NCG030293_COMPLETE FILE - HISTORICAL_20160527

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STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
IV U& d 0
DOC TYPE
HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE
❑ (� L9 l b 0
YYYYM M D D

aceAnalytical
.pacelabs.cnm
May 27, 2016
Daniel Cox
Colfax Fluid Handling
1710 Airport Road
Monroe. NC 28110
RE: Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
Dear Daniel Cox:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
NCG-3 o a 9'3
Ma"db aI
Enclosed are the analytical results for sample(s) received by the laboratory on May 18, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
�„ C,.-- cc,,
Liamm Harrison
[e-mail]
Project Manager
Enclosures
cc: Melinda Greene
Accounts Payable, Colfax Fluid Handling
SQ.pGCRp�T
_` �o REPORT OF LABORATORY ANALYSIS
TNI This report shall not be reproduced, except in full,
9 �y without the written consent of Pace Analytical Services, Inc..
BOZO.
Page 1 of 36

Pace Analytical Services, Inc.
0
aceAnaiytical
9800Kincey Ave. Suite 100
rsville,
HunleNC 28078078
w Pacwabs.c%n
[phone]
CERTIFICATIONS
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification #: 37706
FloridalNELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
VirginiafVELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
FloridalNELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
VirginiaNELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 36

a'ceAnalytical
/ w ,pacalabs.cam
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Aye. Suite 100
Huntersylle, NC 28078
[phone]
Project:
Pace Project No.:
Colfax Fluid Handling 1150109-
92298198
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92298198001
OF-004
EPA 608
SWB
27
PASI-C
EPA 200.7
CDF
8
PASI-A
EPA 245.1
ANB
1
PASI-A
EPA625
RES
58
PASI-C
EPA624
GAW
34
PASI-C
SM 2540D
MSH
1
PASI-A
EPA 9040
TEP
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 36

Pace Analytical Services, Inc.
® 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville, NC 28078
w .pacelebs.cwn [phone]
ANALYTICAL RESULTS
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
Sample: OF-004 Lab ID: 92298198001 Collected: 05/17/16 16:20 Received: 05/18/16 13:43 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3510
Aldrin
NO
ug/L
0.050
1
05/19/16 11:01
05/19/16 21:43
309-00-2
alpha-BHC
NO
ug/L
0,050
1
05/19/16 11:01
05/19/16 21:43
319-84-6
beta-BHC
NO
ug/L
0.050
1
05/19116 11:01
05/19/16 21:43
319-85-7
delta-BHC
NO
ug/L
0.050
1
.05/19/16 11:01
05/19/1621:43
319-86-8
gamma-BHC (Lindane)
NO
ug/L
0,050
1
05/19/16 11:01
05/19/16 21:43
58-89-9
Chlordane( Technical)
NO
ug/L
0.50
1
05119/1611:01
05119/1621:43
57-74-9
4,4'-DDD
NO
ug/L
0.050
1
05/19/16 11:01
05/19/16 21:43
72-54-8
4,4'-DDE
NO
ug/L
0,050
1
05/19/16 11:01
05/19/16 21:43
72-55-9
4,4'-DDT
NO
ug/L
0.050
1
05/1911611:01
05119/1621:43
50-29-3
Dieldrin
NO
ug/L
0.050
1
05/19/16 11:01
05/19/16 21:43
60-57-1
EndosulfanI
NO
ug/L
0.050
1
0511911611:01
05/19/16 21:43
959-98-8
Endosulfan II
NO
ug/L
0,050
1
05/19/16 11:01
05/19/16 21:43
33213-65-9
Endosulfan sulfate
NO
ug/L
0.050
1
06/19/1611:01
05/19/16 21:43
1031-07-8
Endrin
NO
ug/L
0.050
1
05/1911611:01
05/19/16 21:43
72-20-8
Endrin aldehyde
NO
ug/L
0,050
1
05/19/16 11:01
05/19/16 21:43
7421-93-4
Heptachlor
NO
ug/L
0.050
1
05/19/16 11:01
05/19/16 21:43
76-44-8
Heptachlor epoxide
NO
ug/L
0.050
1
05/1911611:01
05119/1621:43
1024-57-3
PCB-1016 (Aroclor 1016)
NO
ug/L
0.50
1
05/19/16 11:01
05/19/16 21:43
12674-11-2
PCB-1221 (Aroclor 1221)
NO
ug/L
0.50
1
05/19/16 11:01
05/19/16 21:43
11104-28-2
PCB-1232 (Aroclor 1232)
NO
ug/L
0.50
1
05/19/16 11:01
05/19/16 21:43
11141-16-5
PCB-1242 (Aroclor 1242)
NO
ug/L
0.50
1
05/19/16 11:01
05/19/16 21:43
53469-21-9
PCB-1248 (Aroclor 1248)
NO
uglL
0.50
1
05/19/16 11:01
05/19/16 21:43
12672-2"
PCB-1254 (Aroclor 1254)
NO
ug/L
0.50
1
05/19/16 11:01
05/19/16 21:43
11097-69-1
PCB-1260 (Aroclor 1260)
NO
ug/L
0.50
1
05/19/16 11:01
05/19/16 21:43
11096-82-5
Toxaphene
NO
ug/L
0.50
1
05/1911611:01
05/19/1621:43
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
73
%
20-110
1
05/19/16 11:01
05/19/16 21:43
877-09-8
Decachlorobiphenyl (S)
46
%
20-138
1
05/19/16 11:01
05/19/16 21:43
2051-24-3
200.7 MET ICP
Analytical Method:
EPA 200.7
Preparation Method:
EPA
200.7
Arsenic
ND
ug/L
10.0
1
05/20/161045
05/23/1613:25
7440-38-2
Cadmium
NO
ug/L
1.0
1
05/20/161045
05/23/1613:25
7440-43-9
Chromium
NO
ug/L
5.0
1
05/20/16 10:45
05/23/1613:25
7440-47-3
Copper
8.2
ug/L
5.0
1
05/20/161045
05/23/1613:25
7440-50-8
Lead
NO
ug/L
5.0
1
05/20/16 10:45
05/23/161325
7439-92-1
Nickel
NO
ug/L
5.0
1
05/20/16 10:45
05/23/16 13:25
7440-02-0
Silver
NO
ug/L
5.0
1
05/20/16 10:45
05/23/161325
7440-22-4
Zinc
53.9
uglL
10.0
1
05/20/16 10:45
05/23/16 1325
7440-66-6
245.1 Mercury
Analytical Method:
EPA 245.1
Preparation Method:
EPA
245.1
Mercury
NO
ug/L
0.20
1
0511911614:00
0512311610:23
7439-97-6
625 MSSV
Analytical Method:
EPA 625 Preparation Method: EPA 625
Acenaphthene
NO
uglL
5.0
1
05/19/16 10:40
05/23/16 02:50
83-32-9
Acenaphthylene
NO
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
208-96-8
Anlhracene
NO
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
120-12-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 36

aceAnalytical e
v pacelabs.corn
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
Sample: OF-004
Lab ID: 92298198001
Collected: 05/17116
16:20
Received: 05/18/16 13:43 Matrix:
Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Benzo(a)anthracene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/1602:50
50-32-8
Benzo(b)Fluoranthene
ND
ug/L
5.0
1
05/1911610:40
05/2311602:50
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
05/1911610:40
05/23/16 02:50
191-24-2
Benzo(k)0uoranthene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
05/19/16 10:40
05/23/1602: 50
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
05/19/16 10:40
05/23/16 02:50
111-91-1
bis(2-Chloroelhyl) ether
ND
ug/L
5.0
1
05119/1610:40
05/23/1602:50
111-44-4
bis(2-Chloraisopropyl) ether
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
108-60-1
2-Chloronaphthalene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
0511911610:40
05/2311602:50
7005-72-3
Chrysene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
05/19/16 10:40
05/23/16 02:50
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
05/19/16 WAO
05/23/16 02:50
120-83-2
Diethylphthalate
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
05/19/16 10:40
05/23/16 02:50
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
05/19/16 WAO
05/23/16 02:50
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
1
05/19/16 10:40
05/23/16 02:50
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
05/19/16 10:40
05/23/16 02:50
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
117-81-7
Fluoranthene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
206-44-0
Fluorene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
118-74-1
Hexachlorocyclopenladiene
ND
ug/L
10.0
1
05/19/16 10:40
05/23/16 02:50
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
193-39-5
Isophorone
ND
ug/L
10.0
1
05/19/16 10:40
05/23/16 02:50
78-59-1
Naphthalene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
05/19/16 10:40
05/23/1602:50
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
05/19/16 10:40
05/23/16 02:50
100-02-7
N-Nitmsodimethylamine
ND
ug/L
5.0
1
05119/1610:40
05/2311602:50
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
05/1911610:40
05/23/1602:50
86-30-6
Pentachlorophenol
ND
ug/L
10.0
1
05/19/16 10:40
05/23/16 02:50
87-86-5
Phenanthrene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/1602:50
85-01-8
Phenol
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
Pyrene
ND
ug/L
5.0
1
05/19/16 10:40
05/23/16 02:50
129-00-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 36

ace Analytical
.Pacclabscom
ANALYTICAL RESULTS
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: OF-004 Lab ID: 92298198001 Collected: 05/17/16 16:20 Received: 05/18/16 13:43 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA625 Preparation Method: EPA 625
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
05/1911610:40
05/2311602:50
120-82-1
2,4,6-Trichlorophenol
NO
ug/L
10.0
1
05/1911610:40
05/2311602:50
88-06-2
Surrogates
Nitrobenzene-d5(S)
72
%
10-120
1
05/19/1610:40
05/23/1602:50
4165-60-0
2-Fluorobiphenyl(S)
70
%
15-120
1
05/19/1610:40
05/2311602:50
321-60-8
Terphenyl-d 14(S)
68
%
11-131
1
05/19/161040
05/23/1602:50
1718-51-0
Phenol-d6(S)
30
%
10-120
1
05/19/1610:40
05/23/1602:50
13127-88-3
2-Fluorophenol(S)
41
%
10-120
1
05/1911610:40
05/23/1602:50
367-12-4
2,4,6-Tribromophenol(S)
78
%
10-137
1
05/19/16 10:40
05/23/16 02:50
118-79-6
624 Volatile Organics
Analytical Method:
EPA 624
Benzene
ND
ug/L
2.0
1
05/1911619:54
71-43-2
Bromodichloromethane
NO
ug/L
2.0
1
05/1911619:54
75-27-4
Bromoform
ND
ug/L
2.0
1
05/19/16 19:54
75-25-2
Bromomethane
ND
ug/L
2.0
1
05/19/161954
74-83-9
Carbon tetrachloride
NO
ug/L
2.0
1
05/19/16 19:54
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
05/19/16 19:54
108-90-7
Chloroethane
ND
ug/L
2.0
1
05/19/16 19:54
75-00-3
Chloroform
ND
ug/L
2.0
1
05/19/16 19:54
67-66-3
Chloromethane
ND
ug/L
2.0
1
05/1911619:54
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
05119/1619:54
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
05/19/16 19:54
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
05/1911619:54
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
05/19/16 19:54
106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1
05/19/16 19:54
75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
1
05/19/16 19:54
107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1
05/19/16 19:54
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
1
05/19/16 19:54
156-59-2
bans-12-Dichloroethene
ND
ug/L
2.0
1
05/19/16 19:54
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
1
05/19/16 19:54
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2.0
1
05/19/16 19:54
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
2.0
1
05/19/16 19:54
10061-02-6
Ethylbenzene
ND
ug/L
2.0
1
05119/1619: 54
100-41-4
Methylene Chloride
ND
ug/L
2.0
1
05/19/16 19:54
75-09-2
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
05/19/16 1954
79-34-5
Tetrachloroethene
ND
ug/L
2.0
1
05/19/16 1954
127-18-4
Toluene
ND
ug/L
2.0
1
05/19/16 19:54
108-88-3
1,1,1-Trichloroethane
NO
ug/L
2.0
1
05/19/16 19:54
71-55-6
1,1,2-Trichloroethane
NO
ug/L
2.0
1
05/19/16 19:54
79-00-5
Trichloroethene
ND
ug/L
2.0
1
05119/1619:54
79-01-6
Trichlorofluoromethane
ND
ug/L
2.0
1
05/19/16 19:54
75-69-4
Vinyl chloride
ND
ug/L
2.0
1
05/19/16 19:54
75-01-4
Surrogates
4-BromoOuorobenzene (S)
117
%
70-130
1
05/19/16 19:54
460-00-4
Toluene-d8(S)
101
%
70-130
1
05/19/16 19:54
2037-26-5
1,2-Dichloroethane-d4(S)
102
%
70-130
1
05119/1619:54
17060-07-0
REPORT OF LABORATORY ANALYSIS
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Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 36

aceAnalytical.
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
Sample: OF-004 Lab ID: 92298198001 Collected: 05/17/16 16:20 Received: 05/18/16 13:43 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 12.2 mg/L 2.5 1 05/19/16 16:42
9040 pH Analytical Method: EPA 9040
pH 6.9 Std. Units 0.10 1 05/20/16 13:40 H6
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
OC Batch: MERP19453
Analysis Method: EPA
245.1
QC Batch Method: EPA 245.1
Analysis Description: 245.1 Mercury
Associated Lab Samples: 92298198001
METHOD BLANK: 1737673
Matrix: Water
Associated Lab Samples: 92298198001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Mercury ug/L
NO 0.20
05/23/1609:36
LABORATORY CONTROL SAMPLE: 1737674
'
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
%Rec Limits
Qualifiers
Mercury ug/L
2.5
2.6
102 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1737675
1737676
MS
MSD
92297989001
Spike
Spike MS
MSD MS
MSD
%Rec
Parameter Units Result
Conc.
Conc. Result
Result %Rec
%Rec
Limits
RPD Qual
Mercury ug/L ND
2.5
2.5 1.9
1.8 74
73
70-130
2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1737677
1737678
MS
MSD
92298007003
Spike
Spike MS
MSD MS
MSD
%Rec
Parameter Units Result
Conc.
Conc. Result
Result %Rec
%Rec
Limits
RPD Qual
Mercury ug/L NO
2.5
2.5 2.6
2S 103
100
70-130
3
Results presented on this page are in the units Indicated by the'UniW column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc..
Page 8 of 36

aceAnalytical
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QUALITY CONTROL DATA
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
OC Batch: MPRP/21765 Analysis Method: EPA 200.7
OC Balch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92298198001
METHOD BLANK: 1737587
Matrix:
Water
Associated Lab Samples: 92298198001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
ug/L
NO
10B
05/24/1613:48
Cadmium
ug/L
NO
1.0
05/2411613:48
Chromium
ug/L
NO
5.0
05/2411613:48
Copper
ug/L
NO
5.0
05/24/1613:48
Lead
uglL
NO
5.0
05/24/1613:48
Nickel
ug/L
NO
5.0
05/24/1613:48
Silver
ug/L
NO
5.0
05/24/1613:48
Zinc
ug/L
NO
10.0
05/24/1613:48
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL
SAMPLE: 1737588
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
e/ Rec
Limits
Qualifiers
Arsenic
ug/L
500
475
95
85-115
Cadmium
ug/L
500
482
96
85-115
Chromium
ug/L
500
472
94
85-115
Copper
ug/L
500
484
97
85-115
Lead
ug/L
500
479
96
85-115
Nickel
ug/L
500
480
96
85-115
Silver
ug/L
250
242
97
85-115
Zinc
ug/L
500
480
96
85-115
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE:
1737589
1737590
-
MS
MSD
92298198001
Spike
Spike
MS
MSD
MS MSD
%Rec
Parameter
Units
Result
Cone.
Conc.
Result
Result
% Rec p/ Rec
Limits
RPD Qual
Arsenic
ug/L
NO
500
500
478
473
95
94
70-130
1
Cadmium
ug/L
NO
500
500
482
473
96
95
70-130
2
Chromium
ug/L
NO
500
500
474
465
94
92
70-130
2
Copper
ug/L
8.2
500
500
494
482
97
95
70-130
2
Lead
ug/L
NO
500
500
476
473
95
95
70-130
1
Nickel
ug/L
NO
500
500
479
471
95
94
70-130
2
Silver
ug/L
NO
250
250
241
237
96
95
70-130
2
Zinc
ug/L
53.9
500
500
534
526
96
94
70-130
2
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Colfax Fluid Handling 1150109-
92298198
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE: 1737591
1737592
MS
MSD
92298213002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result
Conc.
Conc.
Result
Result
e/ Rec
e/ Rec
Limits
RPD Qual
Arsenic
ug/L ND
500
500
487
493
97
98
70-130
1
Cadmium
ug/L ND
500
500
485
491
97
98
70-130
1
Chromium
ug/L ND
500
500
477
483
95
96
70-130
1
Copper
ug/L ND
500
500
487
494
97
98
70-130
1
Lead
ug/L ND
500
500
486
495
97
99
70-130
2
Nickel
ug/L ND
500
500
485
491
97
98
70-130
1
Silver
ug/L ND
250
250
243
246
97
98
70-130
1
Zinc
ug/L ND
500
500
499
507
99
100
70-130
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 36

aceAnalytical
.pacefelu.com
QUALITY CONTROL DATA
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
OC Batch: MSV/36907 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92298198001
METHOD BLANK: 1737784
Associated Lab Samples: 92298198001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
2.0
05/19/16 17:35
1,1,2,2-Tetrachloroethane
ug/L
ND
2.0
05/19/16 17:35
1,1,2-Tdchloroethane
ug/L
NO
2.0
05/19/16 17:35
1,1-Dichloroethane
ug/L
ND
2.0
05/19/16 17:35
1,1-Dichloroethene
ug/L
ND
2.0
05/19/16 1735
1,2-Dichlorobenzene
ug/L
ND
2.0
05/19/16 17:35
1,2-Dichloroethane
ug/L
ND
2.0
05/19/16 17:35
1,2-Dichloropropane
ug/L
ND
2.0
05/19/161735
1,3-Dichlorobenzene
ug/L
ND
2.0
05/19/161735
1,4-Dichlorobenzene
ug/L
ND
2.0
0511911617:35
Benzene
ug/L
ND
2.0
0511911617:35
Bromodichloromelhane
ug/L
ND
2.0
05/19/16 17:35
Bromoform
ug/L
ND
2.0
05119/1617:35
Bromomethane
ug/L
ND
2.0
05/1911617:35
Carbon tetrachloride
ug/L
ND
2.0
05119/1617:35
Chlorobenzene
ug/L
ND
2.0
05/19/16 17:35
Chloroethane
ug/L
ND
2.0
05/19/16 17:35
Chloroform
ug/L
ND
2.0
05/191161735
Chloromelhane
ug/L
ND
2.0
05/19/16 17:35
cis-1,2-Dichloroethene
ug/L
ND
2.0
05/19/16 17:35
cis-1,3-Dichloropropene
ug/L
ND
2.0
05/19/16 17:35
Dibromochloromethane
ug/L
ND
2.0
05/19/16 17:35
Ethylbenzene
ug/L
ND
2.0
05/19/161735
Methylene Chloride
ug/L
ND
2.0
05/19/16 17:35
Tetrachloroelhene
ug/L
ND
2.0
65/19/16 17:35
Toluene
ug/L
ND
2.0
05/1911617:35
trans-1,2-Dichloroethene
ug/L
ND
2.0
05/19/16 17:35
trans-1,3-Dichloropropene
ug/L
ND
2.0
05/19/16 17:35
Trichlorcethene
ug/L
NO
2.0
05/1911617:35
TrichloroFluoromethane
ug/L
NO
2.0
05/1911617:35
Vinyl chloride
ug/L
NO
2.0
05/19/16 17:35
1,2-Dichloroethane-d4 (S)
%
102
70-130
05/19/16 17:35
4-Bromofluorobenzene (S)
p/
116
70-130
05/19/16 17:35
Toluene-d8 (S)
%
101
70-130
05/19/16 17:35
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1737785
Spike LCS 1-CS % Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1,1-Tdchloroethane ug/L 50 45.4 91 52-162
1,1,2,2-Tetrachloroethane ug/L 50 49.3 99 46-157
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 36

aceAnalytical
wwxpace/absrom
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
LABORATORY CONTROL SAMPLE:
1737785
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
%Rec
Limits
Qualifiers
1,1,2-Trichloroethane
ug/L
50
52.7
105
52-150
1,1-Dichloroethane
ug/L
50
42.3
85
59-155
1,1-Dichloroethene
ug/L
50
48.1
96
1-234
1,2-Dichlorobenzene
ug/L
50
49.4
99
18-190
1,2-Dichloroethane
ug/L
50
45A
90
49-155
1,2-Dichloropropane
ug/L
50
46.3
93
1-210
1,3-Dichlorobenzene
ug/L
50
51.8
104
59-156
1,4-Dichlorobenzene
ug/L
50
48.9
98
18-190
Benzene
ug/L
50
49.7
99
37-151
Bromodichloromethane
ug/L
50
51.6
103
35-155
Bromoform
ug/L
50
54.9
110
45-169
Bromomethane
ug/L
50
81.0
162
1-242
Carbon tetrachloride
ug/L
50
56.2
112
70-140
Chlorobenzene
ug/L
50
51.7
103
37-160
Chloroethane
ug/L
50
46.8
94
14-230
Chloroform
ug/L
50
46.5
93
51-138
Chloromethane
ug/L
50
45.3
91
1-273
cis-1,2-Dichloroethene
ug/L
50
44.7
89
68-146
cis-1,3-Dichloropropene
ug/L
50
51.6
103
1-227
Dibromochloromethane
ug/L
50
53.2
106
53-149
Ethylbenzene
ug/L
50
51A
102
37-162
Methylene Chloride
ug/L
50
38.0
76
1-221
Tetrachloroethene
ug/L
50
53.8
108
64-148
Toluene
ug/L
50
50.6
101
47-150
trans-1,2-Dichloroethene
ug/L
50
44.7
89
54-156
trans-1,3-Dichloropropene
ug/L
50
52.0
104
17-183
Trichlaroethene
ug/L
50
45.5
91
71-157
Trichlorofluoromethane
ug/L
50
45.7
91
17-181
Vinyl chloride
ug/L
50
44.6
89
1-251
1,2-Dichloroethane-d4(S)
%
104
70-130
4-Bromofluorobenzene (S)
p/
114
70-130
Toluene-d8(S)
%
100
70-130
MATRIX SPIKE SAMPLE:
1737787
92298198001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
%Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
NO
20
25.1
125
46-171
1,1,2,2-Tetrachloroethane
ug/L
ND
20
24.6
123
73-159
1,1,2-Trichloroethane
ug/L
ND
20
25.0
125
64-152
1,1-Dichloroethane
ug/L
ND
20
22.1
110
43-172
1,1-Dichloroethene
ug/L
ND
20
24.2
121
48-189
1,2-Dichlorobenzene
ug/L
NO
20
25.2
126
54-154
1,2-Dichloroethane
ug/L
NO
20
23.3
117
42-171
1,2-Dichloropropane
ug/L
ND
20
25.4
127
55-157
1,3-Dichlorobenzene
ug/L
NO
20
24.5
122
57-148
Results presented on this page are in the units indicated by the 'Units' column except where an alternate on It is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 12 of 36

ace Analytical
wwwpacelabs.mm
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
MATRIX SPIKE SAMPLE:
1737787
92298198001
Spike
MS
MS
% Red
Parameter
Units
Result
Conc.
Result
%Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
ND
20
25.5
128
58-149
Benzene
ug/L
ND
20
26.5
133
54-163
Bromodichloromethane
ug/L
ND
20
2T6
138
56-152
Bromoform
ug/L
ND
20
25.7
128
53-151
Bromomethane
ug/L
ND
20
34.4
172
10-200
Carbon tetrachloride
ug/L
ND
20
30.5
153
41-175
Chlorobenzene
ug/L
ND
20
27.1
135
67-152
Chloroelhane
ug/L
ND
20
26.7
133
23-200
Chloroform
ug/L
ND
20
24.0
120
51-166
Chloromethane
ug/L
ND
20
24.0
120
40-175
cis-1,2-Dichloroethene
ug/L
ND
20
24.5
122
45-174
cis-1,3-Dichloropropene
ug/L
ND
20
25.8
129
38-146
Dibromochloromethane
ug/L
ND
20
27.9
140
65-144
Ethylbenzene
ug/L
ND
20
27.2
136
57-152
Methylene Chloride
ug/L
ND
20
19.8
99
40-167
Tetrachloroethene
ug/L
ND
20
28.9
145
59-155
Toluene
ug/L
ND
20
26.0
130
47-162
trans-1,2-Dichloroethene
ug/L
ND
20
25.5
128
47-178
trans-1,3-Dichloropropene
ug/L
ND
20
24.4
122
39-148
Trichloroethene
ug/L
ND
20
24.4
122
60-153
Trichlorofluoromethane
ug/L
ND
20
25.6
128
42-199
Vinyl chloride
ug/L
ND
20
22A
112
46-176
1,2-Dichloroethane-d4(S)
%
97
70-130
4-Bromofluorobenzene (S)
%
118
70-130
Toluene-d8(S)
%
97
70-130
SAMPLE DUPLICATE: 1738320
92297973001
Cup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1-Trichloroethane
ug/L
<0.0020 mg/L
ND
1,1,2,2-Tetrachloroethane
ug/L
<0.0020 mg/L
ND
1,1,2-Trichloroethane
ug/L
<0.0020 mg/L
ND
1,1-Dichloroethane
ug/L
<0.0020 mg/L
ND
1,1-Dichloroethene
ug/L
<0.0020 mg/L
ND
1,2-Dichlorobenzene
ug/L
<0.0020 mg/L
ND
1,2-Dichloroethane
ug/L
<0.0020 mg/L
ND
1,2-Dichloropropane
ug/L
<0.0020 mg/L
ND
1,3-Dichlorobenzene
ug/L
<0.0020 mg/L
ND
1,4-Dichlorobenzene
ug/L
<0.0020 mg/L
ND
Benzene
ug/L
<0.0020 mg/L
NO
Bromodichloromethane
ug/L
<0.0020 mg/L
ND
Bromoform
uglL
<0.0020 mg/L
ND
Bromomethane
ug/L
<0.0020 mg/L
ND
Carbon tetrachloride
ug/L
<0.0020 mg/L
ND
Chlorobenzene
ug/L
<0.0020 mg/L
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 13 of 36

aceAnalytical
.pacotabscom
QUALITY CONTROL DATA
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
SAMPLE DUPLICATE: 1738320
Parameter
Units
92297973001
Result
Dup
Result
Chloroethane
ug/L
<0.0020 mglL
ND
Chloroform
ug/L
<0.0020 mg/L
ND
Chloromethane
ug/L
<0.0020 mg/L
ND
cis-1,2-Dichloroethene
ug/L
<0.0020 mg/L
ND
cis-1,3-Dichloropropene
ug/L
<0.0020 mglL
ND
Dibromochloromethane
ug/L
<0.0020 mg/L
ND
Ethylbenzene
ug/L
<0.0020 mg/L
ND
Methylene Chloride
ug/L
<0.0020 mg/L
ND
Tetrachlomethene
ug/L
<0.0020 mg/L
ND
Toluene
ug/L
<0.0020 mg/L
ND
trans-1,2-Dichloroethene
ug/L
<0.0020 mg/L
ND
trans-1,3-Dichloropropene
ug/L
<0.0020 mg/L
ND
Trichlomethene
ug/L
<0.0020 ri
ND
Trichlorofluoromethane
ug/L
<0.0020 mg/L
ND
Vinyl chloride
ug/L
<0.0020 mg/L
ND
1,2-Dichloroethane-d4 (S)
%
98
101
4-Bromofluorobenzene(S)
%
118
121
Toluene-d8 (S)
%
100
99
RPD Qualifiers
3
2
0
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units indicated by the -Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 14 of 36

aceAnalytical
wvmpscakbafcarn
QUALITY CONTROL DATA
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
QC Batch: OEXT/42659
OC Batch Method: EPA 3510
Associated Lab Samples: 92298198001
Analysis Method:
Analysis Description:
EPA 608
608 GCS Pest PCB
METHOD BLANK: 1737577
Matrix: Water
Associated Lab Samples: 92298198001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
4,4'-DDD
ug/L
NO
0.050
05/20/1600:06
4,4'-DDE
ug/L
NO
0.050
05/20/1600:06
4,4'-DDT
ug/L
NO
0.050
05/20/1600:06
Aldrin
ug/L
NO
0.050
05/20/1600:06
alpha-BHC
ug/L
NO
0.050
05/20/1600:06
beta-BHC
ug/L
NO
0.050
05/20/1600:06
Chlordane (Technical)
ug/L
NO
0.50
05/2011600:06
delta-BHC
ug/L
NO
0.050
05/2011600:06
Dieldrin
ug/L
NO
0.050
05/2011600:06
EndosulfanI
ug/L
NO
0.050
05/2011600:06
Endosulfan ll
ug/L
ND
0.050
05/2011600:06
Endosulfan sulfate
ug/L
NO
0.050
05/20/16 00:06
Endrin
ug/L
NO
0.050
05/20/16 00:06
Endrin aldehyde
ug/L
NO
0.050
05/20/16 00:06
gamma-BHC (Lindane)
ug/L
NO
0,050
05/20/16 00:06
Heptachlor
ug/L
NO
0.050
05/20/16 00:06
Heptachlor epoxide
ug/L
NO
0,050
05/20/16 00:06
PCB-1016 (Aroclor 1016)
ug/L
NO
0.50
05/20/16 00:06
PCB-1221 (Aroclor 1221)
ug/L
NO
0.50
05/20/16 00:06
PCB-1232 (Aroclor 1232)
ug/L
NO
0.50
05/20/16 00:06
PCB-1242 (Aroclor 1242)
ug/L
NO
0.50
05/20/16 00:06
PCB-1248 (Aroclor 1248)
ug/L
NO
0.50
05/20/16 00:06
PCB-1254 (Aroclor 1254)
ug/L
NO
0.50
05/20/16 00:06
PCB-1260 (Aroclor 1260)
ug/L
NO
0.50
05/20/16 00:06
Toxaphene
ug/L
NO
0.50
05/20/16 00:06
Decachlorobiphenyl (S)
e/
57
20-138
05/20/16 00:06
Tetrachloro-m-xylene (S)
%
fib
20-110
05/20/16 00:06
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1737578
Spike
LCS
LCS
%Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
ug/L
.25
0.25
100
31-141
4,4'-DDE
ug/L
.25
0.23
91
30-145
4,4'-DDT
ug/L
.25
0.25
101
25-160
Aldrin
ug/L
.25
0.19
76
42-122
alpha-BHC
ug/L
.25
0,21
84
37-134
beta-BHC
ug/L
.25
0,24
99
17-147
delta-BHC
ug/L
.25
0.25
100
19-140
Dieldrin
ug/L
.25
0.23
92
36-146
Endosulfan I
ug/L
.25
0.24
95
45-153
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 36

aceAnalytical
xwwpacefabs.com
QUALITY CONTROL DATA
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
LABORATORY CONTROL SAMPLE:
1737578
Spike
LCS
LCS
% Red
Parameter
Units
Conc.
Result
p/ Red
Limits
Endosulfan II
ug/L
.25
0.26
105
1-202
Endosulfan sulfate
ug/L
.25
0.27
110
26-144
Endrin
ug/L
.25
0,24
96
30-147
Endrin aldehyde
ug/L
.25
0.25
100
50-150
gamma-BHC (Lindane)
ug/L
.25
0.22
88
32-127
Heptachlor
ug/L
.25
0.21
83
34-111
Heptachlor epoxide
ug/L
.25
0.23
92
41-126
Decachlorobiphenyl(S)
%
54
20-138
Tetrachloro-m-xylene (S)
%
80
20-110
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE SAMPLE:
Parameter
1737579
Units
92298007002
Result
Spike
Conc.
MS
Result
MS
%Rec
% Red
Limits Qualifiers
4,4'-DDD
ug/L
NO
.25
0.21
85
31-141
4,4'-DDE
ug/L
NO
.25
0.20
80
30-145
4,4'-DDT
ug/L
ND
.25
0.21
85
25-160
Aldrin
uglL
NO
.25
0.18
74
42-122
alpha-BHC
ug/L
ND
.25
0.21
86
37-134
beta-BHC
ug/L
ND
.25
0.21
86
17-147
delta-BHC
ug/L
ND
.25
0.23
91
19-140
Dieldrin
ug/L
ND
.25
0.20
81
36-146
Endosulfan I
ug/L
ND
.25
0.22
87
45-153
Endosulfan II
ug/L
ND
.25
0.22
89
1-202
Endosulfan sulfate
ug/L
ND
.25
0.23
92
26-144
Endrin
ug/L
ND
.25
0.20
81
30-147
Endrin aldehyde
ug/L
ND
.25
0.21
84
50-150
gamma-BHC (Lindane)
ug/L
ND
.25
0.22
87
32-127
Heptachlor
ug/L
ND
.25
0.20
79
34-111
Heptachlor epoxide
ug/L
ND
.25
0.21
85
41-126
Decachlorobiphenyl (S)
%
56
20-138
Tetrachloro-m-xylene (S)
p/
79
20-110
SAMPLE DUPLICATE: 1737580
92298011002
Dup
Parameter
Units
Result
Result RPD Qualifiers
4,4'-DDD
ug/L
ND
NO
4,4'-DDE
ug/L
NO
ND
4,4'-DDT
ug/L
NO
NO
Aldrin
ug/L
NO
NO
alpha-BHC
ug/L
NO
NO
beta-8HC
ug/L
ND
NO
Chlordane (Technical)
ug/L
ND
NO
delta-BHC
ug/L
ND
NO
Dieldrin
ug/L
ND
ND
Results presented on
this page are in the units
indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc..
Page 16 of 36

aceAnalytical
a pace/el oxen
QUALITY CONTROL DATA
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
SAMPLE DUPLICATE: 1737580
Parameter
Units
92298011002
Result
Dup
Result
Endosulfan I
ug/L
ND
ND
Endosulfan II
ug/L
ND
ND
Endosulfan sulfate
uglL
ND
ND
Endrin
ug/L
ND
ND
Endrin aldehyde
ug/L
ND
ND
gamma-BHC (Lindane)
ug/L
ND
ND
Heptachlor
ug/L
ND
ND
Heptachlor epoxide
ug/L
ND
ND
PCB-1016 (Aroclor 1016)
ug/L
ND
ND
PCB-1 221 (Aroclor 1221)
ug/L
IND
ND
PCB-1232 (Aroclor 1232)
ug/L
ND
ND
PCB-1242 (Aroclor 1242)
ug/L
ND
ND
PCB-1248 (Aroclor 1248)
ug/L
ND
ND
PCB-1254 (Aroclor 1254)
ug/L
ND
ND
PCB-1260 (Aroclor 1260)
ug/L
ND
ND
Toxaphene
ug/L
ND
ND
RPD Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of 36

aceAnalytical
~pacelabs.mrn
QUALITY CONTROL DATA
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
QC Batch: OEXT142658 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 92298198001
METHOD BLANK: 1737546
Associated Lab Samples: 92298198001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
NO
5.0
05/22/16 21:00
2,4,6-Tdchlorophenol
ug/L
ND
10.0
05/22/16 21:00
2,4-Dichlorophenol
ug/L
ND
5.0
05/22/16 21:00
2,4-Dimethylphenol
ug/L
ND
10.0
05/22/16 21:00
2,4-Dinitrophenol
ug/L
ND
50.0
05/22/16 21:00
2,4-Dinitrotoluene
ug/L
NO
5.0
05/22/16 21:00
2,6-Dinitrotoluene
ug/L
NO
5.0
05/22/16 21:00
2-Chloronaphthalene
ug/L
NO
5.0
05/22/1621:00
2-Chlorophenol
ug/L
NO
5.0
05/22/16 21:00
2-Nitrophenol
ug/L
NO
5.0
05/2211621:00
3,3'-Dichlorobenzidine
ug/L
NO
25.0
05/22/16 21:00
4,6-Dinitro-2-methylphenol
ug/L
NO
20.0
05/22/1621,00
4-Bromophenylphenyl ether
ug/L
NO
5.0
05/22/16 21:00
4-Chloro-3-methylphenol
ug/L
NO
5.0
05/22/1621:00
4-Chlorophenylphenyl ether
ug/L
NO
5.0
05/22/1621:00
4-Nitrophenol
ug/L
NO
50.0
05/22/16 21:00
Acenaphthene
ug/L
NO
5.0
05/22/1621:00
Acenaphthylene
ug/L
NO
5.0
05/22/1621:00
Anthracene
ug/L
NO
5.0
05/22/16 21:00
Benzo(a)anthracene
ug/L
NO
5.0
05/22/16 21:00
Benzo(a)pyrene
ug/L
NO
5.0
05/22/16 21:00
Benzo(b)fluoranthene
ug/L
NO
SO
05/22/16 21:00
Benzo(g,h,i)perylene
ug/L
NO
5.0
05/22/1621:00
Benzo(k)fluoranthene
ug/L
ND
5.0
05/22/16 21:00
bis(2-Chloroethoxy)methane
ug/L
NO
10.0
05/22/16 21:00
bis(2-Chloroethyl) ether
ug/L
NO
5.0
05/22/16 21:00
bis(2-Chloroisopropyl) ether
ug/L
NO
5.0
05/22/16 21:00
bis(2-Ethylhexyl)phthalate
ug/L
NO
5.0
05/22/16 21:00
Butylbenzylphthalate
ug/L
NO
5.0
05/22/16 21:00
Chrysene
ug/L
NO
5.0
05/22/16 21:00
Di-n-bulylphthalate
ug/L
NO
5.0
05/22/1621:00
Di-n-octylphthalate
ug/L
NO
5.0
05/22/1621:00
Dibenz(a,h)anthracene
ug/L
NO
5.0
05/22/16 21:00
Diethylphthalate
ug/L
NO
5.0
05/22/16 21:00
Dimethylphthalale
ug/L
NO
5.0
05/22/16 21:00
Fluoranthene
ug/L
NO
5.0
05/22/16 21:00
Fluorene
ug/L
NO
5.0
05/22/16 21:00
Hexachloro-1,3-butadiene
ug/L
NO
5.0
05/22/16 21:00
Hexachlorobenzene
ug/L
NO
5.0
05/22/16 21:00
Hexachlorocyclopentadiene
ug/L
NO
10.0
05/22/1621:00
Hexachloroethane
ug/L
NO
5.0
05/22/1621:00
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2016 08,13 AM without the written consent of Pace Analytical Services, Inc.. Page 18 of 36

aceAnalytical
..pacelabs.com
QUALITY CONTROL DATA
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
METHOD BLANK: 1737546
Associated Lab Samples: 92298198001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Indeno(1,2,3-cd)pyrene
ug/L
NO
5.0
05/22/16 21:00
Isophorone
ug/L
NO
10.0
05/22/16 21:00
N-Nitroso-di-n-propylamine
ug/L
NO
5.0
05/22/16 21:00
N-Nitrosodimethylamine
ug/L
ND
5.0
05/22/16 21:00
N-Nitrosodiphenylamine
ug/L
ND
10.0
05/22/16 21:00
Naphthalene
ug/L
NO
5.0
05/22/16 21:00
Nitrobenzene
ug/L
ND
5.0
05/22/1621:00
Pentachlorophenol
ug/L
ND
10.0
05/22/1621:00
Phenanthrene
ug/L
ND
5.0
05/22/16 21:00
Phenol
ug/L
ND
5.0
05/22/16 21:00
Pyrene
ug/L
ND
5.0
05122/1621:00
2,4,6-Tdbromophenol(S)
%
72
10-137
05/2211621:00
2-Fluorobiphenyl(S)
%
69
15-120
05/2211621:00
2-Fluorophenol(S)
%
38
10-120
05/22/16 21:00
Nitrobenzene-d5 (S)
%
73
10-120
05/22/16 21:00
Phenol-d6 (S)
p/
27
10-120
05/22/16 21:00
Terphenyl-d 14(S)
%
74
11-131
05/22/16 21:00
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1737547
Units
Spike
Conc.
1-CS
Result
1-CS
e/ Rec
p/ Rec
Limits
1,2,4-Tdchlorobenzene
ug/L
50
34.8
70
44-142
2,4,6-Trichlorophenol
ug/L
50
47.3
95
37-144
2,4-Dichlorophenol
ug/L
50
42.4
85
1-191
2,4-Dimethylphenol
ug/L
50
42.2
84
32-119
2,4-Dinitrophenol
ug/L
250
185
74
1-181
2,4-Dinitrololuene
ug/L
50
48.1
96
39-139
2,6-Dinitrotoluene
ug/L
50
48.1
96
50-158
2-Chloronaphthalene
ug/L
50
38.9
78
60-118
2-Chlorophenol
ug/L
50
38.9
78
23-134
2-Nitrophenol
ug/L
50
45.8
92
29-182
3,3'-Dichlorobenzidine
ug/L
100
86.8
87
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
99.9
100
1-181
4-Bromophenylphenyl ether
ug/L
50
40.2
80
53-127
4-Chloro-3-methylphenol
ug/L
100
85.2
85
22-147
4-Chlorophenylphenyl ether
ug/L
50
43.6
87
25-158
4-Nitrophenol
ug/L
250
89.4
36
1-132
Acenaphthene
ug/L
50
39.6
79
47-145
Acenaphthylene
ug/L
50
40.7
81
33-145
Anthracene
ug/L
50
37.7
75
1-166
Benzo(a)anthracene
ug/L
50
41.4
83
33-143
Benzo(a)pyrene
ug/L
50
45.3
91
17-163
Benzo(b)Fluoranthene
ug/L
50
43.5
87
24-159
Benzo(g,h,i)perylene
ug/L
50
46.8
94
1-219
Pace Analytical Services, Inc.
9800 Kincery Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units- column except vmere an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 19 of 36

aceAnalytical
.pacelabs.com
QUALITY CONTROL DATA
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
LABORATORY CONTROL SAMPLE:
Parameter
1737547
Units
Spike
Conc.
LCS
Result
LCS
%Rec
%Rec
Limits
Benzo(k)fiuoranthene
ug/L
50
45.1
90
11-162
bis(2-Chloroethoxy)methane
ug/L
50
41.8
84
33-184
bis(2-Chloroethyl) ether
ug/L
50
41.9
84
12-158
bis(2-Chloroisopropyl) ether
ug/L
50
39.5
79
36-166
bis(2-Elhylhexyl)phthalate
ug/L
50
47.5
95
8-158
Butylbenzylphthalate
ug/L
50
58.6
117
1-152
Chrysene
ug/L
50
40.6
81
17-168
Di-n-butylphthalate
ug1L
50
46.3
93
1-118
Di-n-octylphthalate
ug/L
50
50.4
101
4-146
Dibenz(a,h)anthracene
ug/L
50
4Z0
94
1-227
Diethylphthalate
uglL
50
46.4
93
1-114
Dimethylphthalale
ug/L
50
45.6
91
1-112
Fluoranthene
ug/L
50
36.7
73
26-137
Fluorene
ug/L
50
42.6
85
59-121
Hexachloro-1,3-butadiene
ug/L
50
32.3
65
24-116
Hexachlorobenzene
ug/L
50
39.7
79
1-152
Hexachlorocyclopentadiene
ug/L
50
40.8
82
25-150
Hexachloroelhane
ug/L
50
30.5
61
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
47.8
96
1-171
Isophorone
ug/L
50
41.2
82
21-196
N-Nitroso-di-n-propylamine
ug/L
50
41.9
84
1-230
N-Nitrosodimelhylamine
ug/L
50
21.1
42
25-150
N-Nitrosodiphenylamine
ug/L
50
37.1
74
25-150
Naphthalene
ug/L
50
34.7
69
21-133
Nitrobenzene
ug/L
50
40.2
80
35-180
Pentachlorophenol
ug/L
100
90.1
90
14-176
Phenanthrene
ug/L
50
38.3
77
54-120
Phenol
ug/L
50
16.6
33
5-112
Pyrene
ug/L
50
38.5
77
52-115
2,4,6-Tnbromophenol (S) -
%
93
10-137
2-Fluorobiphenyl(S)
%
84
15-120
2-Fluorophenol(S)
%
47
10-120
Nitrobenzene-d5 (S)
°%
86
10-120
Phenol-d6 (S)
e/
33
10-120
Terphenyl-014 (S)
%
84
11-131
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunters,ille, NC 28078
[phone]
Qualifiers
MATRIX SPIKE SAMPLE:
1737548
92298007001
Spike
MS
MS
e/ Rec
Parameter
Units
Result
Conc.
Result
%Rec
Limits Qualifiers
1,2,4-Tdchlorobenzene
ug/L
ND
50
34.6
69
44-142
2,4,6-Tdchlorophenol
ug/L
NO
50
44.2
88
37-144
2,4-Dichlorophenol
ug/L
ND
50
40.4
81
1-191
2,4-Dimethylphenol
ug/L
NO
50
37.9
76
32-119
2,4-Dinitrophenol
ug/L
NO
250
183
73
1-181
2,4-Dinitrololuene
ug/L
ND
50
43.8
88
39-139
Results presented on this page are in the units Indicated by the'UmW column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 20 of 36

aceAnalytical
mnypscetabs.mm
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hmmers0le, NC 28078
[phone]
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
MATRIX SPIKE SAMPLE:
1737548
92298007001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2,6-Dinitrotoluene
ug/L
ND
50
43.8
88
50-158
2-Chlomnaphthalene
ug/L
ND
50
36.1
72
60-118
2-Chlorophenol
ug/L
ND
50
36.0
72
23-134
2-Nitrophenol
ug/L
ND
50
46.0
92
29-182
3,3'-Dichlorobenzidine
ug/L
ND
100
79.0
79
1-262
4,6-Dinitro-2-methylphenol
ug/L
ND
100
98.6
99
1-181
4-Bromophenylphenyl ether
ug/L
ND
50
37.8
76
53-127
4-Chloro-3-methylphenol
ug/L
ND
100
82Y
83
22-147
.4-Chlorophenylphenyl ether
ug/L
ND
50
40A
80
25-158
4-Nitrophenol
ug/L
ND
250
82.9
33
1-132
Acenaphthene
ug/L
ND
50
36.3
73
47-145
Acenaphthylene
ug/L
ND
50
36.9
74
33-145
Anthracene
ug/L
ND
50
34.2
68
1-166
Benzo(a)anthracene
ug/L
ND
50
38.7
77
33-143
Benzo(a)pyrene
ug/L
ND
50
40.9
82
17-163
Benzo(b)Fluoranthene
ug/L
ND
50
40.4
81
24-159
Benzo(g,h,i)perylene
ug/L
ND
50
41.6
83
1-219
Benzo(k)fiuoranlhene
ug/L
ND
50
40.1
80
11-162
bis(2-Chloroethoxy)melhane
ug/L
ND
50
38.9
78
33-184
bis(2-Chloroethyl) ether
ug/L
ND
50
39.2
78
12-158
bis(2-Chloroisopropyl) ether
ug/L
ND
50
37.0
74
36-166
bis(2-Ethylhexyl)phthalate
ug/L
ND
50
46.1
92
8-158
Butylbenzylphthalate
ug/L
ND
50
56.6
113
1-152
Chrysene
ug/L
ND
50
37.9
76
17-168
Di-n-butylphlhalate
ug/L
ND
50
43.2
86
1-118
Di-n-octylphthalate
ug/L
ND
50
51.5
103
4-146
Dibenz(a,h)anthmcene
ug/L
ND
50
44.6
89
1-227
Diethylphthalate
ug/L
ND
50
41.6
83
1-114
Dimethylphthalate
ug/L
ND
50
41.4
83
1-112
Fluoranlhene -
ug/L
ND
50
34.5
69
26-137
Fluorene
ug/L
ND
50
38.5
77
59-121
Hexachloro-1,3-butadiene
ug/L
ND
50
32.2
64
24-116
Hexachlorobenzene
ug/L
ND
50
36A
73
1-152
Hexachlorocyclopentadiene
ug/L
ND
50
41.9
84
25-150
Hexachloroethane
ug/L
ND
50
30.5
61
40-113
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
43.7
87
1-171
Isophorone
ug/L
ND
50
39.4
79
21-196
N-Nitroso-di-n-propylamine
ug/L
ND
50
41.4
83
1-230
N-Nitmsodimethylamine
ug/L
ND
50
20.3
41
25-150
N-Nitrosodiphenylamine
ug/L
ND
50
25.4
51
25-150
Naphthalene
ug/L
ND
50
33.5
67
21-133
Nitrobenzene
ug/L
ND
50
37.9
76
35-180
Pentachlorophenol
ug/L
ND
100
83.0
83
14-176
Phenanthrene
ug/L
ND
50
34.9
70
54-120
Phenol
ug/L
ND
50
16.5
33
5-112
Pyrene
ug/L
ND
50
34.9
70
52-115
2,4,6-Tribromophenol (S)
p/
86
10-137
Results presenter! on
this page are in the units indicated
by the'Units- column
except where
an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 05/27/2016 08A3 AM without the written consent of Pace Analytical Services, Inc.. Page 21 of 36

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QUALITY CONTROL DATA
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
1737548
92298007001 Spike MS MS
%Rec
Parameter
Units
Result Cone. Result % Rec
Limits Qualifiers
2-Fluorobiphenyl (S)
%
76
15-120
2-Fluorophenol (S)
%
42
10-120
Nitrobenzene-d5 (S)
%
81
10-120
Phenol-d6 (S)
%
32
10-120
Terphenyl-d14 (S)
%
71
11-131
SAMPLE DUPLICATE: 1737549
Parameter
Units
92298011001
Result
Dup
Result
1,2,4-Tdchlorobenzene
ug/L
ND
ND
2,4,6-Tdchlorophenol
ug/L
ND
ND
2,4-Dichlorophenol
ug/L
ND
ND
2,4-Dimethylphenol
ug/L
ND
ND
2,4-Dinitrophenol
ug/L
ND
ND
2,4-Dinitrotoluene
ug/L
ND
ND
2,6-Dinitrotoluene
ug/L
ND
ND
2-Chloronaphthalene
ug/L
ND
ND
2-Chlorophenol
ug/L
ND
ND
2-Nitrophenol
ug/L
ND
ND
3,3'-Dichlorobenzidine
ug/L
ND
ND
4,6-Dinitro-2-methylphenol
ug/L
ND
ND
4-Bromophenylphenyl ether
ug/L
ND
ND
4-Chloro-3-methylphenol
ug/L
ND
ND
4-Chlorophenylphenyl ether
ug/L
ND
ND
4-Nitrophenol
ug/L
ND
ND
Acenaphthene
ug/L
ND
ND
Acenaphthylene
ug/L
ND
ND
Anthracene
ug/L
ND
ND
Benzo(a)anthracene
ug/L
ND
ND
Benzo(a)pyrene
ug/L
ND
ND
Benzo(b)fluoranthene
ug/L
ND
ND
Benzo(g,h,i)perylene
ug/L
ND
ND
Benzo(k)fluoranthene
ug/L
ND
ND
bis(2-Chloroethoxy)methane
ug/L
ND
ND
bis(2-Chloroethyl) ether
ug/L
ND
ND
bis(2-Chloroisopropyl) ether
ug/L
ND
ND
bis(2-Ethylhexyl)phthalate
ug/L
ND
ND
Butytbenzylphthalate
ug/L
ND
ND
Chrysene
ug/L
ND
ND
Di-n-butylphthalate
ug/L
ND
ND
Di-n-octylphthalate
ug/L
ND
ND
Dibenz(a,h)anthracene
ug/L
ND
ND
Diethylphthalate
ug/L
ND
ND
Dimethylphthalate
ug/L
ND
ND
Fluoranthene
ug/L
ND
ND
RPD Qualifiers
Results presentee on this page are in the units indicated by the "Unix' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 22 of 36

aceAnalytical
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QUALITY CONTROL DATA
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
SAMPLE DUPLICATE: 1737549
Parameter
Units
92298011001
Result
Dup
Result
Fluorene
ug/L
ND
ND
Hexachlom-1,3-butadiene
ug/L
ND
ND
Hexachlorobenzene
ug/L
ND
ND
Hexachlorocyclopentadiene
ug/L
ND
ND
Hexachloroethane
ug/L
ND
ND
Indeno(1,2,3-cd)pyrene
ug/L
ND
ND
Isophorone
ug/L
ND
ND
N-Nitmso-di-n-propylamine
ug/L
ND
ND
N-Nitrosodimethylamine
ug/L
ND
ND
N-Nitrosodiphenylamine
ug/L
ND
ND
Naphthalene
ug/L
ND
ND
Nitrobenzene
ug/L
ND
ND
Pentachlorophenol
ug/L
ND
ND
Phenanthrene
ug/L
ND
ND
Phenol
ug/L
ND
ND
Pyrene
ug/L
ND
ND
2,4,6-Tdbromophenol (S)
%
63
67
2-Fluorobiphenyl (S)
%
33
55
2-Fluorophenol(S)
e/
18
28
Nitrobenzene-d5 (S)
%
34
59
Phenol-d6 (S)
%
12
20
Terphenyl-d14 (S)
%
53
43
RPD Qualifiers
7
50
44
54
47
20
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Himtersville, NC 28078
[phone]
Results presented on this page are In the units indicated by the' Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2016 08:13 AM without the written consent cf Pace Analytical Services, Inc.. Page 23 of 36

aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
HuntersWle, NC 28078
[phone]
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
QC Batch: WET/45049
Analysis Method:
SM 2540D
QC Balch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92298198001
METHOD BLANK: 1738052
Matrix:
Water
Associated Lab Samples: 92298198001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
NO
2.5 05/19/16 16:40
LABORATORY CONTROL SAMPLE: 1738053
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250
254
102 90-110
SAMPLE DUPLICATE: 1738054
92298186001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
281
303 8 D6
SAMPLE DUPLICATE: 1738055
92298207003
Cup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
ND
NO
Results presented on this page are in the units Indicated by the "Units" column exceptwhere an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 24 of 36

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QUALITY CONTROL DATA
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
QC Batch: WET/45044 Analysis Method: EPA 9040
QC Balch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92298198001
SAMPLE DUPLICATE: 1737834
92297956001 Cup
Parameter Units Result Result RPD Qualifiers
pH Sid. Units 7.1 7.1 0 H6
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presentee on this page are in the units indicated by the 'Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc..
Page 25 of 36

aceAnalytical
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QUALIFIERS
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyze is
a combined concentration.
Consistent with EPA guidelines, unbounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproducer, except in full, '
Date: 05/27/2016 08:13 AM without the written consent of Pace Analytical Services, Inc.. Page 26 of 36

aceAnalytical e
m Pacalabs.mm
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Colfax Fluid Handling 1150109-
Pace Project No.: 92298198
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
OC Batch Method
CC Batch
Analytical Method
Batch
92298198001
OF-004
EPA 3510
0EXT/42659
EPA608
GCSV/25039
92298198001
OF-004
EPA 200.7
MPRP/21765
EPA 200.7
ICP/19527
92298198001
OF-004
EPA 245.1
MERP/9453
EPA 245.1
MERC/9089
92298198001
OF-004
EPA 625
OEXT142658
EPA625
MSSV/12280
92298198001
OF-004
EPA 624
MSV/36907
92298198001
OF-004
SM 2540D
WET/45049
92298198001
OF-004
EPA 9040
WET/45044
Date: 05/27/2016 08:13 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 27 of 36

Document Name: Document Revised: 18FE82016
Condition Upon Receipt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F-ruR-rg-m3-rev.1R Pace Huntersvllle Quality Office
Client Name:
W®#:92298198 "
• • •
Skeld
t
II�II
Courier:
❑F Ex OUP'❑LISPS
❑ClIenient
�I�II��IIII��IIII
❑ Commercial
ace ❑Other:_
92298198
Custody Seal Present?
Oyes No Seals Intact? ❑Yes
ONO
Date/Initials Person Examining Contents:
Packing Material:
Thermometer:
[-]Bubble Wrap Bubble Bags ❑None
Fa, 1505 oWet
❑Other:_
❑Blue
[]None 05annples on Ice, cooling process has begun
Correction Factor: 0.0•C
❑ Type of Ice:
Cooler Temp Corrected (°C): 0. 9
Biological
r
Tissue Frozen? Oyes ONO ,./A
IQ
Temp should be above ft5lxing to 6'C
USDA Regulated Soil ( Z
N/A, water sample)
Did samples nate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
�5141io
Did samples originate from a foreign source (inter5akro nally,
A.Alne No,„aii and Puerto R m17 f1Ye5 PfNo
COMMENTS:
Chain of Custody Present?
Yes
❑No
❑N/A
1.
Chain of Custody Filled Out?
es
[IN.
❑N/A
2.
Chain of Custody Relinquished?
es
ON.
❑N/A
3.
Sampler Name and/or Signature on COC?
es
❑No
❑N/A
4.
Samples Arrived within Hold Time?
es
[IN.-
❑N/A
5.
Short Hold Time Analysis (02 hr.)?
[]Yes
GIC.,
❑N/A
6.
Rush Turn Around Time Requested?
❑Yes
a
❑IJ/A
7.
Sufficient Volume?
Yes
[-]No
❑N/A
8.
Correct Containers Used?
2TYes
[]NO
❑N/A
9.
-Pace Containers Used?
es
[]NO
❑N/A
_
Containers Intact?
gles
❑No
❑N/A
10.
Filtered Volume Received for Dissolved Tests?
Dyes
[]No
/A
11. Note if sediment is visible in the dissolved container
Sample Labels Match COC?
es
(:IN-
❑N/A
12,
-Includes Date/Time/ID/Analysis Matrix: Vr
All containers needing acid/base preservation have been
13,
checked?
✓
01e;
[]NO
❑N/A
,
All. containers needing preservation are found to be in
compliance with EPA recommendation?
(HNO3, H2SOa, HCI<2; NaOH>9 Sulfide, NaOH>12 Cyanide)
ZYs
[]NO
❑N/A
Exceptions: VOA, Coliform, TOC, Oil and Grease,
DRO/8015 (water) DOC,LLHg
es
ONO
❑N/A
Samples checked for dechlorination
OKs
❑No
❑NIA
14.
Headspace in VOAVials(>5-6mm)?
Dyes
o
❑N/
15.
Trip Blank Present?
❑Yes
❑No
N
16.
Trip Blank Custody Seals Present?
❑yes
[]NON/A
Pace Trip Blank Lot q (if purchased):
.1 CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Resolution:
Project Manager SCURF Review: L1'�
Field Data Required? ❑Yes []NO
Date/Time:
Date: Cs 19, t ".
Project Manager SRF Review: Lirl Date: tU`i I ct I �
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
.Out of hold, incorrect preservative, out of temp, Incorrect containers)
Page 28 of 36

o
PaceAnalytical
w"'PacelaPLPem
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain-ol-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. 2
Or
11
Section A Section ISof
Section C
Page: p
m
Required Client InlwmaPon: Required Project Information: Invoice Information:
2043196
Cron P""ysH,tr•L� L�llf-.%t/ ,,.JG RuP01l
To: F?ELr.tt�lF C�iZCcALc'
AIIenlgn:
ndarass: Corry
H3o T GG' CREoK fiD
To:
'Ais-uSL CoX
Carr Nfre
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REGULATORY AGENCY
Ci4ARLn'FT8 , Iy G e `3ecg
C&t(I AXC F400 %j4WPIJ0`4"
Address;
(j/NPDES 7- GROUNDWATER r DRINKING WATER
r UST r RCRA (� OTHER
Email Ta: Purchase
Order No.:
Pace Ouo,
E'nC nP+ri o.c•;,•
Hcmr«e�:�
Phone
7ar-i-��f-G 9/3
Fat: Praject
'Tc�-3/}-EILG'
Name:
CULFAK FLUfD
Pa Poied
%,%A
Site Location
%{fWiDL//J4
M:rn:mir Lw-9 RAISt//
STATE:
`I
,V C,
Requested Due DateRATs,,,,,,D, Project
Number: IsJ 109-dL
Pnce PoelaW `1 j,}^
Requested Analysis Filtered (YIN)
Section Maui. Codes
-
a
Imemrmclarnunwn.loon MATRIX I p0DE
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COLLECTED
Preservatives
i
Drinking Water DW
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Sample IDs MUST BE UNIQUE Tither TS
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ADDITIONAL COMMENTS
RELINQUISHED BY I AFFILIATION
DATE
TIME
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DATE
TIME
SAMPLE CONDITIONS
TiG ; �o�, c z6,«r:v�,
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ORIGINAL
SAMPLER NAME AND SIGNATURE
c
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PRINT Name of SAMPLER: _D40f/fY /{�
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SIGNATURE of SAMPL I
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(I'MIDDIYYj:
m
m
nmP,nnm umn:Ovs.nnnq nnx term rue nrn acciPe�q Pecn's nEr0e "ar a..... enrouml ae•rniPbleanviinsmly%pn ��.wmtarnro ��ivdcc i/'ein wm.n�. dir FALL-O-020rev.07. 15.May 2007

NI NCO Labo-F r t on'es
Accurate. Timeh,I. Responsive. Innovative.
4810 Executive Park Court, Suite 111
Jacksonville FL, 32216-6069
Phone: [phone] FAX: [phone]
Thursday, May 26, 2016
Pace Analytical (PA007)
Attn: Liamm Harrison
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
RE: Laboratory Results for
Project Number: Colfax Fluid Handling 1150109, Project Name/Desc: 92298198
ENCO Workorder(s): BZ02206
Dear Liamm Harrison,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, May 20, 2016.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Jacksonville.
Data from outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Chris Tompkins
Project Manager
Enclosure(s)
FINAL
This report relates only, to the sample as received by Me laboratory, and may only be reproduced in M.
Page 30 of 36
Page 1 of 7

w .encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: OF-004
Lab ID: BZ02206-01
Sampled:
05/17/16 16:20 Received: 05/20/16 11:00
Parameter
Hold Date/Timefs) Prep Date/Time(s)
Analysis Date/Timefsl
EPA 1664E
06/14/16 05/24/16
15:13
05/25/16 19:39
Page 31 of 36
FINAL This report relates only to lye sample as received by lye Wboratory, and may only be reproduced in U. Page 2 of

Calm
v .encolalss.cors
SAMPLE DETECTION SUMMARY
No positive results detected.
Page 32 of 36
FINAL This report relates only to the sample as received by lye abaratory, artl may only be repracimed in U. Page 3 of

S Nhq co
�.encolabs.com
ANALYTICAL RESULTS
Description: OF-004 Lab Sample ID: BZ02206-01 Received: 05/20/16 11:00 I
Matrix: Water Sampled: 05/17/16 16:20 Work Order: BZ02206
Project: 92298198 Sampled By:
Chemistry Parameters
Analyte [CAS Number]
Oil & Grease (HEM) [C-0007]A
Results Flaa Units DF MDL PQL Batch Method Analyzed By Notes
0.638 U mg/L 0.266 0.638 1.33 6E24002 EPA 1664B 05/25/16 18:39 SMA
Page 33 of 36
FINAL This report relates only to the sample as reeewe l by Me laboratory, and may only M reproduced in full. Page 4 of 7

QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Hatch 6E14001- EPA 1664A
Blank (6E24002-BLRI)
Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39
Spike Source %REC
RPD
Analvte
Result
F.Iao
POL
Units
Level Result %REC Limits RPD
Limit Notes
Oil & Grease (HEM)
0.613
U
1.28
ri
LCS (6E24002-BSI)
Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39
Spike Source %REC
RPD
Analvte
Result
FIIR
POL
Una
Level Result %REC Limits RPD
LaiLaft Notes
Oil & Grease (HEM)
154
5.00
mg/L
159 97 78-114
LCS Cup (6E24002-BSDI)
Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39
Spike Source %REC
RPD
Analvte
Result
Had
POL
Units
Level Result %REC Limits RPD
LIMA Notes
Oil & Grease(HEM)
156
5.00
mg/L
160 98 78-114 2
18
Matrix Spike (6E24002-14SI)
Prepared: 05/24/2016 15:13 Analyzed: 05/25/2016 18:39
Source: B202144-01
Spike Source %REC
RPD
AJrahQe
Result
Fte
POL
Una
Level Result a7aREC Limits RPD
L1011.1 Notes
Oil & Grease (HEM)
155
5.00
mg/L
148 2.40 U 105 78-114
Page 34 of 36
FINAL This report relates only to the sample as received by lye laboratory, ard may only be reproduced in full. Page 5 of 7

L
e Nik,e0
www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
I The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
Page 35 of 36
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- - --------
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Q99QRICIA Wnrknrrlpr Name- Colfax.Fluid Ilardlino 1150109-
---- ------ ... . .. ... ..... .
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Results Requested By: 5/25J2016
Repon: i Invoice To_ .i 10
Rea steel Anal ysis
Liamm Harrison
efr\ L-0, P.O. t-A
Pace Analytical Charlotte
9800 Kincey Ave. Suite 100 Ljq-,k<) F
Huntersville NC 28078
Phone [phone]
-Tzu 32U,
Email: [e-mail]
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State of Sample Origin. NC :iRmsomedCont,1166fs-.'-z
item
sam ia 'ID
Lab ID
Matrix
LAD USE ONLY
1
OF-004
5117=16 16:20
92298198001
Water
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Received on lee rYjor N
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Wednesday, May 18, 2016 5:42:49 PM
FMTALL-C-002rev.00 24Manch2009 PIqe 1 of 1