NCG030145_MONITORING INFO_20191220

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/V
DOC TYPE.
❑ HISTORICAL FILE
MONITORING REPORTS
DOC DATE
❑
YYYYMMDD

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGENO. NCG030145 SAMPLE COLLECTION YEAR: 2019
FACILITY NAME: Newton Instruments SAMPLE PERIOD[:] Jan -June❑ July -Dec
COUNTY: Granville or®Monthly' November 2019
PERSON COLLECTING SAMPLES: Nicholas Murphrey �/ DISCHARGING TO CLASS❑ORW®HQW❑Trout❑PNA
LABORATORY:: Pace Analytical Lab Cert. #: 40 ��j V ��Zero-flow❑Water Supply[ —
Comments Comments on sample collection or analysis: Monthly sam;311i g 0 �,,J]Other
DEC PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 34
i�il
Part A: Stormwater Benchmarks and Monitoring Results,NAIR at Cf
❑ No discharge this period?z
Non -Polar
outfall No.
Date Sample
24-hour rainfall
Total Suspended
pH,
Standard
Copper
Lead
Zinc
O&G/ Total
Total Toxic
s
Collected'
amount,
Solids
Petroleum
Organics
(mo/dd/yr)
Inches'
units
Hydrocarbons
Benchmarks ===>
-
-
100 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
001
11/12/19
0.3
29.8 mg/L
7.6
0.0057 mg/L
0.0018 mg/L
0.0400 mg/L
1.3 mg/L
Not Detected
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
ZFor sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan mayso certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
Permit Date: 11/1/2017-10/31/2022 SWU-245, last revised 10/25/2012
Page 1 of 3

stormwater runoff has occurred. since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
(Signature)
(Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging> 55 gal of new oil per month.
❑ No dischar e this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664(SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
-
-
15 mg/L
100 mg/L or 50 mg/L•
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
' See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
Permit Date: il/1/2017-10/31/2022
SWU-245, last revised 10/25/2012
Page 2 of 3

FOR PART AAND. PART B MONITORING RESULTS: - - --
A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL?YES ®NO ❑
IF YES,HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE?YES ® NO ❑
REGIONAL OFFICE CONTACT NAME: John Holley
Mail an oriainal and one copv of this DMIR including all "No Discharge" reports within 30 days of receiptof the lab results for at end of monitoring period in
the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
�/6 9
(Date)
Permit Date: 11/1/2017-10/31/2022 SWU-245, last revised 10/25/2012
Page 3 of 3

aceAnalytical
ww.pacelaba.cem
November 26, 2019
Mr. Pete Dressel
Piedmont Geologic
6003 Chapel Hill Road
Suite 109
Raleigh, NC 27607
RE: Project: Newton Instruments/1912
Pace Project No.: 92453418
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HuntersWle, NC 28078
(704)8759092
Dear Mr. Dressel:
Enclosed are the analytical results for sample(s) received by the laboratory on November 12, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Jonathan Murphrey, Piedmont Geologic
REPORT OF LABORATORY ANALYSIS
This report shall not be repmtluced except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 25

lace Analytical
wimprtelebe.com
Project: Newton Instruments/1912
Pace Project No.: 92453418
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
!'Pace Analytical Services Asheville
CERTIFICATIONS
South Carolina Cedification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
Pace Analytical Services, LLC
9500 Kincey Ave. Suite 100
Huntersvdle, NC 28078
[phone]
2225 Riverside Drive, Asheville. NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification M M-NC030
VirginiaNELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712 .
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633
North Carolina Drinking Water Certification #: 37738 VirginiaNELAP Certification #: 460025
:4al.:4c.12W-1 :Vi_121r_1 WIRIEy
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 25

lace Analytical e
www.Pacelabs.com
Project: Newton Instruments/1912
Pace Project No.: 92453418
Lab ID Sample ID
SAMPLE SUMMARY
Matrix Date Collected Date Received
92453418001 Outfall 001 Water 11/12/1908:30 1111211910:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunteisville, NC 28078
[phone]
Page 3 of 25

m
aceAnalytical
wwer.peceleb.conn
SAMPLE ANALYTE COUNT
Project: Newton Instruments/1912
Pace Project No.: 92453418
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92453418001 Outfall 001 SM 2540D-2011
AMI
1
PASI-E
EPA 1664E
HH
1
PASI-C
EPA 608.3
SEM
29
PASI-C
EPA 200.7 Rev 4.4 1994
DS
12
PASI-A
EPA 245.1 Rev 3.0 1994
SOO
1
PASI-A
EPA625.1
Bpi
62
PASI-C
EPA 420.4 Rev 1.O 1993
KDF1
1
PASI-A
SM 4500-CN-E-2011
DMN
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 25

lace Analytical
rw.psnlebs.com
f_1,r_1ArI[H_i�:aln
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project: Newton Instruments/1912
Pace Project No.: 92453418
Sample: Outfall 001 Lab ID: 92453418001 Collected: 11/12/19 08:30 Received: 11112119 10:50 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua[
2540D Total Suspended Solids Analytical Method: SM 2WD-2011
Total Suspended Solids
29.8
mg/L
4.0
4.0
1
11/1411912:25
,. HEM, Oil and Grease
Analytical Method: EPA
1664E
Oil and Grease
1.3J
mg/L
5.0
1.3
1
11/25119 11:59
608 PCB Pest RVE
Analytical Method: EPA
608.3 Preparation
Method: EPA608.3
Aldrin
ND
ug/L
0.050
0.022
1
11/19/19 11:02
11/20/19 13:48
309-00-2
,alpha-BHC
ND
ug/L
0.050
0.019
1
11119/1911:02
11/20/1913:48
319-84-6
beta-BHC
ND
ug/L
0.050
0.014
1
11/19/1911:02
11/20/1913:48
319-85-7
delta-BHC
ND
ug/L
0.050
0.020
1
11/19/19 11:02
1112011913:48
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
0.012
1
11/1911911:02
11/20/19 13:48
58-89-9
Chlordane (Technical)
ND
ug/L
0.50
0.20
1
11/19/19 11:02
11/20/19 13:48
57-74-9
alpha -Chlordane
ND
ug/L
0.050
0.0090
1
11/19/19 11:02
11/20/19 13:48
5103-71-9
gamma -Chlordane
ND
ug/L
0.050
0.017
1
11/19/19 11:02
11/20/19 13:48
5103-74-2
4,4'-DDD
ND
ug/L
0.050
0.0069
1
11119/1911:02
11/2011913:48
72-54-8
4,4'-DDE
ND
ug/L
0,050
0.0064
1
11/19/19 11:02
11/20/19 13:48
72-55-9
4,4'-DDT
ND
ug/L
0.050
0.018
1
11/1911911:02
11120/1913:48
50-29-3
Dieldrin
ND
ug/L
0.050
0,0073
1
11119/19 11:02
11/20/19 13:48
60-57-1
'Endosulfan I
ND
ug/L
0.050
0.0094
1
11/19/1911*02
11/2011913:48
959-98-8
Endosulfan II
ND
ug/L
0.050
0.0065
1
11/19/19 11:02
11/2011913:48
33213-65-9
Endosulfan sulfate
ND
ug/L
0.050
0.0091
1
11/19/19 11:02
11/2011913:48
1031-07-8
Endrin
ND
ug/L
0.050
0.0089
1
11/19/19 11:02
11/2011913:48
72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.013
1
11/19/1911:02
11/20/1913:48
7421-934
Heptachlor
ND
ug/L
0.050
0.016
1
11/1911911:02
11/20/19 13:48
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
0.0097
1
11/1911911:02
11/20/19 13:48
1024-57-3
PCB-1016 (Arodor 1016)
ND
ug/L
0.50
0.22
1
11/19/19 11:02
11/20/19 13:48
12674-11-2
PCB-1 221 (Arodor 1221)
ND
ug1L
0.50
0.32
1
11/19/19 11:02
11120/1913:48
11104-28-2
PCB-1232 (Arodor 1232)
ND
ug/L
0.50
0.21
1
11/19/19 11:02
11/20/19 13:48
11141-16-5
PCB-1242 (Arodor 1242)
NO
ug/L
0.50
0.44
1
11/19/19 11:02
11120/1913:48
53469-21-9
PCB-1248 (Arodor 1248)
ND
ug/L
0.50
0.34
1
11/19/19 11:02
11/20/19 13:48
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.24
1
11/19/1911:02
11/20/1913:48
11097-69-1
PCB-1260 (Arodor 1260)
ND
ug/L
0.50
0.30
1
11/19/19 11:02
11/20/19 13:48
11096-82-5
Toxaphene
ND
ug/L
0.50
0.20
1
11/19/19 11:02
1112011913:48
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
147
%
10-130
1
11/19/19 11:02
11/20/1913*48
877-09-8 S3
Decachlorobiphenyl (S)
107
%
10-130
1
11/1911911:02
11/20/19 13:48
2051-24-3
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Antimony
ND
ug/L
5.0
3.0
1
11/19/19 01:13
11/19/19 19:01
7440-36-0
Arsenic
4.11.1
ug/L
10.0
4.7
1
11/19/19 01:13
1111911919:01
7440-38-2
Beryllium
ND
ug/L
1.0
0.20
1
11/19/19 01:13
11119/1919:01
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
11/19/19 01:13
11119/1919:01
7440-43-9
Chromium
2.1J
ug/L
5.0
1.0
1
11/19/19 01:13
11/19/19 19:01
7440.47-3
Copper
5.7
ug/L
5.0
2.1
1
1111911901:13
11/1911919:01
7440-50-8
Lead
1.11J
ug1L
5.0
1.6
1
11/19/19 01:13
11/19/19 19:01
7439-92-1
Nickel
2.3.1
ug1L
5.0
0.90
1
11/19/19 01:13
11/19/19 19:01
7440-02-0
REPORT OF LABORATORY ANALYSIS
BC
This report shall not be reproduced, except in full,
Date: 11/26/2019 07:26 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 25

s
aceAnalytical
wwal.p¢slabs.cmn
I,
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Newton Instruments/1912
Pace Project No.: 92453418
Sample: Outfall 001 Lab ID: 92453418001 Collected: 11/12/1908:30 Received: 11/12/1910*50 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method* EPA 200.7 Rev 4.4 1994
Selenium
NO
ug/L
10.0
4.7
1 11119/1901*13
11/19/1919:01
7782-49-2
Silver
NO
ug/L
5.0
2.5
1 11/19/1901:13
11/19/1919:01
7440-224
'I Thallium
2.9.1
ug/L
10.0
2.6
1 11/19/1901:13
11/19/1919:01
7440-28-0 B
Zinc
40.0
ug/L
10.0
3.9
1 11/19/19 01:13
11/19/19 19:01
7440-66-6
� 245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0
1994 Preparation
Method: EPA 245.1 Rev 3.0 1994
Mercury
0.11.1
ug/L
0.20
0.10
1 11114/1919:43
11/15/1915:28
7439-97-6 B,BC
625 MSSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Acenaphlhene
ND
ug/L
4.9
0.24
1
11/18/19 14:48
11/2411917:16
83-32-9
Acenaphthylene
NO
ug/L
4.9
0.20
1
11118/1914:48
11/24/19 17:16
208-96-8
Anthracene
NO
ug/L
4.9
0.14
1
11/18/19 14:48
11/24/19 17:16
120-12-7
' Benzidine
NO
ug/L
48.5
5.0
1
11/18/19 14:48
11/24/19 17:16
92-87-5
Benzo(a)anthracene
NO
ug/L
4.9
0.32
1
11/18/19 14:48
11/24/19 1716
56-55-3
Benzo(a)pyrene
NO
ug/L
4.9
0.29
1
11/18/19 14:48
11/24/19 17:16
50-32-8
Benzo(b)Ruoranthene
ND
ug/L
4.9
0.27
1
11/18/19 14:48
11/24/19 1716
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
4.9
0.37
1
11/18/19 14:48
11/24/19 17:16
191-24-2
Benzo(k)Fluoranthene
NO
ug/L
4.9
0.42
1
11/18/19 14:48
11/24/1917:16
207-08-9
14-Bromophenylphenyl ether
NO
ug/L
4.9
0.80
1
111181191448
11/24/19 17:16
101-55-3
Butylbenzylphthalate
NO
ug/L
4.9
0.77
1
11/18/191448
11/24/19 17:16
85-68-7
4-Chloro-3-methylphenol
NO
ug/L
4.9
3.6
1
11/18/19 14:48
11/24/19 17:16
59-50-7
bis(2-Chloroelhoxy)methane
ND
ug/L
9.7
0.89
1
11/18/19 14:48
11/24/19 17:16
111-91-1
bis(2-Chloroethyp ether
NO
ug/L
4.9
0.97
1
11/18/19 14:48
11/24/19 17:16
111-44-4
2-Chloronaphlhalene
NO
ug/L
4.9
0.95
1
11118/1914:48
11/24/1917:16
91-58-7
2-Chlorophenol
NO
ug/L
4.9
1.3
1
11/18/19 14:48
11/24/19 17:16
95-57-8
4-Chlorophenylphenyl ether
NO
ug/L
4.9
0.84
1
11/18/19 14:48
11/24/19 17:16
7005-72-3
Chrysene
ND
ug/L
4.9
0.20
1
11/18/19 14:48
11/24/19 17:16
218-01-9
Dibenz(a,h)anthracene
NO
ug/L
4.9
0.53
1
11/18/19 14:48
11/24/19 17:16
53-70-3
1,2-Dichlorobenzene
NO
ug/L
4.9
0.85
1
11/18/19 14:48
11/24/19 17:16
95-50-1
1,3Dichlorobenzene
NO
ug/L
4.9
0.79
1
11/18/19 14:48
11/24/19 17:16
541-73-1
1,4-Dichlorobenzene
NO
uglL
4.9
0.92
1
11/18/19 14:48
11/24/19 17:16
106-46-7
3,3'-Dichlorobenzidine
NO
ug/L
24.3
2.0
1
11/18/19 14:48
11/24/1917:16
91-94-1
2,4-Dichlorophenol
ND
ug/L
4.9
1.7
1
11/18/19 14:48
11/24/19 17:16
120-83-2
Diethylphthalate
NO
ug/L
4.9
0.56
1
11/18/19 14:48
11/24/19 17:16
84-66-2
2,4-Dimethylphenol
NO
ug/L
9.7
1.2
1
11/18/19 14:48
11/24/19 17:16
105-67-9
Dimelhylphthalate
NO
ug/L
4.9
0.74
1
11/18/19 14:48
11/24/19 17:16
131-11-3
Di-n-butylphthalate
NO
ug/L
4.9
0.73
1
11/18/19 14:48
11/24/19 17:16
84-74-2
4;6-Dinitro-2-methylphenol
NO
ug/L
19.4
2.5
1
11/18/19 14:48
11/24/1917:16
534-52-1
2,4-Dinitrophenol
ND
ug/L
48.5
8.7
1
11/18/19 14:48
11/24/19 17:16
51-28-5
2;4-Dinitrotoluene
NO
ug/L
4.9
0.87
1
11/18/19 14:48
11/24/19 17:16
121-14-2
2,6-Dinitrotoluene
NO
ug/L
4.9
0.95
1
11/18/19 14:48
11/24/19 17:16
606-20-2
Di-n-octylphthalate
NO
ug/L
4.9
0.64
1
1111811914:48
11124/1917:16
117-84-0
1,2-Diphenylhydrazine
NO
ug/L
4.9
0.87
1
11/18/19 14:48
11/24/19 17:16
122-66-7
bis(2-Ethylhexyl)phthalate
NO
ug/L
4.9
0.77
1
110811914:48
11/24/1917:16
117-81-7
Fluoranlhene
ND
ug/L
4.9
0.20
1
11/18/19 14:48
11/24/19 17:16
206-44-0
Fluorene
NO
ug/L
4.9
0.20
1
11/18/19 14:48
11/24/19 17:16
86-73-7
REPORT OF LABORATORY
ANALYSIS
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shall not be reproduced, except in
full,
Date: 11/26/2019 07:26 AM
without the written consent of Pace Analytical Services. L-C.
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ANALYTICAL RESULTS
Project: Newton Instruments/1912
Pace Project No.: 92453418
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Outfall 001
Lab ID:
92453418001
Collected:
11/12/1908:30
Received: 11/12/1910:50 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
OF
Prepared
Analyzed
CAS No. Oual
626 MSSV
Analytical
Method: EPA 625.1 Preparation Method:
EPA 625.1
Hexachloro-1,3-butadiene
ND
ug/L
4.9
0.91
1
11/18/19 14:48
11/24/19 1716
87-68-3
Hexachlorobenzene
NO
ug/L
4.9
0.70
1
11/1 all 914:48
11/24/19 17:16
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
9.7
0.85
1
11/18/19 1448
11/24/19 17:16
77-47-4
Hexachloroethane
ND
ug/L
4.9
1.1
1
11/18/19 14:48
11/24/19 17:16
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
4.9
0.28
1
11/18/19 14:48
11/24119 17:16
193-39-5
Isophorone
ND
ug/L
9.7
0.86
1
11/18/19 14:48
11124/19 17:16
78-59-1
I Naphthalene
NO
ug/L
4.9
0.33
1
11/18/19 14:48
11/2411917:16
91-20-3
I, Nitrobenzene
ND
ug/L
4.9
1.1
1
11/18/19 14:48
11/24/1917:16
98-95-3
2-Nitrophenol
NO
ug/L
4.9
0.88
1
11/1811914:48
11/24/19 17:16
88-75-5
4-Nitrophenol
NO
ug/L
48.5
4.0
1
11/18/1914:48
11/2411917:16
100-02-7
" N-Nitrosodimethylamine
NO
ug/L
4.9
0.88
1
11/18/19 14:48
11/24/19 17:16
62-75-9
N-Nitroso-di-n-propylamine
NO
ug/L
4.9
0.96
1
11/18/19 14:48
11/24/19 17:16
621-64-7
N-Nitrosodiphenylamine
NO
ug/L
9.7
0.97
1
11/18/19 14:48
11/24/19 17:16
86-30-6
Pentachlorophenol
NO
ug/L
9.7
4.5
1
11/18/19 14:48
11124/19 17:16
87-86-5
Phenanthrene
ND
ug/L
4.9
0.21
1
111181191448
11/24/19 17:16
85-01-8
Phenol
NO
ug/L
4.9
1.8
1
11/18/19 14:48
11/24/19 17:16
108-95-2
„Pyrene
NO
ug/L
4.9
0.18
1
11/18/19 14:48
11/24/19 17:16
129-00-0
i1,2,4-Tdchlorobenzene
NO
ug/L
4.9
0.95
1
11/18/19 14:48
11/24/19 17:16
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
9.7
1.3
1
11/18/19 14:48
11124/19 17:16
88-06-2
Surrogates
Nitrobenzene-d5(S)
56
%
10-120
1
1111 all 914:48
11/24/19 17:16
4165-60-0
,2-Fluorobiphenyl(S)
64
%
15-120
1
11/18/19 14:48
11/24/19 17:16
321-60-8
Terphenyl-014 (S)
71
%
11-131
1
11/18/1914:48
11/24/1917:16
1718-51-0
!Phenol-d6 (S)
20
%
10-120
1
11/18/19 14:48
11124/19 17:16
13127-88-3
2-Fluorophenol(S)
22
%
10.120
1
11/18/19 14:48
11/24/19 17:16
367-12-4
2,4,6-Tribromophenol(S)
53
%
10-137
1
11/1 all 14:48
11/24/19 17:16
118-79-6
420.4 Phenolics, Total Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.01993
Phenol NO mg/L 0.020 0.0050 1 11120/1909:12 1112011912:32 108-95-2 M1,R1
460OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Cyanide ND mg/L 0.0080 0.0060 1 11/181191630 11/19/1912:21 57-12-5
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REPORT OF LABORATORY ANALYSIS
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Project: Newton Instruments/1912
Pace Project No.: 92453418
QC Batch: 509542
QC Batch Method: SM 254OD-2011
Associated Lab Samples: 92453418001
METHOD BLANK: 2734477
Associated Lab Samples: 92453418001
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE: 2734478
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2734479
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 2734480
Parameter
Total Suspended Solids
QUALITY CONTROL DATA
Analysis Method: SM 254OD-2011
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit MDL Analyzed
NO 2.5 2.5 11/14/1912:21
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
(704)8759092
Qualifiers
Spike LCS LCS %Rec
Conc. Result %Rec Limits Qualifiers
250 250 100 90-110
92453376001 Dup
Units Result Result
mg/L NO NO
92453492001 Dup
Units Result Result
mg/L <5.0 NO
Max
RPD RPD Qualifiers
25
Max
RPD RPD Qualifiers
25
Results presented on this page arein the untts Indicated by the "Units" column except where an alternate unit Is presented to the right of the resu g.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Newton Instruments/1912
Pace Project No.: 92453418
QC Batch: 511562 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92453418001
METHOD BLANK: 2743969
Associated Lab Samples: 92453418001
Parameter Units
Oil and Grease mg/L
LABORATORY CONTROL SAMPLE: 2743970
Parameter Units
Oil and Grease mg/L
MATRIX SPIKE SAMPLE: 2743971
Parameter Units
Oil and Grease mg/L
Matrix: Water
Blank Reporting
Result Limit
NO 5.0
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MDL Analyzed Qualifiers
1.3 11/2511911:57
Spike LCS 1-CS
Cone. Result % Rec
40 35.9 90
e/ Rec
Limits Qualifiers
78-114
92453418001 Spike MS MS % Rec
Result Cone. Result %Rec Limits Qualifiers
1.3J 40 37.8 91 78-114
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is preseMe4 to the rlgM of the result.
REPORT OF LABORATORY ANALYSIS
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Project: Newton Instruments/1912
Pace Project No.: 92453418
OC Batch: 509634
QC Batch Method: EPA 245.1 Rev 3.0 1994
Associated Lab Samples: 92453418001
METHOD BLANK: 2735157
Associated Lab Samples: 92453418001
Parameter Units
Mercury ug/L
Pace Analytical Services, LLC
98001Gncey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 245.1 Rev 3.0 1994
Analysis Description: 245.1 Mercury
Matrix: Water
Blank Reporting
Result Limit MOIL Analyzed Qualifiers
0.131 0.20 0.10 11/15/1915:09 BC
LABORATORY CONTROL SAMPLE: 2735158
Spike LCS 1-CS %Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.6 104 85-115
i VATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2735159
2735160
MS
MSD
92453358001 Spike
Spike
MS MSD
MS MSD %Rec Max
Parameter Units Result Cone.
Cone.
Result Result
%Rec %Rec Limits RPD RPD Qual
Mercury ug/L NO 2.5
2.5
2.0 2.0
75 76 70-130 2 20
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the ri of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments/1912
Pace Project No.: 92453418
QC Batch: 510260
Analysis Method:
EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994
Analysis Descnption: 200.7 MET
Associated Lab Samples: 92453418001
METHOD BLANK: 2738015
Matrix: Water
Associated Lab Samples: 92453418001
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
Qualifiers
Antimony
ug/L
NO
5.0
3.0
11/19/19 17:57
Arsenic
ug/L
ND
10.0
4.7
11/19/19 17:57
Beryllium
ug/L
ND
1.0
0.20
11/19/19 17:57
Cadmium
ug/L
NO
1.0
0.40
11119/1917:57
Chromium
ug/L
NO
5.0
1.0
1111911917:57
Copper
ug/L
ND
5.0
2.1
11/19/19 17:57
Lead
ug/L
NO
5.0
1.6
11/19/19 17:57
Nickel
ug/L
ND
5.0
0,90
11/19/19 17:57
Selenium
ug/L
ND
10.0
4.7
11/19/1917:57
Silver
ug/L
NO
5.0
2.5
11/19/19 17:57
Thallium
ug/L
3.0J
10.0
2.6
11/19/19 17:57
BC
Zinc
ug/L
NO
10.0
3.9
11/19/19 17:57
LABORATORY CONTROL SAMPLE: 2738016
Spike
LCS
LCS
%Rec
Parameter
Units
Conc.
Result
%Rec
Limits Qualifiers
Antimony
ug/L
500
481
96
85-115
Arsenic
ug/L
500
475
95
85-115
Beryllium
ug/L
500
484
97
85-115
Cadmium
ug/L
Soo
477
95
85-115
Chromium
ug/L
500
480
96
85-115
'Copper
ug/L
500
474
95
85-115
Lead
ug/L
500
474
95
85-115
I Nickel
ug/L
500
472
94
85115
'Selenium
ug/L
500
466
93
85-115
Silver
ug/L
250
241
96
85-115
Thallium
ug/L
500
473
95
85-115
Zinc
ug/L
500
472
94
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2738017
2738018
MS
MSD
92453188001
Spike
Spike
MS
MSD
MS MSD
%Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result
%Rec %Rec
Limits
RPD RPD Qual
,Antimony ug/L
ND
500
500
508
499
101 99
70-130
2 20
Arsenic ug/L
ND
500
500
513
510
102 101
70-130
1 20
Beryllium ug/L
2.5
500
500
505
506
100 101
70-130
0 20
Cadmium ug/L
NO
500
500
506
501
101 100
70-130
1 20
Chromium ug/L
195
Soo
500
692
701
99 101
70-130
1 20
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Newton Instruments/1912
92453418
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2738017
2738018
MS
MSD
92453188001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
1, Parameter
Units Result
Conc.
Cone.
Result
Result
%Rec
%Rec
Limits
RPD
RPD Qua]
Copper
uglL 108
500
500
614
608
101
100
70-130
1
20
Lead
ug/L 16.2
500
500
492
490
95
95
70-130
0
20
Nickel
ug/L 1120
500
500
1620
1630
99
101
70-130
1
20
Selenium
ug/L NO
500
500
526
517
105
103
70-130
2
20
Silver
ug/L NO
250
250
250
248
100
99
70-130
1
20
Thallium
ug/L ND
500
500
460
462
92
92
70-130
0
20
Zinc
ug/L 51.7
500
500
544
545
98
99
70-130
0
20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2738019
MS
92453418001 Spike
Parameter Units Result Cone.
MSD
Spike
Conc.
2738020
MS
Result
MSO
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD Qual
Antimony
ug/L
NO
500
500
504
501
101
100
70-130
1
20
Arsenic
uglL
4.8J
500
500
508
508
101
101
70-130
0
20
Beryllium
ug/L
ND
500
500
499
498
100
100
70-130
0
20
Cadmium
ug/L
NO
500
500
511
508
102
102
70-130
0
20
Chromium
ug/L
2.1J
500
500
501
497
100
99
70-130
1
20
Copper
uglL
5.7
500
500
504
507
100
100
70-130
1
20
Lead
ug/L
1.8J
500
500
496
497
99
99
70.130
0
20
Nickel
ug/L
2.3J
500
500
493
494
98
98
70-130
0
20
Selenium
ug/L
NO
500
500
538
533
107
107
70-130
1
20
Silver
ug/L
NO
250
250
252
253
101
101
70-130
0
20
Thallium
ug/L
2.9J
500
500
477
480
95
95
70.130
1
20
Zinc
ug/L
40.0
500
500
532
534
98
99
70-130
0
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/26/2019 07:26 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 25

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n
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QUALITY CONTROL DATA
Project: Newton Instrumentsl1912
Pace Project No.: 92453418
QC Batch: 510331
OC Batch Method: EPA608.3
Associated Lab Samples: 92453418001
Analysis Method:
Analysis Description:
EPA608.3
608 PCB Pest Red Vol
METHOD BLANK: 2738254
Matrix: Water
Associated Lab Samples: 92453418001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
4,4'-DDD
ug/L
NO
0.050
0.0069
11120/1909:48
4,4'-DOE
ug/L
ND
0.050
0.0064
11/20/19 09:48
4,4'-DDT
uglL
ND
0.050
0.018
11/20/19 09:48
Aldrin
ug/L
ND
0.050
0.022
11120/1909:48
alpha-BHC
ug/L
ND
0.050
0.019
11/2011909:48
alpha -Chlordane
ug/L
ND
0.050
0.0090
11/20/19 09:48
beta-BHC
ug/L
ND
0.050
0.014
11/20/19 09:48
Chlordane (Technical)
ug/L
ND
0.50
0.20
11/20/1909:48
delta-BHC
ug/L
ND
0.050
0.020
11 /20/19 09*48
Dieldrin
ug/L
ND
0.050
0,0073
11/20/19 09:48
Endosulfan)
ug/L
ND
0.050
0.0094
11/20/1909:48
Endosulfan II
ug/L
ND
0.050
0.0065
11/20/19 09:48
Endosulfan sulfate
ug/L
ND
0.050
0.0091
11/2011909:48
,Enddn
ug/L
ND
0.050
0.0089
11/20/1909:48
Enddn aldehyde
ug/L
ND
0,050
0.013
11/20/19 09:48
gamma-BHC(Lindane)
ug/L
ND
0,050
0.012
11120/1909:48
gamma -Chlordane
ug/L
ND
0.050
0.017
11/20119 09:48
Heptachlor
ug/L
NO
0.050
0.016
11/20/19 09:48
Heptachlor epoxide
ug/L
NO
0.050
0.0097
11/20/19 09:48
PCB-1016(Arodor 1016)
ug/L
ND
0.50
0.22
11/20/19 09:48
,!PCB-1221(Arodor 1221)
ug/L
ND
0.50
0.32
11120/1909:48
PCB-1232 (Arodor 1232)
ug/L
ND
0.50
0.21
11/20/19 09:48
PCB-1242(Arodor 1242)
ug/L
ND
0.50
0.44
11/20/19 09:48
PCB-1248 (Arodor 1248)
ug/L
ND
0.50
0.34
11/20/19 09:48
PCB-1254 (Aroclor 1254)
ug/L
ND
0.50
0.24
11/20/19 09:48
'PCB- 1260(Aroclor 1260)
ug/L
ND
0.50
0.30
11/20/19 09:48
Toxaphene
ug/L
NO
0.50
0.20
11/20/19 09:48
Decachlorobiphenyl(S)
%
124
10-130
11/20/1909:48
Tetrachloro-m-xylene (S)
%
82
10-130
11/20/19 09:48
Pace Analytical Services, LLC
9800 Kmcey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
LABORATORY CONTROL SAMPLE:
2738255
Spike
LCS
LCS
%Rec
Parameter
Units
Conc.
Result
%Rec'
Limits Qualifiers
4,4'-DDD
ug/L
0.25
0.24
98
31-141
4,4'-DDE
ug/L
0.25
0.23
92
30-145
4A'-DDT
ug/L
0.25
0.33
133
25-160
Aldrin
ug/L
0.25
0.26
102
42-140
alpha-BHC
ug/L
0.25
0.25
100
37-140
alpha -Chlordane
ug/L
0,25
0.27
108
45-140
beta-BHC
ug/L
0.25
0.31
122
17-147
Results presented on this page am In the units Indicated by the 'Lnlb" column except where an alternate unit Is preseme0 to the dam of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/26/2019 07:26 AM without the written consent of Pace Analytical Services, -I-C. Page 13 of 25

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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments/1912
Pace Project No.: 92453418
LABORATORY CONTROL SAMPLE:
2738255
Spike
LCS
LCS
% Rec
Parameter
Units
Conic.
Result
% Rec
Limits
Qualifiers
delta-BHC
ug/L
0.25
0,25
99
19-140
Dieldrin
ug/L
0.25
0.27
106
36-146
Endosulfan I
ug/L
0.25
0.26
105
45.153
Endosulfan II
ug/L
0.25
0.27
109
1-202
Endosulfan sulfate
ug/L
0,25
0.28
113
26-144
Endrin
ug/L
0.25
0.27
110
30-147
Endrin aldehyde
ug/L
0.25
0.25
101
50-150
I gamma-BHC (Lindane)
ug/L
0.25
0.26
103
32-140
gamma -Chlordane
ug/L
0.25
0.19
76
45-140
Heptachlor
ug/L
0.25
0.26
104
34-140
Heptachlor epoxide
ug/L
0.25
0.27
106
37-142
Decachlorobiphenyl(S)
%
126
10-130
Tetrachloro-m-xylene (S)
%
98
10-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2738256
2738257
MS
MSD
92453933001
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
I
Units
Result
Conic.
Conc.
Result
Result
%Rec %Rec
Limits
RPD
RPD Qua]
4,4'-DDD
ug/L
NO
0.25
0.25
0.27
0.27
109
109
31-141
1
39
4,4'-DOE
ug/L
NO
0.25
0.25
0.26
0.26
103
104
30-145
1
35
4,4'-DDT
ug/L
ND
0.25
0.25
0.37
0.37
147
148
25-160
1
42
Aldrin
ug/L
ND
0.25
0.25
0.27
0.27
108
107
42-140
1
35
alpha-BHC
ug/L
NO
0.25
0.25
0.26
0.25
104
100
37-140
3
36
alpha -Chlordane
ug/L
NO
0.25
0.25
0.29
0.29
116
115
45-140
1
35
beta-BHC
ug/L
NO
0.25
0.25
0.35
0.35
140
141
17-147
1
44
.'delta-BHC
ug/L
NO
0.25
0.25
0.27
0.27
110
108
10-140
1
52
Dieldrin
ug/L
ND
0.25
0,25
0.28
0.28
114
113
36-146
1
49
Endosulfan I
ug/L
ND
0.25
0.25
0.28
0.28
112
111
45-153
1
28
Endosulfan II
ug/L
NO
0.25
0.25
0.29
0.29
117
115
1-202
1
53
Endosulfan sulfate
ug/L
NO
0.25
0.25
0.31
0.30
122
122
26-144
1
38
','Endrn
ug/L
NO
0.25
0.25
0.30
0.29
118
117
30-147
1
48
Endrn aldehyde
ug/L
NO
0.25
0.25
0.27
0.27
109
108
50-150
1
30
gamma-BHC (Lindane)
ug/L
NO
0.25
0.25
0.28
0.27
112
109
32-140
3
39
';gamma -Chlordane
ug/L
ND
0.25
0.25
0.20
0.20
81
82
45-140
1
35
Heptachlor
ug/L
ND
0.25
0.25
0.28
0.28
113
111
34-140
2
43
Heptachlor epoxide
ug/L
NO
0.25
0.25
0.28
0.28
ill
111
37-142
0
26
Decachlorobiphenyl(S)
%
ill
110
10-130
�Tetrachloro-m-xylene(S)
%
101
96
10-130
Results presented on this page are in the units indicated by the 'Units' column except where an alternate unit Is presented to the right of the result.
Date: 11/26/2019 07:26 AM
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 25

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QUALITY CONTROL DATA
Project: Newton Instruments/1912
Pace Project No.: 92453418
QC Batch: 510118 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Associated Lab Samples: 92453418001
METHOD BLANK: 2737305
Associated Lab Samples: 92453418001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,2,4-Tdchlorobenzene
uglL
NO
5.0
0.98
11/19/19 12:17
1,2-Dichlorobenzene
ug/L
NO
5.0
0.88
11/19/19 12:17
1,2-Diphenylhydrazine
ug/L
ND
5.0
0.90
11/19/19 12:17
. 1,3-Dichlorobenzene
ug/L
ND
5.0
0.81
11/19/19 12:17
1,4-Dichlorobenzene
ug/L
ND
5.0
0.95
11/19/19 12:17
2,4,6-Trichlorophenol
ug/L
NO
10.0
1.3
11/19/19 12:17
'I 2,4-Dichlorophenol
ug/L
ND
5.0
1.7
11/19/19 12:17
2,4-Dimethylphenol
ug/L
ND
10.0
1.2
11/19/19 12:17
2,4-Dinitrophenol
ug/L
ND
50.0
9.0
11/19/19 12:17
2,4-Dinitrotoluene
ug/L
NO
5.0
0.90
11/19/1912:17
2,6-Dinitrotoluene
ug/L
NO
5.0
0.98
11/19/19 12:17
2-Chloronaphthalene
ug/L
ND
5.0
0.98
11/19/19 12:17
1 2-Chlorophenol
ug/L
ND
5.0
1.3
11/19/19 12:17
2-Nitrophenol
ug1L
NO
5.0
0.91
1111911912:17
i 3,3-Dichlorobenzidine
ug/L
NO
25.0
2.1
11/19/1912*17
4,6-Dinitro-2-methylphenol
ug/L
ND
20.0
2.6
11/19/19 12:17
4-Bromophenylphenyl ether
ug/L
ND
5.0
0.82
11/19/19 12:17
4-Chloro-3-methylphenol
ug/L
ND
5.0
3.7
11/19/19 12:17
4-Chlorophenylphenyl ether
ug/L
NO
5.0
0.87
11/19/19 12:17
4-Nitrophenol
ug/L
ND
50.0
4.1
11/1911912:17
Acenaphthene
ug/L
NO
5.0
0.25
11/19/19 12:17
Acenaphthylene
ug/L
ND
5.0
0.21
11/1911912:17
Anthracene
ug/L
NO
5.0
0.14
11/19/19 12:17
Benzidine
ug/L
NO
50.0
5.1
11/19/19 12:17
Benzo(a)anthracene
ug/L
NO
5.0
0.33
11/19/19 1217
. Benzo(a)pyrene
ug/L
ND
5.0
0.30
11/19/19 12:17
Benzo(b)fluoranlhene
ug/L
NO
5.0
0.28
11/19/19 12:17
Benzo(g,h,i)perylene
ug/L
NO
5.0
0.38
11/19/19 12:17
Benzo(k)fluoranthene
ug/L
ND
5.0
0.43
11/19/19 12:17
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
0.92
11/19/19 12:17
bis(2-Chloroethyl) ether
ug/L
ND
5.0
1.0
11/19/19 12:17
b is(2- Ethyl hexyl) phthal ate
ug/L
NO
5.0
0.79
11/19/19 12:17
Butylbenzylphthalate
ug/L
NO
5.0
0.79
11/19/19 12:17
. Chrysene
ug/L
ND
5.0
0.21
11/19/1912:17
'Di-n-butylphthalate
ug/L
ND
5.0
0.75
11/19/19 12:17
Di-n-octylphlhalate
ug/L
ND
5.0
0.66
11/19/19 12:17
Dibenz(a.h)anthracene
ug/L
ND
5.0
0.55
11/19/19 12:17
Diethylphthalate
ug/L
ND
5.0
0.58
11/19/19 12:17
Dimethylphthalale
ug/L
NO
5.0
0.76
11/19/1912:17
Fluoranthene
ug/L
ND
5.0
0.21
11/19/19 12:17
,Fluorene
ug/L
ND
5.0
0.21
11/19/19 12:17
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is proserned to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/26/2019 07:26 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 25

aceAnalytical
ware pacelabs.carn
Project: Newton Instruments/1912
Pace Project No.: 92453418
METHOD BLANK: 2737305
Associated Lab Samples: 92453418001
Parameter
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propyla mi ne
" N-Nitrosodimelhylamine
N-Ni trosod iphe nylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
i, 2,4,6-Tribromophenol (S)
2-Fluorobiphenyl(S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
'j Terphenyl-d14 (S)
I
QUALITY CONTROL DATA
Matrix: Water
Units
Blank
Result
Reporting
Limit
MOIL
Analyzed
ug/L
NO
5.0
0.94
11/19/19 12:17
ug/L
NO
5.0
0.72
11/19/19 12:17
ug/L
NO
10.0
0.88
11/19/19 12:17
ug/L
NO
5.0
1.1
11/19/19 12:17
ug/L
NO
5.0
0.29
11/19/19 12:17
ug/L
NO
10.0
0.89
11/19/19 12:17
ug/L
NO
5.0
0.99
11/19/19 12:17
ug/L
NO
5.0
0.91
11/1911912:17
ug/L
NO
10.0
1.0
11/19/19 12:17
ug/L
NO
5.0
0.34
11/19/19 12:17
ug/L
NO
5.0
1.1
11119/1912:17
ug/L
NO
10.0
4.6
11/19/19 12:17
ug/L
NO
5.0
0.22
11/19/19 12:17
ug/L
NO
5.0
1.9
11/1911912:17
ug/L
NO
5.0
0.19
11/19/19 12:17
%
54
10-137
1111911912:17
%
69
15-120
1111911912:17
%
44
10-120
11/1911912:17
%
72
10-120
11/19/19 12:17
%
31
10-120
11/19/19 12:17
%
79
11-131
11/19/19 12:17
LABORATORY CONTROL SAMPLE:
Parameter
2737306
Units
Spike
Conc.
LCS
Result
LCS
e/ Rec
% Rec
Limits
1,2,4-Tichlorobenzene
ug/L
50
34.1
68
44-142
1,2-Dichlorobenzene
ug/L
50
34.5
69
32-129
1,2-Diphenylhydrazine
ug/L
50
64.4
129
25-150
1,3-Dichlorobenzene
ug/L
50
33.1
66
1-172
1,4-Dichlorobenzene
ug/L
50
33.6
67
20-124
2,4,6-Tdchlorophenol
ug/L
50
39.3
79
37-144
2,4-Dichlorophenol
ug/L
50
38.8
78
39-135
2,4-Dimethylphenol
ug/L
50
39.4
79
32-120
2,4-Dinitrophenol
ug/L
250
214
86
1-19l
2,4-Dinitrotoluene
ug/L
50
41.1
82
39-139
2,6-Dinitrotoluene
ug/L
50
43.0
86
50-158
2-Chloronaphthalene
ug/L
50
44.8
90
60-120
2-Chlorophenol
ug/L
50
37.9
76
23-134
2-Nitrophenol
ug/L
50
42.2
84
29-181
3,3'-Dichlorobenzidine
ug/L
100
69.9
70
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
88.0
88
1-181
4-Bromophenylphenyl ether
ug/L
50
35.2
70
53-127
4-Chloro-3-methylphenol
ug/L
100
81.1
81
22-147
4-Chlorophenylphenyl ether
ug/L
50
38.3
77
25-158
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Qualifiers
Qualifiers
Results presented on this page are In the units Indicated by the "units" column except wTere an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/26/2019 07:26 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 25

Ice Analytical
www.pactlaltn.cum
I'
Project: Newton Instruments/1912
Pace Project No.: 92453418
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Hunterswile, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2737306
Spike
-CS 1-CS
%Rec
Parameter
Units
Conc.
Result %Rec
Limits
Qualifiers
. 4-Nitrophenol
ug/L
250
112
45
1-132
Acenaphthene
ug/L
50
40.4
81
47-145
Acenaphthylene
ug/L
50
42.9
86
33-145
Anthracene
ug/L
50
40.4
81
27-133
Benzidine
ug/L
100
ND
4
25-150 L2
Benzo(a)anthracene
ug/L
50
39.9
80
33-143
` Benzo(a)pyrene
ug/L
50
40.6
81
17-163
Benzo(b)fluoranthene
ug/L
50
41.9
84
24-159
Benzo(g,h,i)perylene
ug/L
50
464
93
1-219
Benzo(k)fluoranlhene
ug/L
50
41.3
83
11-162
bis(2-Chloroethoxy)methane
ug/L
50
38.4
77
33-184
bis(2-Chloroethyp ether
ug/L
50
39.7
79
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
41.0
82
8-158
Butyl benzylphthalate
ug/L
50
41.2
82
1-152
Chrysene
ug/L
50
36.2
72
17-168
Di-n-butylphthalale
ug/L
50
38.7
77
1-120
Di-n-octylphthalate
ug/L
50
40.9
82
4-146
Dibenz(a,h)anthracene
ug/L
50
47.2
94
1-227
Diethylphthalate
ug/L
50
38.0
76
1-120
Dimethylphthalale
ug/L
50
37.6
75
1-120
Fluoranthene
ug/L
50
38.4
77
26-137
Fluorene
ug/L
50
41.4
83
59-121
Hexachloro-1,3-butadiene
ug/L
50
29.9
60
24-120
Hexachlorobenzene
ug/L
50
35.2
70
1-152
Hexachlorocydopentadiene
ug/L
50
30.3
61
25-150
Hexachloroethane
ug/L
50
33.1
66
40-120
Indeno(1,2,3-cd)pyrene
ug/L
50
45.5
91
1-171
Isophorone
ug/L
50
39.3
79
21-196
N-Nitroso-di-n-propylamine
ug/L
50
42.0
84
1-230
N-Nitrosodimethylamine
ug/L
50
28.0
56
25-150
N-Nitrosodiphenylamine
ug/L
50
37.8
76
25-150
Naphthalene
ug/L
50
39.9
80
21-133
Nitrobenzene
uglL
50
41.6
83
35-180
Pentachlorophenol
ug/L
100
72.0
72
14-176
Phenanthrene
ug/L
50
38.7
77
54-120
Phenol
ug/L
50
20.8
42
5-120
Pyrene
ug/L
50
40.3
81
52-120
2,4,6-Tnbromophenol (S)
%
77
10-137
2-Fluorobiphenyl(S)
%
82
15-120
2-Fluorophenol(S)
%
59
10-120
Nitrobenzene-d5 (S)
%
85
10-120
Phenol-d6 (S)
%
43
10-120
Terphenyl-dl4 (S)
%
76
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is pres nned to the ABM of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/26/2019 07:26 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 25

aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments/1912
.i Pace Project No.: 92453418
J MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2737307
2737308
MS
MSD
92449985005
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units Result
Cone.
Cone.
Result
Result
%Rec
%Rec
Limits
RPD
RPD Dual
. 12,4-Trichlorobenzene
ug/L
ND
50
50
34.3
24.5
69
49
44-142
33
50
1,2-Dichlorobenzene
ug/L
NO
50
50
33.3
24.4
67
49
32-129
31
30 R1
1,2-Diphenylhydrazine
ug/L
NO
50
50
64.1
60.1
128
120
25-150
6
30
1,3-Dichlorobenzene
ug/L
NO
50
50
31.9
23.1
64
46
1-172
32
30 R1
1,4-Dichlorobenzene
ug/L
NO
50
50
32.4
23.3
65
47
20.124
32
30 R1
2,4,6-Tdchlorophenol
ug/L
NO
50
50
27.7
19.0
55
38
37-144
38
58
2,4-Dichlorophenol
ug/L
NO
50
50
32.1
19.6
64
39
39-135
48
50
2,4-Dimethylphenol
ug/L
ND
50
50
37.6
27.9
75
56
32-120
30
58
2,4-Dinitrophenol
ug/L
NO
250
250
103
84.9
41
34
1-191
19
132
2,4-Dinitrotoluene
ug/L
NO
50
50
40.5
39.4
81
79
39-139
3
42
2,6-Dinitrotoluene
ug/L
NO
50
50
42.7
40.7
85
81
50-158
5
48
2-Chloronaphthalene
ug/L
NO
50
50
46.3
37.0
93
74
60-120
23
24
2-Chlorophenol
ug/L
NO
50
50
31,2
17.3
62
35
23-134
57
61
2-Nitrophenol
ug/L
NO
50
50
32.9
18A
66
36
29-182
58
55 RI
3,S-Dichlorobenzidine
ug/L
NO
100
100
70A
71.7
70
72
1-262
2
108
4,6-Dinitro-2-methylphenol
ug/L
NO
100
100
48.2
38.6
48
39
1-181
22
30
4-Bromophenylphenyl ether
ug/L
NO
50
50
35.7
33.9
71
68
53-127
5
43
4-Chloro-3-methylphenol
ug/L
NO
100
100
77.9
66.7
78
67
22-147
16
73
4-Chlorophenylphenyl ether
ug/L
NO
50
50
38.7
35.3
77
71
25-158
9
61
4-Nitrophenol
ug/L
NO
250
250
85.3
62.7
34
25
1-132
30
131
Acenaphthene
ug/L
ND
50
50
41.1
35.6
82
71
47-145
14
48
Acenaphthylene
ug/L
NO
50
50
43.8
37.5
88
75
33-145
15
74
Anthracene
ug/L
NO
50
50
40.3
39.3
81
79
27-133
3
66
Benzidine
ug/L
NO
100
100
21.9J
22.9J
22
23
25-150
30 Mo
Benzo(a)anlhracene
ug/L
NO
50
50
39.2
38.8
78
78
33-143
1
53
Benzo(a)pyrene
ug/L
NO
50
50
40.4
38.9
81
78
17-163
4
72
Benzo(b)fluoranthene
ug/L
NO
50
50
41.9
39.4
84
79
24-159
6
71
Benzo(g,h,i)perylene
ug/L
NO
50
50
45.0
44.0
90
88
1-219
2
97
Benzo(k)Fluoranthene
ug/L
NO
50
50
40.4
38.1
81
76
11-162
6
63
bis(2-
ug/L
NO
50
50
37.6
27.5
75
55
33-184
31
54
C h loroethoxy) methane
bis(2-Chloroethy0 ether
ug/L
NO
50
50
37.8
27.5
76
55
12-158
32
108
' bis(2-Ethylhexypphthalate
ug/L
NO
50
50
40.0
38.9
80
78
8-158
3
82
Burylbenzylphthalate
ug/L
NO
50
50
40.5
39.3
81
79
1-152
3
60
" Chrysene
ug/L
NO
50
50
35.9
35.7
72
71
17-168
1
87
Di-n-butylphthalate
ug/L
NO
50
50
38.0
38.4
76
77
1-120
1
47
Di-n-octylphthalate
ug/L
NO
50
50
39.5
41.7
79
83
4-146
5
69
Dibenz(a,h)anthracene
ug/L
NO
50
50
45.0
44.8
90
90
1-227
0
126
Diethylphthalate
ug/L
NO
50
50
37.9
37.3
76
75
1-120
1
100
Dimethylphthalate
ug/L
NO
50
50
37.6
36.3
75
73
1-120
4
183
Fluoranthene
ug/L
NO
50
50
37.5
38.1
75
76
26-137
2
66
Fluorene
ug/L
NO
50
50
41.8
38.9
84
78
59-121
7
38
'. Hexachtoro-1,3-buladiene
ug/L
NO
50
50
30.7
21.1
61
42
24-120
37
62
Hexachlorobenzene
ug/L
NO
50
50
35.3
34.3
71
69
1-152
3
55
Hexachlorocyclopentadiene
ug/L
NO
50
50
31.2
19.3
62
39
25-150
47
30 Rt
Hexachloroethane
ug/L
NO
50
50
32.5
23.0
65
46
40-120
34
52
Results presented on this page am In
the units indicated by the
"Units' column
except wherean alternate unit Is presented to the
right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/26/2019 07:26 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 25

aceAnalytical a
I rw.paulebs.coln
I
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments/1912
Pace Project No.: 92453418
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2737307
2737308
MS
MSD
,
92449985005
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
e/ Rec
% Rec
Limits
RPD
RPD Qual
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
50
44.1
43.6
88
87
1-171
1
99
Isophorone
ug/L
ND
50
50
38.5
29.6
77
59
21-196
26
93
N-Nitroso-di-n-propylamine
ug/L
ND
50
50
41.1
30.6
82
61
1-230
29
87
N-Nitrosodimethylamine
ug/L
ND
50
50
33.1
22.0
66
44
25-150
40
30 R7
N-Nitrosodiphenylamine
ug/L
ND
50
50
38.6
36.7
77
73
25-150
5
30
Naphthalene
ug/L
ND
50
50
39.3
28.6
79
57
21-133
31
65
Nitrobenzene
ug/L
ND
50
50
40.8
29.4
82
59
35-180
33
62
Pentachlorophenol
ug/L
ND
100
too
44.7
35.3
45
35
14-176
23
86
'I Phenanthrene
ug/L
ND
50
50
39.0
37.8
78
76
54-120
3
39
Phenol
ug/L
ND
50
50
25.2
12.7
50
25
5-120
66
64 R1
Pyrene
ug/L
ND
50
50
39.9
37.7
80
75
52-120
6
49
2,4,6-Tdbromophenol (S)
%
58
47
10-137
2-Flucrobiphenyl(S)
%
78
64
15-120
2-Fluorophenol(S)
%
47
24
10-120
Nitrobenzene-d5 (S)
%
79
59
10-120
Phenol-d6 (S)
%
50
26
10-120
„ Terphenyl-dl4(S)
%
61
58
11-131
Results presented on this page are in the units Indicated by the"Units" column except where an alternate unit Is presented to the right of the result.
Date: 11/26/2019 07:26 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 25

a
aceAnalytical
w"pacelabs.core
QUALITY CONTROL DATA
Project: Newton Instruments/1912
Pace Project No.: 92453418
OC Batch: 510339 Analysis Method: EPA 420.4 Rev 1.01993
OC Batch Method: EPA420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics
Associated Lab Samples: 92453418001
METHOD BLANK: 2738282
Associated Lab Samples: 92453418001
Parameter Units
Phenol mg/L
LABORATORY CONTROL SAMPLE: 2738283
Parameter Units
Phenol mg/L
Matrix: Water
Blank Reporting
Result Limit
NO 0.020
Spike LCS
Conc. Result
0.05 0.048
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MDL Analyzed Qualifiers
0.0050 11/20/19 1226
LCS % Rec
% Rec Limits Qualifiers
96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2738284
2738285
MS
MSD
92453833001 Spike
Spike
MS
MSD
MS MSD e/ Rec
Max
Parameter Units Result Cone.
Conc.
Result
Result
%Rec %Rec Limits
RPD RPD Qua[
Phenol mg/L 0.029 0.05
0.05
0.071
0.072
84 85 90-110
1 10 M7
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2738286
2738287
MS
MSD
92453418001 Spike
Spike
MS
MSD
MS MSD % Rec
Max
Parameter Units Result Conc.
Conc.
Result
Result
%Rec %Rec Limits
RPD RPD Qual
Phenol mg/L NO 0.05
0.05
0.059
0.047
112 89 90-110
22 10 Mi,R1
Results presentee on in s page am In the units indicated by the "Units" column except where an alternate unit Is presentee to the dam or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/26/2019 07:26 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 25

s
laceAnallytili
ww.paelabs.cam
QUALITY CONTROL DATA
Project: Newton Instruments/1912
Pace Project No.: 92453418
QC Balch: 510066 Analysis Method: SM 4500-CN-E-2011
QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total
Associated Lab Samples: 92453418001
Pace Analytical Services, Li
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
�- METHOD BLANK: 2737025 - Matrix: Water
Associated Lab Samples: 92453418001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Cyanide mg/L ND 0,0080 0.0060 11/19/1912:00
LABORATORY CONTROL SAMPLE: 2737026
Spike LCS LCS %Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Cyanide mg/L 0.1 0Al 107 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2737027
2737028
MS
MSD
92453147002 Spike
Spike
MS
MSD MS
MSD
%Rec Max
Parameter Units Result Cone.
Conc.
Result
Result %Rec
%Rec
Limits RPD RPD Qual
'Cyanide mi ND 0.1
0.1
0.10
0.10 101
101
80-120 0 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2737029 2737030
MS MSD
92453147003 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
'Cyanide mi ND 0.1 0.1 0.10 0.10 102 103 80-120 0 10
Results presented on this page are in the units indicated by the "links' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 11/26/2019 07:26 AM without the wrinen consent of Pace Analytical Services, LLC. Page 21 of 25

Pace Analytical Services, LLC
55?eAnalyticl 9900 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.cem (704)8759092
QUALIFIERS
Project: Newton Instruments/1912
Pace Project No.: 92453418
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitdle by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
B Analyte was detected in the associated method blank.
BC The same analyle was detected in an associated blank at a concentration above 112 the reporting limit but below the
laboratory reporting limit.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
Mo Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded OC limits. Batch accepted based on laboratory control sample (LCS) recovery.
RI RPD value was outside control limits.
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/2612019 07:26 AM without the written wnsent of Pace Analytical Services, LLC. Page 22 of 25

Pace Analytical Services, LLC
?veAnalyticala 9800 nceyAve Suite 100
Hutersville, nNC 28078078
wwwgecelabs.oem [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Newton Instruments/1912
92453418
I
Analytical
I Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92453418001
Outfall 001
SM 254OD-2011
509542
92453418001
Outfall 001
EPA 1664B
511562
92453418001
Outfall 001
EPA608.3
510331
EPA 608.3
510562
92453418001
Outfall 001
EPA 200.7 Rev 4.4 1994
510260
EPA 200.7 Rev 4.4 1994
510278
92453418001
Outfall 001
EPA 245.1 Rev 3.0 1994
509634
EPA 245.1 Rev 3.0 1994
509756
92453418001
Outfall 001
EPA 625.1
510118
EPA625A
510985
92453418001
Outfall 001
EPA420.4 Rev 1.0 1993
510339
EPA 420.4 Rev 1.0 1993
510597
92453418001
I
Outfall 001
SM 4500-CN-E-2011
510066
SM 4500-CN-E-2011
510244
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/26/2019 0726 AM without the written consent of Pace Analytical Services, LLC.
Page 23, of 25

CHAIN -OF -CUSTODY Analytical Request Document_
Chainof-Custody Is a LEGAL DOCUMENT- Complete all rele rent fields
Piedmont
Rd. Raleigh, NC 27607
Report To: Jonathan
C.py To:
same
Newton Instruments
/ 1912
INC / Butner t 1 PT 1 ] MT [ I CT VJ ET
Phone: [phone]
Site/Facility ID N:
Compliance Monitoring?
Email: ynuy:[e-mail]:mm
[ ) Yes [ )NO
Collected By (print):
(
Purchase Order N:
DW PWS ID N:
i µnCl05 Mufti"
Quote R:
DW Location Code:
Collected By (signatur ):
Turnaround Data Required:
Immediately Pplc onIce:
IvfYes_ ( ) No
mZpie Disposal: I
Rush:
Field Filtered (if applicable):
] Otpose as appr.prlate I 1 Remm
I ]Same Da ( y ' ] Next Day
[ )Yes I ] No
I Arddva:
l 12 Day 1 13 Day 1 ) 4 Day [ 15 Day
1 Hold:
(Eapedae Charges Apply)
Analysis:
' Matrix Codes (Insert in Matrix bog below): Drinking Water (DW), Ground Water (GW), Wastewater (WV),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tmsue (TS), Bioassay (B), Vapor (V), Other CT)
Customer Sample ID
I
Matra •
Comp /
Grab
Collected («
Composhe Start)
Composite End
Res
cl
N of
Cars
Gate
I Time
I Date
Time
Outfall-001
I
I Gyy
I Grab
hiAwml
15
Customer Remarks / Special Conditions/ Possible Narards:
PH='7.G
Dabe/nme:
WO# : 9245341R= ---dmroum�..or
.. .r.nu r.a l III anlaI of off NLY
92453418
U: 3 : 1'.1 3..1_ [...1 U I.:a tI v L..,.. I t
Prese ,Ia Types:(1) NVk add,(2) a(un<add,(3)hydreN«Icacd,(<)wdlum hvdro4du,(5) uncacets[c
6) -ethanol. (7) sodium bisulfate; (a) so iium dtksWh[e, (9) hexane. (A) ascorbic adtl, (B)ammonium sdfare,
Q emmmium hydr«Ide, (0) TSP, (U) UmprewNW, (0) other
a.6t/[.Lett YNx
Cun[odY-. 519naturee. Pr acnt �Y.W BA
[
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stetngestucvr<"Pr sent y�[YN
•�
CsOurEr¢ ecl BoCCI
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SHORTHOLDS`PRESENT(<72hows)b Y "N
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tab Sample Temperature.Info " -'
`Temp BWrtk'.Reoelveil Y N NA .
Lab TractlrgP -
rm IDa;OOS
'Cover 1 Temp Upon Redelpti a -r oC
Cooler l7fiemi[m'FaaoC
Sample rernrved via : -;; -. �.
EDDf UPS ) client [porter Pace Courier
-�CoolerlCartedted Temp oC
- "Cammenb
D.teRlore:
}: MTI[ IAB IAE ONL
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Date/Time:
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TND Blank Rebexued' Y : N NA -
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Page:_
NO,.

Document Name:
Document Issued: March 14, 2019
Bottle Identification Form (BIF)
Page 1 of 1
Document No.:
Issuing Authority:
i BCBAlIBIyl�CBj
F-CAR•CS-043•Rev.00
Pace Carolinas Quality Office
'Check mark top half of box If pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptlans: VOA, Caliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLH9
"Bottom half of box is to list number of bottle
Projects WO# : 92453418
PM: TIH Due Date: 11/26/19
CLIENT: 92—PIED GEOL
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pH Adjustment Log for Preserved Samples
Sample to
Type of preservative
pH upon receipt
Date preservation adjusted
Time preservation
Amount of Preservative
Lot If
adjusted
added
N nr a. lAlAnn ui....
rl. �... l.. Jr. .-„��.r�_•r
_.�in_,
___r_ _ .....
.... ..
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Out of hold, Incorrect preservative, out of temp. Incorrect containers.
Page 25 of 25