NCG030145_MONITORING INFO_20191113

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
DOCTYPE.
❑ HISTORICAL FILE
[)' MONITORING REPORTS
DOC DATE
❑ Q 9.
YYYYMMDD

Semi-annualStormwaterDischarge MonitoringReport
for North Carolina Division of Water Qu lit General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGENO. NCG030145 SAMPLE COLLECTION YEAR: 2019
FACILITY NAME: Newton Instruments SAMPLE PERIOD❑ Jan -June[:] July -Dec
COUNTY: Granville ECEIVE ®Monthly' October2019
R
PERSON COLLECTING SAMPLES: Nicholas Murphrev EC SCHARGING TO CLASS❑ORW®HQW❑Trout❑PNA
LABORATORY: : Pace Analytical Lab Cert. N: 40 NOV 18 20 OZero-flow❑Water Supply❑SA
Comments on sample collection or analysis: Monthly sampling ❑Other
GENTi UAL FILES
DWR SECTIOi*LEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3-->
Part A: Stormwater Benchmarks and Monitoring Results
n No discharge this period?z
Non -Polar
Outfall No.
Date Sample
24-hour rainfall
Total Suspended
PH,
Standard
Copper
Lead
Zinc
O&G/ Total
Total Toxic
Collected'
amount,
Solids
Petroleum
Organics'
(mo/dd/yr)
Inches'
units
Hydrocarbons
Benchmarks =__>
-
-
100 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
001
10/16/19
0.3
32.6 mg/L
7.5
0.0059 mg/L
0.0024 mg/L
0.0385 mg/L
1.7 mg/L
Not Detected
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
"See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan mayso certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
Permit Date: 11/1/2017-10/31/2022 SWU-245, last revised 10/25/2012
Page 1 of 3

stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing theallthe provisions of the
solvent management plan included in the stormwater Pollution Prevention Plan."
Name (Print me)
Title (Pr' t title)
(Signature) ( ate)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. see General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging> 55 gal of new oil per month.
❑ No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Non -polar O&G/TPH by
EPA 1664(SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
-
15 mg/L
100 mg/L or 50 mg/L•
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
" See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. see General Permit text.
Permit Date:11/1/2017-10/31/2022
SWU-245, last revised 10/25/2012
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL?YES ® NO ❑
IF YES,HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE?YES ® NO ❑
REGIONAL OFFICE CONTACT NAME: John Holley
Mail an original and one copy of this DMR including all "No Discharge" reports within 30 days of receiptof the lab results for at end of monitoring period in
the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Date)
Permit Date:11/1/2017-10/31/2022 SWU-245, last revised 10/25/2012
Page 3 of 3

aceAnalytical
wwwpacelaes.com
October 30, 2019
Mr. Pete Dressel
Piedmont Geologic
6003 Chapel Hill Road
Suite 109
Raleigh, NC 27607
RE: Project: Newton Instruments / 1912
Pace Project No.: 92449952
Dear Mr. Dressel:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 16, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Jonathan Murphrey, Piedmont Geologic
Acci
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 30

'I
Pace Analytical Services, LLO
aceAnalytical s
9900 Kincey Ave. Suite100
Huntersville, NC 28078078
www pacelabs.11
[phone]
CERTIFICATIONS
Project: Newton Instruments 11912
Pace Project No.: 92449952
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
VirginialVELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification If: M-NC030
Vifginia/VELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
Eden Certification IDS
205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633
North Carolina Drinking Water Certification #: 37738 Virginia/VELAP Certification M 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. -LC. Page 2 of 30

s
aceAnalytical
wwwpacelaCs.wm
Project: Newton Instruments / 1912
Pace Project No.: 92449952
Lab ID Sample ID
SAMPLE SUMMARY
Matrix Date Collected Date Received
92449952001 Outfall-001 Water 10/1611908:00 10/16/1914:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)B75-9092
Page 3 of 30

e
ace Analytical
wwrw.pacelaCs.tom
SAMPLE ANALYTE COUNT
Project: Newton Instruments / 1912
Pace Project No.: 92449952
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytts
Reported
Laboratory
92449952001 Outfall-001 SM 254OD-2011
NMH
1
PASI-E
EPA 1664B
AAC1
1
PASI-C
EPA 608.3
SEM
29
PASI-C
EPA 200.7 Rev 4.4 1994
SER, SH1
12
PASI-A
EPA 245.1 Rev 3.01994
SOO
1
PASI-A
EPA625.1
PKS
62
PASI-C
EPA 624.1
SAS
32
PASI-C
EPA 420.4 Rev 1.0 1993
KDF1
1
PASI-A
SM 4500-CN-E-2011
3J1-11
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 30

0
aceAnalytical
w pacelabs.mm
ANALYTICAL RESULTS
Project: Newton Instruments / 1912
Pace Project No.: 92449952
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Sample: Outfall-001
Parameters
Lab ID:
Results
92449952001
Units
Collected:
Report
Limit
1011611908:00
MDL OF
Received: 10/16/1914:30 Matrix: Water
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
32.6
mg/L
4.0
4.0
1
10/17/19 12:39
HEM, Oil and Grease
Analytical
Method: EPA 1664E
Oil and Grease
1.7.1
mg/L
4.8
1.2
1
10/30/19 11:09
608 PCB Pest RVE
Analytical
Method: EPA 608.3 Preparation Method: EPA 608.3
Aldrin
NO
ug/L
0.050
0.022
1
10/22/19 16:57
10/25/19 00:47
309-00-2
alpha-BHC
NO
ug/L
0.050
0.019
1
10/22/19 16:57
10/25/19 00:47
319-84-6
beta-BHC
NO
ug/L
0.050
0.014
1
10/22/19 16:57
10/25/19 00:47
319-85-7
delta-BHC
NO
ug/L
0.050
0.020
1
10/2211916:57
10/25/19 00:47
319-86-8
,gamma-BHC (Lindane)
NO
ug/L
0.050
0.012
1
10/22/19 16:57
10/25/19 00:47
58-89-9
Chlordane (Technical)
ND
ug/L
0.50
0.20
1
10/22/19 16:57
10/25/19 00:47
57-74-9
alpha -Chlordane
ND
ug/L
0.050
0.0090
1
10/22/19 16:57
10/25/19 00:47
5103-71-9
gar0ma-Chlordane
ND
ug/L
0.050
0.017
1
10/22/19 16:57
10/25/19 00:47
5103-74-2
4,4'-DDD
NO
ug/L
0.050
0.0069
1
1012211916:57
10/25/19 00:47
72-54-8
4,4'-DDE
NO
ug/L
0.050
0.0064
1
10/22/19 16:57
10/25119 00:47
72-55-9
4 4'-DDT
NO
ug/L
0.050
0.018
1
10/22/19 16:57
10/25/19 00:47
50-29-3
Dieldrin
ND
ug/L
0,050
0.0073
1
10/22/19 16:57
10/25/19 00:47
60-57-1
Endosulfan I
ND
ug/L
0.050
0,0094
1
10/22119 16:57
10/25/19 00:47
959-98-8
Endosulfan II
NO
ug/L
0,050
0.0065
1
10/22/19 16:57
10/25/19 00:47
33213-65-9
Endosulfan sulfate
NO
ug/L
0.050
0.0091
1
10/22/19 16:57
10/25/19 00:47
1031-07-8
Endrin
NO
ug/L
0.050
0.0089
1
10/22/19 16:57
10/25/19 00:47
72-20-8
Endrin aldehyde
NO
ug/L
0.050
0.013
1
10/22/19 16:57
10/25/19 00:47
7421-93-4
Heptachlor
NO
ug/L
0.050
0.016
1
10/22/19 16:57
10/2511900:47
76-44-8
Heptachlor epoxide
NO
ug/L
0.050
0.0097
1
10/22/19 16:57
10/25/19 00:47
1024-57-3
PCB-1016 (Arodor 1016)
NO
ug/L
0.50
0.22
1
10/22/19 16:57
10/25/19 00:47
12674-11-2
PCB-1221 (Aroclor 1221)
NO
ug/L
0.50
0.32
1
10/22119 16:57
10/25/19 00:47
11104-28-2
PCB-1232 (Aroclor 1232)
NO
ug/L
0.50
0.21
1
10/22/19 1657
10/25/19 00:47
11141-16-5
PCB-1242 (Aroclor 1242)
NO
ug/L
0.50
0.44
1
10/22/19 16:57
10/25/19 00:47
53469-21-9
PCB-1248 (Aroclor 1248)
NO
ug/L
0.50
0.34
1
10/22/19 16:57
10/25/19 00:47
12672-29-6
PCB-1254 (Arodor 1254)
ND
ug/L
0.50
0.24
1
10122/19 16:57
10/25/19 00:47
11097-69-1
PCB-1260 (Arodor 1260)
NO
ug/L
0.50
0.30
1
10/22/19 16:57
10/25/19 00:47
11096-82-5
Toxaphene
NO
ug/L
0.50
0.20
1
10/22/19 16:57
10/25/19 00:47
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
127
%
10-130
1
10/22/19 16:57
10/25/19 00:47
877-09-8
Decachlorobiphenyl (S)
86
%
10-130
1
10/22/19 16:57
10/25/19 00:47
2051-24-3
200.7 MET ICP
Analytical Method: EPA200.7 Rev 4.4 1994 Preparation Method: EPA200.7 Rev 4.41994
Antimony
NO
ug/L
5.0
3.0
1
10123119 23:38
10/28/19 09:05
7440-36-0
Arsenic
NO
ug/L
10.0
4.7
1
10/23/19 23:38
10/28/19 09:05
7440-38-2
Beryllium
NO
ug/L
1.0
0.20
1
10/23/19 23:38
10/29/19 03:09
7440.41-7
Cadmium
NO
ug/L
1.0
0.40
1
10/23/19 23:38
10/28/19 09:05
7440-43-9
Chromium
1.ad
ug/L
5.0
1.0
1
10123/1923:38
10/2811909:05
7440-47-3
Copper
5.9
ug/L
5.0
2A
1
10/23/19 23:38
10/28/19 09:05
7440-50-8
Lead
2.4.1
ug/L
5.0
1.6
1
10/23/19 23:38
10/28/19 09:05
7439-92-1
Nickel
2.1.1
ug/L
5.0
0.90
1
10/23/19 23:38
10128/19 09:05
7440-02-0
REPORT OF LABORATORY ANALYSIS
This report shall not 6e reproduced, except in full,
Date: 10/30/2019 05:52 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 30

s
lace Analytical
.Pacela6s.cam
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunter ille, NC 28a78
[phone]
Project: Newton Instruments / 1912
Pace Project No.: 92449952
Sample: Outfall-001
Lab ID:
92449952001
Collected:
10/16/1908:00
Received: 10/16/1914:30
Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Selenium
ND
ug/L
10.0
4.7
1
10/23/19 23:38
10/28/19 09:05
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
10/23/19 23:38
10/28/19 09:05
7440-22-4
Thallium
3.8J
ug/L
10.0
2.6
1
10/23/19 23:38
10/29/1903:09
7440-28-0 B
Zinc
38.5
ug/L
10.0
3.9
1
10/23/19 23:38
10/28/19 09:05
7440-66-6
245.1 Mercury
Analytical
Method: EPA245.1 Rev 3.0 1994 Preparation
Method: EPA 245.1
Rev 3.0 1994
Mercury
ND
ug/L
0.20
0.10
1
10/29/19 16:40
10/29/19 21:23
7439-97-6
625 RVE
Analytical
Method: EPA625.1 Preparation
Method: EPA625.1
Acenaphthene
ND
ug/L
5.0
1.6
1
10/22/19 15:58
10/2311913:27
83-32-9
Acenaphthylene
ND
ug/L
5.0
IS
1
10/22/19 15:58
10/23/1913:27
208-96-8
Anlhracene
ND
ug/L
5.0
1.7
1
10/22/191558
10/23/19 13:27
120-12-7
Benzidine
ND
ug/L
50.0
2.7
1
10/22/19 15:58
10/23/19 13:27
92-87-5
Benzo(a)anthracene
ND
ug/L
5.0
1.8
1
10/22/19 15:58
10/23/19 13:27
56-55-3
Benzo(a)pyrene
ND
uglL
5.0
2.1
1
10/22/19 15:58
10/2311913:27
50-32-8
Benzo(b)fluoranthene
ND
uglL
5.0
1.9
1
10/22/19 1558
10/23/19 13:27
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1.4
1
10/22/19 15:58
10/23/19 13:27
191-24-2
Benzo(k)0uoranthene
ND
ug/L
5.0
1.9
1
10122/1915:58
10/23/19 13:27
207-08-9
4-Bromophenylphenyl ether
ND
1
5.0
1.6
1
10/22/19 15:58
10/23/19 13:27
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1.6
1
10/22/19 15:58
10/23/19 13:27
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
2.8
1
10/22/19 15:58
10/23/19 13:27
59-50-7
!bis(2-Chloroelhoxy)methane
ND
ug/L
10.0
1.8
1
10/22/19 15:58
10/23/1913:27
111-91-1
'bis(2-Chloroelhyp ether
ND
ug/L
5.0
1.8
1
10/22/19 15:58
10/23/19 13,27
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1.5
1
10/22/19 15:58
10/23/19 13:27
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1.2
1
10/22/19 15:58
10123/19 13:27
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1.6
1
10/22/19 1558
10/23/19 13:27
7005-72-3
Chrysene
ND
ug/L
5.0
1.7
1
10122/1915:58
10/23/19 13:27
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1.6
1
10/22/19 1558
10/23/19 13:27
53-70-3
1,2-Dichlorobenzene
ND
ug/L
5.0
1.3
1
10/22/19 15:58
10/23/19 13:27
95-50-1
1,3-Dichlorobenzene
ND
ug/L
5.0
1.5
1
10/22/19 15:58
10/23/19 13:27
541-73-1
1,4-Dichlorobenzene
ND
ug/L
5.0
2.1
1
10/22/19 15:58
10/23/19 13:27
106-46-7
33'-Dichlorobenzidine
ND
ug/L
25.0
3.0
1
10/2211915:58
10/23/1913:27
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1.4
1
10/22/19 15:58
10123/19 13:27
120-83-2
Diethylphthalate
ND
ug/L
5.0
2.4
1
10/22/191558
10/2311913:27
84-66-2
2.4-Dimethylphenol
ND
1
10.0
1.4
1
10/22/19 15:58
10123/19 13:27
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1.6
1
10/22/19 15:58
10/23119 1327
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1.8
1
10/22/19 15:58
10/23/1913:27
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
15.2
1
10/22/19 15:58
10/23/19 13:27
534-52-1
2,4-Dinitrophenol
ND
1
50.0
40.5
1
10/22/191558
10/23/19 13:27
51-28-5
2,4-Dinitrololuene
ND
ug/L
5.0
1.2
1
10/22/19 15:58
10/23/19 13:27
121-14-2
2,6-Dinitrololuene
ND
ug/L
5.0
1.4
1
10122/1915:58
10/23/19 13:27
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1.8
1
10/22/19 15:58
10/23/19 13:27
117-84-0
1,2-Diphenylhydrazine
ND
ug/L
5.0
2.3
1
10/22/19 15:58
10/23/19 13:27
122-66-7
bis(2-Ethylhexyl)phthalate
ND
uglL
5.0
2.1
1
10/22/19 15:58
10/23/19 13:27
117-81-7
Fluoranlhene
ND
ug/L
5.0
1.7
1
10/22/1915:58
101231191327
206-44-0
Fluorene
ND
ug/L
5.0
1.6
1
10/22/19 15:58
10/23/19 13:27
86-73-7
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
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Huntersville, NC 28078078
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ANALYTICAL RESULTS
Project: Newton Instruments / 1912
Pace Project No.: 92449952
Sample: Outfall-001 Lab ID: 92449962001 Collected: 10/16/19 08:00 Received: 10/16/19 14:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
OF
Prepared
Analyzed
CAS No. Coal
625 RVE
Analytical Method: EPA625.1 Preparation
Method: EPA625.1
Hexachloro-1,3-butadiene
NO
ug/L
5.0
2.0
1
10/22/19 15:58
10/23/19 13:27
87-68-3
Hexachlorobenzene
NO
ug/L
5.0
1.7
1
10/22/19 15:58
10/23/1913:27
118-74-1
Hexachlorocyclopentadiene
NO
ug1L
10.0
1.7
1
10/22/19 15:58
10/23/19 13:27
77-47-4
Hexachloroethane
NO
ug/L
5.0
2.0
1
10/22/19 15:58
10/23/1913:27
67-72-1
Indeno(1,2,3-cd)pyrene
NO
ug/L
5.0
1.6
1
10/22/19 15:58
10/23/19 13:27
193-39-5
Isophorone
NO
ug/L
10.0
1.6
1
10/2211915:58
10/23/1913:27
78-50-1
Naphthalene
NO
ug/L
5.0
14
1
10/22/19 15:58
10/23/19 13:27
91-20-3
Nitrobenzene
NO
ug/L
5.0
2.1
1
10122/1915:58
10/23/19 13:27
98-95-3
2-Nitrophenol
NO
ug/L
5.0
14
1
10/2211915:58
10123/1913:27
88-75-5
4-Nitrophenol
NO
ugll-
50.0
3.5
1
10/22/19 15:58
10/23/19 13:27
100-02-7
N-Nitrosocimethylamine
NO
ug/L
5.0
1.2
1
10/22119 15:58
10123/19 13:27
62-75-9
N-Nitroso-di-n-propylamine
NO
ug/L
5.0
2.2
1
10/22/19 15:58
10123/19 13:27
621-64-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
1.7
1
10/22/19 15:58
10/2311913*27
86-30-6
Pentachlorophenol
NO
ug/L
10.0
2.2
1
10/22/19 15:58
10/23/19 13:27
87-86-5
Phenanthrene
NO
ug/L
5.0
1.7
1
10122/1915:58
10/2311913:27
85-01-8
Phenol
NO
ug/L
5.0
0.91
1
10/22/19 15:58
10/23/19 13:27
108-95-2
Pyrene
NO
ug/L
5.0
2.1
1
10/22/19 15:58
10/23/19 13:27
129-00-0
1,2A-Tdchlorobenzene
NO
ug/L
5.0
1.5
1
10/22/19 15:58
10/2311913:27
120-82-1
2,4,6-Tdchlorophenol
NO
ug/L
10.0
1.5
1
10122/19 15:58
10/23/19 13:27
88-06-2
Surrogates
,Nitrobenzene-d5 (S)
71
%
10-120
1
10/22/19 15:58
10/23/19 13:27
4165-60-0
'2-Fluorobiphenyl(S)
71
%
15-120
1
10/22/19 15:58
10/23/19 13:27
321-60-8
Terphenyl-d14(S)
80
%
11-131
1
10/2211915:58
10/23/19 13:27
1718-51-0
Phenol-d6 (S)
45
%
10-120
1
10/22/19 15:58
10/23/19 13:27
13127-88-3
2-Fluorophenol (S)
62
%
10-120
1
10/22/19 15:58
10/23/19 1327
367-12-4
2,4,6-Tribromophenol(S)
90
%
10-137
1
10/22/19 15:58
10/23/19 13:27
118-79-6
624 Volatile Organics
Analytical Method: EPA 624.1
Acrolein
NO
ug/L
5.0
3.8
1
10/18/19 21:18
107-02-8
Acrylonitrile
NO
ug/L
5.0
1.5
1
10/18/1921:18
107-13-1
Benzene
NO
ug1L
to
0.38
1
10/18/19 21:18
71-43-2
Bromodichloromethane
NO
ug/L
2.0
0.24
1
10/18/19 21:18
75-27-4
Bromoform
NO
ug/L
2.0
0.40
1
10/18/19 21:18
75-25-2
Bromomethane
NO
uglL
2.0
1.2
1
10/18/19 21:18
74-83-9
Carbon tetrachloride
NO
ug/L
2.0
0.29
1
10/18/19 21:18
56-23-5
Chlorobenzene
NO
ug/L
2.0
0.37
1
10/18/19 21:18
108-90-7
Chloroethane
NO
ug/L
2.0
1.4
1
10/18/19 21:18
75-00-3
2-Chloroethylvinyl ether
NO
ug/L
5.0
0.73
1
10/18/19 21:18
110-75-8 P5,c3
Chloroform
NO
ug/L
2.0
0.58
1
10/18/19 21:18
67-66-3
Chloromethane
NO
ug/L
2.0
0.73
1
10/18/19 21:18
74-87-3
Dibromochloromethane
NO
ug/L
2.0
0.32
1
10/18/19 21:18
124-48-1
M-Dichloroethane
NO
ug/L
2.0
0.51
1
10/18/19 21:18
75-34-3
1,2-Dichloreethane
NO
ug/L
2.0
0.34
1
10/18/19 21:18
107-06-2
1;1-Dichloroethene
NO
ug/L
2.0
0.41
1
10/18/19 21:18
75-35-4
trans-1,2-Dichloroethene
NO
ug/L
2.0
0.42
1
10/18119 21:18
156-60-5
1,2-Dichloropropane
NO
ug/L
2.0
0.27
1
10/18/19 21:18
78-87-5
REPORT OF LABORATORY ANALYSIS
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ace Analytical e
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ANALYTICAL RESULTS
Project: Newton Instruments / 1912
Pace Project No.: 92449952
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Sample: Outfall-001 Lab ID: 92449952001 Collected: 10/16/19 08:00 Received: 10/16/19 14:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
624 Volatile Organics
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroelhane
t Tetrachloroethene
Toluene
11, 1,1-Trichloroethane
11,2-Trichloroethane
Trichloroethene
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
11,2-Dichloroethanei14 (S)
420.4 Phenolics, Total
Phenol
4500CNE Cyanide, Total
Cyanide
Dale: 10/30/2019 05:52 PM
Analytical Method: EPA 624.1
ND
ug/L
2.0
0.33
1
10/18/19 21:18
10061-01-5
ND
ug/L
2.0
0.41
1
10/18/19 21:18
10061-02-6
ND
ug/L
1.0
0.28
1
10/18/19 21:18
100-41-4
ND
ug/L
2.0
0.24
1
10/18/19 21:18
75-09-2
ND
ug/L
2.0
0,34
1
10/18/19 21:18
79-34-5
ND
ug/L
2.0
0.28
1
10/18119 21:18
127-18-4
ND
uglL
1.0
0.44
1
1011811921:18
108-88-3
ND
ug/L
2.0
0.35
1
10/18/19 21:18
71-55-6
ND
ug/L
2.0
0.31
1
10/18/19 21:18
79-00-5
ND
ug/L
2.0
0.36
1
10/18/19 21:18
79-01-6
ND
ug/L
2.0
0.72
1
10/18/19 21:18
75-01-4
95
%
70-130
1
10/18/19 21:18
460-00-4
104
%
70-130
1
10/18/19 21:18
2037-26-5
97
%
70-130
1
10/18119 21:18
17060-07-0
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
ND mg/L 0.020 0.0050 1 10/28/19 09:40 10/28/19 14:49 108-95-2
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
ND mg/L 0.0080 0.0060 1 10/1911915:30 10/20/1911:28 57-12-5
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntemville, NC 28078
[phone]
Project: Newton Instruments / 1912
Pace Project No.: 92449952
QC Balch: 504212
Analysis Method:
SM 254OD-2011
QC Batch Method SM 254OD-2011
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92449952001
METHOD BLANK: 2709643
Matrix: Water
Associated Lab Samples: 92449952001
Blank Reporting
Parameter
Units
Result Limit
MDL Analyzed Qualifiers
Total Suspended Solids
l
mg/L
ND
2.5 2.5 10/17/19 12:36
LABORATORY CONTROL SAMPLE: 2709644
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
%Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 230
92 90-110
SAMPLE DUPLICATE: 2709645
92449916001 Cup
Max
Parameter
Units
Result Result
RPD RPD Qualifiers
Total Suspended Solids
mg/L
289
281 3 5
SAMPLE DUPLICATE: 2710806
92450126001 Cup
Max
Parameter
Units
Result Result
RPD RPD Qualifiers
Total Suspended Solids
mg/L
NO
ND 5
Results presentee on this page are In the units indicated by the "Unite" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Project: Newton Instruments 11912
Pace Project No.: 92449952
QC Batch: 506605
QC Batch Method: EPA 16646
Associated Lab Samples: 92449952001
METHOD BLANK: 2720433
Associated Lab Samples: 92449952001
Parameter Units
Oil and Grease mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit MDL Analyzed
NO 4.8 1.2 10/30/1910:53
Pace Analytical Services, LLC
9800 Kincey, Ave. Suite 100
Huntersville, NC 2807B
[phone]
Qualifiers
LABORATORY CONTROL SAMPLE: 2720434
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Oil and Grease mg/L 38.5 32.9 86 78-114
MATRIX SPIKE SAMPLE:
2720435
92449952001 Spike
MS MS % Rec
Parameter
Units
Result Conic.
Result %Rec Limits Qualifiers
Oil and Grease
mg/L
1.7J 38.5
33.3 82 78-114
Results presenter) on this page arc In the units Indicated by the "Units" column except where an alternate unit Is pmsented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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QUALITY CONTROL DATA
Project: Newton Instruments / 1912
Pace Project No.: 92449952
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 506453
Analysis Method: EPA 245.1 Rev 3.0 1994
OC Batch Method: EPA 245.1 Rev 3.01994
Analysis Description: 245.1 Mercury
Associated Lab Samples: 92449952001
METHOD BLANK: 2719896
Matrix: Water
Associated Lab Samples: 92449952001
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
Qualifiers
Mercury
ug/L
NO 0.20
0.10 10/29/19 20:33
LABORATORY CONTROL SAMPLE:
2719897
Spike
LCS
LCS
%Rec
Parameter
Units
Conc.
Result
%Rec
Limits
Qualifiers
Mercury
ug/L
2.5
2.3
93
85-115
4ABORATORY CONTROL SAMPLE:
2719933
Spike
LCS
LCS
%Rec
Parameter
Units
Conc.
Result
%Rec
Limits
Qualifiers
Mercury
ug/L
2.5
2.4
97
85-115
LABORATORY CONTROL SAMPLE:
2719934
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Mercury
ug/L
2.5
2.4
95
85-115
LABORATORY CONTROL SAMPLE:
2719935
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
%Rec
Limits
Qualifiers
Mercury
ug/L
2.5
2.3
91
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2719898
2719899
MS
MSD
92449628001
Spike
Spike MS
MSD
MS MSD
%Rec Max
Parameter Units
Result
Conc.
Conc. Result
Result
%Rec %Rec
Limits RPD RPD Qual
Mercury ug/L
ND
2.5
2.5 2.5
2.3
97 90 70-130 8 20
R
Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Newton Instruments / 1912
Pace Project No.: 92449952
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2719900
2719901
MS
MSD
_ 92449628002 Spike
Spike
MS
MSD MS MSD
e/ Rec Max
Parameter Units Result Conc.
Cone.
Result
Result e/ Rec % Rec
Limits RPD RPD Qual
Mercury ug/L ND 2.5
2.5
2A
2.5 97 100
70-130 4 20
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/30/2019 05:52 PM without the written consent of Pace Analytical Services. LLC.
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QUALITY CONTROL DATA
Project: Newton Instruments / 1912
Pace Project No.: 92449952
QC Batch: 505412
QC Batch Method: EPA 200.7 Rev 4.4 1994
Associated Lab Samples: 92449952001
Analysis Method:
Analysis Description:
EPA 200.7 Rev 4.4 1994
200.7 MET
METHOD BLANK: 2715416
Matrix: Water
Associated Lab Samples: 92449952001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
Antimony
ug/L
NO
5.0
3.0
10/28/19 07:33
Arsenic
ug/L
NO
10.0
4.7
10/28/19 07:33
Beryllium
ug/L
0.23J
1.0
0.20
10/29/19 02:46
Cadmium
ug/L
NO
1.0
0.40
10/28/19 07:33
Chromium
ug/L
ND
5.0
1.0
10/2811907:33
Copper
ug/L
ND
5.0
2.1
10/28/1907:33
Lead
ugi
NO
5.0
1.6
10/28119 07:33
Nickel
ug/L
NO
5.0
0.90
10/28/19 07:33
Selenium
ug/L
ND
10.0
4.7
10/28/19 07:33
Silver
ug/L
ND
5.0
2.5
10/28/19 07:33
Thallium
ug/L
4.3J
10.0
2.6
10/29119 02:46
Zinc
ug/L
ND
10.0
3.9
10/28/19 07:33
'LABORATORY CONTROL SAMPLE: 2715417
Pace Analytical Services, Li
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Antimony
ug/L
500
520
104
85-115
Arsenic
ug/L
500
521
104
85-115
Beryllium
ug/L
500
483
97
85-115
Cadmium
ug/L
500
485
97
85-115
-Chromium
ug/L
500
446
89
85-115
Copper
uglL
500
490
98
85-115
Lead
ug/L
500
499
100
85-115
Nickel
ug/L
500
479
96
85-115
Selenium
ug/L
500
501
too
85-115
Silver
ug/L
250
246
98
85-115
Thallium
ug/L
500
_
459
92
85-115
Zinc
uglL
500
491
98
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2715418
2715419
MS
MSD
92449868002
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
%Rec %Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
519
524
104 105
70-130
1
20
Arsenic
ug/L
ND
500
500
528
529
105 105
70-130
0
20
Beryllium
ug/L
ND
500
500
444
452
89 90
70-130
2
20
Cadmium
ug/L
NO
500
500
495
498
99 100
70-130
1
20
Chromium
ug/L
5.8
500
500
461
465
91 92
70-130
1
20
Results presented on this page am in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/30/2019 05:52 PM without the written consent of Pace Analytical Services, LLC.
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(�IaceAnalyfical'
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Nuntersville, NC 28078
[phone]
Project: Newton Instruments / 1912
Pace Project No.: 92449952
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2715418
2715419
MS
MSD
92449868002
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Cone.
Cone,
Result
Result
%Rec
%Rec
Limits
RPD
RPD Dual
Copper
ug/L
- 9.3
500
500
503
506
99
99
70-130
1
20
Lead
ug/L
ND
500
500
505
512
100
102
70-130
1
20
Nickel
ug/L
ND
500
500
484
489
96
97
70-130
1
20
Selenium
ug/L
ND
500
500
534
536
107
107
70-130
0
20
Silver
ug/L
ND
250
250
252
252
101
101
70-130
0
20
Thallium
ug/L
ND
500
500
473
479
94
95
70-130
1
20
Zinc
ug/L
349
500
500
831
842
96
99
70-130
1
20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2715420
2715421
MS
MSD
92449922001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Cone.
Cone,
Result
Result
%Rec
%Rec
Limits
RPD
RPD Dual
Antimony
ug/L
7.0
500
500
536
539
106
106
70-130
0
20
Arsenic
ug/L
ND
500
500
564
570
112
113
70-130
1
20
Beryllium
ug/L
ND
500
500
492
498
98
100
70-130
1
20
Cadmium
ug/L
ND
500
500
504
507
101
101
70-130
1
20
Chromium
ug/L
ND
500
500
461
463
92
93
70-130
1
20
Copper
ug/L
6.0
500
500
520
523
103
103
70-130
1
20
Lead
ug/L
ND
500
500
500
498
100
99
70.130
0
20
,!Nickel
ug/L
10.6
500
500
486
487
95
95
70-130
0
20
Selenium
ug/L
ND
500
500
518
514
103
102
70-130
1
20
Silver
ug/L
ND
250
250
260
261
104
104
70-130
1
20
,Thallium
ug/L
ND
500
500
408
421
82
84
70-130
3
20
,Zinc
ug/L
122
500
500
631
636
102
103
70-130
1
20
Results presented on this page are In the units
Indicated by the "Units" column
except where an alternate
unit is presented to the
right of the result.
REPORT OF
LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/30/2019 05:52 PM
without the written
consent of Pace Analytical Services,
LLC.
Page 14 of 30

Pace Analytical Services, LLC
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aceAnalytical
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Huntersville, NC 28078
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[phone]
QUALITY CONTROL DATA
Project: Newton Instruments 11912
Pace Project No.: 92449952
OC Batch: 504567
Analysis Method: EPA 624.1
OC Balch Method: EPA 624.1
Analysis Description: 624 MSV
Associated Lab Samples: 92449952001
METHOD BLANK: 2711636
Matrix:
Water
Associated Lab Samples: 92449952001
- Blank
Reporting
Parameter
Units
Result
Limit MOIL
Analyzed Qualifiers
1,1,1-Tdchloroethane
ug/L
NO
2.0
0,35
10/18/19 15:22
1,1,2,2-Tetrachloroethane
ug/L
NO
2.0
0.34
10/18/19 15:22
1,1,2-Trichloroethane
ug/L
NO
2.0
0.31
10/18/19 1522
1,1-Dichloroethane
ug/L
NO
2.0
0.51
10/18/19 15:22
" 1,1-Dichloroethane
ug/L
NO
2.0
0.41
10/18/19 15:22
1,2-Dichloroethane
ug/L
NO
2.0
0.34
10/18/19 15:22
1,2-Dichloropropane
ug/L
NO
2.0
0.27
10118/19 15:22
2-Chloroelhylvinyl ether
ug/L
NO
5.0
0.73
10/18/19 15:22
Acrolein
ug/L
NO
5.0
3.8
10/18/19 15:22
Acrylonitrile
ug/L
NO
5.0
1.5
10/1811915:22
,I Benzene
ug/L
NO
1.0
0.38
10/18/19 15:22
Bromodichloromethane
ug/L
NO
2.0
0.24
10/18/191522
Bromoform
ug/L
NO
2.0
0.40
10/18/19 15:22
Bromomethane
ug/L
NO
2.0
1.2
10/18/19 15:22
Carbon tetrachloride
ug/L
NO
2.0
0.29
10118/19 15:22
Chlorobenzene
ug/L
NO
2.0
0.37
10/18/19 15:22
I,Chloroethane
ug/L
NO
2.0
1.4
10/1811915:22
i Chloroform
ug/L
NO
2.0
0.58
10118119 15:22
Chloromethane
ug/L
NO
2.0
0.73
1011811915:22
cis-1.3-Dichloropropene
ug/L
NO
2.0
0.33
10/18/19 15:22
Dibromochloromethane
ug/L
NO
2.0
0.32
10/18/19 15:22
Ethylbenzene
ug/L
NO
1.0
0.28
10/18/19 15:22
Methylene Chloride
ug/L
NO
2.0
0.24
10/18/19 15:22
Tetrachloroethene
ug/L
NO
2.0
0,28
10/18/19 15:22
Toluene
ug/L
NO
1.0
0.44
10/18/19 15:22
trans-1,2-Dichloroethene
ug/L
NO
2.0
0.42
10/18/19 15:22
,trans-1,3-Dichloropropene
ug/L
NO
2.0
0.41
10/18/19 15:22
Trichlorcethene
ug/L
NO
2.0
0.36
10/18/19 15:22
Vinyl chloride
ug/L
ND
2.0
0.72
10/18/19 15:22
'1,2-Dichloroethane-d4 (S)
%
98
70-130
10/18/19 15:22
4-Bromofluorobenzene (S)
%
110
70-130
10/18/19 15:22
Toluene-d8 (S)
%
110
70-130
10/18/19 15:22
LABORATORY CONTROL SAMPLE: 2711637
Spike
LCS 1-CS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
1,1,1-Tdchloroethane
ug/L
20
21.3 107
70-130
1,1,2,2-Tetrachloroethane
ug/L
20
21.8 109
60-140
1,1,2-Trichloroethane
ug/L
20
24.3 122
70-130
1,1-Dichloroethane
ug/L
20
22.6 113
70-130
Results presented on this page are in the units Indicated by the "Units"
column except where an alternate unions
presented to the right ofthe result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/30/2019 05:52 PM without the written consent of Pace Analytical Services, LLC. Page 15 0f 30

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QUALITY CONTROL DATA
Project: Newton Instruments / 1912
Pace Project No.: 92449952
LABORATORY CONTROL SAMPLE:
Parameter
2711637
Units
Spike
Conic.
LCS
Result
LCS
%Rec
%Rec
Limits
1,1-Dichloroethene
ug/L
20
21.8
109
50-150
1,2-Dichloroethane
ug/L
20
20.7
103
49-155
1,2-Dichloropropane
ug/L
20
22.6
113
35-165
2-Chloroethylvinyl ether
ug/L
40
85.1
213
1-225
Acrolein
ug/L
100
122
122
60-140
Acrylonitrile
ug/L
100
118
118
60-140
Benzene
ug/L
20
24.0
120
65-135
Bromodichloromethane
ug/L
20
21.7
108
65-135
Bromoform
ug/L
20
20.4
102
70-130
Bromomethane
ug/L
20
23.4
117
15-185
Carbon tetrachloride
ug/L
20
20.5
102
70-130
Chlorobenzene
ug/L
20
19.9
100
65-135
Chloroethane
ug/L
20
24.4
122
40-160
Chloroform
ug/L
20
22.5
112
70-135
Chloromelhane
ug/L
20
24.6
123
1-205
cis-1,3-Dichloropropene
ug/L
20
24.7
124
25-175
Dibromochloromethane
ug/L
20
19.2
96
70-135
Ethylbenzene
ug/L
20
20.9
104
60-140
Methylene Chloride
ug/L
20
21.3
106
60-140
Tetrachlorcethene
ug/L
20
20.0
100
70-130
Toluene
ug/L
20
23.2
116
70-130
trans-1,2-Dichloroethene
ug/L
20
21.5
107
70-130
trans-1,3-Dichloropropene
ug/L
20
23.9
119
50-150
Trichlorcethene
ug/L
20
23.3
117
65-135
Vinyl chloride
ug/L
20
24.8
124
5-195
1,2-Dichloroethane-d4 (S)
%
87
70-130
4-Bromofluorobenzene (S)
%
105
70-130
Toluene-d8 (S)
%
105
70-130
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2711638
MS
92449952001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2711639
MS
Result
MSD
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD Qual
1,1,1-Tdchloroethane
ug/L
NO
20
20
25.2
25.3
126
127
52-162
0
36
1,1,2,2-Tetrachloroethane
ug/L
NO
20
20
21.2
21.8
106
109
46-157
3
61
1,1,2-Tdchloroethane
ug/L
NO
20
20
24.2
24.6
121
123
52-150
2
45
1,1-Dichlorcethane
ug/L
ND
20
20
24.6
25.3
123
126
59-155
3
40
1,1-Dichloroethene
ug/L
NO
20
20
25.0
25.2
125
126
1-234
1
32
1,2-Dichloroethane
ug/L
NO
20
20
22.5
22.7
113
114
49-155
1
49
1,2-Dichloropropane
ug/L
NO
20
20
24.0
24.5
120
123
1-210
2
55
2-Chloroethylvinyl ether
ug/L
NO
40
40
NO
NO
0
0
1-305
71 P5
Acrolein
ug/L
NO
100
100
110
119
110
119
40-160
8
60
Acrylonitrile
ug/L
NO
100
100
105
107
105
107
40-160
2
60
Benzene
ug/L
NO
20
20
23.6
24A
118
121
37-151
2
61
Bromodichloromethane
ug/L
NO
20
20
24.5
24.6
122
123
35-155
0
56
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/30/2019 05:52 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 30

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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave: Suite 100
Huntersville, NC 28078
[phone]
. Project: Newton Instruments / 1912
Pace Project No.: 92449952
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2711638
2711639
MS
MSD
92449952001
Spike
Spike
MS
MSD
MS
MSD
e/ Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD
RPD Dual
. Bromoform
ug/L
NO
20
20
23.6
23.6
118
118
45-169
0
42
Bromomethane
ug/L
ND
20
20
21.8
25.2
109
126
1-242
15
61
" Carbon tetrachloride
ug/L
NO
20
20
23.2
23.3
116
117
70-140
1
41
Chlorobenzene
ug/L
NO
20
20
21.6
21.7
108
109
37-160
1
53
„ Chloroelhane
ug/L
NO
20
20
29.4
28.7
147
144
14-230
2
78
Chloroform
ug/L
NO
20
20
24.6
24.8
123
124
51-138
1
54
Chloromethane
ug/L
NO
20
20
34.4
33.7
171
167
1-273
2
60
' cis-1,3-Dichloropropene
ug1L
ND
20
20
25.6
26.6
128
133
1-227
4
58
Dibromochloromethane
ug/L
NO
20
20
23A
23.6
117
118
53-149
1
50
Elhylbenzene
ug/L
NO
20
20
21.6
21.4
108
107
37-162
1
63
Methylene Chloride
ug/L
NO
20
20
19.7
20.1
99
100
1-221
2
28
Telrachloroelhene
uglL
ND
20
20
21.5
21.1
107
106
64-148
2
39
Toluene
ug/L
ND
20
20
22A
22.8
112
114
47-150
2
41
trans-1,2-Dichloroethene
uglL
NO
20
20
25.5
25.7
128
128
54-156
1
45
trans-1,3-Dichloropropene
ug/L
NO
20
20
25.0
26.0
125
130
17-183
4
86
Trichloroethene
ug/L
NO
20
20
23.0
23.2
115
116
70-157
1
48
Vinyl chloride
ug/L
NO
20
20
33.0
32.9
165
164
1-251
0
66
1,2-Dichloroelhane-d4 (S)
%
104
104
70-130
i4-Bromoffuorobenzene(S)
e/
102
98
70-130
. Toluene-d8(S)
%
100
100
70-130
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right at the resu h.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 10/30/2019 05:52 PM without the wriften consent of Pace Analytical Services, L-C.
Page 17 of 30

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.pacelebs.00m
QUALITY CONTROL DATA
Project: Newton Instruments / 1912
Pace Project No.: 92449952
QC Batch: 504938
QC Batch Method: EPA 608.3
Associated Lab Samples: 92449952001
Analysis Method:
Analysis Description:
EPA608.3
608 PCB Pest Red Vol
METHOD BLANK: 2713158
Matrix: Water
Associated Lab Samples: 92449952001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
4,4'-DDD
ug/L
NO
0.050
0.0069
10125/1902:15
4,4'-DDE
ug/L
NO
0.050
0,0064
10/25/19 02:15
4,4'-DDT
ug/L
NO
0.050
0,018
10/25/19 02:15
Aldrin
ug/L
ND
0.050
0.022
10125/19 02:15
alpha-BHC
ug/L
ND
0.050
0.019
10/25/19 02:15
alpha -Chlordane
ug/L
NO
0.050
0.0090
10/25/19 02:15
beta-BHC
ug/L
ND
0.050
0.014
10/25/19 02:15
Chlordane (Technical)
ug/L
NO
0.50
0.20
10/25/19 02:15
delta-BHC
ug/L
ND
0,050
0.020
10125/1902:15
Dieldrin
ug/L
ND
0.050
0,0073
10/25/19 02:15
Endosulfan)
uglL
ND
0.050
0.0094
10/25/19 02:15
Endosulfan ll
ug/L
ND
0.050
0.0065
10/25/19 02:15
Endosulfan sulfate
ug/L
ND
0.050
0.0091
10/25/19 02:15
Endrin
ug/L
NO
0.050
0.0089
10125/1902:15
Endrin aldehyde
ug/L
NO
0.050
0,013
10/25/19 02:15
gamma-BHC (Lindane)
ug/L
ND
0.050
0.012
10/25/19 02:15
gamma -Chlordane
ug/L
ND
0.050
0,017
10/25/19 02:15
Heptachlor
ug/L
NO
0.050
0,016
10/25/19 02:15
Heptachlor epoxide
ug/L
NO
0.050
0.0097
10/25/19 02:15
PCB-1016 (Arodor 1016)
ug/L
ND
0.50
0.22
10/25/19 02:15
PCB-1221 (Aroclor 1221)
ug/L
NO
0.50
0.32
10/25/19 02:15
PCB-1232 (Arodor 1232)
ug/L
ND
0.50
0.21
10/25119 02:15
PCB-1242 (Arodor 1242)
ug/L
ND
0.50
0.44
10/25/19 02:15
PCB-1248 (Arodor 1248)
ug/L
ND
0.50
0.34
10/25/19 02:15
PCB-1254 (Arodor 1254)
ug/L
NO
0.50
0.24
10/25/19 02:15
PCB-1260 (Arodor 1260)
ug/L
NO
0.50
0.30
10/25/19 02:15
Toxaphene
ug/L
ND
0.50
0.20
10/2511902:15
Decachlorobiphenyl (S)
%
113
10-130
10/25/19 02:15
Tetrachloro-m-xylene (S)
%
102
10-130
10/25/19 02:15
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
LABORATORY CONTROL SAMPLE:
2713159
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
%Rec
Limits Qualifiers
4,4'-DDD
ug/L
0.25
0.26
104
31-141
4,4'-DDE
ug/L
0.25
0.24
94
30-145
4,4'-DDT
ug/L
0,25
0.25
101
25-160
Aldrin
ug/L
0.25
0.18
72
42-140
alpha-BHC
ug/L
0.25
0.24
94
37-140
alpha -Chlordane
ug/L
0.25
0.24
96
45-140
beta-BHC
ug/L
0.25
0.34
134
17-147
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the rose R.
REPORT OF LABORATORY ANALYSIS
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Date: 10/30/2019 05:52 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 30

i
aceAnalytical
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QUALITY CONTROL DATA
Project: Newton Instruments 11912
Pace Project No.: 92449952
LABORATORY CONTROL SAMPLE:
Parameter
2713159
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
delta-BHC
ug/L
0.25
0.25
100
19-140
Dieldrin
ug/L
0.25
0,25
102
36-146
Endosulfan I
uglL
0.25
0.27
108
45-153
Endosulfan 11
uglL
0.25
0,26
106
1-202
Endosulfan sulfate
ug/L
0.25
0.25
100
26-144
Endrin
ug/L
0.25
0.26
106
30-147
Endrin aldehyde
ug/L
0.25
0.22
88
50-150
gamma-BHC (Lindane)
ug/L
0.25
0.23
94
32-140
gamma -Chlordane
ug/L
0.25
0,24
97
45-140
Heptachlor
ug/L
0.25
0,19
78
34-140
Heptachlor epoxide
ug/L
0.25
0.24
95
37-142
Decachlorobiphenyl (S)
%
110
10-130
,I Tetrachloro-m-xylene (S)
%
84
10-130
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2713160
MS
92450365001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2713161
MS
Result
MSD
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD Qual
4,4'-DDD
ug/L
NO
0.25
0.25
0.30
0.31
118
123
31-141
4
39
4,4'-DDE
ug/L
ND
0.25
0.25
0.25
0.29
100
116
30-145
14
35
4,4'-DDT
ug/L
ND
0.25
0.25
0.31
0.33
122
133
25-160
8
42
Aldrin
ug/L
NO
0.25
0.25
0.21
0.28
84
111
42-140
28
35
alpha-BHC
ug/L
NO
0.25
0.25
0.26
0.31
105
124
37-140
17
36
alpha -Chlordane
ug/L
NO
0,25
0.25
0.26
0.31
105
123
45-140
15
35
beta-BHC
ug/L
NO
0.25
0.25
0.26
0.30
105
121
17-147
14
44
delta-BHC
ug/L
ND
0.25
0.25
0.28
0.31
110
123
19-140
11
52
Dieldrin
ug/L
ND
0.25
0.25
0.27
0.30
108
121
36-146
11
49
. Endosulfan I
ug/L
ND
0.25
0.25
0.28
0.32
110
128
45-153
15
28
Endosulfan II
ug/L
NO
0.25
0.25
0.27
0.32
110
126
1-202
14
53
Endosulfan sulfate
ug/L
NO
0.25
0.25
0.27
0.32
109
128
26-144
16
38
Endrin
ug/L
NO
0.25
0.25
0.28
0.32
113
127
30-147
12
48
Endrin aldehyde
ug/L
NO
0.25
0.25
0.25
0.28
101
113
50-150
11
30
gamma-BHC (Lindane)
ug/L
NO
0.25
0.25
0.27
0.32
107
126
32-140
16
39
gamma -Chlordane
ug/L
ND
0.25
0.25
0.26
0.31
103
126
45-140
20
35
Heptachlor
ug/L
NO
0.25
0.25
0.24
0.29
95
115
34-140
19
43
Heptachlor epoxide
ug/L
NO
0.25
0.25
0.25
0.29
102
118
37-142
15
26
Decachlorobiphenyl (S)
%
95
116
10-130
Tetrachloro-m-xylene IS)
%
82
108
10-130
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the fight of the result.
i
Date: 10/30/2019 05:52 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 30

aceAnalytili
wawpacelabscom
QUALITY CONTROL DATA
Project: Newton Instruments / 1912
Pace Project No.: 92449952
QC Batch: 504976 Analysis Method: EPA625.1
QC Batch Method: EPA625.1 Analysis Description: 625 MSS
Associated Lab Samples: 92449952001
METHOD BLANK: 2713443
Associated Lab Samples: 92449952001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MOIL
Analyzed
1,2,4-Tdchlorobenzene
ug/L
NO
5.0
1.5
10/22/19 22:12
1,2-Dichlorobenzene
ug/L
NO
5.0
1.3
10122/19 22:12
1,2-Diphenylhydrazine
ug/L
NO
5.0
2.3
10/22/19 22:12
1,3-Dichlorobenzene
ug/L
NO
5.0
1.5
10122/19 22:12
1,4-Dichlorobenzene
ugli-
NO
5D
2.1
10/22/1922:12
2,4,6-Trichlorophenol
ug/L
NO
10.0
1.5
10/22/19 22:12
2,4-Dichlorophenol
ug/L
NO
5.0
1.4
10/22/19 22:12
2,4-Dimethylphenol
ug/L
NO
10.0
1.4
10/22/19 22:12
2,4-Dinitrophenol
uglL
NO
50.0
40.5
10/22/1922:12
2,4-Dinitrotoluene
ug/L
NO
5.0
1.2
10/22/19 22:12
2,6-Dinitrotoluene
ug/L
NO
5.0
1.4
10/22/19 22:12
2-Chloronaphthalene
ug/L
NO
5.0
1.5
10/22/19 22:12
2-Chlorophenol
ug1L
NO
5.0
1.2
10/22/19 22:12
2-Nitrophenol
ug1L
NO
5.0
1.4
10/22/19 22:12
3,3'-Dichlorobenzidine
ug/L
- NO
25.0
3.0
10/22/19 22:12
'. 4,6-Dinitro-2-methylphenol
ug/L
NO
20.0
15.2
10/22/19 22:12
4-Bromophenylphenyl ether
ug/L
NO
5.0
1.6
10/22/19 22:12
4-Chloro-3-methylphenol
ug/L
NO
5.0
2.8
10/22/19 22:12
4-Chlorophenylphenyl ether
ug/L
NO
5.0
1.6
10/22/19 22:12
4-Nitrophenol
ug/L
NO
50.0
3.5
10/22/19 22:12
Acenaphthene
ug/L
NO
5.0.
1.6
10/22/19 22:12
Acenaphthylene
ug/L
NO
5.0
1.6
10/22/19 22:12
Anthracene
ug/L
ND
5.0
1.7
10/22/19 22:12
Benzif ine
ug/L
ND
• 50.0
2.7
10/22/19 22:12
Benzo(a)anthracene
ug/L
NO
5.0
1.8
10/22/19 22:12
Benzo(a)pyrene
ug/L
NO
5.0
2.1
10/22/19 22:12
Benzo(b)fluoranthene
ug/L
NO
5.0
1.9
10/22/19 22:12
Benzo(g,h,i)perylene
ug/L
NO
5.0
1.4
10/22/19 22:12
Benzo(k)fluoranthene
ug/L
ND
5.0
1.9
10/22/19 22:12
bis(2-Chloroethoxy)methane
ug/L
NO
10.0
1.8
10/22/19 22:12
bis(2-Chloroethyl) ether
ugli-
NO
5.0
1.8
10/22/19 22:12
bis(2-Ethylhexypphthalate
ug/L
NO
5.0
2.1
10/22/1922*12
Butylbenzyl phthalate
ug/L
NO
5.0
1.6
10/22/19 22:12
Chrysene
ug/L
NO
5.0
1.7
10/22/19 22:12
Di-n-butylphthalate
ug/L
ND
5.0
1.8
10/22/19 22:12
I'Di-n-octylphthalate
ug/L
NO
5.0
1.8
10/22/19 22:12
Dibenz(a,h)anthracene
ug/L
ND
5.0
1.6
10/22/19 22:12
Diethylphthalale
ug/L
NO
5.0
2.4
10122/19 22:12
Dimethylphtha late
ug/L
NO
5.0
1.6
10/22/19 22:12
Fluoranthene
ug/L
NO
5.0
1.7
10/22/19 22:12
Fluorene
ug/L
ND
5.0
1.6
10/22/19 22:12
Pace Analytical Services, LLC
9800 Kncey Ave. Suite 100
Huntersville, NC 2BO78
[phone]
Qualifiers
Results presentee on this page are In the units Indicated by the "Units" column except wbom an alternate unit is presentee to the dgbt of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/30/2019 05:52 PM without the written consent of Pace Analytical Services, -I-C. Page 20 of 30

it
ro
aceAnalytical
ewwpecrelabs.rom
Project: Newton Instruments 11912
Pace Project No.: 92449952
METHOD BLANK: 2713443
Associated Lab Samples: 92449952001
Parameter
Hexachloro-1,3-butadiene
Hexachlorobenzene
HexachIorocyclopentatiene
Hexachlorc ethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Ni troso-di-n-propyl a mi ne
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
q PeMachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,6-Tdbromophenol(S)
2-Fluorobiphenyl(S)
2-Fluorophenol(S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
I� Terphenyl-d14 (S)
QUALITY CONTROL DATA
Matrix: Water
Units
Blank
Result
Reporting
Limit
MDL
Analyzed
ug/L
NO
5.0
2.0
10/22/19 22:12
ug/L
NO
5.0
1.7
10/22/19 22:12
ug/L
NO
10.0
1.7
10/22/19 22:12
ug/L
NO
5.0
2.0
10/22/19 22:12
ug/L
NO
5.0
1.6
10/22/19 22:12
ug/L
NO
10.0
1.6
10/22/19 22:12
ug/L
NO
5.0
2.2
10/22/19 22:12
ug/L
NO
5.0
1.2
10/22/19 22:12
ug/L
NO
10.0
1.7
10/22/19 22:12
ug/L
NO
5.0
1.4
10/22/19 22:12
ug/L
NO
5.0
2.1
10/2211922:12
ug/L
NO
10.0
2.2
10/22/19 22:12
ug/L
NO
5.0
1.7
10/22/19 22:12
ug/L
NO
5.0
0.91
10/22/19 22:12
ug/L
NO
5.0
2.1
10/22/19 22:12
%
96
10-137
10/22/19 22:12
%
69
15-120
10122/1922:12
a/
69
10-120
10/22/19 22:12
%
75
10-120
10/22/19 22:12
%
52
10-120
10/22119 22:12
%
105
11-131
10122/1922:12
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersinhe, NC 28078
[phone]
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2713444
Units
Spike
Conc.
LCS
Result
LCS
%Rec
e/ Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
32.4
65
44-142
1,2-Dichlorobenzene
ug/L
50
31.1
62
32-129
1,2-Diphenylhydrazine
ug/L
50
61.3
123
25-150
1,3-Dichlorobenzene
ug/L
50
30.5
61
1-172
1,4-Dichlorobenzene
ug/L
50
30.4
61
20-124
2,4,6-Trichlorophenol
ug/L
50
40.8
82
37-144
'2,4-Dichlorophenol
ug/L
50
4L5
83
1-191
2,4-Dimethylphenol
ug/L
50
43.0
86
32-119
2,4-Dinitrophenol
ug/L
250
264
106
1-181
2,4-Dinitrotoluene
ug/L
50
48.3
97
39-139
2,6-Dinitrotoluene
ug/L
50
49A
98
50-158
2-Chloronaphthalene
ug/L
50
41.7
83
60-118
2-Chlorophenol
ug/L
50
38.7
77
23-134
2-Nitrophenol
ug/L
50
41.2
82
29-182
3,3'-Dichlorobenzidine
ug/L
100
92.9
93
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
108
108
1-181
4-Bromophenylphenyl ether
ug/L
50
38.0
76
53-127
4-Chloro-3-methylphenol
ug/L
100
91.2
91
22-147
4-Chlorophenylphenyl ether
l
ug/L
50
38.0
76
25-158
Results presented on this pageam in the units Indicated by the "Unit" column except where an alternate unit Is pmsemed to the dgM of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
IDale: 10/30/2019 05:52 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 30

aceAnalytical
wwwpacelabs.com
QUALITY CONTROL DATA
Project: Newton Instruments / 1912
Pace Project No.: 92449952
LABORATORY CONTROL SAMPLE:
2713444
Spike
1-CS
1-CS
%Rec
Parameter
Units
Conc.
Result
%Rec
Limits
I4-Nitrophenol
ug/L
250
174
70
1-132
Acenaphthene
ug/L
50
38.7
77
47-145
I, Acenaphthylene
ug/L
50
41.8
84
33-145
Anthracene
ug/L
50
44.5
89
1-166
Benzidine
ug/L
100
55.2
55
25-150
Benzo(a)anthracene
ug/L
50
44.0
88
33-143
Benzo(a)pyrene
ug/L
50
46.7
93
17-163
Benzo(b)lluoranthene
ug/L
50
48.1
96
24-159
Benzo(g,h,i)perylene
ug/L
50
46.5
93
1-219
" Benzo(k)fluoranthene
ug/L
50
46,8
94
11-162
bis(2-Chloroethoxy)methane
ug/L
50
38.9
78
33-184
" bis(2-Chloroethyp ether
ug/L
50
37.4
75
12-158
bis(2-Ethylhexypphthalate
ug1L
50
44.8
90
8-158
Butylbenzylphthalate
ug/L
50
46.6
93
1-152
!Chrysene
ug/L
50
41.3
83
17-168
Di-n-butylphthalate
ug/L
50
43.6
87
1-118
Di-n-octylphthalate
ug/L
50
47.4
95
4-146
Dibenz(a,h)anthracene
ug/L
50
46.3
93
1-227
Diethylphthalate
ug/L
50
43.9
88
1-114
Dimelhylphthalate
ug/L
50
42.2
84
1-112
Fluofanthene
ug/L
50
44.3
89
26-137
Fluorene
ug/L
50
42.0
84
59-121
Hexachloro-1,3-butadiene
ug/L
50
29.7
59
24-116
iHexachlorobenzene
ug/L
50
38.9
78
1-152
Hexachlorocyclopentadiene
ug/L
50
35.7
71
25-150
Hexachloroethane
ug/L
50
28.6
57
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
46.0
92
1-171
Isophorone
ug/L
50
40.9
82
21-196
N-Nitroso-di-n-propylamine
ug/L
50
39.7
79
1-230
N-Nitrosodimethylamine
ug/L
50
32.2
64
25-150
N-Nitrosodiphenylamine
ug/L
50
39.9
80
25-150
Naphthalene
ug/L
50
36.5
73
21-133
Nitrobenzene
ug/L
50
39.9
80
35-180
Penlachlorophenol
ug/L
100
96.8
97
14-176
Phenanthrene
ug/L
50
41.7
83
54-120
Phenol
ug/L
50
26.4
53
5-112
Pyrene
ug/L
50
42.7
85
52-115
2,4,6-Tiibromophenol(S)
%
99
10-137
2-Fluorobiphenyl(S)
%
67
15-12l)
2-Fluorophenol(S)
%
67
10-120
Nitrobenzene-d5(S)
%
73
10-120
Phenol-d6 (S)
%
54
10-120
Terphenyl-dl4 (S)
%
85
11-131
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvige, NC 28078
[phone]
Qualifiers
Results presenter) on th Is page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/30/2019 05:52 PM without the written consent of Pace Analytical Services, LLC, Page 22 of 30

aceAnalytical
wwwpace)abs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9B00 Kincey Ave. Suite 100
Huntemville, NC 2807E
[phone]
Project: Newton Instruments / 1912
Pace Project No.: 92449952
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2713445
2713446
MS
MSD
92448559007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
%Rec
Limits
RPD
RPD Dual
1,2,4-Tdchlorobenzene
ug/L
ND
50
50
39.9
35.5
80
71
44-142
12
30
1,2-Dichlorobenzene
ug/L
NO
50
50
43.3
38.5
87
77
32-129
12
30
1,2-Diphenylhydrazine
ug/L
NO
50
50
72.3
69.6
145
139
25-150
4
30
1,3-Dichlorobenzene
ug/L
ND
50
50
38.8
34.9
78
70
1-172
11
30
1,4-Dichlorobenzene
ug/L
ND
50
50
38.6
34.7
77
69
20-124
11
30
2,4,6-Tdchlorophenol
ug/L
ND
50
50
44A
43.7
88
87
37-144
1
30
2,4-Dichlorophenol
ug/L
ND
50
50
48.6
45.7
97
91
1-191
6
30
2,4-Dimethylphenol
ug/L
NO
50
50
50.6
47.6
101
95
32-119
6
30
2,4-Dinitrophenol
ug/L
NO
250
250
ND
ND
16
14
1-181
30
2,4-Dinitrotoluene
ug/L
NO
50
50
56.2
58.4
112
117
39-139
4
30
2,6-Dinitrotoluene
ug/L
ND
50
50
58.0
59.0
116
118
50-158
2
30
2-Chloronaphthalene
uglL
ND
50
50
48.0
44.6
96
89
60-118
7
30
2-Chlorophenol
ug/L
ND
50
50
48.2
43.7
96
87
23-134
10
30
2-Nitrophenol
ug/L
ND
50
50
51.5
48.7
103
97
29-182
6
30
3,3'-Dichlorobenzidine
ug/L
NO
100
100
64.5
60.0
65
60
1-262
7
30
4,6-Dinitro-2-methylphenol
ug/L
NO
100
100
69.4
72.2
69
72
1-181
4
30
4-Bromophenylphenyl ether
ug/L
NO
50
50
43.8
43.0
88
86
53-127
2
30
4-Chloro-3-methylphenol
ug/L
ND
100
100
108
106
108
106
22-147
2
30
4-Chlorophenylphenyl ether
ug/L
ND
50
50
43.8
43.3
88
87
25-158
1
30
4-Nitrophenol
ug/L
ND
250
250
105
107
42
43
1-132
2
30
Acenaphthene
ug/L
NO
50
50
43.9
41.9
88
84
47-145
5
30
Acenaphthylene
ug/L
ND
50
50
48.6
46.0
97
92
33-145
5
30
Anthracene
ug/L
ND
50
50
51.7
51.2
103
102
1-166
1
30
Benzidine
ug/L
ND
100
100
72.3
70.0
72
70
25-150
3
30
Benzo(a)anthracene
ug/L
ND
50
50
52.8
52.1
106
104
33-143
1
30
Benzo(a)pyrene
ug/L
ND
50
50
55.0
55.5
110
111
17-163
1
30
Benzo(b)fluoranthene
ug/L
NO
50
50
58.6
59.4
117
119
24-159
1
30
Benzo(g,h,i)perylene
ug/L
NO
50
50
52.6
54.6
105
109
1-219
4
30
Benzo(b)fluoranthene
ug/L
ND
50
50
55.2
54.8
110
110
11-162
1
30
bis(2-
ug/L
ND
50
50
45.9
42.8
92
86
33-194
7
30
Chloroeth oxy) methane
bis(2-Chloroethyl) ether
ug/L
NO
50
50
45.5
41.9
91
84
12-158
8
30
bis(2-Elhylhexyl)phthalate
ug/L
NO
50
50
53.6
52.4
107
105
8-158
2
30
Butyl benzylphlhalate
ug/L
NO
50
50
56.9
55.4
114
111
1-152
3
30
Chrysene
ug/L
ND
50
50
49.0
48.6
98
97
17-168
1
30
Di-n- butylphth a late
ug/L
ND
50
50
51A
50A
102
101
1-118
1
30
Di-n-octylphthalate
ug/L
ND
50
50
58.3
57.4
117
115
4-146
2
30
Dibenz(a,h)anthracene
ug/L
NO
50
50
52.9
54.5
106
109
1-227
3
30
Diethylphthalate
ug/L
NO
50
50
52.1
53.1
104
106
1-114
2
30
Dimethylphthalate
ug/L
ND
50
50
49.9
50.3
100
101
1-112
1
30
Fluoranthene
ug/L
NO
50
50
51.4
51A
103
103
26-137
0
30
Fluorene
ug/L
ND
50
50
48.6
47.5
97
95
59-121
2
30
Hexachloro-1,3-butadiene
ug/L
ND
50
50
37.9
33.2
76
66
24-116
13
30
Hexachlorobenzene
ug/L
NO
50
50
46.5
45.5
93
91
1-152
2
30
Hexachlorocyclopentadiene
ug/L
NO
50
50
43.7
39.1
87
78
25.150
11
30
Hexachloroethane
ug/L
NO
50
50
37.5
33.5
75
67
40-113
11
30
Results presented on this page are In the units Indicated by the "Units" column except where an altemate unit Is preserved to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/30/2019 05:52 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 30

e
aceAnalytical
.pacelabscom
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Newton Instruments / 1912
Pace Project No.: 92449952
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2713445
2713446
MS
MSD
92448559007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD
RPD Qual
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
50
52.8
54.5
106
109
1-171
3
30
Isophorone
ug/L
NO
50
50
48.6
46.3
97
93
21-196
5
30
,I N-Nitroso-di-n-propylamine
ug/L
NO
50
50
49.0
45.0
98
90
1-230
8
30
N-Nitrosodimethylamine
ug/L
NO
50
50
39.0
35.6
78
71
25-150
9
30
N-Nilrosodiphenylamine
ug/L
NO
50
50
47.2
46.9
94
94
25.150
1
30
Naphthalene
ug/L
ND
50
50
48.5
44.7
97
89
21-133
8
30
Nitrobenzene
ug/L
ND
50
50
56A
52.0
113
104
35-180
8
30
Pentachlorophenol
ug/L
ND
100
100
45.1
36.3
45
36
14-176
22
30
Phenanthrene
ug/L
ND
50
50
48.0
47.7
96
95
54-120
1
30
Phenol
ug/L
NO
50
50
36.6
32.1
73
64
5-112
13
30
Pyrene
ug/L
NO
50
50
51.2
51.0
102
102
52-115
0
30
12,4,6-Tribromophenol(S)
%
115
112
10-137
2-Fluorobiphenyl(S)
%
89
80
15-120
'2-Fluorophenol(S)
%
87
78
10-120
Nitrobenzene-d5(S)
%
95
86
10-120
Phenol-tl6 (S)
%
81
69
10-120
Terphenyl-d14(S)
%
92
86
11-131
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/30/2019 05:52 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 30

laceAnalyficalb
awxpecels65.cpm
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project:
Newton Instruments / 1912
Pace Project No.:
92449952
QC Batch:
506036 Analysis Method: EPA 420.4 Rev 1.01993
QC Batch Method
EPA420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics
Associated Lab Samples:
92449952001
METHOD BLANK: 2718242 Matrix: Water
Associated Lab Samples: 92449952001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Phenol mg/L NO 0.020 0.0050 10/28/1914:38
LABORATORY CONTROL SAMPLE: 2718243
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phenol ml 0.05 0.048 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2718244
2718245
MS
MSD
92449641002 Spike
Spike
MS
MSD
MS MSD % Rec
Max -
Parameter Units Result Conc.
Conc.
Result
Result
%Rec %Rec Limits
RPD RPD Qual
Phenol mg/L NO 0.05
0.05
0.049
0.046
95 89 90-110
6 10 Mt
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2718246
2718247
MS
MSD
92449693001 Spike
Spike
MS
MSD
MS MSD % Rec Max
Parameter Units Result Conc.
Conc.
Result
Result
%Rec %Rec Limits RPD RPD Qual
Phenol mg/L 0.024 0.05
0.05
0.061
0.066
74 84 90-110 8 10 M1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the resuh.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/30/2019 05:52 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 30

ace Analytical e
www.pacelabs.rom
Project: Newton Instruments 11912
Pace Project No.: 92449952
QC Batch: 504628
QC Batch Method: SM 4500-CN-E-2011
Associated Lab Samples: 92449952001
METHOD BLANK: 2711914
Associated Lab Samples: 92449952001
Parameter
Cyanide
QUALITY CONTROL DATA
Analysis Method: SM 4500-CN-E-2011
Analysis Description: 450OCNE Cyanide, Total
Matrix: Water
Blank Reporting
Units Result Limit
mg/L NO 0.0080
LABORATORY CONTROL SAMPLE: 2711915
Spike LCS
I, Parameter Units Cone. Result
Cyanide mg/L 0.1 0.095
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MDL Analyzed Qualifiers
0.0060 10/20/19 11:44
LCS %Rec
%Rec Limits Qualifiers
95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2711916
2711917
MS
MSD
92450321001 Spike
Spike
MS
MSD
MS MSD %Rec Max
Parameter Units Result Cone.
Cone.
Result
Result
%Rec %Rec Limits RPD RPD Qual
Cyanide mg/L ND 0.1
0.1
0.066
0.085
63 82 80-120 25 10 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2711918
2711919
MS
MSD
92449899002 Spike
Spike
MS
MSD
MS MSD %Rec Max
Parameter Units Result Cone.
Cone.
Result
Result
%Rec %Rec Limits RPD RPD Qual
Cyanide mg/L NO 0.1
0.1
0.090
0.095
83 88 80-120 5 10
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presentee to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/30/2019 05:52 PM without the written consent or Pace Analytical Services, LLC. Page 26 of 30

Pace Analytical Services, LLC
laceAnalytical"'
9800 Kincey Ave. Suite 100
Huntersville, NC 26078
wwwpacelabs.mm [phone]
QUALIFIERS
Project: Newton Instruments 11912
Pace Project No.: 92449952
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP- Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services- Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
B Analyte was detected in the associated method blank.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
P5 The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.
R1 RPD value was outside control limits.
c3 Analysis of 2-chloroethyl vinyl ether was performed from a sample that was field preserved to pH < 2 with HCI. Acid
preservation is not allowed for this parameter by the test method or for NPDES compliance per 40CFR Part 136.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 10/30/2019 05:52 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 30

Pace Analytical Services, LLC
aceAnalytical ® 9600 uncey Ave. Suite 100
078
' Huntersville, NC 29078
swxparolebs com [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Newton Instruments / 1912
92449952
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92449962001
Outfall-001
SM 2540D-2011
504212
92449952001
Outfall-001
EPA 1664B
506605
92449952001
Outfall-001
EPA 608.3
504938
EPA608.3
505304
92449952001
Outfall-001
EPA 200.7 Rev 4.4 1994
505412
EPA 200.7 Rev 4.4 1994
505466
92449952001
Outfall-0Ot
EPA245.1 Rev 3.01994
506453
EPA 245.1 Rev 3.01994
506498
^92449952001
Outfall-001
EPA625.1
504976
EPA625.1
505096
1.92449952001
Outfall-001
EPA 624.1
504567
92449952001
Outfall-001
EPA 420.4 Rev 1.0 1993
506036
EPA 420.4 Rev 1.0 1993
506071
92449952001
Outfall-001
SM 4500-CN-E-2011
504628
SM 4500-CN-E-2011
504647
Date: 10/30/2019 05:52 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, LLC.
Page 28 of 30

-W0#-92449952
CHAIN -OF -CUSTODY Analytical Request Document
imberor
ace Analytical
Chain -of -Custody Is a LEGAL DOCUMENT. Complete all relevent fields
9240952
Company:
Piedmont Geologic
Billing Inforcration:
same
Address: 6003-145 Chapel Hill Rd, Raleigh, NC 27607
Connt,net Preservative
TV e
U
7
Repo" TO:
Jonathan Murphrey
Email To:
jmurphrey@piedmontgeologic:.com
PfesernardyeTYM: (a)-ftric-did,U)s.1faric acid. G)hydirachlo 14
16) nieth.nol, (7) s.diu. bis.late. (8) sedum thiccuffee, (9) hx�nj
10 ammonium hv&oxid.. (D) TSP, (Ul Ur%pe,;.ri,td. (0) Dithu,
kL(.)scxfiu.hd'o"xJ ;. F-) 7-7.�.—.Ie-
(A) �r is acid, W) ammonium sulfate.
Copy To:
Site Collection Info/Address:
Customer Project Name/Number:
Slate: County/City: Time Zone Colli,cited;
Analyses
pnofilei'Llue:
LIP-Sticap'. 1!eceipt:chei,�"c0t:
Cuat6dy S..Ib Pc..eqt/1cii.ciw ......
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Newton Instruments if 1912
PTVIET
NC Butner I )( IMT[ I cT
Phone: [phone]
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Turnaround Date Required:
Immediately Packed on Ice:
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Sample Disposal: I/ Rush: Field Filtered (if apPliable)
114 Dispose as appropriate J Return Same Day I Next Gay
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M,scrips
I jArchii,c: I 120ay [ 13Day (.14Day f 15 Day AnatInsis:
j
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to
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Product (P), Sad/Solid (51.1, CHI (OL), Wipe (WP), Air (AR). Tissue rrSj, Bioassay (B). Vapor M, Other (OT)•
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Customer Sample 10
Matrix•Grab
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Date
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GW
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Customer Remarks/ Special Condit tons/ Possible Hazards:
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Date/Time: Received ?7 _,!p;a Date/'nme:
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cfiCcuhfimroance(i):Page:_

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'Check mark top half of box If pH and/or dechiorination Is Project is WOfI ; 92449952
verified and within the acceptance range for preservation
samples, PM: TIN Due Date: 10/30/19
Ercepf w.. VOA, COMM, Tor 00 and Grease, OA018035 (ester( Doc, LLHg CLIENT: 92—PIED GEOL
**Bottom half of box Is to list number of bottle
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Sample ID Type or prtservative PH upon receipt 02le preservatlon adituted Time presarnden amount of Preservative Lot e
adiu5ted added
Note: Whenever there h a ff—rlm..a.,..•
Page 30 of 30
.0 of neld, incorrect JrlflMUva, eu[Or Temp, i0[ilrreR Ceeblr,elf.