NCG030251_MONITORING INFO_20191230

/r
STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
,v L( b3 b a 5 i
DOC TYPE
❑ HISTORICAL FILE
li MONITORING REPORTS
DOC DATE
❑ a 3
YYYYM M DD

DOC TYPE 1 ❑ HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE 1 ❑
YYYYMMDD

December 6. 2019
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699
RE: Semi -Annual Stormwater Discharge Monitoring Report
Certificate of Coverage Number NCG030251
Watts Water Technologies
100 Watts Rd.
Spindalc, NC 28160
To Whom It May Concern:
REUFf ro
DEC $ 0 2019
CLzf"fTTVU Flf_ ;
LV/13 3L; 17b,'
In accordance with the North Carolina Department of Environment and Natural Resources (NC
DENR) stormwater discharge permit. ARM Environmental Services. Inc. collected the second
semi-annual stormwater samples at the referenced facility on November 12. 2019.
All parameters were below the permitted range benchmarks in the sample except for copper.
Since this is the second copper exceedance of the past two consecutive sampling events, a 'tier 11
response is triggered per the permit. The site will immediately begin monthly monitoring Rx all
parameters at outlall 2. The pl-I was performed in the field upon sample collection: was within
the recommended holding time of' 15 minutes: and showed results within the permitted range
benchmark value ol'6.0-9.0. The Stormwater Discharge Monitoring Report (SDO), which also
shows the analytical results for the outlall is attached. Please contact Tiffany Crosby. Sr. 1-1-IS
Engineer via phone [phone] or email tilTmiy.crosby(7wattswater.com with any questions.
Sincerely.
Brad Bowen
Operations Manager

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted J
CERTIFICATE
FACILITY NAI
COUNTY lK
PERSON COL
Comments on sample
0S
Lab Cert. #
or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR �•n
SAMPLE PERIOD ❑ Jan -June Q'July-Dec
or ❑ Monthly' /month)
DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
❑Other
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?"
Non -Polar 0&G/
Total Toxic
Outfall No.
Date Sample
24-hour rainfall
Total Suspended Solids
P
Total Copper
Total Lead
TotapH,l Zinc
Total Petroleum
Or anicss
g
Collected'
amount,
Standard units
and
Hydrocarbons
Benchmarks
(mo/dd/yr)
Inches3
-
100 mg/L or 50 mg/L"
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
46529
C0530
00400
01119
01051
01094
r"y
00552
78141
!i"� �i
'cn—
G •
U-U
/. ' mJ,
) D7J
D dr.
c�c�
i7/, .2
t
t the same outfall
3 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parame er a
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
A See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of file total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance witfit I ie permit monitoring requirement for total toxic organics
( ITO), I certily that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runolf has occured since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in fire Stormwater Pollution Prevention Plan."
•—�iCl.9�j3sraGt_.t�
Name (Print name)
Title rinl title)
Signature Dan
Nate: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
n Nn rlisrhnrne this oeriod?t
Outtall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches'
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or SO mg/L'
Porxmeter Code
-
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Dale: 1111/201Ad15/31/2.021 SWLI-245, last revised 11/1/2018
Page 2,43

}
\\
ir
\){
( n
-_
<
-\ Lm
!
/k \}{
) }}
j\/&§
\(\{
\�§{Q
\
}\\\
0
-
0
!+7
©«�
)\}{}
C3
0\\\
\\\\
}
}!\®
®§)
_
;)
Ic
}k
\\\
�\
o

I I.C.
Environmenral
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling oul this fbrm, please visil https://deq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: or Certificate of Coverage No.: N/C/G/ j /S/ O/ -)/ S/ I /
Facility
Date of Inspection:
Time of Inspection:
Total Event Precipitation (inches): b• U'
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the perminee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the perminee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
3ennittee or Designee)
1. Outfall Description:
Outfall No. ex',;�
ReceivinpNStrcam:
Structure (pipe, ditch, etc.):
7 iZic V4, 4--4 � ( 4 r— 4- `54r"n O . 0 V `N-e f— (
the industrial activities that occur within the outfall drainage
Page I of 2
SWU-242. Last modified 06101/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.):
4. Clarit♦ : Choose the number which best describes the clarity of the discharge. where I is clear
and 5 is very cloudy:
2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of Floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids:
2 3 4 5
v/
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where l is no solids and 5 is extremely muddy:
2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes e No.
8. Is there an oil sheen in the stormwater discharge? OYes A No.
9. Is there evidence of erosion or deposition at the outfall? O Yes © No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SwU-242. Last modified 06,01/2018

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
ARM Environmental Services, Inc.
11164 Downs Road
Pineville, NC 28134
Attention: Tim McCorkle
Project Name: Watts Water SW
Lot Number:UK13083
Date Completed:11/2612019
i
11/29/2019 8:46 AM
Approved and released by:
Lab Director - Greenville: Lucas Odom
AW
A
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc. -
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fox [phone] w .shealylab.com
Page I or 11

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
ARM Environmental Services, Inc.
Lot Number: UK13083
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Pesticides/PCBs by GC
The following sample was diluted due to the nature of the sample matrix: UK13083-001. The LOQ has
been elevated to reflect the dilution.
Shealy Environmental Services, Inc.
106 Vantage Paint Drive West Columbia, SC 29172 [phone] Fax [phone] vi ahealylab.com
Page 2 or 1 I

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
ARM Environmental Services, Inc.
Lot Number: UK13083
Sample Number Sample ID Matrix Date Sampled Date Received
001 002 Aqueous 11112120 19 1035 11/13/2019
(1 sample)
'Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvm.shealylab.com
Page 3 of I I

SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
ARM Environmental Services, Inc.
Lot Number: UK13083
Sample Sample ID
Matrix Parameter Method
Result a
Units
Page
001 002
Aqueous Copper 200.8
34
uglL
8
001 002
Aqueous Lead 200.8
3.3
uglL
8
001 002
Aqueous Zinc 200.8
32
uglL
8
(3 detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] w .shealylah.com
Page 4 of I I

Client: ARM Environmental Services, Inc. Laboratory ID:UK13083-001
Description: 002 Matrix: Aqueous
(Date Sampled:1111212019 1035
Date Received: 11/1312019
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (TSS) SM 2540D-2011 1 11/18/2019 2239 MOM 36139
1 (SGT - HEM (n) 1664B 1 11/25/20191006 SMA 36913
CAS Analytical
Parameter
Number Method
Result O
LOO
Units Run
TSS
SM 2540D-
NO
1.3
mg/L 1
SGT - HEM (non -polar material)
1664B
NO
5.0
mg/L 1
Volatile Organic Compounds by GUMS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 624.1 624.1 1 11/14/20191623 TML 35671
CAS Analvtical
Parameter
Number
Method
Result O
L00
Units
Acrolein
107-02-8
624A
NO
5.0
ug/L
Acrylonitrile
107-13-1
624.1
NO
5.0
ug/L
Benzene
71-43-2
624.1
NO
1.0
it
Bromodichloromethane
75-27-4
624.1
NO
1.0
ug/L
Bromoform
75-25-2
624.1
NO
1.0
ug/L
Bromomethane (Methyl bromide)
74-83-9
624.1
NO
2.0
ug/L
Carbon tetrachloride
56-23-5
624.1
NO
1.0
ug/L
Chlorobenzene
108-90-7
624.1
NO
1.0
ug/L
Chloroelhane
75-00-3
624.1
NO
2.0
ug/L
2-Chloroethylvinylether
110-75-8
624.1
NO
5.0
ug/L
Chloroform
67-66-3
624.1
NO
1.0
ug/L
Chloromethane (Methyl chloride)
74-87-3
624.1
NO
2.0
ug/L
Dibromochloromethane
124-48-1
624.1
NO
1.0
ug/L
1;2-Dichlorobenzene
95-50-1
624.1
NO
1.0
ug/L
1,3-Dichlorobenzene
541-73-1
624.1
NO
1.0
ug/L
1,4-Dichlorobenzene
106-46-7
624.1
NO
1.0
ug/L
Dichlorodifluoromethane
75-71-8
624.1
NO
2.0
ug/L
1,1-Dichloroethane
75-34-3
624.1
NO
1.0
ug/L
1,2-Dichloroethane
107-06-2
624.1
NO
1.0
ug/L
1,1-Dichloroethene
75-35-4
624.1
NO
1.0
ug/L
cis-1,2-Dichloroethene
156-59-2
624.1
NO
1.0
ug/L
trans-1,2-Dichloroethene
156-60-5
624.1
NO
1.0
ug/L
1,2-Dichloropropane
78-87-5
624.1
NO
1.0
ug/L
cis-1,3-Dichloropropene
10061-01-5
624.1
NO
1.0
ug/L
trans-1,3-Dichloropropene
10061-02-6
624.1
NO
1.0
ug/L
Ethylbenzene
100-41-4
624.1
NO
1.0
ug/L
Methylene chloride
75-09-2
624.1
NO
1.0
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
624.1
NO
1.0
ug/L
Tetrachloroethene
127-18-4
624.1
NO
1.0
ug/L
Toluene
108-88-3
624.1
NO
1.0
ug/L
LOO Limit of Ouenha,bon B = Detected In the method blank E =Ouantilation of compound exceeded 0e calibration range
NO = Not detected at or above the L00 N = Recovery is out of criteria P =The RPD between We GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services. Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of I I

Client: ARM Environmental Services, Inc. Laboratory ID:UK13083.001
Description: 002 Matrix: Aqueous
Date Sampled:11/12120191035
Date Received: 11/13/2019
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 624.1 624.1 1 11/14/20191623 TML 35671
CAS
Analytical
Parameter
Number
Method
Result O
LOO
Units
Run
1,2,4-Trichlorobenzene
120-82-1
624.1
NO
1.0
ug/L
1
1,1,1-Trichloroethane
71-55-6
624.1
NO
1.0
ug/L
1
1,1,2-Trichloroethane
79-00-5
624.1
NO
1.0
ug/L
i
Trichloroethene
79-01-6
624.1
NO
1.0
ug/L
1
Trichlorofluoromethane
75-69-4
624.1
NO
1.0
ug/L
1
Vinyl chloride
75-01-4
624.1
NO
1.0
ug/L
1
Run 1 Acceptance
Surrogate 0 % Recovery Limits
Bromofluorobenzene 78 70-130
1,2-Dichloroethane-d4 85 70-130
Toluene-d8 80 70-130
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 625.1
625.1
1 11/23/20192140 SCD
11119/20191719 36273
CAS
Analytical
Parameter
Number
Method
Result 0
LOO
Units
Run
Acenaphthene
83-32-9
625.1
NO
1.6
ug/L
1
Acenaphthylene
208-96-8
625.1
ND
1.6
ug/L
1
Anthracene
120-12-7
625.1
ND
1.6
ug/L
1
Benzidine
92-87-5
625A
ND
8.0
ug/L
1
Benzo(a)anthracene
56-55-3
625.1
NO
1.6
ug/L
1
Benzo(a)pyrene
50-32-8
625.1
NO
1.6
ug/L
1
Benzo(b)fluoranthene
205-99-2
625.1
NO
1.6
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625.1
NO
1.6
ug/L
1
Benzo(k)fluoranthene
207-08-9
625.1
NO
1.6
ug/L
i
4-Bromophenyl phenyl ether
101-55-3
625.1
ND
1.6
ug/L
1
Butyl benzyl phthalate
85-68-7
625.1
ND
1.6
ug/L
i
his(2-Chloro-l-methylethyl) ether
108-60-1
625.1
NO
1.6
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625.1
NO
1.6
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625.1
NO
1.6
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
625.1
NO
1.6
ug/L
1
2-Chloronaphlhalene
91-58-7
625.1
NO
1.6
ug/L
1
2-Chlorophenol
95-57-8
625.1
NO
1.6
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625.1
NO
1.6
ug/L
i
Chrysene
218-01-9
625.1
ND
1.6
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625.1
NO
1.6
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625.1
NO
8.0
ug/L
1
2,4-Dichlorophenol
120-83-2
625.1
NO
1.6
ug/L
1
LOO a Limit of Guantitation
B = Detected in the method blank
E = Ouantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOO
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
H = Out of holding time
W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia. SC 29172 [phone] Fax [phone] wwW.shealylab.com
Page 6 of 1 I

Client:ARM Environmental Services, Inc. Laboratory ID:UK13083-001
Description: 002 Matrix: Aqueous
Date Sampled:11/1212019 1035
Date Received: 11/13/2019
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 11/23/20192140 SCD 11/19/20191719 36273
Parameter
CAS
Number
Analytical
Method
Result O
LOO
Units
Run
Diethylphlhalate
84-66-2
625.1
ND
1.6
ug/L
i
Dimethyl phthalate
131-11-3
625.1
ND
1.6
ug/L
1
2,4-Dimethylphenol
105-67-9
625.1
ND
1.6
ug/L
1
Di-n-butyl phthalate
84-74-2
625.1
ND
1.6
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625.1
ND
8.0
uglL
1
2,4-Dinitrophenol
51-28-5
625A
ND
8.0
ug/L
1
2,4-Dinitrololuene
121-14-2
625.1
ND
3.2
ug/L
1
2,6-Dinitrololuene
606-20-2
625.1
ND
3.2
ug/L
1
Di-n-octylphthalate
117-84-0
625.1
ND
1.6
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625.1
ND
1.6
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625.1
ND
8.0
ug/L
1
Fluoranlhene
206-44-0
625.1
ND
1.6
ug/L
1
Fluorene
86-73-7
625.1
ND
1.6
ug/L
1
Hexachlorobenzene
118-74-1
625.1
ND
1.6
ug/L
1
Hexachlorobutadiene
87-68-3
625.1
ND
1.6
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625A
ND
8.0
ug/L
i
Hexachloroethane
67-72-1
625.1
ND
1.6
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625A
ND
1.6
uglL
1
Isophorone
78-59-1
625.1
ND
1.6
uglL
1
Naphthalene
91-20-3
625.1
ND
1.6
ug/L
1
Nitrobenzene
98-95-3
625.1
ND
1.6
ug/L
1
2-Nitrophenol
88-75-5
625.1
ND
3.2
ug/L
1
4-Nitrophenol
100-02-7
625.1
ND
8.0
ug/L
1
N-Nitrosodimethylamine
62-75-9
625.1
ND
1.6
ug/L
1
N,Nitrosodi-n-propylamine
621-64-7
625.1
ND
1.6
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625.1
ND
1.6
ug/L
1
Pentachlorophenol
87-86-5
625.1
ND
8.0
ug/L
1
Phenanlhrene
85-01-8
625.1
ND
1.6
uglL
1
Phenol
108-95-2
625.1
ND
1.6
ug/L
1
Pyrene
129-00-0
625.1
ND
1.6
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625.1
ND
1.6
ug/L
1
Run 1
Acceptance
Surrogate
O % Recovery
Limits
2-Fluorobiphenyl
62
37-129
2-Fluorophenol
40
24-127
Nitrobenzene-d5
60
38-127
Phenol-d5
46
28-128
Terphenyl-dl4
85
10-148
2,4,6-Tribromophenol
73
41-144
L00 a Limit of Ouanewtion B = Detected in the method blank E=Ouantitalion of compound exceeded the calibration range
ND = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of I I

Client: ARM Environmental Services, Inc. Laboratory ID:UK13083-001
Description: 002 Matrix: Aqueous
Date Sampled:1111212019 1035
Date Received: 11/13/2019
Organochlorine Pesticides and PCBs
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 608.3 3665A 608.3 10 11/20/20192333 CHG 11118/20191520 36091
2 608.3 3665A 608.3 1 11/20/2019 1403 CHG 11/18/20191520 36091
Parameter
CAS
Number
Analytical
Method
Result
Q
LOQ
Units
Run
Aldrin
309-00-2
608.3
NO
0.40
ug/L
1
Aroclor 1016
12674-11-2
608.3
NO
0.40
ug/L
2
Aroclor 1221
11104-28-2
608.3
NO
0.40
ug/L
2
Aroclor 1232
11141-16-5
608.3
NO
0.40
ug/L
2
Aroclor 1242
53469-21-9
608.3
NO
0.40
ug/L
2
Aroclor 1248
12672-29-6
608.3
NO
0.40
ug/L
2
Aroclor 1254
11097-69-1
608.3
NO
0.40
ug/L
2
Aroclor 1260
11096-82-5
608.3
NO
0.40
ug/L
2
gamma-BHC (Lindane)
58-89-9
608.3
NO
0.40
ug/L
1
alpha-BHC
319-84-6
608.3
NO
0.40
ug/L
1
beta-BHC
319-85-7
608.3
NO
0.40
ug/L
1
delta-BHC
319-86-8
608.3
NO
0.40
ug/L
1
Chlordane
57-74-9
608.3
NO
4.0
ug/L
1
4,4'-DDD
72-54-8
608.3
NO
0.40
ug/L
1
4,4'-DDE
72-55-9
608.3
ND
0.40
ug/L
1
4,4'-DDT
50-29-3
608.3
NO
0.40
ug/L
1
Dieldrin
60-57-1
608.3
NO
0.40
ug/L
1
Endosulfan 1
959-98-8
608.3
NO
0.40
ug/L
1
Endosulfan II
33213-65-9
608.3
NO
0.40
ug/L
1
Endosulfan sulfate
1031-07-8
608.3
NO
0.40
ug/L
1
Ehdrin
72-20-8
608.3
NO
0.40
ug/L
1
Endrin aldehyde
7421-93-4
608.3
NO
0.40
ug/L
1
Heptachlor
76-44-8
608.3
NO
0.40
ug/L
1
Heptachlor epoxide
1024-57-3
608.3
NO
0.40
ug/L
1
Toxaphene
8001-35-2
608.3
NO
4.0
ug/L
1
Run 1 Acceptance
Run 2 Acceptance
Surrogate
Q %Recovery Limits
Q %Recovery
Limits
Decachlorobiphenyl
80 20-131
68
20-131
Tetrachloro-m-xylene
85 30-132
88
30-132
ICP-MS
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 11/20/2019 2348 BNW 11/20/2019 0954 36174
CAS
Analytical
Parameter
Number
Method
Result Q
LOO
Units
Run
Copper
7440-50-8
200.8
34
10
ug/L
1
Lead
7439-92.1
200.8
3.3
2.0
ug/L
1
Zinc
7440.66.6
200.8
32
10
ug/L
1
L00 • Limit of Ouantilation B = Detected in the method blank E=0uantitation of compound exceeded the calibration range
ND = Not detected at or above the 100 N = Recovery IS out of criteria P =The RPO between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of I I

Chain of Custody
FLL:J
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of I 1

y.
SHEALY ENVIRONMENTAL SERVICES, INC.
72
SDI E� ` Chain Of CustodyROCord Inn Vanlaoe . 20Polm Oflve • West (lx No. la, -7 29111
Telephone No. POCi-791-5700 Fas No. k9,4791-9111
www.shealylab.curn
Number 100?06
�(tll I�r•1`w\ , : �.��w.-�� �c?rur .�.n
--_"r',e^::�'�a�y
�i�1 . �� ����C��
� - EFi_Gl �-r
-
I7' 1J
&-.a,(n.^6S .af•�
Ar*W"M
..M
J m-.re
mero
9re
ed)
ra;e_L,� _
—
�(- _ _ _ _ 'C AY!4
••I�IP�•�111�V
r�J1!l�l-r� c,-a•nva��5„v.uk:
+
I�
C\J ,I
y;
�•
''
�jp 11I''j{�Ia1!N1{{tl JJrQI����1N�rI
LLI C1111
UK13o83
I ?�rrurr: cxra•GD
i w.,r
!Plwv W {/
�^ M.0 '.-t ._)a!�
P.a W.
?
•�
$•
3
,lASfti
A."
ert .fto^ne
Svr,h�ln:ir-nµ•?n,
in,-rsre.�1,•A,x ar..rle.rr5!a�si'e+lmcnc�r
7s9 I The
f
'h'• r
I -
q
$
13
I ?
;
i
1 r�
;/D">.i
I
I�
(
I
�2
.4�
I
I
(
I
I
I
III
I
I
it
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
!
I
I
rum Am Mllm Agwu #Ww hb.VlmV 111M 0WC=dr'e rAL
^ 9te M J RUM pediryJ
Se,yro LanonStl
Tl aabyn to Me'r 1:1 0'�Fxof'W 1aA
iiue_fa.•lvere mh,LS.v4ai
❑ rlr.r-F Mld 11 "S'nmonlh =Stll In And I] �ri;:an O llnlrnnn
C;c' ^.'amx:.a 1_te:eyl
Ogre Tie
rav:
n,m :FIII1
ac7
ram.
7e
1.pw-"a C/
ji-Ls �Lr'e-^'
za�r•�s,ei
rL !•!
aP6Ttill0 n..
iia(e
foil '
r..:m
jl//T/i�
r-m
1h,a
?� a
rr,a
n�7. _
Th'�
.i. Fe'.•.i'1gVRril'U+y/
A. IY.'.iiQtashod5y
Cam Thee
S.„MN!ay.,l+aa'ad by Care irre
ulo urrL ONLY ((--��
(Rrm'w:n nn ar, (::.:cisl /'Q')
Noic: rVl s Lr^,ofcs aro rc Ced refrom raceioi
unless cther arm remvnm a m marte.
C,9rR1BUMJ_NxLr..�„alcw.z ylw.,.b Lxnrevr,n,F15+J.,n1ar�L r+wcf;elCG6.m e<V"r A,ar;•,nt MrrloPr �.an..'.?.v =nr-;YAn nm liar _x:ri
W
m
X
m
cn
Z
n

SHEALY ENVIRONMENTAL SERVICES, INC.
EhcaA: I:nvivnmcnpl $ery irs, liw.
, Uo:umn:l Nunlc:: MIJVIa(:11
Client: ARM ENVL.
vq: 14rI
Sample Receipt Checldist (SRC) I:17"INv Dal, Viilola
Cooler Inspected bv,'deh: UM ; 11-I3-2019 Lot L: IIR 13083
Moms ofrcccipf: 13 SESI ❑Client ❑ UPS ❑ FedEF Other.
❑ YMWNol
11. Were cu"ody swats presonton too cooler?
Ycs
Nol
P1 NA
1 lrcu5lod' seals we'rG pnsenl, wem Ihev intact and unbroken?
pli Strip ID: 19-2194 Clllurine Suip ID: NA 'fasted by: I.KH
Original ternperalurc upon :eccipt i Deriv'cd (Corrected) Ieln, ernturc upon receipt %Solid Snap -Cup ID:
iA i 1.1 'C NA ;NA -C NA /NA ^C NA iyA .0
Mclhud: j�Tcn:peratura Hlvil: ❑Against Hades IR Gu1t ID: 5, lR Gun Corrcctinn Factor. 0 'C
Method oforiolant: ® WN Irc ❑ Ice Pack ❑ Dry Ix ❑ Non:
❑ Yes
❑No
®NA
'' lftemperatux ofany coolereaceeded 6.0`C.-,vas Project N4tniager Nolifiol?
PAT •.vas Notified by: phone! email i face-to-face (circle
❑ Yes
❑ Nol
®NA
4- Is die ottinnerciul courier's packing slip attached to this t'orm'2
Yeti
❑ Nol
5. Were proper custody procedwres (ielinquishadrr:ceivcxfl fnllowc.d7
0 Yes
L1 No
6. Were simple IDs listed on the COC?
VJ Yes
❑ No
7. Wcm sample IDs listed on all svnplp conlainct.?
0 Yes
❑ No
S. Was aillcclion dole & time listed nil the
i4 Yes
❑ No
9. Was collection date S Buie 61cd on all sample containers'?
V1 Yes
❑ No
10. Did all cunlaiucr Iu1x:I information (ID, dare, limn) agree with the COC?
❑ Ycs
❑ No
I I. Were test: to ix Iw r rmcd listed on the COO?
m Yes
❑ No
12. Did all samples arrive ;it the proper cantxincts for each tact anrVor in good condition
(unbroken, lids on, c1e.)? _
Ycs
r'1
❑ No
13. Ww adN=u: sainpie vnlliloc available'?
Ya;
❑ No
14. Wen: all samples received within r the holding time ou 48 hours, whichever comes first:'
Yes
No
15. Were any samples cuulninars missinl texcess (circle one) samples Not listed ou C(X)?
❑ Yes
❑ No
❑ NA
1 G. For VOA and RSK-175 samples, were bul)Wes pmmnl >,,pca.size•• (S6'or 6111112 III dldllieter)
m any of the VOA vial.?
® Ycs
Ne
NA
17. Well: all DROirn tals!nutrient svnnles rrx:eivcd at a pH of < 2?
❑ Yrs
❑ K"'ol
60 NA
I8. Wereall ryanicde aN?nJ(sulfide smmnls rrceivcd a a 9?
%a
❑ Ye
El No
® NA
pH',o
I9;Nfrepsildi
Were .inip•1)+pcs Ircc ot l
chlorine?
❑ Yes
QU
❑ No
® N.4
`t0. Were client remark;%requusts (i.e. requested dilutions, MS,'N4SD desigitations, clu... I
oirrmfiv transcribed from the COC into the couuneurst-Ctiini in t-AMS:'
Yes
Nu
21. Wus Ills 4UULC numhcr listed oil file container label:' If ves. uutc J? 21673
Sample 1'recrrvarion (Must be coniplrted for uny samples) incorrectly preserved ix with hnnlspacr..) -
Sample(s) NA Hose w.civcd incorrectly pir;crved and were adjusted acrordingly
in sample receiving wish N4 ml. ofoirrle one: H2SO4, HNO3, 140, Nti01i using SR i NA _
Time of preservation NA If ntoir dual one prescrva!iee is naeded. please nn du note !it anincnts below.
Sample(s) NA were mveived with bubbles;-6 rem in ditunicter.
Snmples(s) NA here received with TH(: '> 05 inWI, (If419 is no', and wcin
ndiusla;i accindingly in sample receiving Willi sodiuul Ihiosulfgc (Na_ScO,} with Shealy ID: NA
SR hm-code labels applied hy: HMS Date: 1 t-I,9-2Qi9
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] w .shealylab.com
Page I I of I 1