 10041-4 Methylene Chloride ND ug/L 2.0 1 09/07/16 18:02 75-09-2 1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 09/07/16 18:02 79-34-5 Tetra chloroethe ne ND ug/L 2.0 1 09/07/16 18:02 127-18-4 Toluene ND ug/L 2.0 1 09/07/16 18:02 108-88-3 1,1,1-Trichloroethane ND ug/L 2.0 1 09/07/16 18:02 71-55-6 1,1,2-Trichloroethane ND ug/L 2.0 1 09/07/16 18:02 79-00-5 Trichloroethene ND ug/L 2.0 1 09/07/16 18:02 79-01-6 Trichlorofluoromethane ND ug/L 2.0 1 09/07/16 18:02 75-694 Vinyl chloride ND ug/L 2.0 1 09/07/16 18:02 75-014 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 09/07/16 18:02 460-00-4 Toluene-d8(S) 100 % 70-130 1 09/07/16 18:02 2037-26-5 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 09/07/16 18:02 17060-07-0 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 5.0 1 09/09/16 10:47 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 28 ZI 55'ceAnalyfical'� F ANALYTICAL RESULTS Project: STORMWATER Pace Project No.: 92311091 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 HunlerswIle, NC 28078 (704)875-9092 Sample: OUTFALL NO.4 Lab ID: 92311091001 Collected: 09/02/16 11:00 Received: 09/02/16 13:55 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 9040 pH Analytical Method: EPA 9040 pH 6.1 Std. Units 0.10 1 09/06/16 10:39 H6 Date: 09/13/2016 12:47 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 28 aceAnalytical r miwpacelaDsoxn QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92311091 QC Batch: 327559 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92311091001 METHOD BLANK: 1814964 Associated Lab Samples: 92311091001 Parameter Units Total Petroleum Hydrocarbons mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 09/07/16 08:24 LABORATORY CONTROL SAMPLE: 1814965 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 19.3 96 64-132 MATRIX SPIKE SAMPLE: 1814966 92311274001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L NO 20 13.2 fib 64-132 - Results presented on this page are in the units indicated by the 'Units' column except where an alternate unit is presented to the night of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 28 laceAnalytical' m+wpacefabsam QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntemville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92311091 QC Batch: 327492 Analysis Method: EPA 200.7 OC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92311091001 METHOD BLANK: 1814749 Matrix: Water Associated Lab Samples: 92311091001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Capper ug/L ND 5.0 09/0711618:13 Lead ug/L NO 5.0 09/0711618:13 Zinc ug/L NO 10.0 09/07/1618:13 LABORATORY CONTROL SAMPLE: 1814750 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 484 97 85-115 Lead ug/L 500 455 91 85-115 Zinc uglL 500 457 91 85-115 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1814751 1814752 MS MSD 92310898002 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Copper ug/L 0.84 500 500 1360 1410 104 113 70-130 3 mg/L Lead ug/L 0.11 500 500 562 531 90 84 70-130 6 mg/L Zinc ug/L 5.7 500 500 6240 5910 101 36 70-130 5 M6 mg/L MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1814753 MS 92310972008 Spike Parameter Units Result Conc. Copper ug/L 21.4 500 Lead ug/L ND 500 Zinc ug/L 10.6 500 1814754 MSD Spike MS MSD MS MSD % Rec Conc. Result Result %Rec %Rec Limits RPD 500 510 527 98 101 70-130 3 500 458 474 91 95 70-130 3 500 476 491 93 96 70-130 3 Results presented on this page are In the units indicated by the'Units' column eacept where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Qua[ Page 9 of 28 aceAnalytical mwwpace/nhs.com QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 OC Batch: 327676 Analysis Method: EPA 624 QC Batch Method: EPA 624 Analysis Description: 624 MSV Associated Lab Samples: 92311091001 METHOD BLANK: 1815839 Associated Lab Samples: 92311091001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,1,1-Tdchloroethane ug/L ND 2.0 09107/1612:03 1, 1,2,2-Tetrachloroethane ug/L NO 2.0 09/07/16 12:03 1,1,2-Trichloroethane ug/L NO 2.0 09/07/16 12:03 1,1-Dichloroethane ug/L NO 2.0 09/07/16 12:03 1,1-Dichloroethene ug/L NO 2.0 09/07/1612:03 1,2-Dichlorobenzene ug/L NO 2.0 09/07/16 12:03 1,2-Dichloroethane ug/L NO 2.0 09/07/16 12:03 1,2-Dichloropropane ug/L NO 2.0 09/07/16 12:03 1,3-Dichlorobenzene ug/L NO 2.0 09/07/16 12:03 1,4-Dichlorobenzene ug/L ND 2.0 09/07/16 12:03 Benzene ug/L NO 2.0 09/07/16 12:03 Bromodichloromethane ug/L ND 2.0 09/07/16 12:03 Bromoform ug/L ND 2.0 09/07/16 12:03 Bromomelhane ug/L ND 2.0 09/0711612:03 Carbon tetrachloride ug/L NO 2.0 09/07/16 12:03 Chlorobenzene ug/L NO 2.0 09/07/1612:03 Chlomethane ug/L NO 2.0 09/0711612:03 Chloroform ug/L NO 2.0 09/0711612:03 Chloromethane ug/L NO 2.0 09/07/16 12:03 cis-1,2-Dichloroethene ug/L NO 2.0 09/07/16 12:03 cis-1,3-Dichloropropene ug/L NO 2.0 09/07/16 12:03 Dibromochloromethane ug/L NO 2.0 09/07/16 12:03 Ethylbenzene ug/L NO 2.0 09/07/1612:03 Methylene Chloride ug/L ND 2.0 09/07/16 12:03 Tetrachloroethene ug/L NO 2.0 09/07/161203 Toluene ug/L NO 2.0 09/07/16 12:03 trans-1,2-Dichloroethene ug/L ND 2.0 09/07/16 12:03 trans-1,3-Dichloropropene ug/L ND 2.0 09/07/16 12:03 Trichloroethene ug/L NO 2.0 09/07/16 12:03 Trichlorofluoromethane ug/L NO 2.0 09/07/16 12:03 Vinyl chloride ug/L NO 2.0 09/07/16 12:03 1,2-Dichloroethane-d4 (S) % 99 70-130 09/07/16 12:03 4-Bromofluorobenzene (S) % 99 70-130 09/07/16 12:03 Toluene-d8 (S) % 103 70-130 09/07/16 12:03 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1815840 Spike LCS LCS % Rec Parameter Units Conic. Result % Rec Limits Qualifiers 1,1,1-Trichloroethane ug/L 20 24.3 122 52-162 1,1,2,2-Tetrachloroethane ug/L 20 20.5 103 46-157 Results presented on this page are in the units indicated by the -units" column except where an alternate unit is presented to the night of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09113/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 28 ace Analytical x pacelaGemm QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville. NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92311091 LABORATORY CONTROL SAMPLE: 1815840 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,2-Trichloroethane uglL 20 20A 100 52-150 1,1-Dichloroethane uglL 20 22.8 114 59-155 1,1-Dichloroethene ugll- 20 24.5 123 1-234 1,2-Dichlorobenzene ug/L 20 22.7 113 18-190 1,2-Dichloroethane ug/L 20 21.6 108 49-155 1,2-Dichloropropane ug/L 20 21.3 106 1-210 1,3-Dichlorobenzene ug/L 20 22.5 112 59-156 1,4-Dichlorobenzene ug/L 20 22.4 112 18-190 Benzene ug/L 20 22.6 113 37-151 Bromodichloromethane ug/L 20 22.0 110 35-155 Bromoforn ug/L 20 21.0 105 45-169 Bromcmethane ug/L 20 26.3 132 1-242 Carbon tetrachloride ug/L 20 24.4 122 70-140 Chlorobenzene ug/L 20 22.1 110 37-160 Chloroethane ug/L 20 21.2 106 14-230 Chloroform ug/L 20 23.1 116 51-138 Chloromethane ug/L 20 23.9 120 1-273 cis-1,2-Dichloroethene ug/L 20 22.9 115 68-146 cis-1,3-Dichloropropene ug/L 20 22.2 111 1-227 Dibromochloromethane ug/L 20 23.1 116 53-149 Ethylbenzene ug/L 20 22.0 110 37-162 Methylene Chloride ug/L 20 23.9 120 1-221 Tetrachloroethene ugll- 20 22.9 114 64-148 Toluene ug/L 20 21.9 109 47-150 trans-1,2-Dichloroethene ug/L 20 24.0 120 54-156 trans-1,3-Dichloropropene ug/L 20 21.2 106 17-183 Trichloroethene ug/L 20 22.7 113 71-157 Tdchlorofiuoromethane ug/L 20 23.0 115 17-181 Vinyl chloride ug/L 20 22.7 113 1-251 1,2-Dichloroethane-d4 (S) % 100 70-130 4-Brcmofluorobenzene (S) % 100 70-130 Toluene-d8(S) % 98 70-130 MATRIX SPIKE SAMPLE: 1815842 92311128003 Spike MS MS % Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers 1,1,1-Trichloroethane ug/L ND 20 25.8 129 46-171 1, 1,2,2-Tetrachloroethane ug/L ND 20 22.1 111 73-159 1, 1,2-Trichloroethane ug/L ND 20 21.5 107 64-152 1,1-Dichloroethane ug/L ND 20 24.5 122 43-172 1,1-Dichloroethene ug/L ND 20 28.6 143 48-189 1,2-Dichlorobenzene ug/L ND 20 23.2 116 54-154 1,2-Dichloroethane ug/L ND 20 22.3 111 42-171 1,2-Dichloropropane ug/L ND 20 22.7 113 55-157 1,3-Dichlorobenzene ug/L ND 20 23.7 118 57-148 Results presented on this page are in the units indicated by the 'Units' column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 28 aceAnalytical xewpece/aDscam QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92311091 MATRIX SPIKE SAMPLE: 1815842 92311128003 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,4-Dichlorobenzene ug/L ND 20 22.6 113 58-149 , Benzene ug/L ND 20 24.7 124 54-163 Bromodichloromethane ug/L ND 20 22.6 113 56-152 Bromofonn ug/L ND 20 21.7 109 53-151 Bromomelhane ug/L ND 20 23.4 117 10-200 Carbon tetrachloride ug/L ND 20 26.5 132 41-175 Chlorobenzene ug/L ND 20 23.9 119 67-152 Chloroethane ug/L ND 20 23.1 116 23-200 Chloroform ug/L ND 20 24.3 122 51-166 Chloromethane ug/L ND 20 22.8 110 40-175 cis-1,2-Dichloroethene ug/L ND 20 24.6 123 45-174 cis-1,3-Dichloropropene ug/L ND 20 22.6 113 38-146 Dibromochloromethane ug/L ND 20 23.3 117 65-144 Ethylbenzene ug/L ND 20 24.1 121 57-152 Methylene Chloride ug/L ND 20 25.0 125 40-167 Tetrachloroethene ug/L ND 20 24.9 119 59-155 Toluene ug/L ND 20 24.2 120 47-162 trans-1,2-Dichloroethene ug/L ND 20 26.0 130 47-178 trans-1,3-Dichloropropene ug/L ND 20 21.2 106 39-148 Trichloroethene ug/L ND 20 24.5 123 60-153 Tnchlorofluoromethane ug/L ND 20 26.0 130 42-199 Vinyl chloride ug/L ND 20 23.2 116 46-176 1,2-Dichloroethane-d4 (S) % 105 70-130 4-Bromofuorobenzene (S) % 97 70-130 Toluene-d8(S) % 99 70-130 SAMPLE DUPLICATE: 1815841 92311128002 Dup Parameter Units Result Result RPD Qualifiers 1,1,1-Trichloroethane ug/L ND ND 1,1,2,2-Tetrachloroethane ug/L ND ND 1,1,2-Trichloroethane ug/L ND ND 1,1-Dichloroethane ug/L ND ND 1,1-Dichloroethene ug/L ND ND 1,2-Dichlorobenzene ug/L ND ND 1,2-Dichloroethane ug/L ND ND 1,2-Dichloropropane ug/L ND ND 1,3-Dichlorobenzene ug/L ND ND 1,4-Dichlorobenzene ug/L ND ND Benzene ug/L ND ND Bromodichloromethane ug/L ND ND Bromoform ug/L ND ND Bromomethane ug/L ND ND Carbon tetrachloride ug/L ND ND Chlorobenzene ug/L ND ND Results presented on this page are in the units indicated by the -Unite' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM vdthout the written consent of Pace Analytical Services, Inc.. Page 12 of 28 aceAnalytical wuwpacelabsam QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 SAMPLE DUPLICATE: 1815841 Parameter Units 92311128002 Result Dup Result Chloroethane ug/L NO NO Chloroform ug/L NO NO Chloromethane ug/L NO NO cis-1,2-Dichloroethene ug/L NO NO cis-1,3-Dichloropropene ug/L NO NO Dibromochloromethane ug/L ND NO Ethylbenzene ug/L ND NO Methylene Chloride ug/L ND NO Tetrachlomethene ug/L ND NO Toluene ug/L NO NO trans-1,2-Dichloroethene ug/L ND NO trans-1,3-Dichloropropene ug/L ND NO Trichloroethene ug/L NO NO Trichlorofluoromethane ug/L NO NO Vinyl chloride ug/L NO NO 1,2-Dichloroethane-d4 (S) % 99 103 4-Bromofluorobenzene (S) % 98 99 Toluene-d8 (S) % 103 103 RPD Qualifiers 3 1 0 Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented an this page arc in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall net be reproduced, except in full, Dale: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 28 aceAnalytical w»w.pnelab&. QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 QC Batch: 327752 Analysis Method: EPA 608 QC Batch Method: EPA 3510 Analysis Description: 608 GCS Pest PCB Associated Lab Samples: 92311091001 METHOD BLANK: 1816118 Associated Lab Samples: 92311091001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 4,4'-DDD ug/L ND 0.050 09/09/16 22:35 4,4'-DDE ug/L ND 0.050 09/09/16 22:35 4,4'-DDT ug/L ND 0.050 09109/1622:35 Aldrin ug/L ND 0.050 09/09/16 22:35 alpha-BHC ug/L ND 0.050 09/09/16 22:35 beta-BHC ug/L NO 0.050 09/09/16 22:35 Chlordane (Technical) ug/L NO 0.50 09/09/16 22:35 delta-BHC ug/L ND 0.050 09/09/16 22:35 Dieldrin ug/L NO 0.050 09/09/16 22:35 Endosulfan I ug/L ND 0.050 09/09/16 22:35 Endosulfan II ug/L NO 0.050 09/09/16 22:35 Endosulfan sulfate ug/L ND 0.050 09/09/16 22:35 Endrin ug/L ND 0.050 09/09/16 22:35 Endrin aldehyde ug/L ND 0.050 09/09/16 22:35 gamma-BHC (Lindane) ug/L ND 0.050 09/09/16 22:35 Heptachlor ug/L ND 0.050 09/09/16 22:35 Heptachlor epoxide ug/L ND 0.050 09/0911622:35 PCB-1016 (Aroclor 1016) ug/L NO 0.50 09/09/16 22:35 PCB-1221(Aroclor 1221) ug/L NO 0.50 09/0911622:35 PCB-1232 (Aroclor 1232) ug/L ND 0.50 09/09/16 22:35 PCB-1242 (Aroclor 1242) ug/L NO 0.50 09/09/16 22:35 PCB-1248 (Aroclor 1248) ug/L ND 0.50 09/09/16 22:35 PCB-1254 (Aroclor 1254) ug/L NO 0.50 09/09/16 22:35 PCB-1260 (Aroclor 1260) ug/L ND 0.50 09/09/16 22:35 Toxaphene ug/L ND 0.50 09/09/16 22:35 Decachlorobiphenyl (S) % 72 20-138 09/09/16 22:35 Tetrachloro-m-xylene (S) % 67 20-110 09/09/16 22:35 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078' (704)8759092 LABORATORY CONTROL SAMPLE: 1816119 Spike LCS LCS % Red Parameter Units Cone. Result % Rec Limits Qualifiers 4,4'-DDD ug/L .25 0.23 93 31-141 4,4'-DDE 1 .25 0.21 84 30-145 4,4'-DDT ug/L .25 0.19 78 25-160 Aldrin ug/L .25 0.19 77 42-122 alpha-BHC ug/L .25 0.22 88 37-134 beta-BHC ug/L .25 0.22 90 17-147 delta-BHC ug/L .25 0.22 87 19-140 Dieldrin ug/L .25 0.21 83 36-146 Endosulfan I ug/L .25 0.22 90 45-153 Results presented on this page arc in the units indicated by the 'Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 28 (1ceAnalytical" .pacelabs<ym QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)878-9092 Project: STORMWATER Pace Project No.: 92311091 LABORATORY CONTROL SAMPLE: 1816119 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Endosulfan II ug/L .25 0.23 93 1-202 Endosulfan sulfate ug/L .25 0.24 96 26-144 Endrin ug/L .25 0.24 96 30-147 Endrin aldehyde ug/L .25 0.20 81 50-150 gamma-BHC (Lindane) ug/L .25 0.22 90 32-127 Heptachlor uglL .25 0.21 84 34-111 Heptachlor epoxide ug/L .25 0.22 87 41-126 Decachlorobiphenyl (S) % 47 20-138 Tetrachloro-m-xylene (S) % 85 20-110 MATRIX SPIKE SAMPLE: 1816120 92311094002 Spike MS MS e/ Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 4,4'-DDD ug/L NO .25 0.15 60 31-141 4,4'-DDE ug/L ND .25 0.15 59 30-145 4,4'-DDT ug/L ND .25 0.15 60 25-160 Aldrin ug/L ND .25 0.14 55 42-122 alpha-BHC ug/L NO .25 0.15 59 37-134 beta-BHC ug/L ND .25 0.17 70 17-147 delta-BHC ug/L ND .25 0.15 59 19-140 Dieldrin ug/L ND .25 0.14 56 36-146 Endosulfan I ug/L NO .25 0.16 65 45-153 Endosulfan II ug/L NO .25 0.15 62 1-202 Endosulfan sulfate ug/L NO .25 0.16 65 26-144 Endrin ug/L NO .25 0.17 68 30-147 Endrin aldehyde ug/L NO .25 0.13 53 50-150 gamma-BHC (Lindane) ug/L NO .25 0.15 59 32-127 Heptachlor ug/L NO .25 0.15 62 34-111 Heptachlor epoxide ug/L NO .25 0.14 57 41-126 Decachlorobiphenyl (S) % 21 20-138 Tetrachloro-m-xylene (S) % 61 20-110 SAMPLE DUPLICATE: 1816121 92311094003 Dup Parameter Units Result Result RPD Qualifiers 4,4'-DDD ug/L NO ND 4,4'-DOE ug/L ND NO 4,4'-DDT ug/L ND NO Aldrin ug/L ND ND alpha-BHC ug/L ND ND beta-BHC ug/L ND NO Chlordane (Technical) ug/L ND ND delta-BHC ug/L ND ND Dieldrin ug/L ND NO Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 28 �;ZeAnalj6cal' l b,wwP.ce1ah& n I QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 SAMPLE DUPLICATE: 1816121 Parameter Units 92311094003 Result Dup Result Endosulfan I ug/L NO NO Endosulfan II ug/L NO NO Endosulfan sulfate ug/L NO NO Endrin ug/L NO NO Endrin aldehyde ug/L NO NO gamma-BHC (Lindane) ug/L ND NO Heptachlor ug/L ND NO Heptachlor epoxide ug/L ND NO PCB-1016 (Aroclor 1016) ug/L ND ND PCB-1221 (Aroclor 1221) ug/L NO NO PCB-1232 (Aroclor 1232) ug/L NO NO PCB-1242 (Aroclor 1242) ug/L NO ND PCB-1248 (Aroclor 1248) ug/L NO NO PCB-1254 (Aroclor 1254) ug/L NO NO PCB-1260 (Aroclor 1260) ug/L NO ND Toxaphene ug/L NO NO RPD Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 28 aceAnalytical 1 QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 QC Batch: 327638 Analysis Method: EPA 625 QC Batch Method: EPA625 Analysis Description: 625 MSS Associated Lab Samples: 92311091001 METHOD BLANK: 1815492 Associated Lab Samples: 92311091001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,2,4-Trichlorobenzene ug/L ND 5.0 09/08/16 12:15 2,2'-Oxy1bis(1-chlorcpropane) ug/L NO 5.0 09/08/16 12:15 2,4,6-Trichlorophenol ug/L ND 10.0 09/08/16 12:15 2,4-Dichlorophenol ug/L NO 5.0 09/08/16 12:15 2,4-Dimethylphenol ug/L NO 10.0 09/08/16 12:15 2,4-Dinitrophenol ug/L ND 50.0 09/08/16 12:15 2,4-Dinitrotoluene ug/L ND 5.0 09/0811612:15 2,6-Dinitrotoluene ug/L NO 5.0 09/0811612:15 2-Chloranaphthalene ug/L NO 5.0 09/08/1612:15 2-Chlorophenol ug/L NO 5.0 09/08/16 12:15 2-Nitrophenol ug/L NO 5.0 09/08/1612:15 3,3'-Dichlorobenzidine uglL NO 25.0 09/0811612:15 4,6-Dinitro-2-methylphenol ug/L NO 20.0 09/0811612:15 4-Bromophenylphenyl ether ug/L NO 5.0 09/08/16 12:15 4-Chloro-3-methylphenol ug/L NO 5.0 09/08/16 12:15 4-Chlorophenylphenyl ether ug/L NO 5.0 09/08/16 12:15 4-Nitrophenol ug/L NO 50.0 09108/1612:15 Acenaphthene ug/L NO 5.0 09/08/1612:15 Acenaphthylene ug/L ND 5.0 09/08/16 12:15 Anthracene ug/L NO 5.0 09/08/16 12:15 Benzo(a)anthracene ug/L NO 5.0 09/08/16 12:15 Benzo(a)pyrene ug/L NO 5.0 09108/1612:15 Benzo(b)fluoranthene ug/L NO 5.0 09/08/16 12:15 Benzo(g,h,i)perylene ug/L NO 5.0 09/08/16 12:15 Benzo(k)fluoranthene ug/L ND 5.0 09/08/16 12:15 bis(2-Chloroethoxy)methane ug/L ND 10.0 09/08/16 1215 bis(2-Chloroethyl) ether ug/L ND 5.0 09/08/16 12:15 bis(2-Ethylhexyl)phthalate ug/L ND 5.0 09/08/16 12:15 Butylbenzylphthalate ug/L ND 5.0 09/08/161215 Chrysene ug/L ND 5.0 09/08/16 12:15 Di-n-butylphthalate i ND 5.0 09/08/16 12:15 Di-n-octylphthalate ug/L ND 5.0 09/0811612:15 Dibenz(a,h)anthracene ug/L NO 5.0 09/08/16 12:15 Diethylphthalate ug/L NO 5.0 09/08/16 12:15 Dimethylphthalate ug/L NO 5.0 09/08/16 12:15 Fluoranthene ug/L NO 5.0 09/08/16 12:15 Fluorene ug/L NO 5.0 09/08/16 12:15 Hexachloro-1,3-butadiene ug/L NO 5.0 09/08/16 12:15 Hexachlorobenzene ug/L NO 5.0 09/08/16 12:15 Hexachlorocyclopentadiene ug/L NO 10.0 0910811612:15 Hexachloroethane ug/L NO 5.0 09108/1612:15 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09113/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 28 aceAnalytical www.parek6s.can QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 METHOD BLANK: 1815492 Matrix: Water Associated Lab Samples: 92311091001 Blank Reporting Parameter Units Result Limit Analyzed Indeno(1,2,3-cd)pyrene ug/L NO 5.0 09/08/16 12:15 Isophorone ug/L NO 10.0 09/0811612:15 N-Nitroso-di-n-propylamine ug/L NO 5.0 09/08/16 12:15 N-Nitrosodimethylamine ug/L NO 5.0 09/08/16 12:15 N-Nitrosodiphenylamine ug/L NO 10.0 09/08/1612:15 Naphthalene ug/L NO 5.0 09/08/16 12:15 Nitrobenzene ug/L NO 5.0 09/0811612:15 Pentachlorophenol ug/L NO 10.0 09/0811612:15 Phenanthrene ug/L ND 5.0 09108/1612,15 Phenol ug/L NO 5.0 09/08/16 12:15 Pyrene ug/L ND 5.0 09108/1612:15 2,4,6-Thbromophenol(S) % 97 10-137 09/08/16 12:15 2-Fluorobiphenyl(S) % 84 15-120 09/08/16 12:15 2-Fluorophenol (S) % 49 10-120 09/08/16 12:15 Nitrobenzene-d5 (S) % 89 10-120 09/08/16 12:15 Phenol-d6 (S) % 32 10-120 09/08/1612:15 Terphenyl-d 14 (S) % 104 11-131 09/08/16 12:15 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1815493 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2,4-Trichlorobenzene ug/L 50 25.3 51 44-142 2,2'-Oxybis(1-chloropropane) ug/L 50 42.7 85 36-166 2,4,6-Trichlorophenol ug/L 50 50.4 101 37-144 2,4-Dichlorophenol ug/L 50 45.1 90 1-191 2,4-Dimethylphenol ug/L 50 51.4 103 32-119 2,4-Dinitrophenol ug/L 250 173 69 1-181 2,4-Dinitrotoluene ug/L 50 50.5 101 39-139 2,6-Dinitrotoluene ug/L 50 51.4 103 50-158 2-Chloronaphthalene ug/L 50 33.0 66 60-118 2-Chlorophenol ug/L 50 39.9 80 23-134 2-Nitrophenol ug/L 50 49.7 99 29-182 3,3'-Dichlorobenzidine ug/L 100 84.7 85 1-262 4,6-Dinitro-2-methylphenol ug/L 100 112 112 1-181 4-Bromophenylphenyl ether ug/L 50 47.5 95 53-127 4-Chloro-3-methylphenol ug/L 100 75.9 76 22-147 4-Chlorophenylphenyl ether ug/L 50 41.0 82 25-158 4-Nitrophenol ug/L 250 106 42 1-132 Acenaphthene ug/L 50 37.9 76 47-145 Acenaphthylene ug/L 50 41.5 83 33-145 Anthracene ug/L 50 48.9 98 1-166 Benzc(a)anthracene ug/L 50 47.6 95 33-143 Benzo(a)pyrene ug/L 50 44.9 90 17-163 Benzc(b)fiuoranthene ug/L 50 47.9 96 24-159 Pace Analytical services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 ' (704)8759092 Qualifiers Results presented on this page are in the units indicated by the -Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 28 aceAnalytical® I P QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Project: STORMWATER Pace Project No.: 92311091 LABORATORY CONTROL SAMPLE: 1815493 Spike LCS LCS %Rec Parameter Units Cone. Result % Rae Limits Qualifiers Benzo(g,h,i)perylene ug/L 50 47.8 96 1-219 Benzo(k)fluoranthene ug/L 50 46.5 93 11-162 bis(2-Chloroethoxy)methane ug/L 50 42.6 85 33-184 bis(2-Chloroethyl) ether ug/L 50 41.1 82 12-158 bis(2-Ethylhexyl)phthalate ug/L 50 56.6 113 8-158 Butylbenzylphthalate ug/L 50 59.5 119 1-152 Chrysene ug/L 50 46.0 92 17-168 Di-n-butylphthalate ug/L 50 52.9 106 1-118 Di-n-octylphthalate ug/L 50 56.6 113 4-146 Dibenz(a,h)anlhracene ug/L 50 46.4 93 1-227 Diethylphthalate ug/L 50 44.5 89 1-114 Dimethylphthalale ug/L 50 44.2 88 1-112 Fluoranthene ug/L 50 45.9 92 26-137 Fluorene ug/L 50 43.2 86 59-121 Hexachloro-1,3-butadiene ug/L 50 20.7 41 24-116 Hexachlorobenzene ug/L 50 49.7 99 1-152 Hexachlorocyclopentadiene ug/L 50 24.1 48 25-150 Hexachloroethane ug/L 50 21A 42 40-113 Indeno(1,2,3-cd)pyrene ug/L 50 46.6 93 1-171 Isophorone ug/L 50 47.2 94 21-196 N-Nitroso-di-n-propylamine ug/L 50 39.3 79 1-230 N-Nitrosodimethylamine ug/L 50 22.0 44 25-150 N-Nitrosodiphenylamine ug/L 50 46.7 93 25-150 Naphthalene ug/L 50 31.3 63 21-133 Nitrobenzene ug/L 50 46.0 92 35-180 Pentachlorophenol ug/L 100 105 105 14-176 Phenanthrene ug/L 50 47.3 95 54-120 Phenol ug/L 50 21.3 43 5-112 Pyrene ug/L 50 49.5 99 52-115 2,4,6-Tribromophenol (S) % 114 10-137 2-Fluorobiphenyl(S) % 75 15-120 2-Fluorophenol (S) % 51 10-120 Nitrobenzene-d5 (S) % 81 10-120 Phenol-d6 (S) % 35 10-120 Terphenyl-d14 (S) % 100 11-131 MATRIX SPIKE SAMPLE: 1815494 92311124009 Spike MS MS % Rae Parameter Units Result Cone. Result % Rae Limits Qualifiers 1,2,4-Thchlorobenzene ug/L NO 50 30.0 60 44-142 2,2'-Oxybis(1-chloropropane) ug/L ND 50 43.0 86 36-166 2,4,6-Thchlorophenol ug/L NO 50 55.2 110 37-144 2,4-Dichlorophenol ug/L NO 50 45.6 91 1-191 2,4-Dimethylphenol ug/L NO 50 49.1 98 32-119 2,4-Dinitrophenol ug/L NO 250 167 67 1-181 Results presented on this page are in the units indicated by the -units" column except where an altemate unit is presented to the tight of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 28 aceAnalytical t wwwpacelabscom QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NO 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92311091 MATRIX SPIKE SAMPLE: 1815494 92311124009 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2,4-Dinitrotoluene ug/L ND 50 56.9 114 39-139 2,6-Dinitrotoluene ug/L ND 50 58.6 117 50-158 2-Chloranaphthalene ug/L ND 50 43.1 86 60-118 2-Chlorophencl ug/L ND 50 41.2 82 23-134 2-Nitrophenol ug/L NO 50 57.7 115 29-182 3,3'-Dichlorobenzidine ug/L ND 100 84.0 84 1-262 4,6-Dinitro-2-methylphenol ug/L NO 100 110 110 1-181 4-Bromophenylphenyl ether ug/L NO 50 49.2 98 53-127 4-Chloro-3-methylphenol ug/L ND 100 86.5 86 22-147 4-Chlorophenylphenyl ether ug/L NO 50 47.3 95 25-158 4-Nitrophenol ug/L NO 250 125 50 1-132 Acenaphthene ug/L NO 50 44.4 89 47-145 Acenaphthylene ug/L NO 50 47.3 95 33-145 Anthracene ug/L NO 50 48.3 97 1-166 Benzo(a)anthracene ug/L ND 50 49.2 98 33-143 Benzo(a)pyrene ug/L NO 50 46.0 92 17-163 Benzo(b)fluoranthene ug/L ND 50 48.4 97 24-159 Benzo(g,h,i)perylene ug/L ND 50 46.9 94 1-219 Benzo(k)fluoranthene ug/L ND 50 45.1 90 11-162 bis(2-Chloroethoxy)methane ug/L NO 50 43.9 88 33-184 bis(2-Chloroethyl) ether ug/L ND 50 42.5 85 12-158 bis(2-Ethylhexyl)phthalate ug/L NO 50 59.6 119 8-158 Butylbenzylphthalate ug/L NO 50 60.7 121 1-152 Chrysene ug/L NO 50 47.8 96 17-168 Di-n-butylphthalate ug/L NO 50 52.7 105 1-118 Di-n-octylphthalate ug/L NO 50 59.0 118 4-146 Dibenz(a,h)anthracene ug/L NO 50 46.6 93 1-227 Diethylphthalate ug/L NO 50 46.8 94 1-114 Dimethylphthalate ug/L NO 50 45.3 91 1-112 Fluoranthene ug/L NO 50 49.4 99 26-137 Fluorene ug/L NO 50 48.3 97 59-121 Hexachloro-1,3-butadiene ug/L NO 50 24.3 49 24-116 Hexachlorobenzene ug/L ND 50 49.8 100 1-152 Hexachlorocyclapentadiene ug/L ND 50 34.8 70 25-150 Hexachloroethane ug/L NO 50 22.3 45 40-113 Indeno(1,2,3-cd)pyrene ug/L NO 50 46.1 92 1-171 Isopharone ug/L NO 50 44.8 90 21-196 N-Nitroso-di-n-propylamine ug/L NO 50 37.6 75 1-230 N-Nitrosodimethylamine ug/L NO 50 23.9 48 25-150 N-Nitrosodiphenylamine ug/L NO 50 45.5 91 25-150 Naphthalene ug/L NO 50 35.1 70 21-133 Nitrobenzene ug/L NO 50 49.1 98 35-180 Pentachlorophenol ug/L NO 100 109 109 14-176 Phenanthrene ug/L NO 50 49.4 99 54-120 Phenol ug/L NO 50 22.5 45 5-112 Pyrene ug/L ND 50 52.4 105 52-115 2,4,6-Tribromophenol(S) % 117 10-137 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the wntten consent of Pace Analytical Services, Inc.. Page 20 of 28 aceAnalytical / wwwpeae/aAscam QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 Pace Analytical Services, Inc. 9800 Kinney Ave. Suite 100 Huntersville, NC 28078 (704)8759092 MATRIX SPIKE SAMPLE: 1815494 92311124009 Spike MS MS % Rec Parameter Units Result Conc. Result % Red Limits Qualifiers 2-Fluorobiphenyl (S) % 87 15-120 2-Fluorophenol(S) % 55 10-120 Nitrobenzene-d5 (S) % 88 10-120 Phenol-d6 (S) % 39 10-120 Terphenyl-d 14 (S) % 93 11-131 SAMPLE DUPLICATE: 1815495 Parameter Units 92311091001 Result Dup Result 1,2,4-Trichlorobenzene ug/L NO NO 2,2'-Oxybis(1-chloropropane) ug/L ND ND 2,4,6-Trichlorophenol ug/L ND ND 2,4-Dichlorophenol ug/L ND ND 2,4-Dimethylphenol ug/L ND ND 2,4-Dinitrophenol ug/L ND ND 2,4-Dinitrotoluene ug/L ND ND 2,6-Dinitrotoluene ug/L ND ND 2-Chloronaphthalene ug/L ND ND 2-Chlorophenol ug/L ND ND 2-Nitrophenol ug/L ND ND 3,3'-Dichlorobenzidine ug/L ND ND 4,6-Dinitro-2-methyl phenol ug/L ND ND 4-Bromophenylphenyl ether ug/L NO NO 4-Chloro-3-methylphenol ug/L NO NO 4-Chlorophenylphenyl ether ug/L NO NO 4-Nitrophenol ug/L NO NO Acenaphthene ug/L NO NO Acenaphthylene ug/L NO NO Anthracene ug/L ND NO Benzo(a)anthracene ug/L NO ND Benzo(a)pyrene ug/L NO ND Benzo(b)fluoranthene ug/L ND ND Benzo(g,h,i)perylene ug/L NO NO Benzo(k)fluoranthene ug/L NO NO bis(2-Chlaroethoxy)methane ug/L ND NO bis(2-Chloroethyl) ether ug/L ND NO bis(2-Ethylhexyl)phthalate ug/L NO NO Butylbenzylphthalate ug/L ND NO Chrysene ug/L ND NO Di-n-butylphthalate ug/L ND NO Di-n-actylphthalate ug/L ND NO Dibenz(a,h)anthracene ug/L ND NO Diethylphthalale ug/L ND NO Dimethylphthalate ug/L ND NO Fluoranthene ug/L ND NO RPD Qualifiers Results presented on this page are in the units indicated by the -Unite- column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 28 ace Analytical' waw.pacekbs.cgn QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92311091 SAMPLE DUPLICATE: 1815495 Parameter Units 92311091001 Result Dup Result Fluorene ug/L ND ND Hexachloro-1,3-butadiene ug/L ND ND Hexachlorobenzene ug/L ND ND Hexachlorocyclopentadiene ug/L ND ND Hexachloroethane ug/L ND ND Indeno(1,2,3-cd)pyrene ug/L ND ND Isophorone ug/L ND ND N-Nitroso-di-n-propylamine ug/L ND ND N-Nitrosodimethylamine ug/L ND ND N-Nitrosodiphenylamine ug/L ND ND Naphthalene ug/L ND ND Nitrobenzene ug/L ND ND Pentachlorophenol ug/L ND ND Phenanthrene ug/L ND ND Phenol ug/L ND ND Pyrene ug/L ND ND 2,4,6-Tribromophenol(S) % 85 96 2-Fluorobiphenyl (S) % 63 79 2-Fluorophenol(S) % 36 42 Nitrobenzene-d5 (S) % 62 73 Phenol-d6 (S) % 25 25 Terphenyl-d14 (S) % 82 87 RPD Qualifiers 12 23 17 15 1 5 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 " (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 28 aceAnalytical / mrwpacelabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvllle, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92311091 QC Batch: 327933 Analysis Method: SM 2540D OC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92311091001 METHOD BLANK: 1817160 Matrix: Water Associated Lab Samples: 92311091001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L NO 2.5 09/09/16 10:47 LABORATORY CONTROL SAMPLE: 1817161 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 248 99 90-110 SAMPLE DUPLICATE: 1817162 92311091001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND NO SAMPLE DUPLICATE: 1817163 92311112005 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 13.6 17.0 22 D6 Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/13/2016 12:47 PM without the wnuen consent of Pace Analytical Services, Inc.. Page 23 of 28 aceAnalytical wxw.pecelabsaxn QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite100 Huntersville, NC 28078 ` (704)875-9092 Project: STORMWATER Pace Project No.: 92311091 QC Batch: 327407 Analysis Method: EPA 9040 QC Batch Method: EPA9040 Analysis Description: 9040 pH Associated Lab Samples: 92311091001 SAMPLE DUPLICATE: 1814193 Parameter pH 92310609002 Dup Units Result Result RPD Qualifiers Std. Units 8.1 8.1 0 H6 Results presented on this page are In the units indicated by the 'Units-- column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 09/13/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 24 of 28 �;ZeAnalytical' r.pareJabsarn QUALIFIERS Project: STORMWATER Pace Project No.: 92311091 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. POL- Practical Quantitalion Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvllle, NC 28078 (704A75-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D)- Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA required holding time. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 09113/2016 12:47 PM without the written consent of Pace Analytical Services, Inc.. Page 25 of 28 (:�;ZeAnalytical' nwwpace/x6.ccam QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)878-9092 Project: Pace Project No.: STORMWATER 92311091 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92311091001 OUTFALL NO. 4 EPA 1664E 327559 92311091001 OUTFALL NO. 4 EPA 3510 327752 EPA 608 327914 92311091001 OUTFALL NO.4 EPA 200.7 327492 EPA 200.7 327549 92311091001 OUTFALL NO.4 EPA625 327638 EPA 625 327818 92311091001 OUTFALL NO.4 EPA 624 327676 92311091001 OUTFALL NO. 4 SM 2540D 327933 92311091001 OUTFALL NO.4 EPA 9040 327407 Date: 09/13/2016 12:47 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 26 of 28 Document Name: Document Revised:April 25, 2016 Sample Condition Upon Receipt(SCUR) Page 1 of 2 111!aCBAnaly6Ca�8 Document No.: Issuing Authority: F-CHR-CS-003-rev.19 Pace Huntersvfl le Quality 0_ ice u nti-4231.1091 O4 . .. Client Name: Project p •®v -- C Courier: OFed Ex ❑UPS ❑USPS ❑Client ,92311091 ❑ Commercial ©P ce ❑Other._ - Custody Seal Present? ❑Yes 090 Sealslntact? k]Yes ❑No _ �t"s Date/Initials Person Examining Contents. - r^i 0 Packing Material: ❑Bubble Wrap 089U6le Bags ❑None ❑other:_ Thermometer: T1505 Type of)e: ❑VJet []slue ❑None ampies on ice, cooling process has begun Correction Factor: 0.0-C Cooler Temp Corrected (°C): . -(7 Biological Tissue Frozen? ❑Yes ❑No ONE Temp should he above f�reee Ing to 6'C USDA Regulated Soil ([xN/A, water sample) Did samples o¢ginate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internatlo ally, ;,..I, igine Hawaii and Puerto Rico)? ❑Yes ❑Yes DKO ...-._.... Com menu/DI sere pa ncy: Chain of Custody Present? s ONO ❑N/A 1. Samples Arrived within Hold Time? Elyi,, ONO ❑N/A 2. Short Hold Time Analysis (<72 hr.)? ❑yes Oil [:]N/A 3. Rush Turn Around Time Requested? ❑Yes/ ®o ❑N/A 4. Sufficient Volume? ❑�Yess ❑No ❑N/A S. Correct Containers Used? 6 Q�*� ONO ❑N/A 6.. -Pace Containers Used? 111res ONO ❑N/A Containers Intact? ❑Yes ONO ❑N/A 7. ❑Yes ONO Ek%- 8. Note if sediment is visible in the dissolved container Samples Field Filtered? Sample Labels Match COC? ©Yr, ONO ❑N/A 9. -Includes Date/Time/ID/Analysis Matrix: 10. xna00 `xaon<x All containers needing acid/base preservation have been es....❑No --❑N/A ..checked?_._._... _. ____......_ .__.._.... _.....__.. ., All containers needing preservation are found to be in compliance with EPA recommendation? ON. ❑N/A xssoa px« (HNDa, HzSOx HCI<2; N30H >9 Sulfide, NaOH>12 Cyanide) es x.ox pwu Exceptions: VOA, Coliform, TOC, Oil and Grease, s ONO ❑N/A x.ox/z�aa<obs DRO/8015 (water) DOC,LLHg Samples checked for dechlorination? a es' ONO ❑N/A 11. Headspace in VOA Vials (>5-6mm)? Dyes POO ❑N/A 12. Trip Blank Present? Oyes ONO [��13. Trip Blank Custody Seals Present? Oyes ❑No ,.___ r-.. vL.d, I..r a of nu rah accdl• _ CLIENT NOTIFICATION/RESOLUTION Person Contacted:- Comments/Sample. Discrepancy: Date/Time: Field Data Required? f jYes UNO Project Manager SCURF Review: '((— Date: 910A Project Manager SRF Review: TL .Date: q /b//6 Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 27 of 28 II:P CHAIN -OF -CUSTODY 1 Analytical Request Document ::.aceAINMicaf' The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must he completed accurately. Section A Section 8 Section C Required Client Information: Requimd Project information: immice Information: Page : 1 Of 1 Company: CoBax Fluid Handling Report To: Daniel Cox Attention; � Atltlress'. 1710 Airpod Road Copy To :i-/A: %f-: x�-' Company Name. Monroe. NC 28110 5&I{-iJAlGsfi G`.Q)�G Atltlress; -i Regulatory A en Email: darnel cax co8axlluldhandlin .com Purchase Doer p:'. Par»Cuero: Phonei Ooa12Bg.6511 Fax Piojed Name: Slormwmor Pace Projed Manager: liamm.harrisOh@padeiabs com. ,.'ia ">StatelLwation ` Requested Duo Date'. Project N' lPeen Pile #: 6479-2 NC =Rnr.caad Analysis Fit red YiN ij - D CDLLECTED Preservatives >: r%' WE. cone U Q DiNNn9 Ytme ow N U w SAMPLE ID of u START END D ° as a 4 oaysola One Character per Box wm. wP y Omx1 Or u r '� 2. m0 e a a bb Sample Ids mustbe, unique T.. is w o N m m. W .x B e s a m 0 O n DATE TIME DATE TIME y* O z i E O �1^' w u f O e n ¢ ' "fs a� 1}o:%{'eaf lf/irt. 9-2 1t cc V ti ✓ ✓ Uu 2:,x 4 6 tI +1 1 1 't Y 12?: MDITIONAL COMMEMS a.+ r nt S, RELINgUISHED DYtAFFILIATION _u DATES g TIME �r'w� AGCEPim BYI'AFFitAATIDN OATEr)TIME rGi,." SAMPLE CONDITIDNS� .i p Ij ,iZlF�:, .= •. SAMPLER NAME 0.N0 SIGNATURE v, PRINT Name of SAMPLER /. p /�. �,� m SIGNATURE of SAMPLER Se-4`1"�/�- DATE SIgnetl: �ry f & F m = V y o,y y D.y N 0 N m 0 June 15, 2016 Jason Reichert Director, Global Environmental, Health & Safety Colfax Fluid Handling 1710 Airport Road Monroe, North Carolina 28110 Subject: Monthly Stormwater Sampling— May 2016 Certificate of Coverage No. NCG030293 Colfax/11%10 Industries — Monroe, NC Shield Project No. 1150109-02 Dear Mr. Reichert: RECEIVED JUN: 16 2016 CENTRAL FILES DWR SECTION Shield Engineering, Inc. (Shield) successfully collected a monthly stormwater sample for Stormwater Discharge Outfall (SDO) #004 at the Colfax — Monroe facility for the month of May. During the May 17, 2016 sampling event, Shield's field measurement of pH was 7.4 at SDO #004. Total event precipitation was 0.43 inches. In addition to collection of samples, Shield performed Qualitative Monitoring at SDO #004 (attached). As discussed between Melinda M. Greene of Shield and Krista Baker of Colfax on June 7, 2016, Colfax — Monroe facility should complete all relevant sections of the Stormwater Discharge Monitoring Report (DMR) using the results of analyses from the commercial laboratory that the Colfax facility has contracted with and the field pH values indicated above. The completed DMR form should then be mailed along with the Qualitative Monitoring Report Form to the regulatory agency's Central Files. Shield will continue to perform monthly sampling per Tier Two requirements until instructed to halt by Colfax. Shield greatly appreciates the opportunity to provide environmental services to the Colfax/IMO Industries. If you have any questions in reference to this document or require further information, please feel free to contact either of the undersigned at.(704) 394-6913. Respectfully, SHIELD ENGINEERING, INC. /),. ;z l a ' Melinda d. reene Keith A. Anthony, PE Senior En � eer Chief Engineer ATTACHMENT F COPY 001'rojecis\2014\1140109-02 Mount Ilolly SW Sampling 20161120ver Levers\Cover L tier- May 2016 -Nit Holly Facility.docxy.docx 4301 Taggart Creek Road Telephone 704.394.6913 Charlotte, NC 28208 wwwshieldengineering.com Fax 704.394.6968 C� Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 6 15 16 = CERTIFICATE OF COVERAGE No. NCG030293 SAMPLE COLLECTION YEAR 2016 FACILITY NAME Colfax/IMO Industries, Inc. SAMPLE PERIOD ❑ Jan -June ❑ July -Dec PERSON COLLECTING SAMPLES Danny Hefner, Shield Engineering or ® Monthly' May LABORATORY: Pace Analytical Services, Inc. Lab Cert. # 12 DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA Comments on sample collection or analysis: Benchmark was exceeded QZero-flow ❑Water Supply ESA for Copper. RECEIVED ®Other _ClassC—Dry Fork Creek JUN ] 6 2016 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTRAL FILES Part A: Stormwater Benchmarks and Monitoring Results DWR SECTION ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics5 Benchmarks ===> - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SDO 004 05/17/16 0.43 12.2 mg/L 7.4 0.0082 0.005 0.0539 0.638 0.4873 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for 70 monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics - (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." Name (Print name) C�laS birecyBr Title (Print title) 211 r S/G (S ature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc, in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664(SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES x NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports/ to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee) Permit Date:11/1/2012-10/31/2017 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 <i NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this please visit: IILW:/IPO"tal-Ilcticllt'O"glwgb/wu/ws/sull)12(16ssw4tl)-4 Permit No.: or Certificate of Coverage No.: Y/C/G/O/3/ o/ ?/ 3/- Facility Name: CoLr4Y- FLU1- 44AIDL - County: UNloAl Phone No. Inspector: 7c AFG,tfy 1165"W6X— Date of Inspection: Time of Inspection: Total Event Precipitation (inches): 0,13 DW R SECTION RECEIVE�J Was this a'"Representative Storm Event' or "Measureable Storm Event" as efined by the permit? (See information below.) Just 1 G ZU16 fR Yes ❑ No CEN iRAL FILES DWR SECTION Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be 11 performed during a representative storm event' or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0,1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee '-obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) SWU-242, Last modified 10/25/2012 Page 1 of 2 1.' Outfall Description: Outfall No. OF- 00't Structure (pipe, ditch, etc.) —PlTC/i Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: CLF4� 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): /JOI.:E 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 D 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: g 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 0 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes Q 9. Is there evidence of erosion or deposition at the outfall? Yes 9D 10. Other Obvious Indicators ofStormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 Semi-annual Stormwater Discharge Monitoring Re for North Carolina Division of Water Quality General Permit No. NI Date submitted 4/15/16 4� CERTIFICATE OF COVERAGE NO. NCG030293 SAMPLE COLLECTION YE FACILITY NAME Colfax/IMO Industries, Inc. SAMPLE PERIOD ❑ Jan - PERSON COLLECTING SAMPLES, Danny Hefner, Shield Engineering or ® Moi LABORATORY: Pace Analytical Services, Inc. Lab Cert. # 12 DISCHARGING TO CLASS Comments on sample collection or analysis: No Benchmark exceedances Part A: Stormwater Benchmarks and Monitoring Results 3000t)J � � 44$�, clop40, 2016 f� El July -Dec 888 April /month) IRW ❑HQW []Trout ❑PNA :ero-flow ❑Water Supply ❑SA )ther Class C — Dry Fork Creek PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this oeriod?Z Outfall No. Date Sample P collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids PH. Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics s Benchmarks 100 mg/L or 50 mg/L 6.0 —9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SDO 004 4/1/16 0.34 10 6.5 <0.005 <0.005 0.0616 <5.0 0.0058 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. " See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Storm water Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Son iee � c he�f Name (Print name) Title (Print title) (S ature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits; they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note; If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n No discharge this Deriod?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664(SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L• 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B ' See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are s!rnif�nt penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee) Permit Date: 11/1/2012-10/31/2017 �5 16 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 4/15/16 CERTIFICATE OF COVERAGE No. NCG030293 FACILITY NAME Colfax/IMO Industries, Inc. PERSON COLLECTING SAMPLES Danny Hefner, Shield Engineerine LABORATORY: Pace Analytical Services, Inc. Lab Cert. # 12 Comments on sample collection or analysis: Benchmark exceedance for Copper Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2016 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' March (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA []Zero -flow ❑Water Supply [_]SA ®Other_Class C— Dry Fork Creek PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, 3 Inches Total Suspended Solids PH Standard units Copper Lead Zinc Non -Polar 0&G/ Total Petroleum Hydrocarbons Total Toxic Organics' Benchmarks =__> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SDO 004 3/28/16 0.34 34.8 6.6 0.0122 <0.005 0.0469 <5.0 0.0048 - Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. "See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." a5on /C2,GitPr- Name (Print name) 15//S D; rec-a r Title (Print title) /iA gnature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L• 6.0 — 9.0 SU Footnotes from Part A also apply to this Part 6 " See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES Q NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES 7 NO REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mall Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are sipg�Pc 0t penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee) Permit Date: 11/1/2012-10/31/2017 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 *---- SHIELD EIdGIKEERIIdG, IPIC. April 15, 2016 Jason Reichert Director, Global Environmental, Health & Safety Colfax Fluid Handling 1710 Airport Road Monroe, North Carolina 281 W Subject: Monthly Stornwater Sampling — April 2016 RECEIVED Certificate of Coverage No. NCG030293 MAY 13 Z016 Colfax/I140 Industries — Monroe, NC Shield Project No. 1150109-02 CENTRAL FILES DWR SECTION Dear Mr. Reichert: Shield Engineering, Inc. (Shield) successfully collected a monthly stormwater sample for Stormwater Discharge Outfall (SDO) #004 at the Colfax — Monroe Facility for the month of April. The analytical results of the stonnwater sample collected during a qualifying storm event on April 1, 2016 are attached to this cover letter. In addition, a completed qualitative monitoring report and partially completed DMR form are attached to this cover letter. Results from the April 1, 2016 sampling event shows that all of the parameters were below the corresponding benchmarks. Colfax - Monroe Facility remains in Tier Three of the NPDES General Permit No. NCG030000. The person designated to act as the permittee by Colfax - Monroe Facility should complete all "Red" sections of the attached Stormwater Discharge Monitoring Report (DMR). The completed DMR form should then be mailed to the regulatory agency Central Files. Shield greatly appreciates the opportunity to provide environmental services to Colfax. If you have any questions in reference to this document or require further information, please feel free to contact either of the undersigned at (704) 394-69 L3. Respectfully, SHIELD ENGINEERING, INC. MelindakM. Greene M rk C. Boland, P.E. Senior Engineer Pr ncipal Engineer Attachments: Analytical Results Qualitative Monitoring Report Stonmwater Discharge Monitoring Report I1:\Projects\2015\1150109-02 Colfax Stormwater\cover letters\cover letter - Mar 2016.doex 4301 Taggart Creek Road Telephone 704.394.6913 Charlotte, NC 26208 wwwshieldengineering.com Fax 704.394.696E NX NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidanceonfilling out thisform,Please visit: bttnE//oottafttttienrorg/web7wil/wc%/np[IcaawMCab-h Permit No.: orCertiflcate.ofCoverage No.: NV/_C/;/b/3/W]ZJ,! 3/ Facility Name: CcG-FAK AL -)a) !in-u'Dj)nPG County: Uu/(211 Phone No. Inspector: —PMLIA/Y �fcFa/EL Date of Inspection: Time of Inspection: o5,30 Total Event Precipitation (inches): d• 37 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit (See information below.) 0 Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event' or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A'"representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certif)pthat this report is accurate and complete to the best of my knowledge: ttee or Designee) Page 1 of 2 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. OF-" Structure (pipe, ditch, etc.) 7i iTCj/ Receiving Stream: Describe the industrial activities that occurwithin the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: e%64R-- 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): ,uvF/c 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 0 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes 0 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modirted 10/25/2012 ace Analytical e { awwpe[alapa.00m April 11, 2016 Daniel Cox Colfax Fluid Handling 1710 Airport Road Monroe, NC 28110 RE: Project: STORMWATER Pace Project No.: 92292235 Dear Daniel Cox: Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Hunlersville, NC 25078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on April 01, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Liamm Harrison liamm.harrison@pacelabs.com Project Manager Enclosures cc: Accounts Payable, Colfax Fluid Handling REPORT OF LABORATORY ANALYSIS This report shall not be repmducaq except in lull, without the written consent of Pace Analytical Services, Inc.. Page 1 of 25 aceAnalytical .PSWeesmn Project: STORMWATER Pace Project No.: 92292235 Charlotte Certification IDS 9800 Kincey Ave. Ste 100. Huntersville, INC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Cerlification #: 12 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be relcmduce4, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9000 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 25 aceAnalytical www.pace(e0s.com SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunter.Ale, NC 28078 (704)875-9092 Project: Pace Project No.: STORMWATER 92292235 Analytts Lab ID Sample ID Method Analysts Reported Laboratory 92292235001 OF-004 EPA 1664E JMS 1 PASI-C EPA 608 SWB 27 PASI-C EPA 200.7 CDF 8 PASI-A EPA 245.1 HVK 1 PASI-A EPA 625 Bpi 58 PASI-C EPA 624 GAW 34 PASI-C SM 2540D MJP 1 PASI-A EPA 9040 MLS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc., Page 3 of 25 ace Analytical e a pscelabs. cars ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92292235 Sample: OF-004 Lab ID: 92292235001 Collected: 04/0111608:35 Received: 04/0111613:34 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO mg/L 5.0 1 04/05/15 07:48 608 GCS Pesticides and PCBs Analytical Method: EPA608 Preparation Method: EPA 3510 Aldrin NO ug/L 0.050 1 04104/16 11:03 04/04116 20:44 309-00-2 alpha-BHC NO ug/L 0.050 1 04/04116 11:03 04/04/16 20:44 319-84-6 beta-BHC NO ug/L 0.050 1 04/04/16 11:03 04/04/16 20:44 319-85-7 delta-BHC NO ug/L 0.050 1 04/04/16 11:03 04/04116 20:44 319-86-8 gamma-BHC (Lindane) NO ug/L 0.050 1 04/04/16 11:03 04/04/16 20:44 58-89-9 Chlordane (Technical) NO ug/L 0.50 1 04/04116 11:03 0410411620:44 57-74-9 4,4'-DDD NO ug/L 0,050 1 04/04/16 11:03 04/04/16 20:44 72-54-8 4,4'-DDE NO ug/L 0.050 1 04/04/16 11:03 04/04116 20:44 72-55-9 4 4'-DDT NO ug/L 0.050 1 04/04/16 11:03 04/04/16 20:44 50-29-3 Dieldrin ND ug/L 0.050 1 04/04/16 11:03 04/04/16 20:44 60-57-1 Endosulfan) NO ug/L 0.050 1 04/04/16 11:03 04/04/16 20:44 959-96-8 Endosulfan ll NO ug/L 0,050 1 04/04116 11:03 04104/1620:44 33213-65-9 Endosulfan sulfate ND ug/L 0,050 1 04104/1611:03 04/04/1620:44 1031-07-8 Endrin NO ug/L 0,050 1 04/U4116 11:03 04/04/16 20:44 72-20-8 Endrin aldehyde NO ug/L 0,050 1 041G4/16 11:03 04/04/16 20:44 7421-93-4 Heptachlor NO ug/L 0.050 1 04/04/16 11:03 04/04/16 20:44 76-44-8 Heptachlor epoxide NO ug/L 0,050 1 04/04/16 11:03 04/04116 20:44 1024-57-3 PCB-1016 (Aroclor 1016) NO ug/1- 0.50 1 04/04/16 11:03 04/04/16 20:44 12674-11-2 PCB-1221 (Aroclor 1221) NO ug/L 0.50 1 04/04116 11:03 04/04/16 20:44 11104-28-2 PCB-1232 (Aroclor 1232) NO ug/L 0.50 1 04/04/16 11:03 04/04116 20:44 11141-16-5 PCB-1242 (Aroclor 1242) NO ug/L 0,50 1 04104/1611:03 04/04/16 20:44 53469-21-9 PCB-1248 (Aroclor 1248) NO ug/L 0.50 1 04/04/1611-:03 04/04/16 20:44 12672-29-6 PCB-1254 (Aroclor 1254) NO ug/L 0.50 1 04/04/16 11:03 04/04/16 20:44 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/1- 0.50 1 04104/1611:03 04/04/16 20:44 11096-82-5 Toxaphene ND ug/L 0.50 1 04/04/16 11:03 04/04/16 20:44 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 53 % 20-110 1 04/04/16 11,03 04/04/16 20:44 877-09-8 Decachlorobiphenyl (S) 30 % 20-138 1 04/04/16 11:03 04/04/16 20:44 2051.24-3 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Arsenic ND ug/L 10.0 1 04/04116 19:30 04106/1602:06 7440-38-2 Cadmium NO ug/L 1.0 1 04/04/16 19:30 04106/1602:06 7440-43-9 Chromium ND ug/L 5.0 1 04/04116 19:30 04106/1602:06 7440-47-3 Copper NO ug/L 5.0 1 04104/1619:30 04/O6/1602:06 7440-50-8 Lead NO ug/L 5.0 1 04104/1619:30 04106/16 02:06 7439-92-1 Nickel ND ug/L 5.0 1 04/04116 19:30 04/O6/16 02:06 7440-02-0 Silver NO ug/L 5.0 1 04/04/16 19:30 04/06116 02:06 7440-22-4 Zinc 61.6 ug/L 10.0 1 04/04/16 19:30 04/06/16 02:06 7440-66-6 245.1 Mercury Analytical Method: EPA 245.1 Preparation Method: EPA 245A Mercury NO ug/L 0.20 1 04/0611613:05 04/08/1615:06 7439-97-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/11/2016 10:31 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 25 Pace Analytical Services, Inc. ® 9900 ncey Ave. aceAnalytical H.ntersville, NCC28078078 nwwPeceleas.can (704)875-9092 ANALYTICAL RESULTS Project: STORMWATER Pace Project No.: 92292235 Sample: OF-004 Lab ID: 92292235001 Collected: 04/0111608:35 Received: D410111613:34 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 625 MSSV Analytical Method: EPA 625 Preparalion Method: EPA 625 Acenaphthene ND ug/L 5.0 1 04/0211610:00 04/05/16 10:31 83-32-9 L2 Acenaphthylene NO uglL 5.0 1 04/0211610:00 04105/1610:31 208-96-8 Anthracene NO ugli- 5.0 1 04/02/16 10:00 04/06/16 10:31 120-12-7 Benzo(a)anthracene NO uglL 5.0 1 04/02M6 10:00 04/05/16 10:31 56-55-3 Benzo(a)pyrene ND ug/L 5.0 1 04/02/16 10:00 04/05/16 10:31 50-32-8 Benzo(b)fluoranlhene ND ug/L 5.0 1 04/02/16 10:00 04/05/16 10:31 205-99-2 Senzo(g,h,i)perylene NO ug/L 5.0 1 04102/16 10:00 04/05/16 10:31 191-24-2 Benzo(k)0uoranthene NO ug/L 5.0 1 04/02/16 10:00 04/051161031 207-08-9 4-Bromophenylphenyl ether NO ugli- 5.0 1 04/02/16 10:00 04/05/16 10:31 101-55-3 Butylbenzylphthalate NO ug/L 5.0 1 04/02/16 10:00 04/05/16 10:31 85-68-7 4-Chloro-3-methylphenol NO ugli- 5.0 1 04102116 10:00 04/05/16 10:31 59-50-7 bis(2-Chloroethoxy)methane NO ug/L 10.0 1 04/02/16 10:00 04/05/16 10:31 111-91-1 bis(2-Chloroelhyl) ether NO ug/L 5.0 1 04/02/16 10:00 04105/16 10:31 111-44-4 bis(2-Chloroisopropyl) ether ND ugli- 5.0 1 04102M6 10:00 04/05/16 1031 108-60-1 L2 2-Chloronaphthalene ND uglL 5.0 1 04/02/16 10:00 04/05/16 10:31 91-58-7 L2 2-Chlorophenol NO ug/L 5.0 1 04102/16 10:00 04/05/16 10:31 95-57-8 4-Chlorophenylphenyl ether NO ug/L 5.0 1 04/02/16 10:00 04/05/16 1031 7005-72-3 Chrysene NO ug/L 5.0 1 04/02/16 10:00 04/0511610,31 218-01.9 Dibenz(a,h)anthracene ND ug/L 5.0 1 04/02/16 1000 04/05/16 10:31 53-70-3 3,3'-Dichlorobenzidine ND ug/L 25.0 1 04/02/16 10:00 04/05/16 10:31 91-94-1 2,4-Dichlorophenol NO ug/L 5.0 1 04/02/16 10:00 04/05/16 10:31 120-83-2 Diethylphthalate ND ug/L 5.0 1 04/02/16 10:00 04/051161031 84-66-2 2,4-Dimethylphenol NO ug/L 10.0 1 04/02/16 10:00 04/05/16 10:31 105-67-9 Dimethylphthalate ND ug/L 5.0 1 04/0211610:00 04105/1610:31 131-11-3 Di-n-butylphthalate ND ug/L 5.0 1 04/02/16 10:00 04/05/16 10:31 84-74-2 4,6-Dinitro-2-methylphenol ND ug/L 20.0 1 04/02/16 10:00 04/05/16 10:31 534-52-1 2,4-Dinitrophenol ND ug/L 50.0 1 04/02/16 10:00 04105/16 1031 51-28-5 2,4-Dinitrotoluene NO ug/L 5.0 1 0410211610:00 04/05/1610:31 121-14-2 2,6-Dinitrotoluene ND ug/L 5.0 1 04/02/16 10:00 G4105/16 10:31 606-20-2 Di-n-octylphthalate ND ug/L 5,0 1 04/02/16 10:00 04/05/16 10:31 117-84-0 bis(2-Ethylhcxyl)phthalate NO ug/L 5.0 1 04/02/16 10:00 04/05061031 117-81-7 Fluoranthene NO ug/L 5.0 1 04/02/16 10:00 04/05/16 10:31 206-44-0 Fluorene ND ug/L 5.0 1 04/02/16 10:00 04/05/16 10:31 86-73-7 Hexachloro-1,3-butadiene ND ug/L 5.0 1 04/02/16 10:00 04/05116 10:31 87-68-3 Hexachlorobenzene ND ug/L 5.0 1 0410211610:00 04/05/16 10:31 118-74-1 Hexach to rocyclopentad iene ND ug/L 10.0 1 04/02/16 10:00 04/05/16 10:31 77-47-4 Hexachloroethane ND ugli- 5.0 1 04/02/16 10:00 04/05/16 10:31 57-72-1 L2 Indeno(1, 2,3-cd)pyrene ND ug/L 5.0 1 04/02115 10:00 04/05116 10:31 193-39-5 Isophorone ND ug/L 10.0 1 04/02/16 10:00 04/05/16 10:31 78-59-1 Naphthalene ND ug/L 5.0 1 04/02/16 10:00 04/05/16 10:31 91-20-3 Nitrobenzene ND ug/L 5.0 1 04/02/161000 04105/1610:31 98-95-3 2-Nitrophenol ND ug/L 5.0 1 04/0211610:00 04/05/16 10:31 88-75-5 4-Nitrophenol ND ug/L 50.0 1 04/0211610:00 0410511610:31 100-02-7 N-Nitrosodimethylamine ND ug/L 5.0 1 04102/1510:00 04/05/1610:31 62-75-9 N-Nitroso-di-n-propylamine NO ug/L 5.0 1 04/02/16 10:00 04/05/16 10:31 621-64-7 N-Nitrosodiphenylamine NO ug/L 10.0 1 04/0211610:00 04/05116 10:31 86-30-6 Pemachlorophenol NO ug/L 10.0 1 04/02/16 10:00 04/05M610:31 87-86-5 REPORT OF LABORATORY ANALYSIS This report shall no: be reproduced, except in full, Date: 04/11/2016 10:31 AM without the written consent of Pace Analytical Services, Inc- Page 5 of 25 Pace Analytical Services, Inc. acAnaltica!® 9800mesreN7dH�, c 280 wmypacelabs.mm (704)575-9092 ANALYTICAL RESULTS Project: STORMWATER Pace Project No.: 92292235 Sample: OF-004 Lab ID: 92292235001 Collected: 0410111608:35 Received: 04/0111613:34 Matrix: Water Parameters Results Units Report Limit DF Prepared 625 MSSV Phenantmene Phenol Pyrene 1,2,4-Trichlorebenzene 2,4, 6-Trichlo rophenol Surrogates Nitrobenzene-05 (S) 2-Fluorobiphenyl (S) Terphenyl-d 14 (S) Phenol-d6 (S) 2-Fluorophenol(S) 2,4,6-Tribromophenol(S) 624 Volatile Organics Benzene Bromod ichl oromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroelhane Chloroform Chloromethane Di bromoch loro metha ne 1,2-Dichlorobenzene 1 3-Dichlorobenzene IA-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroelhene cis-1,2-Dichloroelhene trans-1.2-D ichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Methylene Chloride 1,1,2,2-Tetrachloroethane Tetrachloroelhene Toluene 1,1,1-Trichloroethane 1,1.2-Trichloroethane Trichloroethene Trich I orofl uorometha ne Vinyl chloride Surrogates 4-Bromofluorobenzene (S) Analytical Method: EPA 625 Preparation Method: EPA 625 Analyzed CAS No. Coal NO ug/L 5.0 1 04/02/16 10:00 04/05116 10:31 85-01-8 ND ug/L 5.0 1 04/02/16 10:00 04/05/16 10:31 NO ug/L 5.0 1 04/02/16 10:00 04/05/16 10:31 129-00-0 ND ug/L 5.0 1 04/02/16 10:00 04/05/16 10:31 120-82-1 L2 ND ug/L 10.0 1 04/02/16 10:00 04/05/16 10:31 88-06-2 50 % 10-120 1 04/02/16 10:00 04/05/16 10:31 4165-60-0 50 % 15-120 1 04/02/1610:00 04/0511610:31 321-60-8 79 % 11-131 1 04/02/16 1D:00 04/05/16 10:31 1718-51-0 18 % 10-120 1 04/02/1610:00 04105/1610:31 13127-88-3 27 % 10-120 1 04/02/1610:00 04105/1610:31 367-12-4 68 % 10-137 1 04J02/16 10:00 04/05/16 10:31 118-79-6 Analytical Method: EPA 624 NO uglL 2.0 1 D4/06/16 16:08 71-43-2 NO ug/L 2.0 1 D4/06/16 16:08 75-27-4 ND ug1L 2.0 1 04106/1616:08 75-25-2 NO uglL 2.0 1 04/06/16 16:08 74-83-9 NO ug/L 2.0 1 04/06/16 16:08 56-23-5 NO ug/L 2.0 1 0410611616:08 108-90-7 NO ug/L 2.0 1 04/05/16 16:08 75-00-3 ND ug/L 2.0 1 04/06/16 16:08 67-66-3 NO ug1L 2.0 1 04/06/1616.08 74-87-3 ND ug/L 2.0 1 04/06/16 16:08 124-48-1 ND ug/L 2.0 1 04/06/16 1608 95-50-1 ND ug/L 2.0 1 04/06/16 16:08 541-73-1 NO ug/L 2.0 1 04/06/16 16:08 106-46-7 NO ug/L 2.0 1 04/06/1616.08 75-34-3 ND ug/L 2.0 1 04/06/16 16:08 107-06-2 NO ug/L 2.0 1 04/06/16 16:08 75-35-4 ND ug/L 2.0 1 0410611616:08 156-59-2 ND ug,L 2.0 -1 04/0611616:08 156-60-5 ND ug/L 2.0 1 04/06116 16:08 78-87-5 ND ug/L 2.0 1 0410611616:08 10061-01-5 NO ug/L 2.0 1 04106/1616:08 10061-02-6 ND ug/L 2.0 1 04/06116 16:08 100-41-4 5.8 ug/L 2.0 1 04/06/16 16:08 75-09-2 ND ug/L 2.0 1 04/06116 16:08 79-34-5 ND uglL 2.0 1 04/06116 16:08 127-18-4 ND ug/L 2.0 1 04106/1616:08 108-88-3 NO uglL 2.0 1 04/0611616:08 71-55-6 NO ug/L 2.0 1 04/06/16 16:08 79-00-5 ND ug/L 2.0 1 04/06/1616:08 79-01-6 ND ug/L 2.0 1 04/06/16 16:08 75-69-4 NO ug/L 2.0 1 04/06/16 16:08 75-01-4 102 % 70-130 1 04/06/1616*08 460-00-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/11/2016 10:31 AM without the written consent of Pace Analytical Services, Inc., Page 6 of 25 aceAnalytical e sw bsbvebs.= ANALYTICAL RESULTS Pace Analytical Services, Inc. 9BOOKincey Ave. Suitelo0 Huntersville. NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92292235 Sample: OF-004 Lab ID: 92292235001 Collected: 04/0111608:35 Received: 04/01/1613:34 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 624 Volatile Organics Analytical Method: EPA 624 Surrogates Toluene -rill (S) 101 % 70-130 1 04/06/16 16:08 2037-26-5 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 04/06M6 16:08 17060-07-0 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 10 mglL 5.0 1 04/05/16 10:12 D6 9040 pH Analytical Method: EPA 9040 pH 6.5 Std. Units 0.10 1 G4104/1612:55 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in full. Date: 04/11/2016 10:31 AM without the written consent of Pace Analytical Services, Inc., Page 7 of 25 aceAnalyticale wawpacelaasmm QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92292235 OC Batch: GCSV/24587 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92292235001 METHOD BLANK: 1701578 Matrix: Water Associated Lab Samples: 92292235001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 04/05/16 07:44 LABORATORY CONTROL SAMPLE: 1701579 Parameter Units Oil and Grease mg/L Spike LCS LCS Conc. Result % Rec 40 37.5 94 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite too Huntersville, NC 28078 (704)875-9092 e/ Rec Limits Qualifiers 78-114 MATRIX SPIKE SAMPLE: 1701580 92291787002 Spike MS MS e/ Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Oil and Grease mg/L NO 40 37.9 91 78-114 Results presentee on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the tight of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 04/11/2016 10:31 AM without me written consent of Pace Analytical Services, Inc., Page 8 of 25 ZeAnalytical' wwx.paceleAv.xvn i QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92292235 QC Batch: MERP/9197 Analysis Method: EPA 245.1 QC Balch Method: EPA 245.1 Analysis Description: 245.1 Mercury Associated Lab Samples: 92292235001 METHOD BLANK: 1701803 Matrix: Water Associated Lab Samples: 92292235001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L NO 0.20 04108/1614:47 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntereville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1701804 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Mercury ug/L 2.5 2.4 98 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1701805 1701806 MS MSD 92292154008 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Mercury ug/L NO 2.5 2.5 2.5 2A 99 95 70-130 5 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1701807 1701808 MS MSD 92292277003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Mercury ug/L NO 2.5 2.5 2.4 2.5 98 101 70-130 4 Results presented on this page are In the units Indicated by the 'Units" column except when an alternate unit Is presented to the right at the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/11/2016 10:31 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 25 aceAnalytical n xwxpecelees.cnrtl I QUALITY CONTROL DATA Pace Analytical Services, Inc. 9600 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92292235 QC Batch: MPRP/21230 Analysis Method: EPA 200.7 QC Batch Method: EPA 206.7 Analysis Description: 200.7 MET Associated Lab Samples: 92292235001 METHOD BLANK: 1701316 Matrix: Water Associated Lab Samples: 92292235001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Arsenic ug/L NO 10.0 04/06116 02:00 Cadmium ug/L NO 1.0 04/06/16 02:00 Chromium ug/L NO 5.0 04/06116 02:00 Copper ug/L NO 5.0 04/06/16 02:00 Lead ug/L NO 5.0 04/06/16 02:00 Nickel ug/L NO 5.0 04/06116 02:00 Silver uglL NO 5.0 04/06/16 02:00 Zinc ug/L NO 10.0 04/06/16 02:00 LABORATORY CONTROL SAMPLE: Parameter 1701317 Units Spike Conic. LCS Result LCS % Rec % Rec Limits Qualifiers Arsenic ug/L 500 488 98 85-115 Cadmium ug/L 500 504 101 85-115 Chromium ug/L 500 539 108 85-115 Copper ug/L 500 512 102 85-115 Lead ug/L 500 510 102 85-115 Nickel ug/L 500 510 102 85-115 Silver ug/L 250 239 95 85-115 Zinc ug/L 500 530 106 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1701318 1701319 MS MSD 92292235001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conic. Conc. Result Result %Rec %Rec Limits RPD Qual Arsenic ug/L NO 500 500 448 420 89 83 70-130 6 Cadmium ug/L NO 500 500 461 434 92 87 70-130 6 Chromium ug/L NO 500 500 493 460 99 92 70-130 7 Copper ug/L NO 500 500 473 441 94 87 70-130 7 Lead ug/L NO 500 500 464 437 93 87 70-130 6 Nickel ug/L NO 500 500 466 436 93 87 70-130 7 Silver ug/L ND 250 250 219 208 88 83 70-130 5 Zinc ug/L 61.6 500 500 540 517 96 91 70-130 4 Hesuite presented on this page are In the unite Indicated by the 'Units" column except where an altemete unit Is presented 10 the deM of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04111/2016 10:31 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 25 aceAnalytical srrx peralass.can QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Muntersvllls, NC 26078 (704)875-9092 Project: Pace Project No:: STORMWATER 92292235 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1701320 1701321 MS MSD 92292073001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qua[ Arsenic ug/L ND 500 500 455 450 91 90 70-130 1 Cadmium uglL ND 500 500 471 465 94 93 70-130 1 Chromium ug/L ND 500 500 508 501 101 100 70-130 1 Copper ug/L ND 500 500 479 470 96 94 70-130 2 Lead uglL ND 500 500 478 470 95 94 70-130 2 Nickel ug/L ND 500 500 479 471 95 94 70-130 2 Silver ug/L ND 250 250 222 221 89 88 70-130 1 Zinc ug/L 1070 500 500 735 495 -68 -116 70-130 39 M1,R1 Results presented on this page are In the units In cleated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/11/2016 10:31 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 25 aceAnalyticale ww.upace4sru.cper QUALITY CONTROL DATA Pace Analytical Servlcas, Inc. 9800 Kincey Ave. Suite 100 Huntermlle, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92292235 QC Batch: MSV/36271 Analysis Method: EPA 624 QC Batch Method: EPA 624 Analysis Description: 624 MSV Associated Lab Samples: 92292235001 METHOD BLANK: 1703241 Associated Lab Samples: 92292235001 Parameter Units Matrix: Water Blank Reporting Result Limit Analyzed 1,1,1-Trichloroethane ug/L ND 2.0 04106/1614:27 1,1,2,2-Tetrachloroethane ug/L ND 2.0 04/06/16 14:27 1,1,2-Trichloroethane ug/L ND 2.0 04/06/16 14:27 1,1-Dichloroethane ug/L ND 2.0 04/06/16 1427 1,1-Dichoroethene ug/L NO 2.0 04106/16 14:27 1,2-Dichlorobenzene ug/L NO 2.0 04/06/16 14:27 1,2-Dichloroethane ug/L NO 2.0 041G6/16 14:27 1,2-Dichloropropane ug/L NO 2.0 04/06/16 1427 1,3-Dichlorobenzene ug/L NO 2.0 04/06/16 14:27 1,4-Dichlorobenzene ug/L NO 2.0 04/06/16 14:27 Benzene ug/L NO 2.0 0410611614:27 Bromodichloromethane ug/L NO 2.0 0410611614:27 Bromotorrn ug/L ND 2.0 04/05/1614:27 Bromomelhane ug/L ND 2.0 0410611614:27 Carbon tetrachloride ug/L ND 2.0 04/06/16 14:27 Chlorobenzene ug/L ND 2.0 0410611614:27 Chloroethane ug/L ND 2.0 0410611614:27 Chloroform ug/L NO 2.0 04106/16 14:27 Chloromethane ug/L ND 2.0 0410611614:27 cis-1,2-Dichloroethene ug/L ND 2.0 04/06/16 1427 cis-1,3-Dichloropropene ug/L ND 2.0 04/06/16 14:27 Dibromochloromethane ug/L ND 2.0 04106/16 14:27 Ethylbenzene ug/L NO 2.0 04/06/16 14:27 Methylene Chloride ug/L ND 2.0 04/06/16 14:27 Tetra cheroethene ug/L NO 2.0 04/06/16 14:27 Toluene ug/L NO 2.0 04/05/16 14:27 trans-1,2-Dichloroethene ug/L NO 2.0 04/06/16 14:27 trans-1,3-Dichloropropene ug/L NO 2.0 04106/16 14:27 Trichloroethene ug/L NO 2.0 04/06/16 14:27 Trichlorofluoromethane ug/L ND 2.0 041061161427 Vinyl chloride ug/L NO 2.0 04/06/16 14:27 1,2-Dichloroethane-d4 (S) % 97 70-130 04106/16 14:27 4-Bromofluorobenzene (S) % 98 70-130 04106/16 14:27 Toluene-d8 (S) a/ 99 70-130 04106/16 14:27 Qualifiers LABORATORY CONTROL SAMPLE: 1703242 Spike LCS LCS %Rec Parameter Units Cone. Result % Rec Limits Qualifiers 1, 1, 1-Trichloroethane ug/L 50 44.2 88 52-162 1, 1,2,2-Tetrachloroethane ug/L 50 48.9 98 46-157 Results presented on this page are In the units Ind tested by the "Units" column except whom an alternate unit Is presented to the right of the reault. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 04/11/2016 10:31 AM without the written consent of Pace Analytical Services, Inc., Page 12 of 25 aceAnalyticale wx+ypacelebs cam i QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92292235 LABORATORY CONTROL SAMPLE: - Parameter 1703242 Units Spike Conc. LCS Result LCS %Rec %Rec Limits 1,1.2-Tdchloroelhane ug/L 50 45.5 91 52-150 1,1-Dichloroethane ug/L 50 43.7 87 59-155 1,1-Dichloroethene ug/L 50 45.9 92 1-234 1,2-Dichlorobenzene uq/L 50 45.9 92 18-190 1,2-Dichloroethane ug/L 50 40.4 81 49-155 1,2-Dichloropropane ug/L 50 44.4 89 1-210 1,3-Dichlorobenzene ug/L 50 46.2 92 59-156 1,4-Dichlorobenzene ug/L 50 46.9 94 18-190 Benzene ug/L 50 47.2 94 37-151 Bromodichloromethane ug/L 50 48.9 98 35-155 Bromoforrn ug/L 50 48.4 97 45-169 Bromomethane ug/L 50 48.1 96 1-242 Carbon tetrachloride ug/L 50 48.5 97 70-140 Chlorobenzene ug/L 50 45.9 92 37-160 Chloroethane ug/L 50 41.2 82 14-230 Chloroform ug/L 50 45.1 90 51-138 Chloromemane ug/L 50 42.1 84 1-273 cis-1,2-Dichloroethene uglL 50 43.9 88 68-146 cis-1,3-Dichloropropene ug/L 50 46.7 93 1-227 Dibromochloromelhane ug/L 50 48.1 96 53-149 Ethylbenzene ug/L 50 46.3 93 37-162 Methylene Chloride ug/L 50 33.4 67 1-221 Tetrachloroethene ug/L 50 46.9 94 64-148 Toluene ug/L 50 46.5 93 47-150 trans-1,2-Dichloroethene ug/L 50 44.8 90 54-156 trans-1,3-Dichloropropene ug/L 50 45.5 91 17-183 Trichloroethene ug/L 50 43.9 88 71-157 Trichloro0uoromethane ug/L 50 42.5 85 17-181 Vinyl chloride ug/L 50 46.6 93 1-251 1,2-Dichloroethane-d4 (S) % 91 70-130 4-Bromofluorobenzene (S) % 102 70-130 Toluene-d8 (S) % 100 70-130 Pace Ana lyticaI Servic ea, Inc. 9600 Klncey Ave. Suite 100 HuntersWla, NC 28078 (704)875-9092 Qualifiers Results presented on this page are In the unite Indlcated by the "units" column except where an altemate unit Is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 04/11/2016 10:31 AM without the written consent of Pace Analytical Services, Inc.. Page 13 of 25 aceAnalytical m'.w.pBCBIB09.N(n I QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92292235 OC Batch: OEXT/41754 Analysis Method: EPA 608 QC Batch Method: EPA 3510 Analysis Description: 608 GCS Pest PCB Associated Lab Samples: 92292235001 METHOD BLANK: 1701041 Associated Lab Samples: 92292235001 Parameter Units Matrix: Water Blank Reporting Result Limit Analyzed 4A-DDD uglL ND 0,050 04/05116 00:37 4,4'-DDE ug/L ND 0.050 04/05/16 00:37 4,4'-DDT ug1L NO 0.050 04/05/16 00:37 Aldrin ug/L NO 0.050 04/05/16 00:37 alpha-BHC uglL NO 0.050 0410511600:37 beta-BHC uglL NO 0.050 0410511600:37 Chlordane (Technical) uglL NO 0.50 04/05/1600:37 delta-BHC uglL NO 0.050 04/05/1600:37 Dieldrin ug/L ND 0.050 04105/1600:37 Endosulfan I ug/L ND 0.050 04105/16 00:37 Endosulfan II ug/L ND 0,050 04/05/16 00:37 Endosulfan sulfate ug/L ND 0.050 04/05/16 00:37 Endrin ug/L ND 0,050 04/05116 00:37 Endrin aldehyde ug/L ND 0.050 04105/15 00:37 gamma-BHC(Lindane) ug/L ND 0,050 04105/1600:37 Heptachlor ug/L NO 0.050 04/05/16 00:37 Heptachlor epoxide ug/L ND 0.050 04/05/16 00:37 PCB-1016 (Aroclor 1016) ug/L NO 0.50 04/05116 00:37 PCB-1221 (Aroclor 1221) ug/L NO 0,50 04/05/16 00:37 PCB-1232(Aroclor 1232) uglL ND 0.50 04/05/1600:37 PCB-1242 (Aroclor 1242) ug/L ND 0.50 04105/16 00:37 PCB-1248 (Aroclor 1248) ug/L ND 0.50 04/05/16 00:37 PCB-1254 (Aroclor 1254) ug/L ND 0.50 04/05/16 00:37 PCB-1260 (Aroclor 1260) uglL ND 0.50 04/05/16 00:37 Toxaphene uglL ND 0.50 04/05/1600:37 Decachlorobiphenyl (S) % 48 20-138 04/05/16 00:37 Telrachloro-m-xylene (S) % 77 20-110 04/05116 00:37 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1701042 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers 4A-DDD ug/L ,25 0.26 103 31-141 4,4'-DDE ug/L ,25 0.24 97 30-145 4,4'-DDT uglL .25 0.26 105 25-160 Aldrin uglL .25 0.21 86 42-122 alpha-BHC uglL 25 0.25 99 37-134 beta-BHC ug/L .25 0.26 104 17-147 delta-BHC ug/L .25 0.28 113 19-140 Dieldrin uglL .25 0.25 100 36-146 Endosulfan I uglL .25 0.26 106 45-153 Resuas presented on this pap. ere In the..U. Indicated by the "Units" column except where an altem ate unit Is presented to the rain of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/11/2016 10:31 AM without the wneen consent of Pace Analytical Services, Inc.. Page 14 of 25 aceAnalytical e wdwpeceloDsmm l QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92292235 Pace Analytical Sorvicos, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: Parameter 1701042 Units Spike Conc. LCS Result 1-CS e/ Rec %Rec Limits Qualifiers Endosulfan II ugIL 25 0.27 110 1-202 Endosulfan sulfate ug/L .25 0.28 114 26-144 Endrin ug/L .25 0.26 106 30-147 Endrin aldehyde ug/L .25 0.26 103 50-150 gamma-BHC (Lindane) ug/L .25 0.25 101 32-127 Heptachlor ug/L .25 0.24 95 34-111 Heptachlor epoxide ug/L .25 0.26 104 41-126 Decachlorobiphenyl (S) % 56 20-138 Tetrachloro-m-xylene (S) % 97 20-110 MATRIX SPIKE SAMPLE: Parameter 1701043 Units 92292235001 Result Spike Conc. MS Result MS %Rec % Rec Limits Qualifiers 4,4'-DDD ug/L ND .25 0.20 80 31-141 4,4'-DDE ug/L ND .25 0.20 83 30-145 4 4'-DDT ug/L NO .25 0.20 82 25-160 Aldrin ug/L ND .25 0.19 75 42-122 alpha-BHC ug/L NO .25 0.19 78 37-134 beta-BHC ug/L ND 25 0.28 115 17-147 delta-BHC ug/L ND .25 0.23 91 19-140 Dieldrin ug/L ND .25 0.20 80 36-146 Endosulfan I ug/L ND ,25 0.21 87 45-153 Endosulfan II ug/L ND .25 0.22 88 1-202 Endosulfan sulfate uglL ND ,25 0.22 91 26-144 Endrin ug/L ND .25 0.22 87 30-147 Endrin aldehyde ug/L ND .25 0.21 84 50-150 gamma-BHC (Lindane) ug/L ND .25 0.20 81 32-127 Heptachlor uglL ND .25 0.20 80 34-111 Heptachlor epoxide ug/L ND .25 0.21 84 41-126 Decachlorobiphenyl (S) % - 35 20-138 Tetrachloro-m-xylene (S) % 77 20-110 SAMPLE DUPLICATE: 1701044 92292244001 Dup Parameter Units Result Result RPD Qualifiers 4,4'-DDD ug/L ND ND 4A-DDE ug/L NO ND 4,4'-DDT uglL ND ND Aldrin ug/L ND ND alpha-BHC ug/L ND ND bela-BHC ug/L ND NO Chlordane (Technical) ug/L ND ND delta-BHC ug/L ND ND Dieldrin ug/L ND ND Results presented on this page are In the units Indicated by the "Units" column except Wbere an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 04M1/2016 10:31 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 25 aceAnalytical e wewpecsieD]cdm QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92292235 SAMPLE DUPLICATE: 1701044 Parameter Units 92292244001 Result DuP Result Endosulfan I ug/L NO NO Endosulfan II ug/L NO NO Endosulfan sulfate ug/L NO NO Endrin ug/L NO NO Endrin aldehyde ug/L 0.077 0,092 gamma-BHC (Lindane) ug/L NO NO Heplachlor ug/L NO NO Heplachlor epoxide ug/L NO NO PCB-1016 (Aroclor 1016) ug/L NO NO PCB-1221 (Aroclor 1221) ug/L NO NO PCB-1232 (Aroclor 1232) ug/L NO NO PCB-1242 (Aroclor 1242) uglL NO NO PCB-1248 (Aroclor 1248) ug/L ND NO PCB-1254 (Aroclor 1254) ug/L NO NO PCB-1260 (Aroclor 1260) ug/L NO NO Toxaphene ug/L ND NO RPD Qualifiers 18 Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersville, NC 28070 (704)875-9092 Res uas presented on this page ere In the units Indicated by the'Unit.- column except where an alternate unll la presented to the fight of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/11/2016 10:31 AM without me written consent of Pace Analytical Services, Inc.. Page 16 of 25 aceAnalytical wwwpecNeas.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hord ersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92292235 QC Batch: OEXT/41731 Analysis Method: EPA 625 QC Batch Method: EPA 625 Analysis Description: 625 MSS Associated Lab Samples: 92292235001 METHOD BLANK: 1700269 Matrix: Water Associated Lab Samples: 92292235001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,2,4-Trichlorobenzene uglL ND 5.0 04/02/16 03:00 2,4,6-Trichlorophenol ug/L ND 10.0 04/02/1603:00 2,4-Dichlorophenol ug/L ND 5.0 04/02/16 03:00 2,4-Dimethylphenol ug/L ND 10.0 04/02116 03:00 2,4-Dinitrophenol ug/L NO 50.0 04/0211603:00 2,4-Dinitrotoluene ug/L NO 5.0 04/02/16 03:00 2,6-Dinitrotoluene ug/L NO 5.0 04/02/16 03:00 2-Chlono naphthalone ug/L NO 5.0 04/02/16 03:00 2-Chlorophenol ug/L NO 5.0 04/02116 03:00 2-Nitrophenol ug/L ND 5.0 04/02/16 03:00 3,3'-Dichlorobenzidine ug/L NO 25.0 04/02/16 03:00 4,6-Dinitro-2-methylphenol ug/L NO 20.0 04/02116 03:00 4-Bromophenylphenyl ether uglL NO 5.0 04/02/16 03:00 4-Chloro-3-methylphenol ug/L ND 5.0 04/02/16 03:00 4-Chlorophenylphenyl ether ug/L ND 5.0 04/02/16 03:00 4-Nitrophenol ug/L NO 50.0 04/02/16 03:00 Acenaphthene ug/L NO 5.0 0410211603:00 Acenaphthylene ug/L ND 5.0 04102/1603:00 Anthracene ug/L ND 5.0 04/0211603*00 Benzo(a)anthracene ug/L NO 5.0 04/02/16 03:00 Benzo(a)pyrene ugh- NO 5.0 04/02/16 03:00 Benzo(b)fluoranthene ug/L NO 5.0 04/02/16 03:00 Benzo(g,h,i)perylene ug/L NO 5.0 04/020603:00 Benzo(k)fluoranthene uglL NO 5.0 04/02/16 03:00 bis(2-Chlorcethoxy)methane ug/L NO 10.0 04/02tl6 03:00 bis(2-Chloroethyl) ether ug/L NO 5.0 04/02/16 03:00 bis(2-Chloroisopropyp ether ug/L NO 5.0 04/02116 03:00 bis(2-Ethylhexypphthalate ug/L NO 5.0 04/02/16 03:00 Butylbenzylphthalate ug1L NO 5.0 04/02116 03:00 Chrysene ug/L NO 5,0 04/02/16 03:00 Di-n-butylphthalate ug/L ND 5.0 04/02/16 03:00 Di-n-octylphthalate ug/L NO 5.0 04/02/16 03:00 Dibenz(a,h)anthrocene ug/L ND 5.0 04/02/16 03:00 Diethylphthalate ug/L NO 5.0 04/02/16 03:00 Dimethylphthalate ug/L NO 5.0 04/02/16 03:00 Fluoranthene ug/L NO 5.0 04/02/16 03:00 Fluorene ug/L NO 5.0 04/02/16 03:00 Hexachl0ro-1,3-butadiene ug/L NO 5.0 04/02/16 03:00 Hexachlorobenzene ug/L NO 5.0 04/02/16 03:00 Hexachlorocyclopentadiene ug/L NO 10.0 04/02/16 03:00 Hexachloroelhane ug/L NO 5.0 04/02/16 03:00 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the nght of the renuh. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/1112016 10:31 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of 25 aceAnalytica!m wwwpecelsea.com t QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Hunlersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92292235 METHOD BLANK: 1700269 Matrix: Water Associated Lab Samples: 92292235001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Indeno(1,2,3-cd)pyrene ug/L ND 5.0 04102/16 03:00 Isophorone ug/L ND 10.0 04/02/16 03:00 N-Nitroso-di-n-propylamine ug/L NO 5.0 04/02/16 03:00 N-Nilrosodimethylamine ug/L NO 5.0 04/02/16 03:00 N-Nitrosodiphenylamine ug/L NO 10.0 04/02/16 03:00 Naphthalene uglL NO 5.0 04/02/16 03:00 Nitrobenzene ugli- NO 5.0 04/02/16 03:00 Pentachlorophenol ug/L NO 10.0 04/02/16 03:00 Phenanthrene uglL NO 5.0 04/02/16 03:00 Phenol ug/L NO 5.0 04/02/16 03:00 Pyrene uglL NO 5.0 04/02/16 03:00 2,4,6-Tribromophenol (S) % 57 10-137 04102/16 03:00 2-Fluorobiphenyl(S) % 61 15-120 04102/16 03:00 2-Fluorophenol (S) % 34 10-120 04/02/16 03:00 Nitrobenzene-d5 (S) % 59 10-120 04102/16 03:00 Phenol-d6 (S) % 24 10-120 04/02/16 03:00 Terphenyl-d14 (S) % 86 11-131 04/02/16 03:00 LABORATORY CONTROL SAMPLE &LCSD: 1700270 1700271 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result e/ Rec %Rec Limits RPD RPD Qualifiers 1,2,4-Trictllorobenzene uglL 50 30.7 16.3 61 33 44-142 61 30 L0,Rl 2,4,6-Trichlorophenol ug/L 50 23.0 21.6 46 43 37-144 6 30 2,4-Dichlorophenol ug/L 50 25.4 17.4 51 35 1-191 37 30 R7 2.4-Oimethylphenol ug/L 50 34.6 18.3 69 37 32-119 62 30 R1 2,4-Dinitrophenol ug/L 250 100 98.4 40 39 1-161 2 30 2 4-Dinitrotoluene ug/L 50 40.9 39.1 82 78 39-139 5 30 2,6-Dinitrotoluene ug/L 50 39.4 35.2 79 70 50-158 11 30 2-Chloronaphthalene ug(L 50 34.8 19.0 70 38 60-118 59 30 L0,R1 2-Chlorophencl ug/L 50 27.1 17.9 54 36 23-134 41 30 R1 2-Nitrophenol ug/L 50 24.7 18.3 49 37 29-182 30 30 3,3'-Dichlorobenzidine ug/L 100 82.6 74.8 83 75 1-262 10 30 4,6-Dinitrc-2-methylphenol ug/L 100 47.2 54.0 47 54 1-181 13 30 4-Bromophenylphenyl ether ug/L 50 36.1 31.4 72 63 53-127 14 30 4-Chloro-3-methylphenol ug(L 100 66.1 45.9 66 46 22-147 36 30 R1 4-Chlorophenylphenyl ether uglL 50 37.1 28.4 74 57 25-158 26 30 4-Nitrophenol ug/L 250 42.5J 58.4 17 23 1-132 30 Acenaphthene ug/L 50 34.1 21.5 68 43 47-145 45 30 L0,R1 Acenaphthylene ug/L 50 36.2 23.0 72 46 33-145 45 30 R1 Anthracene ug/L 50 37.5 35.0 75 70 1-166 7 30 Benzo(a)anthracene ug/L 50 37.7 36.2 75 72 33-143 4 30 Benzo(a)pyrene ug/L 50 38.5 36.8 77 74 17-163 4 30 Benzo(b)fiuoranthene uglL 50 34.1 33.6 68 67 24-159 1 30 Benzo(g,h,i)perylene ug/L 50 37.7 35.2 75 70 1-219 7 30 Results presented on this page are In Me units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/11 /2016 10:31 AM without the written consent of Pace Analytical Services, Inc.. Page 18 of 25 aceAnalyticala wwwpeceleDacam f QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92292235 LABORATORY CONTROL SAMPLE S LCSD: Parameter 1700270 Units Spike Conc. 1700271 LCS LCSD Result Result LCS LCSD %Rec %Rec % Rec Limits Benzo(k)fluoranthene ug/L 50 35.9 34.9 72 70 11-162 bis(2-Chloroelhoxy)methane ug/L 50 34.0 17.4 68 35 33-184 bis(2-Chloroelhyl) ether ug/L 50 35.5 19.3 71 39 12-158 bis(2-Chloroisopropyl) ether ug/L 50 31.4 16.5 63 33 36-166 bis(2-Ethylhexyl)phlhalale ug/L 50 45.0 42.4 90 85 8-158 Butylbenzylphthalate ug/L 50 41.7 40.7 83 81 1-152 Chrysene ug/L 50 36.2 35.1 72 70 17-168 Di-n-butylphthalale ug/L 50 45.6 42.0 91 84 1-118 Di-n-octylphthalate ug/L 50 46.1 40.9 92 82 4-146 Dibenz(a,h)anthracene ug/L 50 38.8 36.4 78 73 1-227 Diethylphthalate ug/L 50 40.4 37.9 81 76 1-114 Dimethylphlhalate ug/L 50 39.3 35.4 79 71 1-112 Fluoranthene ug/L 50 38.4 33.9 77 68 26-137 Fluorene ug/L 50 37.6 29.5 75 59 59-121 Hexachloro-1,3-butadiene ug/L 50 29.2 14.6 58 29 24-116 Hexachlorobenzene ug/L 50 37.3 33.8 75 68 1-152 Hexachlorocyclopentadiene ug/L 50 29.6 12.3 59 25 25-150 Hexachloroethane ug/L 50 31.2 15.9 62 32 40-113 Indeno(1,2,3-cd)pyrene ug/L 50 41.6 38.4 83 77 1-171 Isophorone ug/L 50 35.7 19.3 71 39 21-196 N-Nilroso-di-n-propylamine ug/L 50 36.2 18.6 72 37 1-230 N-Nitrosodimethylamine ug/L 50 23.3 13.3 47 27 25-150 N-Nitrosodiphenylamine uglL 50 37.1 33.7 74 67 25-150 Naphthalene ug/L 50 31.0 16.7 62 33 21-133 Nitrobenzene ug/L 50 33.8 18.3 66 37 35-180 Pentachlorophenol ug/L 100 39.0 42.3 39 42 14-176 Phenanthrene ug/L 50 37.6 34.8 75 70 54-120 Phenol ug/L 50 16.0 9.2 32 18 5-112 Pyrene ug/L 50 34.7 36.7 69 73 52-115 2,4,6-Tnbfomophenol (S) % 50 67 10-137 2-Fluorobiphenyl(S) % 72 38 . 15-120 2-Fluorophenol(S) % 28 21 10-120 Nitrobenzene-d5(S) % 71 38 10-120 Phenol-d6 (S) % 25 15 10-120 Terphenyl-d14(S) % 72 74 11-131 Pace Analytical Servlcos, Inc. 9800 Kincey Ave. Suite 100 Hurnersvllle, NC 20078 (704)875-9092 Max RPD RPD Qualifiers Resume presented an this page are In the units Indicated by the "Units' column except amen an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS 30 30 R1 30 R1 30 L(),R1 30 30 30 30 30 30 30 30 30 30 30 R1 30 30 R1 30 L0,R1 30 30 R1 30 R1 30 R1 30 30 R1 30 R1 30 30 30 R7 30 This report shall not be reproduced, except in full. Dale: 04/11/2016 10:31 AM without the written consent of Pace Analytical Services, Inc.. Page 19 of 25 acoAnalytical wwwpecelebecom QUALITY CONTROL DATA Pace Analytical Services, Inc. 980D l incey Ave. Suite 100 Hunlersville, NC 2BO78 (704)875-9092 Project: STORMWATER Pace Project No.: 92292235 QC Batch. WET/44010 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92292235001 METHOD BLANK: 1701635 Matrix: Water Associated Lab Samples: 92292235001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L NO 2.5 04/05/16 10:11 LABORATORY CONTROL SAMPLE: 1701636 Spike LCS LCS %Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L - 250 246 98 90-110 SAMPLE DUPLICATE: 1701637 92292235001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 10 12.4 21 D6 SAMPLE DUPLICATE: 1701638 92292278002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L NO 5.8 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full, Date: 04/11/2016 10:31 AM without the written consent of Pace Analytical Services, Inc- Page 20 of 25 aceAnalytical ewwpacNeDs.00m QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92292235 QC Batch: WET/43992 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92292235001 SAMPLE DUPLICATE: 1700877 Parameter pH 92291971002 Dup Units Result Result RPD Qualifiers Std, Units 64 6.5 0 H6 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 29078 (704)875-9092 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full, Date: 04/11/2016 10:31 AM without the written consent of Pace Analytical Services, Inc.. Page 21 of 25 ace Analytical / eww;a0eb3.WM QUALIFIERS Project: STORMWATER Pace Project No.: 92292235 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. I -Adjusted Method Detection Limit. POL- Practical Quarr itation Limit. RL - Reporting Limit. Pace Analytical services, Inc. 9800 Kincey Ave. Suite 100 Huntersvdle, NC 28078 t704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) OUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolem and Acrylonitrile by EPA Method 8260. N-Nitrosociiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA required holding time. LO Analyle recovery in the laboratory control sample (LCS) was outside QC limits. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. Ml Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/11/2016 10:31 AM without the written consent of Pace Analytical Services, Inc., Page 22 of 25 s aceAnalytical wwnpecelaef.txpn QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: STORMWATER Pace Project No.: 92292235 Pace Analytical Services, Inc. 0800 Kincey Ave, Suite 100 Muntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92292235001 OF-004 EPA 1664E GCSV/24587 92292235001 OF-004 EPA3510 0EXT/41754 EPA608 92292235001 OF-004 EPA 200.7 MPRP/21230 EPA 200.7 92292235001 OF-004 EPA 245.1 MERP/9197 EPA245.1 92292235001 OF-004 EPA625 OEXT141731 EPA625 92292235001 OF-004 EPA624 MSV/36271 92292235001 OF-004 SM 2540D WET/44010 92292235001 OF-004 EPA9040 WET/43992 Date: 04/11/2016 10:31 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc - Analytical Batch GCSV/24580 ICP/19078 MERC/8842 MSSV/12085 Page 23 of 25 uocumenz Name: Document Revised: IBFEB2016 nditlon U on Recei t(SCUR) Pa e l of 2 Document No.: Issuing Authority: CHR-CS-003-rev. 18 Pace Huntersville Quality Office Pa"7 of J fnr _I ' " Client Name: W® g2292235 � •`- •t�\ Courler. Fed Ex ❑UPS�Lt❑USPSu ❑ Commercial ❑pa a ❑Other:_ Dc6nojett II III I I I II I I III'I ii� 92292238 Custody Seal Present? ❑Yes QNo Seals Intact? QYes-- ❑No i Date/Initials Person Examining Contents; `-i. 1 Is.;. K • . Packing Material: ❑Bubble Wrap QBGbble Bags ❑None ❑Other:_ Thermometer: EJT1505 ❑ Type o/ice: ❑we't ❑Blue ❑None❑Samprsonice, cooling process has begun Correction Factor: 0,O'C Cooler Temp Corrected ('C): Biological Tissue Frozen? Dyes []No EIN/A---- Temp should be above freezing to 6°C USDA Regulated Sall ( El -N/A, water sample) Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internallonally, Oyes ❑NOS incluillnO Hawall and Pundn e4e11 Mv— flung COMMENTS: Chain of Custody Present? ® es (:]NO ❑N/A 1. Chain OfCustody Filled Out? Ye� ONO N/A 2. Chain of Custody Relinquished? 1p nNO F1N/A 3. Sampler. Name and/or Signature on CDC? Myer— ❑N/A 4 Sam les Arrived within Hold Time? Ejyes ONO ❑N/n S. Short Hold Time Analysis 1<72 hr.)? Oyes []No— ONJA 6. Rush Turn Around Time Requested? ❑Ycs ❑Nd-�❑N/A 7. Sufficient Volume? Correct Containers Used? ©YesONO ❑N/A 9. -Pace Containers Used? jt_]. Yeg• ONO ❑N/A Containers Intact? [Dyes—' ❑No N A 10. Filtered Volume Received for Dissolved Tests? Oyes ONO IDNIA- 11. Note if sediment is visible In the dissolved container Sample Labels Match COC? ©lfes ON. ❑N/A 12. -Includes Date/Tlme/ID/Anal sis Matrix: I..t yf) All containers needing acid/base preservation have been checked? �❑Yes [:)NO ❑N/A 13, All containers needing preservation are found to be In compliance with EPA recommendation? (HNO3, Hz50a, HCI<2; NaOH >9Sulfide, NaOH>I2 Cyanide) L1Yes J ON. ❑N/A Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC,LLHg Dyes ONO f]N/An Samples checked for dechlorinatlon ❑yes^•" ONO QNIA 14. Headspace in VOA Vials I>5-6mnr ? Oyes ❑i NO^' ❑N/A 15. Trip Blank Present? ❑Yes ONO (DN/A' 16, Trip Blank Custody Seals Present? Oyes ONO f]N/A Pace Trie Blank Lot P (If purchased): --"'"""""""•""""" Field Data Required? ❑Yes ❑No Person Contacted: Comments/Resolution: Project Manager SCURF Review: Date/Time: Date: Project Manager SRF Review: )- 1\ Date: ��-'t• \ l_ s 1 s-; Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North CarolinaDEHNR Certilidatlon Office (i.e. Out of hold, Incorrect preservative, out of temp, Incorrect containers) Page 24 of 25 hce,trGrne.,f CHAIN -OF -CUSTODY /Analytical Request Document The Chain-of-Custudy is a LEGAL DOCUMENT. All relevant fields must be Completed accurately, Section A Se i'me B Section C Required Client Inlo:maGon: RCgi Pel dix! ILle . *__ 8 IIIEL April 15, 2016 Jason Reichert Director, Global Environmental, Health & Safety Colfax Fluid Handling 1710 Airport Road Monroe, North Carolina 28110 Subject: Monthly Stormwater Sampling— March 2016 Certificate of Coverage No. NCG030293 Colfax/IMO Industries — Monroe, NC Shield Project No. 1150109-02 Dear Mr. Reichert: Shield Engineering, Inc. (Shield) successfully collected a monthly storrlwater sample for Stormwater Discharge Outfall (SDO) #004 at the Colfax — Monroe Facility for the month of March. The analytical results of the Stormwater sample collected during a qualifying storm event on March 28, 2016 are attached to this cover letter. In addition, a completed qualitative monitoring report and partially completed DMR form are attached to this cover letter. Results from the March 28, 2016 sampling event show an exceedance of the following parameter at or above the corresponding benchmark: • SDO #004 (02/03/16) —Copper — 0.0122 mg/L (Benchmark 0.007 mg/L) Colfax - Monroe Facility remains in Tier Three of the NPDES General Permit No. NCG030000. The person designated to act as the permittee by Coflax - Monroe Facility should complete all "Red" sections of the attached Stormwater Discharge Monitoring Report (DMR). The completed DMR form should then be mailed to the regulatory agency Central Files. Shield greatly appreciates the opportunity to provide environmental services to Colfax. If you have any questions in reference to this document or require further information, please feel free to contact either of the undersigned at (704) 394-6913. Respectfully, SHIELD ENGINEERING, INC. VV 1 Mclinda . Greene M irk C. Boland, P.E. Senior Engineer Pr ncipal Engineer Attachments: Analytical Results Qualitative Monitoring Report Stormwater Discharge Monitoring Report H:\Projects\2015\1150109-02 Colfax Stormwater\cover letters\cover letter - Mar 2016.docx 4301 Taggart Creek Road Telephone 704.394,6913 Charlotte, NC 28208 vrawshieldengineering.com Fax 704.394.6968 t� ®�� .NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For, guidance on filling out this form, please visit: e/web/wq/ws/su/nndesswfttab-4 Permit No.: 0q `or Certificate of Coverage No.: N&/G/>/33� Facility Name: CUL FAK 14�4u/D yAn/DLIN4 County: u.uron/ Phone No. Inspector: -P4 A Y //F AIOL Date of Inspection: 3 -? Time of Inspection: e,77 30 Total Event Precipitation (inches): D -3 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ® Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the j permitted site outfall. The previous measurable storm event must have been at least 7Z hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter i interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, 1 certify Nett this report is accurate and complete to the best of my knowledge: (Signature of Pei't tee or Designee) Page 1 of 2 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. fro'f Structure (pipe, ditch, etc.) -,P/7-0A Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: L i4/fr Uwtay. 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.):. NONE 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 O 3 4 5 S. Floating Solids: Choose the number which best describes the amount of Floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: lD 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 Q) 3 4 5 7. Is there any foam in the stormwater discharge? Yes S. Is there an oil sheen in the stormwater discharge"? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes AD 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU@42, Las[ modified 10/25/2012 aceAnalyticala / .nuwpncelebs.cwn April 08, 2016 Daniel Cox Colfax Fluid Handling 1710 Airport Road Monroe, NC 28110 RE: Project: STORMWATER Pace Project No.: 92291722 Dear Daniel Cox: Pace Analytical Services, Inc. 9B00 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on March 29, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Liamm Harrison liamm-harrison@pacelabs.com Project Manager Enclosures cc: Accounts Payable, Colfax Fluid Handling Y PCCO TNI 40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, without ire written consent of Pace Analytical Services, Inc., Page 1 of 27 aceAnalytical a wwxpeceleee. uvn Project: STORMWATER Pace Project No.: 92291722 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification We 9800 Kincey Ave. Ste 100. Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #; E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Vlrglnia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Vlrginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not oe reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 27 Pace Analytical Services, Inc. • aceAnalytical 9800 Kincey Ave. Suite 100 Hunterswire, NC 2807B -� ewwyecelecs.cwn (704)875-9092 SAMPLE ANALYTE COUNT Project: STORMWATER Pace Project No: 92291722 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92291722001 OF-004 EPA 1664B JMS 1 PASI-C EPA 608 SWB 27 PASI-C EPA 200.7 CDF 8 PASI-A EPA245.1 HVK 1 PASI-A EPA625 Bpi 58 PASI-C EPA 624 GAW 34 PASI-C SM 2540D MJP 1 PASI-A EPA 9040 TEP 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 27 aceAnalyticale ( wwn.pacelees.com f ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersville, NC 26078 (704)875-9092 Project: STORMWATER Pace Project No.: 92291722 Sample: OF-004 Lab ID: 92291722001 Collected: 03/28/1607:35 Received: 03/29/1613:42 Matrix. Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease NO mg/L 5.0 1 04101/1607:22 608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3510 Aldrin NO ug/L 0.050 1 04/06/16 09:30 04/06/16 1351 309-00-2 alpha-BHC ND ug/L 0.050 1 04/06/16 09:30 04/06/16 13:51 319-64-6 beta-BHC NO ug/L 0.050 1 04/06/16 09:30 04/06/1613:51 319-85-7 delta-BHC ND ug/L 0.050 1 04/06/16 09:30 04/06/16 13:51 319-86-8 - gamma-BHC (Lindane) NO ug/L 0.050 1 04/06/16 09:30 04/06/16 13:51 58-89-9 Chlordane (Technical) ND ug/L 0.50 1 04/06/16 09:30 04/06/16 13:51 57-74-9 4,4'-DDD ND ug/L 0.050 1 0410611609:30 04/06/161351 72-54-8 4,4'-DDE NO ug/L 0.050 1 04/06/16 09:30 04/06/16 13:51 72-55-9 4,4'-DDT NO ug/L 0,050 1 04/06/16 09:30 04106/1613:51 50-29-3 Dieldrin ND ug/L 0.050 1 04/06/16 09:30 04/06/16 13:51 60-57-1 EndasulfanI ND ug/L 0.050 1 04/06/16 09:30 04106/1613:51 959-98-8 Endosulfan ll ND ug/L 0.050 1 0410611609:30 04/06/16 13:51 33213-65.9 Endosulfan sulfate ND ug/L 0,050 1 04/06/16 09:30 04106/1613:51 1031-07-8 Endrin ND ug/L 0.050 1 04105/1609:30 04106/1613:51 72-20-8 Endrin aldehyde ND ug/L 0.050 1 04/06/16 09:30 04/0611613:51 7421-93-4 Heptachlor ND ug/L 0.050 1 04/06116 09:30 04/06/16 13:51 76-44-8 Heptachlor epoxide ND ug/L 0.050 1 04/06/16 09:30 04/06/1613:51 1024-57-3 PCB-1016 (Aroclor 1016) ND ug/L 0.50 1 04/06/16 09:30 04/06/16 13:51 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 0.50 1 04/06/1609:30 04/06/16 13:51 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 0.50 1 04/05/16 09:30 04/06/16 1351 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 0.50 1 04/06/16 09:30 04/06/16 13:51 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.50 1 04/06116 09:30 04/06/16 13:51 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.50 1 04/06116 09:30 04/06/16 13:51 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.50 1 04/06/16 09:30 04106/16 13:51 11096-82-5 Toxaphene ND ug/L 0.50 1 0410611609:30 04106/1613:51 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 78 % 20-110 1 04/06116 09:30 04/06/16 13:51 877-09-8 H5 Decachlorobiphenyl (S) 21 % 20-138 1 04/06/16 09:30 04/06/16 13:51 2051-24-3 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Arsenic ND ug/L 10.0 1 03/30116 20:00 03/31/16 21:24 7440-38-2 Cadmium NO ug/L 1.0 1 03/3011620:00 03131/1621:24 7440-43-9 Chromium NO ug/L 5.0 1 0313011620:00 0313111621:24 7440-47-3 Copper 12.2 ug/L 5.0 1 03/30116 20:00 03/31/16 21:24 7440-50-8 Lead ND ug/L 5.0 1 03/30/16 20.00 03131/16 21:24 7439-92-1 Nickel NO ug/L 5.0 1 0313011620:00 03/31/1621:24 7440-02-0 Silver NO ug/L 5.0 1 03/30/16 20:00 03/31/16 21:24 7440-22.4 Zinc 46.9 ug/L 10.0 1 03/30116 20:00 03/31/16 21:24 7440-66-6 245.1 Mercury Analytical Method. EPA 245.1 Preparation Method: EPA 245.1 Mercury ND ug/L 0.20 1 0313111614:10 04/04/1615:50 7439-97-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/0812016 01:03 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 27 Paco Analytical Services, Inc. Kincey Ave, te 100 ® 9000Huntenwille. NC128076 J, aceAnalytical J wwwpacalab, tom 1704)875-9092 ANALYTICAL RESULTS Project: STORMWATER Pace Project No.: 92291722 Sample: OF-004 Lab ID: 92291722001 Collected: 03/28/16 07:35 Received: 03/2911613:42 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 Acenaphthene ND ug/L 5.0 1 03/3011613:42 04/01/16 08:34 83-32-9 Acenaphthylene ND ug/L 5.0 1 03130/1613:42 04/01/16 08:34 208-95-8 Anthracene NO ug/L 5.0 1 03/3011613:42 04101/1608:34 120-12-7 Senzo(a)anthracene ND ug/L 5.0 1 03/30/1613:42 04/01/1608:34 56-55-3 Benzo(a)pyrene ND ug/L 5.0 1 03/30116 13:42 04/01/16 08:34 50-32-8 Benzo(b)0uoranthene NO ug/L 5.0 1 03/30M613:42 D4/0111608:34 205-99-2 Benzo(g,h,i)perylene ND ug/L 5.0 1 03/30/16 13:42 04/01/16 08:34 191-24-2 Benzo(k)6uoranthene NO ug/L 5.0 1 03/30/16 13:42 04/01/16 08:34 207-08-9 4-Bromophenylphenyl ether NO ug/L 5.0 1 03/30/16 13:42 04/01/16 08:34 101-55-3 Butylbenzylphthalate NO ug/L 5.0 1 03/3011613:42 04101/1608:34 85-68-7 4-Chloro-3-methylphenol NO ug/L 5.0 1 03/30/16 13:42 04/01/16 08:34 59-50-7 b1s(2-Chloroethoxy)melhane NO ug/L 10.0 1 03130/1613:42 04/01/1608*34 111-91-1 bis(2-Chloroethyp ether ND ug/L 5,0 1 03/3011613:42 04/01/16 08:34 111-44-4 bis(2-Chloroisopropyl) ether NO ug/L 5.0 1 031301161342 04/01/16 08:34 108-60-1 2-Chloronaphthalene NO ug/L 5.0 1 03/3011613:42 04/0l/1608:34 91-58-7 2-Chlorophenol NO ug/L 5.0 1 0313011613:42 0410111608:34 95-57-8 4-Chlorophenylphenyl ether NO ug/L 5.0 1 03/30/1613:42 04/01/1605:34 7005-72-3 Chrysene NO ug/L 5.0 1 D3/3011613:42 04/01/16 08:34 218-01-9 Dibenz(a,h)anthracene NO ug/L 5.0 1 03/3011613:42 04/01116 08:34 53-70-3 3,3'-Dichlorobenzidine NO ug/L 25.0 1 03/30/16 13:42 04/01/16 08:34 91-94-1 2,4-Dichlorophenol NO ug/L 5.0 1 03/30/16 13:42 04/01/15 08:34 120-83-2 Dlethylphthalate NO ug/L 5.0 1 03/3011613:42 04/0111608*34 64-66-2 2,4-Dimethylphenol NO ug/L 10.0 1 03/30/16 13:42 04/01/16 08:34 105-67-9 Dimethylphthalate NO ug/L 5.0 1 03/3011613:42 04/01/1508:34 131-11-3 Di-n-butylphthalate NO ug/L 5.0 1 03/30/16 13:42 04/01/16 08:34 84-74-2 4,6-Dinitro-2-methylphenol NO ug/L 20.0 1 03/3011613:42 04101/1508:34 534-52-1 2,4-Dinilrophenol NO ug/L 50.0 1 03/30/16 13:42 04101It 808:34 51-28-5 2,4-Dinitrotoluene NO ug/L 5.0 1 03/3011613:42 04/01/16 08:34 121-14-2 2,6-Dinitrotoluene NO ug/L 5.0 1 03/3011613:42 04/01/16 08:34 606-20-2 Di-n-octylphthalate NO ug/L 5.0 1 03/30/16 13:42 04/01116 08:34 117-84-0 bis(2-Ethylhexyl)phthalate NO ug/L 5.0 1 03/30116 13:42 04/01/16 08:34 117-81-7 Fluoranthene NO ug/L 5,0 1 03/30/16 13:42 04/01/16 08:34 206-44-0 Fluorene NO ug/L 5.0 1 03/30/16 13:42 04/01116 08:34 86-73-7 Hexachloro-1,3-butadiene NO ug/L 5.0 1 03/30/16 1342 04/01/16 08:34 87-68-3 Hexachlorobenzene NO ug/L 5.0 1 03/30/16 13:42 04/01116 08:34 118-74-1 Hexachlorocyclopentadiene NO ug/L 10.0 1 03/30/16 13:42 04/01/16 08:34 77-47-4 Hexachloroethane NO ug/L 5.0 1 03/30/16 13:42 04/01/16 08:34 67-72-1 Indeno(1,2,3-cd)pyrene NO ug/L 5,0 1 03/30/16 13:42 04/01/16 08:34 193-39-5 Isophorone NO ug/L 10.0 1 03/3011613:42 04/01/16 08:34 78-59-1 Naphthalene NO ug/L 5.0 1 03/30/16 13:42 04/01/16 08:34 91-20-3 Nitrobenzene NO ug/L 5.0 1 03/30/16 13:42 04/01/16 08:34 98-95-3 2-Nitrophenol NO ug/L 5.0 1 03/30/16 13:42 04/01/1608.34 88-75-5 4-Nitrophenol ND ug/L 50.0 1 03/30/16 13:42 04/01116 08:34 100-02-7 N-Nitrosodimethylamine NO ug/L 5.0 1 03/3011613:42 04/01/1608:34 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 5.0 1 03/30/16 13:42 04101/1608:34 621-64-7 N-Nitrosodiphenylamine ND ug/L 10.0 1 03/3011613:42 04/01/16 08:34 86-30-6 Penlachlerophenol NO ug/L 10.0 1 03/3011613:42 04/0111608:34 87-86-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/08/2016 01:03 PM without tho writlen consent of Paco Analytical Services, Inc.. Page 5 of 27 Paco Analytical Services, Inc. ace® 9800 unceyAve, 28100 Analytical Hntersville, NCG28078078 rmw.perxlab.con (704)875-9092 ANALYTICAL RESULTS Project: STORMWATER Pace Project No.: 92291722 Sample: OF-004 Lab ID: 92291722001 Collected: 03/28/1607:35 Received: 0312911613*42 Matrix:Water Parameters Results Units Report Limit OF Prepared 625 MSSV Phenanthrene Phenol Pyrene 1, 2, 4-Trichlorobe nzene 2,4,6-Trichlorophenol Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl(S) Terphenyl-d 14 (S) Phenol-d6 (S) 2-Fluorophenol(S) 2,4,6-Tribromophenol (S) 624 Volatile Organics Benzene Bro mod i ch loromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Dibromochlorometh ane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Methylene Chloride 1,1,2,2-Tetrachloroethane Tetrachloroelhene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloreethene Trichlo rofluoromet ha ne Vinyl chloride Surrogates 4-Sromofluorobenzene (S) Analytical Method: EPA 625 Preparation Method: EPA 625 Analyzed CAS No. Qual NO ug/L 5.0 1 0313011613:42 04101/1608:34 85-01-8 NO ug/L 5.0 1 03/30/1613:42 04/01/1608:34 NO ug/L 5.0 1 03/30/16 13:42 04/01/16 08:34 129-00-0 NO ug/L 5.0 1 03/30/16 13:42 04101/16 08:34 120-82-1 NO ug/L 10.0 1 03/30/16 13:42 04/01/16 08:34 88-06-2 75 % 10-120 1 03/3011613:42 04101/1608:34 4165-60-0 75 % 15-120 1 03/30/1613:42 04101/1608:34 321-60-8 74 % 11-131 1 03/30/1613:42 04/01/1608:34 1718-51-0 27 % 10-120 1 03/30/1613:42 04101/1608:34 13127-86-3 40 % 10-12D 1 03/30/1613:42 04101/1606:34 367-12-4 83 % 10-137 1 03/30/1613:42 04101/1608:34 118-79-6 Analytical Method: EPA 624 NO ug/L 2.0 1 04106/1615:18 71-43-2 NO ug/L 2.0 1 04/06/16 15:18 75-27-4 NO ug/L 2.0 1 04106/1615:18 75-25-2 NO ug/L 2.0 1 04/06/16 15:18 74-83-9 NO ug/L 2.0 1 04/06/16 15:18 56-23-5 NO ug/L 2.0 1 04106/1615:18 108-90-7 NO ug/L 2.0 1 04/06/16 15:18 75-00-3 NO ug/L 2.0 1 04/05/16 15:18 67-66-3 NO ug/L 2.0 1 04/06/16 15:18 74-87-3 ND ug/L 2.0 1 04/06/16 15:18 124-48-1 NO ug/L 2.0 1 04/06/16 15:18 95-50-1 NO ug/L 2.0 1 04/06/16 15:18 541-73-1 ND ug/L 2.0 1 04/06/16 15:18 106.46-7 NO ug/L 2.0 1 04/06/16 15:18 75-34-3 NO ug/L 2.0 1 04/06/16 15:18 107-06-2 NO ug/L 2.0 1 0410611615:18 75-35-4 NO ug/L 2.0 1 04/06/16 15:18 156-59-2 ND ug/L 2.0 1 04106/16 15:18 156-60-5 NO ug/L 2.0 1 04/06/16 15:18 78-87-5 NO ug/L 2.0 1 04/06/16 15:18 10051-01-5 NO ug1L 2.0 1 04/0611615:18 10061-02-6 NO ug/L 2.0 1 04/06/16 15:18 100-41-4 4.8 ug/L 2.0 1 04/06/161518 75-09-2 C9 ND ug/L 2.0 1 04/06/16 15:18 79-34-5 ND ug/L 2.0 1 04/06/16 15:18 127-18-4 ND ug/L 2.0 1 04106/1615:18 108-86-3 ND ug/L 2.0 1 04106/1615:18 71-55-6 ND ug/L 2.0 1 04/06/16 15:18 79-00-5 ND ug/L 2.0 1 04/06/16 15:18 79-01-6 ND ug/L 2.0 1 04/06/16 15:18 75-69-4 NO ug/L 2.0 1 04/06/16 15:18 75-01-4 99 % 70-130 1 04/06/1615: 18 460-00-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, Date: 04/08/2016 01:03 PM without Me written consent of Pace Analytical Services, Inc.. Page 6 of 27 aceAnalyticale ewwpece0pv.com i ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92291722 Sample: OF-004 Lab ID: 92291722001 Collected: 03/28/16 07:35 Received: 03/29/16 13:42 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 624 Volatile Organics Analytical Method: EPA 624 Surrogates Toluene-d8 (S) 101 % 70-130 1 04/06/1615:18 2037-26-5 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 04/06/16 15:18 17060-07-0 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 34.8 mglL 5.0 1 03/30/16 11:50 9040 pH Analytical Method: EPA 9040 pH 6.6 Std. Units 0.10 1 04/01/16 10:30 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 04/08/2016 01:03 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 27 Place Analytical w pecereos.rom QUALITY CONTROL DATA Pace Analytical Services, Inc. 9000 Kincey Ave. Suite 100 Runlersville, NC 20078 (704)875-9092 Project: STORMWATER Pace Project No.: 92291722 QC Batch: GCSW24558 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92291722001 METHOD BLANK: 1699639 Associated Lab Samples: 92291722001 Parameter Units Oil and Grease mg/L LABORATORY CONTROL SAMPLE: 1699640 Parameter Units Oil and Grease mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 04/01/16 07:14 Spike LCS LCS %Rec Conc. Result % Rec Limits Qualifiers 40 37.3 93 78-114 MATRIX SPIKE SAMPLE: 1699641 35236276001 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Oil and Grease mg/L 4.8J 40 44.4 99 78-114 Results presented on this page are In the unite Indicated by the 'Units" column except where an eltemate unit Is pmsented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in full, Date: 04/08/2016 01:03 PM wiUcut the written consent of Pace Analytical Services, Inc.. Page 8 of 27 _ aceAnalyticalo wn+ypersleas.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvillo, NC 28078 1704)875-9092 Project: STORMWATER Pace Project No.: 92291722 OC Batch: MERP/9162 Analysis Method: EPA 245.1 QC Batch Method: EPA 245.1 Analysis Description: 245.1 Mercury Associated Lab Samples: 92291722001 METHOD BLANK: 1697838 Matrix: Water Associated Lab Samples: 92291722001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 04104/1615:29 LABORATORY CONTROL SAMPLE: 1697839 Spike LCS LCS % Rec Parameter Units Cone. Result %Rec Limits Qualifiers Mercury ug/L 2.5 2.4 97 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1697840 1697841 MS MSD 92291612002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual Mercury ug/L NO 2.5 2.5 2.4 2.6 96 102 70-130 5 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1697842 1697843 MS MSD 92291732005 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Cone. Result Result %Rec %Rec Limits RPD Qual Mercury ug/L NO 2.5 2.5 2.4 2.5 96 99 70-130 2 Re suite presented on this page are In the units Indicated by the "Unite" column except where an alternate unit Is prevented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/08/2016 01:03 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 27 aceAnalytical iwwwpacdatu. n QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92291722 QC Batch: MPRP/21163 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92291722001 METHOD BLANK: 1698026 Matrix: Water Associated Lab Samples: 92291722001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Arsenic ug/L ND 10.0 03/31/1620:38 Cadmium ug/L ND 1.0 03/31/1620:38 Chromium ug/L ND 5.0 03/31/16 20:38 Copper ug/L ND 5.0 03/31/1620:38 Lead ug/L ND 5.0 03/31/1620:38 Nickel ug/L ND 5.0 03/31/16 20:38 Silver ug/L ND 5.0 03/31/1620:38 Zinc ug/L ND 10.0 03/31/16 20:38 LABORATORY CONTROL SAMPLE: Parameter 1698027 Units Spike Conc. LCS Result LCS % Rec %Rec Limits Qualifiers Arsenic ug/L 500 463 93 85-115 Cadmium ug/L 500 496 99 85-115 Chromium ug/L 500 527 105 85-115 Copper ug/L 500 498 100 85-115 Lead ug/L 500 488 98 85-115 Nickel ug/L 500 496 99 85-115 Silver ug/L 250 248 99 85-115 Zinc ug/L 500 472 94 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1698028 1698029 MS MSD 92291512002 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Dust Arsenic ug/L NO 500 500 449 449 90 90 70-130 0 Cadmium ug/L NO 500 500 479 479 96 96 70-130 0 Chromium ug/L 7.1 500 500 514 508 101 100 70-130 1 Copper ug/L ND 500 500 481 474 96 95 70-130 2 Lead ug/L ND 500 500 465 465 93 93 70-130 0 Nickel ug/L 3.01 500 500 476 477 95 95 70-130 0 Silver ug/L ND 250 250 240 237 96 95 70-130 1 Zinc ug/L ND 500 500 454 455 90 91 70-130 0 Reauas presentee on this page are In the units Indicated by the "Units" column except where an alternate unit le presented to the right al the n auC. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/08/2016 01:03 PM without the written consent of Pace Analytical Services, Inc,. Page 10 of 27 aceAnalytical WNWpfire(ab9 Cain r QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92291722 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1698030 1698031 MS MSD 92291732002 Spike • Spike MS MSC, MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Arsenic ug/L ND 500 500 437 429 87 86 70-130 2 Cadmium ug/L ND 500 500 470 461 94 92 70-130 2 Chromium ug/L 3.5J 500 500 495 483 98 96 70-130 2 Copper ug/L ND 500 500 474 465 95 93 70-130 2 Lead ug/L ND 500 500 461 453 92 91 70-130 2 Nickel ug/L ND 500 500 472 461 94 92 70-130 2 Silver ug/L ND 250 250 237 234 95 93 70-130 2 Zinc ug/L 32.2 500 Soo 486 474 91 88 70-130 2 Results presented on this page are In the units Indicated by the "Unite" column except where an alternate unit Is praeontad to the d9ht of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/08/2016 01:03 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 27 aceAnalytical ."celnesmm t QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kimey Ave, Suite 100 Huntersviile, NC 28078 (704)875-9092 Project: STORMWATER . Pace Project No.: 92291722 OC Batch: MSV/36271 Analysis Method: EPA 624 OC Batch Method: EPA 624 Analysis Descripliom 624 MSV Associated Lab Samples: 92291722001 METHOD BLANK: 1703241 Associated Lab Samples: 92291722001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,1,1-Trichloroethane ug/L NO 2.0 04/0611614:27 1,1,2,2-Tetrachloroethane ug/L NO 2.0 04/06/16 14:27 1,1,2-Trichloroethane uglL NO 2.0 04/05/16 14:27 1,1-Dichloroethane ug/L NO 2.0 04/06/16 14:27 1,1-Dichloroelhene ug/L NO 2.0 04/05/16 14:27 1,2-Dichlorobenzene ug/L NO 2.0 04/06MIS 14:27 1,2-Dichloroethane ug/L NO 2.0 04/06/16 14:27 1,2-Dichloropropane ug/L NO 2.0 04/06/16 14:27 1,3-Dichlorobenzene ug/L NO 2.0 04106M614:27 1,4-Dichlorobenzene ug/L NO 2.0 0410611614:27 Benzene ug/L NO 2.0 04/06/16 14:27 Bromodichloromelhane ug/L NO 2.0 04/0611614:27 Bromoform ug/L NO 2.0 04/0611614:27 Bromomethane ug/L ND 2.0 04/0611614:27 Carbon tetrachloride ug/L NO 2.0 04106/16 14:27 Chlorobenzene ug/L ND 2.0 04/06/16 14:27 Chlorcethane ug/L NO 2.0 04/06/16 14:27 Chloroform ug/L NO 2.0 0410611614:27 Chloromethane ug/L NO 2.0 04/06/16 14:27 cis-1,2-Dichloroethene ug/L NO 2.0 04106/16 14:27 cis-1,3-Dichloropropene ug/L ND 2.0 04106/16 14:27 Dibromochloromethane ug/L NO 2.0 04/06/16 14:27 Ethylbenzene ug/L NO 2.0 04/06/16 14:27 Methylene Chloride ug/L NO 2.0 04/06/16 14:27 Tetrachloroethene ug/L NO 2.0 04/06/16 14:27 Toluene ug1L NO 2.0 04/06/16 14:27 trans-1,2-Dichloroethene ug/L NO 2.0 04/06/16 14:27 trans-1,3-Dichloropropene ug/L ND 2.0 04/06/16 14:27 Trichloroethene ug/L NO 2.0 04/0611614:27 Trichloro0uoromethane ug/L ND 2.0 0410611614:27 Vinyl chloride ug/L ND 2.0 04/06/16 14:27 1.2-Dichloroethane-d4 (S) % 97 70-130 04/06/16 14:27 4-Bromofluorobenzene (S) % 98 70-130 G4106/16 14:27 Toluene -dB (S) % 99 70-130 04/06/16 14:27 Qualifiers LABORATORY CONTROL SAMPLE: 1703242 Spike LCS LCS %Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1-Trichloroethane ug/L 50 44.2 88 52-162 1,1,2,2-Tetrachloroethane ug/L 50 48.9 98 46-157 Results presentee on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04108/2016 01:03 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 27 aceAnalytical e a»w pecelem.tdm QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92291722 LABORATORY CONTROL SAMPLE: Parameter 1703242 Units Spike Conc. LCS Result LCS % Rec %Rec Limits 1,1,2-Trichlorcethane ug/L 50 45.5 91 52-150 1,1-Dichloroethane ug/L 50 43.7 87 59-155 1,1-Dichloroethene ug/L 50 45.9 92 1-234 1,2-Dichlorobenzene ug/L 50 45.9 92 18-190 1,2-Dichloroethane ug/L 50 40.4 81 49-155 1,2-Dichloropropane ug/L 50 44.4 89 1-210 1,3-Dichlorobenzene ug/L 50 46.2 92 59-156 1,4-Dichlorobenzene ug/L 50 46.9 94 18-190 Benzene ug/L 50 47.2 94 37-151 Bromodichloromethane ug/L 50 48.9 98 35-155 Bromoform ug/L 50 48.4 97 45-169 Bromomethane ug/L 50 48.1 96 1-242 Carbon tetrachloride ug/L 50 48.5 97 70-140 Chlorobenzene ug/L 50 45.9 92 37-160 Chlorcethane ug/L 50 41.2 82 14-230 Chloroform ug/L 50 45.1 90 51-138 Chloromelhane ug/L 50 42.1 84 1-273 cis-1,2-Dichloroethene ug/L 50 43.9 68 68-146 cis-1,3-Dichloropropene ug/L 50 46.7 93 1-227 Dibromochloromethane ug/L 50 48.1 96 53-149 Ethylbenzene ug/L 50 46.3 93 37-162 Methylene Chloride ug/L 50 33.4 67 1.221 Telrachloroethene ug/L 50 46.9 94 64-148 Toluene ug/L 50 46.5 93 47-150 trans-1,2-Dichloroethene ug/L 50 44.8 90 54-156 trans-1,3-Dichloropropene ug/L 50 45.5 91 17-183 Trichloroethene ug/L 50 43.9 88 71-157 Trichlorofluoromethane ug/L 50 42.5 05 17-181 Vinyl chloride ug/L 50 46.6 93 1-251 1,2-Dichloroethane-d4 (S) % 91 70-130 4-Bromoffuorobenzene (S) % 102 70-130 Toluene-dB(S) % 100 70-130 Pace Analytical services, Inc. 9800 Kincey Ave. Suite 100 Hunters"le, NC 20078 (704)875-9092 Qualifiers Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit b presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full. Dale: 04/08/2016 01:03 PM without the written consent of Pace Analytical Services, Inc,. Page 13 of 27 b aceAnalytical QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92291722 QC Batch: OEXT/41796 Analysis Method: EPA608 QC Batch Method: EPA3510 Analysis Description: BOB GCS Pest PCB Associated Lab Samples: 92291722001 METHOD BLANK: 1702658 Associated Lab Samples: 92291722001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 4,4'-DDD ug/L NO 0,050 04106/1614:09 4,4'-DDE ug/L NO 0.050 04106/1614:09 4,4'-DDT ug/L NO 0.050 04)0611614:09 Aldrin ug/L NO 0.050 04/06116 14:09 alpha-BHC ug/L NO 0.050 0410611614:09 beta-BHC ug/L NO 0,050 04/06/16 14:09 Chlordane (Technical) ug/L NO 0.50 04/06/16 14:09 delta-BHC ug/L NO 0.050 04/06116 14:09 Dieldrin ug/L NO 0.050 04/06116 14:09 Endosulfan I ug/L NO 0.050 04/06116 14:09 Endosulfan II ug/L NO 0.050 04/06/16 14:09 Endosulfan sulfate ug/L NO 0.050 04/06116 14:09 Endrin ug/L ND 0.050 04/06/16 14:09 Endrin aldehyde ug/L NO 0,050 04/06/16 1409 gamma-BHC (Lindane) ug/L NO 0.050 04/06/16 14:09 Heptachlor ug/L ND 0.050 0410611614:09 Heptachlor epoxide ug/L ND 0.050 04/06/16 1409 PCB-1016 (Arodor 1016) ug/L ND 0.50 04/06/16 14:09 PCB-1221 (Aroclor 1221) ug/L ND 0.50 04/06/16 14:09 PCB-1232 (Aroclor 1232) ug/L ND 0.50 04/06/16 14:09 PCB-1242 (Aroclor 1242) ug/L NO 0.50 04/06/16 14:09 PCB-1248 (Aroclor 1248) ug/L ND 0.50 04/06/16 14:09 PCB-1254 (Aroclor 1254) ug/L ND 0.50 04/06/16 14:09 PCB-1260 (Arodor 1260) ug/L NO 0.50 04/06/16 14:09 Toxaphene ug/L ND 0.50 04/06116 14:09 Decachlorobiphenyl (S) % 31 20-138 04/06/16 14:09 Tetrachloro-m-xylene (S) % 79 20-110 04/06/16 14:09 LABORATORY CONTROL SAMPLE &LCSD: Parameter 1702659 Units Spike Conc. 1702660 LCS LCSD Result Result 4,4'-DDD ug1L .25 0.19 0.20 4,4'-DDE u9/1- .25 0.18 0.19 4,4'-DDT ug1L .25 0.20 0.21 Aldrin ug/L .25 0.18 0.19 alpha-BHC ug1L .25 0.19 0.20 beta-BHC ug1L .25 0.20 0.22 delta-BHC ug/L .25 0.22 0.22 Dieldrin ug/L .25 0.19 0.20 Endosulfan I ug1L .25 0.23 0.23 Pace Analytical Services, Inc. 9900 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Qualifiers LCS old Rec LCSD %Rec %Rec Limits RPD Max RPD 78 82 31-141 5 30 73 78 30-145 7 30 80 85 25-160 5 30 74 76 42-122 3 30 76 81 37-134 6 30 81 90 17-147 10 30 90 88 19-140 2 30 78 83 36-146 5 30 93 91 45-153 1 30 Results presented on this page are In the true Indicated by the "Unite" column esceptwhere an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS Qualifiers This report shall not be reproduced, except in full. Date: 04/08/2016 01:03 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 27 aceAnalyticalm aww.pecelaes.com i QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92291722 LABORATORY CONTROL SAMPLE 8 LCSD: 1702659 Spike Parameter Units Conc. Endosulfan II ug/L .25 Endosultan sulfate ug/L .25 Endrin ug/L .25 Endrin aldehyde ug/L .25 gamma-BHC (Lindane) ug/L .25 Heptachlor ug/L .25 Heptachlor epoxide ug/L .25 Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % Pace Analytical Services, Inc. 9800 Kincey Ave. -Suite too Huntorsville, NC 28078 (704)875-9092 1702660 LCS LCSD LCS LCSD % Rec Max Result Result %Rec %Rec Limits RPD RPD Qualifiers 0.21 0.22 86 90 1-202 5 30 0.22 0.23 89 93 26-144 5 30 0.20 0.21 82 86 30-147 5 30 0.19 0.20 76 81 50-150 6 30 0.20 0.21 82 87 32-127 6 30 0.19 0.20 77 80 34-111 3 30 0.20 0.22 83 87 41-126 5 30 40 47 20-138 85 90 20-110 Resuhs presentee on this page are In the units Indicated by the "Untls' column except wham an alternate unit Is presentee to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 04/08/2016 01:03 PM without the written consent of Pace Analytical Services, Inc., Page 15 of 27 aceAnalytical e wwwpe[elabs.m+n QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 2BO78 (704)875-9092 Project: STORMWATER Pace Project No.: 92291722 OC Balch: OEXT/41675 Analysis Method: EPA625 OC Batch Method: EPA 625 Analysis Description: 625 MSS Associated Lab Samples: 92291722001 METHOD BLANK: 1697920 Associated Lab Samples: 92291722001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed Qualifiers 1,2,4-Trichlorobenzene ug/L NO 5.0 03/31/16 1849 2,4,6-Trichlorophenol ug/L NO 10.0 03131/1618:49 2,4-Dichlorophenol ug/L NO 5.0 0313l/1618:49 2,4-Dimethylphenol ug/L NO 10.0 03/31/16 18:49 2,4-Dinilrophenol ug/L NO 50.0 03/31/1618:49 2,4-Dinitrotoluene ug/L NO 5.0 03131/1618:49 2,6-Dinitrotoluene ugfL ND 5.0 03/3111618:49 2-Chloronaphthalene ug/L NO 5.0 03/31/16 18:49 2-Chlorophenol ug/L NO 5.0 03/31/16 18:49 2-Nitrophenol ug/L NO 5.0 0313111618:49 3,3'-Dichlorobenzidine ugf- NO 25.0 03/31/16 18:49 4,6-Dinitro-2-methylphenol ug/L NO 20.0 03/31/1618:49 4-Bromophenylphenyl ether ug/L NO 5.0 03/31/16 1849 4-Chloro-3-methylphenol ug/L ND 5.0 0313111618:49 4-Chlorophenylphenyl ether ug/L NO 5.0 03/31/16 16:49 4-Nitrophenol ugf- NO 50.0 03131/1618:49 Acenaphthene ugfL NO 5.0 03131/1618:49 Acenaphlhylene ug/L NO 5.0 03131/1618:49 Anthracene ugfL NO 5.0 0313l/1618:49 Benzo(a)anthracene ug/L NO 5.0 031311161BA9 Benzo(a)pyrene ug/L NO 5.0 03/31/16 18:49 Benzo(b)lluoranthene ug/L NO 5.0 0313111618:49 Benzo(g,h,i)perylene ug/L NO 5.0 03131/1618:49 Benzo(k)Buoranthene ug/L ND 5.0 03/31/1618:49 bis(2-Chloroelhoxy)methane ug/L NO 10.0 0313111618:49 bis(2-Chloroethyl) ether ug/L NO 5.0 03/31/16 18:49 bis(2-Chloroisopropyl) ether ug/L ND 5.0 03/31/16 18:49 bis(2-Ethylhexyl)phthalate ug/L NO 5.0 03131/1618:49 Butylbenzylphihalate ug/L NO 5.0 0313111618:49 Chrysene ug/L NO 5.0 03131/1618:49 Di-n-bulylphthalate ug/L ND 5.0 0313111618:49 Di-n-octylphthalate ug/L ND 5.0 03/31/1618:49 Dibenz(a.h)anthracene ug/L NO 5.0 03/31/16 18:49 Dlethylphthalate ug/L NO 5.0 03/31/16 18:49 Dimethylphthalate ug/L NO 5.0 03131/1618:49 Fluoranthene uglL NO 5.0 03131/16 18:49 Fluorene ug/L NO 5.0 03/31/16 18:49 Hexachloro-1,3-buladiene ugf- NO 5.0 03131/1618:49 Hexachicrobenzene ug/L NO 5.0 0313111618:49 Hexachlorocyclopentadiene ug/L NO 10.0 0313111618:49 Hexachlomethane ug/L NO 5.0 031311161849 Results presentee an this page are In the units Indicated by the "Units" column except where an alternate unit Is presentee to the pant of the mpUtt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 04/08/2016 01:03 PM without the wriffen consent of Pace Analytical Services, Inc,. Page 16 of 27 aceAnalytical wmvpeceleDd.mn l QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92291722 ME IHOD BLANK: 1697920 Matrix: Water Associated Lab Samples: 92291722001 Blank Reporting Parameter Units Result Limit Analyzed Indeno(1,2,3-cd)pyrene ug/L NO 5.0 03/31/1618:49 Isophorone ug/L NO 10.0 03131/1618:49 N-Nitroso-di-n-propylamine ug/L NO 5.0 03/3111618:49 N-Nitrosodimethylamine ug/L ND 5.0 03/31/1618:49 N-Nitrosodiphenylamine ug/L NO 10.0 03/31/1618:49 Naphthalene ug/L ND 5.0 03/31/1618:49 Nitrobenzene ug/L ND 5.0 03/3111618:49 Pentachlorophenol ug/L ND 10.0 03/3111618:49 Phenanthrene ug/L NO 5.0 03/31/1618:49 Phenol ug/L ND 5.0 03131/1618:49 Pyrene ug/L ND 5.0 03131/1618:49 2,4,6-Tribromophenol(S) % 83 10-137 03/31/16 18:49 2-Fluorobiphenyl (S) % 81 15-120 03/31/16 18:49 2-Fluorophenol (S) % 44 10-120 03/31/16 18:49 Nitrobenzene-d5 (S) % 82 10-120 03/31/16 18:49 Phenol-d6 (S) % 30 10-120 03/31/16 18:49 Terphenyl-d 14 (S) % 97 11-131 03/31/16 18:49 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1697921 Units Spike Conc. LCS Result LCS % Rec %Rec Limits 1,2,4-Trichlorobenzene ug/L 50 32.5 65 44-142 2,4,6-Trichlorophenol ug/L 50 45.1 90 37-144 2.4-Dichlorophenol ug/L 50 39.5 79 1-191 2,4-Dimethylphenol ug/L 50 39.3 79 32-119 2,4-Dinitrophenol ug/L 250 216 86 1-181 2,4-Dinitrololuene ug/L 50 49.4 99 39-139 2,6-Dinitrotoluene ug/L 50 47.1 94 50-158 2-Chloronaphthalene ug/L 50 38.7 77 60-118 2-Chlorophenol ug/L 50 37.5 75 23-134 2-Nitrophenol ug/L 50 41.9 84 29-182 3,3'-Dichlorobenzidine ug/L 100 99.8 100 1-262 4,6-Dinitro-2-methylphenol ug/L 100 94.5 95 1-181 4-Bromophenylphenyl ether ug/L 50 42.2 84 53-127 4-Chloro-3-methylphenol ug/L 100 83.6 84 22-147 4-Chlorophenylphenyl ether ug/L 50 43.3 87 25-158 4-Nitrophenol ug/L 250 91.9 37 1-132 Acenaphthene ug/L 50 38.7 77 47-145 Acenaphthylene ug/L 50 41.9 84 33-145 Anthracene ug/L 50 43.8 88 1-166 Benzo(a)anthracene ug/L 50 45.8 94 33-143 Benzo(a)pyrene ug/L 50 45.0 90 17-163 Benzo(b)iluoranthene ug/L 50 41.2 82 24-159 Benzo(g,h,i)perylene ug/L 50 43.4 87 1.219 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersvllle, NC 28078 (704)875-9092 Qualifiers Results presented on this page are In the units Indicated by the"Unhs" column except "ere an alternate unit la presented to the right of the result. REPORT OF LABORATORY ANALYSIS This repot shall not be repmduced, except in full. Date: 04/08/2016 01:03 PM without the written consent of Pace Analytical Services, Inc„ Page 17 of 27 aceAnalyttcal" wivwpecelabxcom I QUALITY CONTROL DATA Pace Analytical Services, Inc. 98DO Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92291722 LABORATORY CONTROL SAMPLE: 1697921 Spike LCS LCS %Rec Parameter Units Cone. Result % Rec Limits Qualifiers Benzo(k)Ouoranthene ug/L 50 42.1 84 11-162 bis(2-Chloroethoxy)methane ug/L 50 38.4 77 33-184 bis(2-Chloroethyp ether ug/L 50 39.2 78 12-158 bis(2-Chloroisopropyp ether ug/L 50 34.2 68 36-166 bis(2-Ethylhexyl)phthalate ug/L 50 59.1 118 8-158 Butylbenzylphthalate ug/L 50 56.1 112 1-152 Chrysene ug/L 50 44.1 88 17-168 Di-n-butylphthalate ug/L 50 52.6 105 1-118 Di-n-octylphthalate uglL 50 63.4 127 4-146 Dibenz(a,h)anthracene uq/L 50 45.3 91 1-227 Diethylphthalale ug/L 50 47.3 95 1-114 Dimethylphthalale uq/L 50 45.6 91 1.112 Fluoranthene u9IL 50 43.5 87 26-137 Fluorene ug/L 50 43.7 87 59-121 Hexachloro-1,3-butadiene ug/L 50 29.6 59 24-116 Hexachlorobenzene u9/1- 50 43.3 87 1-152 H exa chlorocyclo pent adiene uq/L 50 28.6 57 25-150 Hexachloroethane ug/L 50 30.3 61 40-113 Indeno(1,2,3-cd)pyrene u9I1- 50 48.4 97 1-171 Isophorone ug/L 50 40.7 81 21-196 N-Nilroso-di-n-propylamine u9IL 50 41.0 82 1-230 N-Nitrosodimethylamine ug/L 50 27.1 54 25-150 N-Nitrosodiphenylamine ug/L 50 42.7 85 25-150 Naphthalene ug/L 50 33.6 67 21-133 Nitrobenzene ug/L 50 38.4 77 35-180 Pentachlorophenol ug/L 100 78.3 78 14-176 Phenanthrene ug/L 50 43.3 87 54-120 Phenol ug/L 50 19.7 39 5-112 Pyrene ug/L 50 45.6 91 52-115 2,4,6-Tribromophenol (S) % 93 10-137 2-Fluorobiphenyl(S) % 81 15-120 2-Fluorophenol(S) % 47 10-120 Nitrobenzene-d5 (S) % 82 10-120 Phenol-d6 (S) % 33 10-120 Terphenyl-d14 (S) % 96 11-131 MATRIX SPIKE SAMPLE: 1697922 92291455001 Spike MS MS % Rae Parameter Units Result Cone. Result %Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/L ND 50 30.1 60 44-142 , 2 4,6-Trichlorophenol ug/L ND 50 47A 95 37-144 2,4-Dichlorophenol ug/L ND 50 40.4 81 1-191 2,4-Dimethylphenol ug/L NO 50 40.6 81 32-119 2,4-Dinitrophenol ug/L NO 250 255 102 1-181 2,4-Dinitrotoluene ug/L ND 50 47.3 95 39-139 Results presentee on this page are In the units Indicated by the "units" column except "am in alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/08/2016 01:03 PM without the written consent of Pace Analytical Services, Inc., Page 18 of 27 aceAnalytical I vnvnpecdebxwm QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hum... Was, NC 28078 1704)8759092 Project: STORMWATER Pace Project No.: 92291722 MATRIX SPIKE SAMPLE: 1697922 92291455001 Spike MS MS %Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2,6-Dinitrotoluene ug/L ND 50 46.7 93 50-158 2-Chloronaphthalene ug/L ND 50 39.9 80 60-118 2-Chlorophenol ug/L ND 50 31.9 64 23-134 2-Nitrophenol ug/L ND 50 38.9 78 29-182 3,3'-Dichlorobenzidine ug/L ND 100 75.8 76 1-262 4,6-Dinilro-2-methyiphenol ug/L ND 100 96.3 96 1-181 4-Bromophenylphenyl ether ug/L ND 50 41.3 83 53-127 4-Chloro-3-melhyiphenol ug/L ND 100 89.5 90 22-147 4-Chlorophenylphenyl ether ug/L ND 50 43.4 87 25-158 4-Nitrophenol ug/L ND 250 99.9 39 1-132 Acenaphlhene ug/L ND 50 40.2 80 47-145 Acenaphthylene ug/L ND 50 43.0 86 33-145 Anthracene ug/L ND 50 41.5 83 1-166 Benzo(a)anthracene ug/L ND 50 44.8 87 33-143 Benzo(a)pyrene ug/L ND 50 43.6 85 17-163 Benzo(b)iluoranthene ug/L ND 50 41.0 80 24-159 Benzo(g,h,i)perylene ug/L ND 50 41.1 82 1-219 Benzo(k)tluoranthene ug/L ND 50 41.0 80 11-162 bis(2-Chloroethoxy)methane ug/L ND 50 36.5 73 33-184 bis(2-Chioroethyl) ether ug/L ND 50 32.9 66 12-15B bis(2-Chioroisopropyl) ether ug/L ND 50 29.0 58 36-166 bis(2-Ethylhexypphthalate ug/L ND 50 56.1 109 8-158 Butylbenzylphthalate ug/L ND 50 54.8 107 1-152 Chrysene ug/L ND 50 42.1 81 17-168 Di-n-butylphthalate ug/L ND 50 49.9 100 1-118 Di-n-octylphthalate ug/L ND 50 56.8 114 4-145 Dibenz(a,h)anthracene ug/L ND 50 43.0 86 1-227 Dielhylphthalate ug/L ND 50 45.8 92 1-114 Dimethylphthalate ug/L ND 50 44.1 88 1-112 Fluoranthene ug/L ND 50 40.3 81 26-137 Fluorene ug/L ND 50 43.8. 88 59-121 . Hexachloro-1,3-buladiene ug/L ND 50 27.6 55 24-116 Hexachlorobenzene ug/L ND 50 41.9 84 1-152 Hexachlorocyclopentadiene ug/L ND 50 32.6 65 25-150 Hexachloroethane ug/L ND 50 27.4 55 40-113 Indeno(1.2,3-cd)pyrene ug/L ND 50 45.6 91 1-171 Isophorone ug/L ND 50 41.5 83 21-196 N-Nitroso-di-n-propylamine ug/L ND 50 39A 79 1-230 N-Nitrosodimethylamine ug/L ND 50 22.7 45 25-150 N-Nitrosodiphenylamine ug/L ND 50 40.6 81 25-150 Naphthalene ug/L ND 50 31.1 62 21-133 Nitrobenzene ug/L ND 50 33.5 67 35-180 Pentachlorophenol ug/L ND 100 81.5 80 14-176 Phenanthrene ug/L ND 50 41.0 82 54-120 Phenol ug/L ND 50 18.1 36 5-112 Pyrene ug/L ND 50 46.8 91 52-115 2 4,6-Tribromophenol (S) % 89 10-137 Results presented on this page am In the unite Indic steel by the "Units" column except where an alternate unit Is phisom d to the right of the nasult. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/08/2016 01:03 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 27 aceAnalyticale mvwpecelesernm QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92291722 Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersvd1e, NC 28078 (704)875-9092 MATRIX SPIKE SAMPLE: 1697922 92291455001 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers 2-Fluorobiphenyl(S) % 79 15-120 2-Fluorophenol(S) % 38 10-120 Nitrobenzene-d5 (S) % 70 10-120 Phenol-d6 (S) e/ 31 10-120 Terphenyl-dl4 (S) % 66 11-131 SAMPLE DUPLICATE: 1697923 Parameter Units 92291455002 Result Dup Result 1,2,4-Trichlorobenzene ug/L NO NO 2,4,6-Tdchlorophenol ug/L NO NO 2,4-Dichlorophenol ug/L NO NO 2,4-Dimethylphenol ug/L NO NO 2,4-Dinitrophenol ug/L NO NO 24-Dinitrotoluene ug/L NO NO 2,6-Dinitrotoluene ug/L ND NO 2-Chloronaphthalene ug/L NO NO 2-Chlorophenol ug/L NO NO 2-Nilrophenol ug/L NO NO 3,3'-Dichlorobenzidine ug/L NO NO 4,6-Dinitro-2-methylphenol ug/L NO NO 4-Bromophenylphenyl ether ug/L NO NO 4-Chloro-3-methylphenol ug/L NO NO 4-Chlorophenylphenyl ether ug/L NO NO 4-Nitrophenol ug/L NO NO Acenaphthene ug/L NO NO Acenaphthylene ug/L NO NO Anthracene ug/L ND NO Benzo(a)anthracene ug/L ND NO Benzo(a)pyrene ug/L ND NO Benzo(b)fluoranthene ug/L ND NO Benzo(g,h,i)perylene uglL ND NO Benzo(k)Fluoranthene ug/L ND NO bis(2-Chloroethoxy)methane ug/L ND NO bis(2-Chloroethyl) ether ug/L ND NO bis(2-Chloroisopropyp ether ug/L ND ND bis(2-Ethylhexyl)phlhalate ug/L NO ND Butylbenzylphthalate ug/L NO NO Chrysene ug/L NO NO Di-n-butylphthalate ug/L NO NO Di-n-octylphthalale ug/L NO NO Dibenz(a,h)anthracene ug/L NO NO Diethyl phtha late ug/L NO NO Dimethylphthalate ug/L NO NO Fluoranlhene ug/L NO NO RPD Qualifiers Results presented on this page are In the units Indicated by the "Unit." column except vTere an alternate unit Is presented to the daht of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/08/2016 01:03 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 27 aceAnalyticale nwrvpecelaDa.am t QUALITY CONTROL DATA Project: 9TORMWATER Pace Project No.: 92291722 SAMPLE DUPLICATE: 1697923 Parameter Units 92291455002 Result Oup Result Fluorene ug/L NO NO Hexachloro-1,3-butadiene ug/L NO NO Hexachlorobenzene ug/L ND NO Hexachlorocyclopentadiene ug/L NO NO Hexachloroethane ug/L NO NO Indeno(1,2,3-cd)pyrene ug/L NO NO Isophorone ug/L NO NO N-Nitroso-di-n-propylamine ug/L ND NO N-Nitrosodimethylamine ug/L ND NO N-Nitrosodiphenylamine ug/L NO NO Naphthalene ug/L ND ND Nitrobenzene ug/L ND NO Penlachlorophenol ug/L ND NO Phenanthrene ug/L ND NO Phenol ug/L NO NO Pyrene ug/L NO NO 2,4,6-Tribromophenol(S) % 76 67 2-Fluorobiphenyl(S) % 83 83 2-Fluorophenol(S) % 43 42 Nitrobenzene-d5(S) % 84 81 Phenol-d6 (S) % 29 28 Terphenyl-dl4 (S) % 98 94 RPD Qualifiers 13 1 3 3 1 5 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlerevllle, NC 20078 (704)875-9092 Results presented on this page are In the units In dicatod by the "Unite" column except where an alternate unit le presonted to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 04/08/2016 01:03 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 27 aceAnalytical r awwpecslab.pcvn QUALITY CONTROL DATA Project: STORMWATER Pace Project No.: 92291722 QC Batch: WET/43889 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92291722001 METHOD BLANK: 1697482 Associated Lab Samples: 92291722001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 1697483 Parameter Units Total Suspended Solids mg/L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28070 (704)875.g092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 03/30/1611:48 Spike LCS LCS %Rec Conic. Result %Rec Limits Qualifiers 250 240 96 90-110 SAMPLE DUPLICATE: 1697484 92291655001 Cup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 48.0 48.7 1 SAMPLE DUPLICATE: 1697485 92291732008 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L NO NO Results presented on this page are In the units Indicated by the 'Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/08/2016 01:03 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 27 ace Analytical / wwwpacelebs.com t Project: STORMWATER Pace Project No.: 92291722 QC Batch: WET/43936 QC Batch Method: EPA 9040 Associated Lab Samples: 92291722001 SAMPLE DUPLICATE: 1699259 Parameter Units pH Std. Units SAMPLE DUPLICATE: 1699260 Parameter Units pH Sid. Units QUALITY CONTROL DATA Analysis Method, EPA 9040 Analysis Description: 9040 pH 9229151DO01 Dup Result Result RPD Qualifiers 7.8 7.8 0 H6 92291779002 Dup Result Result RPD Qualifiers 6.9 6.9 0 H6 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntereville, NO 28078 (704)875-9092 Results presented on this page are In the units Indicated bythe "Units" column axceptwhers an alternate unit Is presented Wine nght ofthe result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/06/2016 01:03 PM without the written consent of Pace Analytical Services, Inc.. Page 23 of 27 aceAnalytical e xwxpa[ekDs.MrD j QUALIFIERS Project: STORMWATER Pace Project No.: 92291722 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitatlon Limit. RL- Reporting Limit. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunterwile, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyle is a combined concentration. Consistent with EPAguidelines, unrounded data are displayed and have been used to calculate % recovery and RED values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) OUP- Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS C9 Common Laboratory Contaminant. H5 Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time. H6 Analysis initiated outside of the 15 minute EPA required holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 04/08/2016 01:03 PM without the written consent of Pace Analytical Services, Inc.. Page 24 of 27 aceAnalyticale � xwwperaleaa.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: STORMWATER Pace Project No.: 92291722 Pace Analytical Services, Inc. 9800 Klncey Ave. Suite 100 Huntersville, NC 26078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92291722001 OF-004 EPA 1664E GCSV/24558 92291722001 OF-004 EPA3510 0EXT/41796 EPA608 92291722001 OF-004 EPA 200.7 MPRP/21163 EPA 200.7 92291722001 OF-004 EPA245.1 MERP/9162 EPA245.1 92291722001 OF-004 EPA 625 OEXT/41675 EPA 625 92291722001 OF-004 EPA 624 MSV/36271 92291722001 OF-004 SM 2540D WET/43889 92291722001 OF-004 EPA9040 WET/43936 Date: 04/08/2016 01:03 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch GCSV124607 CP/19030 MERC/8809 MSSW12072 Page 25 of 27 Document Name: Document Revised: 18FEB2016 Sample Condition U on Recef t SCURI Page 1 of 2 i ceARr7j}y�ICc7i� Document No.: issuing Authority: _ /,. F-CHR•CS.003-rev.18 Pace Huntersvllle Qualit Office f II + [� Pave 2 of 2 for Internal Ilse DNLY ° Client Name: '`, C) L�� F l-t L� �` U-kCl.� WOW 92291722 Project k: Courier: ❑Fed Ex ❑UPS ❑USPS ❑Client 111111 WIN 111I II II1 ❑ Commercial (Pace ❑Other:_ 92291722 Custody Seal Present. ❑Yes No Seals Intact, []Yes ®No n ! L, T P Date/Initials Person Examining Contents: J 2 / (sue Packing Material: ❑Bubble Wrap [Bubble Bags []None ❑Other._ Thermometer: ® T1505 E_ Type of Ice:'1 ®Wet ❑Blue ❑None []samples on ice, cooling process has begun Correction Factor: 0.O'C Cooler Temp Corrected ('Cl: Biological Tissue Frozen? ❑Yes ONO []N/A Temp should be above freezing to 6-C USDA Regulated Soil (❑ N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Old samples originate from a foreign source (Internationally, —i.mi— wa.eaii and Puerto Muni? nYes nNo COMMENTS: Chaln of Custody Present? QYes ON. ❑N/n 1. Chain of Custodyfilled Out? OYcs (:)No ❑NIA 2. Chain of Custody Relinquished? ❑Yes ONO N/A 3. Sampler Name and/or Signature on COC? Myes ONO ❑N/A 4. Samples Arrived within Hold Time? ❑Yes ONO ❑N/A 5. Short Hold Time Analysis(02 hr.)? Dyes [gNo ❑N/A 6. Rush Turn Around Time Requested? Dyes ©No N/A 7. Sufficient Volume? QYes ON,_ E N/n S. Correct Containers Used? [Dyes ❑No ❑N/A 9. -Pace Containers Used? U_L, []No ❑N/A Containers Intact? RY YCs ONO ❑N/A 30. Filtered Volume Received for Dissolved Tests? Dyes []No ONIA 11, Note If sediment is visible In the dissolved container Sample Labels Match COC? [Yes ONO ❑N/A 12. i% -Includes 'Date/rme/ID/Anal sis Matrix: 1 LL f y All containers needing acid/base preservation have been 13, checked? [Yes ONO ❑N/A , All containers needing preservation are found to be in compliance with EPA recommendation? (HNOa, H:SOa, HCk2; Na0H>9 SulRde, NaOH>12 Cyanide) ®Yes ONO ❑N/A Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC LLHg 0Yes ONO ❑N/A Samples checked for dechlorination f]Yes ONO ❑N/A. 14, Headspace in VOA Vials >5-6mni)? Dyes ❑No DN/A 15. Trip Blank Present? Dyes [�No ❑N/A 16. Tilp Blank Custody Seals Present? Dyes [QNO ❑N/A Pace Trip Blank Lot II (if purchased): CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Resolution: Project Manager SCURF Review: Field Data Required? ❑Yes LJNO Date/Time: Date: Project Manager SRF Review: _L. it+• Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina OEHNP Certification Office (Le. Out of hold, Incorrect preservative, out of temp, Incorrect containers) Page 26 of 27 aaq ez CHAIN -OF -CUSTODY I Analytical Request Document The Chain-of-Cuslody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B .. _ Semi-annual Stormwater Discharge Monitoring Report ti for North Carolina Division of Water Quality General Permit No. NCG030000� Date submitted 3/5/16 CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME _Colfax/IMO Industries, Inc. PERSON COLLECTING SAMPLES Danny Hefner, Shield Engineering LABORATORY: _ Pace Analytical Services, Inc. Lab Cert. # 12 Comments on sample collection or analysis: Benchmark exceedance for Copper Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2016®� SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' February (month) DISCHARGING TO CLASS F]ORW ❑HQW ❑Trout ❑PNA RECEIVED ❑Zero -flow ❑Water Supply [_]SA ®Other —Class C — Dry Fork Creek MAR 0 7 Z016 CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 � n Nn rYkrhnrnP thi< nPr;nr02 Outfall No. Date Sample Collected r 24hour rainfall amount, Inches' Total Suspended Solids P H Standard units Copper Lead Zinc FNnPolar O&G/ Petroleum rocarbonsOrganics(mo/dd/yr) Total Toxic s Benchmarks ===> - - 100 mg/L or 50 mg/L 6.0-9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SDO 004 2/23/16 0.62 26.2 6.4 1 0.0111 <0.005 0.0600 1 <5.0 BDL Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. "See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 W - -, Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be'waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." ,JC(5Dn 11' L e r f Name (Print name) 61S 61cfe&--Or Title (Print title) (Si ure) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. Ej No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L• 6.0 — 9.0 sU Footnotes from Part A also apply to this Part B ' See General Permit text, Table 5, identifying the especially sentitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significantyenglties for submitting false information, including the possibility of fines and imprisonment for knowing violations." re of Permittee) Permit Date: 11/1/2012-10/31/2017 3 yl4 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 ®fin NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisform,please visit: bM•//portiincdelu•org/wgb/wci/vs/sutnpdes er,b Permit No.: N/C/C1/ el3/� Facility Name: tAlo } County: CNaioa Inspector: P/NvuY Date of Inspection: z e Time of Inspection: o 7- /lr� or Certificate of Coverage No.: N/E/_C/o/'3/ e/ Total Event Precipitation (inches): D, tp ?— Phone No. Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hoes prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that.th report is accurate and complete to the best of my knowledge: of Permittee or Page 1 of 2 SWU-242, Last modified 10/25/20 t2 1. Outfall Description: Outfall No. 00q Structure (pipe, ditch, etc.) "DI TU/ Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: _ L IG//Y 13Roh/N 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): _ ng o pyoP, _ 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 D 3 4 5 5. Floating Solids: Choose the number which best describes the amount of Floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 7 U 9. 1 (V 3 Is there any foam in the stormwater discharge? 4 5 Yes Is there an oil sheen in the stormwater discharge? Yes lU Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 Semi-annual Stormwater Discharge Monitoring Report v { for North Carolina Division of Water Quality General Permit No. NCG030000 yer A�� CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME Colfax/IMO Industries, Inc. PERSON COLLECTING SAMPLES LABORATORY: Date submitted 2/15/16 Lab Cert. p Comments on sample collection or analysis: Unable to collect sample during January due to rain events occurring at night making sampling conditions unsafe for technicians. Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR _2016 �® SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' January (month) DISCHARGING TO CLASS ❑ORW ❑HQW [-]Trout ,QPNA ❑Zero -flow ❑Water Supply ❑SA cr ®Other_Class C — Dry Fork Creek J FEB 16 2016 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTRAL FILES DWR SECTION ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids PH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Orgamcss Benchmarks ===> - - —Too mg/L or 50 mg/L 6.0 - 9.0 0.007 mg/L 1 0.03 mg/I 0.067 mg/L 15 mg/L 1 mg/L SDO 004 No qualifying event during normal business hours Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 ,.Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution �Pr vention f Ian." lkso>, �er'che,f Name (Print name) / i�fFs L fec fv r Title (Print title) (Sig ure) (Dat ) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664(SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 1S mg/L 100 mg/L or SO mg/L* 6.0 — 9.0 sU Footnotes from Part A also apply to this Part B Permit Date: 11/1/2012-30/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. %Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one cony of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period in the case of No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significapppenAes for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee) Permit Date: 11/1/2012-10/31/2017 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3