NCG030134_MONITORING INFO_20190903

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
Iv U% 030 3
DOC TYPE.
❑ HISTORICAL FILE
MONITORING REPORTS
DOC DATE
❑ a b) 1 U ! L)
YYYYM M DD

44ell '01
IlE
Thermo Maher
SCIENTIFIC
August 26, 2019
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RECEIVED
GE
S�f' � 2019
CTION
RE: Stormwater Analytical Monitoring Results for Thermo Fisher Scientific, LLC
I have attached the analytical monitoring results from stormwater sampling that was collected on
July 23, 2019 at Thermo Fisher Scientific, LLC's four outfalls.
Per our General Storm Water Permit No. NCG03000 requirements of monthly monitoring for
applicable parameters during a storm event, I have sampled each outfall for copper, zinc, pH,
lead, TSS, and Non -Polar Oil/Grease/TPH. Results for zinc at three of the four outfalls and
copper at one outfall were above the benchmark values, as noted in Table 3 of the general storm
water permit. All other results were below the benchmark values. We have implemented a Tier
Three response for the site and Thermo Fisher Scientific, LLC has notified the Asheville
Regional Office. Thermo Fisher Scientific, LLC is currently working with an environmental
consultant to help achieve compliance with the benchmark values set forth in the facility's storm
water permit. I have attached the completed Monitoring Report containing the monitoring results
from the four outfalls.
If you have any questions, please feel free to contact me at 828-658-2845
Jeremy Putnam
Sr. EHS Manager
Attachments: 1

Stormwater- Discharge -Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted: 07/01/19
CERTIFICATE OF COVERAGE NO. N00030134
FACILITY NAME: Thermo Fisher Scientific (Asheville) LLC
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Jeremy Putnam, EHS
LABORATORY: Pace Analytical Lab Cert. #
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR
SAMPLE PERIOD —Jan-June _July -Dec
Or X Monthly: Juiv
DISCHARGING TO CLASS C["1R / ❑ HQW [ Trout ❑ PNA
❑Zero -flow ❑Hater Supply ❑SA
Other
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -
FlVo discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hourrainfall
amount,
Inches'
Total Suspended Solids
p H,
Standard units
Total Capper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics'
Benchmarks
-
-
100 mg/Lor 50 mg/L°
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code.
-
46529
C0530.
00400
01119
01051
01094
00552
78141
Outfall1
07/23/19
0.76
11.9
6.5
10.0075
0.005
0.143
<5
N/A
Outfall2
07/23/19
0.76
9.6
6.4
0.0344
0.005
0.238
<5
N/A
Outfall3
07/23/19
10.76
2.5
6.3
0.0055
0.005
0.0761
<5
N/A
Outfall4
07/23/19
10.76
2.5
6.4
0.0074
0.005
0.208
<5
N/A
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
The total precipitation must be recorded using data from'an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes: For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/l/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO
monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the
General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO),
I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent
management plan included in the Stormwater Pollution Preven ion IaIan�."
Name (Print name)
Titl Print title)
Signatur Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
F�No discharge this P eriod 22
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches3
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
15 mg/L
100 mg/L or 50 mg/L°
Parameter Code
-
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL?
YES X NO
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES NO REGIONAL OFFICE CONTACT NAME: Ms. Laura Herbert
(Asheville Regional Office)
Mail an original copv of this DMR, including all "No Discharge"reports within 30 days of receipt of the lab results (or at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am a e that are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature
VV
Date —
Permit Date:11/1/2018-05/31/2021
11/1/2018
SWU-245, last revised

aceAnalXical
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August 05, 2019
Mr. Jeremy Putnam
Thermo Electron Corp.
275 Aiken Road
Asheville, NC 28804
RE: Project: JULY 2019 SW 7/23/19
Pace Project No.: 92438099
Dear Mr. Putnam:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(826)2547176
Enclosed are the analytical results for sample(s) received by the laboratory on July 23, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This repo" shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

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Project: JULY 2019 SW 7/23/19
Pace Project No.: 92438099
Pace Analytical services, LLC
2225 Riverside Dr
Asheville, NC 28804
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florda/NELAP Certification #: E87W
Massachusetts Certification #: M-NCO30
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 13

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i
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)2547178
Project:
Pace Project No.:
JULY 2019 SW 7/23/19
92438099
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92438099001
1
EPA 1664E
JMS
1
PASI-C
EPA 200.7 Rev 4.41994
SH1
3
PASI-A
SM 2540D-2011
JP1
1
PASI-A
92438099002
2
EPA 1664B
JMS
1
PASI-C
EPA 200.7 Rev 4.41994
SH1
3
PASI-A
SM 2540D-2011
JP1
1
PASI-A
92438099003
3
EPA 1664E
JMS
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
SM 25400-2011
JPt
1
PASI-A
92438099004
4
EPA 1664B
JMS
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
SM 2540D-2011
JPt
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wnnen consent of Pace Analytical Services, L-C.
Page 3 of 13

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ANALYTICAL RESULTS
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)2547176
Project: JULY 2019 SW 7123/19
Pace Project No.: 92438099
Sample: 1 Lab ID: 92438099001 Collected: 07/23/19 08:30 Received: 07/23/19 14:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
07/30/19 06:07
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Copper
•- jiS 7.5 ug/L
5.0
1
08/01/19 16:08 08/02/19 23:34 7440-50-8
Lead
ND ug/L
5.0
1
08/01/19 16:08 08/0211923:34 7439-92-1
Zinc
\4J) 143 ug/L
10.0
1
08/01/19 16:08 08/02/19 23:34 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
11.9 mg/L
3.1
1
07/26/19 23:27
Sample: 2 Lab ID: 92438099002 Collected: 07/23/19 08:45 Received: 07/23/19 14:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Total Petroleum Hydrocarbons
NO mg/L
4.9 1
07/30/19 06:07
200.7 MET ICP
Analytical Method: EPA200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Copper
34.4 ug/L
5.0 1
08/01/19 16:08 08/0211923:37 7440-50-8
Lead
ND ug/L
5.0 1
08101 /19 16:08 08/02/1923:37 7439-92-1
Zinc
238 ug/L
10.0 1
08/01/19 16:08 08/02/1923:37 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
9.6 mg/L
2.7 1
07/26/19 23:27
sample: 3 Lab ID: 92438099003 Collected: 07/23/19 09:00 Received: 07/23/19 14,30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Total Petroleum Hydrocarbons
200.7 MET ICP
Copper
Lead
Zinc
2540D Total Suspended Solids
Total Suspended Solids
Date: 0810512019 11:17 AM
Analytical Method: EPA 1664B
ND mg/L
4.9
1
07/30/19 06:07
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
5.5 ug/L
5.0
1
08/01/19 16:08 08/02/19 23:41 7440-50-8
ND ug/L
5.0
1
08/01 /19 16:08 08/02/1923:41 7439-92-1
76.1 ug/L
10.0
1
08/01/19 16:08 08/02/19 23:41 7440-66-6
Analytical Method: SM 254OD-2011
ND mg/L
3.0
1
07/26/19 23:27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28604
(626)2547176
Project: JULY 2019 SW 7/23/19
Pace Project No.: 92438099
Sample: 4 Lab ID: 92438099004 Collected: 07/23/19 09:15 Received: 07/23/19 14:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Total Petroleum Hydrocarbons
ND mg/L
4.8 1
07/30/19 06:07
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Copper
7.4 ug/L
5.0 1
08/01/19 16:08 08/02/19 23:50 7440-50-8
Lead
ND ug/L
5.0 1
08/01/19 16:08 08/02/19 23:50 7439-92-1
Zinc
208 ug/L
10.0 1
08/01/19 16:08 08/02/19 23:50 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
ND mg/L
2.8 1
07/26/19 23:27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/05/2019 11:17 AM without the written consent of Pace Analytical Services, I.I.C.
Page 5 of 13

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QUALITY CONTROL DATA
Project: JULY 2019 SW 7/23/19
Pace Project No.: 92438099
QC Batch: 489150 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH
Associated Lab Samples: 92438099001,92438099002,92438099003,92438099004
METHOD BLANK: 2639920 Matrix: Water
Associated Lab Samples: 92438099001, 92438099002,92438099003,92438099004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L NO 4.8 07/30/19 06:01
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
2639921
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Total Petroleum Hydrocarbons
mg/L
19.2
20.9
108
64-132
MATRIX SPIKE SAMPLE:
2639922
92438314002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
NO
19.2
21.4
110
64-132
Results presented on this papa are in the units indicated by the'Units' column except wtmm an alternate unit Is presented to fire right of the result.
Date: 08/05/2019 11:17 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: JULY 2019 SW 7/23/19
Pace Project No.: 92438099
QC Batch: 489804
Analysis Method: EPA 200.7 Rev 4.4 1994
OC Batch Method: EPA 200.7 Rev 4.4 1994
Analysis Description: 200.7 MET
Associated Lab Samples: 92438099001,
92438099002, 92438099003, 92438099004
METHOD BLANK: 2642775
Matrix: Water
Associated Lab Samples: 92438099001,
92438099002, 92438099003, 92438099004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Copper
ug/L
NO 5.0
08/02/19 22:38
Lead
ug/L
NO 5.0
08/02/19 22:38
Zinc
ug/L
NO 10.0
08/02/19 22:38
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
2642776
Spike
1-CS
1-CS
%Rec
Parameter
Units
Conc.
Result
%Rec
Limits Qualifiers
Copper
ug/L
500
430
86
85-115
Lead
ug/L
500
427
85
85-115
Zinc
ug/L
500
502
100
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2642777
2642778
MS
MSD
92438004001
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units Result
Conc.
Conic.
Result
Result
% Rec % Rec
Limits RPD
.Copper
ug/L 60.6
500
500
507
502
89 88
70-130 1
Lead
ug/L NO
500
500
427
424
85 85
70-130 1
Zinc
ug/L 80.0
500
500
506
503
85 85
70-130 1
Qual
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2642779
2642780
MS
MSD
92438099003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conic.
Conic.
Result
Result
% Rec
% Rec
Limits RPD Qual
Copper
ug/L
5.5
500
500
484
490
96
97
70-130 1
Lead
ug/L
NO
500
500
467
475
93
95
70-130 2
Zinc
ug/L
76.1
500
500
532
539
91
93
70-130 1
Results presented on this page are In the units Indicated by the -Units' column except where an alternate unit Is presented to the dgid of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 08105/2019 11:17 AM without the written consent of Pace Analytical Services, L-C.
Page 7 of 13

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QUALITY CONTROL DATA
Project: JULY 2019 SW 7123/19
Pace Project No.: 92438099
QC Batch: 488843 Analysis Method: SM 254OD-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92438099001, 92438099002, 92438099003, 92438099004
METHOD BLANK: 2638662 Matrix: Water
Associated Lab Samples: 92438099001, 92438099002, 92438099003, 92438099004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L NO 2.5 07/26/19 2324
Pace Analytical services:, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)25r 7176
LABORATORY CONTROL SAMPLE & LCSD:
2638663
2638670
Spike
LCS LCSD
LCS LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec % Rec
Limits RPD RPD Qualifiers
Total Suspended Solids
mg/L
250
250 250
100 100
90-110 0 5
SAMPLE DUPLICATE: 2638665
92438180001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 20.0 23.3 15 D6
Results presented on the paps are in the units indicated by the 'Units' column except where an altemate unit is presented to the ripM of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0810512019 11:17 AM without the wrdten consent of Pace Analytical Services, -I-C.
Page 8 of 13

Pace Analytical Services, LLC
RiverZeAnalj4ical N 2225 Asheville, NC 28804
e Dr.
8804
l wew.Vamlebs.Gom [phone]
QUALIFIERS
Project: JULY 2019 SW 7123/19
Pace Project No.: 92438099
Ia14yINIIIIIQVb9
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC -Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL- Reporting Limit -The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCSO) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
INC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
;ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)2547176
Project:
Pace Project No.:
JULY 2019 SW 7123/19
92438099
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical
Method
Batch
92438099001
1
EPA 1664E
489150
92438099002
2
EPA 1664E
489150
92438099003
3
EPA1664B
489150
92438099004
4
EPA 1664E
489150
92438099001
1
EPA 200.7 Rev 4.4 1994
489804
EPA 200.7
Rev 4A 1994
489935
92438099002
2
EPA 200.7 Rev 4.4 1994
489804
EPA 200.7
Rev 4A 1994
489935
92438099003
3
EPA 200.7 Rev 4.4 1994
489804
EPA 200.7
Rev 4A 1994
489935
92438099004
4
EPA 200.7 Rev 4.4 1994
489804
EPA 200.7
Rev 4.4 1994
489935
92438099001
1
SM 2540D-2011
488843
92438099002
2
SM 2540D-2011
488843
92438099003
3
SM 2540D-2011
488843
92438099004
4
SM 2540D-2011
488843
Date: 08/05/2019 11:17 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
MOW the written consent of Pace Analytical Services, L-C.
Page 10 of 13

lraceAnalXical
L.
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
Issuing Authority:
;
17 F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville Q Eden[] Greenwood ❑ Huntersville ❑ Raleigh[:] Mechanicsville[]
Client Name: Project k: Wo# : 92438099
Ap.-M, PS F she✓- 1111111111111111111111111
Courier: []Fed Ex ❑UPS ❑LISPS XLTien[
❑Commercial []Pace❑other: 92438099
Custody Seal Present? []Yes ®No Seals Intact? ❑Yes X' No
Packing Material: []Bubble Wrap Bubble Bags ❑None ❑
Thet
Date/Initials Person Examining Contents: 6--' T
Other Biological Tissue Frozen?
rmome ec "� T7.5 []Yes ❑No ,18N/A
jlRGun ID:
J ] =LI b Type of IyWet ❑Blue ❑None
Cooler Temp ('C):ii Correction Factor: Add/Subtract ('C)
Temp should be above freezing to 6°C
Cooler Temp Corrected ('C): 3 .z• "Z ❑Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil l' N/A, water sample)
Did samples on6inate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (intrre,�rrnationally,
r1Yes WNn including Hawaii and Puerto Rico)? []Yes CaNo
No
Comm ents/Discrepancy:
I
Chain of Custody Present?
es
[]NO
❑H/A
1.
Samples Arrived within Hold Time?
(RYes
ON.
❑N/A
2.
Short Hold Time Analysis (c72 hr.)?
Des
JO No
❑N/A
3.
Rush Turn Around Time Requested?
Elves
No
❑N/A
4.
Sufficient Volume?
Yes
❑ND
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
Yes
ves
❑No
❑No
❑N/A
❑N/A
6.
Containers Intact?
Yes
[-)No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
[-]Yes
❑No
N/A
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
U Yes
❑No
[]N/A
9.
Headspace in VOA Vials(>S-6mm)?
❑1'es
❑No
IIN/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑w_s
❑No
[]No
ZIN/A
JtNiA
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Date:
Date:
Field Data Required? []Yes ❑No
Page 11 of 13

I
.3
VA
G'^`Y
Document Name: Document Revised: February 7, 2018
-f�CBAilB��?ICd(
Sample Condition Upon Receipt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Off ice
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VDA, Coliform, TOC, Oil and Grease, DRO/8015 (Water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project # W0# : 92438099
PM: CD1 Due Date: 08/06/19
CLIENT: 93-Thermo
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PH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adlutted
Amount of Preservative
added
Lot q
Note: Whenever there is a discrepancy affecting North Carolina compliance samples,a copy of this form Will ue sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 12 of 13

CHAIN -OF -CUSTODY I Analytical Request Document
PBCeAnalXtcal • The Chaln-of-Custorly Is a LEGAL DOCUMENT All relevant fields must be comDlead accurately. o
Www,.aceleae.c.m
Section A Section B Section C
01 a
R.q.had CII.nl Inlormalien : Required Project Inlormmlon'. Invoice IDlormatlon: -�,
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(qnIP YRol. To: Atlenli
c/t'
9 239
AetlrosaaY (,���� COPY
To:
Company Name:
REGULATORY AGENCY - '-
} VJ�\PP�tq ,� 1ilU-}�c'
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Atlaess:
F NPDES ( GROUNDWATER f- DRINKING WATER
(' UST RCRA IX OTHER SW
EmaJ To. Purchase
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Order No,:
F.
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uv.
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STATE:
R.queac.d Be. D.t.ITAT: Pl.i.1
Number
Pm Aullu e:
Requested Analysis Filtered (YIN)
Sdctlan D ..Ida C.d..
RequtmdCNmt ml lnl.atm MATRIX ICODE
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COLLECTED
Preservatives
5,
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ADDITIONAL COMMENTS
t`� RELINQUISHED BY I AFFILIATION
TIME
ACCEPTED BY r AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
\An .-~-`�.—�-
}DATE
nl��i��
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ORIGINAL
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IMMIDDIYYI:��\d�j
-'LryMdm Its. By [IgninVtx%term v.0 aru acWFllnll Paws Nil 311d, R,n.A terms dntl nnuumB I. I.,. L5°%per n.'n I.r wry uwnmx nm'.w "tan 30 'J.", F-ALL-0-020rev.07, 15-May-2007

Stormwater Discharge -Monitoring Report - for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted: 07/01/19
CERTIFICATE OF COVERAGE NO. NCG030134 SAMPLE COLLECTION YEAR
FACILITY NAME: Thermo Fisher Scientific (Asheville) LLC
COUNTY: Buncombe 110"
PERSON COLLECTING SAMPLES: Jeremy Putnam, EHS
LABORATORY: Pace Analytical Lab Cert. q
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE PERIOD —Jan-June _July -Dec
Or X Monthly: June
DISCHARGING TO CLASS CJ V [:]HQW [X f trout []PNA
Zero -flow ONater Supply []SA
Other
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -
nNo discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
p H,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Orgahicss
Benchmarks
-
-
100 mg/L or 50 mg/L'
6.0 — 9.0
0.010 mg/L
0.07S mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
Outfall1
06/09/19
2.1
<2.5
7.20
0.0065
<0.005
0.0771
<5
N/A
Outfall2
06/09/19
2.1
2.5
7.12
0.0084
0.005
0.0481
<5
N/A
Outfall3
06/09/19
2.1
2.5
6.80
0.0092
0.005
0.0594
<5
N/A
Outfall4
06/09/19
2.1
2.5
6.60
0.0065
0.005
0.0558
<5
N/A
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfau.
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO
monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the
General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO),
I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent
management plan included in the Stormwater Pollution Prevent Plan."
Name (Print name)
tle (Print title)
Signature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format "<XX mg/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
o dischor th d 22
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inche53
New Motor Oil or
Hydraulic Oil Usage
ge
Non -Polar O&G/ Total
Petroleum Hydrocarbons
s peso .
Total Suspended
Solids
Benchmarks
15 mg/L
100 mg/L or 50 mg/L"
Parameter Code
-
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
A BENCHMARK EXCEE DANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEE DANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL?
YES X NO
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES NO REGIONAL OFFICE CONTACT NAME: Ms. Laura Herbert
(Asheville Regional Office)
Mail an original copv of this DMR, including all "No Discharge"reports, within_30 days of receipt of the lab results (or at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. -Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
amjware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
�34�D> >�
Date
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised
11/1/2018

aceAnal ical
ww.upacelabs.cwn
June 24, 2019
Mr. Jeremy Putnam
Thermo Electron Corp.
275 Aiken Road
Asheville, INC 28804
RE: Project: SW JUNE 2019
Pace Project No.: 92432379
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Dear Mr. Putnam:
Enclosed are the analytical results for sample(s) received by the laboratory on June 10, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
4—
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
. 2�JY F.CC&o'�
IMmmj'l
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 15

aceAnalj6cal
xw+vpatela0.5.ccm
Project: SW JUNE 2019
Pace Project No.: 92432379
Pace Analytical Services, LLC
2225 Riveisioe Dr
Asheville, NC 28804
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproGuced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 15

aceAnalytical e
/ wmvpacelaes.rnm
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(82B)254-7176
Project: SW JUNE 2019
Pace Project No.: 92432379
Sample: 1 Lab ID: 92432379001 Collected: 06/09/19 09:15 Received: 06/10/19 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua(
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mg/L
5.0
1
06/20/19 06:38
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
NO mglL
5.0
1
06/20/19 06:38
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.41994
Copper
6.5 - ug/L
5.0
1
06/19/19 16:04 06/21/19 1434 7440-50-8
Lead
NO ug/L
5.0
1
06119/1916:04 06/21/1914:34 7439-92-1
Zinc
` 77.1 ug/L
10.0
1
06/19/19 16:04 06/21/19 14:34 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
it
IlTotal Suspended Solids
- ND mglL
2.6
1
06114/1912:19
Sample: 2
Lab ID: 92432379002 Collected:
06/09/19 09:30
Received: 06/10/19 13:00 Matrix: Water
Parameters
Results Units Report Limit OF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
,Oil and Grease
NO mg/L
5.0 1
06/20/19 06:38
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons NO mg/L
5.0 1
06/20/19 06:38
200.7 MET ICP
Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Copper
,Analytical
� rQ) �Jp,lT-{` 8.4 ug/L
5.0 1
06119/1916:04 06/21/1914:37 7440-50-8
'Lead
NO ug/L
5.0 1
06/19/19 16:04 06/21/1914:37 7439-92-1
Zinc
�rQ�-�1 48.1 ug/L
10.0 1
06119/1916:04 06/21/1914:37 7440-66-6
2540D Total Suspended Solids Analytical Method: SM 254OD-2011
Total Suspended Solids
NO mg/L
2.6 1
06/14/19 12:25
Sample: 3
Lab ID: 92432379003 Collected:
06/09/19 09:45
Received: 06/10/19 13:00 Matrix: Water
Parameters
Results Units Report Limit OF
Prepared Analyzed CAS No. Qual
'HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mg/L
5.0 1
06/20/19 06:39
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Total Petroleum Hydrocarbons NO mg/L
5.0 1
06/20/19 06:39
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Copper
9.2 ug/L
5.0 1
06/19/19 16:04 06/21/19 16:16 7440-50-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/24/2019 11:08 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 15

aceAnalytical
wawpaCBIa0.5. roln
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
2225 Resent de Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
SW JUNE 2019
92432379
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92432379001
1
EPA 1664B
JMS
1
PASI-C
EPA 16646
JMS
1
PASI-C
EPA 200.7 Rev 4.41994
SH1
3
PASI-A
SM 2540D-2011
MJP
1
PASI-A
92432379002
2
EPA 1664E
JMS
1
PASI-C
EPA1664B
JMS
1
PASI-C
EPA 200.7 Rev 4.41994
SHi
3
PASI-A
SM 2540D-2011
MJP
1
PASI-A
92432379003
3
EPA 1664B
JMS
1
PASI-C
EPA1664B
JMS
1
PASI-C
EPA 200.7 Rev 4.41994
SHi
3
PASI-A
SM 2540D-2011
MJP
1
PASI-A
92432379004
4
EPA 1664B
JMS
1
PASI-C
EPA1664B
JMS
1
PASI C
EPA 200.7 Rev 4.41994
SHi
3
PASI-A
SM 2540D-2011
MJP
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This repo" shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 3 of 15

1�5ace Analytical
wewpseeJe0.t.rom
I
ANALYTICAL RESULTS
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: SW JUNE 2019
Pace Project No.: 92432379
Sample: 3 Lab ID: 92432379003 Collected: 06/09/19 09:45 Received: 06/10/19 13:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Lead NO ug/L 5.0 1 06/19/19 16:04 06/21/1916:16 7439-92-1
Zinc Q5:zA 59.4 ug/L 10.0 1 06/19/19 16:04 06/21/19 16*16 7440-66-6
2540D Total Suspended Solids Analytical Method: SM 2540D-2011
Total Suspended Solids ND mg/L 2.7 1 06/14/19 12:26
Sample: 4 Lab ID: 92432379004 Collected: 06/09/19 10:00 Received: 06/10/19 13:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mg/L
5.0
1
06/20/19 06:39
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
NO mg/L
5.0
1
06/20/19 06:39
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Copper
6.5 ug/L
5.0
1
06/1911916:04 06/21/1916:19 7440-50-8
Lead NO ug/L
1r)r(JS,V
5.0
1
06/19/19 16:04 06/21/19 16:19 7439-92-1
Zinc
55.8 ug/L
10.0
1
06/1911916:04 06/21/1916*19 7440-66-6
I:
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
NO mg/L
3.0
1
06/14/19 12:26
REPORT OF LABORATORY ANALYSIS
° This report shall not be reproduced, except in full,
Dale: 0624/2019 11:08 AM without the written consent of PaceAnalytical Seroces, LLC,
Page 5 of 15

172ceAna,l e
/ wwd',p9Celaas.CPn1
j
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr
Asheville, NC 28804
[phone]
Project: SW JUNE 2019
Pace Project No.: 92432379
QC Batch. 482233
Analysis Method:
EPA 1664B
QC Batch Method: EPA 1664B
Analysis Description:
1664 HEM, Oil and
Grease
Associated Lab Samples: 92432379001,92432379002,92432379003,92432379004
METHOD BLANK: 2607679
Matrix: Water
Associated Lab Samples: 92432379001,92432379002,92432379003,92432379004
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Oil and Grease
mg/L
NO 4.8
06/20/19 06:37
LABORATORY CONTROL SAMPLE:
2607680
Spike LCS
LCS
% Rec
Parameter
Units
Conic. Result
°% Rec
Limits Qualifiers
Oil and Grease
mg/L
38.5 37.2
97
78-114
MATRIX SPIKE SAMPLE:
2607681
92432650001 Spike
MS
MS
%Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 38.5
39.4
99
78-114
MATRIX SPIKE SAMPLE:
2607682
92433386001 Spike
MS
MS
%Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
NO 38.5
37.6
97
78-114
Results presented on this page are in the units indicated by the -Units- column except where an alternate unit is presented to the night of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 0624/2019 11:08 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 15

aceAnalytical e
wwwpacala0s.cwn
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: SW JUNE 2019
-
Pace Project No.: 92432379
. QC Balch: 482234
Analysis Method:
EPA 1664E
QC Batch Method: EPA 1664B
Analysis Description:
1664 SGT-HEM, TPH
Associated Lab Samples: 92432379001, 92432379002,
92432379003, 92432379004
METHOD BLANK: 2607683
Matrix: Water
Associated Lab Samples: 92432379001,92432379002,92432379003,92432379004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND 4.8
06/20/19 06:37
LABORATORY CONTROL SAMPLE:
2607684
Spike LCS
LCS %Rec
Parameter
Units
Conc. Result
%Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
19.2 19.9
104 64-132
MATRIX SPIKE SAMPLE:
2607685
92432650001 Spike
MS MS
e/ Rec
Parameter
Units
Result Conc.
Result %Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
NO 19.2
21.2 110
64-132
MATRIX SPIKE SAMPLE:
2607686
92433386001 Spike
MS MS
%Rec
Parameter
Units
Result Conc.
Result %Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
NO 19.2
20.3 105
64-132
Results presented on this page are In the units indicated by the -Units- column except where an alternate un It is pmsented to the Hem of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/24/2019 11:08 AM without the written consent of Pace Analytical Services, LLC.
Page 7 of 15

aceAnalytical w
wnwpapaleDs.nxm
I
QUALITY CONTROL DATA
Project: SW JUNE 2019
Pace Project No.: 92432379
uu cinch: 462U87 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92432379001, 92432379002, 92432379003, 92432379004
METHOD BLANK: 2606668
Matrix: Water
Associated Lab Samples: 92432379001,92432379002,92432379003,92432379004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Copper
ug/L
NO 5.0
06/21/1914:16
Lead
ug/L
ND 5.0
06/21/1914:16
Zinc
ug/L
NO 10.0
06/21/19 14:16
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
2606669
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
e/ Rec
Limits Qualifiers
Copper
ug/L
500
502
100
85-115
Lead
ug/L
500
481
96
85-115
Zinc
ug/L
500
486
97
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2606670
2606671
MS
MSD
92432349001
Spike
Spike
MS
MSD
MS MSD
%Rec
Parameter
Units Result
Conic.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
Copper
ug/L NO
500
500
512
515
101 102
70-130
1
Lead
ug/L NO
500
500
477
476
95 95
70-130
0
Zinc
ug/L 22.3
500
500
498
501
95 96
70-130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2606672
2606673
MS
MSD
92432955001
Spike
Spike
MS
MSD
MS MSD
%Rec
Parameter
Units Result
Conc.
Conic.
Result
Result
% Rec e/ Rec
Limits
RPD Qual
Copper
ug/L 17.2
500
500
542
536
105 104
70-130
1
Lead
ug/L NO
500
500
487
490
97 98
70-130
1
Zinc
ug/L 110
500
500
609
615
100 101
70-130
1
Results presented on this papa are In the units Indicated by the -Units- column except where an alternate unit Is presented to the right otth. result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/24/2019 11:08 AM without the write. consent of Pace Analytical Services, L-C. Page 8 of 15

i a
1�5ace Analytical
wwwpacslags.cam
QUALITY CONTROL DATA
Project: SW JUNE 2019
Pace Project No.: 92432379
QC Batch: 481177 Analysis Method: SM 254OD-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92432379001
METHOD BLANK: 2602778 Matrix: Water
Associated Lab Samples: 92432379001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
I Total Suspended Solids mg/L NO 2.5 06/14/1912:15
Pace Analytical Services, LLD
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE:
2602779
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
Total Suspended Solids
mgt-
251
246 98
90-110
" SAMPLE DUPLICATE: 2602780
.,
92432547001
Dup
,
Parameter
Units
Result
Result RPD
Qualifiers
Total Suspended Solids
mg/L
27.4
19.2
35 D6
!• SAMPLE DUPLICATE: 2602781
92432553002
Dup .
Parameter
Units
Result
Result RPD
Qualifiers
Total Suspended Solids
li
�I
mg/L
17.6
30.4
53 D6
Results presented on this pap. are in the units Indicated by the 'Ur iti column except vmera sn alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/24/2019 11:08 AM without the written consent of Pace Analytical Services, L-C. Page 9 of 15

ace Analytical
wwwpawla0.t.can
j
QUALITY CONTROL DATA
Pace Analytical Service::, LLC
2225 Riverside D,.
Asheville, NC 28804
(828)25a-7176
Project: SW JUNE 2019
Pace Project No.: 92432379
QC Batch: 481178
Analysis Method:
SM 254OD-2011
QC Batch Method: SM 254OD-2011
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92432379002, 92432379003, 92432379004
METHOD BLANK: 2602782
Matnx:
Water
Associated Lab Samples: 92432379002, 92432379003, 92432379004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
NO
2.5 06/14/19 12:25
LABORATORY CONTROL SAMPLE:
2602783
Spike
LCS
LCS e/ Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
251
250
100 90-110
SAMPLE DUPLICATE: 2602784
92432316001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
525
572 9 D6
SAMPLE DUPLICATE: 2602785
92432341001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
14.0
15.2 8 D6
Results presented on this paps are In the units Indicated by the -Units- column except where an alternate unit is pre tented to the dam of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/24/2019 11 :08 AM without the wntten consent of Pace Analytical services, LLC. Page 10 of 15

�2cleAnalXicalo
w Mcelabs.corn
QUALIFIERS
Project: SW JUNE 2019
Pace Project No.: 92432379
DEFINITIONS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MOL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL- Reporting Limit -The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
ii Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
IJ LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0612412019 11:08 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 15

Pace Analytical Services, LLC
2eAnalytical"' 2225 Riverside Dr.
Asheville, NC 28804
w»wpsale0.s.rom
(826)2547176
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SW JUNE 2019
Pace Project No.: 92432379
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92432379001
1
EPA1664B
482233
92432379002
2
EPA 1664B
482233
92432379003
3
EPA1664B
482233
92432379004
4
EPA1664B
482233
92432379001
1
EPA 1664B
482234
92432379002
2
EPA 16648
482234
92432379003
3
EPA1664B
482234
92432379004
4
EPA1664B
482234
92432379001
1
EPA 200.7 Rev 4 4 1994
482067
EPA 200.7
Rev 4.4 1994
482125
92432379002
2
EPA 200.7 Rev 4.4 1994
482067
EPA 200.7
Rev 4.4 1994
482125
92432379003
3
EPA 200.7 Rev 4.4 1994
482067
EPA 200.7
Rev 4.4 1994
482125
92432379004
4
EPA 200.7 Rev 4.4 1994
482067
EPA 200.7
Rev 4.4 1994
482125
92432379001
1
SM 2540D-2011
481177
92432379002
2
SM 2540D-2011
481178
92432379003
3
SM 2540D-2011
481178
92432379004
4
SM 2540D-2011
481178
Date: 06/24/2019 11:08 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 15

Document Name: Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR) Page 1 of 2
PaceAnalytieal Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville z Eden❑ Greenwood ❑ Huntersville I❑ Raleigh❑
Client NamMechanicsville❑
• e: L110 : 9,2432379
�I • Project«: I�IIdIISeI�IIIIIIIEII
Courier: []Fed Ex []UPS ❑USPS ❑Elient
❑ Commercial ❑Pace ❑Other._ 92�}32379
II Custody Seal Present? []Yes PNo Seals Intact? (]Yes E]�N`o
R
Packing Material: ❑Bubble Wrap Bubble Bags []None ❑ Other
Thermomete. 2�p Type of lce: []Wet ❑Bite
OR Gun ID: �
Cooler Temp ('C): b, D I p`Correction Factor: Add/Subtract ('Cl 0 ! C)Cooler Temp Corrected (°C): `u �y
USDA Regulated Soil (�/A, seater sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
Date/Initials Person Examining Contents: `' -(O /o I2, Biological Tissue oxen?
❑Yes ❑No F41,11A
(done J �y 11./ (ocit e Qt)
Temp should be above freezing to 6'C
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
L_JYeS UNo
--
Commence/Discrepancy:
Chain of Custody Present?
1
rs
❑No
❑N/A
1.Samples
Arrived within Hold Time?
iiji'E
5'es
❑No
❑N/A
2.Short
Hold Time Analysis (<72 hr.)?
yes
No
❑N/A
3.
Rush Turn Around Time Requested?
❑Yrs
No
❑N/A
4.
Sufficient Volume?
yes
❑No
❑N/A
5.
Correct Containers Used?
Dyes
❑No
❑N/A
6.
-Pace Containers Used?
res
❑No
❑N/A
Containers Intact?
pyas
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
Sample Labels Match COC? ') G// D/f 9
❑yes
OYcs
No
o
❑N/A
❑N/A
8.
9. C
C), t'd-- &/C C 5 c- / f /' C/ ^o"-
,'//A
Nr.Q%}
�iCfL/✓a
-Includes Date/Time/ID/Analysis Matrix:__-,_
Headspace in VOA Vials (>S-6mml?
❑Yes
❑No
/A
10.
Trip Blank Present?
❑yes
❑No
N/A
11.
Tripelank Custody Seals Present?
❑yes
❑No
N/A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
n
Date/Time:
Field Data Required? ❑Yes ANo
Date:
Date:
/
Page 13 of 15

rt__ a.__�. 1__,
-Pkehid17NG.11
Document Name: Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
(
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project 9IOi�t� : 9;2432379
Ptl: col Due Date: 06/24/19
CL.lENF: 93-1•hermo
Z
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot x
Note: Whenever there is a disc repancy affecting North Carolina compliance samples,a copy of this form wlllce sent to the Plorth Carolina DEHNR Certincation Office (i.e.
Out of hold, incorrect preservative, out of temo, incorrect containers.
Page 14 of 15

p'?
FaceAnalyical'
CHAIN -OF -CUSTODY If Analytical Request Document N
The Chainot-Custody is .LEGAL DOCUMENT. All relevant fields must oe completed accurately. o
N
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Page: 01
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Required Client Information: Required Project Information: Invoice Micronesia .r /� !� A [j
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phone Fax: Pmlect Name: Site Location �\
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Requested Duo DdtertAT: Pmryn Numeec v:�Pr°uw a; STATE:
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CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a. LEGAL DOCUMENT. All relevant fields must be completed. accurately. —
• ww.paceum.com
Page: of
Section A Section B Section C
1962348
Required Client Information: Required Project Information: Invoice Inform tlop: �J
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Company. Report To: 4t , \` - C \^ ,. T t pJL,,SN
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U A v
N
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SIGNATURE SAMPLER:
of
-tmppdant Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5%per Trader for any invoices not paid within 30 days. F-ALL-U-U2UreV.0 /, 1 b-May-ZUU/

Instructions for completing Chain of Custody (COC)
1. Section A and B: Complete all Client information at top of shed company name, address, phone; fax_ contact (the person to contact if thew arc
questions, and who will receive the final report.), c-mail address (if available), PO#, Project Name and/or Project Number as you would like to see it
appear on the report.
2. Section C: Invoice Information: Billing information is included in this section. "flux information should include the name and address of thv person
receiving the invoice.
3. Quote Reference should be completed if quotation was provided by pace Anahtical. The Project Manager, and profile No. will be completed by
pace Anahtical Services.
4. Site Location: A separate COC must be tilted out for each day of sample collection. Record the two letter postal code for the US state in which the
samples wen collected.
5. Re2ulatory Agency: List the prouram that is guiding the work to ensure proper regulations are followed.
6. Section D: Complete a Sample Description in the "SAMPLE ID' section as you would like it to appear on the laboratory report. 'file following
information should also be included: the sample matrix, sample type (G (grab) or C (composite). When collecting a composite, the start time and end
time should be documented in the respective boxes. The collection time for a grab (G) sample should be entered in the boxes marked 'Composite
Eud/Grab'), Sample temp at collection (if required by state), the total number of containers, and preservative used.
7. Mark if the sample was filtered in the field by marking Y or N in `I'iltcred' row by the An lysis requested.
8. Requested Analysis: List the required analvsis and methods on the lines provided and place a check in the column for the samples requiring the
analysis. Additional comments should be referenced in the bottom left hand comer or include attachments for extended lists of parameters.
9. The sampler should print their name in the space provided and sign their name followed by the date of the sampling event at the bottom of the COC in
the spaces designated for `SAMPLER NAME AND SIGNATURE'.
10. When relinquishing custody of the samples to a representative of the laboratory or other organization, indicate the Item Numbers of those samples
being transferred; sign relinquished by, date and time, and include your affiliation.
*Important Note:
Standard Turnaround Time is 2 Weeks/10 business days. Results will be delivered by end of business on the date due unless other arrangements
have been made with },our project manager.
Special Project Requirements such as Low Level Detection Limits or level of QC reported must be included on the chain of custody in the Additional
Comments section.

Thermo Fisher
SCIENTIFIC
June 12, 2019
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: Stormwater Analvtical Monitoring Results for Thermo Fisher Scientific, LLC
I have attached the monthly storm water discharge monitoring report. For the month of May,
there was no discharge at any single outfall.
If you have any questions, please feel free to contact me at 828-658-2845
Jeremy Putnam
EHS Manager
Attachments: 1

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted: 06/12/19
CERTIFICATE OF COVERAGE NO. NCG030134
FACILITY NAME: Thermo Fisher Scientific (Asheville) LLC
COUNTY: Buncombe
PERSON COLLECTING SAMPLES: Jeremy Putnam, EHS
LABORATORY: Pace Analytical Lab Cert. #
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR
SAMPLEPERIOD _Jan-June_July-Dec
Or X Monthly: May
DISCHARGING TO CLASS C R1 ❑ HQW nrrout ❑ PNA
❑Zero -flow ❑NaterSupply ❑SA
RECEIVE [-]Other
JUL 9 r20t9
CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -
DWR SECTION
o discharge this period?'
Outfall No.
Date Sample
Collected ,
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
p H,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons .
Total Toxic
Organics s
Benchmarks
-
-
100 mg/L or 50 mg/L"
6.0 - 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
Outfall 1
Outfall 2
Outfall 3
Outfall 4
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfan.
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO
monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the
General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO),
I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent
management plan included in the Stormwater Pollution Pre n 'on Plan."
Name (Print name)
i e (Prin title)
la -
Signature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format "<XX mg/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
F_7At
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches'
New Motor Oil or
Hydraulic Oil Usage
Non -Polar 0&G Total
/
Petroleum Hydrocarbons
Total Suspended
p
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or So mg/L^
Parameter Code
-
46529
NCOIL
00552
CO530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
2 EXCEE DANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL?
YES X NO
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES NO REGIONAL OFFICE CONTACT NAME: Ms. Laura Herbert
(Asheville Regional Office)
Mail an oriainal copv of this DMR, including all "No Discharge"reports, within 30 days of receipt of the lab results for at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am pyare that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
_Permit. Date: 11/1/2018-05/31/2021
11/1/2018
�iu�Ll�
Date
SWU-245, last revised-

Thermo fisher
SCIENTIFIC
RECEIVE®
June 27, 2019
JUL (1.r2019
Division of Water QualityCENTRAL FILES
Attn: DWQ Central Files DWR SECTION
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: Stormwater Analvtical Monitoring Results for Thermo Fisher Scientific, LLC
I have attached the analytical monitoring results from stormwater sampling that was collected on
June 9, 2019 at Thermo Fisher Scientific, LLC's three outfalls.
Per our General Storm Water Permit No. NCG03000 requirements of monthly monitoring for
applicable parameters during a storm event, I have sampled each outfall for copper, zinc, pH,
lead, TSS, and Non -Polar Oil/Grease/TPH. All results were within the benchmark values as
noted in Table 3 of the general storm water permit. We have implemented a Tier Three response
for the site and Thermo Fisher Scientific LLC has notified the Asheville Regional Office. Thermo
Fisher Scientific LLC is currently working with an environmental consultant to help achieve
compliance with the bench mark values set forth in the facility's storm water permit. I have
attached the completed Monitoring Report containing the monitoring results from the three
outfalls.
If you have any questions, please feel free to contact me at 828-658-2845
Jeremy Putnam
EHS Manager
Attachments: 1