HomeMy WebLinkAboutNCG030130_MONITORING INFO_20190827STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/V U& U 3 0 1-J z)
DOC TYPE.
❑ HISTORICAL FILE
tG MONITORING REPORTS
DOC DATE
❑ 9 b ��
YYYYMMDD
MILD
S
ENGINEERING, INC.
August 13, 2019
Mr. Ryan Pennington
Gastonia Components and Logistics
Daimler Trucks North America, LLC
1400 Tulip Drive
Gastonia, NC 28052
p % I Z01s
Cr
CT O IN,
Subject: Monthly Sampling — July 2019
NPDES General Permit No. NCG030000 - CoC No. NCG030130
Daimler Trucks, Gastonia Components and Logistics, LLC
1400 Tulip Drive Gastonia, North Carolina
Shield Project No. 1140099-07
Dear Mr. Pennington:
Shield Engineering, Inc. (Shield) was able to successfully collect a monthly stormwater sample for Stormwater
Discharge Outfall (SDO) #001 at the Daimler Trucks Gastonia facility during the month of July 2019. During
the July 23`d sampling event, Shield's measurement for pH was 8.7 at SDO #001. The Qualitative Monitoring
Reports and a partially completed Discharge Monitoring Report (DMR) form are attached to this cover letter. In
addition, the analytical results for the stormwater samples collected during the qualifying storm event are
attached to this cover letter. Results from the July 23rd sampling event show no exceedances. However, the
semi-volatiles components of the total toxic organics (TTO) parameter were not analyzed by the commercial
laboratory within the 7 day holding time. Since the facility does implement a Solvent Management Plan, Shield
recommends that the Gastonia facility provide a signature for the TTO monitoring waiver for the July 2019
DMR on the top of page 2 of the DMR. Shield is in communication with the commercial laboratory to address
the holding time issue.
Daimler's Gastonia facility remains in Tier Three of the NPDES General Permit No. NCG030000 at SDO #001
for Copper and pH. Shield will continue to perform monthly sampling at SDO #001 per Tier Two requirements
until instructed to halt by Daimler. Shield greatly appreciates the opportunity to provide environmental services
to Daimler Trucks, of North America. If you have any questions in reference to this document or require further
information, please feel free to contact either of the undersigned at (704) 394-6913.
Respectfully,
SHHIF.L]D ENGINEERING, INC.
Melind M. Greene
Senior Engineer
Attachments
Robert L. Griffin, PE
President
4301 Taggart Creek Road Telephone 704.394.69 f3
Charlotte, NC 28208 w .shieldengineering.com Fax 704.394,6968
StormwaterDischarge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCG03 0 1 3 0
FACILITY NAME D imler Trucks -Gastonia Components 8 Logistics
COUNTY Gaston
PERSON COLLECIING SAMPLES B. Huggins /Shield Engineering, Inc.
LABORATORY.Shealy Environmental Services Lab Cert. # 329
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
8n/20tg
SAMPLE COLLECTION YEAR 2019
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or 0 Monthly'. July (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow []Water Supply []SA
Mother
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No dischome this period7'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24hour rainfall
amount,
Inches3
Total Suspended Solids
PH
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Or anlcss
g
Benchmarks
_
-
100 mg/L or 50 mg/L4
6.0-9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
Most
01094
00552
78241
SDO#001
07/23/19
0.25
1 24
8.7
1 0.0085
0.00083
0.023
1 <5.0
1 0.76024
SDO#002
NA
NA
NA
NA
NA
NA
NA
NA
NA
SDO#003
NA
NA
NA
NA
NA
NA
NA
NA
NA
Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outrall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
° See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Seo» 56W+In i
Name (Print name)
R.wir Mar�aa��
fide (Prin ' le
signs a Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
No discharge this period?2
n
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches'
New Motor Oil or
Hydraulic Oil Usage
Non -Polar 0&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or So mg/L"
Parameter Code
-
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3
FOR PART AAND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEE DANCES IN A ROW FORTH E SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ®NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an oriainal copv of this DMR, includinq all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the
case of No Discharge" reportsl to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 3 of 3
Envtronmentul
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidam;e on filling out this form, please visit https://dcq.nc.gov/about/divisiom/energy-mineral-land-resources/
npdes-stormwater.gps
Permit No.: N_/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/
Facility Name: t�:.r,.I Fj ( -a 6 -,: p
County: iV.— Phone No.
u
Inspector:(`/�(vr-i.an--
Date of Inspection:
Time of Inspection: SSprr.-
Total Event Precipitation (inches): Q. L S
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittec or Designee)
1. Outfall Description:
Outfall No. 3 r» 001 Structure (pipe, ditch, etc.): Go r r re.f -e— 44'
Receiving Stream:
Describe the industrial activities that occur within the outfall drainage area:
Page 1 of 2
SWU-242, L= modified 06/01/2019
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: g( r Ori s S,C� ' oN
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): AJO Nt=
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy: 10
2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
n2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solids'and 5 is extremely muddy:
0 2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes 4/No. _
8. Is there an oil sheen in the stormwater discharge? OYes kKNo.�_
9. Is there evidence of erosion or deposition at the outfall? O Yes O No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
Indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 061012019
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208--5483
Attention: Melinda Greene
Project Name: Freightliner Gastonia SW
Lot Number:UG24099
Date Completed:08/06/2019
Project Manager:Grant Wilton
08/07/2019 10:32 AM
Approved and released by:
Project Manager: Kelly M. Nance
N
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the vaitten approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (003) 791-9111 w .shealylab.wm
Page 1 or 30
SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Shield Engineering
Lot Number: UG24099
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy') Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Semivolatiles - Method 626.1
Sample -001 was analyzed outside of the 7-day holding time.
Sample -001 was diluted 5X due to the sample matrix. The reporting limits have been raised accordingly.
ICP-MS Metals - Method 200.8
The method blank associated with batch 23922 had zinc detected at a concentration that was below'/
the LOQ. All samples associated with this method blank that have detections for zinc have been flagged
with a "6' qualifier.
Shealy Environmental Services, Inc.
106 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (603) 791-9111 w .shealylab.com
Page 2 of 30
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Shield Engineering
Lot Number: UG24099
Project Name: Freightliner Gastonia SW
Project Number:
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDO-001 Aqueous 07/23120191555 07/24/2019
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 (803)791-9700 Fax (803) 791-9111 v shealylob.00m
Page 3 of 30
SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
Shield Engineering
Lot Number: UG24099
Project Name: Freightliner Gastonia SW
Project Number:
Sample Sample ID
Matrix
Parameter
Method
Result a
Units
Page
001 SOO-001
Aqueous
TSS
SM 254oD-
24
mg/L
5
001 SDO-001
Aqueous
Copper
200.8
8.5
uglL
10
001 SOO-001
Aqueous
Lead
200.8
0.83 J
ug/L
10
001 SDO-001
Aqueous
Zinc
200.8
23 B
ug/L
10
(4 detections)
Shealy Environmental Services, Inc.
105 Vantage Point Drive West Columola, SC 29172 (803) 791-9700 Fax (803) 791-9111 x ahealylao.wrn
Page 4 of 30
Inorganic non-metals
Client:Shleld Engineering Laboratory ID: UG24099-001
Description: SDO-001 Matrix: Aqueous
Dale Sampled:07/2312019 1555 Project Name: Frelghtliner Gastonia SW
Date Received:0712412019 Project Number:
Run Prop Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (TSS) SM 254OD-2011
1 07/28/2019 2140 MOM
23960
1 (SGT - HEM (n) 1664B
1 07126/2019 0948 ARP
23832
CAS Analytical
Parameter
Number Method
Result O
LOO DL
Units Run
TSS
SM 25400-
24
12 1.0
mg/L 1
SGT- HEM (non -polar material)
1664E
NO
5.0 1.6
mg/L 1
LOO - Limit of Ou ni itolion B • CaUxued in Me method bleryt E = Ouantib on of compound exa dad the C libration mnge OL = Datecddn L Imit
NO = Not detactee at or above Me DL N • Recovery is out of entaro P = The RPD batwwn two 3C columns exreeds 40% J = Estdnared result < LOO and . OL
H = Out of holding time W = Reserve an wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Paint Drive West Columbia, SC 29172 (803) 791-97DO Fax (803) 791-9111 wvrw.shealylab,com
Page 5 of 30
Volatile Organic Compounds by GC/MS
Client:Shield Engineering Laboratory ID: UG24099-001
Description: SDO-001 Matrix: Aqueous
Date Sampled:07/23/2019 1555 Project Name: Freightliner Gastonia SW
Date Received:07/24/2019 Project Number.
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 624.1 624.1 1 07/25/2019 0424 STM 23669
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acrolein
107-02-8
624A
NO
5.0
4.0
ug/L
1
Acrylonitrile
107-13-1
624.1
ND
5.0
0.80
ug/L
1
Benzene
7143-2
624.1
NO,
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4
624.1
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2
624.1
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
624.1
ND
2.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5
624.1
IND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7
624.1
NO
1.0
0A0
ug/L
1
Chloroethane
75-00-3
624.1
NO
2.0
0.40
ug/L
1
2-Chloroethylvinylether
110-75-8
624.1
ND
5.0
0.40
ug/L
1
Chloroform
67-66-3
624.1
NO
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
624.1
ND
2.0
0.40
ug/L
1
Dibromochloromethane
124.48-1
624.1
ND
1.0
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
624.1
ND
1.0
0.40
ug/L
1
1,3-Dichlorobenzene
541-73-1
624.1
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
624.1
NO
1.0
0.40
ug/L
1
Dichlorodi0uoromethane
75-71-8
624.1
ND
2.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
624.1
ND
1.0
0.40
ug/L
1
1,2-Dichloroelhane
107-06-2
624.1
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
624.1
NO
1.0
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2
624.1
ND
1.0
0.40
ug/L
1
trans-1,2-Dichloroethene
156-60-5
624.1
ND
1.0
0.40
ug1L
1'
1,2-Dichloropropene
78-87-5
624.1
ND
1.0
0.40
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
624.1
ND
1.0
0.40
ug/L
t
trans-1,3-Dichloropropene
10061-02-6
624.1
NO
1.0
0.40
ug/L
i
Ethyibenzene
100-41.4
624.1
NO
1.0
0.40
ug/L
1
Methylene chloride
75-09.2
624.1
NO
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
624.1
NO
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
624.1
NO
1.0-
0.40
ug/L
1
Toluene
108-BB-3
624.1
ND
1.0
0.40
uglL
1
1,2,4-Trichlorobenzene
120-82-1
624.1
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
624.1
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
624.1
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
624.1
ND
1.0
0.40
ug/L
1
Trichloro8uoromethane
75-69-4
624.1
ND
1.0
0.40
ug/L
1
Vinyl chloride
75-01-4
624.1
ND
1.0
0A0
ug/L
1
Run 1
Acceptance
Surrogate
Q h Recovery
Limits
Bromofluorobenzene
105
70-130
1,2-Dichloroethane-d4
90
70-130
Toluene-d8
105
70-130
L00= Limit or Ou.MW1en B= Detected in the method black E= Ouaolitalion W ccvh a nd exceeded the calibration range DL=Detection Limit
NO= Not detected at or eWve Me DL N= Recovery 15 out or criteria P= The RPD boMeen We GC columns O.Weels 40% J= Estimated result a LOG and >OIL
H = Out W hating lima W = Reponed on wet weight balls
Shealy Environmental Services, Inc.
10a Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (e03) 791-9111 wwwshe tlylatocom
Page 6 or 30
Semivolatile Organic Compounds by GC/MS
Client:Shield Engineering Laboratory ID: UG24099-001
Description: SDO-001 Matrix: Aqueous
Date Sampled:07123120191655 Project Name: Freightliner Gastonia SW
Date Received:0712412019 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 5 08/05/20192022 JCG 08102120191705 24616
CAS
Analytical
Parameter
Number
Method
Result
O
LOO
DL
Units
Run
Acenaphthene
83-32-9
625A
NO
H
8.0
4.0
ug/L
1
Acenaphthylene
208-96-8
625.1
NO
H
8.0
4.0
ug/L
1
Anthracene
120-12-7
625.1
NO
H
8.0
4,0
ug/L
1
Benzidine
92-87-5
625.1
NO
H
40
20
ug/L
1
Benzo(a)anthracene
56-55-3
625.1
NO
H
8.0
4,0
ug/L
1
Benzo(a)pyrene
50-32-8
625.1
ND
H
8.0
4.0
uglL
1
Benzo(b)8uoranthene
205-99-2
625.1
NO
H
8.0
4.0
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625.1
NO
H
8.0
4.0
ug/L
1
Benzo(k)Buoranthene
207-08-9
625.1
NO
H
8.0
4.0
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
525.1
NO
H
8.0
4.0
ug/L
1
Butyl benzyl phthalate
85-68-7
625.1
NO
H
8.0
4.0
ug/L
1
bis (2-Chloro-l-methylethy0 ether
108-60-1
625.1
NO
H
8.0
4.0
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625.1
NO
H
8.0
4.0
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625.1
NO
H
8.0
4.0
ug/L
1
bis(2-Chloroethyl)ether
111.444
625.1
NO
H
8.0
4.0
ug/L
1
2-Chloronaphthalene
91-58-7
625.1
NO
H
8.0
4.0
ug/L
1
2-Chlorophenol
95-57-8
625.1
ND
H
8.0
4.0
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625.1
ND
H
8.0
4.0
ug/L
1
Chrysene
218-01-9
625.1
ND
H
8.0
4.0
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625.1
ND
H
8.0
4.0
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625.1
ND
H
40
4.0
ug/L
1
2,4-Dichlorophenol
120-83-2
625.1
NO
H
8.0
4.0
ug/L
1
Diethylphthalate
84-66-2
625.1
ND
H
8.0
4.0
ug/L
1
Dimethyl phthalate
131-11-3
625.1
NO
H
8.0
4.0
ug/L
1
2,4-Dimethylphenol
105-67-9
625.1
ND
H
8.0
4.0
ug/L
1
Di-n-butyl phthalate
94-74-2
625.1
ND
H
8.0
4.1
uglL
1
4,6-Dinitro-2-methylphenol
534-52-1
625.1
- NO
H
40
4.0
uglL
1
2,4-Dinitrophenol
51-28-5
625.1
NO
H
40
4.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
625.1
NO
H
16
4.0
ug/L
1
2,6-Dinitrotoluene
606-20-2
625.1
NO
H
16
4.0
ug/L
1
Di-n-octylphthalate
117-84-0
625.1
NO
H
8.0
4.0
ug/L
1
1,2-Olphenylhydrazine(as azobenzene)
103-33-3
625.1
NO
11
8.0
4.0
ug/L
1
bis(2-Ethylhexyl)ph tha late
117-81-7
625.1
NO
H
40
20
ug/L
1
Fluoranthene
206-44-0
625.1
NO
H
8.0
4.0
ug/L
1
Fluorene
86-73-7
625.1
ND
H
8.0
4.0
ug/1-
1
Hexachlorooenzene
118-74-1
625A
ND
H
8.0
4.0
ug/L
1
Hexachlorobutadiene
87-68-3
625.1
NO
H
8.0
4.0
ug/L
1
Hexachlorocyclopentediene
77-474
625.1
NO
H
40
20
ug/L
1
Hexachloroethane
67-72-1
625.1
NO
H
8.0
4.0
ugh-
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625.1
NO
H
8.0
4.0
ug/L
1
Isophorone
78-59-1
625.1
NO
H
8.0
4.0
ug/L
1
Naphthalene
91-20-3
625.1
NO
H
8.0
4.0
ug/L
1
Nitrobenzene
98-95-3
625.1
NO
H
8.0
4.0
ug/L
1
2-Nitraphenol
88-75-5
625.1
ND
H
16
4.0
ug/L
1
LOO = Limn of Ouanetation a = Detected in the method blank E = Ouantitution of compound exceeded the calibration range Dr.= Dotecbon Limit
ND Not detected at or above mo OL N= Rocom, is out of Omada P=The RPD bo.0im two GC columns veceeds 40% J= Estimated result< L00 and OIL
H = Out of holding time W = Reported on at weight basis
Shealy Environmental Services, Inc.
106 Va huge Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (003) 791-9111 w .shealylab, com
Pagc 7 of 30
Semivolatile Organic Compounds by GC/MS
Client:Shleld Engineering Laboratory ID: UG24099-001
Description: SDO.001 Matrix: Aqueous
Date Sampled:0712312019 1555 Project Name: Freightliner Gastonia SW
Date Received: 0712412019 Project Number.
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 5 08/05/20192022 JCG 08/0212019 1705 24616
CAS
Analytical
Parameter
Number
Method
Result
O
LOO
DL
Units
Run
4-Nitrophenol
100-02-7
625.1
NO
H
40
20
ug/L
1
N-Nitrosodimethylamine
62-75-9
625.1
NO
H
8.0
4.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625.1
ND
H
8.0
4.0
ug1L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625.1
NO
H
8.0
4.0
ug1L
1
Pentachlorophenol
87-86-5
625.1
NO
H
40
20
ug/L
1
Phenanthrene
85-01-8
625.1
NO
H
8.0
4.0
ug/L
1
Phenol
108-95-2
625.1
NO
H
8.0
4.0
ug/L
1
Pyrene
129-00-0
625.1
NO
H
8.0
4.0
ug/L
1
2,4,6-Thchlorophenol
88-06-2
625.1
NO
H
8.0
4.0
ug/L
1
Run 1 Acceptance
O % Recovery Limits
2-Fluorophenol
H
25
24-127
Nitrobenzene-d5
H
60
38-127
Phenol-d5
H
35
28-128
Terphenyl-014
H
78
10-148
2,4,6-Tribromophenol
H
60
41-144
L00 = Limit of Ouenburtion a = Dinartme In Me method blank E • Ouantitation of compound exceeded the calif abon range OL = Defection Ill
NO v Not detected at or above the 01. N = Recovery is out of cram. P • The RPO between Iwo GC columns exceeds 40% J = Estimated result � L00 and > DL
H = Out of Molding time W = Reported an wet waight basis
Shealy Environmental Services, Inc.
1136 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.ahealylab.com
Page 8 of 30
Organochlorine Pesticides and PCBs
Cllent:Shield Engineering Laboratory ID: UG24099-001
Description: SDO-001 Matrix: Aqueous
Date Sampled:0712312019 1555 Project Name: Freightliner Gastonia SW
Date Received: 0712412019 Project Number:
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 608.3 3665A 608.3 1 0713020192031 CHG 0712612019 1619 23870
2 608.3 3665A 608.3 1 07/302019 1256 CHG 07/26120191619 23870
CAS
Analytical
Parameter
Number
Method
Result O
LOCI
DL
Units
Run
All
309-00-2
608.3
NO
0,040
0.015
ug/L
1
Aroclor 1016
12674-11-2
608.3
NO
0.40
0.15
ug/L
2
Aroclor 1221
11104-28-2
608.3
NO
0A0
0.25
ug/L
2.
Aroclor 1232
11141-16-5
608.3
NO
0,40
0.15
ug/L
2
Aroclor 1242
53469-21-9
608.3
NO
0.40
0.15
uglL
2
Aroclor 1248
12672-29-6
608.3
NO
0A0
0.15
uglL
2
Aroclor 1254
11097-69-1
608.3
NO
0.40
0.15
ug/L
2
Aroclor 1260
11096-82-5
608.3
NO
0.40
0.15
ug/L
2
gamma-BHC (Lindane)
58-89-9
608.3
NO
0.040
0.017
ug/L
1
alpha-BHC
319-84-6
608.3
NO
0,040
0.015
ug/L
1
beta-BHC
319-85-7
608.3
NO
0,040
0.015
ug/L
1
delta-BHC
319-86-8
608.3
ND
0.040
0.015
ug/L
1
Chlordane
57-74-9
608.3
NO
0.40
0.15
ug/L
1
4,4'-DDD
72-54-8
608.3
NO
0.040
0.015
uglL
1
! 4,4'-DDE
72-55-9
508.3
NO
0.040
0.015
ug/L
1
4,4'-DDT
50-29-3
608.3
NO
0.040
0.015
ug/L
1
Dieldrin
60-57-1
608.3
NO
0.040
0.015
ug/L
1
Endosulfan 1
959-98-8
608.3
NO
0,040
0.015
uglL
1
Endosulfan II
33213-65-9
608.3
NO
0.040
0.015
ug/L
1
Endosulfan sulfate
1031-07-8
608.3
NO
0,040
0.015
ug/L
1
Endrin
72-20-8
608.3
NO
0.040
0.015
ugll-
1
Endrin aldehyde
7421-93-4
608.3
NO
0.040
0.015
ug/L
1
Heptachlor
76-44-8
608.3
NO
0.040
0.015
uglL
1
Heptachlor epoxide
1024-57-3
608.3
NO
0.040
0.016
ug/L
1
Toxaphene
8001-35-2
608.3
NO
0.40
0.30
ug/L
1
1 Acceptance Run 2
Decachlorobiphenyl 34 20-131 41 20-131
Tetrachloro-m-xylene 59 30-132 83 30-132
LOG= Limit or connotation B= Deledted in the method blank E= Ouambalion of cameound exceeded the catenation range DL= Detection Limit
ND= Not dammed at or above eW OL N=Recowxyis out of chards P=The RPO belween two GC cnWmns exceeds 40% J= Estimated result< LOG and> OL
H= Out at held trod W= Reached on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Page 9 of 30
ICP-MS
Clienl:Shield Engineering Laboratory ID: UG24099-001
'Description: SDO.001 Matrix: Aqueous
Dale Sampled 0712312019 1555 Project Name: Frelghtliner Gastonia SW
Date Received:0712412019 Project Number:
Run Prop Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 2002 200.8 1 07/26/2019 0138 BNW 07/25/2019 1009 23674
2 200.2 200.8 1 07/29/2019 1136 BNW 07127/2019 1048 23922
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Copper
7440.50.8
200.8
8.5
5.0
1.3
ug/L
1
Lead
7439.92-1
200.8
0.83
J
1.0
0.25
ug/L
1
Zinc
7440.66-6
200.8
23
B
10
2.6
ug/L
2
LOD = Limit of Cuanuarlon B= Detected in this method blank E=0uanhation of compound exceeded the calibration range OL= Detection Limit
NO = Not detected at or above the OL N = Recovery is out of brand P = The RPD bee ven two GC Columns exaeeae 40% J = Estimated result < LOG and > OL
H= 0u10 Indiana time W= Reached an vat weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 wviw.shealyleb.com
Page 10 of 30
QC Summary
Sncaly Environmental Servicee, Inc. GC Data for Lot Number: UG24099
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 w .ehealylab.com
Page I I of 30
Inorganic non-metals - MB
Sample ID: UQ23960-001 Matrix: Aqueous
Batch: 23960
Analytical Method: SM 25400-2011
Parameter Result O Dil LOQ DL Units Analysis Date
TSS ND 1 1.0 1.0 mi 07/28/2019 2140
LOG c Limit of Ouanntation P • TM RPD between two GC columns exooeds 40% N , Recovery is out of ctitena
DL=Detection Limit J= Estimated result< LOG and> OL =RPD is out of wane
LOD = Limn of Detection NO = Not eetecled at or above be DL
Note: Calculations are performed before rounding to avoid round -off errors In calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UG24099
106 vantage Point Drive West Cdun ia. SC 29172 (803) 791-9700 Fail 791-9111 wwwsheolylab.Wnn
Page 12 of 30
Inorganic non-metals - LCS
Sample 10: U023960-002
Matrix: Aqueous
Batch: 23960
Analytical Method: SM 254OD-2011
Spike
Amount
Result
% Rec
_ Parameter
(mglL)
(mg/L)
Q Dil % Rae Limit Analysis Date
TSS
250
250
1 99 90-110 07/28/2019 2140
LOG - Limit W Nimlitetion P = The RPD "Ween Wo CC columns exceeds 40% N = Recovery Is out of criers
DL a Direction Limit J = Eetimaled result < LOG and > DL + = RPD is out of crteda
LOD - Unt of Detection NO= Not dote ted at or of wo me DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UG24099
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 w ahealylab.com
Page 13 of 30
Inorganic non-metals - MB
Sample ID: UQ23832-001 Matrix: Aqueous
Batch:23832
Analytical Method: 1664B
Parameter Result Q Oil LCIQ DL Units Analysis Date
SGT - HEM (non -polar material) ND 1 5.0 1.4 mg/L 07/26/2019 0948
LOD a limit of Ouamlutlon P = The RPD beMsen two GC wWmns exmede 40% N = Recovery Is out of crtede
OL - Detecbm Limit J • Estimatod result < LOD aM > OL • = RPD Is out at anted.
LOD = Limit of Detection NO = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UG24099
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 v .shealylab.com
Page 14 of 30
Inorganic non-metals - LCS
Sample ID: UQ23832-002
Matrix: Aqueous
Batch: 23832
Analytical Method: 16646
Spike
Amount
Result
%Rec
Parameter
(mglL)
(mg/L)
Q Dil %Rec Limit Analysis Date
SGT - HEM (non -polar material)
40
34
1 85 64-132 07/2512019 0948
LOG = Limit of Guantitalion P = The RPD betxaen No GC columns exceeds 40% N = Recovery is out of chtone
DL=Detection Lime d= Estimated." a LOG and? OL = RPD Is out of mfede
LOD = Limit of Detector, NO = Not detected al or above me DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UG24099
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (B03) 791-9111 www.shealylob,com
Page U of 30
Volatile Organic Compounds by GC/MS - MB
Sample ID: UQ23669-001 Matrix: Aqueous
Batch: 23669 Prep Method: 624.1
Analvtieal Method: 624.1
Parameter
Result
Q Dil
LOQ
OL
Units
Analysis Date
Acrolein
NO
1
5.0
4.0
ug/L
07/25/2019 0031
Acrylonitrite
NO
1.
5.0
0.80
ug/L
07125/2019 0031
Benzene
NO
'1
1.0
0.40
ug/L
07125/2019 0031
Bromodichloromelhane
NO
1
1.0
0.40
ug/L
07125/2019 0031
t Bromoform
NO
1
1.0
0.40
ug/L
07/25/2019 0031
Bromomethane (Methyl bromide)
NO
1
2.0
0.40
ug1L
07/25/2019 0031
Carbon tetrachloride
NO
1
1.0
0.40
ug/L
07/25/2019 0031
Chlorobenzene
NO
4
1.0
0A0
ug/L
07125/2019 0031
Chloroethane
NO
1
2.0
0.40
ug/L
07125/2019 0031
2-Chloroethylvinylether
NO
1
5.0
0.40
ug/L
07/25/2019 0031
Chloroform
NO
1
1.0
0.40
ug/L
07125/2019 0031
Chloromelhane (Methyl chloride)
NO
.1
2.0
0.40
ug/L
071250019 0031
Dibromochloromethane
NO
1
1.0
0.40
ug/L
07125/2019 0031
1,2-Dichlorobenzene
NO
1
1.0
0.40
ug/L
07126/20190031
1,3-Dichlorobenzene
NO
1
1.0
0.40
ug/L
07125/2019 0031
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
07/25/2019 0031
Dichlorodi0uoromethane
NO
9
2.0
0.40
ug/L
0712512019 0031
1,1-Dichloroethane
NO
T
1.0
0.40
ug/L
07/25/2019 0031
1,2-Dichloroethane
NO
i
1.0
0.40
ug/L
07/25/2019 0031
1,1-Dichloroethene
NO
1
1.0
0.40
ug/L
07125/2019 0031
cis-1,2-Dichloroethene
NO
1
1.0
0.40
ug/L
07/25/2019 0031
trans-1,2-Dichloroethene
NO
1
1.0
0.40
ug/L
07/25/2019 0031
1,2-Dichloropropane
NO
1
1.0
0.40
ug/L
07/2512019 0031
cis-1,3-Dichloropropene
NO
1
1.0
0.40
ug/L
07125/2019 0031
trans-1,3-Dichloropropene
NO
1
1.0
0.40
ug/L
07125/2019 0031
Ethylbenzene
NO
1
1.0
0.46
ug/L
07/25/2019 0031
Methylene chloride
NO
1
1.0
0.40
ug/L
07/25/2019 0031
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
07/25120190031
Tetrachloroethene
ND
1
1.0
0.40
ug/L
07/25/2019 0031
Toluene
NO
1
1.0
0.40
ug/L
07/25/2019 0031
1,2,4-Trichlorobenzene
NO
1
1.0
0.40
ug/L
07/25/2019 0031
1. 1, 1 -Tricharoethane
ND
1
1.0
0.40
ug/L
07/25/2019 0031
1,1,2-Trlchloroethane
ND
1
1.0
0.40
ug/L
07/25/2019 0031
Trichloroethene
ND
1
1.0
0A0
ug/L
07/25/2019 0031
Trlchloro0uoromelhano
ND
1
1.0
0.40
ug/L
07/25/2019 0031
Vinyl chloride
NO
1
1.0
0.40
ug/L
07/25/2019 0031
Acceptance
Surrogate
Q
%Roo Limit
Bromofluorobenzene
101 70-130
1,2-Dichloroethane-d4
89 70-130
Toluene-d8
f
103 70-130
Loa= Limit of Ouimwmion
P= The RPO between two GO nolumns eaweds 40% N=Recovery;, our of nhina
OL=Detection Limit
l= Estimated result< Loa and >DL
= RPDis
out of cmeda
Loa = limit of Detection
ND = Not detected at or above the OL
Note: Calculations are performed before rounding to avoid round -off errors In
calculated results
Shealy Environmental Services, Inc.
QC Data
for Lot Number: UG24099
106 Vantage Point Drive West Columbia,
SC 29172
(803) 791-9700 Fax (803) 791-9111
Wv e,shestylab,com
Page 16 of 30
Volatile Organic Compounds by GC/MS - LCS
Sample ID: U023669-002
Matrix:
Aqueous
Batch: 23669
Prep Method:
624.1
Analytical Method: 624.1
Spike
Amount Result
%Rec
Parameter
(uglL)
(ug/L) 0
Dil
%Rec
Limit
Analysis Data
Acrolein
200
210
1
103
60-140
07/24/2019 2254
Acrylonitrile
40
37
1
92
60-140
07124/2019 2254
Benzene
20
19
1
94
65-135
07124/2019 2254
Bromodichloromethane
20
17
1
87
65-135
07/24/2019 2254
Bromoform
20
18
1
90
70-130
07/24/2019 2254
Bromomelhane (Methyl bromide)
20
20
1
99
15-185
07124/2019 2254
Carbon tetrachloride
20
17
1
86
70-130
07124/2019 2254
Chlorobenzene
20
19
1
96
65-135
07/24/2019 2254
Chloroethane
20
19
1
96
40-160
07/24/2019 2254
2-Chloroethylvinylether
20
17
1
85
1-225
0712412019 2254
Chloroform
20
18
1
91
70-135
07/24/2019 2254
Chloromelhane (Methyl chloride)
20
17
1
87
1-205
07/24/2019 2254
Oibromochloromethane
20
19
1
94
53-149
07124)'2019 2254
1.2-Dichlorobenzene
20
19
1
95
65-135
07/2412019 2254
1,3-Dichlorobenzene
20
19
1
94
70-130
07124/2019 2254
1,4-Dichlorobenzene
20
19
1
94
65-135
07124/2019 2254
Dichlorodifluoromethane
20
17
1
87
60-140
07/24/2019 2254
1,1-Dichloroelhane
20
18
1
90
70-130
07/24/2019 2254
1,2-Dichloroelhane
20
18
1
88
70-130
07/2412019 2254
1,1-Dichloroethene
20
19
1
97
50-150
07Y2412019 2254
cis-1,2-Dichloroethene
20
19
1
93
70-130
07/24/2019 2254
trans-1,2-Dichloroethene
20
19
1
96
70-130
07124/2019 2254
1,2-Dichloropropane
20
18
1
91
35-165
07/24/2019 2254
cis-1,3-Dichloropropene
20
18
1
91
25-175
07124/2019 2254
trans-1,3-Dichloropropene
20
19
1
96
50-150
07/2412019 2254
Ethylbenzene
20
20
1
98
60-140
07/2412019 2254
Methylene chloride
20
18
1
90
60-140
07124/2019 2254
1,1,2,2-Tetrachloroethane
20
20
1
101
60-140
07/24/2019 2254
Tetrachloroethene
20
20
1
99
70-130
07/24/2019 2254
Toluene
20
20
1
98
70-130
07/2412019 2254
1,2,4-Trichlorobenzene
20
20
1
101
60-140
07124120192254
1,1,1-Trichloroethane
20
17
1
86
70-130
07/24/2019 2254
1,1,2-Trichloroethane
20
19
1
97
70-130
07124/2019 2254
Trichloroethene
20
18
1
91
65-135
07/24/2019 2254
Tdchlorofluoromethane
20
18
1
89
50-150
07124/2019 2254
Vinyl chloride
20
18
1
89
5-195
07/24/2019 2254
Acceptance
Surrogate
0
% Roe Limit
Bromolluorcbenzene
101 70-130
1,2-Dichloroethane-d4
87 70-13C
Toluene-d8
100 70-130
L00= Limit of Ouanfitation
P= The RPD dedneon Me GC columns exceeas 40%
N= Rarnvety is out of omens
OL = Detection Limit
d = Estimated result n LOO and > DL
= RPD is out of
cdteda
LOD = Limn of oeteWon
NO = Not detected at or shove the OL
Note: Calculations are performed before rounding to avoid round -off errors
in calculated results
Shealy Environmental Services, Inc. 0C Data for Lot Number: UG24099
105 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803)791-9111 viww.shealylab,com
Page 17 of 30
Semivolatile Organic Compounds by GCIMS - MB
Sample ID: UQ24616-001 Matrix: Aqueous
Batch: 24616 Prep Method: 625.1
Analvtical Method: 625.1 Prep Date: 08/0212019 1705
Parameter
Result Q
Dil
LOD
DL
Units
Analysis Date
Acenaphthene
NO
1
1.6
0.80
ug/L
08105/20191416
Acenaphthylene
NO
1
1.6
0.80
ug/L
08/05120191416
Anlhrocene
NO
1
1.6
0.80
ug/L
08/05/2019 1416
Benzidine
NO
1
8.0
4.0
ug/L
08105/20191416
Benzo(a)anlhracene
NO
1
1.6
0.80
ug/L
08/05/2019 1416
Benzo(a)pyrene
NO
1
1.6
0.80
uglL
08/05/2019 1416
Benzo(b)Ouoranlhene
NO
1
1.6
0.80
uglL
08105,120191416
Benzo(g,h,i)perylene
NO
1
1.6
0.80
uglL
08105120191416
Benzo(k)0uoranthene
NO
1
1.6
0.80
ug/L
08/05/2019 1416
4-Bromophenyl phenyl ether
NO
'1
1.6
0.80
uglL
08105/20191416
Butyl benzyl phthalate
NO
1
1.6
0.80
u9/1,
08/05/2019 1416
b I s (2-Chloro-1-melhylethyp ether
ND
'1
1.6
0.80
uglL
08/05/2019 1416
4-Chloro-3-methyl phenol
NO
1
1.6
0.80
ug/L
08/05/2019 1416
bis(2-Chloroethoxy)methane
NO
1
1A
0.80
ug/L
08/05120191416
bis(2-Chloroethyl)ether
NO
9.
1.6
0.80
ug/L
08/05/2019 1416
2-Chloronaphthalene
NO
1
1.6
0.80
ug/L
08105/20191416
2-Chlorophenol
NO
1
1.6
0.80
ug/L
08105/20191416
4-Chlorophenyl phenyl ether
NO
1.
1.6
0.80
ug/L
08105/2019 1416
Chrysene
NO
1
1.6
0.80
uglL
08105120191416
Dibenzo(a,h)anthracene
NO
"1
1.6
0.80
ug/L
08/05/2019 1416
3,3'-Dichlorobenzidine
NO
1
8.0
0.80
ug/L
08105/20191416
2,4-Dichlorophenol
NO
1
1.6
0.80
ug/L
08/05/2019 1416
Diethylphthalale
NO
1
1.6
0.80
ug/L
08/05/2019 1416
Dimethyl phthalate
NO
1
1.6
0.80
ug/L
08/05/2019 1416
2,4-Dimethylphenol
NO
1
1.6
0.80
ug/L
08105/20191416
Di-n-butyl phthalate
NO
1
1.6
0.81
ug/L
08/05/2019 1416
4,6-Dinilro-2-methylphenol
NO
1
8.0
0.80
ug/L
08105/20191416
2,4-Dinitrophenol
NO
1
8.0
0.80
ug/L
08/05120191416
2.4-Dinitrololuene
NO
1
3.2
0.80
ug/L
08/05/2019 1416
2,6-Dinitrotoluene
NO
1
3.2
0.80
ug/L
08/05/20191416
Dkn-octylphlhalate
NO
1
1.6
0.80
ug/L
08105120191416
1,2-Diphenylhydrazine(as azobenzene)
NO
1
1.6
0.80
ug/L
08/05/2019 1416
bis(2-Ethylhexyl)phthalate
NO
1
8.0
4.0
ug/L
08/05/2019 1416
Fluoranthene
NO
11
L6
0.80
ug/L
08105120191416
Fluorene
NO
L
1.6
0.80
ug/L
08105/20191416
Hexachlorobenzene
NO
1
1.6
0.80
ug/L
08105/20191416
Hexachlorobutadiene
NO
1
1.6
0.80
uglL
08/05/2019 1416
Hexachlorocyclopenladiene
NO
1
8.0
4.0
ug/L
08/05/2019 1416
Hexachloroelhane
NO
1
1.6
0.80
ug/L
08/05/2019 1416
Indeno(1,2,3-c,d)pyrene
NO
1,
1.6
0.80
ug/L
08/05)2019 1416
Isophorone
NO
1
1.6
0.80
ug/L
08/05120191416
Naphthalene
NO
1.
1.6
0.80
ug/L
08/05/20191416
Nitrobenzene
NO
1
1.6
0.80
ug/L
08/05/2019 1416
2-Nitrophenol
NO
1>
3.2
0.80
ug/L
08/05/2019 1416
LOG• Limit of Gudolitatlon P= the RPO retween two CC columns eoxeds 40% IN Recovery is out of enteha
OL I Detection Limit J= Esumated result< LOD am>OL RPD is out of totem
LOD, Limit of Detection NO = Not detwed at or above the OL
Note: Calculations are performed before rounding to avoid round -oft errors in calculated results
Shealy Environmental Servlms, Inc. QC Data for Lot Number: UG24099
106 Ventage Point Drive West Columbia, SC 29172 (903) 791-9700 Fax (803) 791-9111 www.shealyleb.com
Page 18 of 30
Semivolatile Organic Compounds by GC/MS - MB
Sample ID: UQ24616-001 Matrix: Aqueous
Batch: 24616 Prep Method: 625.1
Analytical Method: 625.1 Prep Date: 08/02/2019 1705
Parameter
Result
CI oil
LOCI
OIL
Units
Analysis Date
4-Nitrophenol
NO
1
8.0
4.0
ug/L
08105/20191416
N-Nitrosodimethylamine
NO
1
1.6
0.60
ug/L
08105120191416
N-Nitrosodi-n-propylamine
ND
1
1.6
0.80
ug/L
08/05/20191416
N-Nitrosodiphenylamine (Diphenylamine)
NO
1
1.6
0.80
ug/L
08/05/2019 1416
Pentachlorophenol
NO
1
8.0
4.0
ug/L
08105/20191416
Phenanthrene
NO
1
1.6
0.80
ui
08105120191416
Phenol
NO
1
1.6
0.80
ug/L
08105/20191416
Pyrene
NO
1
1.6
0.80
ug/L
08/05/20191416
2,4,6-Trichlorophenol
NO
1
1.6
0.80
ug/L
08/05/2019 1416
AcceptanceLimit
9 Surrogate
CI
%s Rec
2-Fluorobiphenyl
70
37-129
2-Fluorophenol
38
24-127
i Nitrobenzene-d5
75
38-127
Phenol-d5
55
28-128
Terphenyl-d14
98
10-148
2,4,6-Tribromophenol
86
41-144
L00= Limit of Ouareitation P= The RPD between two GG columns exceeds 40% N= Recovery, is out of criteria
OL=Detection Limit J= Estimated result <LOD not >OL += RPD is out of rotena
LOD = Limit of Detection NO = Not detected at or amve the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. OC Data for Lot Number: UG24099
106 Ventage Point Drivo West Columbia, SC 29172 (803) 791-9700 Fax (a03) 791-9111 www,shealylab.com
Page 19 of 30
Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: UQ24616-002
Matrix:
Aqueous
Batch:24616
Prep Method:
625.1
Analytical Method: 626.1
Prep Date: 08/02/2019 1705
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
_Q Dil
% Roc
Limit
Analysis Date
Acenaphthene
20
14
1
71
47-145
08/05/2019 1440
Acenaphthylene
20
15
1
73
33-145
08105/2019 1440
Anthracene
20
15
1
76
27-133
08/05/2019 1440
Benzidine
100
55
1
55
1-150
08/05/20191440
Benzo(a)anthracene
20
16
1
78
33-143
08105/2019 1440
Benzo(a)pyrene
20
15
1
75
17-163
08105/2019 1440
Benzo(b)8uoranthene
20
16
1
79
24-159
08/0512019 1440
Benzo(g,h,i)perylene
20
15
1
77
1-219
08105/2019 1440
Benzo(k)Ouoranlhene
20
16
1
78
11-162
08105/2019 1440
4-Bromophenyl phenyl ether
20
15
1
73
53-127
08105/2019 1440
Butyl benzyl phthalate
20
17
1
87
1-152
08/05/2019 1440
bis(2-Chloro-l-methylethyl) ether
20
17
1
86
36-166
08/05/2019 1440
4-Chloro-3-methyl phenol
20
16
1
78
22-147
08/0512019 1440
bis(2-Chloroelhoxy)melhane
20
15
1
74
33-184
08105120191440
bis(2-Chloroethyl)ether
20
19
1
94
12-158
08/05/2019 1440
2-Chloronaphlhalene
20
14
1
69
60-120
08105/2019 1440
2-Chlomphenol
20
12
1
61
23-134
08/0520191440
4-Chlorophenyl phenyl ether
20
15
1
74
25-158
08/05/2019 1440
Chrysene
20
16
1
79
17-168
0810520191440
Dibenio(a,h)anthracene
20
16
1
79
1-227
08/05/2019 1440
3,3'-Dichlorobenzidine
20
13
1
64
1-262
08/05/2019 1440
2,4-Dichlorophenol
20
14
1
69
39-135
08105/2019 1440
Diethylphth a late
20
17
1
84
1-120
08105/2019 1440
Dimethyl phthalate
20
16
1
79
1-120
08105/2019 1440
2,4-Dimethylphenol
20
14
1
70
32-120
08105120191440
Di-n-butyl phthalate
20
17
1
85
1-120
08105/2019 1440
4,6-Dinitro-2-methylphenol
20
17
1
86
1-181
08105/2019 1440
2,4-Dinitrophenol
40
30
1
74
1-191
08/05/2019 1440
2,4-Dinitrotoluene
20
16
1
82
39-139
08/05/2019 1440
2,6-Dinitrotoluene
20
17
1
83
50-158
08/05/2019 1440
Di-n-octylphthalale
20
17
1
86
4-146
08105/2019 1440
1,2-Dlphenylhydrazine(as azobenzene)
20
16
1
78
1-150
08/05/2019 1440
bis(2-Ethylhexyl)phthalate
20
18
1
92
8-158
08/05/2019 1440
Ruoranlhene
20
16
1
78
26-137
08/05/2019 1440
Fluorene
20
14
1
72
59-12l
08/0512019 1440
Hexachlorobenzene
20
15
1,
75
1-152
08/05/2019 1440
Hexachlorobutadiene
20
12
1
58
24-120
08105/2019 1440
Hexactllorocyclopentadiene
100
48
1
48
1-150
08/05/2019 1440
Hexachloroethane
20
12
1
58
40-120
08/05/2019 1440
Indeno(1,2,3-c,d)pyrene
20
15
1
77
1-171
08/0512019 1440
Isophorone
20
16
1
78
21-196
08/05/2019 1440
Naphthalene
20
13
1
67
21-133
08/05/2019 1440
Nitrobenzene
20
14
1
72
35-180
08105120191440
2-Nitrophenol
20
15
1
73
29-182
06/05120191440
LOO= Limit of Ouantitation P= The RPO between two GC columns exceeds 40% N= Recovery is out of cnteris
DL=Detection Limn J= Estimated result -LOD and OL = RPDis out of cdteda
LOD = Limit of Detadtdn ND = Not detected at or stove the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services. Inc. QC Data for Lot Number: UG24099
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 y rs,,shealylab.com
Page 20 of 30
d
Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: U024616-002
Matrix:
Aqueous
Batch:24616
Prep Method:
625.1
Analytical Method: 625.1
Prep Date:
08/0212019 1705
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) 0
Dil
% Rec
Limit
Analysis Date
4-Nitrophenol
40
39
1
97
1-132
08/05/2019
1440
N-Nitrosodlmethylamine
20
14
1
69
1-150
08105120191440
N-Nilrosodi-n-propylamine
20
19
1
94
1-230
08/05/2019
1440
N-Nitrosodiphenylamine (Diphenylamine)
20
15
1
73
1-150
OB/05/2019
1440
Pentachlorophenol
40
33
1
82
14-176
08105120191440
Phenanthrene
20
15
1
75
54-120
08105/2019
1440
Phenol
20
12
1
61
5-120
08/05/2019
1440
Pyrene
20
16
1
78
52-120
08/05/2019
1440
2,4,6-Trichlorophenol
20
15
1
75
37-144
08/05120191440
Acceptance
Surrogate
e
0 /, Rec
Limit
2-Fluorobiphenyl
68
37-129
2-Flucrophenol
33
24-127
Nitrobenzene-d5
72
38-127
Phenol-d5 62 28-128
Terphenyl-dl4 90 10-148
2,4,6-Tribromophenol 83 41-144
LOD = Limit of Ouanetaaon P = The RPD bet«een mo GC columns exceeds 40% N = Recovery is out of chteda
DL= Detection Limit J= Estimated result a L00 and> OIL = RPD is out of cmeda
LOD = Limit of De:ecbon NO = Not detected at or atc re the OL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc, OC Data for Lot Number: UG24099
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 wv.^x. shealylab, com
Page 21 of 30
Organochlorine Pesticides and PCBs - MB
Sample l D: U023870-001 Matrix: Aqueous
Batch:23870 Prep Method: 608.3 Cleanup: 3665A
Analytical Method: 608.3 Prep Date: 07/26/2019 1619
Parameter
Result O
Dil
LOO
DL
Units
Analysis Date
Aldrin
NO
1
0.040
0.015
ug/L
0713OY2019 1945
Aroclor 1016
NO
1
0.40
0.15
ug/L
07/30/2019 0000
h Aroclor 1221
NO
1
0.40
0.25
ug/L
07/30/2019 0000
- Aroclor 1232
NO
1
0.40
0.15
ug/L
07/30/2019 0000
Aroclor 1242
NO
1
0.40
0.15
ug/L
07/3012019 0000
Aroclor 1248
NO
1
0.40
0.15
ug/L
07/3012019 0000
Aroclor 1254
NO
1
0.40
0.15
ug/L
07/30/2019 0000
Arocor 1260
NO
1
0.40
0.15
ug/L
07/30/2019 0000
gamma-BHC (Lindane)
ND
1
0.040
0.017
ug/L
0713012019 1845
alpha-BHC
NO
1
0.040
0.015
ug/L
07130120191845
beta-BHC
NO
1
0.040
0.015
ug/L
07/30120191845
delta-BHC
NO
1
0.040
0.015
ug/L
07/30/2019 1845
Chlordane
NO
1
0.40
0.15
ug/L
07/30/2019 1845
4,4'-DDD
NO
1
0.040
0.015
ug/L
07/30120191845
4,4'-DOE
ND
1
0.040
0.015
ug/L
07/30/2019 1845
4,4'-DDT
NO
1
0.040
0.015
ug/L
07/30/2019 1845
Dieldrin
NO
1
0.040
0.015
ug/L
07/30/2019 1845
Endosulfan I
NO
1
0,040
0.015
ug/L
07/30/2019 1845
Endosulfan 11
NO
1
0,040
0.015
ug/L
07130/2019 1845
Endosulfan sulfate
NO
1
0.040
0.015
ug/L
07/30/2019 1845
Endrin
NO
1
0.040
0.015
ug/L
07/30120191845
Endrin aldehyde
NO
1
0.040
0.015
ug/L
07/30/2019 1845
Heptachlor
NO
1
0.040
0,015
ug/L
07130/20191845
Heptachlor epoxide
NO
1
0.040
0.016
ug/L
07/30/2019 1845
Toxaphene
NO
1
0.40
0.30
ug/L
07/30/20191845
Acceptance
Surrogate 0 %Rea Limit
Decachlorobiphenyl 51 20-131
Tetrachloro-m-xylene 68 30-132
LOD = Limit of Duantitason P = The RPD hatween Me CC columns exceed. 40% N = Recovery is out of orders
DL = Deitch. Limit J = Estimated result < LOD and > DL += RPD Is our of attend
LOD = Limit or Datecton NO = Not detected at or above me OL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. CC Data for Lot Number: UG24099
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vivov. sheelylab.tom
Page 22 of 30
Organochlorine Pesticides and PCBs - LCS
Sample ID: U023870-002
Matrix:
Aqueous
Batch:23870
Prep Method:
608.3
Cleanup:
3665A
Analytical Method: 608.3
Prep Date: 07126/2019 1619
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug1L) Q
Dil
% Rao
Limit
Analysis Date
Aldrin
0.80
0.62
1
78
42-140
07/30120191900
gamma-BHC (Lindane)
0,80
0.63
1
79
32-140
07/30/2019 1900
alpha-BHC
0.80
0.60
1
74
37-140
07/30/2019 1900
beta-BHC
0.80
0.60
1
75
17-147
07/30120191900
delta-BHC
0.80
0.62
1
78
19-140
07/30/2019 1900
4,4'1
0.80
0.69
1
86
31-141
07/30/2019 1900
4,4'1
0.80
0.68
1
85
30-145
07/30120191900
4,4'-DDT
0.80
0.64
1
79
25-160
07/30120191900
Dieldrin
0.80
0.72
1
90
36-146
07/30/2019 1900
Endosulfan 1
0.80
0.59
1
74
45-153
07/30/2019 1900
Endosulfan II
0.80
0.58
1
72
1-202
07/30/2019 1900
Endosulfan sulfate
0.80
0.62
1
77
26-144
07/30/2019 1900
Endrin
0.80
0.63
1
79
30-147
07/30120191900
Endrin aldehyde
0.80
0.54
1
67
60-140
07/3012019 1900
Heptachlor
0.80
0.61
1
76
34-140
07/30120191900
Heptachlor epoxlde
0.80
0.68
1
85
37-142
07/30/2019 1900
Acceptance
Surrogate
Q % Rao
Limit
Decachlorobiphenyl 43 20-131
Tetrachloro-m-xylene 67 30-132
LOG- Limit of Ouantitation P= The RPO between two GG columns exceeds 40% N= Recovery is out of crema
OIL =Detei Limit J= Estinated result LOD and g OIL •= RPD Is out of cnteda
LOD - Limit of DelecLon ND = Not de acte l at or above are DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number UG24099
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 w .sheeylab,wnn
Page 23 of 30
ICP-MS - MB
Sample ID: UQ23674-001 Matrix: Aqueous
Batch: 23674 Prep Method: 200.2
Analytical Method: 200.8 Prep Date: 07/2512019 1009
Parameter Result O DII LOO DL Units Analysis Date
Copper NO 1 5.0 1.3 uglL 07125120191625
Lead NO 1 1.0 0.25 uglL 07/25120191625
LOD= Limit of Ouanlilalion P - The RPO between W. GC columns oxcands 40% N= Recovery is out of criteria
DL= Detection Limit J= Estimated result< LOD end >DL += RPD is out of omens
LOD - Limit of Detection NO = Not hothead at or above Me DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.. OC Data for Lot Number: UG24099
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 ..sheelylab.com
Page 24 of 30
ICP-MS - LCS
Sample ID: UU23674-002
Matrix: Aqueous
Batch: 23674
Prep Method: 200.2
Analytical Method: 200.8
Prep Date: 07/25/2019 1009
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug1L)
C) oil % Rec
Limit Analysis Date
Copper
100
97
1 97
85-115 07/25/2019 1631
Lead
100
100
1 104
85-115 07/25/2019 1631
LOD= Umit of Ouantmmon P- The RPD beNveen two 00 columns..coeds 40% N= Recovery, is out of criers
OL = Detection Limit J . Eetunated result < LOD and . OL = RPD is out of wums
LOD = Limit M Detecton NO - Not detected at or above 0e DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. GIC Data for Lot Number: UG24099
106 Ventage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealyla5com
Page 25 of 30
ICP-MS - MB
Sample l D: UQ23922-001 Matrix: Aqueous
Batch: 23922 Prep Method: 200.2
Analytical Method: 200.8 Prep Date: 07127/2019 1048
Parameter Result Q Dil LOO DL Units Analysis Date
Zinc 3.7 J 1 10 2.6 ug1L 07129/2019 1100
LOD = Limit of Quentitation P = The RPD between two GC columns exceeds 40% N = Recovery is oW of chains
DL = Detwt.n Limit J = Estimated result x LOD and> OL > = RPD is out of Wei
LOD = Limit of Detection ND = Not detected at or above No DL
Note: Calculations are performed before rounding to avoid round -off errors In calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UG24099
106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 wvi v.shealylab,cam
Page 26 of 30
ICP-MS - LCS
Sample ID: UQ23922-002
Matrix: Aqueous
Batch:23922
Prep Method: 200.2
Analytical Method: 200.8
Prep Date: 07/27/2019 1048
Spike
Amount
Result
% Rae
Parameter
(uglL)
(uglL)
Q Dll % Rec Limit Analysis Date
Zinc
100
110
1 114 85-115 07129120191106
LOO= Limit of Quarelation P= The RPD between two GC columns exceeds 40% N= R000very is out of chains,
DL=Detection Limit J=EsUmatelresult -LOO and !DL *= RPDis out of cdlena
LOD - Urril of Dateceon ND = Not detected at or above the OL
Note: Calculations are performed before rounding to avoid rouri errors in calculated results
Shealy Environmental Services, Inc. GIC Data for Lot Number: UG24099
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vnvw.Shea[ylab.wm
a
Page 27 of 30
0
Chain of Custody
and
Miscellaneous Documents
Sbeely Environmental Services, Inc.
i
10S Ventage Point Odve West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 w .sbeelylab.wnn
Page 28 of 30
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SHEALY ENVIRONMENTAL SERVICES, INC.
105 Voll1aC19 Port Dnw - West Calumba SC 29172
SHEALY Chain of Custody Record Telephwe NU. 803 7'Jl-9700 Fax No. M3 1
%NI-1111 wv;viA)oalylib.wm
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SHEALY ENVIRONMENTAL SERVICES, INC.
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Sample Receipt Checklist (SRC)
ci,cnn Shield Enaiaccrinn Coalcr In:,reemJ bh+ddc:'•?\',n 07r24114 I nt W: U624099
Means of rccclpr: SbSl ❑.Clicut .❑ IMPS ❑ 1rcdEa Weir.
1'JSrm VD
I, Picrci'u}I.AIt'ic4l5.rcwul or. Ihcc.colce,
_s: If cu>IJJy sceli were .rxal. wcm acy iuldct and unbml cn'
pH Strip ID; 19-10331 ChlorinejlripTD; NA I zstcd bit I )M N
Orin: final mmperdure upon rxeipl : 7)criru{ {C.nTns:rrdl fr:np!:mtnrr. apnn rtr.,:ipt %L ,o(id Saa.j Cuj LLy: KA
2.i r=? -U NA ;NA =C' NA NA :L NA ;NA "C
A1e11tuJ. ®7empec'a!urr Bled. ❑Avuiusr Bu!Ilcs IR Guu ID: ' TR Gun Currccti::n Fwanr: J 'C
Me lh Lid DIC0111Ant: 2 Net lee ❑ Ten P.,A ❑ TWTr.- ❑ K,nr.
❑Y"GS
No
®NA
i. I:' tetnperalure of any cnolcr eaueedcJ 6.f,•�Cm , MIS PMI'ml Mimaj.r\mired?
PIt1 w;u Veliliedkv: pheur: ernuilr lua-In-Puce icin'.Ic ond),
=. 1, the comnmmiul a,uner's pricking slip .utac:•sd to this form:
❑ Yes
❑ Nol
0 NA
Yea
0 Nuj
15. Wm.. prop:.r ecsrodv ptoce(lures(:elir.,Tulshrdoie r.rd) lulluvcd?
0 yni
U No
I , Wom. vmnp.c II )5 listed on ilia COC"
0 Yc.
❑ Nu
17.. Wnm 5amplr. His listed on alsnrlp6: cunra, ,.ers'
0 Yes
❑ Nu
S, Wm enllcrcna dat:. H lune listed on the. Cbi_'
,0 Yes,
❑ No
0. Was collcct on dare & tune listed oo ;ill mnpl-corrair:e:.c'?
E5 V(1
K Did Al conax.cr label information (11), dale, '.ime) aS'ree wish ILe
0 yes
ClNN.,I1.
Were tests to be p2rformcC ILitOd otl die COC? �i ( c : t' r1'-rt :
®Y
--
❑ No
—
11. Did All sanglks An hr. in llte propel' eon:ai:e_en s fill lest aul•U iof i:, UJ L lUdlUJlt
Rmhrnkan, lids on, M^,)"
0 Y,-s
❑ No
113. Wus udeyualu mmnlc v:::umc avuilabl
Y �
❑ No
I14, R`e:c uil3amplcs rccat:c wrC'llll !; tho adldine one er d8 haul, whichete: enntes lira!
LJ y!5
® No
115, Wc�: anv'slmplcs rnnclircn mi3SulWcxucSb (mrdc one) 3ampics Vat li (cc or. C(N:'
❑ Ys
❑ No
0 NA
16. pot VOA and RSK-I?S �,,mple>, were bui%+lcs prcacrt e"pre. aivr" (!• 'or lmin in dmm_ .zrr,
iu uuy oftl,c VOA
Z Yes
11 No
LJ NA
11-CW-ma111 )k O;mcrais+rlc:rl..t sa:epics recei,ed td e. pli -if 2^
❑ yes
❑ :No
0 NA
I8. LV'cre a ] evHurCC samples recei':ed ale .l[ :• I: and sdlidc ,ample, rc::civcd al a H ? V^
❑ Yes
❑ No
0 NA
19. Weir nl applin7, N1�/fKN:cyaN, Cphenu1G2]0,5wg'L) vur pled U<r of lesidml
elder llle.'
❑ Yes
❑ No
0 N?,
20. Were client retnzrks:'regcecce (i.e. reyueslre dilution.,. W;*10SO de,iymatinnx, ctr....l
coueclly'-lanauibrJ Gum the COC into the;Or,mU,n ycdion in I.11151
Ycs
Na
'i. Wu, tt,c w:,b number lislalon:h:•cennir.:r labcj7 l['-cs, Vueto` NA
Sample I'rcservndon ;Must L`e rmupleled Fur troy >nnple(s) inarrrclly pre<a': eJ or with hcelJspts,)
SAmplc(rt l 1, A_ q'ClU 1'CCZIVeC, nliUrlCe'3\' plCSel teJ W IJ `n C[ C al'tU?lCd 'CCC.:TdlnQly
is sunplo,ecclviq%,Ith NA .nLo£cuce oue. 10SCfa, 11NO3.[ICI. l,u011 using SR;: NA
I isle of preser:anon K.4 if mere r31at1 orx {+T6se:vatire is needal Pleu,c nntc in the coon.. hclnw'.
3nmp(W,) UL :vcrc 2,:citcd With buhhhs : 6 rml :n dizmelc:.
SnmClcs(s) NA v.ere lecei oed ,e iJ: TRC ? l!.S :una. (IC W I9 ;.I..) :V mLl warn
adjusted axcadm6ty iu s:mlp;e ieueilirg I ith. w,dium I will,, 8hu:)y 11): NA
SR barcodc IabcU applied bv: TA NiJiIT pa:-: 07r'4.'I •)
Commence: [Ci(Y!-�'- -�eliPr'•liin CIA . }nINN SZyyy1�Ily 19C:-141e
Shealy Environmental Services, Inc.
106 Vantage Point Dnve West Columbia. SC 29172 (803)791-9700 Fax(803)791-9111 www.shealylab,com
Page 30 of 30