NCG030145_MONITORING INFO_20200114

Zip
STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
IV U& o 3 b i y 5
DOC TYPE
HISTORICAL FILE
�7MONITORING REPORTS
DOC DATE
❑ U b I ��
YYYYMMDD

DOC PE 1 ❑ HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE 1 ❑
YYYYM M D D

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 4w
CERTIFICATE OF COVERAGENO. N00030145
FACILITY NAME: Newton Instruments
COUNTY: Granville
PERSON COLLECTING SAMPLES: Nathan Beauchamp
LABORATORY:: Pace Analytical Lab Cert. #: 40 RE IVED
Comments on sample collection or analysis: Monthl sam In
JAN 14 2020
CENTRAL FILES
Part A: Stormwater Benchmarks and Monitoring RMIt ECTION
n No discharoe this period?'
SAMPLE COLLECTION YEAR: 2019
SAMPLE PERIOD[-] Jan -June❑ July -Dec
or®Monthly' December 2019
DISCHARGING TO CLASS❑ORW®HQW❑Trout❑PNA
❑Zero -flow❑ Water Supply❑SA
❑Other
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 34
Non -Polar
Outfall No.
Date Sample
24-hour rainfall
Total Suspended
PH,
Standard
Copper
Lead
Zinc
O&G/ Total
Total Toxic
Collected'
amount,
Solids
Petroleum
Organicss
(mo/dd/yr)
Inches'
units
Hydrocarbons
Benchmarks =__>
-
-
100 mg/L
6.0 - 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
001
12/17/19
0.3
134 mg/L
7.2
0.0124 mg/L
0.0057 mg/L
0.0817 mg/L
<5.0 mg/L
Not Detected
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan mayso certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
Permit -Date: 11/1/2017-10/31/2022 _ _ , _ - _ - - _ .. _ _. _ _.._ . _ _ -. _SWU-245, last revised.10/25/2012 _ -
---- - - ---- - -- - -- - - - Page l of

l
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
(Signature)
(Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging> 55 gal of new oil per month.
No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
-
-
15 mg/L
100 mg/L or SO mg/L`
6.0 - 9.0 SU
Footnotes from Part A also apply to this Part B
' See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: ll/1/2017-10/31/2022 _ -- - _ - _ - _ - _ ,----- - - - -_ - - - --SWU345,-Iasi revised 10/25/2012'-
---- Page 2of3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL?YES ® NO ❑
IF YES,HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE?YES ® NO ❑
REGIONAL OFFICE CONTACT NAME: John Holley
Mail an original and one copy of this DMR including off "No Discharge" reports within 30 days of receiptof the lob results for at end of monitoring period in
the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of
Permit Date:11/1/2017-10/31/2022
(Date)
— SWU-245,last revised '10/25/2012
Page 3 of 3

I
0
ace Analytical
W WY.pi[alibs.cela
I
January 03, 2020
Mr. Pete Dressel
Piedmont Geologic
6003 Chapel Hill Road
Suite 109
Raleigh, NC 27607
RE: Project: Newton Instruments/ 1912
Pace Project No.: 92457901
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Dressel:
Enclosed are the analytical results for sample(s) received by the laboratory on December 18, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
l�
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Jonathan Murphrey, Piedmont Geologic
?WSQ Kcltt5 �
eTNI
"oo Iop
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 29

aceAnalytical
Pace Analytical Services, LLC
0
9800 Kincey Ave. Suite 100
NC 28078
(�5Huntersville,
www.pacelabs.com
[phone]
CERTIFICATIONS
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
VrginialVELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
I Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
VirginiaNELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 29

0
aceAnalytical
w".pacelabs.com
SAMPLE SUMMARY
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
Lab ID Sample ID Matrix Date Collected Date Received
92457901001 Outfall-001 Water 12/17/19 08:00 12/18/19 10:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the wnuen consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 29

(55?eAnalyticale
www.pacelabs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Newton Instruments/ 1912
92457901
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92457901001
Outfall-001
SM 2540D-2011
AMI
1
PASI-E
EPA 1664B
HH
1
PASI-C
EPA 608.3
PKS
29
PASI-C
EPA 200.7 Rev 4.4 1994
IDS
12
PASI-A
EPA 245.1 Rev 3.0 1994
SOO
1
PASI-A
EPA 625.1
Bpi
62
PASI-C
EPA624.1
DLK
31
PASI-C
EPA 420.4 Rev 1.0 1993
KDF1
1
PASI-A
SM 4500-CN-E-2011
CJH1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 29

aceAnalytical e
ww.pudrbsxom
ANALYTICAL RESULTS
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
., Sample: Outfall-001 Lab ID: 92457901001 Collected: 12/17/1908:00 Received: 12/18/191040 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Oual
2540D Total Suspended Solids
' Total Suspended Solids
I I
Field Data
Collected By
q Collected Date
Collected Time
ipH
HEM, Oil and Grease
Oil and Grease
608 PCB Pest RVE
IAldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Chlordane (Technical)
alpha -Chlordane
gamma -Chlordane
4A'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan 11
Endosulfan sulfate
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epoxide
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
200.7 MET ICP
Antimony
Date: 01/03/2020 10:24 AM
Analytical Method: SM 254OD-2011
134 mg/L 7.8
7.8 1
12/1911909:54
Analytical Method:
NB
1
12/17/19 08:00
12117/19
1
12/17/19 08:00
08:00
1
12/17/19 08:00
7.2 Std. Units
1
12/17119 08:00
Analytical Method: EPA 1664B
NO mg/L 5.0
1.3 1
01/02/2009:59
Analytical Method: EPA608.3 Preparation Method: EPA608.3
NO
ug/L
0.050
0.022
1
12/23/19 10:04
12/23/1917:49
309-00-2
NO
ug/L
0.050
0.019
1
12/2311910:04
12/23/1917:49
319-84-6
NO
ug/L
0.050
0.014
1
1212311910:04
1212311917:49
319-85-7
NO
ug/L
0.050
0.020
1
12123/1910:04
12/2311917:49
319-86-8
NO
ug/L
0,050
0.012
1
12/23/19 10:04
12/23/1917:49
58-89-9
NO
ug/L
0.50
0.20
1
12/23/19 10:04
12/2311917:49
57-74-9
NO
ug/L
0.050
0.0090
1
12123/1910:04
12/23/1917:49
5103-71-9
NO
ug/L
0.050
0.017
1
12/23/19 10:04
12/2311917:49
5103-74-2
NO
ug/L
0.050
0.0069
1
12/2311910:04
12/2311917:49
72-54-8
NO
ug/L
0.050
0.0064
1
12123/1910:04
12123/1917:49
72-55-9
NO
ug/L
0.050
0.018
1
12123/1910:04
1212311917:49
50-29-3
NO
ug/L
0.050
0.0073
1
12/23/1910:04
1212311917:49
60-57-1
NO
ug/L
0.050
0.0094
1
12/23/19 10:04
12/23/1917*49
959-98-8
NO
ug/L
0.050
0.0065
1
12123/1910:04
12/23/1917:49
33213-65-9
NO
ug/L
0.050
0.0091
1
12123/1910:04
12/23/1917:49
1031-07-8
NO
ug/L
0.050
0.0089
1
12/23/1910:04
12/23/1917:49
72-20-8
NO
ug/L
0.050
0.013
1
12/23/19 10:04
12/2311917:49
7421-93-4
NO
ug/L
0.050
0,016
1
12123/1910:04
12/23/1917:49
76-44-8
NO
ug/L
0.050
0.0097
1
12/23/1910:04
12/2311917:49
1024-57-3
NO
ug/L
0.50
0.22
1
12/23/1910*04
1212311917:49
12674-11-2
NO
ug/L
0.50
0.32
1
12/23/19 10:04
12/23/19 17:49
11104-28-2
NO
ug/L
0.50
0.21
1
12/2311910:04
12/23/1917:49
11141-16-5
NO
ug/L
0.50
0.44
1
12/23/19 10:04
12/23/1917:49
53469-21-9
NO
ug/L
0.50
0.34
1
12/23/19 10:04
12/2311917:49
12672-29-6
NO
ug/L
0.50
0.24
1
12/23/1910:04
12123/1917:49
11097-69-1
NO
ug/L
0.50
0.30
1
12123/1910:04
12/23/1917:49
11096-82-5
NO
ug/L
0.50
0.20
1
12/23/19 10:04
12/2311917:49
8001-35-2
102
%
10-130
1
12/23/19 10:04
12/23/1917*49
877-09-8
100
%
10-130
1
12/23/19 10:04
12/23/19 17:49
2051-24-3
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
NO ug/L 5.0 3.0 1 12128/1900:27 12/29/1920:25 7440-36-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 29

aceAnalytical e
www.psctlsbs.com
ANALYTICAL RESULTS
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Oulfall-001 Lab ID: 92457901001 Collected: 12/17/1908:00 Received: 12/1811910:40 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qua[
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Arsenic
ND
ug/L
10.0
4.7
1
12/28/19 00:27
12/29/19 20:25
7440-38-2
Beryllium
ND
uglL
1.0
0.20
1
12/28/19 00:27
12/29/19 20:25
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
12/28/19 00:27
12/29/19 20:25
7440-43-9
Chromium
5.0
ug/L
5.0
1.0
1
12/28/19 00:27
12/29/19 20:25
7440-47-3
Copper
12.4
ug/L
5.0
2.1
1
12/28/19 00:27
12/29/19 20:25
7440-50-8
Lead
5.7
ug/L
5.0
1.6
1
12/28/19 00:27
12/29/19 20:25
7439-92-1
Nickel
10.6
ug/L
5.0
0.90
1
12/28/19 00:27
12/29/19 20:25
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
1212811900:27
12129/1920:25
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
12/28/19 00:27
12/29/19 20:25
7440-22-4
Thallium
ND
ug/L
10.0
2.6
1
12/28/19 00:27
12/29/19 20:25
7440-28-0
Zinc
81.4
ug/L
10.0
3.9
1
12/28/19 00:27
12/29/19 20:25
7440-66-6
245.1 Mercury
Analytical Method: EPA245.1 Rev 3.0
1994 Preparation
Method : EPA 245.1 Rev 3.0 1994
Mercury
ND
ug/L
0.20
0.10
1
12/23/1912:01
12/2311915:56
7439-97-6
625 MSSV
Analytical Method: EPA625.1 Preparation Method: EPA625.1
Acenaphthene
ND
ug/L
4.9
0.25
1
12/23/19 15:29
12/30/19 19:54
83-32-9
Acenaphthylene
ND
ug/L
4.9
0.21
1
12/23/19 15:29
12/30/19 19:54
208-96-8
'Anthracene
ND
ug/L
4.9
0.14
1
12/23/19 15:29
12/30/19 19:54
120-12-7
Benzidine
ND
ug/L
49.0
5.0
1
12/23/19 15:29
12/30/19 19:54
92-87-5 L2
Benzo(a)anthracene
ND
ug/L
4.9
0.32
1
12/23/19 15:29
12/30/19 19:54
56-55-3
Benzo(a)pyrene
ND
ug/L
4.9
0.29
1
12/23/19 15:29
12130/1919:54
50-32-8
Benzo(b)fluoranthene
ND
ug/L
4.9
0.27
1
12/23/1915*29
12/30/19 19:54
205-99-2
I,Benzo(g,h,i)perylene
ND
ug/L
4.9
0.37
1
12/23/19 15:29
12/30/19 19:54
191-24-2
�Benzo(k)0uoranthene
ND
ug/L
4.9
0.42
1
12/23/19 15:29
12/30/1919:54
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
4.9
0.80
1
12/23/19 15:29
12/30/19 19:54
101-55-3
Butylbenzylphthalate
ND
ug/L
4.9
0.77
1
12123/1915:29
12/30/19 19:54
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
4.9
3.6
1
12/23/19 15:29
12/30/19 19:54
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
9.8
0.90
1
12/23/19 15:29
12/30/19 19:54
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
4.9
0,98
1
12/23/19 15:29
12/30/19 19:54
111-44-4
2-Chloronaphthalene
ND
ug/L
4.9
0.96
1
12/23/19 15:29
12/30/19 19:54
91-58-7
2-Chlorophenol
ND
ug/L
4.9
1.3
1
12M/1915:29
12/30/19 19:54
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
4.9
0.85
1
12/23/19 15:29
12/30/19 19:54
7005-72-3
Chrysene
ND
ug/L
4.9
0.21
1
12/23/19 15:29
12/30/1919:54
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
4.9
0.54
1
12/23/19 15:29
12/30/19 19:54
53-70-3
1,2-Dichlorobenzene
ND
ug/L
4.9
0.86
1
12/23/19 15:29
12/30/19 19:54
95-50-1
1,3-Dichlorobenzene
ND
ug/L
4.9
0.79
1
12/23/1915:29
12/3011919:54
541-73-1
1,4-Dichlorobenzene
ND
ug/L
4.9
0.93
1
12/23/19 15:29
12/30/19 19:54
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
24.5
2A
1
12/23/19 15:29
12/30/19 19:54
91-94-1
2',4-Dichlorophenol
ND
ug/L
4.9
1.7
1
12/23/19 15:29
12/30/19 19:54
120-83-2
Diethylphthalate
ND
ug/L
4.9
0.57
1
12123/1915:29
12/3011919:54
84-66-2
2;4-Dimethylphenol
ND
ug/L
9.8
1.2
1
12/23/19 15:29
12/30/19 19:54
105-67-9
Dimethylphthalate
ND
ug/L
4.9
0.75
1
12/23/19 15:29
12/30/19 19:54
131-11-3
Di-n-butylphthalate
ND
ug/L
4.9
0.74
1
12/23/19 15:29
12/30/19 19:54
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
19.6
2.5
1
12/2311915:29
12/30/19 19:54
534-52-1
2,4-Dinitrophenol
ND
ug/L
49.0
8.8
1
12123/1915:29
12/30/1919:54
51-28-5
f 1 1.I:i1111.71A1: 91:L•ril3n.ra111M61
This report shall not be reproduced, except in full,
Dale: 01/03/2020 10:24 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 29

Pace Analytical Services, LLC
Kincey Ave,100
aceAnalytical ® 9900Hun a svlle, C1te 28078
www.pacslrbs.com
[phone]
ANALYTICAL RESULTS
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
Sample: Outfall-001 Lab ID: 92457901001 Collected: 12/17/19 08:00 Received: 12/18/19 1040 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
OF
Prepared
Analyzed
CAS No. Qual
626 MSSV
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
2,4-Dinitrotoluene
NO
ug/L
4.9
0.88
1
12123/1915:29
12/30/1919:54
121-14-2
2,6-Dinitrotoluene
NO
ug/L
4.9
0.96
1
12/23/19 15:29
12/30/19 19:54
606-20-2
Di-n-octylphthalate
NO
ug/L
4.9
0.65
1
12/23/19 15:29
12/30/19 19:54
117-84-0
1,2-Diphenylhydrazine
ND
ug/L
4.9
0.88
1
12/23119 15:29
12/30119 19:54
122-66-7
bis(2- Ethylhexyl) phtha late
NO
ug/L
4.9
0.77
1
12/23/19 15:29
12/30/19 19:54
117-81-7
Fluoranthene
NO
ug/L
4.9
0.21
1
12/23/19 15:29
12/30/19 19:54
206-44-0
Fluorene
ND
ug/L
4.9
0.21
1
12/23/19 15:29
12/30/19 19:54
86-73-7
Hexachloro-1,3-butadiene
NO
ug/L
4.9
0.92
1
12/23/19 15:29
12/30/19 19:54
87-68-3
Hexachlorobenzene
NO
ug/L
4.9
0.71
1
12/23/19 15:29
12/30/19 19:54
118-74-1
Hexachlorocyclopentadiene
NO
uglL
9.8
0,86
1
121231191529
12/30/191954
77-47-4
Hexachloroethane
NO
ug/L
4.9
1.1
1
12/23/19 15:29
12/30/19 19:54
67-72-1
Indeno(1,2,3-cd)pyrene
NO
ug/L
4.9
0.28
1
12/23/19 15:29
12/30/19 19:54
193-39-5
Isophorone
ND
ug/L
9.8
0.87
1
12/23/19 15:29
12/30/19 19:54
78-59-1
I' Naphthalene
NO
ug/L
4.9
0.33
1
12/23/19 15:29
12/30/19 19:54
91-20-3
Nitrobenzene
NO
ug/L
4.9
1.1
1
12/23/19 15:29
12/30/19 19:54
98-95-3
2-Nitrophenol
NO
ug/L
4.9
0.89
1
12/23/19 15:29
12/30/19 19:54
88-75-5
4-Nitrophenol
NO
ug/L
49.0
4.0
1
12/23/19 15:29
12/30/19 19:54
100-02-7
N-Nitrosodimethylamine
NO
ug/L
4.9
0.89
1
12/23/1915:29
12/30/19 19:54
62-75-9
N-Nitroso-di-n-propylamine
NO
ug/L
4.9
0.97
1
12/23/1915:29
12/30/1919:54
621-64-7
N-Nilrosodiphenylamine
NO
uglL
9.8
0.98
1
12/23/1915:29
12/30/1919:54
86-30-6
Pentachlorophenol
ND
ug/L
9.8
4.5
1
12/23/19 15:29
12/30/19 19:54
87-86-5
Phenanlhrene
NO
ug/L
4.9
0.22
1
12/23/19 15:29
12/30/19 19:54
85-01-8
Phenol
NO
ug/L
4.9
1.9
1
12/23/1915:29
12130/1919*54
108-95-2
�Pyrene
NO
ug/L
4.9
0.19
1
12123/1915:29
12/30/19 19:54
129-00-0
1,2,4-Trichlorobenzene
NO
ug/L
4.9
0.96
1
12/23/19 15:29
12130/1919:54
120-82-1
2,4,6-Trichlorophenol
NO
ug/L
9.8
1.3
1
12/23/19 1529
12/30/19 19:54
88-06-2
Surrogates
Nitrobenzene-d5 (S)
61
%
10-120
1
12/23/19 15:29
12/30/19 19:54
4165-60-0
2-Fluorobiphenyl(S)
57
%
15-120
1
12/23/19 15:29
12/30/19 19:54
321-60-8
Terphenyl-d14 (S)
63
%
11-131
1
12/23/19 15:29
12/30/19 19:54
1718-51-0
'Phenol-d6(S)
21
%
10-120
1
12/23/19 15:29
12/30/19 19:54
13127-88-3
2-Fluorophenol (S)
30
%
10-120
1
12/23/19 15:29
12130/19 19:54
367-12-4
'2.4,6-Tribromophenol(S)
64
%
10-137
1
12/23/19 15:29
12/30/19 19:54
118-79-6
624 Volatile Organics Acrolein
Analytical
Method: EPA624.1
Acrolein
ND
ug/L
5.0
3.8
1
12/20/19 15:17
107-02-8 L1,M0
Acrylonitrile
NO
ug/L
5.0
L5
1
12/20/19 15:17
107-13-1
Benzene
NO
ug/L
1.0
0.38
1
12/20/1915:17
71-43-2
Bromodichloromethane
NO
ug/L
2.0
0.24
1
12120/1915:17
75-27-4
Bromoform
ND
ug/L
2.0
0.40
1
12/20119 15:17
75-25-2
Bromomethane
NO
ug/L
2.0
1.2
1
12/20/19 15:17
74-83-9
Carbon tetrachloride
NO
ug1L
2.0
0.29
1
12/20/19 15:17
56-23-5
Chlorobenzene
ND
ug/L
2.0
0.37
1
12/2011915:17
108-90-7
Chloroethane
ND
ug/L
2.0
1.4
1
12/20/19 15:17
75-00-3
2-Chloroethylvinyl ether
NO
ug/L
5.0
0.73
1
12/20/19 15:17
110-75-8
Chloroform
NO
ug/L
2.0
0.58
1
12/20119 15:17
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Dale: 01/03/2020 10:24 AM without the written coon sent of Pace Analytical Services, LLC, Page 7 of 29

(�IaceAnalyfical'
www.pacelahs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
Sample: Outfall-001 Lab ID: 92457901001 Collected: 12/17/1908:00 Received: 12/18/1910:40 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
624 Volatile Organics Acrolein
Chloromethane
Di bromochlo romelhane
1, 1 -Dichloroethane
1,2-Dichloroethane
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1, 3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Ji-ichlomelhene
Vinyl chloride
Surrogates
4-Bromolluorobenzene(S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
420.4 Phenolics, Total
I Phenol
4500CNE Cyanide, Total
Cyanide
it
Date: 01 /03/2020 10:24 AM
Analytical Method: EPA624.1
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
NO
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
2.0
0.73
1
12/20/19 15:17
74-87-3
2.0
0.32
1
12/20/1915:17
124-48-1
2.0
0.51
1
12/20/19 15:17
75-34-3
2.0
0.34
1
12/20/191517
107-06-2
2.0
0.42
1
12/20/1915:17
156-60-5
2.0
0.27
1
12/20/1915:17
78-87-5
2.0
0.33
1
12120/1915:17
10061-01-5
2.0
0.41
1
12/20/19 15:17
10061-02-6
1.0
0.28
1
12/20/19 15:17
100-41-4
2.0
0.24
1
12/20/19 15:17
75-09-2
2.0
0.34
1
12/20/19 15:17
79-34-5
2.0
0.28
1
12/20/191517
127-18-4
1.0
0.44
1
12/20/1915:17
108-88-3
2.0
0.35
1
12/20/19 15:17
71-55-6
2.0
0.31
1
12/20/19 15:17
79-00-5
2.0
0.36
1
12/20/1915:17
79-01-6
2.0
0.72
1
1212011915:17
75-01-4
95 % 70-130 1 12/20/1915:17
460-00-4
98 % 70-130 1 12/20/19 15:17
2037-26-5
101 % 70-130 1 12/20/19 15:17
17060-07-0
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
ND mg/L 0.020 0.0050 1 12/24/19 08:38 12/24/19 11:49
108-95-2
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
0.00631 mg/L 0.0080 0.0060 1 12/21/1915:00 12122/1911:27
57-12-5
REPORT OF LABORATORY ANALYSIS y
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 29

aceAnalytical
www.pacelaba.com
QUALITY CONTROL DATA
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
QC Batch: 515738 Analysis Method: SM 2540D-2011
OC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92457901001
Pace Analytical Services, LLC
9900 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 2763370 Matrix: Water
Associated Lab Samples: 92457901001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 2.5 12/19/19 09:52
LABORATORY CONTROL SAMPLE:
2763371
Spike
LCS LCS
e/ Rec
Parameter
Units
Conc.
Result %Rec
Limits
Qualifiers
Total Suspended Solids
mg/L
250
238 95
90-110
SAMPLE DUPLICATE: 2763372
92457802003
Dup
Max
Parameter
Units
Result
Result RPD
RPD
Qualifiers
Total Suspended Solids
mg/L
1800
1790
0
25
SAMPLE DUPLICATE: 2763373
92457883001
Cup
Max
Parameter
Units
Result
Result RPD
RPD
Qualifiers
Total Suspended Solids
mg/L
22.7
23.0
2
25
Results presented on this page are in the units Indicated by the'Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full,
Date: 01/03/2020 10:24 AM without the written consent of Pace Analytical Services, LLC.
Page 9 of 29

aceAnalytical e
www.pacelabs.cote
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
QC Batch: 517552
Analysis Method:
EPA 1664B
QC Batch Method: EPA 1664B
Analysis Description:
1664 HEM, Oil and Grease
i' Associated Lab Samples: 92457901001
METHOD BLANK: 2771026
Matrix: Water
Associated Lab Samples: 92457901001
Blank Reporting
Parameter
Units
Result Limit
MOIL
Analyzed
Qualifiers
Oil and Grease
I I
ri
ND 5.0 1.3
01/02/2009:58
j! LABORATORY CONTROL SAMPLE:
2771027
Spike LCS
LCS
%Rec
Parameter
Units
Cone. Result
%Rec
Limits Qualifiers
Oil and Grease
mg/L
40 35.6
89
78-114
MATRIX SPIKE SAMPLE:
2771028
92457968001 Spike
MS
MS
%Rec
I Parameter
Units
Result Cone.
Result
%Rec
Limits Qualifiers
Oil and Grease
mg/L
NO 40
37.3
91
78-114
Results presented on this page are In Me units indicated by the' UniW column except where an alternate unit is presentee to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/03/2020 10:24 AM without the written consent of Pace Analytical Services, LLC.
Page 10 of 29

Pace Analytical Services, LLC
aceAnalytical0
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
truspacelebe.com
[phone]
QUALITY CONTROL DATA
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
QC Batch: 516307
Analysis Method: EPA 245.1 Rev 3.0 1994
QC Batch Method: EPA 245.1 Rev 3.0 1994
Analysis Description: 245.1 Mercury
Associated Lab Samples: 92457901001
METHOD BLANK: 2766270
Matrix: Water
Associated Lab Samples: 92457901001
Blank Reporting
Parameter Units
Result Limit MDL Analyzed
Qualifiers
Mercury ug/L
ND 0.20 0.10 12/23/1915*27
LABORATORY CONTROL SAMPLE: 2766271
Spike LCS LCS % Rec
Parameter Units
Cone. Result % Rec Limits Qualifiers
Mercury ug/L
2.5 2.8 112 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2766272 2766273
MS MSD
92458435002
Spike Spike MS MSD MS MSD
%Rec Max
Parameter Units Result
Conc. Cone. Result Result %Rec %Rec
Limits RPD RPD Qua]
Mercury ug/L ND
2.5 2.5 2.7 2.6 108 102
70-130 5 20
Results presented on this page are in the units Indicated by the 'Unl[V column except where an alternate unit is presentee to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01103/2020 10:24 AM without the written consent of Pace Analytical Services, I.I.C. Page 11 of 29

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
,i QC Batch: 517046 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92457901001
METHOD BLANK: 2769322
Associated Lab Samples: 92457901001
1� Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony
ug/L
ND
5.0
3.0
12/29/1919:19
Arsenic
ug/L
NO
10.0
4.7
12/29/1919:19
Beryllium
ug/L
NO
1.0
0.20
12/29/1919:19
Cadmium
ug/L
NO
1.0
0.40
12129/1919:19
Chromium
ug/L
ND
5.0
1.0
12/29/1919:19
Copper
ug/L
NO
5.0
2.1
12129/1919:19
Lead
ug/L
ND
5.0
1.6
12/29/1919:19
Nickel
ug/L
ND
5.0
0.90
12/29/19 19:19
Selenium
ug/L
NO
10.0
4.7
1212911919:19
Silver
ug/L
NO
5.0
2.5
12/29/1919:19
Thallium
ug/L
NO
10.0
2.6
12/29/1919:19
Zinc
ug/L
NO
10.0
3.9
12/29/1919:19
LABORATORY CONTROL SAMPLE:
Parameter
I'
2769323
Units
Spike
Conc.
LCS
Result
LCS
%Rec
%Rec
Limits
Antimony
ug/L
500
466
93
85-115
Arsenic
ug/L
500
453
91
85-115
Beryllium
ug/L
500
517
103
85-115
Cadmium
ug/L
500
481
96
85-115
Chromium
ug/L
500
504
101
85-115
Copper
ug/L
500
492
98
85-115
I' Lead
ug/L
500
476
95
85-115
Nickel
ug/L
500
481
96
85-115
Selenium
ug/L
500
457
91
85-115
Silver
ug/L
250
240
96
85-115
Thallium
ug/L
500
480
96
85-115
Zinc
ug/L
500
450
90
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2769324
MS
92457831001
Spike
Parameter
Units
Result
Conc.
Antimony
ug/L
NO
500
Arsenic
ug/L
NO
500
Beryllium
ug/L
NO
500
Cadmium
ug/L
NO
500
Chromium
ug/L
ND
500
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Qualifiers
2769325
MSD
Spike
MS
MSD
MS
MSD
%Rec
Max
Conc.
Result
Result
e/ Rec
%Rec
Limits
RPD
RPD Qual
500
462
483
92
96
70-130
4
20
500
472
481
94
96
70-130
2
20
500
533
534
107
107
70-130
0
20
500
505
508
101
101
70-130
0
20
500
519
522
104
104
70-130
0
20
!'1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 01/03/2020 10:24 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 29

lace Analytical
W W W.ptttltbf.0010
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project:
Newton Instruments/ 1912
Pace Project No.:
92457901
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2769324
2769325
MS
MSD
92457831001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
e/ Rec
Limits
RPD
RPD Qual
Copper
ug/L
ND
500
500
504
506
101
101
70-130
0
20
Lead
ug/L
ND
500
500
488
490
98
98
70-130
0
20
Nickel
ug/L
ND
500
500
497
500
99
100
70-130
1
20
Selenium
ug/L
ND
500
500
500
502
100
100
70-130
0
20
Silver
ug/L
ND
250
250
247
246
99
99
70-130
0
20
Thallium
ug/L
ND
500
500
475
482
95
96
70-130
2
20
Zinc
ug/L
ND
500
500
477
481
95
96
70-130
1
20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2769326
2769327
MS
MSD
92457888003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
466
494
93
98
70-130
6
20
Arsenic
ug/L
ND
500
500
473
485
95
97
70-130
2
20
„ Beryllium
ug/L
ND
500
500
521
540
104
108
70-130
4
20
Cadmium
ug/L
ND
500
500
493
517
99
103
70-130
5
20
Chromium
ug/L
ND
500
500
504
524
100
104
70-130
4
20
Copper
ug/L
11.4
500
500
510
534
100
104
70-130
4
20
Lead
ug/L
ND
500
500
470
494
93
98
70-130
5
20
Nickel
ug/L
ND
500
500
476
497
95
99
70-130
4
20
Selenium
ug/L
ND
500
500
490
508
98
102
70-130
4
20
Silver
ug/L
ND
250
250
239
250
95
100
70-130
4
20
Thallium
ug/L
ND
500
500
454
480
91
96
70-130
5
20
Zinc
ug/L
71.1
500
500
529
553
92
96
70-130
4
20
Results presentee on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/03/2020 10:24 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 29

aceAnalytical
waw.pacelabs.cole
QUALITY CONTROL DATA
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
QC Batch: 516054 Analysis Method: EPA 624.1
QC Batch Method: EPA 624.1 Analysis Description: 624 MSV with Acrolein
Associated Lab Samples: 92457901001
METHOD BLANK: 2765145
Associated Lab Samples: 92457901001
Parameter
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,2-Dichloroethane
1,2-Dichloropropane
2-Chloroethylvinyl ether
Acrolein
Acrylonitrile
Benzene
Bromod ichloromelhane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,3-Dichloropropene
Di tiro mochl orometha ne
Ethylbenzene
Methylene Chloride
„Tetrachloroethene
Toluene
trans-1,2-Dichloroethane
trans-1,3-Dichloropropene
IlTrichloroethene
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Matrix: Water
Units
Blank
Result
Reporting
Limit
MOIL
Analyzed
ug/L
NO
2.0
0.35
12/20/19 14:39
ug/L
NO
2.0
0.34
12/2011914:39
ug/L
NO
2.0
0.31
12/20/19 14:39
ug/L
ND
2.0
0,51
12/20/19 14:39
uglL
NO
2.0
0.34
12/20119 14:39
ug/L
ND
2.0
0.27
12/20/19 14:39
ug/L
NO
5.0
0.73
12/20/19 14:39
ug/L
NO
5.0
3.8
12/20/19 14:39
ug/L
NO
5.0
1.5
12/20/19 14:39
ug/L
NO
1.0
0.38
12/20/19 14:39
ug/L
NO
2.0
0.24
12/20/19 14:39
ug/L
NO
2.0
0.40
12/2011914:39
ug/L
ND
2.0
1.2
12/20/19 14:39
ug/L
NO
2.0
0.29
12/20/19 14:39
ug/L
NO
2.0
0.37
12/20/19 14:39
ug/L
NO
2.0
1.4
12/20/19 14:39
ug/L
NO
2.0
0.58
12/20/1914*39
ug/L
NO
2.0
0.73
12/20/19 14:39
ug/L
NO
2.0
0.33
12/2011914:39
ug/L
ND
2.0
0,32
12/20/19 14:39
ug/L
NO
1.0
0.28
12/20/19 14:39
ug/L
NO
2.0
0.24
12/2011914:39
ug/L
NO
2.0
0.28
12/20/19 14:39
ug/L
NO
1.0
0.44
12/20/1914*39
ug/L
NO
2.0
0.42
12/20/1914*39
ug/L
NO
2.0
0.41
12/20/1914:39
ug/L
NO
2.0
0.36
12/20/19 14:39
ug/L
NO
2.0
0.72
12/20/19 14:39
e/
100
70-130
12/20/1914:39
e/
95
70-130
12/20/19 14:39
98
70-130
12/20/19 14:39
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Qualifiers
LABORATORY CONTROL SAMPLE:
2765146
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
%Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug1L
20
20.6
103
70-130
1, 1,2,2-Tetrachloroethane
ug/L
20
19.7
99
60-140
.1, 1,2-Trichloroethane
ug/L
20
21.3
107
70-130
8,1-Dichloroethane
ug/L
20
19.9
100
70-130
1,2-Dichloroethane
ug/L
20
19.4
97
49-155
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproducer, except in full,
Date: 01/03/2020 10:24 AM without the written consent of PaceAnalytical Services, L-C. Page 14 of 29

aceAnalytical
www.pacelcbs.com
Project: Newton Instruments/ 1912
, Pace Project No.: 92457901
LABORATORY CONTROL SAMPLE: 2765146
Parameter
Units
J
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Spike LCS LCS %Rec
Conc. Result %Rec Limits Qualifiers
1,2-Dichloropropane
ug/L
20
21.0
105
35-165
2-Chloroethylvinyl ether
ug/L
40
41.2
103
1-225
Acrolein
ug/L
100
206
206
60-1401H,L1
Acrylonitrile
ug/L
100
96.8
97
60-140
Benzene
ug/L
20
19.8
99
65-135
Bromodichloromethane
uglL
20
20.2
101
65-135
Bromoform
ug/L
20
20.3
101
70-130
Bromomethane
ug/L
20
24.4
122
15-185
Carbon tetrachloride
ug/L
20
21.3
106
70-130
Chlorobenzene
ug/L
20
20.5
102
65-135
Chloroethane
ug/L
20
22.1
110
40-160
Chloroform
uglL
20
19.7
99
70-135
Chloromethane
ug/L
20
16.4
82
1-205
'. cis-1,3-Dichloropropene
ug/L
20
20.6
103
25-175
Dibromochloromethane
ug/L
20
19.4
97
70-135
Ethylbenzene
ug/L
20
20.3
101
60-140
Methylene Chloride
uglL
20
20A
102
60-140
Tetrachloroethene
ug/L
20
19.5
97
70-130
Toluene
ug/L
20
19.9
99
70-130
trans-1,2-Dichloroethane
ug/L
20
20.1
101
70-130
trans-1,3-Dichloropropene
ug/L
20
21.2
106
50-150
Trichloroethene
ug/L
20
20.1
101
65-135
Vinyl chloride
uglL
20
17.9
89
5-195
'.1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2765147
MS
92457901001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2765148
MS
Result
MSD
Result
MS
a/ Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD Qual
-1,1,1-Trichloroelhane
ug/L
NO
20
20
22.7
20.4
113
102
52-162
11
36
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.6
22.1
108
110
46-157
2
61
1,1,2-Trichloroelhane
ug/L
ND
20
20
23.8
22.9
119
115
52-150
4
45
1,1-Dichloroethane
ug/L
ND
20
20
23.0
21.2
115
106
59-155
8
40
1,2-Dichloroethane
ug/L
ND
20
20
19.8
20.9
99
104
49-155
5
49
1,2-Dichloropropane
ug1L
NO
20
20
23.4
23.2
117
116
1-210
1
55
'2-Chloroethylvinyl ether
uglL
NO
40
40
45.5
45.1
114
113
1-305
1
71
Acrolein
ug/L
NO
100
100
224
209
224
209
40-160
7
60 MO
Acrylonitrile
ug/L
ND
100
100
104
100
104
100
40-160
4
60
Benzene
ug/L
NO
20
20
23.1
22.2
115
111
37-151
4
61
Bromodichloromethane
ug/L
NO
20
20
23.6
22.7
118
114
35-155
4
56
Bromoform
ug/L
NO
20
20
22.3
22.3
111
111
45-169
0
42
Bromomethane
ug/L
NO
20
20
26.2
23.7
131
119
1-242
10
61
Carbon tetrachloride
ug/L
NO
20
20
25.8
23.7
129
119
70-140
8
41
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/03/2020 10:24 AM without the written consent of Pace Analytical Services, U.C. Page 15 of 29

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2765147
2765148
MS
MSD
92457901001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Dual
Chlorobenzene
ug/L
ND
20
20
22.9
22.8
114
114
37-160
1
53
Chloroethane
ug/L
ND
20
20
14.0
21.7
70
108
14-230
43
78
Chloroform
ug/L
ND
20
20
21.5
20.7
108
103
51-138
4
54
�Chloromethane
ug/L
ND
20
20
14.8
14.6
74
73
1-273
2
60
cis-1,3-Dichloropropene
ug/L
ND
20
20
23.8
24.0
119
120
1-227
1
58
Dibromochloromethane
ug/L
ND
20
20
22.4
22.8
112
114
53-149
2
50
Ethylbenzene
ug/L
ND
20
20
23.1
23.2
115
116
37-162
0
63
Methylene Chloride
ug/L
ND
20
20
22.6
21.2
113
106
1-221
6
28
Tetrachloroethene
ug/L
ND
20
20
22.1
22.7
111
113
64-148
3
39
Toluene
ug/L
ND
20
20
23.1
22.6
115
113
47-150
2
41
trans- 1,2-Dichloroethene
ug/L
ND
20
20
22.7
20.7
114
103
54-156
9
45
Ira ns-1,3-Dichi oropropene
ug/L
ND
20
20
23.6
22.8
118
114
17-183
3
86
Trichloroethene
ug/L
ND
20
20
23.5
22.4
117
112
70-157
5
48
Vinyl chloride
ug/L
ND
20
20
19.9
17.2
100
86
1-251
14
66
1,2-Dichloroethane-d4 (S)
%
98
94
70-130
4-BromoBuorobenzene (S)
%
98
97
70-130
Toluene-d8 (S)
%
105
103
70-130
Results presentee on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
,I This report shall not be reproduced, except in full,
Date: 01/03/2020 10:24 AM without the written consent of Pace Analytical Services, L-C.
Page 16 of 29

aceAnalytical e
rrr.pacelabs.cola
QUALITY CONTROL DATA
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
QC Batch: 516284
Analysis
Method:
EPA608.3
QC Batch Method: EPA 608.3
Analysis
Description:
608 PCB Pest Red Vol
Associated Lab Samples: 92457901001
METHOD BLANK: 2766175
Associated Lab Samples: 92457901001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
4,4'-DDD
ug/L
NO
0.050
0.0069
12/23/19 18:48
4,4'-DDE
ug/L
NO
0.050
0.0064
12/23/19 18:48
4,4'-DDT
ug/L
NO
0.050
0.018
12/2311918:48
Aldrin
ug/L
NO
0.050
0,022
12/23/19 18:48
l alpha-BHC
ug/L
NO
0.050
0.019
1212311918:48
alpha -Chlordane
ug/L
NO
0.050
0.0090
12/23/191848
beta-BHC
ug/L
NO
0.050
0.014
12123/191848
Chlordane (Technical)
ug/L
NO
0.50
0.20
12/23/19 18.48
delta-BHC
ug/L
NO
0.050
0.020
12/23/19 18:48
Dieldrin
ug/L
NO
0.050
0.0073
12/23/19 18:48
Endosulfan I
ug/L
NO
0.050
0.0094
12/23/19 1848
Endosulfan II
ug/L
NO
0.050
0.0065
12/23/19 18:48
Endosulfan sulfate
ug/L
NO
0.050
0.0091
12/23/19 18:48
Endrin
ug/L
NO
0.050
0.0089
12/23/1918:48
Endrin aldehyde
ug/L
NO
0.050
0.013
12/23/19 18:48
gamma-BHC (Lindane)
ug/L
ND
0.050
0.012
12/23/19 18:48
gamma -Chlordane
ug/L
NO
0.050
0,017
12/23/19 18:48
,Heptachlor
ug/L
NO
0.050
0.016
12/23/19 18:48
Heptachlor epoxide
ug/L
NO
0.050
0.0097
12/23/19 18:48
PCB-1016 (Aroclor 1016)
ug/L
NO
0.50
0.22
12/23119 18:48
PCB-1221 (Aroclor 1221)
ug/L
NO
0.50
0.32
12/23/19 18:48
PCB-1232 (Aroclor 1232)
ug/L
NO
0.50
0.21
12123/19 1848
PCB-1242 (Aroclor 1242)
ug/L
NO
0.50
0.44
12/23/19 18:48
,PCB-1248 (Aroclor 1248)
ug/L
NO
0.50
0.34
12/23/19 18:48
PCB-1254 (Aroclor 1254)
ug/L
NO
0.50
0.24
12/23/19 18:48
PCB-1260 (Aroclor 1260)
ug/L
NO
0.50
0.30
12/23/19 18:48
Toxaphene
ug/L
NO
0.50
0.20
12/2311918:48
Decachlorobiphenyl (S)
%
118
10-130
12/23/19 18:48
Tetrachloro-m-xylene (S)
%
76
10-130
12/23/19 18:48
Qualifiers
LABORATORY CONTROL SAMPLE:
2766176
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
%Rec
Limits Qualifiers
4,4'-DDD
ug/L
0.25
0.28
112
31-141
4,4'-DDE
ug/L
0.25
0.26
104
30-145
4,4'-DDT
ug/L
0.25
0.29
117
25-160
Aldrin
ug/L
0.25
0.22
87
42-140
alpha-BHC
ug/L
0.25
0.24
94
37-140
alpha -Chlordane
ug/L
0.25
0.24
97
45-140
beta-BHC
ug/L
0.25
0.29
115
17-147
Results presented on this page are in the units indicated by Me "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 01/03/2020 10:24 AM without the written consent of Pace Analytical Services, L-C. Page 17 of 29

aceAnalytical "
shho pacelaEs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
LABORATORY CONTROL SAMPLE:
2766176
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
%Rec
Limits
Qualifiers
delta-BHC
ug/L
0.25
0.22
87
19-140
Dieldrin
ug/L
0.25
0.24
97
36-146
Entlosulfan 1
ug/L
0.25
0.24
96
45-153
Entlosulfan ll
ug/L
0.25
0.25
101
1-202
Entlosulfan sulfate
ug/L
0.25
0.28
110
26-144
Endrin
Ug/L
0.25
0.25
101
30-147
Endrin aldehyde
ug/L
0.25
0.25
99
50-150
, gamma-BHC (Lindane)
ug/L
0.25
0.25
100
32-140
gamma -Chlordane
ug/L
0.25
0.17
67
45-140
Heptachlor
ug/L
0.25
0.22
89
34-140
Heptachlor epoxide
ug/L
0.25
0.22
89
37-142
Decachlorobiphenyl(S)
%
144
10-130
SO
Tetrachloro-m-xylene (S)
%
96
10-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2766177
2766178
MS
MSD
92457784001
Spike
Spike
MS
MSD
MS MSD
%Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD
RPD Qua]
4,4'-DDD
ug/L
ND
0,25
0.25
0,24
0.24
96
95
31-141
1
39
:, 4,4'-DDE
ug/L
ND
0.25
0.25
0.23
0.22
94
89
30-145
5
35
4,4'-DDT
ug/L
ND
0.25
0.25
0.24
0.25
95
99
25-160
4
42
Aldrin
ug/L
ND
0.25
0.25
0.16
0.13
63
52
42-140
20
35
I alpha-BHC
uglL
NO
0.25
0.25
0.19
0.20
78
80
37-140
2
36
alpha -Chlordane
ug/L
NO
0.25
0.25
0.21
0.21
86
85
45-140
1
35
beta-BHC
ug/L
ND
0.25
0.25
0.25
0.26
100
103
17-147
3
44
delta-BHC
ug/L
ND
0,25
0.25
0.19
0.19
77
78
19-140
1
52
Dieldrin
ug/L
ND
0.25
0.25
0.21
0.21
84
84
36-146
1
49
Entlosulfan I
ug/L
ND
0.25
0.25
0.21
0.21
82
82
45-153
0
28
,Entlosulfan II
ug/L
ND
0.25
0.25
0.21
0.22
85
86
1-202
1
53
Entlosulfan sulfate
uglL
NO
0.25
0.25
0.23
0.23
92
92
26-144
1
38
Endrin
ug/L
ND
0.25
0.25
0.21
0.21
84
85
30-147
1
48
Endrin aldehyde
ug/L
ND
0.25
0.25
0.26
0.28
86
91
50-150
5
30
gamma-BHC (Lindane)
ug/L
ND
0.25
0.25
0.21
0.21
83
84
32-140
2
39
gamma -Chlordane
ug/L
ND
0.25
0.25
0,15
0.17
59
67
45-140
13
35
Heptachlor
ug/L
ND
0.25
0.25
OA7
0.15
70
61
34-140
14
43
Heptachlor epoxide
ug/L
ND
0.25
0.25
0.20
0.20
79
80
37-142
1
26
Decachlorobiphenyl(S)
%
101
100
10-130
Tetrachloro-m-xylene (S)
%
76
70
10-130
Results presented on this page are In the units Indicated by the 'Units" column except where an alternate unit is presented to the right of the result.
Date: 01/03/2020 10:24 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, -I-C.
Page 18 of 29

aceAnalytical o
www.pacelabs.com
QUALITY CONTROL DATA
Project: Nevvton Instruments/ 1912
Pace Project No.: 92457901
" OC Batch: 516430
QC Batch Method: EPA 625A
Associated Lab Samples: 92457901001
Analysis Method:
Analysis Description:
EPA 625.1
625 MSS
METHOD BLANK: 2766956
Matrix: Water
Associated Lab Samples: 92457901001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
ug/L
NO
5.0
0.98
12/30/19 11:32
1,2-Dichlorobenzene
ug/L
NO
5.0
0.88
12/30/19 11:32
1,2-Diphenylhydrazine
ug/L
NO
5.0
0.90
12/30/19 11:32
1,3-Dichlorobenzene
ug/L
NO
5.0
0.81
12/30/19 11:32
1,4-Dichlorobenzene
ug/L
NO
5.0
0.95
12/30/19 11:32
2,4,6-Trichlorophenol
ug/L
ND
10.0
1.3
12/30/19 11:32
2,4-Dichlorophenol
ug/L
ND
5.0
1.7
12/30/19 11:32
2,4-Dimethylphenol
ug/L
NO
10.0
1.2
12/30/19 11:32
2,4-Dinitrophenol
ug/L
NO
50.0
9.0
12/30/19 11:32
2,4-Dinitrotoluene
ug/L
NO
5.0
0.90
12/30/19 11:32
2,6-Dinitrotoluene
ug/L
NO
5.0
0.98
12/30/19 11:32
2-Chloronaphthalene
ug/L
NO
5.0
0.98
12/30/19 11:32
2-Chlorophenol
ug/L
NO
5.0
1.3
12/30/19 11:32
2-Nitrophenol
ug/L
NO
5.0
0.91
12/30119 11:32
3,3'-Dichlorobenzidine
ug/L
NO
25.0
2.1
12/30/1911:32
4,6-Dinitro-2-methylphenol
ug/L
NO
20.0
2.6
12/30/19 11:32
" 4-Bromophenylphenyl ether
ug/L
NO
5.0
0.82
12/30/19 11:32
4-Chloro-3-methylphenol
ug/L
NO
5.0
3.7
12/30/19 11:32
4-Chlorophenylphenyl ether
ug/L
NO
5.0
0,87
12/30/19 11:32
4-Nitrophenol
ug/L
NO
50.0
4.1
1213011911:32
Acenaphthene
ug/L
ND
5.0
0.25
12/30/1911:32
Acenaphthylene
ug/L
NO
5.0
0.21
12/30/1911:32
Anthracene
ug/L
NO
5.0
0.14
12/30/19 11:32
Benzidine
ug/L
NO
50.0
5.1
12/30/1911:32
Benzo(a)anthracene
ug/L
ND
5.0
0.33
12/30/19 11:32
Benzo(a)pyrene
ug/L
ND
5.0
0.30
12/30119 11:32
Benzo(b)fluoranthene
ug1L
NO
5.0
0.28
12130/1911:32
Benzo(g.h,i)perylene
ug/L
NO
5.0
0.38
12/30/19 11:32
Benzo(k)fluoranthene
ug/L
NO
5.0
0.43
12/30/19 11:32
, bis(2-Chloroethoxy)methane
ug/L
NO
10.0
0,92
12/30/19 11:32
'bis(2-Chloroethyl) ether
ug/L
NO
5.0
1.0
12/30/19 11:32
bis(2-Ethylhexypphthalate
ug/L
NO
5.0
0.79
12/30/19 11:32
Butylbenzylphthalate
ug/L
NO
5.0
0.79
12/30/19 11:32
Chrysene
ug/L
NO
5.0
0.21
12/30/19 11:32
Di-n-butylphthalate
ug/L
NO
5.0
0.75
12/30/19 11:32
Di-n-octylphthalate
ug/L
NO
5.0
0.66
12130/1911:32
Dibenz(a,h)anthracene
ug/L
NO
5.0
0.55
12/30/19 11:32
Diethylphthalate
ug/L
NO
5.0
0.58
12/30119 11:32
`. Dimethylphthalate
ug/L
NO
5.0
0.76
1213011911:32
l Fluoranthene
ug/L
NO
5.0
0.21
12/30/19 11:32
Fluorene
ug/L
NO
5.0
0.21
12/30/19 11:32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 01103/2020 10:24 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 29

aceAnalytical
imns pecrtabs.cdrt
QUALITY CONTROL DATA
Project: Newton Instruments/ 1912
Pace Project No.: 92457901 -
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
METHOD BLANK: 2766956
Associated Lab Samples: 92457901001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
Hexachloro-1,3-butadiene
ug/L
NO
5.0
0.94
12130/19 11:32
Hexachlorobenzene
ug/L
NO
5.0
0.72
12/30/19 11:32
Hexachlorocyclopentadiene
ug/L
NO
10.0
0.88
12/30/19 11:32
Hexachloroethane
ug/L
NO
5.0
1.1
12/30/19 11:32
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
0.29
12/30/19 11:32
Isophorone
ug/L
ND
10.0
0.89
12/3011911:32
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
0.99
12/3011911:32
N-Nilrosodimethylamine
ug/L
NO
5.0
0.91
12/3011911:32
N-Nitrosodiphenylamine
ug/L
ND
10.0
1.0
12/30/19 11:32
Naphthalene
ug/L
NO
5.0
0.34
12/30/1911:32
Nitrobenzene
ug/L
ND
5.0
1.1
12/30/19 11:32
Pentachlorophenol
ug/L
ND
10.0
4.6
12/30/19 11:32
Phenanthrene
ug/L
ND
5.0
0.22
12/30/19 11:32
Phenol
ug/L
ND
5.0
1.9
12/30/19 11:32
Pyrene
ug/L
NO
5.0
0.19
12/3011911:32
2,4,6-Tribromophenol(S)
%
35
10-137
12/30/19 11:32
2-Fluorobiphenyl (S)
%
58
15-120
12/30/19 11:32
2-Fluorophenol(S)
%
33
10-120
12/30/19 11:32
'Nitrobenzene-d5(S)
%
64
10-120
12/30/19 11:32
Phenol-d6 (S)
%
43
10-120
12/30/19 11:32
Terphenyl-dl4 (S)
%
73
11-131
12/30/19 11:32
LABORATORY CONTROL SAMPLE:
2766957
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
%Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
35.3
71
44-142
1,2-Dichlorobenzene
ug/L
50
36.6
73
32-129
1,2-Diphenylhydrazine
ug/L
50
52.4
105
25-150
1,3-Dichlorobenzene
ug/L
50
35.9
72
1-172
1 4-Dichlorobenzene
ug/L
50
35.9
72
20-124
2,4,6-Trichlorophenol
ug/L
50
39.0
78
37-144
12,4-Dichlorophenol
ug/L
50
37.7
75
39-135
2,4-Dimethylphenol
ug/L
50
41.9
84
32-120
2,4-Dinitrophenol
ug/L
250
196
78
1-191
2,4-Dinitrotoluene
ug/L
50
42.5
85
39-139
2,6-Dinitrotoluene
ug/L
50
43.5
87
50-158
2-Chloronaphthalene
ug/L
50
39.1
78
60-120
2-Chlorophenol
ug/L
50
37.2
74
23-134
2-Nitrophenol
ug/L
50
36.7
73
29-181
3,3'-Dichlorobenzidine
ug/L
100
9.61
10
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
88.9
89
1-181
4-Bromophenylphenyl ether
ug/L
50
39.3
79
53-127
4-Chloro-3-methylphenol
ug/L
100
87.5
87
22-147
4-Chlorophenylphenyl ether
ug/L
50
39.8
80
25-158
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Dale: 01/03/2020 10:24 AM without the written consent of Pace Analytical Services, LLC.
Page 20 of 29

to
aceAnalytical
w tmen ci lahs.cone
QUALITY CONTROL DATA
Pace Analytical Services, LLC
ga00 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments/ 1912
ii Pace Project No.: 92457901
LABORATORY CONTROL SAMPLE:
2766957
Spike
LCS
LCS
%Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
4-Nitrophenol
ug/L
250
214
86
1-132
Acenaphthene
ug/L
50
43.5
87
47-145
Acenaphthylene
ug/L
50
43.7
87
33-145
Anthracene
uglL
50
43.3
87
27-133
Benzidine
ug/L
100
NO
2
25-150 L2
Benzo(a)anthracene
ug/L
50
44.2
88
33-143
Benzo(a)pyrene
ug/L
50
49.2
98
17-163
Benzo(b)fluoranlhene
ug/L
50
49.0
98
24-159
. Benzo(g,h,i)perylene
ug/L
50
56.8
114
1-219
'- Benzo(k)fluoranthene
ug/L
50
50.8
102
11-162
bis(2-Chloroethoxy)methane
ug/L
50
41.0
82
33-184
bis(2-Chloroelhyl) ether
ug/L
50
41.4
83
12-158
bis(2-Ethylhexypphthalate
uglL
50
46.3
93
8-158
Butylbenzylphthalate
ug/L
50
44.9
90
1-152
Chrysene
ug/L
50
45.0
90
17-168
Di-n-butylphthalate
ug/L
50
45.0
90
1-120
Di-n-octylphthalate
ug/L
50
47.6
95
4-146
Dibenz(a,h)anthracene
ug/L
50
58.6
117
1-227
Diethylphthalate
ug/L
50
41.5
83
1-120
Dimethylphthalate
uglL
50
42.2
84
1-120
Fluoranthene
ug/L
50
46.6
93
26-137
"Fluorene
ug/L
50
43.2
86
59-121
�Hexachloro-1,3-butadiene
ug/L
50
34.1
68
24-120
„ Hexachlorobenzene
ug/L
50
39.5
79
1-152
Hexachlorocyclopentadiene
ug/L
50
33.6
67
25-150
Hexachloroethane
ug/L
50
38.4
77
40-120
Indeno(1,2,3-ed)pyrene
uglL
50
55.2
110
1-171
Isophorone
ug/L
50
45.0
90
21-196
N-Nitroso-di-n-propylamine
ug/L
50
47.3
95
1-230
N-Nitrosodimethylamine
ug/L
50
33.7
67
25-150
N-Nitrosodiphenylamine
ug/L
50
38.3
77
25-150
Naphthalene
ug/L
50
41.1
82
21-133
Nitrobenzene
ug/L
50
43.1
86
35-180
Pentachlorophenol
uglL
100
71.1
71
14-176
Phenanthrene
ug/L
50
45.4
91
54-120
Phenol
ug/L
50
37.9
76
5-120
Pyrene
ug/L
50
46.8
94
52-120
2.4,6-Tribromophenol(S)
%
81
10-137
2-Fluorobiphenyl (S)
%
80
15-120
i2-Fluorophenol(S)
%
74
10-120
•Nitrobenzene-d5(S)
%
85
10-120
`Phenol-d6 (S)
%
81
10-120
Terphenyl-d14 (S)
%
79
11-131
Results presented on this page are in the units Indicated by fine "Units" column except where an alternate unit is presented to the fight of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/03/2020 10:24 AM without the written consent of Pace Analytical Services, -LC. Page 21 of 29

aceAnalyfical
www.pacelabs.cola
QUALITY CONTROL DATA
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2766958 2766959
MS MSD
35519145001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,2-Diphenylhydrazine
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphlhalene
2-Chlorophenol
2-Nitrophenol
3, 3'-Di chlorobenzid i ne
4,6-D initro-2-methyl phenol
4-Bromophenylphenyl ether
4-Chl oro-3-methyl phen of
4-Chlorophenylphenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzidine
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)Fluoranthene
Benzo(g,h,i)perylene
Benzo(k) fl uoranthene
bis(2-
C hloroethoxy)methane
bis(2-Chloroethyl) ether
bis (2-Ethylhexyl)phthal ate
Butylbenzylphthalate
Chrysene
IDi-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Diethylphthalate
Dimelhylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocycl opentadiene
Hexachloroethane
ug/L
0.96U
100
100
53.6
24.8
54
25
44-142
73
50 M1,R1
ug/L
0.86U
100
100
58.3
24.0
58
24
32-129
83
30 M1,R1
ug/L
0.88U
100
100
84.7
71.7
85
72
25-150
17
30
ug/L
0.79U
100
100
56.9
23.5
57
24
1-172
83
30 R1
ug/L
0.93U
100
100
56.7
23A
57
23
20-124
83
30 R1
ug/L
1.31.1
100
100
71.8
52.6
72
53
37-144
31
58
ug/L
1.7U
100
100
61.2
39.9
61
40
39-135
42
50
ug/L
1.2U
100
100
30.6
28.1
31
28
32-120
9
58 M1
ug/L
8.8U
500
500
349
267
70
53
1-191
27
132
ug/L
0.881-1
100
100
75.7
60.7
76
61
39-139
22
42
ug/L
0.96U
100
100
77.2
60.2
77
60
50-158
25
48
ug/L
0.96U
100
100
65.2
43.4
65
43
60-120
40
24 M1,R1
ug/L
1.3U
100
100
63.0
26.5
63
27
23-134
81
61 R1
ug/L
0.89U
100
100
63.0
29.6
63
30
29-182
72
55 R1
ug/L
2.11.1
200
200
ND
33.5J
0
17
1-262
108 M7
ug/L
2.5U
200
200
154
130
77
65
1-181
17
30
ug/L
0.80U
100
100
66.3
52.3
66
52
53-127
24
43 M7
ug/L
3.6U
200
200
141
109
71
54
22-147
26
73
ug/L
0.85U
100
100
68.9
51.3
69
51
25-158
29
61
ug/L
4.OU
500
500
243
172
49
34
1-132
34
131
ug/L
0.25U
100
100
73.1
53.8
73
54
47-145
30
48
ug/L
0.21 U
100
100
76.8
56.8
77
57
33-145
30
74
ug/L
0.14U
100
100
68.9
58.4
69
58
27-133
17
66
ug/L
5.0U
200
200
ND
ND
0
0
25-150
30 MO
ug/L
0.32U
100
100
77.9
66.0
78
66
33-143
17
53
ug/L
0.29U
100
100
70.5
61.4
71
61
17-163
14
72
ug/L
0.27U
100
100
83.4
68.0
83
68
24-159
20
71
ug/L
0.37U
100
100
101
81.3
101
81
1-219
21
97
ug/L
0.42U
100
100
84.9
69.1
85
69
11-162
20
63
ug/L
0.90U
100
100
67.2
35Y
67
36
33-184
61
54 R1
ug/L
0.981-1
100
100
74.5
31.0
74
31
12-158
83
108
ug/L
0.77U
100
100
93.7
67.8
94
68
8-158
32
82
ug/L
0.77U
100
100
76.2
63.7
76
64
1-152
18
60
ug/L
0.21U
100
100
81.5
68.5
82
69
17-168
17
87
ug/L
0.74U
100
100
78.4
64.0
78
64
1-120
20
47
ug/L
0.65U
100
100
85.1
71.2
85
71
4-146
18
69
ug/L
0.54U
100
100
98.1
81.4
98
81
1-227
19
126
ug/L
0.57U
100
100
73.9
59.0
74
59
1-120
22
100
ug/L
0.75U
100
100
76.5
59.9
76
60
1-120
24
183
ug/L
0.21U
100
100
84.9
70.1
85
70
26-137
19
66
ug/L
0.21U
100
100
76.0
57.7
76
58
59-121
27
38
M1
ug/L
0.92U
100
100
49.9
21 4
50
21
24-120
80
62
M1,R1
ug/L
0.71U
100
100
66.9
52.2
67
52
1-152
25
55
ug/L
0.86U
100
100
48.3
21.4
48
21
25-150
77
30
M1,R1
ug/L
1AU
100
100
58.5
24.3
59
24
40-120
83
52
M1,R1
Results presentee on this page am In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/03/2020 10:24 AM without the written consent of Pace Analytical Services, L-C. Page 22 of 29

aceAnalytical e
www.pcslabn.cara
QUALITY CONTROL DATA
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 2766958
2766959
MS
MSD
35519145001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Cone.
Result
Result
%Rec
%Rec
Limits
RPD
RPD
Qual
�. Indeno(1,2,3-cd)pyrene
ug/L
0.28U
100
100
95.9
77.8
96
78
1-171
21
99
Isophorone
ug/L
0.87U
100
100
72.6
42.8
73
43
21-196
52
93
N-Nitroso-di-n-propylamine
ug/L
0.971-1
100
100
78.6
39.0
79
39
1-230
67
87
N-Nitrosodimethylamine
ug/L
0.891-1
100
100
49.9
17.9
50
18
25-150
94
30
M1,R1
N-Nitrosodiphenylamine
ug/L
0.981-1
100
100
69.0
61.2
69
61
25-150
12
30
Naphthalene
ug/L
0.331.1
100
100
66.3
31.5
66
31
21-133
71
65
R1
Nitrobenzene
ug/L
1.1U
100
100
74.8
34.5
75
35
35-180
74
62
R1
Pentachlorophenol
ug/L
4.5U
200
200
113
94.6
57
47
14-176
18
86
Phenanthrene
ug/L
0.22U
100
100
81.4
66.3
81
66
54-120
20
39
Phenol
ug/L
1.91.1
100
100
39.3
17.1
39
17
5-120
79
64
R1
" Pyrene
ug/L
0.19U
100
100
79.6
67.1
80
67
52-120
17
49
2,4,6-Tribromophenol(S)
%
77
61
10-137
2-Fluorobiphenyl(S)
%
73
46
15-120
2-Fluorophenol(S)
%
53
19
10-120
Nitrobenzene-d5(S)
%
77
35
10-120
Phenol-d6(S)
%
43
18
10-120
Terphenyl-d 14(S)
%
60
47
11-131
Results presented on this page arc in the units indicated by the "Units" column except where an altemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 01/03/2020 10:24 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 29

0
aceAnalytical
wom pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
QC Batch: 516524
Analysis Method: EPA 420.4 Rev 1.0 1993
OC Batch Method: EPA 420.4 Rev 1.0 1993
Analysis Description: 420.4 Phenolics
Associated Lab Samples: 92457901001
METHOD BLANK: 2767422
Matrix: Water
Associated Lab Samples: 92457901001
Blank Reporting
Parameter Units
Result Limit
MDL Analyzed
Qualifiers
Phenol mg/L
NO 0.020
0.0050 12/24/1911:38
LABORATORY CONTROL SAMPLE: 2767423
Spike LCS
LCS %Rec
Parameter Units
Cone. Result
n/ Rec Limits Qualifiers
Phenol mg/L
0.05 0.050
100 90-110
' MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2767426 2767427
MS MSD
92457900001
Spike Spike MS
MSD MS MSD
%Rec
Max
Parameter Units Result
Cone. Cone. Result
Result %Rec %Rec
Limits RPD
RPD Qual
p Phenol mg/L 0.052
0.05 0.05 0.096
0.097 89 90
90-110 1
10 101
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2767473 2767474
MS MSD
92457560002
Spike Spike MS
MSD MS MSD
% Rec
Max
Parameter Units Result
Cone. Cone. Result
Result %Rec %Rec
Limits RPD
RPD Qual
'Phenol ni NO
0.05 0.05 0.047
0.043 93 86
90-110 8
10 M1
Results presented on this page are in the units indicated by the "units" column except where an alternate unit Is presentee to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/03/2020 10:24 AM without the written consent of Pace Analytical Services, LLC.
Page 24 of 29

aceAnalyticai
imrsigaalabt.cola
QUALITY CONTROL DATA
I Project: Newton Instruments/ 1912
Pace Project No.: 92457901
QC Batch: 516194 Analysis Method: SM 4500-CN-E-2011
QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 4500CNE Cyanide, Total -
Associated Lab Samples: 92457901001
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HuntersAlle, NC 28078
[phone]
METHOD BLANK: 2765934 Matrix: Water
Associated Lab Samples: 92457901001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Cyanide mg/L NO 0.0080 0.0060 12/22/1911:09
LABORATORY CONTROL SAMPLE: 2765935
Spike LCS LCS %Rec
Parameter Units Cone. Result %Rec Limits Qualifiers
Cyanide mg/L 0.1 0.12 117 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2765936 2765937
MS MSD
92458344005 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Cone. Cone. Result Result e/ Rec %Rec Limits RPD RPD Qual
„Cyanide mg/L 0.030 0.1 0.1 OA2 0.10 86 70 80-120 14 10 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2765938
2765939
MS
MSD
92457868008 Spike
Spike
MS
MSD
MS MSD
%Rec
Max
Parameter Units Result Cone.
Cone,
Result
Result
%Rec %Rec
Limits
RPD RPD Qual
Cyanide mg1L 6.OJ uglL 0.1
0.1
0.12
0.12
109 109
80-120
0 10
Results presented on this page am in the units indicated by the "Units" column except where an alternate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/03/202010:24 AM without the written consent of Pace Analytical Services,LLC.
Page 25 of 29

laceAnalyficii
w",pacslablixort
i
QUALIFIERS
Project: Newton Instruments/ 1912
Pace Project No.: 92457901
DEFINITIONS
Pace Analytical Services, Li
9800 Kincey Ave. Suite 100
Hunlersville, 128078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
POL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate h recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.
L1 Analyle recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
Mo Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
Ml Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R7 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/03/2020 10:24 AM without the written consent of Pace Analytical Services, LLC.
Page 26 of 29

aceAnalytical
I wrw.pacehhs.cwe
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Project:
Pace Project No.:
Newton Instruments/ 1912
92457901
Analytical
' Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92457901001
Outfall-001
SM 254OD-2011
515738
92457901001
Outfall-001
92457901001
Outfall-001
EPA 16646
517552
92457901001
Ouffall-001
EPA 608.3
516284
EPA 608.3
516435
92457901001
Outfall-001
EPA 200.7 Rev 4.4 1994
517046
EPA 200.7 Rev 4.4 1994
517067
92467901001
Outfall-001
EPA 245.1 Rev 3.0 1994
516307
EPA 245.1 Rev 3.0 1994
516375
92457901001
Outfall-001
EPA625.1
516430
EPA 625.1
517158
92457901001
Outfall-001
EPA 624.1
516054
92457901001
Outfall-001
EPA 420.4 Rev 1.0 1993
516524
EPA 420.4 Rev 1.0 1993
516549
92457901001
Outfall-001
SM 4500-CN-E-2011
516194
SM 4500-CN-E-2011
516213
Date: 01 /03/2020 10:24 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 29

LEGAL
�Piedmont Geologic
a|Request Docunment
same
92457901
17
-ustomer
Project NameiNumner:
State: County/Cjty�. Time Zone Collected:
CT
Phone: is
19)8549700
Sitel#acility ID 9:
Compliance Monitoring?
yes
NA
Collected
By (signature):
Turnaround Date Required:
VC&
Sanple
posal;
Field filtered (if applicable);
oo
Matrix (odes
(Imen in Matrix box below): Drinking Water (DW), Ground Water GW), Wastewater (WW),
—
A.'zext.- si.�
Produa
(P), Soil/Solid (SL), Oil (OL),
Wipe WP), Air (ARI, Tissue ITS), BiwssaV (R),
Vapor IV), Other o7r)
Collected for
Composi te End
Res
Grab
Composite Start)
Cl
Orns
W
ime
'rime
Ur
Customei
Remarks/Special Conditions/ Possible Hazards:
f
TYPeolt� V-,
Y6
H LOS
s OftT.Wo P�ESfN�(
Lab Simple Temperature Info:
The
le.
zi
Preltigm
I'M
page:

6Z 10 6Z a6ed
�_Y/'/1 Document Name: Document Revised: February 7, 2018
/ �,,,. n..,,awr,,.,r' Sam le Condltlon Upon Rocei t(SCUR) Page 1 of 2 j
Q pwM*-bf I Document No.: - Issuing Authority:
FLAB-CS033=Rev.06 Pace Carolinas Quality Office
'Check mark top half of box If pH and/or dechlorinatlon is Project N 1 lo{}
verified and within the acceptance range for preservation W Tl
samples. PM: TIH
Exceptions: VOA Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC, LLHg CLIENT.
"Bottom half of box is to list number of bottle
Due Date: 01/03/20
82—PIED GEOL
3 z z a
a
n a no;�r m
C c C Ca Z<
V
E_ E E
v m rji .Ji I T
a a a a a
z
N
E
a
a
O
Z
a
E
a
m
O
°
E
a
O
)u
a
C
nEE
Q
O
ZL
E
4
`u
O
7ty
G
a
O
v
�
i�.jl
a
<
y`
V
B
99�
Z
EE
d
E
C
2
Z
«E
'^
n
m
O
>
E
u
o>>
<
v
r0�
:1
q
a
E
>
?
O
>
E
U'
a
a
>
E
g>>
Z
Y
us
i
O
'Z
�
d
`
2
rt
E
a
Z
u
wt
E
a
O
s
V
a
E
a
o
J
a
E
0
3
N
E
i
[
J
a
E
2
3
4
5
S
6
9
30
It
12
PH Adjustment Log for Preserved Samples
Sample IO
Type of Preselvativa
pH upon ree¢Ipt
Dampreservation adJusted
Time preserntian
adjusted
Pmount of Preservative
added
Lot Y
I
Note: Whenevar there is a discrepancy affect ing North muna compliance samples, a copV of this farm will ba sent to the North Carolina DDINN Cortitlostian office Il.e.
Out of hold, Incorrect preservative, out of rem p, incorrect containers.