NCG030134_MONITORING INFO_20191111

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/v u& 0 3 () /-3 v
DOC TYPE.
❑ HISTORICAL FILE
MONITORING REPORTS
DOC DATE
❑ ] %) J '
YYYYMMDD

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted: 11/11/19
CERTIFICATE OF COVERAGE NO. N00030134
FACILITY NAME: Thermo Fisher Scientific (Asheville) LLC
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Jeremy Putnam, EHS
LABORATORY: Pace Analytical Lab Cert. #
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR
SAMPLEPERIOD —Jan-June_July-Dec
Or X Monthly: October
DISCHARGING TO CLASS CFR1 ❑ HQW X❑rrout ❑PNA
❑Zero -flow ❑Hater Supply ❑SA
❑Other
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -
7_IVo discharge this period?'
Outfall No:
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
PH,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics'
Benchmarks
_
-
100 mg/L or 50 mg/0
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
Outfalll
10/22/19
0.6
30.2
7.1
0.013
<0.005
0.226
<5
N/A
Outfall2
10/22/19
0.6
40.2
7.06
0.851
<0.005
0.39
<5
N/A
Outfall3
10/22/19
0.6
57.0
6.91
0.0204
0.0066
0.12
<5
N/A
Outfall4
10/22/19
0.6
2.5
6.96
0.005
0.005
0.111
<5
N/A
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outtaii.
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO
monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the
General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO),
I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent
management plan included in the Stormwater Pollution Pre tion Plan."
Name (Print name)
Tit (Print title)
Signature
Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
nNn r icrhnrna Chic narinr422
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches'
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
P
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/L4
Parameter code
46529
NCOIL
00552
CO530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date:ll/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
A BENCHMARK EXCEE DANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
2 EXCEEDANCES IN A ROW FORTH E SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL?
YES X NO
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES NO REGIONAL OFFICE CONTACT NAME: Ms. Laura Herbert
(Asheville Regional Office)
Mail an oriainal copv of this DMR, including all "No Discharge" reports within 30 days of receipt of the lab results (or at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am ewa that there-aw significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
Date
=Permit Date:11/1/2018-05/31/2021 -- - -
11/1/2018
SWU-245, last revised

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted: 11/11/19
CERTIFICATE OF COVERAGE NO. NCG030134
FACILITY NAME: Thermo Fisher Scientific (Asheville) LLC
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Jeremy Putnam, EHS
LABORATORY: Pace Analytical Lab Cert. #
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR
SAMPLEPERIOD _Jan-June_July-Dec
Or Monthly: October
DISCHARGING TO CLASS C "V ❑ HQW [X]Trout ❑ PNA
❑Zero -flow QNater Supply [:]SA
❑Other
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -
FlVo discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
P H ,
Standard units
Total Copper
Total Lead.
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics'
Benchmarks
_
-
100 mg/L or 50 mg/L°
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
. 01051
01094
00552
78141
Outfall1
10/22/19
0.6
30.2
7.1
0.013
<0.005
0.226
<5
N/A
Outfall2
10/22/19
0.6
40.2
7.06
0.851
<0.005
0.39
<5
N/A
Outfall3
10/22/19
0.6
57.0
6.91
0.0204
0.0066
0.12
<5
N/A
Outfall4
10/22/19
0.6
<2.5
6.96
<0.005
<0.005
0.111
<5
N/A
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfaii.
] For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
, Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date:11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO
monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the
General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO),
I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent
management plan included in the Stormwater Pollution PrevertE�on Ian."
Name (Print name)
it PrinHi
Signature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format "<XX me/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
I—lAl
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches'
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/L4
Parameter Code
-
46529
NCOIL
00552
CO530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 111112018
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL?
YES X NO
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES NO REGIONAL OFFICE CONTACT NAME: Ms. Laura Herbert
(Asheville Regional Office)
Mail an original copv of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the
case of ."No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am are that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee Date
Permit Date: -11/1/2018-05/31/2021 - -- - -_ - -- -- -- -'- - SWU-245, last revised
11/1/2018

aceAnalXical a
w ..Pacelaes.norn
November 05, 2019
Mr. Jeremy Putnam
Thermo Electron Corp.
275 Aiken Road
Asheville, NC 28804
r RE: Project: OCTOBER 2019 SW 10/22/19
Pace Project No.: 92450663
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Dear Mr. Putnam:
Enclosed are the analytical results for sample(s) received by the laboratory on October 22, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
i�
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
p ACC O'�
_ e\ REPORT OF LABORATORY ANALYSIS
s
r This report shall not be re roducetl, except in full,
NI P P P
! without the written consent of Pace Analytical Services, LLC.
1-219!
Page 1 of 15

Pace Analytical Services, LLC
aceAnalytical a 2225 Riverside Asheville, NC 2980404
/ wwwPacmem [phone]
CERTIFICATIONS
Project: OCTOBER 2019 SW 10/22/19
Pace Project No.: 92450663
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florda/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 15

aceAnalytical e
w,w.pscelaos.corn
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
.Project:
Pace Project No.:
OCTOBER 2019 SW 10/22/19
92450663
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92450663001
1-1,1-2,1-3
EPA 1664B
AAC1
1
PASI-C
EPA1664B
AAC1
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
�I
SM 254OD-2011
CEH
1
PASI-A
192460663002
2-1,2-2,2-3
EPA1664B
AAC1
1
PASI-C
EPA 1664E
AAC1
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
SM 2540D-2011
CEH
1
PASI-A
!92450663003
3-1,3-2,3-3
EPA1664B
AAC1
1
PASI-C
'I
EPA1664B
AAC1
1
PASI-C
EPA 200.7 Rev 4.41994
SHi
3
PASI-A
u
SM 2540D-2011
CEH
1
PASI-A
92450663004
4-1,4-2,4-3
EPA1664B
AAC1
1
PASI-C
EPA1664B
AAC1
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
it
i
I
SM 254OD-2011
CEH
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 15

aceAnalytical e
I w»wpacelabs.cwn
i
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: OCTOBER 2019 SW 10/22/19
Pace Project No.: 92450663
Sample: 1-1,1-2,1-3 Lab ID: 92450663001 Collected: 10/22/1908:30 Received: 10/22/1916:06 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
1664 SGT-HEM, TPH
Total Petroleum Hydrocarbons
200.7 MET ICP
Copper
Lead
Zinc
2540D Total Suspended Solids
Total Suspended Solids
Analytical Method: EPA 1664B
NO mg/L
4.8 1
11/05/1911:13
Analytical Method: EPA 1664B
NO mg/L
4.8 1
11/05/19 11:13
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
13.0 ug/L
5.0 1
10/28/19 23:48 10/29/19 22:43 7440-50-8
NO ug/L
5.0 1
10/28/19 23:48 10/29/19 22:43 7439-92-1
226 ug/L
10.0 1
10/28/19 23:48 10/29/19 22:43 7440-66-6
Analytical Method: SM 2540D-2011
30.2 mg/L
5.0 1
10/26/19 06:21
Sample: 2-1,2-2,2-3 Lab ID: 92450663002 Collected: 10/22/19 08:45 Received: 10/22/19 16:06 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
1664 SGT-HEM, TPH
Total Petroleum Hydrocarbons
200.7 MET ICP
Copper
Lead
Zinc
2540D Total Suspended Solids
Total Suspended Solids
Analytical Method: EPA 1664B
NO mg/L
4.8
1
11/05/1911:13
Analytical Method: EPA 1664B
ND mg/L
4.8
1
11/05/1911:13
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
85.1 ug/L
5.0
1
10/28/19 23:48 10/29/19 22:52 7440-50-8
ND ug/L
5.0
1
10/28/19 23:48 10/29/19 22:52 7439-92-1
390 ug/L
10.0
1
10/28/19 23:48 10/29/19 22:52 7440-66-6
Analytical Method: SM 254OD-2011
40.2 mg/L
5.6
1
10/26/19 06:21
Sample: 3-1,3-2,3-3 Lab ID: 92450663003 Collected: 10/22/19 09:00 Received: 10/22/19 16:06 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
1664 SGT-HEM, TPH
Total Petroleum Hydrocarbons
200.7 MET ICP
Copper
Date: 11/05/2019 04:49 PM
Analytical Method: EPA 1664B
NO mg/L 4.8 1 11/05/1911:13
Analytical Method: EPA 1664E
NO mg/L 4.8 1 11/05/19 11:13
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
20.4 ug/L 5.0 1 10/28/19 23:48 10/29/19 22:55 7440-50-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 4 of 15

lac,
Analytical
wwwpaCBlBes.Lem
l
I
I�
Project: OCTOBER 2019 SW 10/22/19
Pace Project No.: 92450663
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: 3-1,3-2,3-3 Lab ID: 92450663003 Collected: 10/22/19 09:00 Received: 10122119 16:06 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
,200.7 MET ICP
'Lead
Zinc
2540D Total Suspended Solids
Total Suspended Solids
I
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
6.6 ug/L 5.0 1 10/28/19 23:48 10/29/19 22:55 7439-92-1
120 ug/L 10.0 1 10/28/19 23:48 10/29119 22:55 7440-66-6
Analytical Method: SM 25400-2011
57.0 mg/L 12.5 1 10/26/19 06:21
Sample: 4-1,4-2,4-3
Lab ID: 92450663004 Collected:
10/22/19
09:15
Received: 10/22/19 16:06 Matrix: Water
Parameters
f
Results Units Report Limit
OF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mg/L
4.8
1
11/05/19 11:13
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
NO mg/L
4.8
1
11/05/19 11:13
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Copper
NO ug/L
5.0
1
10/29/19 22:55 11/01/19 23:14 7440-50-8
Lead
NO ug/L
5.0
1
10129/1922:55 11/01/1923:14 7439-92-1
Zinc
111 ug/L
10.0
1
10/29/1922:55 11/01/1923:14 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
I
NO mg/L
2.6
1
10/26/19 06:21
i
I
O REPORT OF LABORATORY ANALYSIS
I,
This report shall not be reproduced, except in full,
Date: 11/05/2019 04:49 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 15
I

r_,2eAna1j cal
wmvpecalaDs.cpm
QUALITY CONTROL DATA
Project: OCTOBER 2019 SW 10/22/19
Pace Project No.: 92450663
QC Batch: 507632 Analysis Method. EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92450663001, 92450663002, 92450663003, 92450663004
METHOD BLANK: 2725179 Matrix: Water
Associated Lab Samples: 92450663001,92450663002,92450663003,92450663004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L NO 4.8 11/05/19 11:13
LABORATORY CONTROL SAMPLE: 2725180
Parameter
Oil and Grease
Spike LCS
Units Conc. Result
mg/L 38.5 33.6
Pace Analytical services, LLC
2225 Riverside Dr
Asheville, INC 28804
(82B)254-7176
1-CS % Rec
%Rec Limits Qualifiers
87 78-114
Results presented on this page are in the units indicated by the "Units" column except "are an alternate un It Is presented to the rigid of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 11 /05/2019 04:49 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 15

ace Anal) tical �
w»wparPJs0.5.can
Y
�i QUALITY CONTROL DATA
l
-.' Project: OCTOBER 2019 SW 10/22/19
Pace Project No.: 92450663
I!IQC Batch: 507630 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH
Associated Lab Samples: 92450663001, 92450663002, 92450663003, 92450663004
iMETHOD BLANK: 2725171 Matnx: Water
Associated Lab Samples: 92450663001, 92450663002, 92450663003, 92450663004
'! Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
!Total Petroleum Hydrocarbons mg/L ND 4.8 11/05/1911:13
LABORATORY CONTROL SAMPLE: 2725172
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(82B)254-7176
1)
Spike
LCS LCS %Rec
Parameter
Units
Conc.
Result %Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
19.2
12.5 65 64-132
!MATRIX SPIKE SAMPLE:
2725173
92450614001 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result %Rec Limits Qualifiers
total Petroleum Hydrocarbons
mg/L
NO 192
11.2 54 64-132 M1
Results presented on this page are in the units Indicated bythe "Units" column except where an alternate unit Is presented to the dgM of the result.
REPORT OF LABORATORY ANALYSIS
! This report shall not be reproduced, except in full,
Dale: 11/05/2019 04:49 PM without the written consent of Pace Analytical Services, L-C.
Page 7 of 15

aceAna1j6ca1w
w ..wcela0.t.cnm
QUALITY CONTROL DATA
Project: OCTOBER 2019 SW 10/22/19
Pace Project No.: 92450663
UC Batch: 506253 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92450663001, 92450663002, 92450663003
METHOD BLANK: 2719123
Matrix:
Water
Associated Lab Samples: 92450663001,
92450663002, 92450663003
Blank
Reporting
Parameter
Units Result
Limit
Analyzed Qualifiers
Copper
uglL NO
5.0
10129/1922:16
Lead
ug/L ND
5.0
10/29/1922:16
-Zinc
ug/L ND
10.0
10/29/1922:16
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
2719124
Spike
LCS LCS e/ Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Copper
ug/L
500
489 98 85-115
Lead
ug/L
500
479 96 85-115
Zinc
ug/L
500
475 95 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2719125
2719126
MS
MSD
92450521001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Copper
ug/L
500
500
510
510
101
101
70-130 0
Lead
ug/L
500
500
493
491
98
98
70-130 0
Zinc
ug/L
26S
500
500
516
517
98
98
70-130 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2719127 2719128
MS MSD
92450675007 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Copper ug/L 44.4 500 500 622 618 116 115 70-130 1
Lead ug/L NO 500 500 489 489 97 97 70-130 0
Zinc ug/L 17.8 500 500 496 495 96 96 70-130 0
Results presented on this page am in the units indicated by the "Units' column except More an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /05/2019 04:49 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 15

Pace Analytical Services, LLC
ann nal icala
/YII IY�
2225
lJL li
eNCRiverside28 04
Asheville, NC 25804
wivr/Parelabtcwn
[phone]
QUALITY CONTROL DATA
Project: OCTOBER 2019 SW 10/22/19
Pace Project No.: 92450663
iIQC Batch: 506517
Analysis Method: EPA 200.7 Rev 4.4 1994
,QC Batch Method: EPA 200.7 Rev 4.4 1994
Analysis Description: 200.7 MET
lAssociated Lab Samples: 92450663004
,l
METHOD BLANK: 2720130
Matrix: Water
I Associated Lab Samples: 92450663004
'
4
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
ug/L
NO 5.0
11/01/19 23:08
,Copper
Lead ug/L
ND 5.0
11/0111923:08
Zinc ug/L
NO 10.0
11/01/1923:08
LABORATORY CONTROL SAMPLE: 2720131
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits Qualifiers
;Copper ug/L
500
496
99 85-115
,Copper
ug/L
500
481
96 85-115
Zinc ug/L
500
473
95 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2720132
2720133
MS
MSD
92450663004
Spike
Spike MS
MSD MS MSD
e/ Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Copper ug/L NO
500
500 484
479 96 95
70-130
1
Lead ug/L NO
500
500 478
471 95 94
70-130
1
Zinc ug/L 111
500
500 582
577 94 93
70-130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2720134
2720135
.
I
MS
MSD
92451150001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Copper ug/L 43.7
500
500 569
573 105 106
70-130
1
Lead ug/L NO
500
500 494
497 99 99
70-130
1
Zinc ug/L 81.5
500
500 575
577 99 99
70-130
0
n
Results presented on this page are In the units Indicated by the"OnIG' column except where an alternate unit Is presented to the right or the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /05/2019 04:49 PM without the written consent of Pace Analytical Services, L-C. Page 9 of 15

aceAnalytical "
/ mrwpace/a0.s.com
i
QUALITY CONTROL DATA
Project: OCTOBER 2019 SW 10/22/19
Pace Project No.: 92450663
QC Batch: 505936 Analysis Method: SM 2540D-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92450663001, 92450663002, 92450663003, 92450663004
METHOD BLANK: 2717964 Matrix: Water
Associated Lab Samples: 92450663001, 92450663002, 92450663003, 92450663004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L NO 2.5 10/26/19 06:19
Pace Analytical Services, LLC
2225 Riverside Dr
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
2717965
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result e/ Rec
Limits Qualifiers
Total Suspended Solids
mg/L
251
254 101
90-110
SAMPLE DUPLICATE: 2717976
92450663003
Cup
Parameter
Units
Result
Result RPD
Qualifiers
Total Suspended Solids
mg/L
57.0
55.5
3
SAMPLE DUPLICATE: 2717977
92450669004 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 588 590 0
Results presented on this page are in the units indicated by the "UNta' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 11 /05/2019 04:49 PM without the written consent of Pace Analytical Services, Ll Page 10 of 15

aceAnalytical
wmVp3Ce1955.CM1
QUALIFIERS
Pi Project: OCTOBER 2019 SW 10/22/19
Pace Project No.: 92450663
IU4JRIll Q9]II@
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC -Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit,
PQL- Practical Quantitation Limit.
RL- Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
�bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
i
MS(D) - Matrix Spike (Duplicate)
DUP- Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not Detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
I
PASI-A Pace Analytical Services - Asheville -
1; PASI-C Pace Analytical Services - Charlotte ,
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
i
This report shall not be reproduced, except in full,
Date: 11/05/2019 04:49 PM without the written consent of Pace Analytical Services, L-C.
Page 11 of 15

aceAnalytical
wwwparela0.5.rom
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Servicos, LLC
2225 Riverside Dr
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
OCTOBER 2019 SW 10/22/19
92450663
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92450663001
1-1,1-2,1-3
EPA 1664B
507632
92450663002
2-1,2-2,2-3
EPA 1664B
507632
92450663003
3-1,3-2,3-3
EPA 1664B
507632
92450663004
4-1,4-2,4-3
EPA 1664B
507632
92450663001
1-1,1-2,1-3
EPA 1664B
507630
92450663002
2-1,2-2,2-3
EPA 1664E
507630
92450663003
3-1,3-2,3-3
EPA 1664B
507630
92450663004
4-1,4-2,4-3
EPA1664B
507630
92450663001
1-1,1-2,1-3
EPA 200.7 Rev 4.4
1994
506253
EPA 200.7 Rev 4A 1994
506280
92450663002
2-1,2-2,2-3
EPA 200.7 Rev 4.4
1994
506253
EPA 200.7 Rev 4.4 1994
506280
92450663003
3-1,3-2,3-3
EPA 200.7 Rev 4.4
1994
506253
EPA 200.7 Rev 4.4 1994
506280
92450663004
4-1,4-2,4-3
EPA 2003 Rev 4.4
1994
506517
EPA 200.7 Rev 4.4 1994
506546
92450663001
1-1,1-2,1-3
SM 2540D-2011
505936
92450663002
2-1,2-2,2-3
SM 254OD-2011
505936
92450663003
3-1,3-2,3-3
SM 2540D-2011
505936
92450663004
4-1,4-2,4-3
SM 2540D-2011
505936
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/05/2019 04:49 PM without the wmten consent of Pace Analytical Services, -LC. Page 12 of 15

1.1n# • ®`!11ACMelc�
a
CHAIN -OF -CUSTODY Analytical Request Document
WB USE ONLY orII�II�I��I�III�II�
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III
bisollule,
nitric acid,
TSP.
(21
(8) odium
HH Unpreserved,
sulfuric
thiosulLd,
acid,
10)
(3) hydrochloric
(9)
Other
hexane.
arid, (4) sodium hYdrorMe, (51 zinc acetate,
(A) ascerblc add, HH nmmonlum'.pate,
Copy To:
$i�lCgilec[i _If/Address:
Analyses
SS +'1 rx
Lab Profile/Line:
Customer Project
State: Time Zone Collected:
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Lab Sample Receipt Checklist:
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N6 / Asks VI IiI� I IPTI IMTI ICT �(I ET
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Custody Sigbut •n Present Y NA
Collector Signature Present -N NA
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Site/Facility ID If:
Compliance Monitoring?
Email:
I� Yes I I NO
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B ttl a Irtact - N NA
correct Bottles NA
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Quote If:
DW Location Code:
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Samples Received on. ice YY N NA
"'VOA - HeadaPace Accrr IiI. Y N Np
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Turnaround Date Required:
Immediately Packed on Ice:
Yes ( INC,
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( I Dispose as appropriate I I Return
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'Matrix Codes (insert in Matrix box beiow): Drinking Water(DW), Ground Water(GW), Wastewater(WW),
Product (P), Soil/Solid (SL), Oil (Ol), Wipe (WP), Air (AR), Tissue ITS), Bioassay (B), vapor (V), Other (OTI
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Type of Ice Used: t Blue Dry None
SHORT HOLDS PRESENT(<72.hoursl: Y N/A
Lab Sample Tempera lure Info:
Temp Blank Received: Y NA
Packing Material Used:
Lab Tracking p:
2 349995
It
CelzDpoR
Cooler e eipt:-Z_r7,oC
IYe
Samples received via:
Cooler 1 Therm Corr: Factor: _Goc
Radchem sample(s) screened (<500 cpm): Y N
FEDE% UPS ClKnt Courier Pace Courier
Cooler 1 Corrected Temp: T7r.Zdc
Comments:
Relirquis d by/Comps y:1Signature)
D"att/e/Timg:
nor •ived by/Company: (Signature)
Date/Tirne::
MTJL LAB USE ONLY
Table tl:
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Acctnum:
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Relinquished by/,Compan "( Ygnature)
Date/Time:
Received by/Company: (Sign to )
Date/Time:
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Trip Blank Received: Y A NA
Prelogin:
HCL McOH TSP Other
Relinquished by/Company:(Signature)
Date/Time:
Received by/Company:(Signature) _
Date/Time:.
PM:
=Non Conf'orina ce(51 'Page
PB:

-02eAna!�rtica!' CHAIN -OF -CUSTODY Analytical Request Document
Pac
Chain-of-Custody is a LEGAL DOCUMENT - Complete all reinvent fields
zany: Billing Information:
T � Ul l i
ass: n I J
To:
Copy To:
yeli.1 Ivarner rvumuer. State: County/City: Time Zone Collected:
Du'fi x'r �Gi �j iV�/ ]�$hf Vlil� I IPTI )Mil ICTXET
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I) 2 Day 1 13 Day I 1 4 Day 1 15 Day
I Ilford:
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Analysis:
' Matrix Codes (Insert in Matrix box
below): Drinking Water (DW), Ground Water (GW), Wastewater (WWI.
Product (P), Soil/Solid (SL). Oil (Oil, Wipe (WP), Air (AR), Tissue ITS), Bioassay (B),
Vapor (V), Other (OT)
Comp/
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Customer Sample ID
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Composite Start)
Cornposite End
Date
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Remarks / Special Conditions / Possible Hazards: I Tyof ice Used: Used:Y t Blue Dry None
Packipeng Material
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D�:: Re sal by/Company: (Signature)
LABU WO : 92450663 Numberor
PM: Cot Due Date: 11/05/19
CLIENT: 93-Therms
Project Manager:
' Preservative Types (1) ranr acid, i'-) suliuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) Ymc acetate.
(6) mutbannL Ol sodium bisullam. (8) sodium thiosullare. 191 hevane. IA) ascorbic xai41R1 ammonium x:date,
ICI ammonium hvdroxide, (DI TSP. (UI Unoreser ed. (0) Othcf
Li+b 54NpLC H¢CClpt CIICCK11fU
Custody Seals Present/Intact Y NA
custody Signatures Prenent x I NA
Collector Signature Present N NA
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Bottles tntact N NA
S C
Correct Bottles N NA
t G
Sufficient volur:c N NA
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Samples Received on Ice N NA
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VOA - eeadspice Acceptable Y N irl(
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USDA Regulated Soils Y N tjA
Samples in Holding Tim. XV NA
pesidenl Chlerl— e:-eh'..' 1' N n/
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pit Strips:
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Lead Acetate Strips:
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LAU USE ONLY:
Lab Sample 3 / Comments:
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iRT HOLDS PRESENT (<72 hours): Y 1l . N/A Lab Sample Temperature Info:
Tracking IF Temp Blank Received: Y y( NA
2349996 Thatch Old ce /
Cooler 1 Temp Upon Receipt: r ZpC
pies received via: ''''� Cooler 1 Therm Corr. Factor 1 oC
FEDEX UPS Cgent Courier Pace Courier Cooler 1 Corrected Temp: �'Z70C
Dale/Time: I MTIL LAB USE ONLY Comments:
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Document Name: Cncumen; br
Revised: Feuary 7,?OLS
Sample Condition Upon Receipt(SCUR) Page 1 of Z
-PacellollRICa(� Document No.: Lsuing Authority:
F-CAR-CS-033-Rev05 Pace Carolinas Qual0office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Colifonn, TOC, Oil and Grease, DRO/3015 (•cater( DOC, LHg
"Bottom half of box is to list number of bottle
Project N WO# : 92450663
PM: CDl Due Date: 11/05/19
CLIENT: 93—Thermo
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Norm Cuolina DEnld6 Certification Office (le.
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Page 15 of 15

T ermo Rsher
SCIENTIFIC
November 11, 2019
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RECEIVED
NOV 2 0 2019
CEN lKAL FILES
DWR SECTION
RE: Stormwater Analvtical Monitoring Results for Thermo Fisher Scientific, LLC
I have attached the analytical monitoring results from stormwater sampling that was collected on
October 22, 2019 at Thermo Fisher Scientific, LLC's four outfalls.
Per our General Storm Water Permit No. NCG03000 requirements of monthly monitoring for
applicable parameters during a storm event, I have sampled each outfall for copper, zinc, pH,
lead, TSS, and Non -Polar OiUGrease/TPH. Results for copper at three of the four outfalls and
zinc at two of the four outfalls were above the benchmark values, as noted in Table 3 of the
general storm water permit. TSS was also above the benchmark value at one of the outfalls. All
other results were below the benchmark values. We have implemented a Tier Three response for
the site and Thermo Fisher Scientific, LLC has notified the Asheville Regional Office. Thermo
Fisher Scientific, LLC is currently working with an environmental consultant to help achieve
compliance with the benchmark values set forth in the facility's storm water permit. I have
attached the completed Monitoring Report containing the monitoring results from the four
outfalls.
If you have any questions, please feel free to contact me at 828-658-2845.
Jeremy Putnam
Sr. EHS Manager
Attachments: 1